r - MedKoo · 2020. 11. 1. · CO1686-DA NMR analysis\rSolvent = DMSO-d6 MedKoo Cat#:205796A\rName:...

0.00.51.01.52.02.53.03.54.04.55.05.56.06.57.07.58.08.59.09.510.010.5f1 (ppm)

3.05

2.03

2.03

4.06

3.09

1.90

2.08

2.15

0.77

1.01

1.00

0.98

0.86

0.93

0.00

2.05

2.50

3.05

3.11

3.35

3.58

3.59

3.78

4.99

6.37

6.38

6.64

6.71

6.93

6.95

6.97

7.53

7.56

8.12

8.19

8.24

MedKoo Biosciences www.medkoo.com [email protected]

MedKoo Biosciences Product Quality Control Data

www.medkoo.com | [email protected]





BioMedomics图章

BioMedomics打字机文本CO1686-DA NMR analysisSolvent = DMSO-d6

BioMedomics打字机文本




BioMedomics打字机文本MedKoo Cat#:205796AName: CO1686-DACAS#: unknownLot#BBC40322Chemical Formula: C24H26F3N7O2Exact Mass: 501.21001Molecular Weight: 501.50

=====================================================================

操作者 : 系统序列行 : 3

仪器 : LC1260 位置 : 样品瓶 13

进样日期 : 2014-3-18 16:07:32 进样次数 : 1

进样量 : 0.000 µl

来自于序列的不同进样量! 实际进样量: 3.000 µl

采集方法 : E:\DATA\YI ZHIJUN\DATA\20140318\20130913-01 2014-03-18 15-23-26\50-90 BC

15MIN.M

最后修改 : 2014-3-18 15:23:26 : 系统

分析方法 : C:\CHEM32\1\METHODS\50-90 BC 15MIN.M

最后修改 : 2014-3-17 19:01:39 : 系统

min0 2 4 6 8 10 12 14

mAU

0

200

400

600

800

VWD1 A, Wavelength=220 nm (E:\DATA\YI ZHIJUN\DATA\20140318\20130913-01 2014-03-18 15-23-26\YY-0318-2.D)

6.9

26

7.5

30

=====================================================================

面积百分比报告

=====================================================================

排序　　　　　　 : 信号

乘积因子 : 1.0000

稀释因子 : 1.0000

内标使用乘积因子和稀释因子

信号 1: VWD1 A, Wavelength=220 nm

峰保留时间类型峰宽峰面积峰高峰面积

# [min] [min] [mAU*s] [mAU] %

----|-------|----|-------|----------|----------|--------|

1 6.926 VV 0.1176 3117.00684 405.64795 99.1740

2 7.530 VB 0.1681 25.96042 2.17690 0.8260

总量 : 3142.96725 407.82485

=====================================================================

数据文件: E:\DATA\YI ZHIJUN\DATA\20140318\20130913-01 2014-03-18 15-23-26\YY-0318-2.D

样品名称: yy-0318-2

LC1260 2014-3-18 17:10:40 系统页 1/1

Med

Koo

Bio

scie

nces

ww

w.m

edko

o.co

msa

les@

med

koo.

com







BioMedomics打字机文本CO1686-DA HPLC analysis





BioMedomics图章

=====================================================================Acq. Operator : XYL-M1111 Acq. Instrument : Instrument 1 Location : Vial 1Injection Date : 3/11/2014 10:50:35 AM Inj Volume : 2.0 µlAcq. Method : C:\CHEM32\1\METHODS\20120428-LCMS.MLast changed : 3/11/2014 10:49:51 AM by XYL-M1111 (modified after loading)Analysis Method : C:\CHEM32\1\METHODS\20120409-LC-MS.MLast changed : 3/11/2014 10:16:40 AM by WYB (modified after loading)Method Info : 20120409-lc-ms

min0 1 2 3 4 5 6 7 8 9

mAU

0

200

400

600

800

DAD1 A, Sig=254,16 Ref=360,100 (20140321\HP1000041.D)

4.2

38

Data File D:\DATA\DDDCSYN\20140321\HP1000041.DSample Name: HP1

Instrument 1 3/11/2014 10:11:02 AM WYB Page 1 of 2MedKoo Biosciences www.medkoo.com [email protected]









