WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

76
Bulletin No. 336 DEPARTMENT OF THE INTERIOR UNITED STATES GEOLOGICAL SURVEY . GEORGE OTIS SMITH, DIRECTOR WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF COKE CONDUCTED BY THE UNITED STATES FUEL-TESTING PLANT AT ST. LOUIS, MO. JANUARY 1, 1905, TO JUNE 30, 1907 BY RICHARD MOUDENKE, A. W. BELDEN AND G. R. DELAMATER WITH INTRODUCTION BY J. A. HOLMES IN CHARGE OF TECHNOLOGIC BRANCH WASHINGTON GOVERNMENT PRINTING OFFICE 1908

Transcript of WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

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Bulletin No. 336

DEPARTMENT OF THE INTERIOR

UNITED STATES GEOLOGICAL SURVEY. GEORGE OTIS SMITH, DIRECTOR

WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF COKE

CONDUCTED BY THE

UNITED STATES FUEL-TESTING PLANT AT ST. LOUIS, MO.

JANUARY 1, 1905, TO JUNE 30, 1907

BY

RICHARD MOUDENKE, A. W. BELDEN AND G. R. DELAMATER

WITH INTRODUCTION BY

J. A. HOLMES

IN CHARGE OF TECHNOLOGIC BRANCH

WASHINGTONGOVERNMENT PRINTING OFFICE

1908

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CONTENTS.

I'agc.Introduction, by Joseph A. Holmes......................................... 5Washing tests; by G. R. Delamater......................................... 8

Report for 1905.......................................................... 8Improvement in equipment........................................ 8Personnel......................................................... 9

Report from January, 190G, to June 30, .1.907.............................. 9Equipment and operation.......................................... 9Personnel........................................................... 10Explanation of tables.................................. i............ 10

"Percentage of reduction" and "amount actually removed"..... 10Formulas..........1.....'....................................:.. 11

Tests made........................................................... 11Coking tests, by A. W. Belden.............................................. 18

Equipment. ..J.................................................... ̂ .. 18Personnel............................................................. 19Procedure of tests...................................................... 19Extent of tests........................................................ 19

Tabulation of results.................................:.................. 20Descriptions of cokes and remarks.............................'......... 36Conclusions. ........................................................... '45

Cupola tests of coke, by Richard Moldenke.................................... 48Equipment........................................................... 4.8Personnel............................................................. 48Method of testing....................................................... 48Detailed results....................................................... 49

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ABBREVIATIONS.

In describing fuels, especially as to size, use is made of the following abbreviations:

e.=egg.f. c. = finely crushed.f. scr.=finely screened.l.=lurnp.n.=nut.p.=pea.r. o. m.=run of mine.

s.=slack. sc.=screenings. std.=standard. thr.=through. w.=washed. x/ =inch or inches.

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WASHING AND COKING TESTS OF COAL AND CUPOLATESTS OF COKE CONDUCTED BY THE UNITED

STATES FUEL-TESTING PLANT AT ST. LOUIS,JANUARY 1, 1905, TO JDNE 30, 1907.

By RICHARD MOLDENKE, A. W. BELDEN, and G. R. DELAMATER.

INTRODUCTION.By JOSEPH A. HOLMES.

The tests of washing and coking coals and of the behavior of the resulting coke in cupola practice, as reported herein, were made during the fiscal years 1905 and 1906 at the St. Louis fuel-testing laboratory of the United States Geological Survey. These tests were carried on in connection with similar investigations of the steaming and gas-producing qualities of the same coals and of the possibility of improving such coals by briquetting. This work was a part of the general inquiry concerning the most economical manner

.of utilizing each type of coal tested.Many coals as received from the mine were found to be too high in

ash, in sulphur, or in phosphorus to make satisfactory metallurgical coke without prior treatment, and some coals possessed better coking qualities than others. It was found that the washing of some coals so reduced the percentage of ash and sulphur as .to make available for the production of coke a- coal which otherwise would have had no value for this purpose. In the following pages are reported the details of the washing of coal, the production of coke therefrom, and the behavior of the coke in the cupola when utilized for the production of castings, the results of each test being tabulated in full. A study of these tables indicates many important facts as to the behavior and treatment of the coals mined in the various portions of the 'United States when prepared as metallurgical coke.

The washing tests of 1905 were not as satisfactory as the later tests because of inadequate storage facilities and the lack of certain equip­ ment, but the latter was added in time for the tests of 1906. An

5

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6 WASHING, COKING, AND CUPOLA TESTS.

important result of the washing tests is shown in the percentage of ash and sulphur actually removed. The reduction of these impuri­ ties by washing, of course, increases the percentages of fixed carbon, and volatile matter over the amounts present in raw coal. These facts, the number of washings, and the methods of washing, are recorded, thus furnishing valuable data as a guide to the treat­ ment necessary to render each coal tested most suitable for coking. Altogether there were 101 regular washing tests and 12 special tests.

The results of these tests show an increase in moisture of 10 to 30 per cent, a reduction in ash in the 1905 tests of 15 to 50 per cent and in the 1906 tests of 20 to 60 per cent, and a reduction in sulphur in the 1905 tests of 10 to 40 per cent and in the 1906 tests of 10 to 50 per cent. A few examples of the total amount of reduction may be mentioned. A raw coal containing 5.05 per cent of sulphur con­ tained after washing 2.47 per cent, a total removal of 55 per cent. Proportionate reductions in sulphur were made in coals containing lesser amounts. The ash in a raw coal containing 42.56 per cent was reduced by washing to 29.67 per cent, a total removal of 65 per cent. In a similar manner ash in a raw coal containing 15.72 per cent was reduced to 10.16 per cent, a total removal of 41 per cent; and in a coal containing 9.81 per cent to 5.38 per cent, a total removal of 59 per cent. It is evident that coals which are in the raw state utterly unfit for steaming purposes can be made fairly good steaming coals by washing, and that coals unsuited for coking can be made available in the same way.

It is proposed to conduct during the next fiscal year washing tests with much improved apparatus at the fuel-testing plant recently established at Denver, Colo., where experiments in washing and coking will be made on the coals mined in the Rocky Mountain region, with a view to determining what can be done to make them available for the production of metallurgical coke.

The coking tests were made in ovens of the regular beehive pattern, two of standard size 7 feet high, and one of standard diameter 6 feet 4 inches high. Samples of coke were taken from five different parts of the oven in practically the same location for each test, so as to give a standard method of comparison for each coke. The present report covers 192 tests, made on 100 coals, the samples having been col­ lected from 17 States and 1 Territory. One hundred of these tests were made on raw coal, 82 on washed coal, and 10 under miscellane­ ous conditions. In some of these tests it was found that the addition of pitch produced coke from coal which wben tested raw gave either no coke or coke of an inferior quality. In other tests the addition of pitch did not improve the quality of the coke. The tabulated results of the coking tests should be studied in the light of the description of the resulting coke which accompanies the tables. The physical tests

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INTRODUCTION. 7

to determine the compressive strength of the coke or, in other words, the height of the furnace burden which the coke will sup­ port showed only the worthlessness of such determinations. The compressive strength of a given coke made with the same coal ranged from about 700 pounds ultimate strength per square inch to over 2,000 pounds. As a coke with compressive strength of 48 pounds will support the burden of any modern furnace, it is evident that this test is of little or no practical value, especially as the burden borne by the coke may be greatly modified by the action of heat, by attrition, and by other factors. The inquiries seem to indicate that the yield of coke is increased and the proportion of breeze reduced by preliminary crushing. Further experiments are necessary to verify these determinations, as well as to indicate the limit of fine­ ness of such crushing. Fine crushing appears to increase the strength of the coke, which is apparently influenced also by the amount and distribution of ash.

More complete coking tests will be carried on with a view to pro­ curing more conclusive data along the lines above indicated, also with a view to determining more accurately the loss of sulphur from coal to coke, which varies with the coals and the method of treat­ ment. These coking tests are being continued at the new plant at Denver on beehive ovens with two heights of crown, in order to deter­ mine the treatment necessary to produce good metallurgical coke from the coals mined in the Rocky Mountain region.

The great need of the immediate future in connection with coking experiments is the conduct of such tests in by-product ovens, and it is hoped that funds may soon be had which will permit the erection and operation of such ovens.

The cupola tests of coke in 1905 and 1906 were carried on along lines fully described in Professional Paper No. 48. The. results as set forth in the following tables give the details of 170 cupola tests. The data concerning record of melt, taken in connection with the indications of the source of the coals and the analyses of the corre­ sponding coke, furnish interesting facts as to the melting ratio of iron to coke, the rate of melting per' hour, and the amount of iron recovered. Equally interesting is the table giving the chemical effect on iron from cupola tests of cokes made from coals mined in various States. It is not contemplated that these cupola tests will be continued during the fiscal year, in view of the necessity of devot­ ing the available funds to the study of the coking qualities of western coals.

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WASHING TESTS.

By G. R. DELAMATER.

REPORT FOR 1905.

IMPROVEMENT IN EQUIPMENT.

The lack of adequate storage facilities and the constant demand on the weighing and conveying apparatus for delivering coal to the other sections of the fuel-testing plant, which greatly interfered with the washing tests made during 1904,a were again felt in 1905 and tended somewhat to vitiate the results, although much improvement was made in the equipment.

In order to eliminate these difficulties, important changes were made during the year in the arrangement of the washer equipment. The storage capacity available during 1904 was increased'from 175 tons to 350 tons. Additional "shed bins" of 150 tons aggregate capacity were provided outside the washer plant for storing coal at .times when the regular washer bins were filled.

The coal was shoveled from the cars direct to the crusher or to a topper scale. By means of a combination elevator conveyor the coal could 1)6 ttansleired fr-om the hopper scale or crusher to any one of the twelve regular storage bins, or from-one bin to another; or could be transferred to belt conveyors for delivering the coal to the boiler section and. pther divisions of the plant. The elevator conveyor referred to was relieved of a large portion of the work of handling coals for the gas-producer and boiler sections by a 30-inch Jeffrey belt conveyor, wjiich was installed to run from the car siding to the bins of these sections for the purpose of delivering coal to them direct from the cars.

All washing tests made during 1905 were made on the Stewart jig used during 1904, at a speed of 35 revolutions per minute and 6-inch stroke. The sludge-recovery system, with the customary perforated- bucket elevators, was used in reclaiming the washed coal and refuse

oCompare the following U. S. Geological Survey publications: Bull. No. 261,1905, p. 00; Prof. Paper No. 48, 1906, p. 1460.

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WASHING TESTS. 9

after washing. Owing, however, to the fact that there were only two sludge tanks one for the washed coal and one for the refuse only one jig could be operated at a time, since if two or more jigs were operated their output would become mixed in the sludge tanks.

With the existing arrangement of the washery it was necessary to use the same water over and over again. The washed-coal sludge tank, supplied with water from the city mains, was used as a reser­ voir from which the water was delivered, principally beneath the screens of the jigs. A considerable amount of fine coal was thus car­ ried over from the sludge tank. The bulk of this fine coal settled to the bottom of the jig body, where it became mixed with the refuse and was carried on to the refuse sludge tank.

All coals tested were passed through an 18 by 24 inch Cornish tooth-roll crusher, which breaks the coal down to a maximum size of about 2 inches, although, of course, a considerable proportion may be much smaller, depending on the nature of the coal.

The. power for operating the plant was furnished by a 12 by 16 inch Frost steam engine, belted to a main shaft from which the jigs and other machinery of the plant were driven. The steam for this engine was received from the boiler section.

PERSONNEL.

The 1905 tests were made under the direction of John D. Wick.

REPORT FROM JANUARY i, 1906, TO JUNE 30, 1907.

EQUIPMENT AND OPERATION.

On February 22, 1906, the washery plant was almost entirely destroyed by fire, and with it a few samples of coal that were on hand in the storage bins. The plant was immediately rebuilt, the former arrangement being followed throughout.

From January 1 to December 15, 1906, one Stewart jig was used in making all the washing tests. During December, 1906, a special jig was installed. This jig was of the center-plunger type, i. e., the plunger was directly beneath the screen, and the upstroke of the plunger caused the pulsation. The plunger had no valves, but valves Avere arranged in the sides of the jig body to admit the supply water on the downstroke of the plunger. Cams and springs were used in such a manner that the plunger had a slow downward and a quick upward stroke. The screen of this jig was. 4 feet wide by 5 feet long and was made of strips of No. 10 wire running lengthwise of the screen frame and set one-sixteenth inch apart. The length of the stroke was adjustable up to 4 inches. The depth of the coal bed was also adjustable.

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10 WASHING, COKING, AND CUPOLA TESTS.

Owing to the fact that the power for operating the washer plant was furnished by a 12 by 16 inch Frost steam, engine, belted to a main shaft from which the jigs and other machinery were driven, it was impossible to change the speed of the jigs. Better results could have been obtained on some coals tested had it been possible to change the speed to suit the length of stroke used.

As the only crusher available for this work was an 18 by 24 inch Cornish tooth-roll crusher, it was impossible to crush some coals down as fine as they should have been crushed. However, an adjustable- mesh bumping screen was installed in January, 1907, in such a man­ ner that the coal was first passed over this screen, and the tailings then passed on to the crusher, while the fuel which went through the

.screen dropped into the bin over the jig. The product of the crusher was then elevated again to the screen, and this cycle of operation was repeated until all the coal passed through the screen.

In December, 1906, a float and sink testing equipment was installed. Before each washing test was made, samples of the raw coal, quar­ tered down to 2 kilograms each, were tested on four 'different specific- gravity solutions. In this manner it was possible to make a prelimi­ nary determination of the result of a separation under varying per­ centages of washed coal and refuse. The coal was then washed with the jig regulated to discharge as refuse a percentage about equal to the percentage found advisable from the float and sink tests. After a washing test was made, a sample of the refuse was taken and quar­ tered down to four samples of 2 kilograms each, and these were also tested on the specific-gravity solutions. The test showing the high­ est percentage of float coal and having an analysis which agreed fairly with that of the washed coal was then used in determining the percentage of "loss of good coal in the refuse." In this manner the efficiency of the test was shown.

PERSONNEL.

John D. Wick, assisted by Edward Moore, was in charge of the washing tests from January 1 to June 30, 1906; J. H. Gould from July 16 to October 12, 1906; and G. R. Delamater from November 15, 1906, to June 30, 1907.

EXPLANATION OF TABLES.

"Percentage of reduction" and "amount actually removed." The "percentage of reduction" is the comparison made of the percentages of the impurities in the raw coal and in the washed coal. It will be readily understood that if the ash alone is reduced by washing, the fixed carbon and volatile matter will form a higher percentage of the washed coal than of the raw coal. In actual practice, however, it is

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WASHING TESTS. 11

impossible to make so perfect a separation that the washing process will not remove portions of some constituents other than the impu­ rities, and therefore the percentage of each constituent in the washed coal is affected by the reduction of each of the other constituents. This is clearly indicated in test 192, on Alabama No. 6, and test 198, on Virginia No. 6. A comparison of the raw-coal and washed-coal analyses in these two tests shows that in the test on Alabama No. 6 the percentage of sulphur was the same in the washed coal as in the raw coal; and in the test on Virginia No. 6 the sulphur in the washed coal was higher than in the raw coal. It will therefore be seen that a simple comparison of the raw-coal and washed-coal analyses will not always show whether any of the sulphur in the raw coal was actually removed with the refuse in washing.

Formulas. In order that these percentages might be determined, the following formulas were compiled and used in making up this report. It will be noted by referring to the test data (p. 15) that 10 per cent of the original sulphur in the raw coal was actually removed with the refuse in washing Alabama No. 6, and that 13 per cent was actually removed in washing Virginia No. 6:

Let X = the percentage of reduction of any constituent.Y = the percentage of any constituent removed by washing.M = the percentage that the amount of the constituent in the

washed coal is of the raw coal..a = the percentage that the washed coal is of the raw coal. & = the percentage of the constituent in the washed coal. c = the percentage of the constituent in the raw coal.

Then X = , M = a&, and Y = ̂ ^.c ' ' c

TESTS MADE.

Sixty-three domestic samples of fuel from fourteen States and Ter­ ritories and two samples from Argentina were washed during the period covered by this report. The detailed results of the tests are given in the following tables.

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Details of washing tests of bituminous coals in 1905.

^ s%6i* §̂

101 104 108 102 103 106 107 105 110 111 109

115 112 113 114 118 117 116

130

119 121 122 125 133 138'

137 131

120 124 123 126

134

127

128 132 135 136

129

Field No. of coal.o

Illinois: 6..............70...........7D.. .........9 A...........10.............12.............13.............14.............15.............16.............18.............

Indiana: 3..............4..............6..............7 A...........8..............9B...........10.............

Maryland : 1....... .......

Ohio: 1....... .......2..............3..............

6..............7..............8..............9 B. ..........

Pennsylvania:

6..............7..............

- 9..............

Virginia: 2..............

West Virginia: 4B. ..........

16B.. ........17............20.............21.............

Wyoming: 3..............

Bed.

No.6............do...........do...........do......No. 7.......No. 0.......No. 7.......No. 5.......

No. 7.......No. 2.......

No. 5.......No.6.......No. 4.......No.5.......No. 7............do......No.6........

Lower Kit- tanning.

No.5.......No. G.......No. 8............do......No. 7.......No.6.......

Pittsburg. . .

.....do......Lower Kit-

tanning.

McConnell . .

Upper Free- port.

Pittsburg. . . Bakerstown. Keystone... Peerless.....

(f)

Date of test.

May 15 June 26 July 8 May 22 May 26 July 6 ...do....June 29 July 12 July 28 July 12

Aug. 7 July 25 Aug. 4 Aug. 7 Aug. 31 Aug. 24 Aug. 21

Oct. 20

Sept. 8 Sept. 13 Sept. 19 Sept. 27 Nov. 8 Dec. 16 Dec. 15 Oct. 25

Sept. 13 Sept. 26 Sept. 23 Oct. 5

Nov. 13

Oct. 9

Oct. 14 Oct. 27 Nov. 29 Dec. 11

Oct. 19

Size of coal. (See p. 4.)

As shipped.

r. o. m. s. r. o. m. r. o. in. s. r; o. m. 1J"-0".

I., e. l.,e. 1.

n., s. sc. r. o. m. 1., e., n. 1. r. o. m. 1.

r. o. m.

r. o. m. r. o. m. r. o. m. over J". r. o. m. over 1J". r. o. m. n., s.

over }." r. o. m. r. o. m. r. o. m.

r. o. m.

r. o. m.

s. r. o. m. r. o. m. r. o. m.

r. o. m.

As washed.

thr.- 2". s. thr. 2". thr. 2". s. thr. 2". thr. 2". thr. 2". thr. 2". thr. 2". thr. 2".

thr. lj". thr. li". thr. 2". thr. 2". thr. 2". thr. 2". thr. 2".

thr. 2".

thr. 2". thr. 2". thr. 2". tnr. 2". thr. 2". thr. 2". thr. 2". thr. 2".

thr. 2". thr. 2". thr. 2". thr. 2".

tlir. 2".

thr. 2".

s. thr. 2". thr. 2". thr. 2".

thr. 2".

Amount of coal.

Raw (Ibs.).

14. 710 15,809 14, 000 18. 000 14, 710 18, 000 29, 950 18, 000 18, 000 14,000 18,000

50,000 32, 000 24,000 14,000 16, 000 18, 000 18,000

45,500

26,900 32, 420 47, 125 29, 120 24,000 16,000 17,200 46,530

30,920 50, 000 32,000 12, 000

28,000

26, 000

22,825 29,530 49,150 24,000

24, 120

. Washed.

Lbs.

13, 586 11,238 11, 790 13,920 12, 795 15,900 27, 550 15, 955 13, 035 12, 500 14, 400

36, 000 24, 000 19, 100 12, 240. 15,080 15, 460 15,300

37,450

23, 750 25, 625 34,800 26.000 20,400 14,000 15,560 37,830

29,000 43, 300 27, 180 9,700

24, 550

21, 000

19,800 24,765 24,590 22,000

20,060

Per cent.

92 71 84 78 87 88 92 89 72 89 80

72 75 80 87 94 86 85

82

88 79 74 89 85 88 90 81

94 87 85 81

88

79

87 84 87 92

85

Refuse.

Lbs.

1,124 4, 571 2,210 4,080 1,915 2,100 2,400 2,045 4, 965 1,'500 3,600

14,000 8,000 4,900 1,760

920 2,540 2,700

8,050

3,150 6,795

12, 325 3,120 3,600 2,000 1,640 8,700

1,920 6,700 4,820 2,300

3,450

5, 600

3,025 4,765 0,560 2,000

4,060

Per cent

8 29 16 22 13 12 8

11 28 11 20

28 25 20 13 6

14 15

18

12 21 26 11 15 12 10 19

6 13 15 19

12

21

13 16 13 8

15

a Detailed account of the field origin and collection of each sample of coal may be found in Bull. U. S. Geol. Survey No. 290, 1906.

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WASHING TESTS. 13

Details of washing tests of bituminous coals in 1905 Continued.

Washing test

No.

101104108102103106107105110111109115112113114118117116130119121122125133138137131120124123126134127128132135136129

, Chemical analyses (percent).

Raw coal.

Mois­ ture.

14.4310.6910.8313.549.508.208.31

12.779.958.43

12.3913.1813.9910.808.909.55

13.5310.722.337.719.019.903.53'5.316.657.558.102.463.244.093.093.353.915.573.462.823.57

15.12

Vola­ tile

matter.

29.4833.0836.2435.6931.9832.2631.6534.6834. 7630.0836.8931.9229.40

' 36.0938.5236.1934.8039.2916.1138.3235.8533.6037.4536.7233.9438.0036.8734.4831.7820.6217.2935.1326.6831.6127.2932.2036.3834.36

Fixed carbon.

42.8136.1439.7540.0347.0846.5949.5640.7742.0651.8941.8039.2742.2940.4943.3743.6540.9141.4268.4342.0243.8044.8649.9049.4548.8646.0843.1057.0152. 4662.8268.2955.9459.3054.4561.1356.9555.2033.82

Ash. -

13.2820.0913.1810.7411.4412.9510.4811.7813. 239.608.92

15.6314.3212.62.9.2110.6110.768.57

13.1311.9511.3411.589.128.52

10.558.37

11.936.05

12.5212.4711.335.58

10.118.378.128.034.85

16.70

Sul­ phur.

4.014.064.534.031.453.481.554.16'3.871.143.924.792.314.393.743.723.153 fii .001.494.614.021.813.473.333.132.843.35.88

1.942.082.04

.921.071.201.451.381.-326.66

Washed coal.

