ANALYTICAL REPORT 6 - Asarco · ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Corpus...
Transcript of ANALYTICAL REPORT 6 - Asarco · ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Corpus...
ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Corpus Christi1733 N. Padre Island DriveCorpus Christi, TX 78408Tel: (361)289-2673
TestAmerica Job ID: 560-31034-1TestAmerica Sample Delivery Group: March 1, 2012Client Project/Site: Former ASARCO Groundwater
For:Malcolm Pirnie, Inc. Invoice to Arcadis211 North Florence StreetSuite 202El Paso, Texas 79901
Attn: Ms. Marla Miller
Authorized for release by:3/18/2012 4:29:08 PM
Timothy KelloggCustomer Service [email protected]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accreditedparameters, exceptions are noted in this report. This report may not be reproduced except in full,and with written approval from the laboratory. For questions please contact the Project Managerat the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Definitions/GlossaryTestAmerica Job ID: 560-31034-1Client: Malcolm Pirnie, Inc. Invoice to Arcadis
SDG: March 1, 2012Project/Site: Former ASARCO Groundwater
Qualifiers
Metals
Qualifier Description
U Analyte was not detected at or above the SDL.
Qualifier
J Result is less than the MQL but greater than or equal to the SDL and the concentration is an estimated value.
General Chemistry
Qualifier Description
U Analyte was not detected at or above the SDL.
Qualifier
J Result is less than the MQL but greater than or equal to the SDL and the concentration is an estimated value.
Glossary
These commonly used abbreviations may or may not be present in this report.
☼ Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CNF Contains no Free Liquid
DL, RA, RE, IN Indicates a Dilution, Reanalysis, Re-extraction, or additional Initial metals/anion analysis of the sample
EDL Estimated Detection Limit
EPA United States Environmental Protection Agency
MDL Method Detection Limit
ML Minimum Level (Dioxin)
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RL Reporting Limit
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample ResultsTestAmerica Job ID: 560-31034-1Client: Malcolm Pirnie, Inc. Invoice to Arcadis
SDG: March 1, 2012Project/Site: Former ASARCO Groundwater
Lab Sample ID: 560-31034-1Client Sample ID: EP-85Matrix: WaterDate Collected: 03/01/12 08:00
Date Received: 03/02/12 10:25
Method: 6020 - Metals (ICP/MS)MQL MDL
Aluminum 0.0225 U 0.0500 0.0225 mg/L 03/07/12 09:30 03/07/12 19:36 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00500 0.00161 mg/L 03/07/12 09:30 03/07/12 19:36 1Antimony 0.0422
0.00500 0.00109 mg/L 03/07/12 09:30 03/08/12 19:15 1Arsenic 1.25
0.00500 0.000810 mg/L 03/07/12 09:30 03/07/12 19:36 1Barium 0.0352
0.00200 0.000854 mg/L 03/07/12 09:30 03/07/12 19:36 1Cadmium 0.00168 J
0.500 0.198 mg/L 03/07/12 09:30 03/07/12 19:36 1Calcium 98.9
0.00500 0.00140 mg/L 03/07/12 09:30 03/07/12 19:36 1Chromium 0.00239 J
0.00500 0.00136 mg/L 03/07/12 09:30 03/07/12 19:36 1Cobalt 0.00136 U
0.0100 0.00200 mg/L 03/07/12 09:30 03/07/12 19:36 1Copper 0.00200 U
0.250 0.101 mg/L 03/07/12 09:30 03/07/12 19:36 1Iron 0.101 U
0.00500 0.000733 mg/L 03/07/12 09:30 03/07/12 19:36 1Lead 0.000733 U
0.500 0.113 mg/L 03/07/12 09:30 03/08/12 19:15 1Magnesium 47.9
0.0500 0.0116 mg/L 03/07/12 09:30 03/07/12 19:36 1Manganese 0.0116 U
0.00500 0.00140 mg/L 03/07/12 09:30 03/07/12 19:36 1Molybdenum 0.572
0.00500 0.00217 mg/L 03/07/12 09:30 03/07/12 19:36 1Nickel 0.00217 U
1.00 0.407 mg/L 03/07/12 09:30 03/07/12 19:36 1Potassium 27.3
0.00500 0.00108 mg/L 03/07/12 09:30 03/07/12 19:36 1Selenium 0.132
1.00 0.727 mg/L 03/07/12 09:30 03/08/12 19:52 10Sodium 783
0.00100 0.000693 mg/L 03/07/12 09:30 03/08/12 19:15 1Thallium 0.00974
0.0250 0.00355 mg/L 03/07/12 09:30 03/07/12 19:36 1Zinc 0.00355 U
Method: 6020 - Metals (ICP/MS) - DissolvedMQL MDL
Antimony 0.0394 0.00500 0.00161 mg/L 03/08/12 09:30 03/08/12 23:31 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00500 0.00109 mg/L 03/08/12 09:30 03/08/12 23:31 1Arsenic 1.30
0.00500 0.000810 mg/L 03/08/12 09:30 03/08/12 23:31 1Barium 0.0315
0.00200 0.000854 mg/L 03/08/12 09:30 03/08/12 23:31 1Cadmium 0.000854 U
0.00500 0.00140 mg/L 03/08/12 09:30 03/08/12 23:31 1Chromium 0.00302 J
0.00500 0.00136 mg/L 03/08/12 09:30 03/08/12 23:31 1Cobalt 0.00136 U
0.0100 0.00200 mg/L 03/08/12 09:30 03/08/12 23:31 1Copper 0.00200 U
0.250 0.101 mg/L 03/08/12 09:30 03/08/12 23:31 1Iron 0.101 U
0.00500 0.000733 mg/L 03/08/12 09:30 03/08/12 23:31 1Lead 0.000733 U
0.00500 0.00140 mg/L 03/08/12 09:30 03/08/12 23:31 1Molybdenum 0.537
0.00500 0.00217 mg/L 03/08/12 09:30 03/08/12 23:31 1Nickel 0.00217 U
0.00500 0.00108 mg/L 03/08/12 09:30 03/08/12 23:31 1Selenium 0.130
0.00100 0.000693 mg/L 03/08/12 09:30 03/08/12 23:31 1Thallium 0.0100
0.0250 0.00355 mg/L 03/08/12 09:30 03/08/12 23:31 1Zinc 0.00355 U
Method: 7470A - Mercury (CVAA)MQL MDL
Mercury 0.000130 U 0.00200 0.000130 mg/L 03/07/12 12:30 03/07/12 18:14 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 7470A - Mercury (CVAA) - DissolvedMQL MDL
Mercury 0.000130 U 0.00200 0.000130 mg/L 03/07/12 12:30 03/07/12 18:16 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryMQL MDL
Total Dissolved Solids 2640 10.0 10.0 mg/L 03/05/12 10:45 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
3.00 3.00 mg/L 03/06/12 09:15 1Total Suspended Solids 3.00 U
1.00 0.192 mg/L 03/02/12 16:18 50Chloride 314
0.500 0.200 mg/L 03/02/12 12:59 4Nitrate Nitrite as N 9.37
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Client Sample ResultsTestAmerica Job ID: 560-31034-1Client: Malcolm Pirnie, Inc. Invoice to Arcadis
SDG: March 1, 2012Project/Site: Former ASARCO Groundwater
Lab Sample ID: 560-31034-1Client Sample ID: EP-85Matrix: WaterDate Collected: 03/01/12 08:00
Date Received: 03/02/12 10:25
General Chemistry (Continued)MQL MDL
Sulfate 632 1.00 0.377 mg/L 03/07/12 08:07 50
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.100 0.0200 mg/L 03/05/12 09:50 2Fluoride 3.30
0.0500 0.0131 mg/L 03/02/12 11:10 1Sulfide 0.0131 U
1.00 0.285 mg/L 03/07/12 12:15 1Total Organic Carbon 2.37
5.00 5.00 mg/L 03/05/12 12:55 1Total Alkalinity as CaCO3 396
Lab Sample ID: 560-31034-2Client Sample ID: EP-81Matrix: WaterDate Collected: 03/01/12 09:15
Date Received: 03/02/12 10:25
Method: 6020 - Metals (ICP/MS)MQL MDL
Aluminum 0.0317 J 0.0500 0.0225 mg/L 03/07/12 09:30 03/07/12 19:41 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00500 0.00161 mg/L 03/07/12 09:30 03/07/12 19:41 1Antimony 0.00342 J
0.00500 0.00109 mg/L 03/07/12 09:30 03/08/12 19:20 1Arsenic 0.749
