Engineen and Inc. GeoEnvironmental, GZA l · Public Service of New Hampshire Bow, New Hampshire...

AR-1311 GZA

Inc GeoEnvironmental

Road Harvey 380 Manchester

Hampshire New 03103-3347 603-623-3600

9463 -624-603FAX wwwgzacom

l

middot 2011 16 December 04002930700 No File

Daigneault Arny Coordinator Pretreatment

Utility Wastewater Regional Lowell (Rte-110) Blvd St First 451

1850 O Massachusetts Lowell

Analysis Monitoring Baseline Re 2011 16 December through 2011 1 October

Station Merrimack Hampshire New of Service Public

Hampshire New Bow

Daigneault Ms Dear

Engineen and

Scientists

Inc GeoEnvironmental GZA(PSNH) Hampshire New of middotServicePublic of behalf On e Baselinthe with (SMR) Report Self-Monitoring attached the submit to pleased is (GZA)

11 2016 December through 2011 1October d periothe for BMA) (ysis lAnaonitoring Mthe by PSNH to issued (IDA) Authorization Discharge Interim the with accordance in

2011 28 September dated (Utility) Utility Wastewater Regional Lowell

RESULTS ANALYTICAL WASTEWATER

month last the during Station Merrimack at conducted was program sampling wastewater A the satisfy To Technologies Water Siemens provider system treatment the and GZA by

samples IDA PSNH the of 2 Page on found requirements Analysis Monitoring Baseline data analytical of sets ete complTwo process treatment e thof end the at collected were

As days arate o middot obtaTned samples representative from iled com were on obtained were samples grab only Sheet attached the in erenced re ummary

a on collected were sample grab a and sample composite a both and days separate three those on generated wastewater the of representative were samples four All day fourth

days

by analyzed and protocol chain-of-custody under shipped were samples wastewater The Seattle of Sciences Global Frontier Hampshire New Concord of Inc Analytical Eastern

Wisconsin Rothschild of Services Analytical Enviroscan and Washington

summarized and Reports Data Analytical attached the in presented are results Analytical the within were concentrations pollutant that indicate results The Tables attached the in

Limits Discharge Sewer Local

Inc GeoEnvironmental GZA 2011 Copyrightcopy

An Equal Opportunity EDjgtIOyer MFNH

Lowell Regional Wastewater Utility December 16 2011 File No 04002930700 Page3

Should you have any questions concerning this report please do not hesitate to contact me at (603) 232-8744

Very truly yours

GZA GEOENVIRONMENTAL INC

Ronald A Breton PE Principal

RABrkl P04Jobs0029300s04002930700WorlltSAMPLNG AND REPORTNGIREPORTSLowellBMA REPORlFINAL 29307 LRWU CVR LTR 121611doelt

Attachments SMR Summary Sheet Tables Analytical Data Reports

LOWELL REGIONAL WASTEWATER UTILITY Industrial Sewer User Self-Monitoring Report Summary Sheet

Facility Information Company Name Public Service of New Hampshire - Merrimack Station

Facility Address ___= R=oad _____ Permit No IDA97Rimiddotver _ ________ -=------shy

Facility Contact --H=a=ro=ldK=eyesL___________ Telephone (603) 224-4081

-----UseA$eparate Summary SheetFor Each Monitoring Point----shy

Monitoring Report Monitoring Point At the end ofthe treatment process Submittal Date December 16 2011 Reporting Period circle applicable) ( Baseline ) Annually Semi-Annually Quarterly Monthly Re-Sample

Reporting Period Start Date October 1 2011 Reporting Period End Date __Dece=m=be~r16-2=0c11-shy

Sample Analysis Certified Analytical Lab Eastem Analytical Inc Enviroscan Analytical Services

Authorized Rep Lorraine Olashaw Bruce Schertz Certification No _1=0=12L1--0=0317----~shy

Analytical Sub-Contractor Frontier Global Sciences Certification No E87575--=-=---- - - - shy

Sample CoUection Sampler (labSelfOther) Paul Pepler (GZA) JeffGagne (EAi) Jim Ash (Siemens)

Sample Types) cirde all that apply) f Grab Time Composite Flow Composite

1) 111711 2) 113011----- (1) 1030am (2) Grab Sampling Sample Date _______i(3L)1207--11---- - Sample Time ____10=30=a=m==(3L-)2=pm=-shy

(1) 616 (2) 696

pH (Standard Units) _ (3)L--7 _ Instantaneous Flow Rate (GPM) unknowni 1c3

Composite Sampling Start DateTime Stop DateTime __120~5_11___120_120411 1200 pm _ 0=pm_

No Aliquots _2_4___ Aliquot Volume 800 mL ___ --9_ ___ _ __~__ Sample Volume _1 2 l ___

Flow Data Sampling Interval Volume (Gal) _ ___ = Daily Flow Rate (GPO)unkno=wn_ Variable but lt70000 gpd

Monitoring Period Industrial Wastewater Flow (Gal) ------32=3=2=-=-00___ [ J Meter [ xJ Estimate November30

Monitoring Period Start Date 20~11=------ Monitoring Period End Date December 16 2011

Refer to Self-Monitoring ReportInstructions for details on completing this SMR Summary Sheet LRWWU Use Only Self-Monitoring Report Summary Sheet of 2

TABLES

SUMMARY OF BASELINE MONITORING ANALYTICAL RESULTS METALS

Public Service ofNew Hampshire Merrimack Station

Bow New Hampshire

LOWELL SEWER RESULTS RESULTS PARAMETER DISCHARGE

LIMITS (mgL)

125lOll (mgL)

1272011 Aluminum 2469 lt 00140 lt 020 Antimonv - lt 0032 lt 001 Arsenic 0556 lt 0010 000403 Barium - 0154 022 5 n111ium - lt 090 lt001 Cadmium 0056 lt 00017 lt 001 Chromiumffi 8108 lt 000160 (Ill) lt 001 Coooer 3124 00085 lt001 Lead 0857 lt0016 lt 001 Mercurv 0004 00000067 00000056 Nickel 1541 lt 0003 ltOOl Selenium - 0089 0120 Silver 0053 lt 0006 lt001 Thallium - 0019 lt 001 Zinc 4959 lt0005 ltOo

GZA GeoEnvirorunental Inc ~ oll~JOO~D40029J0700WodtSAMPl1NO AND llEPORT[N(JIOATA RESUITS 12l61 1xltdowdlmet December 16 2011

__flAA____________e_a_s_te_rn_a_n_a_ly_t_i_c_a_l__

Paul Pepler

GZA GeoEnvironmental Inc (NH)

380 Harvey Road

Manchester NH 03103

Subject Laboratory Report Eastern Analytical Inc ID 105347

Client Identification Wastewater Analysis-Weekly Date Received 11172011

Report revisionreissue Revision replaces report dated 112911

Revision information The parameter list on this report has been revised

Dear Mr Pepler

Enclosed please find the laboratory report for the above identified project All analyses were performed in accordance with our QAQC Program Unless otherwise stated holding times preservation techniques container types and sample conditions adhered to EPA Protocol Samples which were collected by Eastern Analytical Inc (EAi) were collected in accordance with approved EPA procedures Eastern Analytical Inc certifies that the enclosed test results meet all requirements of NELAP and other applicable state certifications Please refer to our website at wwweailabscom for a copy of our NELAP certificate and accredited parameters

The following standard abbreviations and conventions apply to all EAi reports Solid samples are reported on a dry weight basis unless otheiwise noted lt less than followed by the reporting limit gt greater than followed by the reporting limit R Recovery

Eastern Analytical Inc maintains certification in the following states Connecticut (PH-0492) Maine (NH005) Massachusetts (M-NH005) New HampshireNELAP (1012) Rhode Island (269) and Vermont (VT1012)

The following information is contained within this report Sample Conditions summary Analytical ResultsData Quality Control data (if requested) and copies of the Chain of Custody This report may not be reproduced except in full without the the written approval of the laboratory

If you have any questions regarding the results contained within please feel free to directly contact me or the chemist(s) who performed the testing in question Unless otherwise requested we will dispose of the sample(s) 30 days from the sample receipt date

We appreciate this opportunity to be of service and look foiward to your continued patronage

Sincerely

middot 12 f5 r q Lorraine Olashaw Lab Director Date of pages (excluding cover letter)

~ Wtl1ilabsc m

middotl

LABORATORY REPORT EAi ID 105347

Client GZA GeoEnvironmental Inc (NH)

Client Designation Wastewater Analysis-Weekly

Sample ID Wastewater

Lab Sample ID 10534701

Matrix aqueous

Date Sampled 111711

Date Received 111711

Units ugn

Date of Analysis 111811

Analyst KJP

Method 624

Dilution Factor

Chloromethane lt5 Vinyl chloride lt2 Bromomethane lt2 Chloroethane lt5 Trichlorofluoromethane lt5 Acrol-ein lt50 Acetone lt 50 11-Dlchloroethene lt 1 Methylene chloride lt5 Carbon disulfide lt5 Acrylonitrile lt 50 Methyl-t-butyl ether(MTBE) lt 10 trans-12-Dichloroethene lt2 Vinyl acetate lt 10 1 1-Dichloroethane lt2 cis-1 2-Dichloroethene lt2 2-Butanone(MEK) lt 10 Chloroform lt2 1 1 1-Trichloroethane lt2 Carbon tetrachloride lt2 Benzene lt 1 12-0ichloroethane lt2 Trichloroethene lt2 12-Dichloropropane lt2 Bromodichloromethane lt2 2-Chloroethylvlnylether lt2 4-Methyl-2-pentanone(MIBK) lt 10 cis-13-Dichloropropene lt2 Toluene 3 trans-13-0ichloropropene lt2 112-Trichloroethane lt2 2-Hexanone lt 10 Tetrachloroethene lt2 Dibromochloromethane lt2 Chlorobenzene lt2 Ethyl benzene lt 1 mp-Xylene lt 1 o-Xylene lt 1 Styrene 4 Bromoform lt2 1122-Tetrachloroethane lt2 13-Dichlorobenzene lt 1 14-Dichlorobenzene lt 1 12-Dichlorobenzene lt1 4-Bromofluorobenzene ( surr) 92R 12-Dichlorobenzene-d4 (surr) 102R Toluene-dB (surr) 98R

eastern analytical inc wwweailabscom Phone (603) 228-0525 2






Matrix aqueous

Date Sampled 111711 Date Received 111711

Units ugf

Date of ExtractionPreparation 111711


Analyst JMR Method 625rnod

Dilution Factor 1

Di-n-butylphthalate lt5 Butylbenzylphthalate lt1

Naphthalene lt1

Acenaphthene lt1

Fluoranthene lt1

Benzo[a]anthracene lt1

Benzo[k]fluoranthene lt1

Dibenz[ah)anthracene lt1 Benzofghi]perylene lt1

Phenol-d6 (surr) 26R

Carbazole lt 1 Dimethylphthalate lt 1 Diethylphthalate lt 1

bis(2-Ethylhexyl)phthalate lt5 Di-n-octylphthalate lt 1 Dlbenzofuran lt 1

2-Methylnaphthalene lt 1 Acenaphthylene lt 1

Fluorene lt 1 Phenanthrene lt 1 Anthracene lt 1

Pyrene lt 1

Chrysene lt 1 Benzo[b]fluoranthene lt 1

Benzo(a]pyrene lt 1 lndeno(123-cd]pyrene lt 1

2-Fluorophenol (surr) 38R

246-T ribrornophenol (surr) 59R Nitrobenzene-05 (surr) 69R 2-Fluorobiphenyl (surr) 66R p-Terphenyl-014 (surr) 69R






Lab Sample ID 10534701 Matrix aqueous Date Sampled 111711 Date Received 111711

Units ug1 Date of ExtractionPrep 111711

Date of Analysis 111711 Analyst JW Method 608

Diluffon Factor 1

PCB-1016 lt03 PCB-1221 lt 03 PCB-1232 lt 03 PCB-1242 lt03 PCB-1248 lt 03 PCB-1254 lt 03 PCB-1260 lt 03 TMX (surr) 88R DCB (surr) 94R





Sample 10 Wastewater


Matrix aqueous

Date Sampled 111711 Analytical Date of

Date Received 111711 Matrix Units Analysis Method Analyst

Molybdenum lt 0005 AqTot mgL 111711 2008 DS


___AAA_____________e_a_s_t_e_r_n_a_n_a_l_y_t_ic_a_l__

Paul Pepler


380 Harvey Road

Manchester NH 03103

Subject Laboratory Report

Eastern Analytical Inc 10 105645

Client Identification Merrimack Station Wastewater Analysis - Weekly



Revision Information The parameter list on this report has been revised

Dear Mr Pepler

Enclosed please find the laboratory report for the above identified project All analyses were performed in accordance with our QAQC Program Unless otherwise stated holding times preservation techniques container types and sample conditions adhered to EPA Protocol Samples which were collected by Eastern Analytical Inc (EAi) were collected in accordance with approved EPA procedures Eastern Analytical Inc certifies that the enclosed test results meet all requirements of NELAP and other applicable state certifications Please refer to our website at wwweallabscom for a copy of our NELAP certificate and accredited parameters

The following standard abbreviations and conventions apply to all EAi reports Solid samples are reported on a dry weight basis unless otherwise noted lt less than followed by the reporting limit gt greater thanbull followed by the reporting limit R Recovery




We appreciate this opportunity to be of service and look forward to your continued patronage

Sincerely

L 15 I Lorraine Olashaw Lab Director Date of pages (excluding cover letter)

11middot111cailabc11m

LABORATORY REPORT EAi I0 105645


Cl[ent Designation Merrimack Station Wastewater Analysis - Weekly



Matrix aqueous

Date Sampled 113011


Units ug1


Analyst KJP

Method 624 Dilution Factor

Chloromethane lt5 Vinyl chloride lt2 Bromomethane lt2 Chloroethane lt5 T richlorofluoromethane lt5 Acrolein lt50 Acetone lt50 1 1-Dichloroethene lt 1 Methylene chloride lt5 Carbon disulfide lt5 Acrylonitrile lt 50 Methyl-t-butyl ether(MTBE) lt 10 trans-12-Dichloroethene lt2 Vinyl acetate lt 10 1 1-Dichloroethane lt2 cis-12-Dichloroethene lt2 2-Butanone(MEK) lt 10 Chloroform lt2 1 1 1-Trichloroethane lt2 Carbon tetrachloride lt2 Benzene lt1 12-0ichloroethane lt2 Trichloroethane lt2 12-Dlchloropropane lt2 Bromodichloromethane lt2 2-Chloroethylvinylether lt2 4-Methyl-2-pentanone(MIBK) lt 10 cis-13-Dichloropropene lt2 Toluene 2 trans-13-Dichloropropene lt2 11 2-Trichloroethane lt2 2-Hexanone lt 10 Tetrachloroethene lt2 Dibromochloromethane lt2 Chlorobenzene lt2 Ethylbenzene lt1 mp-Xylene lt 1 o-Xytene lt1 Styrene lt 1 Bromoform lt2 1 122-Tetrachloroethane lt2 13-Dichlorobenzene lt 1 14-Dichlorobenzene lt 1 12-Dichlorobenzene lt 1 4-Bromofluorobenzene (surr) 96R 12-Dichlorobenzene-d4 surr) 102R Toluene-dB (surr) 97R