Mois­ ture.

15.2316.6412.4515.6511.8013.3011.1516.3211.8110.1414.9915.0216.4911.6510.1611.7614.5510.673.679.25

10.779.963.336.167.47

11.779.494.914.315.674.586.394.475.415.335.706.35

19.16

Ash.

8.648.599.307.576.678.917.499.378.418.005.778.617.259.837.899.528.146.15

10.618.577.427.747.480.386.376.037.454.577.26

10.088.753.957.765.915.504.643.476.52

Sul­ phur.

3.303.253.653.381.382.481.273.293.001.022.983.251.943.493.243.182.563.341.093.722.951.363.272.942.162.072.88

on. y\j1.471.551.24.88.81.92

1.141.071.004.16

Reduction (percent).

Ash.

3557293042'

312920361635454922141024281928353317254028382442192229232932422861

Sul­ phur.

18201916

52918212311243210211315191327192725

612312714

242539

4242321222438

Actually re­ moved (per

cont).

Ash.

4070414fi4ft39342!)542,'i4860ea382<>103.53')3137

' 48. 51

27364735 492950313038393943503407

Sul­ phur.

244332341737252944203951373025203026472942441525393531

335375110

' 313334333047

Details of washing tests, January 1, 1906, to June 30, 1907.

4*

43

¥03£

103 161

159 195 192

187 187a

139 141 144 140

142 160 151 150 146

Field No. of fuel.o

Alabama: 2B. .......... 3.............

4.............5c. ...........6.............

Argentina:

1. ............Arkansas:

IB...........7B. ..........8..............9.............

Illinois: 20............21............22A. ......... 22B. .........23A. .........

Designation of bed.

.Tagger......... Underwood or

Thompson. Youngblood . . . Black Creek . . . Pratt.. ........

Huntington . . . Hartshorne. . .

(?) Huntington . . .

No. 0. .............do.........

.....do.........

.....do.........

.....do.........

Date of test.

May 26,1906 May 23,1906

May 21,1906 Jan. 15,1907 Jan. 12,1907

Nov. 13,1906 Dec. 24,1906

Dec. 30,1905 Jan. 15,1906 Jan. 29,1906 Jan. 4, 1906

Jan. 18,1906May 21,1906 Feb. 16,1906 Feb. 13,1906 Jan. 31.1906

Jig used. 6

Stewart. . .....do....

.....do....

Special . . .

Stewart . . .....do....

.....do....

.....do....

.....do....

.....do....

.....do....

.....do....

.....do....

.....do..'..

.....do....

Size of fuel. (See p. 4.)

om g< «f

r. o. in. r. o. m.

r. o. m.

r. o. m.

r. o. m. r. o. m.

s. s. No. 4.s.

sc.1. 1. sc. 5"1.

e <u3n <

thr. 2". thr. 2".

thr. 2". "tnr'.'l''."

thr. 2". thr. 2".

s. s. "thr. 2".s.

sc. thr. 2". sc. sc. thr. 2".

Weight of raw fuel (tons).

7.93 9.00

8.50

12.00

18.00 5.50

30.59 25.00 11.50 38.65

31. 64 8. .50 9.70

20.00 14.00

Amount washed

fuel.

s>?'53 o £S

6.85 8.25

7.23

10.75

9.00 3.30

23.00 19.00 9.78

28.67

28.50 7.32 8.50

16.00 12.00

fed Ang

86 92

85 ""96

50 60

75 76 85 74

90 86 88 80 86

o Detailed account of the field origin of each sample of fuel may be found in Bull. U. S. Geol. Survey No. 332.

6 Stewart jig speed 35 revolutions per minute, with 6-inch stroke; special jig speed, 70 revolu­ tions per minute, with 2i-inch stroke.

c Not enough coal for other than special float and sink tests.

Page 14: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

14 WASHING; COKING, AND CUPOLA TESTS.

Details of washing tests, January 1, 1906, to June 30, ^907 Continued.

43

MOf'03

£

147 169 166 162 164 165 181 183 184 190 190a 196 197

145 185

176 175

191 191a 148

143 182

149 155 152 154 153

1C8

174 170 167

193

179 188 189 194

171 172

156 157

158 173 178

198

186 180

177

Field No. of Fuel.

Illinois Cont'd. 23 B .......... 24A. ......... 24 B.......... 25A. .........26............27....:.......28C.. ........ 29A. ......... 29A. .........30............30............34A. ......... 34 B ..........

Indiana: 12.............20........:...

Indian Territory: 2B. ..........8.............

Kansas: 2B...........2B. ..........6.............

Kentucky: 2.B. ..........9A. ..........

Missouri: 5.............6<»............7A. ..........7Ao..........7B. ..........

New Mexico : 3C... ........

4A. ..........4B........... 5.............

Ohio: 12............

Pennsylvania: 12............15............

. 17............20............

Tennessee: 1. ............5.............

7B...........8A,8B......

9B/9C. ...... 10.....:......11............

Virginia: 6.............

West Virginia: 22A..........23 B ..........

Miscellaneous : 10............

Designation of bed.

No. 6.. ........ .....do......... .....do......... .....do.........No. 5. .........No. 6..........No. 7.......... No. 5.. ........ .....do.........No. 7.. .............do.........No. 5.. ........ .....do.........

.....do.........Brazil Black . .

Hartshorne'. .. (?)

Weir-Pittsburg

.....do.........

No.9. .'........

(?) (?)

(?) (?) (?)

MainEaton,or Lower Lara- mie.

.....do.........

.....do.........

.....do.........

No. 8..........

B, or Miller.... Upper Freeport. Lower Kittan-

ning.

Brushy Moun­ tain.

Wilder........First above

Sewanee. Sewanee ....... Battle Creek . .

(?)

No. "4. .........

(?) Cedar Grove . . .

Date of test.

Feb. 1, 1906 June 8, 1906 June 1, 1906 May 24,1906 May 26,1906 May 29,1906 Sept. 26, 1906 Oct. 13,1906 Oct. 16,1906Jan. 5, 1907Feb. 11,1907 Feb. 15,1907 Feb. 12,1907

Jan. 30,1906 Nov. 14,1906

July 13,1906 July 1,1906

Jan. 10,1907 Jan. 21,1907Jan. 8, 1906

Jan. 19,1906 Oct. 1, 1906

Feb. 10,1906 Feb. 21,1906 Feb. 17,1906 Feb. 22,1906 Feb. 19,1906

June 6, 1906

June 19,1906 June 9, 1906 June 2, 1906

Jan. 25,1907

Sept. 20, 1906 Feb. 4, 1907 Feb. 6,1907 Jan. 29,1907

June 12,1906 June 13,1906

May 1, 1906 May 15,1906

May 19,1906 June 14,1906 Septi 11, 1906

Feb. 1,1907

Oct. 25,1906 Sept. 25, 1906

Aug. 7, 1906

Jig used.

Stewart . . .....do.... .....do.... .....do.... .....do.... .....do.... .....do..... .....do.... .....do.........do....Special . . . .....do.... .....do....

Stewart. . .....do....

.....do....

.....do....

Special. . . . .....do....Stewart...

.....do....

.....do....

.....do....

.....do....

.....do....

.....do....

.....do....

.....do....

.....do....

.....do....

.....do.....

.....do.... Special.... .....do.... .....do....

Stewart . . .....do....

.....do....

.....do....

.....do....

.....do....

.....do....

Special....

Stewart... .....do....

.....do....

Size of fuel. (Seep. 4.)

TJ ra PJ

<J ft'%

S.sc. -1.r. o. in. r. o. m. r. o. m. 1. sc. sc. n. n. sc. r. o. ni.

r. o. m. sc.

s. S.

s. s.1.

cokebr. n.

r. o. m. 1. No. In.

No.2n.

s.

r. o. m. s. r. o. m.

r. o. in.

r. o. m. r. o. m. r. o. m.r. o. m.

r. o. m. r. o. m.

s. r. o. m.

s. l"s.8.

r. o. m.

n. &s.n. &s.

s.

As used.

s. sc. thr. 2". thr. 2". thr. 2". thr. 2". thr.. 2". sc. sc. thr.2i". thr. 1". thr. 1". thr. 1".

thr. 2". sc.

s. s.

s. s. thr. 2".

coke br. n.

thr. 2", thr. 2". No. 1 n.

No.2».

s.

thr. 2". s. thr. 2".

thr. 2".

thr. 2". thr. 1".thr. 1".thr. 1".

thr. 2". thr. 2".

s. thr. 2".

s. l"s.s.

thr. 1".

n. &s.n. & s.

s.

Weight of raw fuel (tons).

40.00 10.00 9.37 7.27 9.00 9.00

12.00 9.00

29.75 15.00 12.45 24.65 14.00

20.00 30.00

19.00 18.80

23. 00- 39.00 12.00

9.56

7.65

12.50

11.75

21.50

10.00 12.00 7.50

6.70

10.60 20.37 7.28

22.21

10.80 '9.22

15.50 49.00

9.69 30.25 21.00

8.31

19.25 18.00

28.28

Amount washed

fuel.

I?«sP-ii

31.50 7.50 8.33 6.00 8.00 7.77 9.96 6.87

20.75 11.60 10.10 19.55 11.81

17.53 20.30

14.53 16.15

18.10 25.25 11.00

7.84

6.45

10.73

9.30

19.00

8.14 10.50 6.65

5.10

8.45 15.25 6.30

17.25

9.30 8.00

10.50 43.00

7.21 23.70 13.75

6.75

16. 25 16.99

20.08

03^ p^g

79 75 89 83 89 86 74 76 70 77 81 80 85

89 68

78 86

79 65 92

82

84

86

79

88

81 88 89

76

80 76 87 78

8687

6888

75 78 65

81

85 94

71

a Destroyed by fire vhen plant was burned.

Page 15: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

WASHING TESTS. 15

Details of washing tests, January 1, 1906, to June, 30, 1907 Continued.

6

u0 fcj

Iwd^

103101159195192187187ft139141144140142100151150146147169166162164165181183184190190ft190197145185170175

19 la148143182149155152154153108174170107193179188189194171172150157158173 178198180180177

Amountof refuse.

fCw.°0 rt? 2t^*-^

1.08.75

1. 20

1.259.002.207. 59c>! oo1.719.973.141.181.204.002.008.502.501.041.271.001.222.032.129.003.402.355.102.192.479.704.472.054.90

13.751.00

1.711.20

1.70

2.452.50l.SO1.50.85

1.002.155.12.98

4.961. 501.225.006.002.486.557.251.563.001.018.20

R Ooo>

14

15

1050402 £ 'J

2415201014122014212511171114

' 202430231920151132221421358

1810

14

21121912112420251322141332122322351915

629

Chemical analyses of fuel (percent).

Raw.

83W'o3

3.953.036.435. 693.397.107.107 490. 895. 195. 20

14.6815. 3011.9113.0313. 4715. 0811. 4411.4411.3515. 6810.007.78

13. 1013. 1011. 0911.099.337.81

10. 5710. 910.273.778.01.8.019.04

8.7012.92

16.30

16.394.362.783.382.724.141.963.134.354.004.815.597.883.125.082.923. 535.024.593.250.07

Po|J> O

30.7030. 9428. 5053. 2863. 5730.9730.9715.1615. 2310.4914. 7131.3230. 5935. 6532. 0534. 3531.2833. 9333.9334. 0232. 4132.4129. 8530.7830.7839. 42

' 39.4247.8050.2735. 3038.8732.3732. .6545. 2245. 2229.69

35.0033.64

29. 12

29.0132.2134.3134.6331.8547.1830.5569.4555.9969.5732. 9133. 6228.2832.9125.36

20. 7561. 5252.2334.6131. 01

oS O . 0§SJ2.2

Fn

50. 7655. 31.52.0925.0526. 2019.3719.3759. 3802. SS70.3155. 2240.3243.4039. 4339. 7940. 6537. 4543.9243.9240. 6339.8237. 8252. 3940.1240. 1235.7035. 7030. 9233. 5442. 7526. 85

. 47.0751. 1526.3920. 3945. 55

47. 3439.82

35.01

34.4247. 5148.3448. 4550.8639.3058.2417.6127. 7615.8951. 1351. 0346.4349.8550.41

47.8523.0733.3854.5651.19

jw"

14. 5910.7112.9216.086.84

42.5642.5617.9715.0014.0124.8113.6810. 7113.01-14. 5311. 5315. 5910.7110. 7113.4012.09.13. 779.98

10. 0010. 0013. 1913.1911.898.38

11. 6517. 3714.2913. 4320. 3820.3815. 7246.308.96

13.62

19.51

20.1815.9214.5713.5414.579.389.259.81

11.9010. 5411. 159.76

17.4114.1218. 55"22.7427.879.799.807.58

10. 53

3 f}ftfW

1.12.49

1.081.40.59.82.82

1.062.242.051.003.881.43

' 5.344.354.413.984.944.944.703. 524. 051.324.174.174.384.382. 70

. 2.303.871.891.791.794.704.705.01

3. 145. 03

3.53

3.12.83.01.01.69

3.962.193.771. 512.851.583.233.434.74.74.95.90

1. 211.011.221. 55

Washed.

B3 pw'os0.295.820.82

6.6917.2922.736.326.455. 037.78

16. 808.25

14.0216.78.13.8116.8315.1014.3614.1415.9616. 119. 75

15. 86.15. 8612.3613. 678.68

10.1214. 1616. 86

6. 618.97

12.119. 53

12. 0326. 109.09

13.93

17.30

19.706.013.715.974.686.854.636.455.186.485.285.297.041.714.027.025.606.367.064.24

11.06

aw**<

9.3910. 0138.1

4. 7629.6734.578.627.197. 85

14.3010.268.098.589.998.788.759.758.388.989.407. 767.127.707.709.447.897.446.527.857.098.278.408.88

10.8710.10

7.229.08

9.45

11.0512.4311.399.41

11.876.196.405.388.020.765.335.64

10. 129.999.91

13. 7513.474.385.764.876.38

3̂ rtft 3

O2

1.22.58

1.03

.59

.64

. 551.121.892.03.98

3.211.253.093.793.443.223.183.313.052.763.261.053.063.003.203.152.191.763.291/351. 551. 563.723.802.47

2. 013. 02

3.04

3.07.71.58.65.91

3.001.391. 531.101.301.322.402.202.94.85.98.92

1.30.97.93

1.30

Reduction (per cent) .

Aai^

307

71

303019525244.422525343124449

223322432952522840'

372133594237564735441933

52

452222312533314533365243422947405257413439

3aft 3

CO

5

2233

1612

17133113201936333022

2020272726

. 28212015291313

Actually removed

(per cent) .

Am"*<

451474

3765516464525733354245355032304430524703604552503439725540

21 6219 0551 41

a 3428 ' 44

i4 58

2 5015 25

5 3739

......' 289

3759235410243438

42410

50455941505850603860530964504057

M

J3 .

ft '

302

1

19

1061002130172725253930313652414736314244494042373724513225374855

3240

15

222523

7""si

496233652834554514203313192941

Page 16: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

16 - ' WASHING, COKING, AND CUPOLA TESTS. .

Details of special washing tests, January 5 to February 15, 1907.

Washing test No.

195

"192

187

190

196

o!97

151

193

« 188

189

o!94

"198

Field No. of fuel.

Alabama:

5............

6..^.........

Argentina:

1........

Illinois:

30...........

34 A........

34 B ......

Kansas:

2B.. .......

Ohio:

12...........

Pennsylvania:

' 15...........

17...........

20...........

Virginia:

6............

Date and

duration of test.

/Jan. 12, ) 1 J hours

/Jan. 5, 2 1 hours.

/Feb. 15, \ 4} hours

/Feb. 12, \ 2 hours.

/Jan. 10, \ 2 hours.

/Jan. 25, \ f hour.

/Feb. 4, 2 \ hours.

/Feb. 6, \ 1£ hours

/Jan. 29, \ 2J hours

fFeb. 1, I li hours

Float and sink tests with finer crushing.

Spe- cial testNo.

f 1 2 3 4

1 5 i J

( ' \ 1

f * 1 1! i i1 \ iI i i 1

I \3

I .<

I *1 J

1 '1 21 ( 1I li J

Size through square hole ' (inch) .

IJ f ' J

i*

J t

|

f

I

1 1 1

Slack. Slack. Slack. Slack.

3

i

4 4 4 t f

f f 2a1 J1

Specific gravity

of solution used.

1.35 1.40 1.45 1.52 1.36 1.42 1.48 1.56

1.55 1.60 1.65 1.70

1.36 1.41 1.47 1.56 1.36 1.41 1.45 1.51 1.35 1.41 1.46 1.51

1.36 1.41

1.47 1.56

1.35 1.40 1.45 1.52

1.35 1.41 1.45 1.52 1.35 1.40 1.45 1.52 1.35 1.42 1.45 1.52

1.35 1.41 1.45 1.53

Float (per

cent) .

81 85 87 87 87 90 91 94

45 59 59 61

73 84 88 90 84 88 90 92 87 90 92 92

66 74 78 81

77 89 92 94

72 78 80 81 86 90 91 91 83 88 88 89

84 85 85 87

Sink (per

cent) .

19 15 13 13 13 10 9 6

55 41 41 39

27 16 12 10 16 12 10 8

13 10

8 8

34 26 22 19

23 11 8 6

28 22 20 19 14 10

9 9

17 12 12 11

16 15 15 13

Analysis of float (per cent)

Ash.

De­ ter­

mined.

2.18 2.63 2. 66 3.19 2.81 3. 51 3,43 3.75

22.56 24.96 27.68 27.90

7.10 8.69 8.98 9.59 6.07 6.12 7.06 7.10 5.91 6.15 6.20 7.23

4.48 5.31 5.73 6.18

5.12 6.43 6.78 7.31

5.47 5.27 5.54 6.26 5.14 5.69 6.20 7.51 4.95 5.66 4.72 6.07

2.60 2.98 3.44 3.53

Re­ duc­ tion.

86 84 84 80 59 49 50 45

47 41 35 34

46 34 31 27 49

' 48 41 40 29 27 26 14

78 74 72

' 70

45 32 28 22

44 46 43 36 57 52 48 37 53 46 55 42

54 48 42 41

Sulphur.

De­ ter­

mined.

0.81 .98

1.05 1.13 .54 .57 .53 .56

.73

.78

.72 - .70

3.29 3.29 3.33 3.41 1.90 1.83 2.18 1.97 1.71 1.64 1.68 2.17

2.63 2.78 3.19 3.31

3.23 3.63 3.88 3.98

1.30 1.45 1.54 1.71 1.00 1.08 1.26 1.13 .93

1.24 1.02 1.09

.95

.92 . .95

.97

Re­ duc­ tion.

42 30 25 19 8.5 4

10 5

12 12 12 12

23 23 23 22 31 34 21 29 28 31 29

8

44 41 32 30

18 8 2

66 62 59 55 34 28 17 25 67 57 64 62

21 24 21 20

Finer crushing advantageous.

Page 17: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

WASHING TESTS. 17

Details of special washing tests, January 5 to February 15, 1907 Continued.

6 53 .u

Washing tes

o!92

190

190

o!97

191

193

ol88

189

o!94

ol98

Float and sink tests on refuse.

Spe­ cial test No.

f 12 3

{ 4( 1

2 3

I 412 3412312 3412 3412 3

I 4f 1

2 3

I 412 3

I 412 3

I 4

Specific gravity of solu­

tion used.

1.351.40 1.451.521.361.40 1.451.511.351.41 1.451.511.351.401.45

1.351.40 1.461.531.351.41 1.451. 531.351.41 1.461.511.351.411.451.511.351.41 1.451.53

. 1.351.41 1.451.51

Percentage of float-

To refuse.

18.4020.80 20.8022.3015.8020.18 29.9033.5012. 1013.59 14. 2116.7850.0052.0055.009.00

10.00 10.0010.0039.0057.00 59.0081.0011.8013.20 14.5017. 2013.0014.00 19.3023. 7517.2018. 50 .19.8820.2015.3015.75 15.9019. 25

To total sample.

1.912.16 2.162.32'2.984.13 5.636.312.522.82 2.953.437.808.148.601.942. 16 2.162.169.35

13.29 14.0919.302.953.30 3. 644.301.701.80 2.603.203.914.20 4.514.592.902.99 3.023. 65

Analysis of float (percent).

Ash.

2.813.48 4.065.098.00

.11.30 12.0014.606.957.78 9.58

11. 206.275. 99

' 7.404.305.05 7.537.715. 756.42 9.12

10.174.956.50 7.658.155.396.20 8.159.515.425.69 6.457.894.805. 35 5.629.31

Sul­ phur.

0.891.01 1.171.063. 123.42 3.434.632.052.32 2.453.052.362.502.792.582.93 3.573.813.674.04 5.264.971.712.13 2.292.881.281.40 1.471. 671.691.69 2. 152.081.391.78 1.752.79

Lossof good coal in refuse (per

cent) .

1.00

2.98

2.52

11.75

2.16

9.00

2.00

1.50

2.00

2.20

Analysis of refuse (per cent) .

Mois­ ture.

8.21

. 11.22

9.29

15.35

5.78

5.78

4.58

10.21

3.64

Ash.

34.92

46. 50

58.43

61.00

76.50

19. 91

47.18

41.50

Sul­ phur.

2.20

9.59

11.91

15.90

11.32

6.62

19.78

8.85

i

46. 25

63.98

17.40

6.15

o Finer crushing advantageous'.

28975 B nil. 880 08 2

Page 18: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

COKING TESTS.

By A. W. BELDEN.

EQUIPMENT.

The ovens in which the tests of the coking qualities of coals have been made are of the regular beehive pattern. Of the battery of three ovens two are of standard size, 12 feet in diameter and 7 feet high, the third is 12 feet in diameter and 6 feet 4 inches high. This change was made by raising the bottom of one of the standard ovens 8 inches with well-tamped loam and bottom tile of the usual size. The object of the change was to bring the charge nearer the dome of the oven and effect a more rapid penetration of heat.

For the first nineteen tests the small oven only was used. In the twentieth charge one of the 7-foot ovens was blown in, and two ovens were used continuously during the remainder of the work one of each size. Owing to the small supply of coal it has not been possible to use more than two ovens, and they may, therefore, be considered as end ovens. Some suppose that end ovens yield results less favorable than those from ovens located between other heated ovens, but, even if this supposition is correct, the difference is fully balanced by the greater care bestowed on these experimental ovens as compared with ovens operated under normal conditions. As both of the ovens used are, in the sense indicated, end ovens, the results obtained in each are comparable one with the other.