0.00500 0.000810 mg/L 03/07/12 09:30 03/07/12 19:41 1Barium 0.0442
0.00200 0.000854 mg/L 03/07/12 09:30 03/07/12 19:41 1Cadmium 0.00116 J
0.500 0.198 mg/L 03/07/12 09:30 03/07/12 19:41 1Calcium 131
0.00500 0.00140 mg/L 03/07/12 09:30 03/07/12 19:41 1Chromium 0.00140 U
0.00500 0.00136 mg/L 03/07/12 09:30 03/07/12 19:41 1Cobalt 0.00136 U
0.0100 0.00200 mg/L 03/07/12 09:30 03/07/12 19:41 1Copper 0.00466 J
0.250 0.101 mg/L 03/07/12 09:30 03/07/12 19:41 1Iron 0.101 U
0.00500 0.000733 mg/L 03/07/12 09:30 03/07/12 19:41 1Lead 0.000733 U
0.500 0.113 mg/L 03/07/12 09:30 03/08/12 19:20 1Magnesium 51.0
0.0500 0.0116 mg/L 03/07/12 09:30 03/07/12 19:41 1Manganese 0.0116 U
0.00500 0.00140 mg/L 03/07/12 09:30 03/07/12 19:41 1Molybdenum 0.320
0.00500 0.00217 mg/L 03/07/12 09:30 03/07/12 19:41 1Nickel 0.00217 U
1.00 0.407 mg/L 03/07/12 09:30 03/07/12 19:41 1Potassium 30.1
0.00500 0.00108 mg/L 03/07/12 09:30 03/07/12 19:41 1Selenium 0.131
1.00 0.727 mg/L 03/07/12 09:30 03/07/12 19:41 1Sodium 293
0.00100 0.000693 mg/L 03/07/12 09:30 03/08/12 19:20 1Thallium 0.000752 J
0.0250 0.00355 mg/L 03/07/12 09:30 03/07/12 19:41 1Zinc 0.00831 J
Method: 6020 - Metals (ICP/MS) - DissolvedMQL MDL
Antimony 0.00335 J 0.00500 0.00161 mg/L 03/08/12 09:30 03/09/12 00:13 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00500 0.00109 mg/L 03/08/12 09:30 03/09/12 00:13 1Arsenic 0.743
0.00500 0.000810 mg/L 03/08/12 09:30 03/09/12 00:13 1Barium 0.0400
0.00200 0.000854 mg/L 03/08/12 09:30 03/09/12 00:13 1Cadmium 0.000854 U
0.00500 0.00140 mg/L 03/08/12 09:30 03/09/12 00:13 1Chromium 0.00140 U
0.00500 0.00136 mg/L 03/08/12 09:30 03/09/12 00:13 1Cobalt 0.00136 U
0.0100 0.00200 mg/L 03/08/12 09:30 03/09/12 00:13 1Copper 0.00391 J
0.250 0.101 mg/L 03/08/12 09:30 03/09/12 00:13 1Iron 0.101 U
0.00500 0.000733 mg/L 03/08/12 09:30 03/09/12 00:13 1Lead 0.000733 U
0.00500 0.00140 mg/L 03/08/12 09:30 03/09/12 00:13 1Molybdenum 0.295
0.00500 0.00217 mg/L 03/08/12 09:30 03/09/12 00:13 1Nickel 0.00217 U
0.00500 0.00108 mg/L 03/08/12 09:30 03/09/12 00:13 1Selenium 0.127
0.00100 0.000693 mg/L 03/08/12 09:30 03/09/12 00:13 1Thallium 0.000937 J
0.0250 0.00355 mg/L 03/08/12 09:30 03/09/12 00:13 1Zinc 0.00847 J
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Client Sample ResultsTestAmerica Job ID: 560-31034-1Client: Malcolm Pirnie, Inc. Invoice to Arcadis
SDG: March 1, 2012Project/Site: Former ASARCO Groundwater
Lab Sample ID: 560-31034-2Client Sample ID: EP-81Matrix: WaterDate Collected: 03/01/12 09:15
Date Received: 03/02/12 10:25
Method: 7470A - Mercury (CVAA)MQL MDL
Mercury 0.000130 U 0.00200 0.000130 mg/L 03/07/12 12:30 03/07/12 18:18 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 7470A - Mercury (CVAA) - DissolvedMQL MDL
Mercury 0.000130 U 0.00200 0.000130 mg/L 03/07/12 12:30 03/07/12 18:20 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryMQL MDL
Total Dissolved Solids 1740 10.0 10.0 mg/L 03/05/12 10:45 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
3.00 3.00 mg/L 03/06/12 09:15 1Total Suspended Solids 3.00 U
1.00 0.192 mg/L 03/02/12 14:05 4Chloride 159
0.500 0.200 mg/L 03/02/12 14:05 4Nitrate Nitrite as N 4.92
1.00 0.377 mg/L 03/07/12 08:29 25Sulfate 678
0.100 0.0200 mg/L 03/05/12 09:50 2Fluoride 3.22
0.0500 0.0131 mg/L 03/02/12 11:10 1Sulfide 0.0200 J
1.00 0.285 mg/L 03/07/12 12:15 1Total Organic Carbon 1.33
5.00 5.00 mg/L 03/05/12 12:55 1Total Alkalinity as CaCO3 313
Lab Sample ID: 560-31034-3Client Sample ID: OBS-1Matrix: WaterDate Collected: 03/01/12 10:15
Date Received: 03/02/12 10:25
Method: 6020 - Metals (ICP/MS)MQL MDL
Aluminum 0.0225 U 0.0500 0.0225 mg/L 03/07/12 09:30 03/07/12 19:47 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00500 0.00161 mg/L 03/07/12 09:30 03/07/12 19:47 1Antimony 0.0435
0.00500 0.00109 mg/L 03/07/12 09:30 03/08/12 19:26 1Arsenic 1.78
0.00500 0.000810 mg/L 03/07/12 09:30 03/07/12 19:47 1Barium 0.0268
0.00200 0.000854 mg/L 03/07/12 09:30 03/07/12 19:47 1Cadmium 0.00209
0.500 0.198 mg/L 03/07/12 09:30 03/07/12 19:47 1Calcium 149
0.00500 0.00140 mg/L 03/07/12 09:30 03/07/12 19:47 1Chromium 0.00140 U
0.00500 0.00136 mg/L 03/07/12 09:30 03/07/12 19:47 1Cobalt 0.00136 U
0.0100 0.00200 mg/L 03/07/12 09:30 03/07/12 19:47 1Copper 0.00200 U
0.250 0.101 mg/L 03/07/12 09:30 03/07/12 19:47 1Iron 0.101 U
0.00500 0.000733 mg/L 03/07/12 09:30 03/07/12 19:47 1Lead 0.000733 U
0.500 0.113 mg/L 03/07/12 09:30 03/08/12 19:26 1Magnesium 68.7
0.0500 0.0116 mg/L 03/07/12 09:30 03/07/12 19:47 1Manganese 0.0116 U
0.00500 0.00140 mg/L 03/07/12 09:30 03/07/12 19:47 1Molybdenum 0.449
0.00500 0.00217 mg/L 03/07/12 09:30 03/07/12 19:47 1Nickel 0.00462 J
1.00 0.407 mg/L 03/07/12 09:30 03/07/12 19:47 1Potassium 54.8
0.00500 0.00108 mg/L 03/07/12 09:30 03/07/12 19:47 1Selenium 0.222
1.00 0.727 mg/L 03/07/12 09:30 03/08/12 20:24 10Sodium 844
0.00100 0.000693 mg/L 03/07/12 09:30 03/08/12 19:26 1Thallium 0.0163
0.0250 0.00355 mg/L 03/07/12 09:30 03/07/12 19:47 1Zinc 0.0392
Method: 6020 - Metals (ICP/MS) - DissolvedMQL MDL
Antimony 0.0388 0.00500 0.00161 mg/L 03/08/12 09:30 03/09/12 00:19 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00500 0.00109 mg/L 03/08/12 09:30 03/09/12 00:19 1Arsenic 1.77
0.00500 0.000810 mg/L 03/08/12 09:30 03/09/12 00:19 1Barium 0.0245
0.00200 0.000854 mg/L 03/08/12 09:30 03/09/12 00:19 1Cadmium 0.00122 J
0.00500 0.00140 mg/L 03/08/12 09:30 03/09/12 00:19 1Chromium 0.00140 U
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Client Sample ResultsTestAmerica Job ID: 560-31034-1Client: Malcolm Pirnie, Inc. Invoice to Arcadis
SDG: March 1, 2012Project/Site: Former ASARCO Groundwater
Lab Sample ID: 560-31034-3Client Sample ID: OBS-1Matrix: WaterDate Collected: 03/01/12 10:15
Date Received: 03/02/12 10:25
Method: 6020 - Metals (ICP/MS) - Dissolved (Continued)MQL MDL
Cobalt 0.00136 U 0.00500 0.00136 mg/L 03/08/12 09:30 03/09/12 00:19 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0100 0.00200 mg/L 03/08/12 09:30 03/09/12 00:19 1Copper 0.00200 U
0.250 0.101 mg/L 03/08/12 09:30 03/09/12 00:19 1Iron 0.101 U
0.00500 0.000733 mg/L 03/08/12 09:30 03/09/12 00:19 1Lead 0.000733 U
0.00500 0.00140 mg/L 03/08/12 09:30 03/09/12 00:19 1Molybdenum 0.420
0.00500 0.00217 mg/L 03/08/12 09:30 03/09/12 00:19 1Nickel 0.00388 J
0.00500 0.00108 mg/L 03/08/12 09:30 03/09/12 00:19 1Selenium 0.205
0.00100 0.000693 mg/L 03/08/12 09:30 03/09/12 00:19 1Thallium 0.0167
0.0250 0.00355 mg/L 03/08/12 09:30 03/09/12 00:19 1Zinc 0.0357
Method: 7470A - Mercury (CVAA)MQL MDL
Mercury 0.000130 U 0.00200 0.000130 mg/L 03/07/12 12:30 03/07/12 18:23 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 7470A - Mercury (CVAA) - DissolvedMQL MDL