Client GZA GeoEnvlronmental Inc (NH)

Client Designation Merrimack Station Wastewater Analysis - Weekly



Matrix aqueous


Units ug1

Date of ExtractionPreparation 111301 1

Date of Analysls 113011

Analyst JMR Method 625mod

Dilutlon Factor 1

Carbazole lt 1


Naphthalene lt1

Pyrene lt1

Benzo[a)pyrene lt1

Benzo[g hijperylene lt1

Phenol-dB (surr) 27R

Dimethylphthalate lt 1 Diethylphthalate lt 1

bis(2-Ethylhexyl)phthalate lt5 Di-n-octylphthalate lt 1 Dibenzofuran lt 1

2-Methylnaphthalene lt 1 Acenaphthylene lt 1 Acenaphthene lt 1 Fluorene lt 1 Phenanthrene lt 1 Anthracene lt 1 Fluoranthene lt 1

Benzo[ajanthracene lt 1 Chrysene lt 1 Benzo[b]fluoranthene lt 1 Benzo[kfluoranthene lt 1

lndeno[123-cd)pyrene lt1 Dibenz[ah]anthracene lt 1


246-Tribromophenol (surr) 53R Nitrobenzene-05 (surr) 65R 2-Fluoroblphenyl (surr) 55R p-Terphenyl-014 (surr) 79R







Matrix aqueous

Date Sampled 113011 Analysis

Units Date Time Method Analyst Date Received 113011

Solids Suspended lt5 mgL 113011 815 2540D DLS Fluoride 6 mgL 120111 245 3000 KL Cyanide Total lt 001 mgL 120111 845 4500CNE KJR Total Nitrogen 130 mgL 120111 12304500NorgC KL BOD lt6 mgL 113011 1440 52108 SKC coo 110 mgL 113011 1400 H8000 SKC Total Phenols lt 03 mgL 120111 900 4201 JGC pH 71 SU 113011 1400 4500H+B JL

Total Nitrogen is determined by a calculation derived from method EPA 3532 and Standard Methods 4500orgCNH3D Total Phenols Reporting limit is elevated as a result of sample dilution due to matrix interference

eastern analytical inc wwweailabscom Phone (603) 22~525 6

CHAIN-OF-CUSTODY RECORD ~I eastern analytical inc 105645 coprofessional laboratory services

DateTime Composites need start

Sample IDs and stop dateslimes Matrix Parameters and Sample Notes ~ntatners

cdWastewater F ODfSYCODCyanTFpHTPhenols~ffSSN624AE6250G1664ICPMets-AI-Sb-As-Ba Be ~ 1uI~ ~~~ -MR-Mo gtH So Ag Tl a CabullN~bull~~~i02ltoakTlt21S03GhlolT ~ 1D3o

rtt bull bull Dissolved Sample Field FilterefAllCll Sampler confirms ID and parameters are accurate crce preservetvels HCL HNO HSO NaOH MEOH Naso ICE 0

S(R IJ ~MGmiddot lM~~M ~~ STA-n1gt0 ql ~vG1( lt2t1degA)

~ Nmiddot 61)6G

efl I ~ c 1_ -l 5311 h-irINum9 cii +-1(1) of euV~1) V~~i 11

-4 $1gtu-lt J (~ fi-l j ~JJ~~ w- 11Clvlt-l l l~r ~~rs CV~J fv- )VAiv1( 1y~ecYe-e~Cl

~- (ttio ~ J~S~~L

Please ensure this auto COC is accurate adheres to permit or sampling requirements for this sampling event and modify as necessary

EAi Project ID 3902

Project Name Wastewater Analysis-Weekly

State NH

Client (Pro Mgr) Paul Pepler

Customer GZA GeoEnvironmental Inc (NH)

Address 380 Harvey Road

City Manchester NH 03103

Phone 623-36(10 Fax 624-9463 (37)

EmaliMdress paulpepergzacom

~ f1-j R rtl O tiResults Needed by Preferred date M~l epo ng P ons

I IJntaa hn11t ndegrn lAr tbull I JnArlol I lmlh Allllnn lnfn I 181 HC 18 EDD PDF 18 EDD email 18 PDF prelim NO FAX D e-mail Login Confirmation ONO FAX

tVt-_

~ ~lSeb ~G~bullY2-l- ) f- umicrog-~r l 1s S~R--tlt1--(

A-1 li-JCi-u~r S ~iqU0-l rev-shyQC deliverables ~ middot

DA DA+ 1818 OB+ DC D~C i11[

Eastern Analytical Inc 25 CheneI Dr Concord NH 03301 Phone (603) 228-0525

bull$

Relinquished by

PONumber 02259252

Quote No 1009476

Temperature l3 $degdegC Ice present Yes D No ~

i ~~pllt-

Relinquished by DateTime Received by

1-800-287-0525 Fax (603)228-4591

SAMPLE CONDITIONS PAGE EAi ID 105962

Client Northeast Utilities

Client Designation Merrimack Station

Temperature upon receipt (degC) 45 Received on ice or cold packs (YesNo) y Acceptable temperature range (degC) 0-6

Date Date Sample Dry Lab ID Sample ID Received Sampled Matrix Weight ExceptionsComments (other than thermal preservation)

10596201 Treat Tank 121711 12711 aqueous Adheres to Sample Acceptance Policy

10596202 Treat Tank Field Blank 12711 12711 aqueous Adheres to Sample Acceptance Policy

Samples were properlypreserved and the pH measured when applicable unless otherwise noted Analysis ofsolids for pH Flashpoint lgnitiblity Paint Filter Corrosivity Conductivity and Specific Gravity are reported on an middotas received basis Alf results contained in this report relate only to the above listed samples

References include 1) EPA 6004-79-020 1983 2) Standard Methods for Examination ofWater and Wastewater lnorganics 19th Edition 1995 Microbiology 2oth Edition 1998 3) Test Methods for Evaluating Solid Waste SW 84~ 3rd Edition including updates VA and VB 4) Hach Water Analysis Handbook 2nd edition 1992


414 Ponti11s Ave North Seattle WA 98109 Ph 206-622-6960 Fx 206-622-6870

FRONTIERmiddoto GLOBAL SCIENCES

ANALYTICAL REPORT FOR SAMPLES

Laboratory Frontier Global Sciences Inc SDG

Client Eastern Analytical Inc Project Merrimack Station

Sample ID Laboratory ID Matrix Date Sampled Date Received

Treat Tank 1112097-0l Water 07-Dec-ll 1400 08-Dec- l l 0640

T T Field Blank 1112097-02 Water 07-Dec-ll 1400 08-Dec- l l 0640

Treat Tank 1112097-03 Water 07-Dec-l l 1400 08-Dec-ll 0640

T T Field Blank l 112097-04 Water 07-Dec-ll 1400 08-Dec- l l 0640

Frontier Global Sciences Inc

-- - ~ ~

Liz Siska Project Manager

The results in this report onfy apply to the samples analyzed in accordance with the chain ofcustody document This analytical report must be reproduced in its entirety

Page 1 of 17 111211O Final Report

3

FRONTIEmiddotRI

GLOBAL SCIENCES

414 Pontius Ave North Seattle WA 98 l09 Ph 206-622-6960 Fx 206-622-6870

CHAIN OF CUSTODY FORMS

J

8

9

10

ll

Received By

Sample Disposal By signing you deda re that you agree with FGS terms and conditions and tha D Return (shipping fees may apply) you authorize FGS to pe_rform the spedtled analyses 0 Srandard Disposal - 30 Days after report o Reraln for __ weeks after report (storage fees may appty) Customer Approval Date

Frontier Global Sciences Inc The results in this report only apply to the samples analyzed in accordance wllh the chainofcustody document This analytical report must be reproduced in its entirety


Page 3 of17 1112110 Final Report

5

FRONTfEgmiddotmiddot CLOBAL SCtENCES

414 Pontius Ave North Seattle WA 98109 Ph 206-622-6960 Fx 206-622-6870

Mercury Analytical Results

Matrix Water Preparation BrCl Oxidation

Sample Name Result MRL Units Batch Prepared Seaueoce Analyzed Method Notes

T T Field Blank ND 050 ngL Fll2077 120811 IL09012 120911 EPA 163IE u Treat Tank 563 202 ngL Fl12077 1208ll IL090l2 120911 EPA 1631E



The resuJs in this report onlyapply to the samples analyzed in accordance with the chain ofcustody document This analytical report must be reproduced in its enJirety

Page Sof 17 111211 O Final Report

7

FRONTI ER C LO BA L S C l E N C E S


Selenium Analytical Results

Matrix Water Preparation Closed Vessel Nitric Oven Digestion

Sample Name Result lMRL Units Batch Prepared Seauence Analyzed Method Notes

T T Field Blank ND 060 microgL fl 12074 120811 IL09004 120911 FGS-054 u Treat Tank 120 600 microgL Fl 12074 120811 IL09004 120911 FGS-054



The results in this report only apply o the samples analyzed in accordance with Jhe chain ofcustody document This analytical report must be reproduced in its entirety

Page 7 of 17 1112110 Final Report

9

f RQNTJ El GLOBAL SCIENCES

414 Pontius Ave North Seattle WA 98109 Ph 206-622-6960

Fx 206-622-6870

MATRIX SPIKE I MATRIX SPIKE DUPLICATE RECOVERY AND RPD

SOURCE 1112097-03

Matrix Water Sequence 1L09004

Batch fll2074 Lab Number Fll2074-MSMSD1

Preparation Closed Vessel Nitric Oven Digestion

Sample Spike MS MS

Aoalyte Concentration

(microgL) Added (microgL)

Concentration (microgL)

Recovery

RecoveryLimits Method Notes

Arsenic 403 50030 893 980 85 - 115 FGS-054

Selenium 1196 49990 1267 141 59 - 149 FGS-054

Spike Added

MSD Concentration

MSD Oo Recovery RPD

Analyte (microgL) (microgL) Recovery RPD Limits Limit Method Notes

Arsenic 50030 877 947 184 85 - 115 20 FGS-054 Seleniwn 49990 1226 587 329 59- 149 20 FGS-054 QM-02

~



The results in this report only apply to the samples analyzed in accordarue with the chain ofcustody document This analytical report must be reproduad In its entirety

Page9 of 17 111211 O Final Report

1 1


FRONTI _E~ GLOBAL SCIENCES

MATRIX SPIKE MATRIX SPIKE DUPLICATE RECOVERY AND RPO

SOURCE 1112089-17

Matrix Water Sequence IL09012

Batch Fl 12077 Lab Number Fl I2077-MSMS02

Preparation BrCl Oxidation

Sample Spike MS MS Concentraticon Added Concentration RecoveryAnalyte (ngL) (ngL) ngL) Recovery MethodLimits Notes

Mercury 6868 10200 1680 973 71 - 125 EPA 163JE

Spike MSD MSD Added Concentration Recovery RPD

RPD Limits Limit Method Analyte (ngLJ (ngL) Recovery Notes

Mercury 10200 1572 868 660 71 - 125 24 EPA 1631E



The results in this report only apply to the samples analyzed in accordance with Jhe chain ofcustody document This analytical report must be reproduced in its entirety


13

FRONmiddotTJER~ GLOBAL SCIENCES


LABORATORY CONTROL SAMPLE LABORATORY CONTROL SAMPLE DUPLICATE

RECOVERY AND RPD

Matrix Water Sequence lL09004

Batch Fl 12074 Lab Number Fll2074-BSBSD1

Preparation Closed Vessel Nitric Oven Digestion LCSSoorce Blank S11ike

Spike LCS LCS Added Concentration middot Recovery

Analyte (microgL) (microgL) Recovery Limits Method Notes Arsenic 50030 484 968 85 - 115 FGS-054 Selenium 49990 487 974 59 - 149 FGS-054

Spike LCSD LCSD Added Concentration Oo Recovery RPD

Analyte (microgL) (microgL) Recovery RPD Limits Limit Meth-0d Notes Arsenic 50030 471 942 275 85 - 115 20 FGS-054 Selenium 49990 543 109 109 59 - 149 20 FGS-054



The results in this report only apply to the samples analyzed in accordance with the chain ofcustody document This analytical report must be reproduced In its entirety

Page 13 of 17 111211 O Final Report

15


FRONTIER~ G L O B A L S C l E N C E S

PREPARATION BLANKS

Matrix Water Sequence 1109004

Instrument ICPMS-6 Preparation Closed Vessel Nitric Oven Digestion

Lab Sample ID Analyte Found MRL Units Batch Method Notes Fl 12074-BLKI Arsenic -005 015 microgL FII2074 FGS-054 u Fl 12074-BLKl Selenium -001 060 microgL Fl12074 FGS-054 u



The results in this report only apply to the samples analyzed in accordance with the chain ofcustody document This analytical report must be reproduced in its entirety


17 middotmiddot

FRONTIEl( GLOBAL SCIENCES


Notes and Definitions

U Analyte included in the analysis but not detected

QM-02 The MS andor MSD recoveries outside acceptance limits due to spike concentration less than I times the sample concentration Tbe batch was accepted based on LCS and LCSD recoveries within control limits and when analysis permits acceptable ASASD

QB-04 The blank was preserved to 2 BrCl rather than l The control limit for blanks preserved to greater than 1 BrCJ is the preservation percentage multiplied by the MRL

AS This MS andor MSD is an analytical spike andor an analytical spike duplicate

DET Analyte Detected

MRL Minimum Reporting Limit

ND Analyte Not Detected at or above the reporting Jjmit

wet Sample results reported on a wet weight basis

dry Sample results reported on a dry weight basis

RPD Relative Percent Difference

RSD Relative Standard Deviation





19

Ii Io

__JJA(i___________middot ~ middot middotmiddot~~middot~ ~ ~

_e_a_s_t_e_r_n_a_n_a_ly_t_i_c_a_l__

Arthur Auclair

Northeast Utilities 97 River Road

Bow NH 03304


Eastern Analytical Inc ID 105963

Client Identification Merrimack Station


Dear Mr Auclair

Enclosed please find the laboratory report for the above identified project All analyses were performed in accordance with our QAQC Program Unless otherwise stated holding times preservation techniques container types and sample conditions adhered to EPA Protocol Samples which were collected by Eastern Analytical Inc (EAi were collected in accordance with approved EPA procedures Eastern Analytical Inc certifies that the enclosed test results meet all requirements of NELAP and other applicable state certifications Please refer to our website at wwweailabscom for a copy of our NELAP certificate and accredited parameters