In' charging the ovens for the first nineteen tests the larry used held less than 1 ton. This necessitated the filling and emptying of the larry six to eight times before the charge was completed. Each posr tion thus became hot and began invariably to gas, and often to blaze before the next portion of the charge was added. This unfortunate state of affairs is believed to be responsible, at least in some measure, for cross lamination and cross breakage of the coke, layers of coal as charged showing plainly in many of these tests in each oven drawn. The average time of charging with this device was about one hour. After the nineteenth charge a standard-size larry was installed and the time of charging was reduced to an average of seven minutes. With this change the lamination and cross breakage referred to disappeared,, showing that the whole charge should be put in at once.

Page 19: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

COKING TESTS. . 19

PERSONNEL.

The writer took charge of this work in May, 1905, succeeding Fred W. Stammler, of Johnstown, Pa. He was assisted by W. E. Vickers, of Pocahontas, Va., to whom in large measure is due whatever sue-, cess has been obtained during these investigations.

PROCEDURE OF TESTS.

All coal was finely crushed through a Williams mill unless other­ wise tested for definite comparison of results, and these exceptions are noted in the subjoined detailed report (pp. 21-26). The coals not crushed were, when unloaded from the cars, put through rolls having an aperture of 1| inches. The coals put through the Williams mill will vary somewhat, depending on the nature of the coal, but will practically all pass through a 10-mesh sieve, as shown by the following report by the laboratory on an average sample: Amount remaining on 10-mesh, 15.08 per cent; on 20-mesh, 35.71 per cent; on oO-mesh, 12.89 per cent; on 40-mesh, 8.53 per cent; on 60-mesh, 9.33 per cent; on 100-mesh, 9.13 per cent; through 1 OO-mesh, 9.33 per cent.

Both the door and the trunnel head of the oven were always closed directly after the oven was drawn and it was allowed to gather heat, the length of time varying as necessity demanded. The average time was one arid one-half hours.

The sample' of coal was taken at regular intervals as the charge was emptied from bin to larry, by means of a small shovel holding about one-fourth pound. The total weight of the sample averaged 45 pounds.

The sample of coke was taken from five different parts of the oven, as nearly as possible from the same location for each test, as follows: 2 feet from the oven door; 2 feet from each side, on a line drawn from the center of the oven; at the center; and 2 feet from the back wall, on a line with the point of selection of the pieces taken from the door and the center. The separate pieces of coke extended the whole height of the charge and were as nearly uniform in size as possible. -* In beginning the series of tests, before the ovens were fully seasoned, the first'charges showed a rather large percentage of breeze, and black butts due to cold bottom were produced. It was unfortunate that these first tests should have been made on coals that were supposedly noncoking, as the condition of the oven did not permit it to give as effective service as it would probably have given .under other and more favorable conditions.

EXTENT.OF TESTS.

In the scope of this report, covering the period from July 7, 1905, to February 20, 1907, are included results from 192 tests of 102 coals from seventeen States and one Territory, "as shown in the accoin-

Page 20: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

20 WASHING, COKING, AND CUPOLA TESTS.

panying table. Of these tests, 100 were made on raw coal, 82 on washed coal, 1 on raw coal with the addition of pitch, 6 on washed coal with the addition of pitch, 1 on washed coal with the addition of asphalt, and 2 on coals of widely varying composition. Of the 102 different coals, 8, viz, Arkansas No. 9, Illinois No. 19, Indiana Nos. 3 and 18, Ohio No. 3, Maryland No. 1, and. Wyoming Nos. 3 and 5, produced no coke. Arkansas No. 9 and Maryland No. 1 were coked by the addition of pitch to washed coal. Four tests were made on Pennsylvania No. 9 (pp. 24, 32, 41); two tests with raw coal gave only a few pieces of coke; a third, with washed coal', produced coke of inferior quality; and the fourth, with the addition of 5 per cent pitch to raw coal, produced coke of no better quality than that from washed coal. Of Indiana No. 3, Ohio No. 3, and Wyoming Nos. 3 and 5, there was not enough for further tests.

TABULATION OF RESULTS.

The results of the coking tests will be found in the detailed report on each sample, presented below. For convenience of comparison data are given as to the yield of dry coke from dry coal as well as coke as received from coal as charged. The analyses of both coal and coke as received and on dry basis are also given. No distinction is made between breeze and ash, as it was found impossible to separate them with any degree of accuracy, and both are represented in this report in the item "breeze." This breeze includes everything that will pass through a fork with tines 1| inches apart, after thorough shaking, and its percentage is much higher than that from regular operations, but is comparable in all tests. It was not deemed necessary or advisable to size the coke, and under this caption is included everything over the l|-inch tine fork. Except in a few special cases the determina­ tion of phosphorus was not made on coke having over 2 per cent of sulphur, and when more than one test was made on a coal in the same condition this determination was also omitted.

Page 21: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

Det

ails

of c

okin

g te

sts

of

coal

s, J

anua

ry 1

, 19

05,

to J

un

e 80

, 19

07.

Tes

t N

o. 1 142

138

139

131

136

171

172

174 95

96

97

100

104

105 98

99

101

102

103

173 1 4 5 2 3 7 10a h

Fie

ld N

o. o

f co

al.

2

Ala

bam

a:

2 B

(w

.) ...

...

3..........

....

3 (w

.)..-.

.....

4.... ...

....

...

40

V.)

....

-...

.

6..........

....

6(w

.).........

Ark

ansa

s:

IB (

w.)

....

..IB

(w

.)..

....

IB (

w.)

f>..

...

IB (

w.)

c.....

7B

(w

.)..

....

9 (w

.). .

.......

9 (w

.).........

9 (w

.)d

....

...

9 (w

.)6

....

...

a (w

)c

Geo

rgia

:

Illi

nois

: 7

D*

.. ...

.....

7D (

w.)

*.....

11 D

(w

.)*....

13 (

w.)

*..

....

.13

*. ...........

16

*..

....

...-

-.16

(w

)*

Ori

gin

of c

oal

sam

ple.

a

Des

igna

tion

of

bed. 3

Jag

ger.

...........

Und

erw

ood

or

Tho

mps

on.

....

.do

....

....

....

....

.do

....

....

....

....

.do

....

....

....

....

.do..

....

....

..

....

.do..

....

....

..H

unti

ngto

n ......

.. ..

.do.. ...

....

.. .

....

.do..

....

....

.......d

o..... .......

No.

6.............

.....d

o.... ...

....

.N

o. 7

....

....

....

.. .

...d

o... .........

. ....d

o. ....... ..

....

...d

o..

....

....

...d

o .........

At

or n

ear

4

Car

bon

Hil

l. ....

....

..

....

.do..

....

..........

Bel

le E

llen............

....

.do..

....

..........

.....d

o..........

....

..

.....d

o..........

....

....

...d

o..

....

..........

....

.do..

....

..........

....

.do..

....

..........

....

.do..

....

..........

....

.do

. ...............

.....d

o..........

....

.......d

o................

....

.do..

....

..........

....

.do..

....

..........

_t-io

_ . .

..

Add

itio

nal

deta

ils

of o

rigi

n of

sam

ples

tes

ted

in 1

905

(des

igna

te

Dur

tion

of

test

(h

ours

) .

5

51

54 44

47

49

42

40

50 49

71

48

50

67

57

28

24

39

43

46 58 43

65

48

65

65 60

d by*in

c

Size

of c

oal

(see

p. 4

) .

As

ship

ped.

6

r. o

. m.

r. o

. m.

r. o

. m.

r. o

. m.

r. o

. m.

r. o

. m.

r. o

. m.

r. o

. m.

s. s. s. s. s. s. 1|"

s.

1|"

s.

l|" s

. 1J

" s.

1J

" s.

over

Ij"

.

r. o

. m.

r. o

. m.

No.

3.

Ij"b

y6

"e.

Ii"b

y6

"e.

1., e

. I.,

e.

Dlu

rnn

2) c

an

As

used

.

7

f.c.

f.

c.

f.c.

f.

c.

f.c.

f.

c.

f.c.

f.

c.

s.

f.c.

s. s.

s.

f.c.

s. f.

c.

f.c.

f.

c.

f.c.

f.

c.

f.c.

f.

c.

f.c.

be fo

und

i

Phy

sica

l pr

oper

ties

of

coke

.

Spec

ific

gr

avit

y.

Rea

l.

8 1.88

1.

91

1.99

1.

95

1.95

1.

99

1.97

1.

95

1.78

1.

90

1.96

1.

95

2.01

1.

97

2.04

2.

02

2.01

1.91

1.

85

1.87

1.

85

1.90

1.8

5

n B

ull

.

App

ar­

ent. 9 0.92

1.

04 .95

.96

.87

.98

.93

.91

.58

.75

.83

.08

.71

.93

1.00

.9

4

.98

.85

.82

.82

.84

.90

Pounds

per

cubi

c fo

ot.

Dry

.

10

55.6

3 63

.51

58.6

7 59

.70

54.0

6 60

.77

57.7

2 56

.43

35.1

3 46

.18

50.3

7 42

.33

44.2

0 57

.61

58.3

7 58

.45

60.8

5

; 51

.82

, 50

.60

50.1

4 49

.99

54.6

0

. S7

53. i

i

U.S

. G

eol.

Sim

As

re­

ceiv

ed

(wet

).

11

87.4

4 92

.20

91.1

0 91

.52

88.3

5 92

.58

90.7

9 89

.50

76.9

2 83

.59

86.5

3 82

.87

84.7

3 90

.68

90.1

8 91

.52

92.6

6

86.1

1 85

.53

85.0

8 83

.67

87.6

7

86. i

s

ey N

o.

Per

cent

age

by v

olum

e.

Cok

e.

12

49.0

0 54

.00

48.0

0 49

.00

45.0

0 49

.00

47.0

0 47

.00

33.0

0 40

.00

42.0

0 35

.00

35.0

0 47

.00

49.0

0 47

.00

49.0

0

45.0

0 44

.00

44.0

0 46

.00

47.0

0

47.6

6

290;

ofc

Cel

ls.

13

51.0

0 46

.00

52.0

0 51

.00

55.0

0 51

.00

53.0

0 53

.00

67.0

0 60

.00

58.0

0 65

.00

65.0

0 53

.00

51.0

0 53

.00

51.0

0

55.0

0 56

.00

56.0

0 .5

4.00

53

.00

53.6

6

)th

er s

a

6-fo

ot d

rop

test

: P

erce

nt­

age

over

2-i

nch

mes

h.

1. 14

93.0

0 97

.50

95.0

0 96

.00

92.0

0 95

.50

93.5

0 94

.50

97.0

0

96.5

0

94.5

0

97.5

0

99.0

0

92,5

0 91

.50

95.5

0 93

.50

95.0

0

93.5

0

rnp

les

ii

2 15

78.5

0 94

. .50

90.0

0 91

.50

88.0

0 92

.50

87.5

0 91

.50

94.5

0

93.0

0

90.5

0

94.5

0

98.0

0

86.5

0 84

.50

85.0

0 87

.50

89.5

0

84."

50

nB

ull

.

3. 16

77.5

0 92

.00

87.0

0 86

.00

83.5

0 88

.50

83.5

0 88

.00

90.5

0

90,5

0

88.0

0

92.5

0

96.5

0

78.0

0 77

.50

80.5

0 82

.50

85.' 5

0

SO. 5

0

S*o.

332

.

4. 17 58.0

0 88

.00

83.5

0 82

.00

81.0

0 86

.00

79.5

0 85

.00

88.0

0

87.0

0

87.5

0

90.0

0

95.0

0

73.5

0 75

.00

75.0

0 75

.00

81.0

0

76.6

6

6 W

ith

10 p

er c

ent

pitc

h c W

ith

5 pe

r ce

nt p

itch

, d

Wit

h 3J

per

cen

t as

phal

t.

Page 22: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

Det

ails

of c

okin

g te

sts

of c

oals

, Ja

nuar

y 1,

190

5, t

o Ju

ne S

O, 1907 C

on

tin

ued

.fc

O

Tes

t N

o. 1 11 15

19

106

107

126

137

117

118

111

112

114

119

155

. 14

5 12

0 14

0 14

3 14

4 16

6 16

9 17

0 19

0 14'

6 9 8 12

13

16

17

18

51

108

Fie

ld N

o.

of c

oal

.

2

Illi

no

is C

on'td. :

19

A*.........

19 A

*.........

19 B

*..

....

...

20 (

w.1

........

20 (

w.)

........

21.............

21 (

w.)

........

22 B

.....

....

.22

B (

w.)

.....

23 A

(w

.) .....

23 B

(w

.) ...

..23

B (

w.)

.....

24 A

...........

24 A

(w

.)......

24 B

(w

.) .

. . ;

.2

5..

....

....

...

25 (

w.)

. .......

26 (

w.)

. ...

....

27 (

w.)

. ...

....

28C

(w

.)......

29 A

(w

.) ...

..9Q

A

f\

v

~\ t

34 B

(w

.).....

India

na:

3

(w.)

*..

......

4*............

4 (w

.)*..

......

5*............

6(w

.)*

....

....

7 A

(w

.)*.....

9 A

*9

B*.. ...

....

..9

B (

w.)

*.....

11 D

*.........

12

....

....

....

.

Ori

gin

of

coal

sam

ple

.

Des

ignat

ion o

f b

ed.

3

No. 7... ..........

.....d

o............

....

.do

....

....

....

.N

o. 6..

....

....

...

....

.do

....

....

....

....

.do

....

....

....

....

.do

....

....

....

...

...d

o..

....

....

....

...d

o..

....

....

.......d

o....--

-.-.

....

...d

o..

....

....

....

...d

o..

....

....

..N

o. 6

..............

....

.do..

....

....

....

...d

o..

....

....

....

. ..

do

. .........

....

...d

o..

....

....

..N

o. 5

....

....

....

..N

o. 6

....

.. ...

....

.N

o. 7

..............

No.

5..... ..

....

...

.....d

o............

....

.do

....

....

....

No

. 6

....

....

....

.......d

o............

No

. 5

... ..

...

....

..

No

. 5..............

No

. 7..............

....

.do

....

....

....

....

.do

....

....

....

No. 5...... ...

....

.

At

or n

ear

4

.....d

o...... ..........

....

.do

....

....

..:.

....

....

.do

....

....

....

....

.....d

o....... .........

.....d

o....... .........

....

.do

....

....

....

....

....

.do

....

....

....

....

....

.do

....

....

....

....

....

.do

....

....

....

:...

.....d

o................

.....d

o................

.....d

o................

Har

twel

l ...

....

....

...

Dur

tion o

f te

st

(hou

rs) .

a

48

24

47

47 36

44

45

45

76

39

43

72

24

78

55

79

62

59

53

60

74

54

51 24

62

58

49

49

112 90

112 90

50

37

Size

of c

oal

(see

p. 4

) .

As

ship

ped.

6

i"8.

i"8

.i"

s.sc

. sc

.1. 1. sc

. sc

. 1. s.

s.

sc

. sc

.1. r.

o. m

. r.

o. m

. r.

o. m

. r.

o. m

. 1. sc

. sc

. r.

o.

m.

n.,

s.

sc."

sc.

r. o

. m.

r. o

. m.

li".

r.

o. m

. r.

o. m

. 1. r.

o. m

.

As

used

.

7

f.c.

f.

c.

f.c.

f.

c.

f.c.

f.

c.

f.c.

f.

c.

f.c.

f.

c.

f.c.

f.

c.

f.c.

f.

c.

r. o.

m.

f.c.

f.

c.

f.c.

f.

c.

f.c.

f.

c.

f.c.

f.c.

f.

c.

f.c.

f.

c.

f.c.

f.

c.f.

c.

f.c.

f.

c.

f.c.

f.

c.

Phy

sica

l pr

oper

ties

of

coke

.

Spec

ific

gr

avit

y.

Rea

l.

8

App

ar­

ent. 9

i

1.85

1.

82

1.89

1.

84

1.85

1.

81

1.86

1.80

1.89

1.

80

1.82

1.

83

1.83

1.

83

1.85

1.93

1.

86

1.91

1.

89

1.85

1.

86

1.84

1.

84

1.83

1.

92

0.90

.8

4

.98

.89

.79

.79

.85

.93

.88

.89

.84

.86

.78

.80

.78

.89

.79

.82

.85

.76

.95

.91

.87

.84

:97

Pou

nds

per

cubi

c fo

ot.

Dry

.

10

55.8

2 52

.12

60.5

0 55

.17

48.9

2 48

.81

52.2

7

As

re­

ceiv

ed

(wet

).

11

87.6

3 85

.80

90.4

5 87

.59

84.4

7 83

.74

85.9

5

...."..

.I...

---.

54.7

1

53.4

2 52

.58

50.5

6 52

.12

48.3

1 48

.54

48.5

8

52.0

1 49

.00

50.3

7 52

.62

46.8

6 58

.75

56.3

9 53

. 76

51

.59

59. 9

7

84.6

6

'86.

49

84.3

9 84

.24

85.1

9 83

.86

83.4

8 84

.73

85.6

9 84

.54

85.9

2 86

.91

83.6

7 89

.31

87.5

9 86

.83

85.2

7 90

. 53

Per

cent

age

by v

olum

e.

Cok

e.

12

49.0

0 46

.00

52.0

0 48

.00

43.0

0 44

.00

46.0

0

52.0

0

47.0

0 49

.00

46.0

0 47

.00

43.0

0 44

.00

42.0

0

46.0

0 43

.00

43.0

0 45

.00

41.0

0 51

.00

50.0

0 47

.00

46.0

0 51

.00

Cel

ls.

13

51.0

0 54

.00

48.6

6 52

.00

57.0

0 56

.00

54.0

0

48.0

0

53.0

0 51

.00

54.0

0 53

.00

57.0

0 56

.00

58.0

0

54.0

0 57

.00

57.0

0 55

.00

59.0

0 49

.00

50.0

0 53

.00

54.0

0 49

.00

6-f

oo

t dro

p t

est

: P

erce

nt­

ag

e o

ver

2-i

nch

mes

h.

1. 14

92.6

6 94

.00

95.5

0 89

.00

88.5

0 89

.50

88.0

0

2. 15

86.5

0 87

.50

88.5

0 79

.50

78.0

0 78

.50

78.0

0

91.5

0 92

.00

92.0

0

96.5

0 87

.50

96.0

0 92

.50

92.5

0 94

.50

94.5

0 96

.50.

94

.00

95.5

0

82.0

0 84

.00

84.5

0

90.5

0 82

.50

89.5

0 89

.00

84.5

0 87

.50

86.5

0 94

.50

87.5

0 91

.50

3. 16

82.0

0 82

.00

83.0

0 73

.00

68.0

0 69

.00

66.5

0

74.0

0 76

.00

78.0

0

85.5

0 74

.50

85.0

0 86

.50

79.0

0 82

.50

82.5

0 91

.00

82.5

0 88

.50

4. 17 75.0

0 75

.50

75.5

0 68

.50

62.0

0 62

.00

58.5

0

64.0

0 70

.00

74.0

0

80.0

0 68

.50

80.5

0 80

.50

74.5

0 78

.00

79.0

0 88

.50

79.0

0 86

.50

Page 23: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

109

110

163

158

168

613

115 76

71

75

86

90

85

1'64

165

167 50 54 58 148

149

152

150

151

146

147 24 27 31 28 22 59 66 . 89 94 81 93 72 55 57 180

19

f \v

\

12 (

w.)

. ...

....

17

(w.)

.....

....

18 A

(w

.) ...

..18

A (

w.)

...

..K

ansa

s:

6 (w

.). .

........

Ken

tuck

y:

IB*

....

....

...

1C

*..

....

....

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r. o. m.

r. o

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r. o

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sc.

sc.

1. 1. 1" to

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li"

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larg

e I.

larg

e 1.

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r. o. m.

r. o

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f. c.

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f. c.

s. f. c.

f. c.

f. e.

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1.97

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1.94

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1.78

1.83

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1.86

1.91

1.88

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1.85

1.84

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CO

Page 24: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

Det

ails

of

coki

ng t

ests

of c

oals

, Ja

nuar

y 1,

190

5, t

o Ju

ne

30,

19

07

Con

tinu

ed.

bo

Tes

t N

o. 1 25

26

32

34

35

38

41

30

33

29

37

39

42

56

47

53

159

161

162

185

188

178

186

176

177

179

182

183

187

189

191

192

133

153

Fie

ld N

o. o

f co

al.

2

Pen

nsy

lvan

ia :

0*. ...........

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....

...

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....

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(w.)

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....

....

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....

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....

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(w

.)..

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w.)

......

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w.)

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w.)

.......

19

....

....

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....

....

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w.)

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21

Ori

gin

of c

oal

sam

ple.

Des

ignat

ion o

f be

d.A

t or

near

1

Pit

tsburg

........

.....d

o............

.....d

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........

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.....d

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tannin

g

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r M

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Upper

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o ...

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g

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mel

ton ...

....

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o................

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o................

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o................

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o................

Ach

eson

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....

...

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o................

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o................

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e........

........

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o................

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o................

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o................

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o................

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o................

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o................

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Du

ra­

tio

n o

f te

st

(hou

rs)

.

5

62

92

46

45

88

86

72

90

93

51

45

66

51

38

49

47

41

47

48

61

54

52

44

36

40

68

78

70

78

51

47

43 49

43

Size

of c

oal

(see

p. 4

) .

As

ship

ped.

6

!" . o.

m.

. o.

m.

. o.

m.

. o.

m.

. o.

m.

. o.

m.

. o.

m.

. o.

m.

. o.

m.

. o.

m.

. o.

m.

. o.

m.

. o.

m.

. o.

m.

. o.

m.

. o.

rn.

. o.

m.

. o.

m.

. o.

m.

. o.

m.

. o.

m.

. o.

m.

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m.

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m.

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m.

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m.'

. o.

m.

. o.

m.

. o.

m.

. o.

rn.

As

used

.

7

f. c.

f.

c.

f. c

. f.

c.

f. c.

f.

c.

f. c.

f.

c.

f. c

. f.

c.

f. c.

f.

c.

f. c.

f.

c.

f. c.

f.

c.

f. c.

f.

c.

f. c

.

f. c

. f.

c.

f. c

. f.

c.

f. c

. f.

c.

f. c

.

thr.

1"

thr.

f "

f.c.

f. c

.

Physi

cal

pro

per

ties

of

coke

.

Spe

cifi

c gra

vit

y.

Rea

l.

8 1.92

1.

84

1.96

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92

1.91

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1.91

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1.83

1.

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1.99

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1.92

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1.95

1.

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2.01

2.

04

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1.97

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3 1.