Mercury 0.000130 U 0.00200 0.000130 mg/L 03/07/12 12:30 03/07/12 18:25 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryMQL MDL
Total Dissolved Solids 3050 10.0 10.0 mg/L 03/05/12 10:45 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
3.00 3.00 mg/L 03/06/12 09:15 1Total Suspended Solids 3.00 U
1.00 0.192 mg/L 03/02/12 17:02 50Chloride 373
0.500 0.200 mg/L 03/02/12 14:27 4Nitrate Nitrite as N 10.2
1.00 0.377 mg/L 03/07/12 09:35 50Sulfate 1310
0.100 0.0200 mg/L 03/05/12 09:50 2Fluoride 2.90
0.0500 0.0131 mg/L 03/02/12 11:10 1Sulfide 0.0260 J
1.00 0.285 mg/L 03/07/12 12:15 1Total Organic Carbon 2.69
5.00 5.00 mg/L 03/05/12 12:55 1Total Alkalinity as CaCO3 416
Lab Sample ID: 560-31034-4Client Sample ID: FD030212Matrix: WaterDate Collected: 03/01/12 00:00
Date Received: 03/02/12 10:25
Method: 6020 - Metals (ICP/MS)MQL MDL
Aluminum 0.0225 U 0.0500 0.0225 mg/L 03/07/12 09:30 03/07/12 20:14 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00500 0.00161 mg/L 03/07/12 09:30 03/07/12 20:14 1Antimony 0.0452
0.00500 0.00109 mg/L 03/07/12 09:30 03/07/12 20:14 1Arsenic 1.41
0.00500 0.000810 mg/L 03/07/12 09:30 03/07/12 20:14 1Barium 0.0370
0.00200 0.000854 mg/L 03/07/12 09:30 03/07/12 20:14 1Cadmium 0.00178 J
0.500 0.198 mg/L 03/07/12 09:30 03/07/12 20:14 1Calcium 104
0.00500 0.00140 mg/L 03/07/12 09:30 03/07/12 20:14 1Chromium 0.00248 J
0.00500 0.00136 mg/L 03/07/12 09:30 03/07/12 20:14 1Cobalt 0.00136 U
0.0100 0.00200 mg/L 03/07/12 09:30 03/07/12 20:14 1Copper 0.00200 U
0.250 0.101 mg/L 03/07/12 09:30 03/07/12 20:14 1Iron 0.274
0.00500 0.000733 mg/L 03/07/12 09:30 03/07/12 20:14 1Lead 0.000733 U
0.500 0.113 mg/L 03/07/12 09:30 03/08/12 19:31 1Magnesium 50.3
0.0500 0.0116 mg/L 03/07/12 09:30 03/07/12 20:14 1Manganese 0.0116 U
0.00500 0.00140 mg/L 03/07/12 09:30 03/07/12 20:14 1Molybdenum 0.620
0.00500 0.00217 mg/L 03/07/12 09:30 03/07/12 20:14 1Nickel 0.00217 U
1.00 0.407 mg/L 03/07/12 09:30 03/07/12 20:14 1Potassium 28.3
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Client Sample ResultsTestAmerica Job ID: 560-31034-1Client: Malcolm Pirnie, Inc. Invoice to Arcadis
SDG: March 1, 2012Project/Site: Former ASARCO Groundwater
Lab Sample ID: 560-31034-4Client Sample ID: FD030212Matrix: WaterDate Collected: 03/01/12 00:00
Date Received: 03/02/12 10:25
Method: 6020 - Metals (ICP/MS) (Continued)MQL MDL
Selenium 0.135 0.00500 0.00108 mg/L 03/07/12 09:30 03/07/12 20:14 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.00 0.727 mg/L 03/07/12 09:30 03/08/12 20:29 10Sodium 789
0.00100 0.000693 mg/L 03/07/12 09:30 03/07/12 20:14 1Thallium 0.00966
0.0250 0.00355 mg/L 03/07/12 09:30 03/07/12 20:14 1Zinc 0.00544 J
Method: 6020 - Metals (ICP/MS) - DissolvedMQL MDL
Antimony 0.0408 0.00500 0.00161 mg/L 03/08/12 09:30 03/09/12 00:24 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00500 0.00109 mg/L 03/08/12 09:30 03/09/12 00:24 1Arsenic 1.29
0.00500 0.000810 mg/L 03/08/12 09:30 03/09/12 00:24 1Barium 0.0332
0.00200 0.000854 mg/L 03/08/12 09:30 03/09/12 00:24 1Cadmium 0.000854 U
0.00500 0.00140 mg/L 03/08/12 09:30 03/09/12 00:24 1Chromium 0.00226 J
0.00500 0.00136 mg/L 03/08/12 09:30 03/09/12 00:24 1Cobalt 0.00136 U
0.0100 0.00200 mg/L 03/08/12 09:30 03/09/12 00:24 1Copper 0.00200 U
0.250 0.101 mg/L 03/08/12 09:30 03/09/12 00:24 1Iron 0.101 U
0.00500 0.000733 mg/L 03/08/12 09:30 03/09/12 00:24 1Lead 0.000733 U
0.00500 0.00140 mg/L 03/08/12 09:30 03/09/12 00:24 1Molybdenum 0.559
0.00500 0.00217 mg/L 03/08/12 09:30 03/09/12 00:24 1Nickel 0.00217 U
0.00500 0.00108 mg/L 03/08/12 09:30 03/09/12 00:24 1Selenium 0.130
0.00100 0.000693 mg/L 03/08/12 09:30 03/09/12 00:24 1Thallium 0.0100
0.0250 0.00355 mg/L 03/08/12 09:30 03/09/12 00:24 1Zinc 0.00355 U
Method: 7470A - Mercury (CVAA)MQL MDL
Mercury 0.000130 U 0.00200 0.000130 mg/L 03/07/12 12:30 03/07/12 18:27 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 7470A - Mercury (CVAA) - DissolvedMQL MDL
Mercury 0.000130 U 0.00200 0.000130 mg/L 03/07/12 12:30 03/07/12 18:36 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryMQL MDL
Total Dissolved Solids 2660 10.0 10.0 mg/L 03/05/12 10:45 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
3.00 3.00 mg/L 03/06/12 09:15 1Total Suspended Solids 3.00 U
1.00 0.192 mg/L 03/02/12 18:08 50Chloride 310
0.500 0.200 mg/L 03/02/12 14:49 4Nitrate Nitrite as N 8.88
1.00 0.377 mg/L 03/07/12 09:57 50Sulfate 1080
0.100 0.0200 mg/L 03/05/12 09:50 2Fluoride 3.02
0.0500 0.0131 mg/L 03/02/12 11:10 1Sulfide 0.0180 J
1.00 0.285 mg/L 03/07/12 12:15 1Total Organic Carbon 2.22
5.00 5.00 mg/L 03/05/12 12:55 1Total Alkalinity as CaCO3 394
Lab Sample ID: 560-31034-5Client Sample ID: EP-114Matrix: WaterDate Collected: 03/01/12 11:05
Date Received: 03/02/12 10:25
Method: 6020 - Metals (ICP/MS)MQL MDL
Aluminum 0.0376 J 0.0500 0.0225 mg/L 03/07/12 09:30 03/07/12 20:20 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00500 0.00161 mg/L 03/07/12 09:30 03/07/12 20:20 1Antimony 0.00700
0.00500 0.00109 mg/L 03/07/12 09:30 03/07/12 20:20 1Arsenic 50.5
0.00500 0.000810 mg/L 03/07/12 09:30 03/07/12 20:20 1Barium 0.0231
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Client Sample ResultsTestAmerica Job ID: 560-31034-1Client: Malcolm Pirnie, Inc. Invoice to Arcadis
SDG: March 1, 2012Project/Site: Former ASARCO Groundwater
Lab Sample ID: 560-31034-5Client Sample ID: EP-114Matrix: WaterDate Collected: 03/01/12 11:05
Date Received: 03/02/12 10:25
Method: 6020 - Metals (ICP/MS) (Continued)MQL MDL
Cadmium 0.0443 0.00200 0.000854 mg/L 03/07/12 09:30 03/07/12 20:20 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.500 0.198 mg/L 03/07/12 09:30 03/07/12 20:20 1Calcium 560
0.00500 0.00140 mg/L 03/07/12 09:30 03/07/12 20:20 1Chromium 0.00140 U
0.00500 0.00136 mg/L 03/07/12 09:30 03/07/12 20:20 1Cobalt 0.0541
0.0100 0.00200 mg/L 03/07/12 09:30 03/07/12 20:20 1Copper 0.00867 J
0.250 0.101 mg/L 03/07/12 09:30 03/07/12 20:20 1Iron 13.6
0.00500 0.000733 mg/L 03/07/12 09:30 03/07/12 20:20 1Lead 0.00208 J
0.500 0.113 mg/L 03/07/12 09:30 03/08/12 19:36 1Magnesium 216
0.0500 0.0116 mg/L 03/07/12 09:30 03/07/12 20:20 1Manganese 6.34
0.00500 0.00140 mg/L 03/07/12 09:30 03/07/12 20:20 1Molybdenum 0.412
0.00500 0.00217 mg/L 03/07/12 09:30 03/07/12 20:20 1Nickel 0.178
1.00 0.407 mg/L 03/07/12 09:30 03/07/12 20:20 1Potassium 185
0.00500 0.00108 mg/L 03/07/12 09:30 03/07/12 20:20 1Selenium 0.0203
1.00 0.727 mg/L 03/07/12 09:30 03/08/12 20:35 10Sodium 774
0.00100 0.000693 mg/L 03/07/12 09:30 03/07/12 20:20 1Thallium 0.00301