The following standard abbreviations and conventions apply to all EAi reports Solid samples are reported on a dry weight basis unless otherwise noted lt less than followed by the reporting limit gt greater than followed by the reporting limit R Recovery

Eastern Analytical Inc maintains certification in the following states Connecticut (PH-0492) Maine NH005 Massachusetts (M-NH005 New HampshireNELAP (1012) Rhode Island (269) and Vermont (VT1012)




Sincerely

12~ Lorraine Olashaw Lab Director Date of pages (excluding cover letter)

1middot1wltailabscltgtm

Ill I

QC REPORT EAi ID 105963 11Jul Client Northeast Utilities


Date of

Parameter Name Blank LCS LCSD Units Analysis Limits RPO Method

Aluminum lt005 11 (103 R) mgL 12911 85 - 115 20 2008 Antjmony lt 0001 11 (107 R) mgL 12911 85-115 20 2008 Arsenic lt 0001 10 (102 R) mgL 12911 85 -115 20 2008

Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008

Beryllium lt 0001 11 (114 R) mgL 12911 85 - 115 20 2008 Cadmium lt 0001 097 (97 R) mgL 12911 85-115 20 2008

Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008

Mercury lt 00001 00010 (101 R) mgL 12911 85 - 115 20 2008 Nickel lt 0001 095 (95 ooR) mgL 12911 85 - 115 20 2008

Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008

Samples were analyzed within holding times unless noted on the sample results page Instrumentation was calibrated in accordance with the method requirements The method blanks were free of contamination at the reporting limits The associated matrix spikes andor Laboratory Control Samples met the above stated criteria Exceptions to the above statements are flagged or noted above or on the QC Narrative page Flagged analyte recoveries deviated from the QAQC limits

eastemiddotrn analytical inc wwweaifabscom Phone (603) 228-0525 6

voe svoc TCLP M ETALS INORGANICS M ICRO OTHER

i ii i I i - ~ Cgt0 vi I 5 0SAMPLING ei i

C

J a z l uJ 0 ~ ~ ~ -~ ~ ~

D ATE TtM E J ii ~ ~ Ill I

z uJ i-0

IF COMPOSITE LU C

~ u

INDICATE 8 0 TH X i- ~ START amp FINISH cc Ill

S A MPLE ID ~ lt a ~-shyD ATETIME I t C C ww-r l11Ct _ 1h11 l 4degL1gt Imm r ww-r ~Jshy ln711 i gt-00 Mi C

11ATklX A-All S-SOII GW-GkOUND WAm SW-SUkFACE WATER DW-DR INIING WATER WW-WASTE WATEl

Pam1m1vr H-HCLmiddot N-HHO S-HSO Na-NaOHmiddot H-HEOH

PROJECT MANAGER AcUuC Alaic CoMPANY _H__a~ eacf UtiHmiddotfrf ADD AESS 97 t-ivee ampI CITT f)middotmiddotnJ STATE 1Jd PHO NE 6o~ ~4 - to~ FAX (6~ Jj-f_olttJ

~E ~ si~ 1

= ~ l ~ al

J g

jltgt - Eil i2~ 2 s~ ~

0 c ~ E z- i - g Q ~ t

~ e ~ 0 ~ i c 0 pound I g~ I E o z

ltgt C E - ~ C ~ z r

~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~

~ Z s 5 li Ii NOTES5j ei 0

sectI a i i HeOHV1At I l5

r2 it _ iliJ I-I 7L 2

IF01 lJC HAIN-OF-CUSTODY RECORD 105963Page of BOLD F IELD S REQUIRED PLEASE CIRCLE R EQUESTED A NALYSIS

ZIP 0 gtSO t( EXT___

E-HAlt --------- --- - - - ---- shySm NANE MeojQ( I sfz4lton PROJECT =------------------- shySTATE ~ MA ME VT OTHER ________

REGULATORY PROGRAM NPDES lGP POTW STOlltWATEk Ol GWP 01t FUND 8ROWHIIElD OR 0THEl _________

Quon _________ PO_middot------ shy

DATE NEEDED Zlt1(11 0TEKP L gt (

QAQC REPORTINGJ_~VEL

A (s C

OR

PRESUMPTIVE CERTAINTY

R EPORTING OPTIONS ICE1 cfil) No PUUKI YES OR NO middot Ir YEI Fu oa PDF

ELECTRONIC OPTIONS

Ho FAX E-NAIL PDF EQUIS

RELINQUISHED BY DATE TIKE RECIITEDBY

METALS 8 RCRA 13 PP fE HN Pl Cu

OTHER t1UALI _ _________

Dmomo HETAU FIELD FllTEUDI Yll No

NOTES IE SmlAl DETECTION LIKITBlttlHG INFO IF Dmum)

Sm HiITOlY___________

SUSPECTED (OHTAIIIIIAIION_ _______

FIELDREADINGS ___ ___ ___ _ _RELINQUISHED BY DATE TIKE RECEITED BY

2s CHENELl 011ive I C0Nco110 NH ono1 I TEL 60J22sos25 I 1soo2s1os25 I FAX 60J22S4S91 I E-MA11 cuSToMe11_se11v1cEeA1LascoM Iwww EAllAescOMEIeas~~~~nc (WHITE ORIGINAL GREEN PROJECT MANAGER)

SIEMENS Siemens Industry Inc 181 Thom Hill Road Warrendale PA 15086

Attn Frank Sassaman

PROJECT NO PSNH Merrimack Station PerformanCE REPORT NO 1112078 DATE RECD 120611 1124 REPORT DATE 1214111639 PREPARED BY BMS

Sample ID Effluent Mallix Waste Water Sample OatefTlme 120511 1600 lab No 1112078-02

Calculated Trivalent Chromium

Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV

EPA1664A Hexane Extractable Material (HEM) 160 mgL uo 466 1 J 120811 KAM

EPA iQQ7 bull T2lil Total Aluminum

Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB

Total lead ND mgL 0016 0053 S1L S2L 1208111 OJB

Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17

SIEMENS 1 Il-Corfc)any Name

ampiMerS middot IA- rhmiddot1l~ Rq)Olt~~

)5f I Thcfl rlJI Rd

liNolcMdre5$

Motte Omlq ~ oo_____

Wl$Pl(fA~sabjecnoUampC Y e Flaquo~Noeil5 Vbull (S) Stale _____

(lfYes111specff~or~ ~-----

Turnateund Rtquest l l Nomlal (108I Da)c)

~~bt~~Ubanolbull~IO~

WO No 1f cent~)d

~Onlv~~ DatefTine No ctCOll1aJner$

Como I Grab 5ampledeg

JO

gtltrJ 1s-1naa s-middotmiddotmiddot -9~h~5 11h00 )9-illil~ IIb00 middot ~ --li~S lt toa -o~ IJJs 1100-~l~ J hOOI s

-Agt1l --middot i Itoo 1

ITlimiddottev1f 2 Ir~rt f~tmiddotU~t 3 I +a ~ed~ middotl ~~-r~ rn~hdeg 1 ~- -r~~-~~

~CV11~~~~ctE~

RtonQUlshed By

PTojeltt Ps AUi Mtgtrr llccJ Stl__ ~ )r

~~PhoneFax Email middot fr~lt $lticMdeg-

~Orltletbull IIIMgtQCcinaitanc1 Phone No

I ~-~ bull middot- -~ Allaly$eS Rtque$led OefHMd by waac-1n gtmiddot-~

1 I I I I I --ConlOKmiddot ~~ -middoti~ ~~_ middot-jl-rAA-

I )IY( ~(Imiddot

~~ ~

$ell$0la middot middot - ~ middot-NAmiddot Recdonmiddotlcll bull Y middot N middot M(middot

~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r

Oa1e middot- Received Sy

ChairrofCustody ~IX) Record J-11 L middotr-4

~w-Tedlnologie$ 301 W MiltalyRd RolhSdllkl WI $4474 1-800-338-7226

i0 w l

A Enuiranmental 34 Dogwood Lane bull Middletown PA 17057 bull Phlgtne 717middot944middotS541 bull Fax 717middot944middot1430 bull wwwalsglobalcom

NELAP Certifications NJ PA010 NY 11759 PA 22-293 DoD ELAP A2LA 081801 State Certifications CT PH-0224 DE ID 11 GA 914 MA PAO 02 MD 128 LA 04162 VA 421 WY EPA Region 8 WV 343

ANALYTICAL RESULTS middot

Workorder 9940856 Low Level Hg 120611

Lab ID 9940856002 Date Collected 1252011 1700 Matrix Waste Water

Sample ID Hg B Eff Date Received 1262011 0955

Parameters Results Flag Units RDL Method Prepared By Analyzed By Cntr

METALS

Mercury Dissolved ND ngL 50 EPA 1631 12811 MNP 12811 1109 MNP A1 Mercury Total 67 ngL 50 EPA 1631 middot121811 MNP 12911 1243 MNP A2

Sample Comments

cz__~Ju__ Anna G Milliken Technical Manager

ALS Environmental Laboratory Locations Across North America canada Burlington middot Calgary bull Centre of Excellence bull Edmonton middot Fort McMurray middot FortStJohn bull Grande Prairie middot London bull Mississauga bull Richmond Hill middot Saskatoon bull Th11nder Bay

Vancolller Waterloo bull Winnipeg middot Yellowknife United States Onclnnatl bull Everett middot Fort Collins middot Holland middot Houston bull Middletown bull Salt Lake Oty middot Spring City bull York Mexico Monterrey

Report ID 9940856 -1292011 Page 4 of 11

IEnulronmental 34 Dogwood Lalle bull MiamptletowlI PA 17057 bull Phone 717middot944middotSS41 bull Fax 717middot944-1430 wwwalsgfobalcom

NELAPCertifications NJ PA010 NY 11759 PA 22-293 DoD ELAP A2LA08180J State Certifications CT PH-0224 DE ID 11 GA 914 MA PAO 02 MD 128 LA 04162 VA 421 WY EPA Region 8 WV 343

QUALITY CONTROL DATA


QC Batch MDIG34188 Analysis Method EPA 1631

QC Batch Method EPA 1631

Associated Lab Samples 9940856001 9940856002 9940856004

IMETHOD BLANK 924440

Parameter Result Qualifiers Units Reporting

Limit

Mercury Dissolved ND ngL 050

rLABORATORY CONTROL SAMPLE 924441 Ji

Parameter LCS

Result Qualifiers Units Spike Cone

LCS Rec

Rec Limits

Mercury Dissolved 45 ngL 5 902 71-125

MATRIX SPIKE amp MATRIX SPIKE DUPLICATE 924442

-~a R

Original Spike MS MSD MS MSD Rec Max Parameter Result Qualifiers Units Cone Result Result Rec Rec Limit RPD RPO

Mercury Dissolved 21 ngL 250 219 224 867 887 71-125 226 24

ALS Environmental Laboratory Locations Across Nonh America canada Burlington bull Calgary bull Centre ofExcellence bull Edmonton bull Fort McMurray bull Fort St John bull Grande Prairie bull London Mississauga bull Richmond HIii bull Saskatoon Thunder Bay

VancoUler Waterloo bull Winnipeg middot Yellowknife United States Cincinnati bull Everett middot FortCollins middot Holland middot Houston bull Middletown middot Salt Lake Oty bull Spring City middot York Mexico Monterrey

Report ID 9940856 -1292011 Page 7 of 11

Enuironmental 34 Dogwood Laoe bull Middletown PA 17057 bull Phone 717middot944middotSS41 bull Fax 717middot944middot1430 bull wwwalsglobalcom

NELAP Certifications NJ PAO 0 NY 11759 PA 22-293 DoD ELAP A2LA 081801 State Certifications CT PH-0224 DE ID 11 GA 91 4 MA PAO102 MD 128 LA 041 62 VA 421 WY EPA Region 8 WV 34 3

- -

~i---middot~N--L_-__-it-~--middot--1=gt___-~-~shy-- shy ---i-shy-~-----11 ~ j J 1shybull1pounddeg-bull-_---middotmiddotshy----+-bull-+Aqdeg-deg------4(1-J JJ

fylf~--u_____--1middot-+- +----~- shy bull-~ DD[l]O _ iiI--~ r

i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO

ALS Environmental Laboratory Locations Across North America ~ Burlington bull Calgay middot Centre ofExcellence bull Edmonton bull Fort McMurray bull Fort St John bull Grande Ptalrle bull London bull Mississauga middot Richmond Hill bull Saskatoon middot Thunder 8ay

Vancouver Waterloo middot Winnipeg middot Yenowimife United States Oncinnati middot Everett middot Fort Colampns bull Holland bull Houston bull Middletown middot SaltLake Oty bull Spring Crty middot York Mexico Monte~

Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy

A Enuironment al 34 Dogwood Lane bull Middletowrt PA 17057 bull Phone 117middot944middot5541 bull Fax 717middot944middot1430 bull wwwalsglobalcom

NELAP Certifications NJ PAOl O NY 11759 PA 22-293 DoD ELAP A2LA 081801 State Certifications CT PH-0224 DE ID 11 GA 914 MA PAOl 02 MD 128 LA 04162 VA 421 WY EPA Region 8 WV 343





Associated Lab Samples 9940856001 9940856002 9940856003 9940856004

IMETHOD BLANK 924444 -=shy

Reporting

Parameter Result Qualifiers Units Limit

Mercury Total ND ngL 050

ILABORATORY CONTROL SAMPLE 924445

LCS Spike LCS Rec

Parameter Result Qualifiers Units Cone Rec Limits

Mercury Total 47 ngL 5 948 71-125

MATRIX SPIKE amp MATRIX SPIKE DUPLICATE 924446 924447 9940856001

Original Spike MS MSD MS MSD Rec Max

Parameter Result Qualifiers Units Cone Result Result Rec Rec Limit RPO RPO

Mercury Total 107 ngL 250 241 241 921 921 71-125 0 24

ALS Environmental Laboratory Locations Across North America Canada Burlington bull Calgary bull Centre of Excellence bull Edmonton Fort McMurray bull Fort St John Grande Prairie London bull Mississauga Richmond Hill bull Saskatoon bull Thunder Bay

VancouverWaterloo Winnipeg Yellowknife United States Cincinnati bull Everen middot Fort Collins middot Holland middot Houston middot Middletown bull Salt Lake City bull Spring City middot York Mexko Monterrey

Report ID 9940856 - 1292011 Page 8 of 11

A Enulranmental 34 Dogwood Lane bull Middfetow11 fgtA 17057 bull Phone 717middot944middot5541 bull Fax 717middot944middot1430 1 wwwalsglobalcom