BioMedomics图章

===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier: : 1.0000Dilution: : 1.0000Use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 A, Sig=254,16 Ref=360,100 Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 4.238 BB 0.1082 7016.72607 996.24841 100.0000 Totals : 7016.72607 996.24841 ===================================================================== *** End of Report ***

Data File D:\DATA\DDDCSYN\20140321\HP1000041.DSample Name: HP1










BioMedomics图章

Current Chromatogram(s)

min0 1 2 3 4

mAU

0

500

1000

1500

DAD1 A, Sig=254,16 Ref=360,100 (20140321\501000035.D)

0.4

15

0.7

15

1.2

62

min0 1 2 3 4

mAU

0

500

1000

1500

DAD1 B, Sig=214,16 Ref=360,100 (20140321\501000035.D)

0.3

25

0.4

31 0

.490

0.7

00 0

.746

1.2

64

1.8

26

min0 1 2 3 40

20000

40000

60000

80000

MSD1 TIC, MS File (D:\DATA\DDDCSYN\20140321\501000035.D) MM-ES+APCI, Pos, Scan, Frag: 70

0.9

06

min0 1 2 3 4

20000

40000

60000

80000

100000

MSD2 TIC, MS File (D:\DATA\DDDCSYN\20140321\501000035.D) MM-ES+APCI, Neg, Scan, Frag: 70

0.1

11

0.2

73

0.6

70

0.8

33

1.0

19

1.7

00

2.0

42

2.9

94

3.1

32

3.2

53

3.5

81

3.7

91

4.3

01

4.5

36

Print of all graphic windows








BioMedomics打字机文本CO1686-DA LCMS analysis



BioMedomics图章


min0 1 2 3 4

mAU

0

500

1000

1500

DAD1 A, Sig=254,16 Ref=360,100 (20140321\501000035.D)

0.4

15

0.7

15

1.2

62

min0 1 2 3 4

mAU

0

500

1000

1500

DAD1 B, Sig=214,16 Ref=360,100 (20140321\501000035.D)

0.3

25

0.4

31 0

.490

0.7

00 0

.746

1.2

64

1.8

26

min0 1 2 3 40

20000

40000

60000

80000


0.9

06

min0 1 2 3 4

20000

40000

60000

80000

100000


0.1

11

0.2

73

0.6

70

0.8

33

1.0

19

1.7

00

2.0

42

2.9

94

3.1

32

3.2

53

3.5

81

3.7

91

4.3

01

4.5

36

MS Spectrum

m/z100 200 300 400 500 600 700 800 900 1000

0

20

40

60

80

100

*MSD2 SPC, time=0.717:1.402 of D:\DATA\DDDCSYN\20140321\501000035.D MM-ES+APCI, Neg, Scan, Frag: 70

Max: 40420

501

.2 5

00.2











BioMedomics图章


min0 1 2 3 4

mAU

0

500

1000

1500

DAD1 A, Sig=254,16 Ref=360,100 (20140321\501000035.D)

0.4

15

0.7

15

1.2

62

min0 1 2 3 4

mAU

0

500

1000

1500

DAD1 B, Sig=214,16 Ref=360,100 (20140321\501000035.D)

0.3

25

0.4

31 0

.490

0.7

00 0

.746

1.2

64

1.8

26

min0 1 2 3 40

20000

40000

60000

80000


0.9

06

min0 1 2 3 4

20000

40000

60000

80000

100000


0.1

11

0.2

73

0.6

70

0.8

33

1.0

19

1.7

00

2.0

42

2.9

94

3.1

32

3.2

53

3.5

81

3.7

91

4.3

01

4.5

36

MS Spectrum

m/z100 200 300 400 500 600 700 800 900

0

20

40

60

80

100

*MSD1 SPC, time=0.649:1.087 of D:\DATA\DDDCSYN\20140321\501000035.D MM-ES+APCI, Pos, Scan, Frag: 70

Max: 17840

504

.2

524

.1

502

.1 5

02.2











BioMedomics图章

r - MedKoo · 2020. 11. 1. · CO1686-DA NMR analysis\rSolvent = DMSO-d6 MedKoo Cat#:205796A\rName:...

Documents

Transcript of r - MedKoo · 2020. 11. 1. · CO1686-DA NMR analysis\rSolvent = DMSO-d6 MedKoo Cat#:205796A\rName:...