0.0250 0.00355 mg/L 03/07/12 09:30 03/07/12 20:20 1Zinc 8.04
Method: 6020 - Metals (ICP/MS) - DissolvedMQL MDL
Antimony 0.00725 0.00500 0.00161 mg/L 03/08/12 09:30 03/09/12 00:29 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00500 0.00109 mg/L 03/08/12 09:30 03/09/12 00:29 1Arsenic 45.2
0.00500 0.000810 mg/L 03/08/12 09:30 03/09/12 00:29 1Barium 0.0207
0.00200 0.000854 mg/L 03/08/12 09:30 03/09/12 00:29 1Cadmium 0.0427
0.00500 0.00140 mg/L 03/08/12 09:30 03/09/12 00:29 1Chromium 0.00140 U
0.00500 0.00136 mg/L 03/08/12 09:30 03/09/12 00:29 1Cobalt 0.0513
0.0100 0.00200 mg/L 03/08/12 09:30 03/09/12 00:29 1Copper 0.00200 U
0.250 0.101 mg/L 03/08/12 09:30 03/09/12 00:29 1Iron 12.9
0.00500 0.000733 mg/L 03/08/12 09:30 03/09/12 00:29 1Lead 0.000733 U
0.00500 0.00140 mg/L 03/08/12 09:30 03/09/12 00:29 1Molybdenum 0.390
0.00500 0.00217 mg/L 03/08/12 09:30 03/09/12 00:29 1Nickel 0.179
0.00500 0.00108 mg/L 03/08/12 09:30 03/09/12 00:29 1Selenium 0.0187
0.00100 0.000693 mg/L 03/08/12 09:30 03/09/12 00:29 1Thallium 0.00319
0.0250 0.00355 mg/L 03/08/12 09:30 03/09/12 00:29 1Zinc 7.92
Method: 7470A - Mercury (CVAA)MQL MDL
Mercury 0.000189 J 0.00200 0.000130 mg/L 03/07/12 12:30 03/07/12 18:38 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 7470A - Mercury (CVAA) - DissolvedMQL MDL
Mercury 0.000206 J 0.00200 0.000130 mg/L 03/07/12 12:30 03/07/12 18:40 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryMQL MDL
Total Dissolved Solids 5520 10.0 10.0 mg/L 03/05/12 10:45 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
3.00 3.00 mg/L 03/06/12 09:15 1Total Suspended Solids 30.0
1.00 0.192 mg/L 03/02/12 19:14 100Chloride 347
0.500 0.200 mg/L 03/02/12 15:11 4Nitrate Nitrite as N 0.800 U
1.00 0.377 mg/L 03/07/12 10:21 100Sulfate 2820
0.100 0.0200 mg/L 03/05/12 09:50 10Fluoride 7.42
0.0500 0.0131 mg/L 03/02/12 11:10 1Sulfide 0.0190 J
1.00 0.285 mg/L 03/07/12 12:15 1Total Organic Carbon 12.4
TestAmerica Corpus ChristiPage 12 of 30 3/18/2012
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Client Sample ResultsTestAmerica Job ID: 560-31034-1Client: Malcolm Pirnie, Inc. Invoice to Arcadis
SDG: March 1, 2012Project/Site: Former ASARCO Groundwater
Lab Sample ID: 560-31034-5Client Sample ID: EP-114Matrix: WaterDate Collected: 03/01/12 11:05
Date Received: 03/02/12 10:25
General Chemistry (Continued)MQL MDL
Total Alkalinity as CaCO3 614 5.00 5.00 mg/L 03/05/12 12:55 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Lab Sample ID: 560-31034-6Client Sample ID: EP-116Matrix: WaterDate Collected: 03/01/12 14:20
Date Received: 03/02/12 10:25
Method: 6020 - Metals (ICP/MS)MQL MDL
Aluminum 0.532 0.0500 0.0225 mg/L 03/07/12 09:30 03/07/12 20:25 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00500 0.00161 mg/L 03/07/12 09:30 03/07/12 20:25 1Antimony 0.0451
0.00500 0.00109 mg/L 03/07/12 09:30 03/07/12 20:25 1Arsenic 2.19
0.00500 0.000810 mg/L 03/07/12 09:30 03/07/12 20:25 1Barium 0.0315
0.00200 0.000854 mg/L 03/07/12 09:30 03/07/12 20:25 1Cadmium 0.292
0.500 0.198 mg/L 03/07/12 09:30 03/07/12 20:25 1Calcium 249
0.00500 0.00140 mg/L 03/07/12 09:30 03/07/12 20:25 1Chromium 0.00204 J
0.00500 0.00136 mg/L 03/07/12 09:30 03/07/12 20:25 1Cobalt 0.0110
0.0100 0.00200 mg/L 03/07/12 09:30 03/07/12 20:25 1Copper 2.67
0.250 0.101 mg/L 03/07/12 09:30 03/07/12 20:25 1Iron 3.42
0.00500 0.000733 mg/L 03/07/12 09:30 03/07/12 20:25 1Lead 0.299
0.500 0.113 mg/L 03/07/12 09:30 03/08/12 19:41 1Magnesium 15.2
0.0500 0.0116 mg/L 03/07/12 09:30 03/07/12 20:25 1Manganese 0.503
0.00500 0.00140 mg/L 03/07/12 09:30 03/07/12 20:25 1Molybdenum 0.233
0.00500 0.00217 mg/L 03/07/12 09:30 03/07/12 20:25 1Nickel 0.0329
1.00 0.407 mg/L 03/07/12 09:30 03/07/12 20:25 1Potassium 27.2
0.00500 0.00108 mg/L 03/07/12 09:30 03/07/12 20:25 1Selenium 0.488
1.00 0.727 mg/L 03/07/12 09:30 03/08/12 19:41 1Sodium 140
0.00100 0.000693 mg/L 03/07/12 09:30 03/07/12 20:25 1Thallium 0.335
0.0250 0.00355 mg/L 03/07/12 09:30 03/07/12 20:25 1Zinc 1.05
Method: 6020 - Metals (ICP/MS) - DissolvedMQL MDL
Antimony 0.0146 0.00500 0.00161 mg/L 03/08/12 09:30 03/09/12 00:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00500 0.00109 mg/L 03/08/12 09:30 03/09/12 00:34 1Arsenic 1.68
0.00500 0.000810 mg/L 03/08/12 09:30 03/09/12 00:34 1Barium 0.0203
0.00200 0.000854 mg/L 03/08/12 09:30 03/09/12 00:34 1Cadmium 0.256
0.00500 0.00140 mg/L 03/08/12 09:30 03/09/12 00:34 1Chromium 0.00140 U
0.00500 0.00136 mg/L 03/08/12 09:30 03/09/12 00:34 1Cobalt 0.0104
0.0100 0.00200 mg/L 03/08/12 09:30 03/09/12 00:34 1Copper 1.21
0.250 0.101 mg/L 03/08/12 09:30 03/09/12 00:34 1Iron 0.101 U
0.00500 0.000733 mg/L 03/08/12 09:30 03/09/12 00:34 1Lead 0.00933
0.00500 0.00140 mg/L 03/08/12 09:30 03/09/12 00:34 1Molybdenum 0.216
0.00500 0.00217 mg/L 03/08/12 09:30 03/09/12 00:34 1Nickel 0.0299
0.00500 0.00108 mg/L 03/08/12 09:30 03/09/12 00:34 1Selenium 0.441
0.00100 0.000693 mg/L 03/08/12 09:30 03/09/12 00:34 1Thallium 0.291
0.0250 0.00355 mg/L 03/08/12 09:30 03/09/12 00:34 1Zinc 0.836
Method: 7470A - Mercury (CVAA)MQL MDL
Mercury 0.00320 0.00200 0.000130 mg/L 03/08/12 10:00 03/08/12 14:22 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 560-31034-1Client: Malcolm Pirnie, Inc. Invoice to Arcadis
SDG: March 1, 2012Project/Site: Former ASARCO Groundwater
Lab Sample ID: 560-31034-6Client Sample ID: EP-116Matrix: WaterDate Collected: 03/01/12 14:20
Date Received: 03/02/12 10:25
Method: 7470A - Mercury (CVAA) - DissolvedMQL MDL
Mercury 0.000130 U 0.00200 0.000130 mg/L 03/08/12 10:00 03/08/12 14:24 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryMQL MDL
Total Dissolved Solids 3910 10.0 10.0 mg/L 03/05/12 10:45 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
3.00 3.00 mg/L 03/06/12 09:15 1Total Suspended Solids 28.8
1.00 0.192 mg/L 03/02/12 19:36 100Chloride 323
0.500 0.200 mg/L 03/02/12 15:33 4Nitrate Nitrite as N 19.7
1.00 0.377 mg/L 03/07/12 14:01 100Sulfate 1970
0.100 0.0200 mg/L 03/05/12 09:50 2Fluoride 3.68
0.0500 0.0131 mg/L 03/02/12 11:10 1Sulfide 0.0220 J
1.00 0.285 mg/L 03/07/12 12:15 1Total Organic Carbon 3.40
5.00 5.00 mg/L 03/05/12 12:55 1Total Alkalinity as CaCO3 416
Lab Sample ID: 560-31034-7Client Sample ID: EP-117Matrix: WaterDate Collected: 03/01/12 15:20
Date Received: 03/02/12 10:25
Method: 6020 - Metals (ICP/MS)MQL MDL
Aluminum 0.0225 U 0.0500 0.0225 mg/L 03/07/12 09:30 03/07/12 20:31 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00500 0.00161 mg/L 03/07/12 09:30 03/07/12 20:31 1Antimony 0.0161
0.00500 0.00109 mg/L 03/07/12 09:30 03/07/12 20:31 1Arsenic 3.32
0.00500 0.000810 mg/L 03/07/12 09:30 03/07/12 20:31 1Barium 0.0206