ANALYTICAL RESULTS



Sample ID Field Blank Date Received 1262011 0955

Parameters Results Flag Units RbL1bull Method Prepared By Analyzed By Cntr

METALS

Mercury Dissolved Mercury Total

054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments

0-2tu__ Anna G Milliken

Technical Manager

ALS Environmental laboratory Locations Across North America Canada Burlington Calgary Centre of Excellence middot Edmonton middot Fort McMurray bull Fort St John bull Grande Prairie bull London bull Mississauga Richmond Hill bull Saskatoon bull Thunder Bay

Vancouver Waterloo bull Winnipeg middot Yellowknife United States Cincinnati bull Everett middot Fort Collins middot Holland middot Houston middot Middletown middot Salt Lake Oty middot Spring City middot York Mexico Monterrey

Report ID 9940856 -1292011 Page 6 of 11

A Enulranmenlal 34 Dogwood Lane bull Middletown PA 17057 bull Phone 717middot944middotS541 bull Fax 717middot944middot1430 bull wwwalsglobalcom

NELAP Certifications NJ PAOT O NY 11759 PA 22middot293 DoD ELAP A2LA 081801 State Certifications CT PH-0224 DE ID 11 GA 914 MA PAOl 02 MD 128 LA 04162 VA 421 WY EPA Region 8 WV 343

December 9 2011

Mr Jim Fish Siemens Water Technologies Corp-PA 181 Thorn Hill Road Warrendale PA 15086

Certificate of Analysis

Project Name PSNH Merrimack Station FGD Workorder 9940856 Workorder ID Low Level Hg 120611 Purchase Order

Dear Mr Fish

Enclosed are the analytical results for samples received by the laboratory on Tuesday December 06 2011

The ALS Environmental laboratory in Middletown Pennsylvania is a National Environmental Laboratory Accreditation Program (NELAP) accredited laboratory and as such certifies that all applicable test results meet the requirements of NELAP

If you have any questions regarding this certificate of analysis please contact Susan Scherer (Project Coordinator) or Anna G Milliken (Technical Manager) at (717) 944-5541

Please visit us at wwwanalyticallabcom for a listing ofALS NELAP accreditations and Scope of Work as well as other links to Water Quality documentation on the internet

This laboratory report may not be reproduced except in full without the written approval of ALS Environmental

CC Mr Michael Riffe Mr Frank Sassaman

This page is included as part of the Analytical Report and

must be retained as a permanent record thereof

a__2LL2__ Anna G Milliken

Technical Manager

ALS Environmental Laboratory Locations Across North America Canada Surllngton Calgary bull Centre ofExcellence Edmonton middot Fort McMurrav bull Fort StJohn middot Grande Prairie London bull Mississauga bull Richmond Hill bull Saskatoon middot Thunder Bay

Vancouver Waterloo middot Winnipeg Yellowknif~ United States Cincinnati bull Everett middot Fort Collins middot Holland middot Houston bull Middletown bull Salt Lake City bull Spring City middot York Mexico Monterrey

Report ID 9940856 bull 1292011 Page 1 of 11

SIEMENS Qualifier Descriptions

S2L Second sample matrix spike recovery was low

S1L First sample matrix spike recovery was low

J Estimated concentration below l~boralory quanlitatlon level

COMP Completed

Definitions

ugll =Micrograms per Liter parts per billion (ppb)uglkg =Micrograms per kilogram =parts per billion (ppb) mgJI =Mllllgrams per liter = parts per million (ppm mgkg =Milligrams per kilogram = parts per mllllon (ppm)NOT PRES =Not Presentppth =Parts per thousand = Result outside established limitsmgm3 = Milligrams-per meter cubedngL = Nanograms perLiter= Parts per trilllon(ppt) gt = Greater Than

LOD =Limit of Detection (Ollullon Corrected) LOQ Limit of Quanlitation (Dilution Corrected) Reporting Limit LOQ (Dilution Corrected) ND = Not Detected COMP = Complete SUBCON =Subcontfacted analysis mv= millivolts pciL =plcocurles per Liter m[JL =milliliters per Liter mg =milligram When the word dry follows the units on the result page the sample results are dry weight corrected

LOOs and LOQs are dry weight corrected for all soils State ofWisconsin Methanol Soils for WI GRO WI except Wl GRO EPA 8021 and WI DNREPA 8260B DNREPA 8260B and EPA 8021 are reported to the LOQ methanol and WI DNR methylene chloride preserved soils being reported to the State of Wisconsin

(WNC) =The required Wisconsin DNR program certirication Is not held for this analyte

Page 12 of 17

- - --- --------

SIEMENS December 14 2011

Siemens Industry Inc 181 Thorn Hill Road Warrendale PA 15086

Attn Frank Sassaman

REPORT NO 1112078 PROJECT NO PSNH Merrimack Station Performance Test

Please find enclosed the analytical report including the Sample Summary Sample Narrative and Chain of Custody for your sample set received December 6 2011

All analyses were performed in accordance with TNI Standards using approved methods as Indicated on this report

If you have any questions about the results please can Thank you for using Siemens Industry Inc for your analytical needs

Sincerely

Siemens Industry Inc

Bruce Schertz Lab Manager Enviroscan Analytical1M Services

I c11y that the ~Ill containedIn Ws r-son has btngeneratedandremwtd In ccordancbull wlCll lheSiemens lndUllty Inc QualityMWIWl(t ManuaL Exception$ Uany d1$cuuedIn Ihanmpfe narrative Samples wtberetained for 30 dayt from tbe date ofthis -on Ulan disposed In an1pproprlate m111ner SIMlffls l11du8try Inc restrvu thbull right to ~m aemplts ldtnURlaquoIbullbullhitardoUs Reetu ofth~ FlntlRbullpott Ibull tuthorlzed verllltdbylhbull followln9 at9n11tu- T- contents ofthis 1tport apply to thbullsomple(1 antyied No dupHcatfon ofthis report Is allowedexcept In Its entlrtty

Reviewed by

Certifications Wisconsin 737053130 Minnesota 055-999-302 lffinois 100317 bull

Siemens lnduslry Inc 301 West Military Road TeJ 800-338-7226 Rothschild WI 54674 Fax 715bull355-3221

wwwsfemonscomenYl101Ca11

The total number ofpages in tl1is report including this page is 17

QC REPORT EAi ID 105963 ~ bull IW



MSMSD MSMSD Date of Parameter Name Parent ID Parent Matrix Spike MSD Units Analysis Limits RPO Method

A1luminum 10598501 lt 005 12 (108 R) 12 (109 R) (1 RPO) mgL 12911 70-130 20 2008

Antimony 10598501 lt 0 001 11 (109R) 11 (108 R) (1 RPO) mgL 12911 70-130 20 2008

Arsenic 10598501 lt 0 001 10 (102 R) 10 (102 R) (0 RPO) mgL 12911 70-130 20 2008

Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008

Beryllium middot 10598501 lt 0001 10 (102 R) 10 (102 R) (0 RPD) mgL 12911 70-130 20 2008

Cadmium 10598501 lt 0001 10 (100 R) 10 (100 R) (0 RPD) mgL 12911 70-130 20 2008

Chromium 10598501 lt 0001 091 (91 R) 090 (90 R) (1 RPD) mgL 12911 70-130 20 2008

Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008

Mercury 10598501 lt 00001 00010 (97 R) 00009 (94 R) (3 RPO) mgL 12911 70-130 20 2008

Nickel 10598501 lt 0001 081 (81 R) 082 (82 R) (1 RPO) mgL 12911 70-130 20 2008

Selenium 10598501 lt 0001 089 (89 R) 088 (88 R) (1 RPD) mgL 12911 70-130 20 2008

Silver 10598501 lt 0001 10 (100R) 098 (98 R) (2 RPD) mgL 12911 70-130 20 2008

Thallium 10598501 lt 0001 10 (102 R) 10 ( 102 R) (0 RPO) mgL 1291 1 70-130 20 2008

Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008

Samples were analyzed within holding times unless noted on the sample results page Instrumentation was calibrated in accordance with the method requirements The method blanks were free of contamination at the reporting limits The associated matrix spikes andor Laboratory Control Samples met the above stated criteria Exceptions to the above statements are flagged or noted above or on the QC Narrative page bullt Flagged analyte recoveries deviated from the QNQC limits

eastern analytical inc wwweailabscom Phone (603) 228-0525

middot

7

LABO RA TORY REPORT EAi ID 105963~ Client Northeast Utilities


Sample ID WWT Effulent

Lab Sample 10 10596302

Matrix aqueous

Date Sampled 12711 Analytical Date of Date Received 121711 Matrix Units Analysis Method Analyst

Aluminum lt 02 AqTot mgL 1291 1 2008 DS Antimony lt 001 AqTot mgL 12911 2008 DS Barium 022 AqTot mgL 12911 2008 DS Beryllium lt 001 AqTot mgL 12911 2008 D_S

Cadmium lt 001 AqTot mgL 12911 2008 DS Chromium lt 001 AqTot mgL 12911 2008 DS Copper lt 001 AqTot mgL 12911 2008 DS

Lead lt 001 AqTot mgL 12911 2008 DS

Nickel lt 001 AqTot mgL 1291 1 2008 DS Silver lt 001 AqTot mgL 12911 2008 DS Thallium lt 001 AqTot mgL 12911 2008 DS Zinc lt 001 AqTot mgL 12911 2008 DS


5

CHAIN-OF-CUSTODY RECORD 105962Page of _____ ~

SOLD FIELDS REQUIRED PLEASE CIRCLE REQUESTED ANALYSIS 0

voe SVOC TCLP METALS INORGANICS

i w

SAMPLING 0 VI 0 J 0 ~ w

0ATEIT1ME 0) Q - I -

w 0 2~~IF COMPOSITE w ~ u - ~

INDICATE BOTH gtlt +- 1C~ Iiilt START amp FINISH

0) ~ 6 i SAMPLE ID ~ ci

a -shy -Q

DATE TIME I ~~C) ~

~eltT Ja1tlt 1h11 n~ il)Ji r_

-ra L kZ K pound-lt()k 11h11 Ye i(i) Cshy

MATRIX A-AIR S-Soll GW-GWUHO WATEt SW-SURFACE WATEl DW-DRIKllNG WATU WW-WASTE WATEI

PmEmTm H-HCL N-HHO S-HSO Na-NaOHmiddot 11-tEOH

- -

~t - ~ 2 ~ 8c 2 9= ~ e I ~ ~ Jli c ~ cS I j al E l a - - ~ ~ c ~ = oshy ~ ae e 1ix 2shy -s ~

- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~

~ Ii r= i ~~ 9 C ~ ~ ei i ~ NorEsii5 shy ii -I~ a MEOH V1AL ~=3

c

l] 88 sm- Ila

I(

e

CoMPANY Nedlt-q s-1-- u+W+s QAQC REPORTING LEVELshyADOREI 97 frVr iJ

A B C(ITY _ampd STATpound~ ZIP QHolf ORPHONE ( (o~ ZLbull lfo~( EXT _ ___

FAX (GbullgtJ z1-y - y MAMCP

PRESUMPTIVE CERTAINTYE-MAU - ----- ------ - ------shySm NANpound MeuMaLt 5h_nt1u_________ _ _

PROJECT=----- - - - - --- - - ----- - -ST~Tf ~ MA ME VT OTHER _____ _ _ _

REGULATORY PAOGRAH NPDES RGP POTW STOOOIATfR Oamp

GWP OIL FUND 8ROWHflELD Ol OTHER _ ________

Quon PO_ ___ ___

RELINQUISHED BY DATf TINE

METALS 8 RCRA 13 PP FE HH Pa cuDATE NEEDED _ _)+Ic-41-+-it_ ___ _PRoJecr MANAGER ArmiddotHi 1u AlaquoA-c letc TEttr_lS- middotc REPORTING OPTIONS ornER HmL1 A s s fl rmcnt) No 1 PUUIIS YE OR No

Dmomo HETlli FIELD FILTERED YEI NoIf YH FAX Ol PDF Nam IE SPEOAL DETECTI ON l lHIT1 BILUHG INFO If DIFFERENT)

ELECTRONIC OPTIONS ur Colis01 c1( ~ A~(s~middot No FAX E-MAIL PDF EQUIS

l ~3L H7

SITE HIHOampY _____ ______

SUSPECTED (OHTAHINATIOH_ _ _ ___ _ _

flUD JluDJNGS_ _ ________ _RELINQUISHED BY DATE TINpound RECEIVED BYJAcI eastern analytcal nc 2s CHENELL DR1vE ICoNcoRo NH 03301 ITEL 60322sos2s I 1soo2s7os2s IFAx 6032284591 I E-MA1t cuST0Mrnsrnv1ceEA1tA0s coM JwwwEA1LAascogt1

(WHITE ORIGINAL GREEN PROJECT MANAGER)

bull middot middot --~ - lt

FRONTIERmiddot GLOBAL SCJENCES

bull

414 Pontius Ave NorthSeattle WA 98109 Ph 206-622-6960Fx 206-622-6870

PREPARATION BLANKS


Instrument Hg-17 Preparation BrCl Oxidation

Lab Sample ID Analyte Found MRL Units Batch Method Notes

Fl 12077-BLKI Mercury 005 050 ngL Fll2077 EPA 163IE u Fl I2077-BLK2 Mercury 005 050 ngL Fll2077 EPA 1631E u Fl 12077-BLK3 Mercury 005 050 ngL Fl12077 EPA 1631E u Fl l 2077-BLK4 Mercury 013 050 ngL Fl12077 EPA l631E QB-04 U


--I J Iymiddot---~-a~-~


Tk results in this report only apply to the samples analyzed in accordance with the chain ofcustody document This analytical report must be reproduced in its entirety


18


FRmiddotONTIER~middotmiddot middotGLOBAL middotsclENCES


RECOVERY AND RPO


Batch Fl 12077 Lab Number Fl 12077-BSBSDl

Preparation BrCl Oxidation LCS Source Nist lMid

Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery

Limits RPD Limit Method Notes

Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E


~--lt1~~ Liz Siska Project Manager

The results in this report only apply to the samples analyzed in accordance wilh the chain ofcustody document This analytical report must be reproduced in its entirety


16


FRONTI ER GLOBAL SCIENCES


SOURCE 1112097-01RE2


Batch Fl 12077 Lab Number Fl 12077-MSMSD3


Analyte

Sample Spike Concentration Added

(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes

Spike MSD Added Concentration (ngL) (ngL

MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~


The results in this report only apply to the samples analyred in accordance with the chain ofcustody document This analytical report must be reproduced in itsentirety


14

414 Pontius Ave North Seattle WA 98109 Ph 206-622--0960 Fx 206-622-6870

FRONTIERmiddot GLOBAL SCIENCES


SOURCE 1112097-03


Batch FJ12074 Lab Number FI12074-MSMSD2


Analyte

Arsenic

Sample Concentration

(microgL)

403

Spike Added (microgL)