09

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1.18

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8 .9

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00

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Pounds

per

cu

bic

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As

re­

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11

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97.1

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87.7

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0 87

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91.9

7 91

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4 84

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5 94

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4 95

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95.3

6 89

.65

84.5

8 90

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89.4

6 90

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92.1

3 91

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92.7

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Per

centa

ge

by

vol

ume.

Cok

e.

12

49.0

0 45

.00

56.0

0 55

.00

58.0

0 53

.00

62.0

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.00

50.0

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.00

43.0

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. 00

47.0

0 44

.00

52.0

0 50

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47. 0

0 36

.00

39.0

0 49

.00

45.0

0 56

.00

55.0

0 42

.00

37.0

0 50

.00

48.0

0 49

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50.0

0 49

.00

51.0

0 47

.00

Cel

ls.

13

51.0

0 55

.00

44.0

0 45

.00

42.0

0 47

.00

38.0

0 51

.00

50.0

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57.0

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00

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6-fo

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2. 15

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i. nn

Page 25: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

127

128

125

129

154

122

121

123

134

124

156

160

130

141

157 64

65

67

68

77

63

69

70

61

SS

62

1S

1 18

4

135 40

44

46

21

23

20

36

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73

45

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0

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0

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0

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0

80.5

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0(1

7.00

78.0

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0 80

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77.0

0 76

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0

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0

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88

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SO. 5

0

84.5

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78.0

0 85

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79.5

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o W

ith 5

per

cen

t pit

ch.

6 O

ver

3-in

ch s

cree

n, w

ith

IS p

er c

ent

of s

lack

ret

urn

ed t

o it

.c

Mix

ed w

ith o

ne-

thir

d R

hode

Isla

nd N

o. 1

.d

Mix

ed w

ith o

ne-

fou

rth

Rho

de I

slan

d N

o. 1

.O

r

Page 26: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

Det

ails

of

coki

ng t

ests

of

coal

s; J

anua

ry 1

, 19

05,

to J

une

30,

1907 C

onti

nued

.O

S-

Tes

t N

o. 1

i

48

49

60

74

78

79

83

80

84

87

92

82

91

175 52

13

2

^

Fie

ld N

o. o

f co

al.

2

Wes

t V

irgin

ia

Conti

nued

. 16

B (

w.1)

*....

16 B

(w

.)*....

17 (

w.)

*......

18*.

...........

18

*........

....

19*

19*........

....

20*..

....

....

...2

0 (w

.)*......

20 (

w.)

*......

20*..

....

....

..21*..

....

....

..21

(w

.1*......

9<;

Wy

om

ing

: 3(w

.)*.......

Ori

gin

of c

oal

sam

ple.

Des

ignat

ion o

f be

d. 3

....

.do

....

....

....

Sew

ell .

...........

....

.do

....

....

....

....

.do

....

....

....

.....d

o............

.....d

o............

(?)

Roc

k S

prin

gs. .

...

At

or n

ear

4

'.....do........

....

....

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o................

.....d

o................

.....d

o................

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o................

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o................

Du

ra­

tion o

f te

st

(hou

rs)

.

o

47

25

42

43

48

49

53

42

50

53

46

52

44

43 27

39

Size

of c

oal

(see

p. 4

) .

As

ship

ped.

6

. o.

m.

. o.

m.

. o.

m.

. o..

m.

. o.

m.

. o.

m.

. o.

m.

. o.

m.

. o.

m.

. o.

m.

. o.

m.

. o.

m.

. o. m

.

As

used

.

7

f.c.

f.

c.

f.c.

f.c.

f.

c.

f.c.

f.

c.

f.c.

f.c.

f.

c.

f.c.

f.

c.

f.c.

f.

c.

Phy

sica

l p

rop

erti

es o

f co

ke.

Spec

ific

g

rav

ity

.

Rea

l.

8 1.87

1.

84

1.91

1.

93

1.87

1.98

1.

94

1.80

1.

85

1.90

1.

92

1.86

1.

87

1.90

Appar

­ en

t. 9 0.80

.7

3 .9

3 .9

8 .9

0 .8

6 .8

4 1.

12

1.02

1.

01

1.18

.8

9 .8

7 .9

7

Pounds

per

cu

bic

foot

.

Dry

.

10

49.7

2 45

.34

57.0

5 60

.73

55.7

4 53

. 45

52.1

6 69

.72

63.4

4 62

.87

73.4

9 55

.46

53.9

1 60

.31

As

re­

ceiv

ed

(wet

) .

11

85.2

7 82

.75

89.7

6 91

.29

88.1

6 89

.00

87.7

1 93

.42

91.5

2 92

.16

97.1

9 87

.82

86.9

8 90

.87

Per

centa

ge

by v

olum

e.

Cok

e.

12

43.0

0 40

.00

49. 0

0 51

.00

48.0

0 43

.00

43.0

0 62

.00

55.

00

53.0

0 62

.00

48.0

0 47

.00

51.0

0

Cel

ls.

6-fo

ot d

rop

test

: P

erce

nt­

ag

e ov

er 2

-inc

h m

esh.

1.

13

14

57.0

0 60

.00

51.0

0 49

.00

52.0

0 57

.00

57.0

0 38

.00

45.0

0 47

.00

38.0

0 52

.00

53. 0

0 49

.00

94. 0

0 95

.00

96.5

0 93

.00

94.5

0 96

.50

99.0

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.00

97.5

0 94

.50

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0 94

.50

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0'

1 1

2. 15

90.5

0 91

.50

93.5

0 85

.00

89.5

0 95

.50

98.0

0 85

.00

89.5

0 88

.50

87.5

0 90

.50

79.5

0

3. 16

86.5

0 88

.00

90.5

0 78

.00

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.50

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.50

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.50

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.50

73.5

0

4. 17 83.0

0 84

.50

88.0

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.00

83.0

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81.5

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77.0

0 81

.00

69.5

0

I o-.

** a-

o-

W.

H,

H

cc-

Page 27: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

Det

ails

of

coki

ng t

ests

of

coal

s,

Janu

ary

1, 1

905,

to

June

30,

190

7 C

onti

nued

.

Tes

t N

o.

1 142

138

139

131

136

171

172

174 95

96

97

100

104

105 98

10

1 10

2

103

Fie

ld N

o. o

f co

al.

2

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bam

a:

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(w

.).......

3..

....

....

..

.

3 (w.

).. ...

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4(w

.). ..

....

...

5. ...

.. ....

6..

....

. .

6(w

.). ..

....

...

Ark

ansa

s:

IB (

w.)

.......

IB (

w.)

.......

1 B

(w

.).....

lB(w

.).......

7B

(w

.).......

7B

(w

.).......

9 (w

.). ..

....

...

9(w

.). ..

....

...

9(w

.). ..

....

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9 (-

.v.)

. ..

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nd

i-

tio

n.o

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f I

{ I

\ '

1 !

( I

t 1

j- f

1 2 1 9 1 2 1 9

{ \

{ I I

I I

{ I

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ght

of c

oal

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nds)

.

19 10,5

30

9,87

1 12

,180

11

,841

11

,660

10

,918

12

,000

11

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11

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12

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11

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11

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10,0

00

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00

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10,0

00

9,30

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9,

248

10,0

00

9,25

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000

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00

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duct

ion

(po

un

ds)

.

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e.

. Bre

eze.

20

21

6,19

7 6,

009

7,80

2 7,

644

7,07

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002

7,70

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684-

6,

809

6,78

5 7,

950

7,90

3 8,

350

8,31

2 7,

800

7,75

1

5,83

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663

5,80

6 5,

730

6,05

5 5,

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5,97

6 5,

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4,86

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835

6,25

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233

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663

489

479

258

255

281

280

239

238

390

388

316

315

221

220

574

557

1,29

0 1,

273

214

208

391

390

3,75

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457

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n (

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60.6

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56.7

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69.0

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58.0

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72

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04

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34

2.34

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44

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34

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69

1.86

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99

5.74

6.

26

12.9

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26

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14

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84

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l.

24 65.3

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67.5

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.11

62.6

9 66

.13

63.6

7 67

.39

64.8

0 69

.57

64.7

2 69

.51

67.1

0 70

.87

68. 0

0 71

.91

Chem

ical

anal

ysi

s of

co

al.

Mo

is­

ture

.

25 6.26

2.77

6.36

4.17

7.28

3.98

3.28

6.73

10.9

6 "6

." 7

7"

7.80

5.69

6.98

7.52

7.43

6.30

5.

60

5,76

Vola

tile

m

att

er.

26 31.9

9 34

.12

28.9

9 29

.82

30.5

4 32

.61

30.3

7 31

.69

30.4

6 32

.85

26.5

5 27

.65

25.3

0 26

.16

24.8

4 26

.63

16.6

6 18

.71

15.0

4 16

.13

18.9

3 20

.53

17.3

4 18

.39

14.8

6 15

.98

16.6

6

13.8

4 14

.95

14.7

4 17

.22

18.2

4 14

. 84

15.7

5

Fix

ed

carb

on

.

27 52.6

6 56

.18

53.1

4 54

.65

53.1

0 56

.71

54.5

0 56

.87

58.3

8 62

.97

56.9

2 59

.28

64.5

0 66

.69

63.5

7 68

.16

66.5

1 74

.70

69.3

2 74

.35

64.9

2 70

.41

68.6

7 72

.81

70.9

7 76

.29

68.8

57

4 4^

65.5

5 70

.81

65.0

1 64

. 03

67.8

3 66

. 03

70.7

0

Ash

.

28

*

9.0

9

- 9;

70

15.1

0 15

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0 10

.68

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G

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4.18

12

.55

13.0

7 6.

92

7.15

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86

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5.87

6.

59

8.87

9.

52

8.3

5

9.0G

8.

30

S.SO

7.

19

7.73

.

6.97

7 ^4

13.1

8 14

.24

13.9

5 13

.15

13.9

3 12

.77

13.5

5

Sul­

p

hu

r.

29 1.36

1.

45

.62

.64

.62

.66

1.18

1.

23

1.00

1.

08

1.44

1.

50

.59

.61

.5

9 .6

3

1.01

1.

13

1.14

1.

22

1.08

1.

17

1.12

1.

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1.78

1.

91

1.65

1.

78 .96.

1.04

.9

8 1.

01

1.07

1.

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Ch

emic

al a

nal

ysi

s of

co

ke.

Mo

is­

ture

.

30

3.04

2.03 .99

.29

.35

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2.89

^"i

.'ai"

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"

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.90

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3.67

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78

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'

2.47

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29

1.33

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03

2.03

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3 .5

3 .8

5 .8

6 .si

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.8

0

Fix

ed

carb

on

.

32 82.1

5 84

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74.8

9 76

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83.5

1 84

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83.2

1 83

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92.9

9 93

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81.1

0 81

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89.3

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92.3

6 92

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85.2

3 87

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84.5

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85.8

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87

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87.4

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89.8

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89.7

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83.9

8

Ash

.

33 13.7

5 14

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21.2

8 21

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. 59

15. 5

6 15

.71

6.24

6.

26

17.4

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78

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45

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. 9.

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34

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Sul­

phur.

34 1.16

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20

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.61

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.59

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1.

08

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.87

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1.

17

.59

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.60

1.25

1.

29

1.11

1.

12

1.02

1.

05

1.07

1.

07

1.70

1.

71

1.60

1.

61

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Ph

os­

phoru

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9

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3

Con

diti

on 1

mea

ns "

as

char

ged"

wit

h re

fere

nce

to w

eigh

t of

coa

l (c

olum

n 19

), an

d ''a

s re

ceiv

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) w

ith

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oth

er it

ems;

con

diti

on 2

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ns "

on d

ry b

asis

."to

Page 28: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

Det

ails

of

coki

ng t

ests

of

coal

s, J

anua

ry 1

, 19

05,

to J

une

30,

19

07

Con

tinu

ed.

bo GO

Tes

t N

o. 1 173 1 4 5 2 3 10

106

107

126

137

117

118

111

112

114

119

155

145

120

140

Fie

ld N

o.

of c

oal

.

2

Geo

rgia

:

1..

.............

Illi

nois

:

7D

. ..

....

....

.

7D

(w

.)..

.-..

.

11 D

(w

.) ......

13 (

w.)

. ..

....

..

13..............

16 (

w.)

.........

20 (

w.)

.........

20 (

w.)

. ..

....

..21..............

21 (

w.)

. ..

....

..22

B .........

...

22 B

(w

.)..

....

.

23 A

(w

.)....

...

23 B

(w

.)....

...

23 B

(w

.). ......

24 A

............

24 A

(w

.)....

...

24 B

(w

.)....

...

25

....

....

....

..25

(w

.) .........

Co

nd

tion.

18

{ J

1 1

i 2 2 1 2 1 2

1 i

I J

< *

{ | 2 1 2 1 2 1 2

{ 1

{ I

Wei

ght

of c

oal

(pou

nds)

.

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80

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72

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00

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00

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(pounds)

.

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146

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396

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529

574

570

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345

389

385

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593

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691

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duct

ion

(per

cent)

.

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e.

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0 68

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48.8

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0 58

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55.7

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42.5

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.00

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.02

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39.8

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eze.

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65

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20

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94

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73

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6 12

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9.

88

6.28

6.

32

3.98

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61

5.34

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01

4.78

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67

3.47

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00

3.89

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58

4.29

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11.4

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6.

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l.

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1 73

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54.4

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54.6

0 61

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57.0

0 61

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53.1

8 57

.28

55.7

1 60

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64.8

9 70

.41

48.8

3 57

.32

50.5

7 58

.72

55.8

0 62

.78

51.5

8 61

.14

45.5

8 52

.49

47.9

6 56

.45

50.3

1 59

.03

51.2

2 53

.09

51.2

7 57

.59

Chem

ical

anal

ysi

s of

coal

.

Mo

is­

ture

.

25 3.35

10.8

8

12.4

5

8.24

11.4

4

10.5

6

9.79

17.0

4

14.3

6

13.3

7 17

.45

11.9

8

16.1

9

13.7

4

15.8

5

15.9

3

13.2

8 15

.18

8.93

12.9

6 13

.40

Vol

atil

e m

atte

r.

26 16.5

4 17

.11

35.2

7 39

.58

36.1

7 41

.32

31.6

4 34

.48

30.9

5 34

.95

30.0

8 33

.63

30.3

5 33

.64

32.5

9 39

.28

34.6

1 40

.41

31.1

7 30

.01

33.8

7 38

.48

34.1

4 40

.74

36. 4

7 42

.28

35.0

2 41

.62

35.8

8 42

,68

29.9

3 32

.13

35.2

2 38

.67

33.0

1 33

.83

39.0

6

Fix

ed

carb

on.

27 66.0

7 68

.36

38.4

4 43

.13

42.0

8 48

.06

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1 52

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50.1

6 56

.64

49.0

8 54

.87

51.7

9 57

.41

40.7

7 49

.15

42.6

3 49

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43.1

5 44

.74

37.7

2'

42.8

5 39

.53

47.1

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.01

47.5

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.57

48.2

1 40

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47.7

7 39

.03

43.4

6 46

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50.8

3 39

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43.6

6 50

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Ash

.

28

~

14.0

4 14

.53

15.4

1 17

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9.30

10

.62

7.31

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97

7.45

8.

41

10.2

8 11

.50

8.07

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95

9.60

11

.57

8.40

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81

12.3

1 7.

80

16.4

3 18

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10.1

4 12

.09

8.78

10

.18

8.56

10

.17

8.0?

9.

55

17.7

6 9.

23

9.56

10

.50

14.4

3 9.

11

10. 5

2

Sul­

ph

ur.

29 1.29

1.

33

4.53

5.

08

3.64

4.

16

1.55

1.

69

1.25

1.

41

1.71

1.

91

1.09

1.

21

3.23

3.

89

3.23

3.

77

1.46

1.

10

4.74

5.

39

3.79

4.

52

3.57

4.

14

3.27

3.

89

3.25

3.

87

4.05

3.

07

3.41

3.

74

4.09

2.

99

3.45

Ch

emic

al a

nal

ysi

s of

co

ke.

Moi

ture

.

30 0.45

2.26

1.0

4.

1.19

4.60

2.73

2.14 .57

.53

.98

.65

.66

.96

1.36

5.62

2.71

Vol

atil

e m

atte

r.

31 0.35

.3

5

1.86

1.

90

.61

.61

.93

.93

1.68

1.

76

1.36

1.

40

1.46

1.

49

.66

.67

.29

.29

".72

.7

3 1.

60

1.61

.7

4 .7

4 1.

14

1.15

1.

19

1.21

1.64

1.

74

4.67

4.

80

Fix

ed

carb

on.

32 81.6

9 82

.06

72:6

8 74

.36

82.1

0 82

.96

85.9

7 87

.01

82.0

8 86

.04

79.3

0 81

.53

83.9

6 85

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82.4

9 82

.96

84.8

7 85

.32

72.1

8 72

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80.7

6 81

.29

83.4

5 84

.01

82.6

6 83

.46

82.8

3 83

.97

79.0

1 83

.71

77.6

9 79

.85

Ash

.

33 17.5

1 17

.59

23.2

0 23

.74

16.2

5 16

:43

11.9

1 12

.06

11.6

4 12

.20

16.6

1 17

.07

12.4

4 12

.71

16.2

8 16

.37

14.3

1 14

.39

26. i

2 26

.38

16.9

9 17

. 10

15.1

5 15

.25

15.2

4 15

.39

14.6

2 14

.82

13.7

3 14

.55

14.9

3 15

.35

Sul­

phur.

34 1.00

1.

00

3.95

4.

04

3.24

3.

27

1.44

1.

46

1.27

1.

33

1.77

1.

82

1.02

1.

04

3.01

3.

03

2.72

2.

73

4.61

4.

66

3.65

3.

67

3.09

3.

11

2.87

2.

60

2.84

2.

88

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2.

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Pho

phor

us.

35 0. 0

113

.006

5

.007

.016

2

.007

6

Page 29: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

COKING TESTS. 29

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Page 30: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

Det

ails

of c

okin

g te

sts

of

coal

s,

Janu

ary

1, 1

905,

to

June

30,

19

07

Con

tinu

ed.

OS o

Tes

t N

o. 1 71

75

86

90

85

164

165

167 50

54 58

116

148

149

152

150

151

146

147

Fie

ld N

o. o

f co

al.

2

Ken

tuck

y C

ont'd

. 16

C.......:

....

5..

....

....

....

.

6..

....

....

....

.

6..

....

....

....

.

7..

....

....

....

.

8..

....

....

....

.

8..

....

....

....

.

9 A

(w

.) ........

Mar

yla

nd:

l(w

.). .........

l(w

.). .........

Mis

sour

i:

5(w

.)- .........

New

Mex

ico:

3B

.. ...

....

....

3B

(w

.). .

......

3B

, 4

B,

5 (w

.).

4B

....

...

......

4B

(w

.).. ......

5..

....

....

....

.

5..

....

....

....

.

Con

di-

' tio

n.

18

{ \

{ i MI 2 { J

{ J

i *

\ 2 1

{ I

{ i

{ i

[ \ 2 1 2 1 2 1 2 1 2

'Wei

ght

of c

oal

(po

un

ds)

.

19 12,0

00

11,3

23

12,0

00

11, 4

40

12,0

00

11,3

75

12,0

00

11,3

50

12,0

00

10,9

42

12, 4

50

11,8

31

12, 8

40

12, 1

35

12, 1

90

11,0

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8,00

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11,3

84

11,7

90

11,3

55

11,4

30

10, 7

99

11,8

10

11,4

50

11,7

70

11.2

72

Pro

duct

ion

(pou

nds)

.

Cok

e.

20 7,31

9 7,

222

' 7,

993

7,96

9 6,

780

6, 5

89

6,65

9 6,

550

6,86

5 6,

849

7; 2

00

7,16

4 7,

845

7,80

8 6,

360

6,29

6

4,65

0 4,

616

4,90

3 4,

848

7,65

5 7,

597

7,23

3 7,

169

7,5%

7,

544

7,61

0 7,

526

6,98

6 6,

889

7,50

0 7,

422

7,65

0 7,

574

Bre

eze.

21 355

350

256

255

587

571

447

440

342

341

371

369

361

359

309

300

565

561

299

296

410

407

360

357

328

326

362

358

307

303

320

317

280

277

Pro

duct

ion (

per

cen

t).

Cok

e.

22 60.9

9 63

.78

66.6

1 69

.66

56.'5

0 57

. 93

55.4

9 57

.71

57.2

1 62

.59

57.8

3 60

.55

61.1

0 64

.34

52.1

7 56

.83

58.1

3 60

.32

49.0

3 56

.16

63. 1

6 65

. 08

61.7

7 64

.95

63.3

0 66

.27

64.5

5 66

.28

61.1

2 63

.79

63.5

1 64

.82

65.0

0 67

.19

Bre

eze.

23 2.96

3.

09

2.13

2.

23

4.89

5.

02

3.73

3.

88

2.85

3.

12

2.98

3.

12

2.81

2.

96

2.54

2.

76

7.06

7.

33

2.99

3.

43

3.38

3.

49

3.07

3.

23

2.73

2.

86

3.07

3.

15

2.69

2.

80

2.71

2.

77

2.38

2.

46

Tota

l.

24 63.9

5 66

. 87

68.7

4 71

.89

61.3

9 62

.95

' 59.

22

61. 5

9 60

.06

65.7

1 60

.81

63. 6

7 63

.91

67.3

0 54

.71

59.-5

9

65.1

9 67

.65

52.0

2 59

.59

66.5

4 68

.57

64.8

4 68

. 18

66 0

3 69

.13

67.6

2 69

.43

63.8

1 66

.59

66.2

2 67

. 59

67.3

8 69

.65

Che

mic

al a

nal

ysi

s of

coa

l.

Moi

ture

.

25 5.64

4.67

5.21

5! 4

2

8.82

4.97

. 5.

49

9.12

2.24

5.

37

4.35

13.6

8

3.68

5.74 5. is

3.69

"5

." 52

"

'3.0

5

4.23

Vol

atil

e m

atte

r.

26 32.4

1 34

.35

35.3

3 37

.06

30.8

2 38

.84

36.8

2 38

.93

35.0

3 38

.42

30.8

7 32

.49

30.3

6 32

.12

35.4

2 39

.97

13.7

7 14

.23

17.8

1 18

. 62

34.8

2 40

.34

33.0

6 34

.32

33.0

2 35

.03

33.8

8 35

.71

34.6

2 35

.95

35.2

9 37

.35

31.9

6 32

.97

32.2

5 33

.67

Fix

ed

carb

on.