0.00200 0.000854 mg/L 03/07/12 09:30 03/07/12 20:31 1Cadmium 0.0494
0.500 0.198 mg/L 03/07/12 09:30 03/07/12 20:31 1Calcium 200
0.00500 0.00140 mg/L 03/07/12 09:30 03/07/12 20:31 1Chromium 0.00406 J
0.00500 0.00136 mg/L 03/07/12 09:30 03/07/12 20:31 1Cobalt 0.00136 U
0.0100 0.00200 mg/L 03/07/12 09:30 03/07/12 20:31 1Copper 0.00716 J
0.250 0.101 mg/L 03/07/12 09:30 03/07/12 20:31 1Iron 0.101 U
0.00500 0.000733 mg/L 03/07/12 09:30 03/07/12 20:31 1Lead 0.00896
0.500 0.113 mg/L 03/07/12 09:30 03/08/12 19:47 1Magnesium 37.7
0.0500 0.0116 mg/L 03/07/12 09:30 03/07/12 20:31 1Manganese 0.0175 J
0.00500 0.00140 mg/L 03/07/12 09:30 03/07/12 20:31 1Molybdenum 0.248
0.00500 0.00217 mg/L 03/07/12 09:30 03/07/12 20:31 1Nickel 0.0118
1.00 0.407 mg/L 03/07/12 09:30 03/07/12 20:31 1Potassium 78.3
0.00500 0.00108 mg/L 03/07/12 09:30 03/07/12 20:31 1Selenium 2.08
1.00 0.727 mg/L 03/07/12 09:30 03/08/12 20:45 10Sodium 843
0.00100 0.000693 mg/L 03/07/12 09:30 03/07/12 20:31 1Thallium 0.00244
0.0250 0.00355 mg/L 03/07/12 09:30 03/07/12 20:31 1Zinc 0.0660
Method: 6020 - Metals (ICP/MS) - DissolvedMQL MDL
Antimony 0.0159 0.00500 0.00161 mg/L 03/08/12 09:30 03/09/12 00:40 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00500 0.00109 mg/L 03/08/12 09:30 03/09/12 00:40 1Arsenic 3.35
0.00500 0.000810 mg/L 03/08/12 09:30 03/09/12 00:40 1Barium 0.0210
0.00200 0.000854 mg/L 03/08/12 09:30 03/09/12 00:40 1Cadmium 0.0491
0.00500 0.00140 mg/L 03/08/12 09:30 03/09/12 00:40 1Chromium 0.00400 J
0.00500 0.00136 mg/L 03/08/12 09:30 03/09/12 00:40 1Cobalt 0.00136 U
0.0100 0.00200 mg/L 03/08/12 09:30 03/09/12 00:40 1Copper 0.00457 J
0.250 0.101 mg/L 03/08/12 09:30 03/09/12 00:40 1Iron 0.101 U
0.00500 0.000733 mg/L 03/08/12 09:30 03/09/12 00:40 1Lead 0.00434 J
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Client Sample ResultsTestAmerica Job ID: 560-31034-1Client: Malcolm Pirnie, Inc. Invoice to Arcadis
SDG: March 1, 2012Project/Site: Former ASARCO Groundwater
Lab Sample ID: 560-31034-7Client Sample ID: EP-117Matrix: WaterDate Collected: 03/01/12 15:20
Date Received: 03/02/12 10:25
Method: 6020 - Metals (ICP/MS) - Dissolved (Continued)MQL MDL
Molybdenum 0.248 0.00500 0.00140 mg/L 03/08/12 09:30 03/09/12 00:40 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00500 0.00217 mg/L 03/08/12 09:30 03/09/12 00:40 1Nickel 0.0124
0.00500 0.00108 mg/L 03/08/12 09:30 03/09/12 00:40 1Selenium 2.12
0.00100 0.000693 mg/L 03/08/12 09:30 03/09/12 00:40 1Thallium 0.00175
0.0250 0.00355 mg/L 03/08/12 09:30 03/09/12 00:40 1Zinc 0.0675
Method: 7470A - Mercury (CVAA)MQL MDL
Mercury 0.000130 U 0.00200 0.000130 mg/L 03/08/12 10:00 03/08/12 14:27 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 7470A - Mercury (CVAA) - DissolvedMQL MDL
Mercury 0.000130 U 0.00200 0.000130 mg/L 03/08/12 10:00 03/08/12 14:29 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryMQL MDL
Total Dissolved Solids 3260 10.0 10.0 mg/L 03/05/12 10:45 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
3.00 3.00 mg/L 03/06/12 09:15 1Total Suspended Solids 3.00 U
1.00 0.192 mg/L 03/02/12 19:58 50Chloride 376
0.500 0.200 mg/L 03/02/12 15:55 4Nitrate Nitrite as N 27.2
1.00 0.377 mg/L 03/07/12 14:23 50Sulfate 1580
0.100 0.0200 mg/L 03/05/12 09:50 2Fluoride 2.94
0.0500 0.0131 mg/L 03/02/12 11:10 1Sulfide 0.0131 U
1.00 0.285 mg/L 03/07/12 12:15 1Total Organic Carbon 2.11
5.00 5.00 mg/L 03/05/12 12:55 1Total Alkalinity as CaCO3 290
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QC Sample ResultsTestAmerica Job ID: 560-31034-1Client: Malcolm Pirnie, Inc. Invoice to Arcadis
SDG: March 1, 2012Project/Site: Former ASARCO Groundwater
Method: 6020 - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 560-70320/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70352 Prep Batch: 70320
MQL MDL
Aluminum 0.0225 U 0.0500 0.0225 mg/L 03/07/12 09:30 03/07/12 18:09 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
0.00161 U 0.001610.00500 mg/L 03/07/12 09:30 03/07/12 18:09 1Antimony
0.000810 U 0.0008100.00500 mg/L 03/07/12 09:30 03/07/12 18:09 1Barium
0.000854 U 0.0008540.00200 mg/L 03/07/12 09:30 03/07/12 18:09 1Cadmium
0.198 U 0.1980.500 mg/L 03/07/12 09:30 03/07/12 18:09 1Calcium
0.00140 U 0.001400.00500 mg/L 03/07/12 09:30 03/07/12 18:09 1Chromium
0.00136 U 0.001360.00500 mg/L 03/07/12 09:30 03/07/12 18:09 1Cobalt
0.00200 U 0.002000.0100 mg/L 03/07/12 09:30 03/07/12 18:09 1Copper
0.101 U 0.1010.250 mg/L 03/07/12 09:30 03/07/12 18:09 1Iron
0.000733 U 0.0007330.00500 mg/L 03/07/12 09:30 03/07/12 18:09 1Lead
0.0116 U 0.01160.0500 mg/L 03/07/12 09:30 03/07/12 18:09 1Manganese
0.00140 U 0.001400.00500 mg/L 03/07/12 09:30 03/07/12 18:09 1Molybdenum
0.00217 U 0.002170.00500 mg/L 03/07/12 09:30 03/07/12 18:09 1Nickel
0.407 U 0.4071.00 mg/L 03/07/12 09:30 03/07/12 18:09 1Potassium
0.00108 U 0.001080.00500 mg/L 03/07/12 09:30 03/07/12 18:09 1Selenium
0.00355 U 0.003550.0250 mg/L 03/07/12 09:30 03/07/12 18:09 1Zinc
Client Sample ID: Method BlankLab Sample ID: MB 560-70320/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70390 Prep Batch: 70320
MQL MDL
Aluminum 0.0225 U 0.0500 0.0225 mg/L 03/07/12 09:30 03/08/12 16:46 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
0.00161 U 0.001610.00500 mg/L 03/07/12 09:30 03/08/12 16:46 1Antimony
0.00109 U 0.001090.00500 mg/L 03/07/12 09:30 03/08/12 16:46 1Arsenic
0.000810 U 0.0008100.00500 mg/L 03/07/12 09:30 03/08/12 16:46 1Barium
0.000854 U 0.0008540.00200 mg/L 03/07/12 09:30 03/08/12 16:46 1Cadmium
0.198 U 0.1980.500 mg/L 03/07/12 09:30 03/08/12 16:46 1Calcium
0.00140 U 0.001400.00500 mg/L 03/07/12 09:30 03/08/12 16:46 1Chromium
0.00136 U 0.001360.00500 mg/L 03/07/12 09:30 03/08/12 16:46 1Cobalt
0.00200 U 0.002000.0100 mg/L 03/07/12 09:30 03/08/12 16:46 1Copper
0.101 U 0.1010.250 mg/L 03/07/12 09:30 03/08/12 16:46 1Iron
0.000733 U 0.0007330.00500 mg/L 03/07/12 09:30 03/08/12 16:46 1Lead
0.113 U 0.1130.500 mg/L 03/07/12 09:30 03/08/12 16:46 1Magnesium
0.0116 U 0.01160.0500 mg/L 03/07/12 09:30 03/08/12 16:46 1Manganese
0.00140 U 0.001400.00500 mg/L 03/07/12 09:30 03/08/12 16:46 1Molybdenum
0.00217 U 0.002170.00500 mg/L 03/07/12 09:30 03/08/12 16:46 1Nickel
0.407 U 0.4071.00 mg/L 03/07/12 09:30 03/08/12 16:46 1Potassium
0.00108 U 0.001080.00500 mg/L 03/07/12 09:30 03/08/12 16:46 1Selenium
0.727 U 0.7271.00 mg/L 03/07/12 09:30 03/08/12 16:46 1Sodium
0.000693 U 0.0006930.00100 mg/L 03/07/12 09:30 03/08/12 16:46 1Thallium
0.00355 U 0.003550.0250 mg/L 03/07/12 09:30 03/08/12 16:46 1Zinc
Client Sample ID: Lab Control SampleLab Sample ID: LCS 560-70320/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70352 Prep Batch: 70320