20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes

AS Seleniwn 20200 348l 113 663 59 - 149 20 FGS-054 AS


_f ~ A I ~~- __s(J_~


The results in this report onlyapply to the samples analyzed in accordance with the chain ofcustody document This analytical report must be reproduced in its entirety


12

FRO NTI ER_ G L O B A L S C I E N C E S


MATRIX DUPLICATESTRIPLICATES


Matr ix Water Sequence 1L09012

Batch Fl12077 Lab Number- Fl 12077-DUP2



Duplicate Concentration RPD

Analyte ngL ngL MRL RPD Limit Method Notes

Mercury 563 544 202 349 24 EPA 1631E

Frontier Global Sciences Inc The results in this report only apply to the samples analyzed in accordance with the chain ofcustody document This analytical report must be reproduced in its entirety


--d~-L~~ Liz Siska Project Manager 10

f RONTJEI GLOBAL SCIENCES


Arsenic Analytical Results


Sample Name Result MRL Units Batch Prepared Seauence Analyzed Method Notes

FGS-054 u T T Field Blank ND 015 microgL F112074 120811 1L09004 120911

Treat Tank 403 150 microgL Fll2074 120811 1L09004 120911 FGS-054

Frontier Global Sciences Inc The results in this report only apply to 1he samples analyzed in accordance with the chain ofcustody document This analytical report must be reproduced in its entirety

middot---shy_ J =-y--~--middot Page 6 of 17 1112110 Final Report

Liz Siska Project Manager 8

0 Standard D High

Comments

I i IL-oqo1u 1 1bullat I I~ 1lltl 7 ampU iepa I middotmiddot I T I I I I I I I ks$~ s--sr -1t9

6

7

8

9

10

11

Sample Disposal D Retum (shlpplngfees may apply) D Standard Disposal - 30 Days after report

-roL s o576Q

ReceVed By

laquo

By signing you declare that you agree with FGS terms end conditions and tha you authorize FGS to pe_rtorm the specified analyses

D Retllln forshyshy~~eeks after report (storage fees may apply) Customer A_eprovel Date

1 I

Jf) t l Chain of Custody Record amp Laboratory Analysis Request 414 Pontius Ave N Seattle WA 98109 Air Water Sediments Plant and Animal Tissue Phone 206-622~960

Fax 206middot622middot6870~ F RO_ N T I E R- Hydrocarbon amp Other Samples 2-tJCr 1nroftQntierGs com httpfwwwFrontierGScomCLO BA L SCIE NCES Page_j_ of_L_

JcEco Bf 1 4(xP-BtihlJJ- FG5 -- g- crmiddot


FRONTIER GLOBAL SCIENCES


Frontier Global Sciences Inc The results In this report onlyapply to the samples analyed in accordance wiih the chain ofcustody document This analytical report must be reproducedin itsentirety

-~middot ~shy

i __-ltL-lt-v~~ Page4 of 17

111211O Final Report


414 Pontius Ave North Seattle WA 98109 Ph 206-622-6960 Fx 206-622-6870shy

1-


CASE NARRATIVE

Work Order Number I112097

SAMPLE RECEIPT

Samples were received at Frontier Global Sciences (FGS) on December 7th 2011 The samples were received intact on-ice with temperatures measured at 31 degrees Celsius

SAMPLE PREPARATION AND ANALYSIS

Per FGS standard operating procedure FGS-054 aqueous samples should be preserved with acid to pHlt2 for a minimwn of 16 hours at room temperature before preparation andor analysis to completely dissolve the metals adsorbed on the bottle walls Due to the clients requirement for rush sample data samples were preserved with acid to pHlt2 for approximately IO (ten) hours prior to preparation and analysis

Samples were prepared and analyzed for total metals in accordance with FGS-054EPA 163 8 with the exception ofthe preparation deviation noted above

Samples were prepared and analyzed for total mercury in accordance with EPA Method 163 lE

ANALYTICAL AND QUALITY CONTROL ISSUES

There were no analytical difficulties experienced with analysis ofthese samples with the exceptions flagged in the report

Frontier Global Sciences Inc The results in this report only apply to the samples analyzed in accordance with the chain ofcustody documenl This analytical report must be reproduced in its enlirety

~--_--d~-~ Page 2 of 17 111211 O Final Report


bull 414 Pontius Ave North

Seattle WA 98109 Ph 206-622-6960 Fx 206-622-6870 FRONTIER~

GLOBAL SCIENCES

09 December 2011

Jeff Gagne

Eastern Analytical Inc

25 Chenell Drive

Concord NH 03301

RE Merrimack Station

Enclosed are the analytical results for samples received by Frontier Global Sciences All quality control

measurements are within established control limits and there were no analytical difficulties encountered

with the exception of those listed in the case narrative section of this report

Ifyou have any questions concerning this report please feel free to contact me

Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt

(l- ~ 0 shy() -lt lt l


Eastern Analytical Inc ID 105962 Client Identification Merrimack Station

Date Received 12n12011

Dear Mr Auclair

Enclosed please find the report of analysis for the above identified project As discussed analyses were subcontracted and are listed as follows

Analysis Subcontract - Metals Low level

Subcontractor Lab Frontier Global Sciences Inc

A complete copy of the report is attached This report may not be reproduced except in full without the written approval of the laboratory


Sincerely

JJ11 oC

Date of pages (excluding cover letter)

11111middot~il1hsom1

LABORATORY REPORT EAi ID 105645IKM Client GZA GeoEnvironmental Inc (NH)

Client Designation Merrimack Statiomiddotn Wastewater Analysis - Weekly



Matrix aqueous


Date Received 113011 Matri~ Units Analysis Method Analyst

Molybdenum 0010 AqTot mgL 113011 2008 OS


lw LABORATORY REPORT EAi ID 105645





Matrix aqueous

Date Sampled 113011


Units mgL

Date ofExtractionPrep 12111


Analyst LAS

Method 1664A

DIiution Factor 1

Oil amp Grease (HEM) lt5


bull

LABORATORY REPORT EAi ID 105645~ Client GZA GeoEnvironmental klc (NH)




Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1

Pentachlorophenol lt5

4-Nitrophenol lt5 2 4-Dinitrophenol lt5

Hexachloroethane lt1 Hexachlorobutadiene lt1 Hexachlorocyclopentadiene lt5

4-Chloroaniline lt1 2-Nitroaniline lt5

4-Nitroaniline lt1 Benzyl alcohol lt5 Nitrobenzene lt1 lsophorone lt1

Benzidine (estimated) lt5

Pyridine lt5

2-Chlorophenol lt 1 24-Dichlorophenol lt 1 245-Trichlorophenol lt 1 2 46-Trichlorophenol lt 1

2-Nitrophenol lt 1

2-Methylphenol lt 1 34-Methylphenol lt 1 2 4-Dimethylphenol lt 1 4-Chloro-3-methylphenol lt 1 46-Dinitro-2-methylphenol lt5 Benzoic Acid lt50 N-Nitrosodimethyfamine lt1 n-Nitroso-di-n-propylamine lt 1 n-Nitrosodiphenylamine lt 1

lt 1bis(2-Chloroethyl)ether bis(2-chloroisopropyl)ether lt1 bis(2-Chloroethoxy)methane lt 1 13-Dichlorobenzene lt 1 14-0ichlorobenzene lt 1 12-Dichlorobenzene lt 1 124-Trichlorobenzene lt1 2-Chloronaphthalene lt 1

lt 14-Chlorophenyl-phenylether 4-Bromophenyl-phenylether lt1

Hexachlorobenzene lt 1

3-Nitroaniline lt 1

24-Dinitrotoluene lt 1 26-Dinitrotoluene lt 1

33-Dichlorobenzidine lt 1

Azobenzene lt 1


middotrr-1 SAMPLE CONDITIONS PAGE EAi ID 105645

~ Client GZA GeoEnvironmental Inc (NH)

CUent Designation Merrimack Station Wastewater Analysis - Weekly

Temperature upon receipt (degC) 235 Received on ice or cold packs (YesNo) N Acceptable temperature range (degC) 0-6

Date Date Sample Dry lab ID Sample ID Received Sampled Matrix Weight ExceptionsComments (other than thermal preservation)

10564501 Wastewater 113011 113011 aqueous Adheres to Sample Acceptance Policy

Samples were properly preserved and the pH measured when applicable unless otherwise noted Analysis ofsoids for pH Flashpoint lgnitibillty Paint Filter Corrosivity Conductivity and Specific Gravity are reported on an bullas received basis

All results contained in this report relate only to the above Isled samples

References include 1) EPA 6004-79-020 1983 2) Standard Methods for Examination ofWater ancl Wastewater lnorganics 19th Edition 1995 Microbiology 20th Edition 1998 3) Test Methods for Evaluating Solid Waste SW 846 3rd Edition including updates VA and VB 4) Hach Water Analysis Handbook 2nd edition 1992


EAi ID 105347LABORATORY REPORT y ~ middot





Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis

Date Time Method Analyst

Solids Suspended Fluoride

lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL

Cyanide Total Total Nitrogen BOD COD Total Phenols pH

045 151 lt6 59

lt 005 65

mgL mgL mgL mgL mgl SU

112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ

Total Nitrogen is determined by a calculation derived from method EPA 3532 and Standard Methods 4500orgCNH3D

eastern analytical inc wwweailabscom Phone (603 228-0525 7

4 LABORATORY REPORT EAi ID 105347~ Client GZA GeoEnvironmental Inc (NH)


WastewaterSample ID


Matrix aqueous


Units mgL

Date of ExtractionPrep 111811


Analyst LAS Method 1664A

Dilution Factor 1



LABORATORY REPORT EAi ID 105347 ~ Client GZA GeoEnvironmental Inc (NH)



10534701Lab Sample ID Matrix aqueous

Date Sampled 11117111


Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1

Phenol lt1 2-Chlorophenol lt 1 24-Dichlorophenol lt1 245-Trichlorophenol lt1


4-Nitrophenol lt5 24-Dinitrophenol lt5

24-Dimethylphenol lt1

n-Nitroso-di-n-propylamine lt1

Hexachlorocyclopentadiene lt5 Hexachlorobenzene lt1

2-Nitroaniline lt5

Benzyl alcohol lt5

Benzidine (estimated) lt5 33-Dlchlorobenzidine lt1 Pyridine lt5

246-Trichlorophenol lt 1

2-Nitrophenol lt 1

lt 12-Melhylphenol 34-Methylphenol lt 1

lt14-Chloro-3-methylphenol 46-Dinitro-2-methylphenol lt5 Benzoic Acid lt50 N-Nilrosodimethylamine lt 1

n-Nitrosodiphenylamine lt 1 bis(2-Chloroethyl)ether lt 1 bis(2-chlorolsopropyl)ether lt 1 bis(2-Chloroethoxy)methane lt 1 13-Dichlorobenzene lt 1 14-Dichlorobenzene lt 1 12-Dichlorobenzene lt 1 124-Trichlorobenzene lt 1 2-Chloronaphthalene lt 1 4-Chlorophenyl-phenylether lt 1

lt 14-Bromophenyl-phenylether Hexachloroethane lt 1 Hexachlorobutadiene lt 1

4-Chloroanillne lt 1

3-Nitroaniline lt 1 4-Nitroaniline lt 1

Nitrobenzene lt 1 lsophorone lt 1 24-Dinitrotoluene lt 1 26-Dinitrotoluene lt 1

Azobenzene lt 1


SAMPLE CONDITIONS PAGE EAi ID 105347 ~ ~



Received on ice or cold packs (YesNo) YTemperature upon receipt (degC) 8 Acceptable temperature raiige (degC) 0-6

Date Date Sample Dry Received Sampled Matrix Weight ExceptionsComments (other than thermal preservation)Lab ID Sample ID


Samples were properly preserved and the pH measured when applicable unless otherwise noted Analysis ofsolids for pH Flashpoint lgnitibility Paint Filter Corrosivity Conductivity and Specific Gravity are reported on an bullas received basis

All resuffs contained in this report relate only to the above listed samples

References include 1) EPA 6004-79-020 1983 2) Standard Methods for Examination of Water and Wastewater lnorganics 19th Edition 1995 Microbiology 20th Edition 1998 3) Test Methods for Evaluating Solid Waste SW846 3rd Edition including updates VA and VB 4) Hach Water Analysis Handbook 2nd edition 1992


ANALYTICAL DATA REPORTS

SUMMARY OF BASELINE MONITORING ANALITICAL RESULTS WET CHEMISTRY voe AND PCB


Bow New Hampshire

(4)RESULTS (4)RESULTS

PARAMETER LOWELL SEWER

DISCHARGE LIMITS (mgL)

11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110

ICvanide 1895 (3) lt 001

Fluoride - 44 6

Molvbdenum - lt 0005 0010

NitroeenT) - 151 130

OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND

Phenolic Comoounds - lt005 lt03

PCBs - ND(2) No Data

Note I Two compounds wen detected on 111712011 by Method 624 Toluene at 3microgL and Styrene

at 4 microgL One compound was detected by Mclhod 624 on 113011 Toluene These tow levels are likely the result ofresidual adhesive from the piping components

2 PCB compounds analyzed by method 608 were not detected at concentntions greater lhan 03microgL

3 The cyanide value was inconclusive due to matri~ interference 4 Samples were collected after lhe treatment system had been operating for at least lhree weeks

had completed start-up procedures and was operating under nonnal conditions

GZA GeoEnvironmental Inc P~o~9l0igtro400l9J070QoWodSAMPUN0 AND REPOllTlNCDATA December 16 2011 RESULTS 121611xkJLQwelwct

r-- ------ ________________________ ------- -----shy1 LOWELL REGIONAL WASTEWATER UTILITY

Industrial Sewer User Self-Monitoring Report summary Sheet I middot r

SubmitAllCltam ofCUs(oclyandLabcdtoyResultSheets With SMR SummarySheet

l11ltIIYUvdl ft)Ul)

lParamefet~h ~~middot AnalYsis Date L ~ResuttJ~ni middottmiddot P~Jer~ shy middot AnalvslsbullQate - middot ~ bullbull i

__Result rrooll pound bull ~

BOD SEEATTACHED Coooer middotshyCOD - Cvanide ITotaD

OampG 4131 1664 Fluoride

TSS Lead

TOC Mercuri

TTO62482608-amp2511210 Mnlvtvlemmmiddot

Aluminum - Nickel

Antimnnv Nitrooen lKleldahll

Arsenic Phenols notall

Barium Selenium

IBervllium Silver

Cadmium Thalium

cbJ - IJ)IJll middotmiddot--middotmiddotmiddot - middot--middotshy --shy - line --middotmiddotshy middot middot M~bullbull middotmiddotmiddot - middotmiddotmiddotmiddot-middot

