r - MedKoo USP Width 0.114 Resolution 0.000 Height 194463 ... Chromolith Flash RP-18e 25-2mm B: ......
6
8.277 8.256 7.863 7.322 7.285 6.561 6.555 6.546 6.531 6.524 4.860 4.838 4.817 4.292 3.901 3.397 2.737 2.357 2.338 2.316 2.307 2.288 2.067 2.032 2.026 2.018 1.994 1.965 1.915 1.906 1.895 1.885 1.874 1.863 1.854 1.841 1.834 1.727 1.711 1.698 1.02 1.00 0.95 2.03 1.02 1.00 3.12 1.98 7.18 6.50 2.81 2.46 8 7 6 5 4 3 2 1 PPM N N N N O H N O N O USER: SUN-SHINE -- DATE: 14:02:13.556 +0800 root@EP-10062260 Nuts - $wx00002-YCSW-01337-1024_1.1 AZ-3146, CDCl3 400MHz, , F1: 400.130 F2: 1.000 SW1: 8224 OF1: 2471.0 PTS1d: 65536 EX: zg30 PW: 14.5 usec PD: 1.0 sec NA: 4 LB: 0.3 MedKoo Biosciences www.medkoo.com [email protected] MedKoo Biosciences Product Quality Control Data www.medkoo.com | [email protected] MedKoo Biosciences Product Quality Control Data www.medkoo.com | [email protected] MedKoo Biosciences Product Quality Control Data www.medkoo.com | [email protected]
Transcript of r - MedKoo USP Width 0.114 Resolution 0.000 Height 194463 ... Chromolith Flash RP-18e 25-2mm B: ......
8
.27
7 8
.25
6
7
.86
3
7
.32
2 7
.28
5
6
.56
1 6
.55
5 6
.54
6 6
.53
1 6
.52
4
4
.86
0 4
.83
8 4
.81
7
4
.29
2
3
.90
1
3
.39
7
2
.73
7
2
.35
7 2
.33
8 2
.31
6 2
.30
7
2
.28
8 2
.06
7 2
.03
2 2
.02
6 2
.01
8 1
.99
4 1
.96
5 1
.91
5 1
.90
6 1
.89
5 1
.88
5 1
.87
4 1
.86
3 1
.85
4 1
.84
1 1
.83
4 1
.72
7 1
.71
1 1
.69
8
1.02 1.00 0.95
2.03 1.02 1.00
3.12
1.98
7.18 6.50
2.81 2.46
8 7 6 5 4 3 2 1 PPM
N
N N
NO
HN
O
N
O
USER: SUN-SHINE -- DATE: 14:02:13.556 +0800 root@EP-10062260
Nuts - $wx00002-YCSW-01337-1024_1.1
AZ-3146, CDCl3 400MHz, , F1: 400.130 F2: 1.000 SW1: 8224 OF1: 2471.0 PTS1d: 65536 EX: zg30 PW: 14.5 usec PD: 1.0 sec NA: 4 LB: 0.3
MedKoo Biosciences www.medkoo.com [email protected]
MedKoo Biosciences Product Quality Control Data
www.medkoo.com | [email protected]
MedKoo Biosciences Product Quality Control Data
www.medkoo.com | [email protected]
MedKoo Biosciences Product Quality Control Data
www.medkoo.com | [email protected]
BioMedomics
打字机文本
NMR analysis of AZ3146 Solvent = CDCl3
BioMedomics
打字机文本
BioMedomics
打字机文本
BioMedomics
打字机文本
BioMedomics
打字机文本
BioMedomics
打字机文本
MedKoo Code#: 406239 Name: AZ-3146 CAS#: 1124329-14-1 Lot#SSC20131104 Chemical Formula: C24H32N6O3 Exact Mass: 452.25359 Molecular Weight: 452.55
BioMedomics
打字机文本
BioMedomics
打字机文本
BioMedomics
打字机文本
BioMedomics
图章
HPLC REPORT
Compound ID : 1 Sample ID : WX00002-YCSW-01337-1024
Vial# : 7 Injection Volumn : 0.2
Filename : D:\Data\1310\24\WX00002-YCSW-01337-1024.lcd Method Name : D:\method\10-80AB_6min.lcm
Instrument &Column : HPLC-D Innovation C18 UPLC Column 2.1X30mm,2.6um Run time : 10/24/2013 13:17:12
min
mAU
0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 5.0 5.5
0
50
100
150
200 PDA Multi 1
1.7
52
PDA Multi 1 / 220nm 4nm 1
----------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------- Integration result -----------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------
PeakTablePDA Ch1 220nm 4nm
Peak# 1
Total
Ret. Time 1.752
USP Width 0.114
Resolution 0.000
Height 193832 193832
Area 922796 922796
Area % 100.000 100.000
Operater : ________________
Date : ________________
Med
Koo
Bio
scie
nces
ww
w.m
edko
o.co
msa
les@
med
koo.