Aluminum 4.00 3.599 mg/L 90 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Antimony 0.400 0.4095 mg/L 102 80 - 120
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QC Sample ResultsTestAmerica Job ID: 560-31034-1Client: Malcolm Pirnie, Inc. Invoice to Arcadis
SDG: March 1, 2012Project/Site: Former ASARCO Groundwater
Method: 6020 - Metals (ICP/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 560-70320/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70352 Prep Batch: 70320
Barium 0.400 0.4252 mg/L 106 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Cadmium 0.400 0.3868 mg/L 97 80 - 120
Calcium 40.0 41.33 mg/L 103 80 - 120
Chromium 0.400 0.4084 mg/L 102 80 - 120
Cobalt 0.400 0.4091 mg/L 102 80 - 120
Copper 0.400 0.4078 mg/L 102 80 - 120
Iron 40.0 42.51 mg/L 106 80 - 120
Lead 0.400 0.4896 mg/L 122 80 - 120
Manganese 4.00 4.656 mg/L 116 80 - 120
Molybdenum 0.400 0.4000 mg/L 100 80 - 120
Nickel 0.400 0.3987 mg/L 100 80 - 120
Potassium 40.0 39.27 mg/L 98 80 - 120
Selenium 0.400 0.3607 mg/L 90 80 - 120
Zinc 0.400 0.4236 mg/L 106 80 - 120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 560-70320/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70390 Prep Batch: 70320
Aluminum 4.00 3.484 mg/L 87 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Antimony 0.400 0.3680 mg/L 92 80 - 120
Arsenic 0.400 0.3743 mg/L 94 80 - 120
Barium 0.400 0.3731 mg/L 93 80 - 120
Cadmium 0.400 0.3633 mg/L 91 80 - 120
Calcium 40.0 38.74 mg/L 97 80 - 120
Chromium 0.400 0.3654 mg/L 91 80 - 120
Cobalt 0.400 0.3712 mg/L 93 80 - 120
Copper 0.400 0.3611 mg/L 90 80 - 120
Iron 40.0 37.40 mg/L 94 80 - 120
Lead 0.400 0.3882 mg/L 97 80 - 120
Magnesium 40.0 34.83 mg/L 87 80 - 120
Manganese 4.00 3.997 mg/L 100 80 - 120
Molybdenum 0.400 0.3686 mg/L 92 80 - 120
Nickel 0.400 0.3688 mg/L 92 80 - 120
Potassium 40.0 36.23 mg/L 91 80 - 120
Selenium 0.400 0.3636 mg/L 91 80 - 120
Sodium 40.0 33.19 mg/L 83 80 - 120
Thallium 0.200 0.1868 mg/L 93 80 - 120
Zinc 0.400 0.3703 mg/L 93 80 - 120
Client Sample ID: Method BlankLab Sample ID: MB 560-70379/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70390 Prep Batch: 70379
MQL MDL
Antimony 0.00161 U 0.00500 0.00161 mg/L 03/08/12 09:30 03/08/12 23:20 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
0.00109 U 0.001090.00500 mg/L 03/08/12 09:30 03/08/12 23:20 1Arsenic
0.000810 U 0.0008100.00500 mg/L 03/08/12 09:30 03/08/12 23:20 1Barium
0.000854 U 0.0008540.00200 mg/L 03/08/12 09:30 03/08/12 23:20 1Cadmium
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QC Sample ResultsTestAmerica Job ID: 560-31034-1Client: Malcolm Pirnie, Inc. Invoice to Arcadis
SDG: March 1, 2012Project/Site: Former ASARCO Groundwater
Method: 6020 - Metals (ICP/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 560-70379/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70390 Prep Batch: 70379
MQL MDL
Chromium 0.00140 U 0.00500 0.00140 mg/L 03/08/12 09:30 03/08/12 23:20 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
0.00136 U 0.001360.00500 mg/L 03/08/12 09:30 03/08/12 23:20 1Cobalt
0.00200 U 0.002000.0100 mg/L 03/08/12 09:30 03/08/12 23:20 1Copper
0.101 U 0.1010.250 mg/L 03/08/12 09:30 03/08/12 23:20 1Iron
0.000733 U 0.0007330.00500 mg/L 03/08/12 09:30 03/08/12 23:20 1Lead
0.00140 U 0.001400.00500 mg/L 03/08/12 09:30 03/08/12 23:20 1Molybdenum
0.00217 U 0.002170.00500 mg/L 03/08/12 09:30 03/08/12 23:20 1Nickel
0.00108 U 0.001080.00500 mg/L 03/08/12 09:30 03/08/12 23:20 1Selenium
0.000693 U 0.0006930.00100 mg/L 03/08/12 09:30 03/08/12 23:20 1Thallium
0.00355 U 0.003550.0250 mg/L 03/08/12 09:30 03/08/12 23:20 1Zinc
Client Sample ID: Lab Control SampleLab Sample ID: LCS 560-70379/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70390 Prep Batch: 70379
Antimony 0.400 0.3705 mg/L 93 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 0.400 0.3724 mg/L 93 80 - 120
Barium 0.400 0.3752 mg/L 94 80 - 120
Cadmium 0.400 0.3570 mg/L 89 80 - 120
Chromium 0.400 0.3733 mg/L 93 80 - 120
Cobalt 0.400 0.3784 mg/L 95 80 - 120
Copper 0.400 0.3741 mg/L 94 80 - 120
Iron 40.0 37.96 mg/L 95 80 - 120
Lead 0.400 0.3732 mg/L 93 80 - 120
Molybdenum 0.400 0.3643 mg/L 91 80 - 120
Nickel 0.400 0.3694 mg/L 92 80 - 120
Selenium 0.400 0.3536 mg/L 88 80 - 120
Thallium 0.200 0.1841 mg/L 92 80 - 120
Zinc 0.400 0.3668 mg/L 92 80 - 120
Client Sample ID: EP-85Lab Sample ID: 560-31034-1 MS
Matrix: Water Prep Type: Dissolved
Analysis Batch: 70390 Prep Batch: 70379
Antimony 0.0394 0.400 0.4095 mg/L 93 80 - 120
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic 1.30 0.400 1.646 mg/L 88 80 - 120
Barium 0.0315 0.400 0.4126 mg/L 95 80 - 120
Cadmium 0.000854 U 0.400 0.3432 mg/L 86 80 - 120
Chromium 0.00302 J 0.400 0.3777 mg/L 94 80 - 120
Cobalt 0.00136 U 0.400 0.3723 mg/L 93 80 - 120
Copper 0.00200 U 0.400 0.3576 mg/L 89 80 - 120
Iron 0.101 U 40.0 37.72 mg/L 94 80 - 120
Lead 0.000733 U 0.400 0.3651 mg/L 91 80 - 120
Molybdenum 0.537 0.400 0.9009 mg/L 91 80 - 120
Nickel 0.00217 U 0.400 0.3664 mg/L 92 80 - 120
Selenium 0.130 0.400 0.4584 mg/L 82 80 - 120
Thallium 0.0100 0.200 0.1880 mg/L 89 80 - 120
Zinc 0.00355 U 0.400 0.3581 mg/L 90 80 - 120
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QC Sample ResultsTestAmerica Job ID: 560-31034-1Client: Malcolm Pirnie, Inc. Invoice to Arcadis
SDG: March 1, 2012Project/Site: Former ASARCO Groundwater
Method: 6020 - Metals (ICP/MS) (Continued)
Client Sample ID: EP-85Lab Sample ID: 560-31034-1 MSD
Matrix: Water Prep Type: Dissolved
Analysis Batch: 70390 Prep Batch: 70379
Antimony 0.0394 0.400 0.4048 mg/L 91 80 - 120 1 20
Analyte
RPDMSD MSD
DUnitResult Qualifier RPD%Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits Limit
Arsenic 1.30 0.400 1.640 mg/L 86 80 - 120 0 20
Barium 0.0315 0.400 0.4034 mg/L 93 80 - 120 2 20
Cadmium 0.000854 U 0.400 0.3379 mg/L 84 80 - 120 2 20
Chromium 0.00302 J 0.400 0.3755 mg/L 93 80 - 120 1 20
Cobalt 0.00136 U 0.400 0.3736 mg/L 93 80 - 120 0 20
Copper 0.00200 U 0.400 0.3588 mg/L 90 80 - 120 0 20
Iron 0.101 U 40.0 37.75 mg/L 94 80 - 120 0 20
Lead 0.000733 U 0.400 0.3625 mg/L 91 80 - 120 1 20
Molybdenum 0.537 0.400 0.9013 mg/L 91 80 - 120 0 20
Nickel 0.00217 U 0.400 0.3599 mg/L 90 80 - 120 2 20
Selenium 0.130 0.400 0.4627 mg/L 83 80 - 120 1 20
Thallium 0.0100 0.200 0.1892 mg/L 90 80 - 120 1 20
Zinc 0.00355 U 0.400 0.3504 mg/L 88 80 - 120 2 20
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 560-70336/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70342 Prep Batch: 70336
MQL MDL