Chromium CTotan Other

SOD= Biochemical Oxygen Demand COD= Chemical Oxygen Demand OampG=OilampGtease TSS =TotalSuspended Sdids TTO=Total Tolic Olganics TOC (Total Otganic Carbon) =Is the amountofcarbon bound In anorganiccompound andIs often used as anon-speciffcIndicatorofwaterquality roe measWOs both the total carbonpresentas weB as the inorganic catbon (IC) Subtracfing the Inorganiccarboo from the IotaC8lbon yields TOC TTOs Summation ofaJquantifiable values greaterthan 001 mgI for toxicorganics lstadin 4() CFR 41302(i TTOsinclude PCBs (Poly-ChlorinatedBiphenyls) VOCs (Volatile Organic Compounds) SVOCs (SemVo8tile OrgllflicCompoonds) PCBs VOCs end SVOCs shallbe analyz6d using EPA Methods 608 624 i1lld 625 respectivofy

Zero Discharge I Sett-Monitoring (lnltial ifapplicable)

____ No Industrial wastewaterfrom permitted processes has been dischafged to sewer during the monitoring period

_ ___ No sampling has been conducted on permitted sewerdischarges during the monitoring period

Certification Statement

middot1 cenify under penalty of law that this document and all attadmentswete pcepared uooermy cfirection or supervision in 8CCOfdance with asystem designed lo 8SStft that qualified persomel properly 9a1her and evaluate the llfonnation submitted Based on my Inquiry ofthe person or persons who manage the system or those persons directly esponsille for gathemg the ilformation the ilformation submitted is to the best of my knowledge and belief true accurate and COll1)1ete I am aware that there are significant penaffies br submitting false inbmation incllding the possibilityoffine and imprisonmentforknowing violationsbull

Harold~ Station Ma~er Title

1--b ljrD J J

Y- ~e

LRWWU Use Only Self-Monitoring ReportSummary Sheet Page2of2

SMR SUMMARY SHEET

Lowell Regional Wastewater Utility File No 04002930700

December 16 2011 Pag_e2

ai)

Wastewater flow data was estimated based on the actual number of tank trucks sent to the Utility and tanker capacity

ANALYTICAL NOTATION

FGD wastewater requires specialized analytical techniques to overcome matrix interference on some trace metals analysis Many analytical laboratories may be unaware of this We offer an excerpt below from EPAs web site and a link to their draft procedure that contains further guidance

LABORATORY ANALYSIS OF FLUE GAS DESULFURIZATION FOO) WASTEWATER

Wastewater from FGD systems can contain constituents that may interfere with certain laboratory analyses due to high concentrations of total dissolved solids (TDS) or the presence of elements known to cause matrix interferences EPA has observed that during inductively coupled plasma - mass spectrometry (ICP-MS) analysis of FGD wastewater certain elements commonly present in the wastewater may cause polyatomic interferences that bias the detection andor quantization of certain elements of interest These potential interferences may become significant when measuring trace elements such as arsenic and selenium at concentrations in the low parts-pershybillion range

As part of a recent sampling effort for the steam electric power generating effluent guidelines rulemaking EPA developed a standard operating procedure (SOP) that was used in conjunction with EPA Method 2008 to conduct ICP-MS analyses of FGD wastewater The SOP describes critical technical and quality assurance procedures that were implemented to mitigate anticipated interferences and generate reliable data for FGD wastewater EPA regulations at 40 CFR 1366 already allow the analytical community flexibility to modify approved methods to lower the costs of measurements overcome matrix interferences or otherwise improve the analysis The draft SOP developed for FGD wastewater takes a proactive approach toward looking for and taking steps to mitigate matrix interferences including using specialized interference check solutfons (ie a synthetic FGD wastewater matrix) EPAs draft SOP is being made available to laboratories contemplating ICP-MS analysis of FGD wastewater either for adoption as currently written or to serve as a framework for developing their own laboratory-specific SOPs Standard Operating Procedure Inductively Coupled PlasmaMass Spectrometry for Trace Element

Analysis in Flue Gas Desulfurization Wastewaters (30 pp 174K)

CERTIFICATION

I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to ensure that qualified personnel properly gather and evaluate the information submitted Based on my inquiry of the person(s) who manage the system or those persons directly responsible for gathering the- infomiatiori the iriformation-subniittea is fo the besfofmy knowledge and belief true accurate and complete I am aware that there are significant penalties for submitting false information including the possibility of fine and imprisonment for knowing violations

AR-1311

AR-1311-2

Lowell Regional Wastewater Utility December 16 2011 File No 04002930700 Page3

Should you have any questions concerning this report please do not hesitate to contact me at (603) 232-8744

Very truly yours

GZA GEOENVIRONMENTAL INC

Ronald A Breton PE Principal

RABrkl P04Jobs0029300s04002930700WorlltSAMPLNG AND REPORTNGIREPORTSLowellBMA REPORlFINAL 29307 LRWU CVR LTR 121611doelt

Attachments SMR Summary Sheet Tables Analytical Data Reports














(1) 616 (2) 696







Refer to Self-Monitoring ReportInstructions for details on completing this SMR Summary Sheet LRWWU Use Only Self-Monitoring Report Summary Sheet Page 1 of 2

TABLES



Bow New Hampshire


LIMITS (mgL)

125lOll (mgL)




Paul Pepler


380 Harvey Road

Manchester NH 03103





Dear Mr Pepler







Sincerely


~ Wtl1ilabsc m

middotl






Matrix aqueous

Date Sampled 111711


Units ugn


Analyst KJP

Method 624

Dilution Factor








Matrix aqueous


Units ugf




Dilution Factor 1


Naphthalene lt1

Acenaphthene lt1

Fluoranthene lt1









Pyrene lt 1













Diluffon Factor 1








Matrix aqueous






Paul Pepler


380 Harvey Road

Manchester NH 03103







Dear Mr Pepler







Sincerely








Matrix aqueous

Date Sampled 113011


Units ug1


Analyst KJP









Matrix aqueous


Units ug1




Dilutlon Factor 1

Carbazole lt 1


Naphthalene lt1

Pyrene lt1

Benzo[a)pyrene lt1
















Matrix aqueous












~ Nmiddot 61)6G



~- (ttio ~ J~S~~L


EAi Project ID 3902


State NH





Phone 623-36(10 Fax 624-9463 (37)




tVt-_





bull$

Relinquished by

PONumber 02259252

Quote No 1009476


i ~~pllt-


1-800-287-0525 Fax (603)228-4591






















-- - ~ ~




3

FRONTIEmiddotRI

GLOBAL SCIENCES



J

8

9

10

ll

Received By





5











7











9



Fx 206-622-6870


SOURCE 1112097-03




Sample Spike MS MS




Recovery


Arsenic 403 50030 893 980 85 - 115 FGS-054

Selenium 1196 49990 1267 141 59 - 149 FGS-054

Spike Added

MSD Concentration

MSD Oo Recovery RPD



~





1 1




SOURCE 1112089-17





Mercury 6868 10200 1680 973 71 - 125 EPA 163JE



Mercury 10200 1572 868 660 71 - 125 24 EPA 1631E





13




RECOVERY AND RPD












15



PREPARATION BLANKS








17 middotmiddot



















19

Ii Io



Arthur Auclair


Bow NH 03304





Dear Mr Auclair







Sincerely



Ill I



Date of



Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008


Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008


Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008





C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT









~--_--d~-~ of 17 111211 O Final Report




GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2














(1) 616 (2) 696







Refer to Self-Monitoring ReportInstructions for details on completing this SMR Summary Sheet LRWWU Use Only Self-Monitoring Report Summary Sheet Page 1 of 2

TABLES



Bow New Hampshire


LIMITS (mgL)

125lOll (mgL)




Paul Pepler


380 Harvey Road

Manchester NH 03103





Dear Mr Pepler







Sincerely


~ Wtl1ilabsc m

middotl






Matrix aqueous

Date Sampled 111711


Units ugn


Analyst KJP

Method 624

Dilution Factor








Matrix aqueous


Units ugf




Dilution Factor 1


Naphthalene lt1

Acenaphthene lt1

Fluoranthene lt1









Pyrene lt 1













Diluffon Factor 1








Matrix aqueous






Paul Pepler


380 Harvey Road

Manchester NH 03103







Dear Mr Pepler







Sincerely








Matrix aqueous

Date Sampled 113011


Units ug1


Analyst KJP









Matrix aqueous


Units ug1




Dilutlon Factor 1

Carbazole lt 1


Naphthalene lt1

Pyrene lt1

Benzo[a)pyrene lt1
















Matrix aqueous












~ Nmiddot 61)6G



~- (ttio ~ J~S~~L


EAi Project ID 3902


State NH





Phone 623-36(10 Fax 624-9463 (37)




tVt-_





bull$

Relinquished by

PONumber 02259252

Quote No 1009476


i ~~pllt-


1-800-287-0525 Fax (603)228-4591






















-- - ~ ~




3

FRONTIEmiddotRI

GLOBAL SCIENCES



J

8

9

10

ll

Received By




of17 1112110 Final Report

5











7











9



Fx 206-622-6870


SOURCE 1112097-03




Sample Spike MS MS




Recovery


Arsenic 403 50030 893 980 85 - 115 FGS-054

Selenium 1196 49990 1267 141 59 - 149 FGS-054

Spike Added

MSD Concentration

MSD Oo Recovery RPD



~





1 1




SOURCE 1112089-17





Mercury 6868 10200 1680 973 71 - 125 EPA 163JE



Mercury 10200 1572 868 660 71 - 125 24 EPA 1631E





13




RECOVERY AND RPD












15



PREPARATION BLANKS








17 middotmiddot



















19

Ii Io



Arthur Auclair


Bow NH 03304





Dear Mr Auclair







Sincerely



Ill I



Date of



Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008


Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008


Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008





C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2

TABLES



Bow New Hampshire


LIMITS (mgL)

125lOll (mgL)




Paul Pepler


380 Harvey Road

Manchester NH 03103





Dear Mr Pepler







Sincerely


~ Wtl1ilabsc m

middotl






Matrix aqueous

Date Sampled 111711


Units ugn


Analyst KJP

Method 624

Dilution Factor








Matrix aqueous


Units ugf




Dilution Factor 1


Naphthalene lt1

Acenaphthene lt1

Fluoranthene lt1









Pyrene lt 1













Diluffon Factor 1








Matrix aqueous






Paul Pepler


380 Harvey Road

Manchester NH 03103







Dear Mr Pepler







Sincerely








Matrix aqueous

Date Sampled 113011


Units ug1


Analyst KJP









Matrix aqueous


Units ug1




Dilutlon Factor 1

Carbazole lt 1


Naphthalene lt1

Pyrene lt1

Benzo[a)pyrene lt1
















Matrix aqueous












~ Nmiddot 61)6G



~- (ttio ~ J~S~~L


EAi Project ID 3902


State NH





Phone 623-36(10 Fax 624-9463 (37)




tVt-_





bull$

Relinquished by

PONumber 02259252

Quote No 1009476


i ~~pllt-


1-800-287-0525 Fax (603)228-4591






















-- - ~ ~




3

FRONTIEmiddotRI

GLOBAL SCIENCES



J

8

9

10

ll

Received By





5











7











9



Fx 206-622-6870


SOURCE 1112097-03




Sample Spike MS MS




Recovery


Arsenic 403 50030 893 980 85 - 115 FGS-054

Selenium 1196 49990 1267 141 59 - 149 FGS-054

Spike Added

MSD Concentration

MSD Oo Recovery RPD



~





1 1




SOURCE 1112089-17





Mercury 6868 10200 1680 973 71 - 125 EPA 163JE



Mercury 10200 1572 868 660 71 - 125 24 EPA 1631E





13




RECOVERY AND RPD












15



PREPARATION BLANKS








17 middotmiddot



















19

Ii Io



Arthur Auclair


Bow NH 03304





Dear Mr Auclair







Sincerely



Ill I



Date of



Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008


Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008


Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008





C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2



Bow New Hampshire


LIMITS (mgL)

125lOll (mgL)




Paul Pepler


380 Harvey Road

Manchester NH 03103





Dear Mr Pepler







Sincerely


~ Wtl1ilabsc m

middotl






Matrix aqueous

Date Sampled 111711


Units ugn


Analyst KJP

Method 624

Dilution Factor








Matrix aqueous


Units ugf




Dilution Factor 1


Naphthalene lt1

Acenaphthene lt1

Fluoranthene lt1









Pyrene lt 1













Diluffon Factor 1








Matrix aqueous






Paul Pepler


380 Harvey Road

Manchester NH 03103







Dear Mr Pepler







Sincerely








Matrix aqueous

Date Sampled 113011


Units ug1


Analyst KJP









Matrix aqueous


Units ug1




Dilutlon Factor 1

Carbazole lt 1


Naphthalene lt1

Pyrene lt1

Benzo[a)pyrene lt1
















Matrix aqueous












~ Nmiddot 61)6G



~- (ttio ~ J~S~~L


EAi Project ID 3902


State NH





Phone 623-36(10 Fax 624-9463 (37)




tVt-_





bull$

Relinquished by

PONumber 02259252

Quote No 1009476


i ~~pllt-


1-800-287-0525 Fax (603)228-4591






















-- - ~ ~




3

FRONTIEmiddotRI

GLOBAL SCIENCES



J

8

9

10

ll

Received By





5











7











9



Fx 206-622-6870


SOURCE 1112097-03




Sample Spike MS MS




Recovery


Arsenic 403 50030 893 980 85 - 115 FGS-054

Selenium 1196 49990 1267 141 59 - 149 FGS-054

Spike Added

MSD Concentration

MSD Oo Recovery RPD



~





1 1




SOURCE 1112089-17





Mercury 6868 10200 1680 973 71 - 125 EPA 163JE



Mercury 10200 1572 868 660 71 - 125 24 EPA 1631E





13




RECOVERY AND RPD












15



PREPARATION BLANKS








17 middotmiddot



















19

Ii Io



Arthur Auclair


Bow NH 03304





Dear Mr Auclair







Sincerely



Ill I



Date of



Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008


Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008


Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008





C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2


Paul Pepler


380 Harvey Road

Manchester NH 03103





Dear Mr Pepler







Sincerely


~ Wtl1ilabsc m

middotl






Matrix aqueous

Date Sampled 111711


Units ugn


Analyst KJP

Method 624

Dilution Factor








Matrix aqueous


Units ugf




Dilution Factor 1


Naphthalene lt1

Acenaphthene lt1

Fluoranthene lt1









Pyrene lt 1













Diluffon Factor 1








Matrix aqueous






Paul Pepler


380 Harvey Road

Manchester NH 03103







Dear Mr Pepler







Sincerely








Matrix aqueous

Date Sampled 113011


Units ug1


Analyst KJP









Matrix aqueous


Units ug1




Dilutlon Factor 1

Carbazole lt 1


Naphthalene lt1

Pyrene lt1

Benzo[a)pyrene lt1
















Matrix aqueous












~ Nmiddot 61)6G



~- (ttio ~ J~S~~L


EAi Project ID 3902


State NH





Phone 623-36(10 Fax 624-9463 (37)