com
MedKoo Biosciences Product Quality Control Data
www.medkoo.com | [email protected]
MedKoo Biosciences Product Quality Control Data
www.medkoo.com | [email protected]
MedKoo Biosciences Product Quality Control Data
www.medkoo.com | [email protected]
BioMedomics
打字机文本
BioMedomics
打字机文本
BioMedomics
打字机文本
HPLC analysis of AZ-3146
BioMedomics
打字机文本
BioMedomics
打字机文本
BioMedomics
打字机文本
BioMedomics
打字机文本
BioMedomics
图章
BioMedomics
打字机文本
BioMedomics
打字机文本
BioMedomics
打字机文本
BioMedomics
打字机文本
BioMedomics
打字机文本
MedKoo Code#: 406239 Name: AZ-3146 CAS#: 1124329-14-1 Lot#SSC20131104 Chemical Formula: C24H32N6O3 Exact Mass: 452.25359 Molecular Weight: 452.55
HPLC REPORT
Compound ID : 1Sample ID : WX00002-YCSW-01337-1024Filename : D:\Data\1310\24\WX00002-YCSW-01337-1024.lcdMethod Name : D:\method\10-80AB_6min.lcmInstrument &Column : HPLC-D Xtimate C18 2.1*30mm*3um Run time : 10/24/2013 13:17:12
min
mAU
0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 5.0 5.5
0
50
100
150
200 PDA Multi 2
1.7
51
PDA Multi 2 / 215nm 4nm 1
----------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------- Integration result -----------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------
PeakTablePDA Ch2 215nm 4nm
Peak# 1
Total
Ret. Time 1.751
USP Width 0.114
Resolution 0.000
Height 194463 194463
Area 937556 937556
Area % 100.000 100.000
Operater : ________________
Date : ________________
Med
Koo
Bio
scie
nces
ww
w.m
edko
o.co
msa
les@
med
koo.
com
MedKoo Biosciences Product Quality Control Data
www.medkoo.com | [email protected]
MedKoo Biosciences Product Quality Control Data
www.medkoo.com | [email protected]
MedKoo Biosciences Product Quality Control Data
www.medkoo.com | [email protected]
BioMedomics
打字机文本
BioMedomics
打字机文本
AZ-3146 HPLC analysis
BioMedomics
打字机文本
BioMedomics
打字机文本
BioMedomics
打字机文本
BioMedomics
打字机文本
BioMedomics
图章
BioMedomics
打字机文本
MedKoo Code#: 406239 Name: AZ-3146 CAS#: 1124329-14-1 Lot#SSC20131104 Chemical Formula: C24H32N6O3 Exact Mass: 452.25359 Molecular Weight: 452.55
HPLC REPORT
Compound ID : 1Sample ID : WX00002-YCSW-01337-1024Filename : D:\Data\1310\24\WX00002-YCSW-01337-1024.lcdMethod Name : D:\method\10-80AB_6min.lcmInstrument &Column : HPLC-D Xtimate C18 2.1*30mm*3um Run time : 10/24/2013 13:17:12
min
mAU
0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 5.0 5.5
0
50
100
150
200
PDA Multi 3
1.7
52
PDA Multi 3 / 254nm 4nm 1
----------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------- Integration result -----------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------
PeakTablePDA Ch3 254nm 4nm
Peak# 1
Total
Ret. Time 1.752
USP Width 0.114
Resolution 0.000
Height 211473 211473
Area 982538 982538
Area % 100.000 100.000
Operater : ________________
Date : ________________
Med
Koo
Bio
scie
nces
ww
w.m
edko
o.co
msa
les@
med
koo.