Mercury 0.000130 U 0.00200 0.000130 mg/L 03/07/12 12:30 03/07/12 17:37 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 560-70336/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70342 Prep Batch: 70336
Mercury 0.00500 0.004980 mg/L 100 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Method BlankLab Sample ID: MB 560-70362/4-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70392 Prep Batch: 70362
MQL MDL
Mercury 0.000130 U 0.00200 0.000130 mg/L 03/08/12 10:00 03/08/12 14:18 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 560-70362/5-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70392 Prep Batch: 70362
Mercury 0.00500 0.004920 mg/L 98 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
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QC Sample ResultsTestAmerica Job ID: 560-31034-1Client: Malcolm Pirnie, Inc. Invoice to Arcadis
SDG: March 1, 2012Project/Site: Former ASARCO Groundwater
Method: 160.1 - Solids, Total Dissolved (TDS)
Client Sample ID: Method BlankLab Sample ID: MB 560-70251/1
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70251
MQL MDL
Total Dissolved Solids 10.0 U 10.0 10.0 mg/L 03/05/12 10:45 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 560-70251/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70251
Total Dissolved Solids 2250 2172 mg/L 97 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: EP-117Lab Sample ID: 560-31034-7 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70251
Total Dissolved Solids 3260 2250 5605 mg/L 104 75 - 125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: EP-117Lab Sample ID: 560-31034-7 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70251
Total Dissolved Solids 3260 3370 mg/L 3 20
Analyte
RPDDU DU
DUnitResult Qualifier RPD
Sample
Result
Sample
Qualifier Limit
Method: 160.2 - Solids, Total Suspended (TSS)
Client Sample ID: Method BlankLab Sample ID: MB 560-70266/1
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70266
MQL MDL
Total Suspended Solids 3.00 U 3.00 3.00 mg/L 03/06/12 09:15 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Method: 300.0 - Anions, Ion Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 560-70172/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70172
MQL MDL
Chloride 0.192 U 1.00 0.192 mg/L 03/02/12 12:15 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
0.200 U 0.2000.500 mg/L 03/02/12 12:15 1Nitrate Nitrite as N
Client Sample ID: Lab Control SampleLab Sample ID: LCS 560-70172/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70172
Chloride 10.0 9.639 mg/L 96 90 - 110
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
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QC Sample ResultsTestAmerica Job ID: 560-31034-1Client: Malcolm Pirnie, Inc. Invoice to Arcadis
SDG: March 1, 2012Project/Site: Former ASARCO Groundwater
Method: 300.0 - Anions, Ion Chromatography (Continued)
Client Sample ID: FD030212Lab Sample ID: 560-31034-4 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70172
Chloride 310 500 744.2 mg/L 87 80 - 120
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: FD030212Lab Sample ID: 560-31034-4 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70172
Chloride 310 500 730.8 mg/L 84 80 - 120 2 20
Analyte
RPDMSD MSD
DUnitResult Qualifier RPD%Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits Limit
Client Sample ID: Method BlankLab Sample ID: MB 560-70349/39
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70349
MQL MDL
Chloride 0.192 U 1.00 0.192 mg/L 03/07/12 11:27 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
0.200 U 0.2000.500 mg/L 03/07/12 11:27 1Nitrate Nitrite as N
0.377 U 0.3771.00 mg/L 03/07/12 11:27 1Sulfate
Client Sample ID: Method BlankLab Sample ID: MB 560-70349/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70349
MQL MDL
Chloride 0.192 U 1.00 0.192 mg/L 03/06/12 12:37 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
0.200 U 0.2000.500 mg/L 03/06/12 12:37 1Nitrate Nitrite as N
0.377 U 0.3771.00 mg/L 03/06/12 12:37 1Sulfate
Client Sample ID: Lab Control SampleLab Sample ID: LCS 560-70349/40
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70349
Chloride 10.0 10.57 mg/L 106 90 - 110
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Sulfate 25.0 26.24 mg/L 105 90 - 110
Client Sample ID: Lab Control SampleLab Sample ID: LCS 560-70349/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70349
Chloride 10.0 10.60 mg/L 106 90 - 110
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Sulfate 25.0 26.12 mg/L 104 90 - 110
Client Sample ID: EP-81Lab Sample ID: 560-31034-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70349
Chloride 151 250 402.9 mg/L 101 80 - 120
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Sulfate 678 500 1169 mg/L 98 80 - 120
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QC Sample ResultsTestAmerica Job ID: 560-31034-1Client: Malcolm Pirnie, Inc. Invoice to Arcadis
SDG: March 1, 2012Project/Site: Former ASARCO Groundwater
Method: 300.0 - Anions, Ion Chromatography (Continued)
Client Sample ID: EP-81Lab Sample ID: 560-31034-2 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70349
Chloride 151 250 397.4 mg/L 99 80 - 120 1 20
Analyte
RPDMSD MSD
DUnitResult Qualifier RPD%Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits Limit
Sulfate 678 500 1153 mg/L 95 80 - 120 1 20
Method: 340.2 - Fluoride
Client Sample ID: Method BlankLab Sample ID: MB 560-70213/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70213
MQL MDL
Fluoride 0.0200 U 0.100 0.0200 mg/L 03/05/12 09:50 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 560-70213/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70213
Fluoride 0.800 0.7980 mg/L 100 85 - 115
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Method: 376.2 - Sulfide
Client Sample ID: Method BlankLab Sample ID: MB 560-70148/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70148
MQL MDL
Sulfide 0.0131 U 0.0500 0.0131 mg/L 03/02/12 11:10 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 560-70148/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70148
Sulfide 0.535 0.4770 mg/L 89 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: EP-116Lab Sample ID: 560-31034-6 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70148
Sulfide 0.0220 J 0.535 0.5420 mg/L 97 75 - 125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: EP-116Lab Sample ID: 560-31034-6 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70148
Sulfide 0.0220 J 0.535 0.5180 mg/L 93 75 - 125 5 20
Analyte
RPDMSD MSD
DUnitResult Qualifier RPD%Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits Limit