tVt-_





bull$

Relinquished by

PONumber 02259252

Quote No 1009476


i ~~pllt-


1-800-287-0525 Fax (603)228-4591






















-- - ~ ~




3

FRONTIEmiddotRI

GLOBAL SCIENCES



J

8

9

10

ll

Received By





5











7











9



Fx 206-622-6870


SOURCE 1112097-03




Sample Spike MS MS




Recovery


Arsenic 403 50030 893 980 85 - 115 FGS-054

Selenium 1196 49990 1267 141 59 - 149 FGS-054

Spike Added

MSD Concentration

MSD Oo Recovery RPD



~





1 1




SOURCE 1112089-17





Mercury 6868 10200 1680 973 71 - 125 EPA 163JE



Mercury 10200 1572 868 660 71 - 125 24 EPA 1631E





13




RECOVERY AND RPD












15



PREPARATION BLANKS








17 middotmiddot



















19

Ii Io



Arthur Auclair


Bow NH 03304





Dear Mr Auclair







Sincerely



Ill I



Date of



Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008


Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008


Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008





C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2

middotl






Matrix aqueous

Date Sampled 111711


Units ugn


Analyst KJP

Method 624

Dilution Factor








Matrix aqueous


Units ugf




Dilution Factor 1


Naphthalene lt1

Acenaphthene lt1

Fluoranthene lt1









Pyrene lt 1













Diluffon Factor 1








Matrix aqueous






Paul Pepler


380 Harvey Road

Manchester NH 03103







Dear Mr Pepler







Sincerely








Matrix aqueous

Date Sampled 113011


Units ug1


Analyst KJP









Matrix aqueous


Units ug1




Dilutlon Factor 1

Carbazole lt 1


Naphthalene lt1

Pyrene lt1

Benzo[a)pyrene lt1
















Matrix aqueous












~ Nmiddot 61)6G



~- (ttio ~ J~S~~L


EAi Project ID 3902


State NH





Phone 623-36(10 Fax 624-9463 (37)




tVt-_





bull$

Relinquished by

PONumber 02259252

Quote No 1009476


i ~~pllt-


1-800-287-0525 Fax (603)228-4591






















-- - ~ ~




3

FRONTIEmiddotRI

GLOBAL SCIENCES



J

8

9

10

ll

Received By





5











7










of 17 1112110 Final Report

9



Fx 206-622-6870


SOURCE 1112097-03




Sample Spike MS MS




Recovery


Arsenic 403 50030 893 980 85 - 115 FGS-054

Selenium 1196 49990 1267 141 59 - 149 FGS-054

Spike Added

MSD Concentration

MSD Oo Recovery RPD



~





1 1




SOURCE 1112089-17





Mercury 6868 10200 1680 973 71 - 125 EPA 163JE



Mercury 10200 1572 868 660 71 - 125 24 EPA 1631E





13




RECOVERY AND RPD












15



PREPARATION BLANKS








17 middotmiddot



















19

Ii Io



Arthur Auclair


Bow NH 03304





Dear Mr Auclair







Sincerely



Ill I



Date of



Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008


Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008


Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008





C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2






Matrix aqueous


Units ugf




Dilution Factor 1


Naphthalene lt1

Acenaphthene lt1

Fluoranthene lt1









Pyrene lt 1













Diluffon Factor 1








Matrix aqueous






Paul Pepler


380 Harvey Road

Manchester NH 03103







Dear Mr Pepler







Sincerely








Matrix aqueous

Date Sampled 113011


Units ug1


Analyst KJP









Matrix aqueous


Units ug1




Dilutlon Factor 1

Carbazole lt 1


Naphthalene lt1

Pyrene lt1

Benzo[a)pyrene lt1
















Matrix aqueous












~ Nmiddot 61)6G



~- (ttio ~ J~S~~L


EAi Project ID 3902


State NH





Phone 623-36(10 Fax 624-9463 (37)




tVt-_





bull$

Relinquished by

PONumber 02259252

Quote No 1009476


i ~~pllt-


1-800-287-0525 Fax (603)228-4591






















-- - ~ ~




3

FRONTIEmiddotRI

GLOBAL SCIENCES



J

8

9

10

ll

Received By





5











7











9



Fx 206-622-6870


SOURCE 1112097-03




Sample Spike MS MS




Recovery


Arsenic 403 50030 893 980 85 - 115 FGS-054

Selenium 1196 49990 1267 141 59 - 149 FGS-054

Spike Added

MSD Concentration

MSD Oo Recovery RPD



~





1 1




SOURCE 1112089-17





Mercury 6868 10200 1680 973 71 - 125 EPA 163JE



Mercury 10200 1572 868 660 71 - 125 24 EPA 1631E





13




RECOVERY AND RPD












15



PREPARATION BLANKS








17 middotmiddot



















19

Ii Io



Arthur Auclair


Bow NH 03304





Dear Mr Auclair







Sincerely



Ill I



Date of



Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008


Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008


Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008





C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2








Diluffon Factor 1








Matrix aqueous






Paul Pepler


380 Harvey Road

Manchester NH 03103







Dear Mr Pepler







Sincerely








Matrix aqueous

Date Sampled 113011


Units ug1


Analyst KJP









Matrix aqueous


Units ug1




Dilutlon Factor 1

Carbazole lt 1


Naphthalene lt1

Pyrene lt1

Benzo[a)pyrene lt1
















Matrix aqueous












~ Nmiddot 61)6G



~- (ttio ~ J~S~~L


EAi Project ID 3902


State NH





Phone 623-36(10 Fax 624-9463 (37)




tVt-_





bull$

Relinquished by

PONumber 02259252

Quote No 1009476


i ~~pllt-


1-800-287-0525 Fax (603)228-4591






















-- - ~ ~




3

FRONTIEmiddotRI

GLOBAL SCIENCES



J

8

9

10

ll

Received By





5











7











9



Fx 206-622-6870


SOURCE 1112097-03




Sample Spike MS MS




Recovery


Arsenic 403 50030 893 980 85 - 115 FGS-054

Selenium 1196 49990 1267 141 59 - 149 FGS-054

Spike Added

MSD Concentration

MSD Oo Recovery RPD



~





1 1




SOURCE 1112089-17





Mercury 6868 10200 1680 973 71 - 125 EPA 163JE



Mercury 10200 1572 868 660 71 - 125 24 EPA 1631E





13




RECOVERY AND RPD












15



PREPARATION BLANKS








17 middotmiddot



















19

Ii Io



Arthur Auclair


Bow NH 03304





Dear Mr Auclair







Sincerely



Ill I



Date of



Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008


Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008


Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008





C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2






Matrix aqueous






Paul Pepler


380 Harvey Road

Manchester NH 03103







Dear Mr Pepler







Sincerely








Matrix aqueous

Date Sampled 113011


Units ug1


Analyst KJP









Matrix aqueous


Units ug1




Dilutlon Factor 1

Carbazole lt 1


Naphthalene lt1

Pyrene lt1

Benzo[a)pyrene lt1
















Matrix aqueous












~ Nmiddot 61)6G



~- (ttio ~ J~S~~L


EAi Project ID 3902


State NH





Phone 623-36(10 Fax 624-9463 (37)




tVt-_





bull$

Relinquished by

PONumber 02259252

Quote No 1009476


i ~~pllt-


1-800-287-0525 Fax (603)228-4591






















-- - ~ ~




3

FRONTIEmiddotRI

GLOBAL SCIENCES



J

8

9

10

ll

Received By





5











7











9



Fx 206-622-6870


SOURCE 1112097-03




Sample Spike MS MS




Recovery


Arsenic 403 50030 893 980 85 - 115 FGS-054

Selenium 1196 49990 1267 141 59 - 149 FGS-054

Spike Added

MSD Concentration

MSD Oo Recovery RPD



~





1 1




SOURCE 1112089-17





Mercury 6868 10200 1680 973 71 - 125 EPA 163JE



Mercury 10200 1572 868 660 71 - 125 24 EPA 1631E





13




RECOVERY AND RPD












15



PREPARATION BLANKS








17 middotmiddot



















19

Ii Io



Arthur Auclair


Bow NH 03304





Dear Mr Auclair







Sincerely



Ill I



Date of



Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008


Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008


Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008





C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2


Paul Pepler


380 Harvey Road

Manchester NH 03103







Dear Mr Pepler







Sincerely








Matrix aqueous

Date Sampled 113011


Units ug1


Analyst KJP









Matrix aqueous


Units ug1




Dilutlon Factor 1

Carbazole lt 1


Naphthalene lt1

Pyrene lt1

Benzo[a)pyrene lt1
















Matrix aqueous












~ Nmiddot 61)6G



~- (ttio ~ J~S~~L


EAi Project ID 3902


State NH





Phone 623-36(10 Fax 624-9463 (37)




tVt-_





bull$

Relinquished by

PONumber 02259252

Quote No 1009476


i ~~pllt-


1-800-287-0525 Fax (603)228-4591






















-- - ~ ~




3

FRONTIEmiddotRI

GLOBAL SCIENCES



J

8

9

10

ll

Received By





5











7











9



Fx 206-622-6870


SOURCE 1112097-03




Sample Spike MS MS




Recovery


Arsenic 403 50030 893 980 85 - 115 FGS-054

Selenium 1196 49990 1267 141 59 - 149 FGS-054

Spike Added

MSD Concentration

MSD Oo Recovery RPD



~





1 1




SOURCE 1112089-17





Mercury 6868 10200 1680 973 71 - 125 EPA 163JE



Mercury 10200 1572 868 660 71 - 125 24 EPA 1631E





13




RECOVERY AND RPD












15



PREPARATION BLANKS








17 middotmiddot



















19

Ii Io



Arthur Auclair


Bow NH 03304





Dear Mr Auclair







Sincerely



Ill I



Date of



Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008


Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008


Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008





C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2






Matrix aqueous

Date Sampled 113011


Units ug1


Analyst KJP









Matrix aqueous


Units ug1




Dilutlon Factor 1

Carbazole lt 1


Naphthalene lt1

Pyrene lt1

Benzo[a)pyrene lt1
















Matrix aqueous












~ Nmiddot 61)6G



~- (ttio ~ J~S~~L


EAi Project ID 3902


State NH





Phone 623-36(10 Fax 624-9463 (37)




tVt-_





bull$

Relinquished by

PONumber 02259252

Quote No 1009476


i ~~pllt-


1-800-287-0525 Fax (603)228-4591






















-- - ~ ~




3

FRONTIEmiddotRI

GLOBAL SCIENCES



J

8

9

10

ll

Received By





5











7











9



Fx 206-622-6870


SOURCE 1112097-03




Sample Spike MS MS




Recovery


Arsenic 403 50030 893 980 85 - 115 FGS-054

Selenium 1196 49990 1267 141 59 - 149 FGS-054

Spike Added

MSD Concentration

MSD Oo Recovery RPD



~





1 1




SOURCE 1112089-17





Mercury 6868 10200 1680 973 71 - 125 EPA 163JE



Mercury 10200 1572 868 660 71 - 125 24 EPA 1631E





13




RECOVERY AND RPD












15



PREPARATION BLANKS








17 middotmiddot



















19

Ii Io



Arthur Auclair


Bow NH 03304





Dear Mr Auclair







Sincerely



Ill I



Date of



Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008


Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008


Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008





C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2






Matrix aqueous


Units ug1




Dilutlon Factor 1

Carbazole lt 1


Naphthalene lt1

Pyrene lt1

Benzo[a)pyrene lt1
















Matrix aqueous












~ Nmiddot 61)6G



~- (ttio ~ J~S~~L


EAi Project ID 3902


State NH





Phone 623-36(10 Fax 624-9463 (37)




tVt-_





bull$

Relinquished by

PONumber 02259252

Quote No 1009476


i ~~pllt-


1-800-287-0525 Fax (603)228-4591






















-- - ~ ~




3

FRONTIEmiddotRI

GLOBAL SCIENCES



J

8

9

10

ll

Received By





5











7











9



Fx 206-622-6870


SOURCE 1112097-03




Sample Spike MS MS




Recovery


Arsenic 403 50030 893 980 85 - 115 FGS-054

Selenium 1196 49990 1267 141 59 - 149 FGS-054

Spike Added

MSD Concentration

MSD Oo Recovery RPD



~





1 1




SOURCE 1112089-17





Mercury 6868 10200 1680 973 71 - 125 EPA 163JE



Mercury 10200 1572 868 660 71 - 125 24 EPA 1631E





13




RECOVERY AND RPD











of 17 111211 O Final Report

15



PREPARATION BLANKS








17 middotmiddot



















19

Ii Io



Arthur Auclair


Bow NH 03304





Dear Mr Auclair







Sincerely



Ill I



Date of



Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008


Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008


Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008





C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2






Matrix aqueous












~ Nmiddot 61)6G



~- (ttio ~ J~S~~L


EAi Project ID 3902


State NH





Phone 623-36(10 Fax 624-9463 (37)




tVt-_





bull$

Relinquished by

PONumber 02259252

Quote No 1009476


i ~~pllt-


1-800-287-0525 Fax (603)228-4591






















-- - ~ ~




3

FRONTIEmiddotRI

GLOBAL SCIENCES



J

8

9

10

ll

Received By





5











7











9



Fx 206-622-6870


SOURCE 1112097-03




Sample Spike MS MS




Recovery


Arsenic 403 50030 893 980 85 - 115 FGS-054

Selenium 1196 49990 1267 141 59 - 149 FGS-054

Spike Added

MSD Concentration

MSD Oo Recovery RPD



~





1 1




SOURCE 1112089-17





Mercury 6868 10200 1680 973 71 - 125 EPA 163JE



Mercury 10200 1572 868 660 71 - 125 24 EPA 1631E





13




RECOVERY AND RPD












15



PREPARATION BLANKS








17 middotmiddot



















19

Ii Io



Arthur Auclair


Bow NH 03304





Dear Mr Auclair







Sincerely



Ill I



Date of



Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008


Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008


Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008





C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2







~ Nmiddot 61)6G



~- (ttio ~ J~S~~L


EAi Project ID 3902


State NH





Phone 623-36(10 Fax 624-9463 (37)