27 52.7

7 55

.92

56.3

0 59

.06

55.6

2 58

.68

55.3

0 58

.47

46.7

8 51

.30

56.6

6 59

.62

55.4

9 58

.72

47.8

8 52

.68

71.0

4 70

. 54

68. 8

6 71

.99

42.2

6 48

.96

48.9

4 50

.81

48.9

9 51

.97

50.0

6 52

.77

47.8

3 49

.66

49.8

7 52

.78

49..7

1 51

. 27

51.7

9 54

.08

Ash

.

28 9.18

9.

73

3.70

3.

88

2.35

2.

48

2.46

2.

60

9.37

10

.28

7.50

7.

89

8.66

9.

16

7.58

8.

35

12.9

5 9.

868.

98

9.39

9.24

10

.70

14. 3

2 14

.81

12 2

5 13

00

10.9

3 11

.52

13.8

6 14

.39

9.32

9.

87

15.2

8 15

.76

11.7

3 12

.25

Sul

­ phur.

29 Ml

1.18

.4

5 .4

7 .5

1 .5

4 .4

8 .5

1 3.

56

3.90

1.

23

1.29

1.

27

1.34

2.

58

2.84

1.39

1.09

1.

14

3.60

4.

17 .78

.81

.72

.77

.69

.73

.66

.69

.67

.71

.76

.78

.89

.93

Che

mic

al a

naly

sis

of c

oke.

Moi

ture

.

30 1.32 .30

2.81

1.64 .23

.50

.47

1.01 .27

1.12 .76

.88

.69

i.io

1.39

1.04 .99

Vol

atil

e m

atte

r.

31 1.53

1.

55

1.21

1.

21

1.27

1.

31

1.C

9 1.

72

2.16

.

2.17

.6

5 .6

5 .5

0 .5

0 .6

9 .7

0

.88

.88

.73

.74

.67

.67

1.51

1.

52

1.48

1.

49

.94

.95

.85

" .8

6 1.

44

1.46

.84

.85

Fix

ed

carb

on.

32 84.6

8 85

.81

93.2

6 93

.54

91.9

3 94

.59

92.2

6 93

.80

82.9

7 83

. 16

87

.96

88.4

0 86

.10

86.5

1 86

.46

87.3

4

87.4

7 87

.71

82. 6

4 83

.58

78. 1

4 /8

. 74

80.4

2 81

.14

82.1

8 82

.75

78.4

8 79

.35

83.6

6 84

.84

76.9

3 77

.74

81.3

8 82

.19

Ash

.

33 12.4

7 12

.64

5.23

5.

25

3.99

4.10

4.

41

4.48

14

.64

14.6

7 10

.89

10.9

5 12

.93

12.9

9 11

.84

11.9

6

11.3

8 11

.41

15.5

1 -1

5.68

20.4

3 20

.59

17.1

9 17

.34

15.6

5 15

.76

19.4

8 19

.70

14.1

0 14

.30

20.5

9 20

.80

16.7

9 16

.96

Sul

­ phur.

34 0.96

.9

7 .4

1 .4

1 .4

0 ;4

1 .3

7 .3

8 3.

16

3.17

.9

3 .9

3 1.

14

1.15

1.

901.

98 .95

.95

3.40

3.

44 .71

.71

.65

.66

.63

.63

.58

.59

.60

.61 86

.8

7 .7

6 .7

7

Pho

phor

us.

35 0. 0

435

.011

5

.002

1

.003

3

.009

1

.012

0

.027

8

.000

0

.004

2

.034

8

.100

4

.094

6

.000

3

.000

1

Page 31: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

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Page 32: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

Det

ails

of c

oki

ng

tes

ts o

f co

als,

Jan

uary

1,

1905

, to

Jun

e 30

, 1

90

7 C

onti

nued

.O

S to

Tes

t N

o.

1 37

39 42 66

47

53

159

161

162

185

188

178

186

176

177

179

182

183

187

189

Fie

ld N

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coal

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2

Pen

nsy

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ia C

on.

9 g 9 (v

v.).

...

....

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9..

....

....

....

.

10..

....

........

10..

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11..............

12

...-

...........

12 (

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....

...

15 (

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...

....

..

15(w

.). ........

17..............

17 (

w.)

.........

19.....-

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.-

19

....

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....

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20....--

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20 (

w.)

.........

21..............

21..

....

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21..............

Co

nd

tion.

18

1 1 1 2 1 2 1 2 1 2 1 2 1 2 1 2 1 2 1 2 1 2 1 2 1 2 1 2 1 2 1 1 2 1 2 1 2

Wei

ght

of c

oal

(pou

nds)

.

19 7,00

0 8,

000

8,00

0 7,

636

8,00

0 7,

792

12,0

00

11,6

93

12,0

00

11,6

72

12,0

40

11,7

75

11,9

50

11,6

56

12,1

40

11,5

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9,75

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12,4

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11,8

96

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11,6

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11,9

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11, 1

69

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59

11, 7

60

11,0

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15,1

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14,3

27

14, 3

60

13,5

66

12,4

50

11.9

46

Pro

ducti

on

(pounds)

.

Co

ke.

20

5,60

0 5,

570

5,30

0 5,

262

7,40

0 7,

371

8,32

2 8,

301

8,10

0 8,

058

7,88

5 7,

831

8,10

0 8,

058

5, 7

79

5, 7

47

8,14

4 8,

096

7,92

3 7,

906

7,52

3 7,

501

7,80

0 7,

781

8,49

0 8,

479

8,12

9 8,

105

7,35

0 7,

313

10,2

00

10, 1

26

9,98

2 9,

919

8,45

7 S

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Bre

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21 80

1 79

7 49

5 49

1 3

40

33

9 2

68

2

67

29

6 294

286

28

4

257

256

262

261

332

330

356

355

307

306

315

314

336

336

420

419

529

526

401

398

326

324

319

316

Pro

ducti

on (

perc

ent)

.

Co

ke.

22 70.0

0 72

.94

66.2

5 67

.53

61.6

7 63

.04

69.3

5 '

71.1

2 67

.28

68.4

3 65

.98

67.1

8 66

.72

69.5

0 59

.27

63.5

1 65

.36

68.0

6 64

.94

67.7

9 63

.11

67.1

6 64

.41

66.2

5 70

.17

72.6

7 62

.20

64.5

4 62

.50

66.3

7 67

.37

70.6

3 69

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73.1

2 67

.93

70.2

2

Bre

eze.

23 10.0

1 10

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6.19

6.

30

2.83

2.

90

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3 2.

29

2.46

2.

50

2.39

2.

44

2.12

2.

21

2.69

2.

88

2.66

2.

78

2.92

3.

04

2.58

2.

74

2.60

2.

67

2.78

2.

88

3.21

3.

34

4.50

4.

77

2.65

2.

78

2.27

2.

39

2.56

2.

65

Tota

l.

24 80.0

1 83

.38

72.4

4 73

.83

64.5

0 65

.94

71.5

8 73

.41

69.7

4 70

.93

68.3

7 69

.62

68.8

4 71

.71

61.9

6 66

.39

68.0

2 70

.84

67.8

6 70

.83

65.6

9 69

.90

67.0

1 68

.92

72.9

5 75

.55

65.4

1 67

.88

67. 0

0 71

.14

70.0

2 73

.41

71.7

8 75

.51

70.4

9 72

.87

Ch

emic

al a

nal

ysi

s of

coal

.

Moi

ture

.

25 3.26

2.

86

4.55

2.60

2.56

2.73

2.20

2.46

i'50

7.19

4.53

4.41

6.30

3.01

3.57

3.91

6.30

5.37

5.53

4.05

Vola

tile

m

att

er.

26 16.1

8 16

.24

17.5

9 18

.43

17.9

2 18

.40

34.8

0 35

.71

35.4

1 36

.40

33.1

8 33

.93

31.2

8 32

.07

31.3

5 32

.83

17.8

6 19

.24

18.5

6 19

.44

28.8

3 30

.16

28.2

4 30

.14

30.6

6 31

.61

29.5

6 30

.65

16.3

5 17

.01

17.0

4 18

.18

28.3

3 29

.94

27.9

7 29

.61

29.2

6 30

.49

Fix

ed

carb

on

.

27 69.4

4 68

.60

68.8

0 72

.08

69.3

6 71

.21

56.8

1 58

.31

55.5

8 57

.14

55.4

6 56

.71

56.7

0 58

.13

57.6

6 60

.38

69.5

7 74

.96

70.6

3 73

.98

57.8

6 60

.53

57.2

2 61

.07

57.1

7 58

.94

59.1

7 61

.36

68.3

0 71

.08

69.5

8 74

.26

58.0

7 61

.37

57.8

1 61

.19

58.2

9 60

.76

Ash

.

28 11.1

2 12

.30

9.06

9.

49

10.1

2 10

.39

5.83

5.

98

6.28

6.

46

9.16

9.

36

.9.5

6 9.

80

6.49

6.

79

5.38

5.

80

6.28

6.

58

8.90

9.

31

8.24

8.

79

9.16

9.

45

7.70

7.

99

11.4

4 11

.91

7.08

7.

56

8.23

8.

69

8.69

9.

20"

8.40

8.

75

Sul­

p

hu

r.

29 1.90

2.

14

1.39

1.

46

1.80

1.

85

1.25

1.

28

1.36

1.

40

1.36

1.

39

2.03

2.

08

1.40

1.

47

1.63

1.

76

1.85

1.

94

1.39

1.

45

1.19

1.

27

1.16

1.

20

.98

1.02

2.

78

2.89

1.

34

1.43

.8

9 .9

4 .8

6 .9

1 .9

3 .9

7

Che

mic

al a

naly

sis

of c

oke.

Moi

s-'

ture

.

30 0.54 .72

.39

.36

.52

.69

.52

.56

.57

.22

.29

.24

.13

.30

.51

.71

.63

.82

Vol

atil

e m

atte

r.

31 1.21

1.

22

.61

.62

1.14

1.

15

1.14

1.

15

.97

.98

.29

.29

1.28

1.

29

.32

.32

.55

.55

.36

. .3

6 .5

6

.56

.19

.1

9 .4

9 .4

9 -.

28

.28

.58

.58

.12

.12

.66

.66

.21

.21

Fix

ed

carb

on.

32 86.8

4 87

.31

86.0

2 86

.64

90.4

0 90

.75

89.9

3 90

.25

85.0

2 85

.46

86.2

9 86

.89

89.1

3 89

.59

91.1

0 91

.61

90.2

3 90

.75

84.5

5 84

.74

87.9

6 88

.22

88.0

6 88

.27

87.4

5 87

.56

84.9

5 85

.21

89.8

5 90

.31

88.2

4 88

.87

87.7

8 88

.34

88.2

2 88

.95

Ash

.

33

11.4

111

.47

12.6

5 12

.74

8.07

8.

10

8.57

8.

60

13.4

9 13

.56

12.7

3 12

.82

9.07

9.

12

8.02

8.

07

8.65

8.

70

14.8

7 14

.90

11.1

9 11

.22

11.5

1 11

. 54

11.9

3 11

.95

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Page 33: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

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.

Page 34: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

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Page 35: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

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36 WASHING; COKING; AND CUPOLA TESTS.

DESCRIPTIONS' OF COKE AND REMARKS.

The following notes are given to supplement the information contained in the preceding table:

"Cell structure" refers to the general appearance as to size and not to the number of cells as given by percentage of cells by volume. In many tests the cell structure as determined from general appear­ ance is small when the percentage by volume indicates quite the reverse. (See, for example, test 29, Pennsylvania No. 8 coal, p. 24.)Alabama No. 2 B. Test 142: Soft, dense coke; dull appearance; cell structure.Very

small; breakage, lumps of irregular size; 1-inch black butts.Alabama No. 3. Test 138: Dark-gray color, some deposited carbon; cell structure

good; breakage good; long, large pieces; good, hard, heavy coke, with excep­ tion of f-inch black butts, which should.be easily removed; ash high; washing would probably reduce ash and improve quality of coke.

Test 139: Light-gray color, some silvery deposit of carbon; good ring; cell struc­ ture good; breakage good; long, large pieces; good, strong, hard, heavy coke; improved very materially by washing.

Alabama No. 4- Test 131: Light-gray and silv.ery-color; metallic ring; cell structure good; breakage somewhat cross fractured, but pieces of good, large, uniform size; good, strong, heavy coke; ash high; probably could be reduced by washing.

Test 136: Light-gray and silvery color; metallic ring; cell structure rather large; breakage 'somewhat cross fractured, but pieces of good, uniform size; good, strong coke; ash very materially reduced by washing.

Alabama No. 5. Test 171: Light-gray and silvery color; metallic ring; cell structure good; breakage good; uniform size; ash and sulphur high, both would probably be reduced by washing.

Alabama No. 6. Test 172: Light-gray and silvery color; metallic ring; cell structure good; breakage somewhat cross fractured, but pieces of. good, uniform size; good, heavy coke.

Test 174: Light-gray and silvery color; metallic ring; cell structure good; breakage somewhat cross fractured, but pieces of good, uniform size; good, heavy coke, somewhat better than coke from raw coal, but low ash and sulphur of this coal would not warrant washing. ' ......_ . .

Arkansas No. 1 B. Test 95: Dull-gray color; soft, dense, punky coke; cell structurevery small; breakage very bad and irregular; large and small chunks.

Test 96: Dull-gray color; soft, dense, punky coke, with no apparent cell structure; drawn from oven in large and small chunks, very easily crushed; test was run slowly and high enough heat was not obtained, which accounts for the large percentage of breeze.

Test 97: Dull-gray color; soft, dense coke; cell structure small; better than cokefrom washed coal.

Test 100: Dull-gray color; soft, dense, punky coke; possibly little better than coke from this coal, with addition of 10 per cent of pitch.

Arkansas No. 7 B. Test 104: Dull, dark color; very soft, light-weight coke; no appar­ ent cell structure; drawn from oven in large and small lumps; bottom 6 inches did not coke, burning to ash, all volatile being expelled, but did not stick together.

Test 105: Soft, dense, punky coke; drawn from oven in large and small chunks; somewhat better and heavier than coke from coal containing no pitch.

Arkansas No. 9. Test 98: No coke produced; charge ashed over top and down about 5 inches. ," " - ---- -- --

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COKING TESTS. 37

Arkansas-No. 9. Test 99: No coke produced; ashed down about 4 inches. : Test 101: No coke produced; ashed down about 6 inches.

Test 102: Soft, dense, punky coke; drawn from oven in large and small chunks. . Test 103: Soft, dense, punky coke; drawn from oven in large and small chunks;

high yield-of breeze, due to large amount of coal whose volatile was expelled,not sticking together; 5 per cent of pitch not sufficient .for this coal.

Georgia No. 1. Test 173: Poor, dense coke; large pieces of irregular size; ash high;probably reduced ash and materially improved by washing.

Illinois No. 7 D. Test 1: Good, hard coke with medium cell structure; breakagestraight and long. This was the first charge after firing ovens, and results werenot as good as might be expected.

Test 4: Light-gray and silvery color; metallic ring; cell structure good; breakagesomewhat marred by cross fracture, but pieces'of good size; good, strong coke,much improved by washing.

Illinois No. 11 D. Test 5: Light-gray and silvery color; metallic ring; cell structuregood; breakage, good long pieces; good, strong coke.

Illinois No. 18. Test 2: Dull-gray color; cell structure good; breakage marred bycross fracture, probably due to successive charging of small portions.

Test 3: Dull-gray color; cell structure small; cross breakage more pronounced than from washed coal.

Illinois, No. 16. Test 7: Accident to charging larry necessitated discontinuing test.Coal burned to keep oven hot.

Test-10: Dull-gray color; cell structure small.Illinois No. 19 .4. -Tests 11, 15, and 19: No coke produced; the whole charge was

burned and volatile was expelled, but the residue would not bind together.Illinois No. 20. Test 106: Dull-gray color; cell structure small; breakage bad; sepa­

rate and distinct cross fracture all over oven, coking in layers; ash and sulphur high.

Test 107: Dull-gray color; some little deposit of carbon; .metallic ring; cell structure small, but not dense; breakage somewhat marred by cross fracture; pieces of good size; great improvement over former test; ash and sulphur high.

Illinois No. 21. Test 126: No coke produced.Test 137: Burned very vigorously for 12 hours, afterwards falling off rapidly to small

candles all over surface of charge; when pulled, after 45 hours, product was mix­ ture of unburned coal and slightly coherent mass of coal of original size showing no trace of cell structure; all volatile apparently expelled.

Illinois No. 22 B. Test 117: Dull-gray color; cell structure medium; breakage very irregular, probably owing to high amount of slate; poor coke; heavy clinker over whole surface; ash and sulphur high.

Test 118: Light-gray color; upper 12 inches fingered, two 6-inch sections below in chunks; upper 12 inches had metallic ring and good cell structure; the remain­ ing coke poor. This oven was held 72 hours on account of accident. Under more favorable conditions, the whole charge would have probably been better coke. Ash and sulphur high.

Illinois No. 23 A. Test 111: Light-gray color; some silvery deposit of carbon; cell structure a little large; breakage large-fingered pieces; metallic ring; ush and sulphur high.

Illinois No. 23 B. Test 112: Light-gray color; a little silvery deposit of carbon; metal­ lic ring; cell structure a little large; breakage, long, thin pieces; larger charges would probably make better coke; ash and sulphur high.

Test 114: Light-gray color; a little silvery deposit of carbon; metallic ring; cell structure good; breakage, long, thin pieces and large 6-inch chunks; bottom very hot; bottom 6 inches probably coked upward; ash and sulphur high.

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38 WASHING, COKING, AND CUPOLA TESTS.

Illinois No. 24 A. Test 119: No coke produced; ashed down about 4 inches.Test 155: No coke produced; all volatile driven off; high heat of by-product ovens

quickly applied might produce coke.Illinois No. 24 B. Test 145: Dull-gray color; practically no cell structure; barely

stuck together; very poor, dense coke, with high sulphur.Illinois No. 25 A. Test 120: No coke produced.

Test 140: Dull-gray color; cell structure small; soft, dense coke; breakage poor; two distinct layers of 16 inches and 8 inches, the lower coming out in chunks; high ash and sulphur.

Illinois No. 26. Test 143: Dull-gray color, soft, dense coke; breakage poor; practi­ cally no cell structure; ash and sulphur high.

Illinois No. 27. Test 144: Poor, soft, dense coke; breakage poor; sulphur high.Illinois No. 28 C. Test 166: Dark-gray color; cell structure small; breakage, good,

uniform size. .Illinois No. 29 A. Test 169: Dark-gray color; drawn from oven in three distinct

layers; breakage poor; large chunks and small-fingered pieces; poor, dense coke; high sulphur.

Test 170: Dull-gray color; some silvery coloration; metallic ring; drawn from oven in 6-inch chunks of practically uniform size; cell structure good; more rapid burning and higher heat produced gave much better coke than former charge; sulphur high.

.Illinois No. 34 B. Test 190: Light-gray and silvery color; metallic ring; cell structure a little large; breakage good; uniform-sized pieces; yield low on account of burning, but could be easily increased on better acquaintance; good coke; sulphur high.

Indiana No. 3. Test 14: No coke produced; ashed down about 10 inches and blaze lost.

Indiana No. 4- Test 6: Light-gray color; cell structure a little large; breakage some­ what marred by cross fracture.

Test 9: Light-gray and silvery color; metallic ring; fine-fingered pieces; cell structure large; ash and sulphur reduced by washing.

Indiana No. 5. Test 8: Light-gray and silvery color; metallic ring; cell structure large; breakage, good, long pieces; good coke.

Indiana No. 6. Test 12: Light-gray and silvery color; cell structure good; breakage good; metallic ring; good coke, but ash and sulphur high..

Indiana No. 7 A. Test 13: Light-gray and silvery color; metallic ring; cell structure large; breakage somewhat marred by cross fracture, somewhat brittle; ash and sulphur high. %

Indiana No. 9 A. Test 16: Light-gray and silvery color; cell structure small; breakage somewhat marred by cross fracture, brittle; ash and sulphur high.

Indiana No. 9 B. Test 17: Light-gray and silvery c'olor; cell structures mall; long- fingered, heavy coke; high ash and sulphur.

Test 18: Light-gray and silvery color; metallic ring; breakage somewhat brittle; cell structure good; ash and sulphur somewhat reduced by washing, but still high.

Indiana No. 11 D. Test 51: Light-gray color; metallic ring; breakage, long, fine- fingered pieces; cell structure medium.

Indiana No. 12. Test 108: Light gray, with a little silvery coloration; metallic ring;cell structure a little large; breakage, good-sized pieces; ash and sulphur high.

Test 109: Light-gray color; some silvery deposit of carbon; cell structure large; breakage, good-sized pieces; ash and sulphur reduced by washing, but still high.

Test 110: Light-gray color; some silvery deposit of carbon; breakage practically the same as in test 109; somewhat larger size; cell structure not quite so large; metallic ring; good weight; ash and sulphur high.

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COKING TESTS. ' 39

Indiana No. 17. Test 163: Dark-gray color; breakage,-large pieces of irregular si/e;cell structure large; ash and sulphur high.

Indiana No. 18 A. Test 158: No coke produced; ashed down about 3 inches, and blazelost.

Test 168: No coke produced. Kansas No. 6. Test 113: Light-gray color, some silvery coloration; cell structure good;

breakage good; long, large, heavy pieces; heavy clinker over whole surface ofcoke; ash and sulphur high; washing would probably reduce ash very materially,and produce better grade of coke. .

Test 115: Light-gray and silvery color; metallic ring; breakage good; long, large,heavy pieces; cell structure good; strong heavy coke; washing reduces ash andsulphur, but both still high.

Kentucky No. 1 B. Test 76: Light-gray and silvery color; much deposited carbon;metallic ring; cell structure good; a fine-fingered coke; breakage bad, brittle.

Kentucky No. 1 C. Test 71: Light-gray and silvery color; metallic'ring; cell structurea little large; breakage, long, thin-fingered pieces; good coke, but very brittle.

Kentucky No. 5. Test 75: Light-gray and silvery color; much deposited carbon;metallic ring; cell structure good; breakage bad, very brittle.

Kentucky No. 6. Test 86: Light-gray and silvery color; metallic ring; cell structure small; breakage, long, fine-fingered pieces, very brittle.

Test 90: Light-gray and silvery color; metallic ring; cell structure small; breakagebad, brittle; fine-fingered coke.

Kentucky No. 7. Test 85: Light-gray and silvery color; metallic ring; cell structuregood; breakage good; long, large pieces; coke contains a large amount of hardclinker on top and through cracks; good weight coke; ash and sulphur high.