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QC Sample ResultsTestAmerica Job ID: 560-31034-1Client: Malcolm Pirnie, Inc. Invoice to Arcadis
SDG: March 1, 2012Project/Site: Former ASARCO Groundwater
Method: 415.1 - TOC
Client Sample ID: Method BlankLab Sample ID: MB 560-70394/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70394
MQL MDL
Total Organic Carbon 0.285 U 1.00 0.285 mg/L 03/07/12 12:15 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 560-70394/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70394
Total Organic Carbon 25.0 22.93 mg/L 92 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Method: SM 2320B - Alkalinity
Client Sample ID: Lab Control SampleLab Sample ID: LCS 560-70226/1
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70226
Total Alkalinity as CaCO3 100 92.60 mg/L 93 85 - 115
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control SampleLab Sample ID: LCS 560-70226/14
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70226
Total Alkalinity as CaCO3 100 94.00 mg/L 94 85 - 115
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control SampleLab Sample ID: LCS 560-70226/22
Matrix: Water Prep Type: Total/NA
Analysis Batch: 70226
Total Alkalinity as CaCO3 100 97.20 mg/L 97 85 - 115
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
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Certification SummaryClient: Malcolm Pirnie, Inc. Invoice to Arcadis TestAmerica Job ID: 560-31034-1
Project/Site: Former ASARCO Groundwater SDG: March 1, 2012
Laboratory Authority Program EPA Region Certification ID
TestAmerica Corpus Christi E-10362NELACKansas 7
TestAmerica Corpus Christi 9968State ProgramOklahoma 6
TestAmerica Corpus Christi T104704210-11-5NELACTexas 6
TestAmerica Corpus Christi P330-11-00060FederalUSDA
Accreditation may not be offered or required for all methods and analytes reported in this package . Please contact your project manager for the laboratory's
current list of certified methods and analytes.
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Method SummaryTestAmerica Job ID: 560-31034-1Client: Malcolm Pirnie, Inc. Invoice to Arcadis
SDG: March 1, 2012Project/Site: Former ASARCO Groundwater
Method Method Description LaboratoryProtocol
SW8466020 Metals (ICP/MS) TAL CC
SW8467470A Mercury (CVAA) TAL CC
MCAWW160.1 Solids, Total Dissolved (TDS) TAL CC
MCAWW160.2 Solids, Total Suspended (TSS) TAL CC
MCAWW300.0 Anions, Ion Chromatography TAL CC
MCAWW340.2 Fluoride TAL CC
MCAWW376.2 Sulfide TAL CC
MCAWW415.1 TOC TAL CC
SMSM 2320B Alkalinity TAL CC
Protocol References:
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater",
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL CC = TestAmerica Corpus Christi, 1733 N. Padre Island Drive, Corpus Christi, TX 78408, TEL (361)289-2673
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Sample SummaryTestAmerica Job ID: 560-31034-1Client: Malcolm Pirnie, Inc. Invoice to Arcadis
SDG: March 1, 2012Project/Site: Former ASARCO Groundwater
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
560-31034-1 EP-85 Water 03/01/12 08:00 03/02/12 10:25
560-31034-2 EP-81 Water 03/01/12 09:15 03/02/12 10:25
560-31034-3 OBS-1 Water 03/01/12 10:15 03/02/12 10:25
560-31034-4 FD030212 Water 03/01/12 00:00 03/02/12 10:25
560-31034-5 EP-114 Water 03/01/12 11:05 03/02/12 10:25
560-31034-6 EP-116 Water 03/01/12 14:20 03/02/12 10:25
560-31034-7 EP-117 Water 03/01/12 15:20 03/02/12 10:25
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Page 27 of 30 3/18/2012
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Login Sample Receipt Checklist
Client: Malcolm Pirnie, Inc. Invoice to Arcadis Job Number: 560-31034-1
SDG Number: March 1, 2012
Login Number: 31034
Question Answer Comment
Creator: Magee, Alice J.
List Source: TestAmerica Corpus Christi
List Number: 1
N/ARadioactivity either was not measured or, if measured, is at or below
background
TrueThe cooler's custody seal, if present, is intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
FalseIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the sample IDs on the containers and
the COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AVOA sample vials do not have headspace or bubble is <6mm (1/4") in
diameter.
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
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Default Detection LimitsClient: Malcolm Pirnie, Inc. Invoice to Arcadis TestAmerica Job ID: 560-31034-1
Project/Site: Former ASARCO Groundwater SDG: March 1, 2012
Method: 6020 - Metals (ICP/MS)
0.0500 6020Aluminum mg/L
Analyte Units Method
0.0225
MDLMQL
60200.001610.00500Antimony mg/L
60200.001090.00500Arsenic mg/L
60200.0008100.00500Barium mg/L
60200.0008540.00200Cadmium mg/L
60200.1980.500Calcium mg/L
60200.001400.00500Chromium mg/L
60200.001360.00500Cobalt mg/L
60200.002000.0100Copper mg/L
60200.1010.250Iron mg/L
60200.0007330.00500Lead mg/L
60200.1130.500Magnesium mg/L
60200.01160.0500Manganese mg/L
60200.001400.00500Molybdenum mg/L
60200.002170.00500Nickel mg/L
60200.4071.00Potassium mg/L
60200.001080.00500Selenium mg/L
60200.7271.00Sodium mg/L
60200.0006930.00100Thallium mg/L
60200.003550.0250Zinc mg/L
Method: 6020 - Metals (ICP/MS) - Dissolved
0.00500 6020Antimony mg/L
Analyte Units Method
0.00161
MDLMQL
60200.001090.00500Arsenic mg/L
60200.0008100.00500Barium mg/L
60200.0008540.00200Cadmium mg/L
60200.001400.00500Chromium mg/L
60200.001360.00500Cobalt mg/L
60200.002000.0100Copper mg/L
60200.1010.250Iron mg/L
60200.0007330.00500Lead mg/L
60200.001400.00500Molybdenum mg/L
60200.002170.00500Nickel mg/L
60200.001080.00500Selenium mg/L
60200.0006930.00100Thallium mg/L
60200.003550.0250Zinc mg/L
Method: 7470A - Mercury (CVAA)
0.00200 7470AMercury mg/L
Analyte Units Method
0.000130
MDLMQL
Method: 7470A - Mercury (CVAA) - Dissolved
0.00200 7470AMercury mg/L
Analyte Units Method
0.000130
MDLMQL
General Chemistry
10.0 160.1Total Dissolved Solids mg/L
Analyte Units Method
10.0
MDLMQL
160.23.003.00Total Suspended Solids mg/L
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Default Detection LimitsClient: Malcolm Pirnie, Inc. Invoice to Arcadis TestAmerica Job ID: 560-31034-1
Project/Site: Former ASARCO Groundwater SDG: March 1, 2012
General Chemistry (Continued)
1.00 300.0Chloride mg/L
Analyte Units Method
0.192
MDLMQL
300.00.2000.500Nitrate Nitrite as N mg/L
300.00.3771.00Sulfate mg/L
340.20.02000.100Fluoride mg/L
376.20.01310.0500Sulfide mg/L
415.10.2851.00Total Organic Carbon mg/L
SM 2320B5.005.00Total Alkalinity as CaCO3 mg/L
TestAmerica Corpus Christi
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