tVt-_





bull$

Relinquished by

PONumber 02259252

Quote No 1009476


i ~~pllt-


1-800-287-0525 Fax (603)228-4591






















-- - ~ ~




3

FRONTIEmiddotRI

GLOBAL SCIENCES



J

8

9

10

ll

Received By





5











7











9



Fx 206-622-6870


SOURCE 1112097-03




Sample Spike MS MS




Recovery


Arsenic 403 50030 893 980 85 - 115 FGS-054

Selenium 1196 49990 1267 141 59 - 149 FGS-054

Spike Added

MSD Concentration

MSD Oo Recovery RPD



~





1 1




SOURCE 1112089-17





Mercury 6868 10200 1680 973 71 - 125 EPA 163JE



Mercury 10200 1572 868 660 71 - 125 24 EPA 1631E





13




RECOVERY AND RPD












15



PREPARATION BLANKS








17 middotmiddot



















19

Ii Io



Arthur Auclair


Bow NH 03304





Dear Mr Auclair







Sincerely



Ill I



Date of



Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008


Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008


Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008





C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2






















-- - ~ ~




3

FRONTIEmiddotRI

GLOBAL SCIENCES



J

8

9

10

ll

Received By





5











7











9



Fx 206-622-6870


SOURCE 1112097-03




Sample Spike MS MS




Recovery


Arsenic 403 50030 893 980 85 - 115 FGS-054

Selenium 1196 49990 1267 141 59 - 149 FGS-054

Spike Added

MSD Concentration

MSD Oo Recovery RPD



~





1 1




SOURCE 1112089-17





Mercury 6868 10200 1680 973 71 - 125 EPA 163JE



Mercury 10200 1572 868 660 71 - 125 24 EPA 1631E





13




RECOVERY AND RPD












15



PREPARATION BLANKS








17 middotmiddot



















19

Ii Io



Arthur Auclair


Bow NH 03304





Dear Mr Auclair







Sincerely



Ill I



Date of



Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008


Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008


Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008





C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2

FRONTIEmiddotRI

GLOBAL SCIENCES



J

8

9

10

ll

Received By





5











7











9



Fx 206-622-6870


SOURCE 1112097-03




Sample Spike MS MS




Recovery


Arsenic 403 50030 893 980 85 - 115 FGS-054

Selenium 1196 49990 1267 141 59 - 149 FGS-054

Spike Added

MSD Concentration

MSD Oo Recovery RPD



~





1 1




SOURCE 1112089-17





Mercury 6868 10200 1680 973 71 - 125 EPA 163JE



Mercury 10200 1572 868 660 71 - 125 24 EPA 1631E





13




RECOVERY AND RPD












15



PREPARATION BLANKS








17 middotmiddot



















19

Ii Io



Arthur Auclair


Bow NH 03304





Dear Mr Auclair







Sincerely



Ill I



Date of



Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008


Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008


Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008





C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2











7











9



Fx 206-622-6870


SOURCE 1112097-03




Sample Spike MS MS




Recovery


Arsenic 403 50030 893 980 85 - 115 FGS-054

Selenium 1196 49990 1267 141 59 - 149 FGS-054

Spike Added

MSD Concentration

MSD Oo Recovery RPD



~





1 1




SOURCE 1112089-17





Mercury 6868 10200 1680 973 71 - 125 EPA 163JE



Mercury 10200 1572 868 660 71 - 125 24 EPA 1631E





13




RECOVERY AND RPD












15



PREPARATION BLANKS








17 middotmiddot



















19

Ii Io



Arthur Auclair


Bow NH 03304





Dear Mr Auclair







Sincerely



Ill I



Date of



Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008


Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008


Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008





C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2











9



Fx 206-622-6870


SOURCE 1112097-03




Sample Spike MS MS




Recovery


Arsenic 403 50030 893 980 85 - 115 FGS-054

Selenium 1196 49990 1267 141 59 - 149 FGS-054

Spike Added

MSD Concentration

MSD Oo Recovery RPD



~





1 1




SOURCE 1112089-17





Mercury 6868 10200 1680 973 71 - 125 EPA 163JE



Mercury 10200 1572 868 660 71 - 125 24 EPA 1631E





13




RECOVERY AND RPD












15



PREPARATION BLANKS








17 middotmiddot



















19

Ii Io



Arthur Auclair


Bow NH 03304





Dear Mr Auclair







Sincerely



Ill I



Date of



Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008


Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008


Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008





C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2



Fx 206-622-6870


SOURCE 1112097-03




Sample Spike MS MS




Recovery


Arsenic 403 50030 893 980 85 - 115 FGS-054

Selenium 1196 49990 1267 141 59 - 149 FGS-054

Spike Added

MSD Concentration

MSD Oo Recovery RPD



~





1 1




SOURCE 1112089-17





Mercury 6868 10200 1680 973 71 - 125 EPA 163JE



Mercury 10200 1572 868 660 71 - 125 24 EPA 1631E





13




RECOVERY AND RPD












15



PREPARATION BLANKS








17 middotmiddot



















19

Ii Io



Arthur Auclair


Bow NH 03304





Dear Mr Auclair







Sincerely



Ill I



Date of



Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008


Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008


Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008





C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2




SOURCE 1112089-17





Mercury 6868 10200 1680 973 71 - 125 EPA 163JE



Mercury 10200 1572 868 660 71 - 125 24 EPA 1631E





13




RECOVERY AND RPD












15



PREPARATION BLANKS








17 middotmiddot



















19

Ii Io



Arthur Auclair


Bow NH 03304





Dear Mr Auclair







Sincerely



Ill I



Date of



Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008


Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008


Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008





C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2




RECOVERY AND RPD












15



PREPARATION BLANKS








17 middotmiddot



















19

Ii Io



Arthur Auclair


Bow NH 03304





Dear Mr Auclair







Sincerely



Ill I



Date of



Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008


Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008


Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008





C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2



PREPARATION BLANKS








17 middotmiddot



















19

Ii Io



Arthur Auclair


Bow NH 03304





Dear Mr Auclair







Sincerely



Ill I



Date of



Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008


Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008


Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008





C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2



















19

Ii Io



Arthur Auclair


Bow NH 03304





Dear Mr Auclair







Sincerely



Ill I



Date of



Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008


Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008


Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008





C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2

Ii Io



Arthur Auclair


Bow NH 03304





Dear Mr Auclair







Sincerely



Ill I



Date of



Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008


Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008


Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008





C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2

Ill I



Date of



Barium lt 0001 10 (103 R) mgL 12911 85 - 115 20 2008


Chromium lt 0001 10 (100 R) mgL 12911 85 - 115 20 2008

Copper lt 0001 094 (94 R) mgL 12911 85 - 115 20 2008

Lead lt 0001 10 (101 ooR) mgL 1291 1 85 - 115 20 2008


Selenium lt 0001 090 (90 R) mgL 1291 1 85 -115 20 2008

Silver lt 0001 011 (108 R) mgl 12911 85 - 115 20 2008

Thallium lt 0001 10 (102 R) mgl 12911 85 - 115 20 2008

Zinc lt 0005 095 (95 R) mgL 12911 85 - 115 20 2008





C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2



C

J a z l uJ 0 ~ ~ ~ -~ ~ ~


z uJ i-0

IF COMPOSITE LU C

~ u






~E ~ si~ 1

= ~ l ~ al

J g


0 c ~ E z- i - g Q ~ t



~~ s ~ 0 a

~ = = i2 lt bull s ~ e 0 I= ~ 8 ~ - Q deg

gs ~ - iii bull ~ ~











A (s C

OR



ELECTRONIC OPTIONS












Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2


Attn Frank Sassaman




Results

ND

Units

mgll

QQ

000400

DIiution JQQ lli12r

000400

Quallflers

Date

AJsl~ze~

120811

~nallrSl

CKV



Total AnUmony

Total Arsenic

Total Barium

Total Beryllium

Total Cadmium

ND

ND

NO 0154

NO ND

mgI

mgL

mgL

mgIL

ugL

mgL

00140

0032

0010

00030

090

00017

00500

0110

0050

00500

100

00500

1

1

1

1

1

1

S1LS2L

S1L

120811

1208111

1208111

1210811

120811

120811

DJB OJB DJB OJB DJB

OJ8

Total Chromium

Total Copper

ND

00085

mgL

mgL

000160

00040

00500

00500 S1LJ

120811

120811

DJB

OJB


Total Nickel

Total Selenlum

Total Silver

Tola Thalllum

Total Zinc

ND 0089

NO 0019

NO

m~L

mgL

mgL

mgL

mgl

00030

OQ18

00060

0015

00050

00500

0060

00250

0050

00500

1

1

1

S1L S2L

S1L S2l

J

1208111 120811

120811

120811

1208(11

DJS

DJB

OJB

DJS

OJB

Page 5 of 17



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2



)5f I Thcfl rlJI Rd

liNolcMdre5$






WO No 1f cent~)d



JO




~CV11~~~~ctE~

RtonQUlshed By






I )IY( ~(Imiddot

~~ ~


~I[~fl Comrient$

~ Ct~eJ ~-t~t

ffl~rnz

CA~f r




i0 w l








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2








METALS


Sample Comments




Report ID 9940856 -1292011 Page 4 of 11










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2










Limit



Parameter LCS


LCS Rec

Rec Limits



-~a R





Report ID 9940856 -1292011 Page 7 of 11



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2



- -



i f~ ishy

J

f

I~ J l s II i

~

~ - ~ ltO



Report ID 9940856 - 1292011 Page 10 of 11

A

shy shy

shy









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2









Reporting




LCS Spike LCS Rec









Report ID 9940856 - 1292011 Page 8 of 11



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2



ANALYTICAL RESULTS





METALS


054 089

ngL ngL

050 050

EPA 1631 EPA 1631

12811 12811

MNP MNP

128111132 12911 1242

MNP MNP

A1 A2

-Sample Comments


Technical Manager



Report ID 9940856 -1292011 Page 6 of 11



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2



December 9 2011




Dear Mr Fish










Technical Manager








COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2





COMP Completed

Definitions





Page 12 of 17

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2

- - --- --------



Attn Frank Sassaman





Sincerely




Reviewed by












Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2








Barium 10598501 0004 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008




Copper 10598501 0002 091 (91 R) 092 (91 R) (0 RPD) mgL 12911 70-130 20 2008

Lead 10598501 lt 0001 10 (101 R) 10 (101 R) (0 RPD) mgL 12911 70-130 20 2008






Zinc 10598501 lt 0005 098 (98 R) 098 (98 R) (0 RPO) mgL 12911 70-130 20 2008



middot

7





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2





Matrix aqueous







5




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2




i w






a -shy -Q

DATE TIME I ~~C) ~





- -


- 2 ta ~ - a 2

- i 2shy $ ~ = 51I M ~~ ~ a 0 ~ ~ - ~ cS = J- t~ ~~ ~ o = i=

co - I ~ 5

~ =

ds - Q 0 j ~ g

_ f ci e ~ ~o ~ ~ e -shy _ agtZ -

X x

~

MICRO OTHER

g ~


c

l] 88 sm- Ila

I(

e








Quon PO_ ___ ___





l ~3L H7







bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2


bull


PREPARATION BLANKS










18




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2




RECOVERY AND RPO




Analyte

Spike Added (ngL)

LCS Concentration

(ngL)

LCS Oo

Recovery Recovery

Limits Method Notes

Mercury 15679 1514 966 80- 120 EPA 1631E

Analyte

Spike Added (ngL)

LCSD Concentration

(ogL)

LCSD

Recovery

RPD Recovery


Mercury 15679 1534 978 131 80 - 120 24 EPA 1631E





16








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2








Analyte


(ngL) (ngL)

MS Concentration

(ngL)

MS

Recovery Recovery

Limits Method Notes

Mercury

Analyte

Mercury

563 10200 1529 947

Recovery Limits

71 - 125

RPD Limit

EPA 163IE

Method Notes


MSD Oo

RPD Recovery

10200 1558 975 186 71 - 125 24 EPA 1631E


_ - A IL-y __-ltL4--~




14




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2




SOURCE 1112097-03




Analyte

Arsenic


(microgL)

403


20200

MS Concentration

(microgL)

2194

MS

Recovery

107

RecoveryLimits

85 - 115

Method

FGS-054

Notes

AS

Selenium

Analyte

Arsenic

1196


20200

20200

MSD Concentration

(microgL)

2319

3257

MSD Ofo

Recovery

113

0o

RPD

553

102

Recovery Limits

85 - 115

59 - 149

RPDLimit

20

FGS-054

Method

FGS-054

AS

Notes



_f ~ A I ~~- __s(J_~




12











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2











Mercury 563 544 202 349 24 EPA 1631E














0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2











0 Standard D High

Comments


6

7

8

9

10

11


-roL s o576Q

ReceVed By

laquo



1 I








-~middot ~shy





1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2


1-


CASE NARRATIVE


SAMPLE RECEIPT













GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2



GLOBAL SCIENCES

09 December 2011

Jeff Gagne


25 Chenell Drive

Concord NH 03301






Sincerely

-Lmiddot~~~

Liz Siska

Project Manager

2 middot f

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2

bull JJA l

eastern analytical

Arthur Auclair

Northeast Utilities

97 River Road

Bow NH 03304

~ ACCoR -v o

f ~ lt





Dear Mr Auclair






Sincerely

JJ11 oC







Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2





Matrix aqueous










Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2






Matrix aqueous

Date Sampled 113011


Units mgL



Analyst LAS

Method 1664A

DIiution Factor 1



bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2

bull





Matrix aqiueous

Date Sampled 113011


Units ug1




Dllutlon Factor 1

Phenol lt 1







Pyridine lt5


2-Nitrophenol lt 1





3-Nitroaniline lt 1



Azobenzene lt 1

















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2
















Matrix aqueous

Date Sampled

Date Received

111711

111711 Units

Analysis



lt5 44

mgL mgL

111711 1515 111711 1359

2540D 3000

DLS KL


045 151 lt6 59

lt 005 65


112111 900 4500CNE 111811 14304500NorgC 111711 1543 5210B 111811 1110 H8000 111811 900 4201 111711 1727 4500H+B

KJR KL

SKC SKC JCC CJJ





WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2



WastewaterSample ID


Matrix aqueous


Units mgL




Dilution Factor 1









Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2







Units ug1



Analyst JMR

Method 625mod

Dilution Factor 1







2-Nitroaniline lt5

Benzyl alcohol lt5



2-Nitrophenol lt 1








Azobenzene lt 1















Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2














Bow New Hampshire




11172011 (mgL)

11302011

BOD - lt6 lt 6

COD - 59 110


Fluoride - 44 6



OampG 250 lt5 lt5

loH 5-95 65 71

TS$ - lt 5 lt5

VOCEPA624 - (I) 0002 (I)

sVOCEPA625 - ND ND












l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2




l11ltIIYUvdl ft)Ul)





TSS Lead

TOC Mercuri


Aluminum - Nickel



Barium Selenium

IBervllium Silver

Cadmium Thalium










1--b ljrD J J

Y- ~e


SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2

SMR SUMMARY SHEET



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2



ai)


ANALYTICAL NOTATION






CERTIFICATION


AR-1311

AR-1311-2

Engineen and Inc. GeoEnvironmental, GZA l · Public Service of New Hampshire Bow, New Hampshire...

Documents

Transcript of Engineen and Inc. GeoEnvironmental, GZA l · Public Service of New Hampshire Bow, New Hampshire...