Kentucky No. 8. Test 164: Dark-gray color, with some little silvery deposit of car­ bon; cell structure large; breakage good; regular-sized pieces.

Test 165: Light-gray color; breakage good; large pieces of regular si/e; cell struc­ ture a little large; some little improvement over test No. 164.

Kentucky No. 9 A. Test 167: Light-gray color, with black top and some silvery depositof carbon; cell structure good; breakage, long-fingered pieces; sulphur high.

Maryland No. 1. Tests 50, 54: No coke produced.Test 58 (with 10 per cent pitch): Dull-gray color; cell structure small; breakage,

large and small chunks; poor, soft coke. Missouri No. 5. Test 116: Light-gray and silvery color; cell structure good; breakage

somewhat cross fractured but pieces of good, large size; good weight coke; ashand sulphur high.

New Mexico No. 3 B. Test 148: Light-gray color, some silvery deposit of carbon;metallic ring; cell structure medium; breakage good; long, large pieces; good,heavy coke, but ash high.

Test 149: Light-gray color; some silvery deposit of carbon; metallic ring; cellstructure medium; breakage good; long, large pieces; good, heavy cuke; ashreduced by washing, but still high.

New Mexico Nos. 3 B, 4 B, and 5. Test 152: Light-gray and silvery color; metallicring; cell structure good; breakage good; long, large pieces; good, strong, heavycoke.

New Mexico No. 4 B. Test 150: Light-gray color; silvery deposit of carbon; metallic.ring; cell structure good; .breakage somewhat cross fractured, but pieces of good,large, uniform size; good, heavy coke; high ash.

Test 151: Light-gray and silvery color; large deposit of carbon; metallic ring;cell structure good; breakage good; long, large pieces; good, strong, heavy coke;ash reduced by washing.

New Mexico No. 5. Test 146: Light-gray color; cell structure a little large; breakagesomewhat marred by cross fracture; good, heavy coke; ash high; blaze lostafter 15 hours, and necessary heat not attained.

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40 ' WASHING, COKING, AND "CUPOLA

New Mexico No. 5. Test 147: Light-gray color, some silvery deposit of carbon; metallic ring; cell structure a little large; breakage good; long, large, heavy pieces; ash reduced by washing, but still high.

Ohio No. 1. Test 24: Light-gray and silvery color; metallic ring; breakage good; fine- fingered pieces; cell structure good; good weight coke; high sulphur.

Ohio No. 2. Test 27: Dull-gray color; cell structure close; poor coke, soft and easily broken.

Ohio No. 3. Test 31: Charge burned to ash.Ohio No. 4- Test 28: Light-gray and silvery color; metallic ring; breakage good;

long, large pieces; cell structure good; very heavy; sulphur high.Ohio No. 5. Test 22: Light-gray and silvery color; metallic ring; cell structure good;

long-fingered coke, brittle.Ohio No. 6. Test 59: Light-gray and silvery color; metallic ring; cell structure a

little large; breakage good; large, long, heavy pieces; high sulphur. Test 66: Light-gray and silvery color; metallic ring; cell structure large; break­

age somewhat crosswise, but good-sized pieces; ash and sulphur reduced by washing, but sulphur still high.

Ohio No. 7. Test 89: Light-gray and silvery color; metallic ring; cell structure alittle large; breakage good; long pieces; large-fingered coke; high sulphur.

Test 94: Light-gray and silvery color; metallic ring; cell structure a little large; breakage fine-fingered; very brittle; ash and sulphur reduced by washing, but sulphur still high.

Ohio No. 8. Test 81: Light-gray colo.r; metallic ring; breakage long, thin pieces;cell structure small; fingered coke, very brittle; ash and sulphur high.

Test 93: Light-gray color, with black-fused bottom, not a butt; metallic ring; cell . structure small. About three-fourths of oven coked up 8 inches, and the upper

16 inches coked down, showing clear demarcation; the lower 8 inches in chunks, the upper 16 inches fingered; very brittle; ash and sulphur reduced by wash­ ing, but sulphur high.

Ohio No. 9 A. Test 72: Light-gray and silvery color; metallic ring; breakage long and thin pieces; fine-fingered coke, very brittle; sulphur high.

Ohio No. 9 B. Test 55: Dull-gray color; cell structure small; breakage bad; verybrittle; ash and sulphur high.

Test 57: Light-gray color; metallic ring; cell structure good; breakage bad; fine- fingered coke, very brittle; sulphur high; ash greatly reduced by washing.

Ohio No. 12. Test 180: Light-gray color; some silvery, deposit of carbon; metallic ring; cell structure large; breakage somewhat cross fractured; sulphur high.

Pennsylvania No. 5. Test 25: Light-gray and silvery color; much deposited carbon; metallic ring; cell structure a little large; breakage good; long, large pieces; good, heavy coke.

Test 26: Light-gray and silvery color; metallic ring; cell structure good; breakage good; long, large pieces; good, heavy coke; ash and phosphorus reduced by washing, the phosphorus over 50 per cent.

Pennsylvania No. 6. Test 32: Light-gray and silvery color; much deposited carbon; metallic ring; cell structure good; breakage good; long, large pieces; very heavy coke; sulphur and ash high.

- Test 34: Light-gray and silvery color; metallic ring; cell structure good; break­ age somewhat irregular, but not so good as from raw charge; very heavy coke; ash and sulphur reduced by washing.

Test 35: Light-gray and silvery color; metallic ring; cell structure good; break­ age good; long, large pieces; very heavy; ash and sulphur high.

Test 38: Light-gray and silvery color; metallic ring; .cell structure a little small; breakage good; ash and sulphur reduced by washing.

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COKING TESTS, 41

Pennsylvania No. 6. Test 41: Light-gray and silvery color; much deposited carbon; metallic ring; cell structure small; breakage good; long, large pieces; very heavy; ash and sulphur high.

Pennsylvania No. 7. Test 30: Light-gray color; cell structure small; breakage longand irregular, but in large pieces; very heavy; ash and sulphur high.

Test 33: Light-gray color; breakage, large and small lumps, very irregular; cell ' structure small; coke heavy; sulphur reduced by washing; ash not materially affected.

Pennsylvania No. 8. Test 29: Dull-gray color; breakage bad; large and small chunks;cell structure small; soft, dense coke.

Pennsylvania No. 9. Test 37: Some few pieces of coke obtained, but the amount wasso small that it was not determined.

Test 39: Some few pieces of coke; mostly large lumps of closely adhering ash. Test 42: Dull-gray color; cell structure small; poor, dense coke. Test 56 (with 5 per cent pitch): Dull-gray color; cell structure medium; breakage

very irregular; large and small lumps; poor; soft coke, scarcely any better than coke from washed coal.

Pennsylvania No. 10. Test 47: Light-gray and silvery color; metallic ring; breakagepoor, somewhat brittle; cell structure large.

Test 53: Light-gray and silvery col or; metallic ring; cell structure good; breakage bad; increase in yield of coke and decrease in amount of breeze probably due to fine grinding. .

Pennsylvania No. 11. Test 159: Light-gray Color; metallic ring; cell structure a little small; breakage good; long, large pieces.

Pennsylvania No. 12. Test 161: Light-gray and silvery color; metallic ring; cell structure a little small; breakage good; large pieces; good, heavy coke; sul­ phur a little high.

Test 162: Light-gray color; some deposit of carbon; metallic ring; cell structure a little small; breakage good; uniform-sized pieces; ash reduced by washing; good, strong coke.

Pennsylvania No. 15.-^-Test 185: Dull-gray color; soft, dense coke; cell structure small; breakage badly cross fractured, and pieces of irregular si/e; sulphur high: .

Test 188: Light-gray color, some silvery deposit of carbon; cell structure medium; breakage somewhat cross fractured, but pieces of good, uniform si/e; much improvement over coke from finely ground charge; sulphur high.

Pennsylvania No. 17. Test 178: Light-gray and silvery color; cell structure a littlesmall; breakage good; long, large pieces; good, heavy coke.

" Test 186: Light-gray and silvery color; metallic ring; cell structure good; break­ age good; large pieces of uniform size; good, strong, heavy coke; ash and sul­ phur reduced by washing.

Pennsylvania No. 19. Test 176: Light-gray color; some silvery deposit of carbon; cell structure small; breakage marred by cross fracture, probably due in large meas­ ure to uncrushed slate; good, heavy coke, somewhat brittle.

Test 177: Light-gray and silvery color; metallic ring; cell structure a little small; breakage good; .large, uniform pieces; crushing improves physical appearances and increases total yield.

Pennsylvania No. 20. Test 179: Gray color, some .silvery deposit; cell structure small; breakage irregular, but pieces of good size; soft, dense coke; high sulphur.

Test 182: Gray color; soft, dense coke; no evident physical improvement over raw charge; ash and sulphur reduced by washing.

Pennsylvania No. 21. Test 183: Light-gray and silvery color; metallic ring; cell structure small but not dense; breakage somewhat marred by cross fructure, but pieces of good, uniform size; good, heavy coke.

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42 WASHING, COKING, AND CUPOLA TESTS. .

Pennsylvania No. 21. Test 187: Light-gray and silvery color; metallic ring; cell struc­ ture small, not dense; breakage good; long, large pieces; good, heavy coke.

Test 189: Light-gray and silvery color; metallic ring; cell structure small, not dense; breakage somewhat marred by cross fracture, but pieces of good, uniform size; good, heavy coke.

Test 191: Light-gray and silvery color; cell structure small, not dense; metallicring; breakage good; uniform size; good, heavy coke.

Test 192: Light-gray and silvery color; metallic ring; cell structure a little small, not dense; breakage good; uniform size; good, heavy coke.

Tennessee No. 1. Test 133: Light-gray and silvery color; metallic ring; cell structure a little large; breakage good; long, large pieces; good, strong, hard, heavy coke; ash a little high.

Test 153: Light-gray and silvery color; metallic ring; cell structure good; break­ age somewhat marred by cross fracture, but pieces of good, uniform size; good, heavy coke; ash and sulphur reduced by washing.

Tennessee No. 2. Test 127: Light-gray and silvery color; metallic ring; 'cell structure medium; breakage poor; very brittle, long-fingered .pieces.

Tennessee No. 3. Test 128: Light-gray and silvery color; metallic ring; cell struc­ ture good; breakage poor; very brittle, long-fingered pieces. "

Tennessee No. 4- Test 125: Light-gray and silvery color; metallic ring; cell structuregood; breakage, long-fingered pieces; f-inch black butt.

Test 129: Light-gray and silvery color; metallic ring; cell structure good; break­ age, long-fingered pieces; black butt removed.

Tennessee No. 5. Test 154: Light-gray and silvery color; metallic ring; cell structure a little large; breakage good; long, large pieces; good, heavy coke; sulphur high.

Tennessee No. 6. Test 122: Light-gray and silvery color; metallic ring; cell structure good; breakage, good; long, large pieces; good, strong,- heavy coke; ash high; probably reduced by washing.

Tennessee No. 7 B. Test 121: Poor coke; soft, tough, and punky; drawn from ovenin large chunks; ash and sulphur high.

Test 123: Light-gray and silvery color; metallic ring; cell structure a little large; breakage good; large, uniform-sized pieces; strong coke, great.improvement over raw charge; ash and sulphur reduced by washing, but still high.

Tennessee No. 8 B. Test 134: Light-gray and silvery color; metallic ring; cell struc­

ture large; breakage somewhat cross fractured, but pieces of good, large, uni­ form size; sulphur high.

Tennessee No. 9. Test 124: Light-gray color; some silvery deposit of carbon; metallic ring; cell structure large; breaks in irregular pieces of good size.

Tennessee No. 10. Test 156: Poor coke; drawn from oven in large, irregular lumps; very tough and dense; with black butt and high ash.

Tennessee No. 11. Test 160: Poor coke; breakage, large pieces of irregular size;- cell structure small; dense and punky; small amount not coked well at bottom; ash high.

Utah No. 1. Test 130: Dull-gray color; practically no cell structure; soft, dense coke; very fine-fingered pieces, very brittle, and easily broken into small pieces.

Test 141: With K. I. No. 1. No coke produced; all volatile expelled and chargeburned entirely to bottom.

Test 157: With R. I. No. 1. Very poor, dense coke; half the product did not cement together; the other half very finely fingered coke, very brittle and easily broken, similar to coke from Utah No. 1.

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COKING TESTS. 43

Virginia No. 1. Test 64: Light-gray color; metallic ring; cell structure good; break­ age somewhat marred by cross fracture, but pieces of good size; hard, heavy coke, not dense.

Test 65: Light-gray and silvery color; much deposited carbon; cell structure medium; metallic ring; breakage somewhat marred by cross fracture, but pieces of good size; good, hard coke. ;

Test 67: Light-gray and silvery color; much deposited carbon; cell structure medium; metallic ring; breakage somewhat marred by cross fracture, probably due to uncrushed slate; lower yield of coke and higher amount of bree/e proba­ bly due to fact that coal was not crushed.

Test 68: Light-gray and silvery color; much deposited carbon; metallic ring; cell structure medium; breakage somewhat marred by cross fracture, but pieces of good size; large amount of breeze and lowered percentage yield probably due to fact that coal was not crushed.

Test 77: Light-gray and silvery color; much deposited carbon; metallic ring; cell structure good; breakage somewhat marred by cross fracture, but pieces of good size; good, hard, heavy coke; increased yield of coke and decreased amount of breeze probably due to fine grinding.

Virginia No. 2. Test 63: Light-gray and silvery color; metallic ring; cell structure a little large; breakage somewhat marred by cross fracture, but pieces of good size.

Test 69: Light-gray and silvery color; much deposited carbon; metallic ring; cell structure medium; breakage good; long, large pieces, somewhat brittle; decreased yield of coke and increased amount of breeze probably due to fact that coal was not crushed.

Test 70: Light-gray and silvery color; metallic ring; cell structure large; break­ age somewhat marred by cross fracture, but pieces of good size; good, hard coke, somewhat brittle; washing does not seem to benefit it materially.

Virginia No. 3. Test 61: Light-gray and silvery color; much deposited carbon; metallic ring; cell structure small; breakage good; long, large, heavy pieces; very heavy coke.

Test 88: Light-gray and silvery color; much deposited carbon; metallic ring; cell structure small; breakage good; good, heavy coke; decreased yield of coke and increased amount of breeze probably due to fact that coal was not crushed.

Virginia No. 4- Test 62: Light-gray and silvery color; much deposited carbon; metallic ring; cell structure good; breakage, long, thin pieces; light weight; fingered coke.

Virginia No. 6. Test 181: Light-gray color; cell structure small; dense coke; break­ age very irregular; pieces of various sizes; high sulphur.

Test 184: Light-gray and silvery color; much deposited carbon; cell structure small, but not dense; breakage, irregular pieces of various sizes; washing reduces ash and sulphur and improves quality of coke.

Washington No. 2. Test 135: Light-gray color; some deposit of carbon; fair ring; cell structure small; breakage, long-fingered pieces, very brittle; dense coke; high ash.

West Virginia No: 4 B. Test 40: Light-gray and silvery color; much deposited carbon;metallic ring; cell structure good.

Test 44: Light-gray and silvery color; much deposited carbon; metallic ring; cellstructure good; breakage good; long, large pieces.

Test 46: Light-gray and silvery color; metallic ring; cell structure good; breakage somewhat marred by cross fracture, but pieces of good size; high yield of coke and decreased amount of breeze probably due to fine grinding.

West Virginia No. 13. Test 21: Light-gray and silvery color; metallic ring; cell struc­ ture good; breakage good; long, large, heavy pieces.

Page 44: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

44 WASHING, COKING, AND CUPOLA TESTS.

West Virginia Nos. 18 and 14. Test 23: Light-gray and silvery color; metallic ring; cell structure medium; breakage good; long, large, heavy pieces.

West Virginia No. 14- Test 20: Light-gray and silvery color; metallic ring; cell struc­ ture a little large; breakage good; long, large, heavy pieces; good, hard coke.

West Virginia No. 15. Test 36: Light-gray and silvery color; much deposited carbon; metallic ring; cell structure good; breakage good; long, large, pieces; good, heavy coke; high sulphur.

Test 43: Light-gray and silvery color; metallic ring; cell structure a little small; breakage good; long, large pieces; hard, heavy coke; sulphur high.

West Virginia No. 16 A. Test 73: Light-gray'and silvery color; much deposited car­ bon; metallic ring; cell structure a little large; breakage somewhat marred by cross fracture, but pieces of good size; good, hard, heavy coke.

West Virginia No. 16 B. Test 45: Cell structure good; breakage good; long, largepieces; good, heavy coke.

Test 48: Light-gray and silvery color; much deposited carbon; metallic ring; cell structure a little large; breakage somewhat marred by cross fracture, but pieces of good size; somewhat brittle; washing does not appear to improve coke, on the contrary the coke from the raw charge is decidedly better.

Test 49: Light-gray and silvery color; metallic ring; cell structure large; breakage somewhat marred by cross fracture; coke brittle; washing does not appear to improve physical properties of coke; sulphur and ash somewhat lowered.

West Virginia No. 17. Test 60: Light-gray and silvery color; metallic ring; cell struc­ ture good; breakage good.

West Virginia No. 18. Test 74: Light-gray aiid silvery color; much deposited carbon; metallic ring; cell structure good; breakage somewhat crosswise; coke brittle; good, hard, heavy coke.

Test 78: Light-gray and silvery color; metallic ring; cell structure good; breakage somewhat crosswise; coke brittle; good, hard, heavy coke; no appreciable differ­ ence in yield between the crushed and uncrushed charges.

West Virginia No. 19. Test 79: Dull-gray color; some silver; cell structure small,rather dense; breakage good; poor, light-weight coke.

Test 83: Dull-gray color; some silver; cell structure small; breakage good. This oven was burned with a smaller draft and coke was much heavier and b'etter than that from test 79.

West Virginia No. 20 Test 80: Light-gray and silvery color; much deposited carbon; metallic ring; cell structure small, not dense; breakage good; long, large, pieces, somewhat brittle; good, hard, heavy coke.

Test 84: Light-gray and silvery color; metallic ring; cell structure good; breakage marred by cross fracture, but pieces of good size; washing, does not materially benefit; on the contrary, the coke is not as good as that from raw coal.

Test 87: Light-gray and silvery color; much deposited carbon; metallic ring; cell structure a little small; breakage very irregular, but pieces of good size; de­ creased percentage of coke and increased percentage of breeze probably due to fact that coke was not crushed.

Test 92: Light-gray and silvery color; metallic ring; cell structure small, not dense; breakage somewhat marred by cross fracture, but pieces of good size; good, heavy coke.

West Virginia No. 21. Test 82: Light-gray and silvery color; much deposited carbon;, metallic ring; cell structure good; breakage good; long, large pieces; good, hard, heavy coke.

Test 91: Light-gray and silvery color; much deposited carbon; metallic ring; cell structure large; breakage very irregular and brittle; washing does not materially improve coke, on the contrary the coke from raw charge is decidedly better.

Page 45: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

COKING TESTS. 45

West Virginia No. 25. Test 175: Light-gray color, some silvery deposit of carbon; cellstructure a little small; breakage, long, large, fingered pieces, very brittle.

Wyoming No. 3. Test 52: Charge burned to ash down about 8 inches. Wyoming No. 5. Test 132: No coke produced.

CONCLUSIONS.

It is unfortunate that the necessary routine' work in order to cover so many coals permitted so few tests on each, and that the supply of coal in many cases permitted only one test to be made on that par­ ticular coal. The data here presented show the results' obtained under the best conditions possible to one not conversant with the burning -of these coals, based on observations made from time to time.as coking proceeded. These facts should be distinctly'borne in. mind when analyzing the results here presented. It is hoped that in future work it may be possible to vary conditions, make changes as they suggest themselves, and compare results on many different tests of the same coal and thus draw conclusions of a more definite nature. It is to be regretted that no comparisons can be made between beehive and by-product coke, but the nature of the work here recorded and the facilities provided confined operations to ovens of the beehive pattern exclusively.

No data are given in the detailed statement for compressive strength or height of furnace burden supported, as the results obtained" show conclusively the worthlessness of these determinations. This' con­ clusion was reached after careful attempts to obtain results on 1-inch cubes. Four cubes were selected from each coke made, care being taken to obtain pieces with no fracture and representing as nearly as possible the average of the coke. The cubes were cut by means of an emery wheel and guide, and although by no means perfect they were as nearly so as possible and always the two sides used in the machine were parallel. The machine used for breaking was a Tinius Olsen patent machine of 10,000 pounds capacity and gave direct readings of the ultimate strength. '

Only a few of these results, taken at random, are given, and these only to show their great variation and the worthlessness of this method of drawing conclusions. Illinois No. 16, test 10, 910 pounds, 1,330 pounds, 2,190 pounds, and 2,270 pounds; Indiana No. 4, test 6, 640 pounds, 790 pounds,-1,060 pounds, and 1,245 pounds; Kentucky No. 1, test 76, 880 pounds, 1,0.65 pounds, 1,920 pounds, and 2,570 pounds; Ohio No. 9, test 94, 535-pounds, 890 pounds, 1,170 pounds, and 1,600 pounds; Virginia No. 1, .test 68, 740 pounds, 1,120 pounds, 1,280 pounds,: and. 2,060 pounds; West Virginia No. 16, test 49, 520 pounds, 1,500 pounds, 1-,7.80 pounds, and 2,100 pounds.

The difficulty of obtaining a cube, or any number of cubes, to repre­ sent anything more than the piece of coke from which it is taken is so apparent that results pretending to show compressive strength of any

Page 46: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

46 WASHING, .COKING, AND CUPOLA TESTS.

amount of coke are worse than useless in fact, misleading. Even if coke is selected the whole height of the charge and tests are made on cubes in number representing the number of inches the results still show only the strength of the one piece of coke from some par­ ticular part of the oven and it is practically impossible to procure even approximately similar results from other pieces taken from different places. The condition of burning, the quenching either inside or out, and any number of factors which it is not possible to know, much less control, make different portions of the same oven vary greatly.

A simple calculation will show that coke with a compressiye strength of 48 pounds will support the burden of any modern furnace; consequently this test gives no data of practical value. Moreover, there are so many other factors, such as action of heat and gases, attri­ tion of coke against coke, against other ingredients of charge/ and against the side walls, etc., that any calculation to show the burden- bearing capacity of the coke, even if it were possible to select cubes representing the whole charge, would be inaccurate if based simply on a compression test.