com
MedKoo Biosciences Product Quality Control Data
www.medkoo.com | [email protected]
MedKoo Biosciences Product Quality Control Data
www.medkoo.com | [email protected]
MedKoo Biosciences Product Quality Control Data
www.medkoo.com | [email protected]
BioMedomics
打字机文本
AZ-3146 HPLC analysis
BioMedomics
打字机文本
BioMedomics
打字机文本
BioMedomics
打字机文本
BioMedomics
打字机文本
BioMedomics
打字机文本
BioMedomics
图章
BioMedomics
打字机文本
MedKoo Code#: 406239 Name: AZ-3146 CAS#: 1124329-14-1 Lot#SSC20131104 Chemical Formula: C24H32N6O3 Exact Mass: 452.25359 Molecular Weight: 452.55
BioMedomics
打字机文本
BioMedomics
打字机文本
LCMS REPORT
Compound ID : Sample ID : WX00002-YCSW-A2-3146Injection Date : Mon, 28. Oct. 2013Location : P1-C-07Injection volume : 1.000 Acq Method : D:\DATA\131028 1\5-95AB_R_220&254.MData Filename : D:\DATA\WX00002-YCSW-A2-3146.DInstrument : LCMS-B Column: A:Chromolith Flash RP-18e 25-2mm B:infinite C18 2.1X30mm,3.5um ->
min0 0.25 0.5 0.75 1 1.25
mAU
0
500
DAD1 A, Sig=220,4 Ref=off (D:\DATA\WX00002-YCSW-A2-3146.D)
0.6
30
min0 0.25 0.5 0.75 1 1.25
mAU
0
500
1000
DAD1 B, Sig=254,4 Ref=off (D:\DATA\WX00002-YCSW-A2-3146.D) 0
.630
min0 0.25 0.5 0.75 1 1.250
200000
400000
MSD1 TIC, MS File (D:\DATA\WX00002-YCSW-A2-3146.D) ES-API, Pos, Scan, Frag: 70
Report==================================================================
Signal 1 : DAD1 A, Sig=220,4 Ref=off # Meas. Ret. Height Width Area Area % --------------------------------------------------------- 1 0.630 1262.227 0.017 1416.375 100.000---------------------------------------------------------
Signal 2 : DAD1 B, Sig=254,4 Ref=off # Meas. Ret. Height Width Area Area % --------------------------------------------------------- 1 0.630 1447.066 0.017 1611.958 100.000---------------------------------------------------------
Operator:__________________
Date:___________________
Med
Koo
Bio
scie
nces
ww
w.m
edko
o.co
msa
les@
med
koo.
com
MedKoo Biosciences Product Quality Control Data
www.medkoo.com | [email protected]
MedKoo Biosciences Product Quality Control Data
www.medkoo.com | [email protected]
MedKoo Biosciences Product Quality Control Data
www.medkoo.com | [email protected]
BioMedomics
打字机文本
MedKoo Code#: 406239 Name: AZ-3146 CAS#: 1124329-14-1 Lot#SSC20131104 Chemical Formula: C24H32N6O3 Exact Mass: 452.25359 Molecular Weight: 452.55
BioMedomics
打字机文本
AZ-3146 LCMS analysis
BioMedomics
打字机文本
BioMedomics
打字机文本
m/z100 200 300 400 500 600 700 800 9000
5E4
1E5
2E5
2E5
3E5
3E5
*MSD1 SPC, time= 0.63
130
.2 1
53.1
193
.4
227
.2
453
.3 4
54.2
455
.3
501
.4
927
.5 9
28.4
Med
Koo
Bio
scie
nces
ww
w.m
edko
o.co
msa
les@
med
koo.
com
MedKoo Biosciences Product Quality Control Data
www.medkoo.com | [email protected]
MedKoo Biosciences Product Quality Control Data
www.medkoo.com | [email protected]
MedKoo Biosciences Product Quality Control Data
www.medkoo.com | [email protected]
BioMedomics
打字机文本
MedKoo Code#: 406239 Name: AZ-3146 CAS#: 1124329-14-1 Lot#SSC20131104 Chemical Formula: C24H32N6O3 Exact Mass: 452.25359 Molecular Weight: 452.55
BioMedomics
打字机文本
BioMedomics
图章
BioMedomics
打字机文本
AZ-3146 LCMS analysis
BioMedomics
打字机文本
BioMedomics
打字机文本
BioMedomics
打字机文本
![Certificate of Analysis - MedKoo · 2017-08-17 · Certificate of Analysis MedKoo Cat#: Product Name: Lot# 202250 Pixantrone Maleate TZC40615 Chemical name 6,9-bis((2-aminoethyl)amino)benzo[g]isoquinoline-5,10-dione](https://static.fdocuments.us/doc/165x107/5f9f51de7ab88e01124dceca/certificate-of-analysis-medkoo-2017-08-17-certificate-of-analysis-medkoo-cat.jpg)