An endeavor was made to compare the different cokes by approxi­ mating the amount of breakage under conditions of present-day handling, showing the percentage of coke over 2-inch size that may be expected to reach the top of the charge in the blast furnace. Fifty pounds of each coke were selected, as nearly as possible representing the average size of the coke after handling at the ovens. This coke was dropped a distance of 6 feet onto a rigid (1-inch) iron plate. All pieces over 2 inches in size were weighed and again dropped, the operation being repeated three times. The results of these drop tests are shown in the detailed statement.

The yield of coke appears to be increased and the amount of breezereduced by preliminary crushing. Whether there is a limit to the degree of fineness, or whether a point may be reached beyond which finer crushing gives no appreciable improvement or has opposite effects, can not be determined from the present results; but the data available indicate that it would be economical to crush all coal before charging into the ovens, even though a coke of good quality may be obtained without this preliminary treatment. Fine crushing also appears to increase the strength of the coke and make the fracture less irregular, by the greater uniformity and distribution of the ash, but the weight per cubic foot is reduced. The strength of the coke is probably influenced by the amount, composition, and distribution of the ash, but the results so far obtained show no definite relations between these factors or their relative importance.

The matter of investigating the action of C02 on red-hot coke as determining its value for furnace work was thoroughly considered.

Page 47: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

COKING TESTS. 47

The conclusion was reached that it was of no practical importance, as there are so many other factors in the blast furnace. In view of the fact that the gases in the furnace are mixtures of C02 , CO, H, 0, N, water vapor, and probably others, it appears that action of CO2 is of little value unless the action of these other gases, either inde­ pendently or in connection with C02 , is known. An investigation of the action of CO2 on red-hot coke, as a means of making comparison, of hardness, is being made and gives evidence of yielding some positive results, but work along this line has not progressed far enough to draw any definite conclusions.

The loss of sulphur from coal to coke by volatilization varies with, the different coals, depending on several factors, among which, in the order of their importance, are the condition in which sulphur exists in the coal, the heat of the oven, the rapidity of coking, and watering. The sulphur loss ranged from 20.79 per cent on Arkansas No. 1 (test 95) to 63.07 per cent on Illinois No. 29 (test 170), the average for all tests being 43.27 per cent.

Page 48: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

CUPOLA TESTS OF COKE.

By RICHARD MOLDENKK. '

EQUIPMENT.

Owing to the removal of one of the cupolas which served for the foundry tests during the Louisiana Purchase Exposition all the tests made since then have been.conducted in the 36-inch foundry cupola loaned by the Whiting Foundry Equipment Company, of Chicago. The remaining apparatus was rearranged and the 36-inch shell of the cupola was relined to 26 inches internal diameter. There were four horizontal tuyeres measuring 4 by 6 inches on the outside and 3 by 13 inches on the inside of the cupola which' were situated 11 inches above the sand bottom. The total tuyere area was 96 square inches, giving a ratio of Tto 5.96 with the cupola area. A No. 6 Sturtevant fan run at 2,514 revolutions per minute furnished the blast, which was kept at about 7 ounces.

By proper training, the crew was able to run off two heats a day without interruption. The melted iron was poured into molds for sash weights, thus reducing to a minimum the amount of scrap made.

PERSONNEL.

The cupola tests were conducted by W. G. Ireland, under the direction of A. W. Belden, coke expert of the Geological Survey, and by the advice of Richard Moldenke, foundry expert in charge of the cupola tests of the fuel-testing plant.

METHOD OF TESTING.

The method of testing has been fully described in the report of the fuel-testing plant for 1904.° Toward the end of the tests it was some­ times necessary to vary the proportion of scrap to pig iron according to the supply, but the total amounts were kept correct as planned for the general series of tests.

After completing the tests on the available cokes in the regular way, so that the results might be comparable with the previous work

oProf. Paper U. S. Qeol. Survey No. 48, part 3,1906, pp. 1367-1370. -

48

Page 49: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

CUPOLA TESTS OF COKE. 49

of the division, a series of further tests was made on some of these cokes. In these tests the coke bed was not kept at a constant height above the tuyeres, but the carbon content was calculated from the .analysis of the particular coke and an amount taken to make up 175 pounds of carbon regardless of the height above the tuyeres. The results show interesting features. Some cokes gave melting ratios and melting rates per hour which were better than with the ordinary test methods and others gave inferior results. The tests were made to show the advisability on the part of the manufacturer as well as of the foundryman of studying the conditions of cupola practice in order to determine those which give the best results.

D'ETAILED RESULTS.

The detailed results of the regular tests as well as of the special 175- pound carbon bed tests will be found in the following tables. Results of a typical test of Connellsville 72-hour coke are given at the head of the first table as a standard for comparison. All the tests here reported were made within the calendar year 1906 except test 190, on coke from Pennsylvania No. 21 coal, the date of which was February 13, 1907. Many of the coals tested, however, were received during 1905.

23975 Bull. ;«6 OS 4

Page 50: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

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Page 51: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

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585

600

570

600

570

570

600

600

540

600

600

570

920

720

720

540

585

800

600

690

750

720

840

800

600

800

570

180

190

240

220

230

220

200

200

220

220

210

180

195

200

190

200

190

. 19

0

200

200

180

200

190

200

190

180

195

200

230

250

250

240

190

200

190

80 63 60 48 53 50 53

58

58

53

53 oo 63 59 58 60 58 60 60 58 58 62 58 60 58 60 37 49 80 63 59 58 58 50 45 45 48 60 42 75 58 58 60

570

428

420

383

398

390

398

413

413

398

398

405

428

417

413

420

413

420

420

413

413

427

413

420

413

420

520

570

570

428

417

550

413

390

375

375

383

420

540

550

413

550

420

143

140

128

133

130

133

138

138

133

133

135

143

139

138

140

138

140

140

138

138

142

138

140

138-

140

143

139

138

130

125

125

128

140

138

140

80 63 60 48 53 .50 53 58

58

53

53 63 59 58 60 58 60 60 58 58 62 58 60 58 60 36 49 SO 63 59 58 58 50 45 45 48 60 41 75 58 58 60

570

/428

420

383

398

390

398

413

413

398

398

405

428

416

413

420

413

420

420

413

413

427

413

420

413

420

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428

416

550

413

390

"*R

3

420

413

550

430

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140

128

133

130

133

138

138

133

133

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143

139

138

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138

140

140

138

138

14

213

814

013

814

0

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125

125

128

140

138

140

80 62 60 47 52 50 52

57

57

52

52 oo 62 59 57 60 60 60 57 57 63 57 60 57 60 36 49 80 62 59 57 57 50 45 45 47 60 41 75 57 57 60

570

427

420

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397

390

397

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39

0

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420

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140

127

132

130

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137

132

132

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142

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137

140 13

714

014

0

137

137

143

137

140

137

140

142

139

137

130

125

137

146

80 62 60 47 52 50 52-

57

57

52

52 oo 62 58 57 60 57 60 60 57 63 60 57 60 36 48 80 62 58 57 57 50 45 45 47 60 41 57 57 60

570

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412

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570

570

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390

375

420

540

. 55

041

2

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127

132

130

132

137

137

132

132

135

142

138

137

140

137

140

140

137

137

143

137

140

137

140

142

138

137

130

195

125

137

140

500

430

430

430

430-

430

430

430

430

430

430

430

430

430

430

430

430

430

430

430

430

430

430

430

430

430

375

375

500

430

430

430

430

430

430

430

430

430

375

500

430

430

430

3,00

0

2,25

02,

250

2,25

02,

250

2,25

02,

250

2,25

02,

250

2,25

02,

250

2,25

02,

250

2,25

02,

250

2,25

02,

250

.2,2

502,

250

2,25

02,

250

2,25

02,

250

2,25

02,

250

2,25

03,

000

3,00

03,

000

2,25

02,

250

3,00

02,

250

2,25

02,

250

2,25

02,

250

2,25

0

3,00

03.

000

2', 2

503,

000

2,25

0

W 750

750

750

750

750

750

750

750

750

750

750

750

750

' 75

075

075

075

075

0

750

750

750

750

750

750

950

W w w 750

750

750

750

750

750

750

750

(»)

W 750

750

6 7 7 7 7 7 7 7 .7 7 7 7 7 7 7 7 7 7 7 7 7-

7 7 7 7 7 8 8 6 7 7 7 7 7 7 7 7 7 8 6 7 7 7<»

Det

ails

of

orig

in o

f co

al s

ampl

es c

an b

e fo

und

in B

ull.

U.

S. G

eol.

Sur

vey

No.

290

,190

0.*>

Pig

iro

n us

ed f

rom

car

131

943.

c P

lus

10 p

er c

ent

pitc

h.d

Pig

iro

n us

ed f

rom

car

276

33.

e P

lus

5 pe

r ce

nt p

itch

.

Page 52: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

Cupola

tes

ts o

f co

ke fr

om

coa

ls r

ecei

ved

in 1

90

5 C

on

tin

ued

.O

r

Cup

ola

test

N

o. 1 86

20

51

49

167

168

182

169

170 50

36

37

77

181 38

39

46

45

62

41

43

63

90

17

7 71.

42

44

72

88

Des

igna

tion

of

coke

.

Fie

ld N

o. o

f co

al.

2

VV

est V

irgi

nia C

on.

4B (

w.).

...:.

..15...............

15

....

....

....

...

15...............

15...............

15...............

16..............

16...............

16 B

............

16 A

............

16 B

(w

.).......

16 B

(w

.).......

16 B

(w

.)..

...:

.17

(w

.).........

18

....

....

....

...

18- ....

....

....

..1

9..

....

....

....

.19

. .....

....

....

.19...............

20 A

(w

.).......

20

A (

w.)

- -.

..-.

20 A

.....

.20

A ...

....

....

20 A

(w

.).......

20 A

(w

.).......

21.......

......

21 (

w.)

. ..

....

..21

(w

.) ...

....

..

Co

ke

test

N

o.

Dat

e.

3 4

46

23

36

43

3C

30

43

45

45

45

73

48 49

. 49 60 78

79

S3

83

84

84

80

80

87

87

82

91

91

Oct

. 1

July

7

Sep

t. 1

4 S

ept.

12

No

v.

23

No

v.

24

Dec

. 4

No

v.

24

No

v.

26

Sep

t. 1

4 Ju

ly

24

....do ...

Sep

t. 2

4 D

ec.

4 Ju

ly

25

Sep

t. 1

1 S

ept.

10

Au

g.

13

Sep

t.

5 S

ept.

6

Au

g.

13

Oct

. 5

Dec

. 1

Au

g.

18

Sep

t.

6 S

ept.

8

Au

g.

20

Au

g.

29

Char

ges

(pounds)

.

Co

ke

bed

.

5 190

190

220

220

230

230

200

180

190

190

190

190

170

195

210

220

200

190

190

190

220

220

240

200

230

210

180

200

190

Pig

ir

on.

6 570

570

880

880

920

920

600

720

760

760

570

570

510

585

630

660

600

570

570

570

660

C60

720

600

690

630

540

600

570

Scr

ap.

7 190

190

200

190

190

170

195

210

220

200

. 19

0 19

0 19

0 22

0 22

0 '

240

200

230

210

180

200

190

Cok

e.

8 60

60

53

53

37

68

58

' 49

78

60

60

60

65

59

55

52

58

60

60

.

60

53

53

48

58

. 50

55

63

58

60

.Pig

ir

on

.

9 420

420

530

530

520

520

. 41

3 57

0 56

0 56

0 42

0 42

0 43

5 41

7 40

5 39

7 41

3 42

0 42

0 42

0 39

8 39

8 38

3 41

3 39

0 40

5 42

8 41

3 42

0

Scr

ap.

10 140

140

138

140

140

145

139

135

132

138

140

140

140

133

133

128

138

130

135

143

138

140

Cok

e.

11 60

60

53

53

36

68

58

49

78

60

60

60

65

59

55

52

58

60

60

60

53

53

48

58

50

55

63

58

60

Pig

ir

on.

12 420

420

530

530

520

520

413

570

560

560

420

420

435

416

405

397

413

420

420

420

398

398

383

413

390

405

428

413

420

Scr

ap.

13 140

140

138

140

140

145

139

135

132

138

140

140

140

133

133

128

138

130

135

143

138

140

Cok

e.

14 60

60

52

52

36

67

57

49

77

60

60

60

65

59

55

53

57

60

60

60

52

52

47

57

50

55

62

57

60

Pig

. ir

on.

15 420

420

530

530

520

520

412

570

560

560

420

420

435

416

405

398

412

420

420

420

397

397

382

412

390

405

427

412

420

Scr

ap.

16 140

140

137

140

140

145

139

135

133

137

140

140

140

132

132

127

137

130

135

142

137

140

Cok

e.

17 60

60

52

52

36

67

57

48

77

60

60.

60

65

58

55

53

57

60.

60

60

52

52

47

57

50

55

62

57

60

Pig iron.

18 420

420

530

530

520

520

412

570

560

560

420

420

435

416

405

398

412

420

420

420

397

397

382

412

390

405

427

412

420

Scr

ap.

19 140

140

137

140

140

145

138

135

133

137

140

140

140

132

132

127

137

130

135

142

137

140

To

tal.

%

Co

ke

20 43

0 43

0 43

0 43

0 37

5 50

0 43

0 37

5 50

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0

Pig

ir

on

.

21

2,25

0 2,

250

3,00

0 3,

000

3,00

0 3,

000

2,25

0 3,

000

3,00

0 3,

000

2,25

0 2,

250

2,25

0 2,

250

2,25

0 2,

250

2,25

0 2,

250

2,25

0 2,

250

2,25

0 2,

250

2,25

0 2,

250

2,25

0 2,

250

2,25

0 2,

250

2,25

0

Scr

ap.

22 750

750

(«)

(a) 75

0 (a

)<»

> 750'

750

750

750

750

750

750

750

750

750

750

750

'750

75

0 75

0 75

0 75

0 75

0 75

0

Rat

io

iron t

o

coke

.

23

7 7 .

7 7 8 6 7 8 6 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7

o a I t-3 te)

Pig

iro

n us

ed f

rom

car

131

943.

Page 53: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

Cup

ola

test

s of c

oke fr

om

coa

ls r

ecei

ved

in 1

905 C

on

tin

ued

.

Cupola test

No. 1 19 54

21

93

94 82

83

187 48

175

173

174 81

185-

22

18

4 29

26

27

28

89

67

47

55 75

Des

igna

tion

of c

oke.

Fiel

d N

o. o

f coa

l.

2

Con

nell

svil

le

Illi

nois

: 11

D (

w.)

...

13 (

w.)

......

13...........

16. .

.........

Ind

ian

a:

4(w

.). ......

5............

7 A

(-07

"I

7 A

(w

.)....

9............

9. ...........

9B

(w

.) ...

.9B

(w

.)....

11...........

11...........

Ken

tuck

y:

1C

.........

IB

.........

5............

6............

6............

6............

7............

7............

Mar

ylan

d:

1 (w

.)«

....

..

Coke

test

No. 3 5 2 3 10 9 8 8 13 13 17 17 18 18 51

51 71

76

75

90 90

86

85 85 58

Anal

ysi

s of

cok

e (p

er c

ent)

."

Moisture.

24 0.18

1.19

4.

60

2.73

2.

14 .55

.76

.76

1.13

1.13 .68

.68

.91

.91

1.55

1.

55

1.32

.9

3 .3

0 1.

641.

64

2.81

.2

3.2

3

.27

Volatile

matter. 25 0.32 .93

1.68

1.

36

1.46 .38

.54

.54

2.35

2.35

2.85

2.85 .97

.97

1.66

1.

66

1.53

1.

25

1.21

1.

.69

1.69

1.

27

2.16

2.16 .88

Fixed

carbon.

26

88.7

5

85.9

7 82

.08

79.3

0 83

.96

85.9

181

.29

81.2

983

.23

83.2

378

.44

78.4

484

.60

84.0

9 84

.09

84.6

8 91

.40

93.2

6 92

.26

92.2

6 91

.93

82.9

782

.97

87.4

7

< 27

10.7

5

11.9

1 11

.64

16.6

1 12

.44

13.1

617

.41

17.4

113

.29

13.2

918

.03

18.0

313

.52

13.5

212

.70

12.7

0

12. 4

7 '6

.42

5.23

4.

41

4.41

3.

99

14.6

414

.64

11.3

8

Su

lph

ur.

In

coke.

28 0.87

1.44

1.

27

1.77

1.

02

2.06

4.21

4.21

2.69

2.69

3.50

3.50

2.24

2.24

1.34

1.

34 .96

1.05

.4

1 .3

7 .3

7 .4

0 3.

163.

16 .95

In

ash. 29

0.03

3

.135

.1

5 .1

0 .0

5 16

Phosphorus.

30

0.01

8

.006

5 .0

07

.016

2 .0

076

.20

!.......

.20

'...

....

.07

....

...

.07

.......

.210

'.......

.210

'.......

.04

.04

.07

.04

.025

.0

5 .0

5 .0

2 .0

1.0

1

.09

.042

.0

42

.044

.0

3 .0

12

.003

3.

.003

3 .0

021

.027

8

Specific

gravity.

31 1.92

1.87

1.

85

1.90

1.

85

1.86

1.

91

1.91

1.

85

1.85

1.

84

1.84

1.

84

1.84

1.

83

1.83

1.88

1.

94

1.84

1.

78

1.78

1.

79

1.83

1.

83

1.91

3 o t~* o 2^i

>>

2

£ 32 (»)

99.9

99

.9

97.2

2 81

.94

99.9

99

.9

93.0

5 90

.28

94.4

4 94

.44

88.8

8 99

.9

94.4

4 99

.9

99.9

97.2

95

.83

94.4

4 99

.10

98 6

1 99

.30

95.8

3 97

.91

99.9

Maximum

blast pres­

sure (ounces) .

33

73 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7

Rec

ord

of

rnel

t.

Pounds

of i

ron.

Poured.

34

2,47

0

1,87

4 82

2 1,

770

1,23

0

1,56

8 1,

562

1,62

2 1,

761

2,24

7 78

2 1,

854

1,83

4 1,

827

1,36

4 2,

163

1,63

9 1,

970

1,88

5 1,

624

1,87

2 1,

885

2,12

0 1,

849

1,74

8

Additi on a 1 melted

.

35 490

86

0 46

257

8

347

605

145

719

403

235

276

279

363

357

253

450

284

482

290

247

314

529

377

326

p 36

2,47

0

2,36

4 1,

682

2,23

2 1,

808

1,91

5 2,

167

1,76

7 2,

480

2,65

0 1,

017

2,13

0 2,

113

2,19

0 1,

721

2,41

6

2,08

9 2,

254

2,36

7 1,

914

2,11

9 2,

199

2,64

9 2,

226

2,07

4

Mel

ting

ra

te.

-f

' 3

S-i

O«3

37

5,48

9

4,72

8 2,

925

5,35

6 3,

874

3,93

0 4,

642

3,02

9 4,

022

5,48

3 2,

653

3,65

1 4,

372

4,10

6 1,

912

4,S

32

2,50

7 5,

009

3,73

7 3,

589

4,38

4 4,

123

4,96

7 5,

136

3,96

9

Increase or

decrease.

38 Inc.

Dec

. (d

) In

c.

Rec

over

ed

(pou

nds)

.

0 frn

£ o O

39

j 40

283

418

1,06

4 60

6 95

8

921

611

920

258 22

1,

836

650

717

608

899

233

773

475

552

845

709

490

209

435

732

20 71

110 71

59 57

62

47

67

65

59

44

66

48

51

49 35

30

64

43

77

52

59

62 114

+

?te

gc 5

"o

'r£ 41 8.2

7.23

8.

46

5.4

7. S

O

5.47

7.

4 10

.43

6.55

10

.93

4.90

7.

33

5.67

6.

73

12.6

6 11

.7

4.60

9.

03

2.70

8.

03

5.73

10

.36

4.73

11

.3

6.47

Mel

ting

rati

o.

Iron

to

coke. 42 6.02

6.58

5.

26

6.22

4.

87

5.13

5.

89

3.90

6.

83

7.26

3.

22

4.67

5.

80

5.73

4.

54

6.34

5.29

5.

64

6.47

4.

95

6.00

5.

82

7.14

6.

05

6.56

Increase or

decrease.

43 Inc.

Dec

.

Inc.

Cok

e be

d .

Increase

(+) ordecreas

e( ) (pounds

).

44

c+45

c+25

c+15

-'

Heightabove to

p of

tu­ yeres

(inche

s).

45 21.4

17.9

16.2

o Fb

r'che

mic

al a

naly

ses

of c

oals

fro

m w

hich

the

se c

okes

wer

e m

ade,

see

pp.

27-

35.

<* T

roub

le w

ith i

ron

notc

h ac

coun

ts f

or lo

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me

betw

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ent p

itch.

CO

Page 54: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

Cup

ola

test

s o

f cok

e fr

om

coa

ls r

ecei

ved

in 1

905 C

on

tin

ued

.en

Cupola

test

No. 1 23

80

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180 60

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8.

57

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31 1.84

1.

82

1.86

1.

88

1.81

1.

86

1.86

1.84

1.

84

1.96

1.

91

1.91

1.

92

1.92

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1.84

1.

83

1.92

1.

76

1.76

1.

94

1.99

1.

99

1.85

1.

92

1.80

1.

79

1.87

1.

83

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Fluidity

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.

32

99.9

98

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97.9

1 99

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98.6

1 92

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93.0

5

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Page 55: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

CUPOLA TESTS OF COKE. 55

PCOPCOt^ Ot^cOl^PfCiooooos

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Page 56: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

Cup

ola

test

s o

f co

ke fr

om

coa

ls r

ecei

ved

in 1

90

5 C

onti

nued

.O

r 05

Cu­

po

la

test

N

o. 1 19 54

21

93

94 82

83

187 48

175

173

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26

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last

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at

11.1

1 a.

in

.; b

elt

011

fan

bro

ke w

hil

e p

ou

rin

g s

ixte

enth

lad

le.

Page 62: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

Cup

ola

test

s of c

oke f

rom

, co

als

rece

ived

in 1

905 C

onti

nued

.05

Cu­

p

ola

te

st

N

o. 1 19 54

21 93

94 82

83

187 48

17

5 17

3 17

4 81

185 22 184 29

26

27

28

89

67

47 55

75 23

80

57

Des

ignat

ion o

f co

ke.

Fie

ld N

o. o

f co

al.

o

Illi

nois

: 11

D (

w.)

.........

13 (

w.)

. ....

....

..

13.................

16....-.

..-.

--.....

Indi

ana:

5..................

7 A

(w

.) .........

7 A

(w

.). .........

9 9.-

-..........-

.-..

9 B

(w

.) .....

....

.9

B (

w.)

.....

....

.11..........

....

...

11.................

Ken

tuck

y:

1C

....

....

....

...

IB

........

....

...

5. ............. ....

6..

....

............

6..

....

............

6..................

7. .........

....

....

7. . ................

Mar

ylan

d:

1 (w

.)*

. .........

Ohi

o:

5..................

6 A

, 6

B (

w.)

.....

7 (w

.)..

.. ........

Cok

e te

st

No. 3

5 3 10 9 8 8 13

13 17

18 18 £1 51 71 76

75

90 90

86

85 85

58 22

66 94

Rec

ord

of

mel

t C

onti

nued

.

Wei

gh

t an

d t

ime

of e

ach l

adle

of

mel

ted i

ron-

^Con

tinu

ed.

21.

Lbs

.

88 89 90

62

91 46 30 69 42

71

52 81

45

83 75 113

100

At

89 11. 5

5J

11. 3

2J

10. 5

6i

11.1

5

4.31

ii.3

2

4.22

10.1

6 2.

57

9.52

ii. 2

610

.26

3. 5

8J

5.05

2.34

4.32

22.

Lbs

.

90 72 44

79

79 90 96

31

45 86

97 87 83

At

91

11.5

6

11.4

3 10

.57

11.1

7

10.1

7 2.

58

9.57

10.2

7 3.

59

2.34

*

4.32

J

23.

Lbs.

92 49

101

130 60 95

47 31 86

At-

93

10.5

8 11

. 17J

4.23

10.1

8

10.2

8 4.

01

2.36

4.33

24.

Lbs

.

94 54

91 71

41

At

95 11.0

1 11

.18

4.24

10.2

0

,77 99

4.01

J

4.37

25.

Lbs

.

96 46

65 88

'23

106 89

At

97

11.0

2 11

.20

4.25

10.2

1

4.02

4.37

J

26.

Lbs

.

98 93 33 41 91

At

99

11.2

1

10.2

3

4.03

4.38

Mel

ting

ti

me

(min

­ ute

s) .

-

100

27 30

34J

25

28 30

28

45

37

29

23

35

29

32

54 30 50

27

38

32

29

32

32 26

31 39

24

36

Rem

ark

s.

101

Iron h

ot.

Do.

Ir

on v

ery h

ot

and f

luid

, but c

hill

ed a

t bott

om

; be

d burn

ed o

ut.

T

emp

erat

ure

of

iron m

ediu

m.

Iron c

old.

Tem

per

ature

of

iron m

ediu

m.

Tem

per

ature

of

iron m

ediu

m;

bla

st o

ff 1

min

ute

. T

emper

ature

of

iron m

ediu

m.

Iron c

old.

T

emp

erat

ure

of

iron m

ediu

m.

' Ir

on c

old.

T

emper

ature

of

firs

t 7

ladl

es m

ediu

m ;

bal

ance

hot.

Ir

on h

ot.

T

emper

ature

of

iron m

ediu

m.

Iron v

ery h

ot

and

flu

id;

coke

rec

omm

ende

d fo

r fu

ther

tri

al.

Iro

n h

ot.

Do.

Ir

on v

ery h

ot.

Ir

on h

ot

and f

luid

. Ir

on h

ot.

Iron h

ot

and f

luid

. Ir

on h

ot;

all

pig

iro

n u

sed

to d

eter

min

e ef

fect

of

sul­

phur;

27

th l

adle

80

po

un

ds

at

4.03

£; 2

8th

ladle

67

pounds

at

4.04

; 29

th l

adle

35

pounds

at

4.06

. Ir

on h

ot

and f

luid

.

Iron h

ot.

Iron v

ery

hot

and

flu

id.

Iron h

ot.

Ir

on v

ery h

ot

and f

luid

; 27

th l

adle

76

po

un

ds

at

4.39

; 28

th l

adle

65

pounds

at

4.41

.

Page 63: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

70 56 165

166 68 180 60 85 87 84 176 ?5 61 66 79 65 188 64 76 189 30 73 24 78 31 69 186 59 183

158

171

17? 9? 178 5? 3? 33 91 58 40 34

7.................

8 A

(w

.). ..

....

..

9..

....

....

....

...

9..

....

....

....

...

Pen

nsy

lvan

ia:

5 B

(vv

.) .........

5 B

(w

.) .........

6....

......

.....:

.6

....

....

....

....

.

6.................

6 A

.6B

(w

.) .

...

6 A

, 6

B (

w.)

...

.6

A,

6 B

(w

.) .

...

6 A

.6B

(w

.) .

...

7 A

.7B

(w

.) ...

..7

A,7

B ..........

8..

....

....

....

....

8..

....

....

....

....

9 (w

.)6. ..........

9(w

.)..

....

....

..9

(w.)

....

.. ......

10

....

....

....

....

.10..

....

...........

Vir

gin

ia:

1 A

...............

1 A

...............

IB

...............

1 A

....

....

....

...

1 A

...............

1 A

...............

1 A

....

....

....

...

1. ...... ...........

2(w

.)..

.. ...

....

.2(w

.)... .........

2B

.. .......

....

..2B

........

...

....

2B

.. .....

....

....

2 B

(w

.)..........

3..........

....

...

3..

....

....

....

....

3..................

3..................

4..

....

....

....

....

89 93 72 72 26 26 32 41 41 34 34 38 38 33 30 29 29 56 42 42 47 53 64 65 77 67 67 68 68 69 70 70 63 63 69 70 61 61 88 88 62

4? 79 80 101

10? 41 50 66 48 55 81 61 7? 68 83 10

1Q

C 33 74 14 27 99 48 98 101

12.0

2

3m

3.54

3.31

10.2

2

4 01

4. 2

210

.08

4.11

A

*>Q

1

3.37

11. 4

0J11

.32

11. 1

7$4.

174 2

428

8.22

10.5

6J4.

42

4.06

10. 0

5J

9.30

*

35 10?

101 41 80 79 07 84 55 9?

100 .33 8? 46 104

121 95 149 37 1?1

103 60 74

12.0

4

11.5

9

3.02

3.54

J

3.31

*10

.25

12.0

84.

02

4224

.10

.12

41

2

431

3. 3

7411

.41

11.3

611

.18

A

10

8.22

J

11.0

1444

408

11.0

611

.58

9.31

36 80 97 77 88 43 Q5

87 70 60 94 27 77 65 83 52 104

65 64 77 78

12.0

44.

3.55

3.3

410

.26

12. 0

84.

4024

.

423

4124

.

432

3.4

011

.42

11.3

6J11

.20

42

0

8.23

11.0

94.

11. 5

94.

9.3

5

3fi

69 87 96 95 110 48 88 74 60 59 26 51 99 92 28 97

i-2. 0

5

12.0

0

3.05

3.58

3.35

10. 2

64.

12. 1

04.

4 0

4

i is

3.41

11.4

3

11.2

2A

O

ftl

894

12 0

09.

36

90 53 9? 40 58 ?6 92 57 / - 66

3.05

J

3.59

3.36

10.2

7

ii ii

4 04

4

_

414

4 2

1

9.37

73 89 67A

O

O

33 40 32 00 30 00 30 29 00 26 40 32 28 29 29 OO 30 35 OQ

27 9Q O

Q

Ol

OQ

01 25 27

-O

O 29 on OO

OQ

01 07 36

Iron

ver

y hot

and

flui

d.Ir

on h

ot a

nd f

luid

; bla

st o

fl 9

min

utes

on

acco

unt o

lhar

d i

ron

notc

h.

Tem

pera

ture

ol

iron

med

ium

.

Iron h

ot.

Iron c

old.

Ir

on c

old;

cok

e in

bed

ve

ry h

ard t

o ig

nite

; be

dbu

rned

ver

y sl

owly

. B

otto

m d

ropp

ed a

t 1.

40 p

. m

.; bla

st o

n 30

min

utes

;no

iro

n m

elte

d.

Iron c

old.

Iron h

ot;

bla

st o

fl 1

min

ute.

Ir

on v

ery

ho

t.

Iron

hot

; ch

arge

s hu

ng in

cup

ola

and

bott

om

had

tobe

dro

pped

; b

last

ofl

2 m

inut

es.

Iron h

ot.

Tem

pera

ture

ol

iron

med

ium

. Ir

on h

ot.

Do.

Ir

on h

ot;

27th

ladle

79 p

ound

s at

4.0

7; 2

8th

lad

le

58 p

ound

s at

4.08

. Ir

on c

old.

Ir

on h

ot.

Tem

pera

ture

ol

iron

med

ium

. Ir

on h

ot

and

flui

d; b

last

off

6 m

inut

es.

Iron h

ot.

Iron h

ot

alte

r th

ird

lad

le.

Tem

pera

ture

ol

iron

med

ium

.Ir

on v

ery

hot

and

flui

d; b

last

ofl

4 m

inut

es.

Tem

pera

ture

ol

iron

med

ium

.Ir

on h

ot.

Tem

pera

ture

ol

iron

med

ium

.Ir

on h

ot.

Do.

Do.

Do.

Tem

pera

ture

ol

iron

med

ium

. Ir

on h

ot.

Iron

hot

; al

l pi

g ir

on u

sed

tox d

eter

min

e ef

fect

, ol

sulp

hur.

Iron

ver

y hot

and f

luid

. Ir

on h

ot

and

flui

d;

mel

ting

to

o la

st

to

hand

le;

bla

st o

fl 4

min

utes

. Ir

on h

ot.

Iron

hot

; bla

st o

fl 5

min

utes

. T

empe

ratu

re o

l ir

on m

ediu

m.

Iron v

ery

hot

and f

luid

.o

Plu

s 10

per

cen

t pi

tch.

t> P

lus

5 per

cen

t pi

tch.

O5

OO

Page 64: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

Cup

ola

test

s of

coke

from

coa

ls r

ecei

ved

in 1

90

5 C

on

tin

ued

.C

5

Cu­

po

la

test

N

o. 1 159

160 35

53 74

86

20

51 49

167

'168

182

169

170 50 36

37

77

181 38

39

46

45

62

41

43

63

90

17

7 71

42

44

72

88

Des

igna

tion

of c

oke.

Fiel

d N

o. o

f coa

l.

2

Wes

t Vir

gini

a:

4..........

....

....

4B

...... ...

....

..4B

(w

.)..

....

....

4 B

(w

.) ...

....

...

4 B

(w

.) ...

....

...

13 a

nd 1

4..

....

...

15

........-.

.---

-.-

15....... ..........

15........

.........

15........

.........

16.................

16 B

......-

-...-

..

16 A

..............

16 B

(w

.)..

....

...

16 B

(w

.)......-..

16 B

(w

.).........

17 (

w.)

. ....

....

..18........

.........

18

...-

..--

-....-

-..

19 19 1Q 20 A

(w

)

20 A

.....

.........

on

A

20 A

(w

.) ...

....

..21 21

(w

.)...........

21 (

w.)

... ........

Co

ke

test

No

.

3 44 44

40

44 46

46 23

36 43 36

43 45

45 73

48

49 49

60

74

78

79

83

83

84

84

80

80 87

87

82

91

91

Reco

rd o

f m

elt

C

onti

nued.

Weig

ht

and t

ime o

f each l

ad

le o

f m

elt

ed

iro

n C

onti

nued.

21.

Lb

s.

88

119

101 91 72 78

71 30 96

14

8

102 63

44 77

42

77

67

97

104 84

52

82

94 78

83

50

107 70

At 89

11.3

04

3.0

44

10.2

8

8.5

7

3.0

3

2.0

44

4.2

6

11

.39

4.4

2J

11.2

94

9.5

9

3.1

9

11

.44

10

.11

3.4

94

11.0

2

3.4

44

10

.29

4

.04

4

4.0

6

4.0

84

1

1.0

0

11

.37

11

.37

1

1.0

9

4164

22.

Lb

s.

90 97

83

92 61 10

7 85 102

140

92 52

43 49

62

91

87

69

55

76

110

90

52 66 54 69

At

91

11.3

1 3

.05

10

.32

8.5

9

3.0

4

2.07

11.3

94

443

11.3

0

10.0

0 3

.20

11.4

5 10

.13

3.51

1

1.0

4

3.4

5

10.2

94

405

410

409

11.0

3

11

.38

il.3

8

417

23.

Lbs.

,

92 65

43

35 157 72

10

2 83 83 118 82 70

77

92

73

52

45

98

86

88 120

At

93

11.3

2 3.0

54

10.3

4

8.5

94

3.0

7

2.0

74

.11.

40

11.3

4

10.0

2 3.2

1

10.1

4 3.5

211

.044

3.4

6

10.3

2 4.

07

410

11.0

4

4.1

8

24.

Lb

s.

91 100 47 64

85 97 100 89 42 54

11

8 66

100 92 68

At

95

3.1

2

9.0

0

3.1

0

2.0

8

11

.42

11. 3

44

10

.03

3

.21

4

10

.15

3.

5J

11

.05

3.4

7

10. 3

24

4.1

1

25.

Lbs.

96

At

97

92

793.1

2

2.1

0

100

11.

4.J

8811.3

5

49 43

27

70

72

82

3.2

2

10.1

6 3

.54

11.0

8

3.4

8

10.3

3

i

26.

Lbs.

| A

t

98

.

99

|

64

! 3.

13

69

2. 1

2

45, ;

11

.36

31

3.2

3

68

3. 5

6 78

11

-09

75

3. 5

0

i

Melt

ing

ti

me

(min

­ u

tes)

.

10

0

33

31

34

25 33

28

36

29

' 42

31

32

23

40

29

25 33

46

29

30

-

38

34

37

36

24

33

34

30

30

33

34

27

29

29

31

Rem

ark

s.

101

Tem

per

ature

of

iron m

ediu

m.

Iron h

ot.

Ir

on v

ery

hot

and

flu

id.

Iron h

ot;

all

pig

ir

on

used

to d

eter

min

e ef

fect

of

sulp

hur.

Ir

on h

ot.

T

emp

erat

ure

of

iron m

ediu

m.

Iron v

ery

hot

and

flu

id.

Iron h

ot;

all

pig

ir

on u

sed

to d

eter

min

e ef

fect

of

sulp

hu

r.

Do.

Iron h

ot.

T

emp

erat

ure

of

iron m

ediu

m.

Iron v

ery

col

d.

Iron h

ot.

T

emper

ature

of

iron m

ediu

m;

nil

pig

iron u

sed

to

det

erm

ine

effe

ct o

f su

lphur.

Ir

on h

ot;

bla

st o

ff 4

min

ute

s.

Iron f

airl

y h

ot but

slug

gish

. Ir

on h

ot.

D

o.

Iron h

ot

but

slug

gish

. Ir

on v

ery h

ot

and

flu

id.

Iron h

ot.

'

Do.

Ir

on h

ot

and

flu

id.

Iron h

ot.

D

o.

Iron h

ot

and

flu

id.

Iron h

ot.

Ir

on c

old.

Ir

on h

ot

and f

luid

. T

emper

ature

of

iron

med

ium

. D

o.

Iron h

ot.

D

o.

Page 65: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

Cup

ola

test

s of c

oke f

rom

coa

ls r

ecei

ved fr

om

January

1,

1906

, to

Ju

ne

SO,

1907

.

o «

Cup

ola

5 te

st

Jt N

o.

£ ^ 1

/5

JO »

107

131

0

132

*

101

108

103

j,

124

109

133 96

115

116

142 95

117

125

150

157

164

121

148

122

147

155

156

149

162

163

Des

igna

tion

of

coke

.

Fie

ld N

o. o

f co

al."

2

Ala

bam

a:

2B

(w

.)........

2B

(w

.)........

3................

3(w

.). ..........

3 (w

.)..... ......

4.................

4................

4(w

.).. .........

4 (w

.).. .........

Ark

ansa

s:IB

(W

.)6.......

IB

(W

.)6.......

. 7

B (

w.)

c.......

9 (w

.)&

-...

......

9 (w

.)».-

-. ......

Illi

nois

: 22

B (

w.)

...

....

9Q f\

v ^

29 (

w.)

..........

9Q f

\v )

India

na:

12

(w

.).. ........

17 (

w.)

... .......

Kan

sas:

6(w

.)..........

Ken

tuck

y:

8................

8................

8.................

9 A

(w

.) ...

....

.9

A (

w.)

........

9 A

(w

.)........

Cok

e te

st

No. 3 14

2 14

2 13

813

9 13

9 13

1 13

1 13

6 13

6 97

97

105

105

102

102

118

170

170

170

110

163

115

164

164

164

167

167

167

Dat

e.

4

Aug

. 1

Aug

. 25

Sep

t.

7 A

ug.

2 S

ept.

8

Aug

. 21

A

ug.

3 A

ug.

27

Sep

t.

4 A

ug.

9 A

ug.

10

Sep

t.

1 S

ept.

4

Aug

. 11

Aug

. 21

N

ov.

13

Nov

. 16

N

ov.

22

Aug

. 17

N

ov.

12

Aug

. 23

Nov

. 10

N

ov.

15

Nov

. 16

N

ov.

12

Nov

. 21

....do...

Cha

rges

(pounds)

.

Cok

e be

d. 5 200

200

210

210

210

200

220

190

200

190

190

220

220

210

220

210

190

190

200

180

190

180

200

210

200

170

170

190

Pig

ir

on.

6 600

600

630

630

630

600

660

570

600

570

570

660

660

630

660

630

760

760

800

540

760

540

800

840

800

680

6SO

760

Scr

ap.

7 200

200

210

210

210

200

220

190

200

190

190

220

220

210

220

210

180

180

Cok

e.

8 58

58

55

55

55

58

53

60

58 60

60

53

53

55

53 55

60

78

44 63

60 63 58

73

44

65

52

78

Pig

ir

on.

9 413

413

405

405

405

413

398

420

413

420

420

398

398

405

398

405

560

560

550

428

560

428

550

540

550

580

580

560

Scr

ap.

10 138

138

135

155

135

138

133

140

138

140

140

133

133

135

133

135

143

143

Cok

e.

11 58

58

55

55

55

58

53

60-

58 60

60

53

53

55

53 55

60

78

44 63

60 63 58

73

44

65

51

78

Pig

ir

on.

12 413

413

405

405

405

413

398

420

413

420

420

398

398

405

398

405

560

560

550

428

560

428

550

540

550

580

580

560

Scr

ap.

.13 13

8 13

8 13

5 13

5 13

5 13

8 13

3 14

0 13

8

140

140

133

133

135

133

135

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143

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e.

14 57

57

55

55

55

57

52

60

57 60

60

52

52

55

52 55

60

77

44 62

60 62 57

72

44

65

51

77

Pig

ir

on

.

15 412

412

405

405

405

412

397

420

412

420

420

397

397

405

397

405

560

560

550

427

560

427

550

540

550

580

580

560

Scr

ap.

16 137

137

135

135

135

137

132

140

137

140

140

132

132

135

132

135

142

142

Cok

e.

17 57

57

55

55

55

57

52

60

57 60

60

52

52

55

52 55

60 77 43 62

60 62 57

72

43

65

51

77

Pig

ir

on.

18 412

412

405

405

405

412

397

420

412

420

420

397

397

405

397

405

560

560

550

427

5,60 427

550

540

550

580

580

560

Scr

ap.

19 137

137

135

135

135

137

132

140

137

140

140

132

132

135

132

135

142

142

To

tal.

Cok

e.

20 430

430

430

430

430

430

430

430

230

430

430

430

430

430

430

430

430

500

375

430

430

430

430

500

375

430

375

500

Pig

ir

on

.

21

2,25

0 2,

250

2,25

0 2,

250

2,25

0 2,

250

2,25

0 2,

250

2,25

0

2,25

0 2,

250

2,25

0 2,

250

2,25

0 2,

250

2,25

0 3,

000

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0 3,

000

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0 3,

000

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0

3,00

0 3,

000

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0 3,

000

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0 3.

000

Scr

ap.

22 750

750

750

750

750

750

750

750

750

750

750

750

750

750

750

750

(<*)

(d)

(e) 750

(d) 75

0

(<*) (d)

(d)

(«*>

(e)

< «)

Rat

io

of i

ron

to

cok

e.

23

7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 6 8 7 7 7 7 6 8 7 8 6

o D

etai

ls o

f ori

gin

of c

oal s

ampl

es c

an b

e fo

und in

Bul

l. U

. S.

Geo

l. S

urv

ey N

o. 3

32.

6 P

lus

10 p

er c

ent

pit

ch.

« Plu

s 5

per

cen

t pit

ch.

d P

ig i

ron u

sed

from

car

276

33.

e Pig

iro

n u

sed

from

car

131

943.

Oi

Or

Page 66: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

Cup

ola

test

s of c

oke f

rom

coa

ls r

ecei

ved f

rom

Jan

uary

1,1

906,

to

June

30,1

907 C

on

tin

ued

.O

S

OS

Cup

ola

test

N

o. 1 123

119

120 98

13

0

143

161

145

146

151

152

153

154

190

126 99

128

100

140

104

139

102

105

138

106

129

112

141

113

137

114

135

110

136

Des

igna

tion

of

coke

.

Fie

ld N

o. o

f co

al.

2

Mis

sour

i:

5(w

.)..

.. ...

....

New

Mex

ico:

4B

(w

.)........

5(w

.)..... ......

f 3 4

B (

w.)

....,...

I 5:.

..... ..

....

...

Pen

nsyl

vani

a:

11

.... ...

. ..

....

.12 12

(w

.)........-.

19 12 12

(w

.). ..

....

.--

12 (

w.)

.. ........

21

....

....

....

...

Ten

nes

see:

I..

....

....

....

..l(

w.)

...........

l(w

.).. ...

....

..2................

2. .....

....

....

..3................

3..... ..

....

....

.4................

5 (w

.)... ........

5(w

.)..

...

....

..

6......

..........

7B

(w

.)..

....

..7

B (

w.)

........

8B

(w

.)..

....

..8

B (

w.)

...

....

.9

(w.)

.. ...

....

.9

(w.)

..........

Cok

e te

st

No

.

3 116

151

147

I 15

2

159

159

161

162

161

161

162

162

187

133

153

153

127

127

128

128

125

129

129

154

154

122

.122

- 12

3 12

3 13

4 13

4 12

4 12

4

Dat

e.

4=

Au

g.

20

Au

g.

15

....do.. .

/Ju

ly

27

\Aug.

24

No

v.

8 N

ov.

20

Nov.

9 N

ov.

10

Nov.

13

No

v.

14

....do...

No

v.

15

Feb

. 13

c

Au

g.

22

July

30

A

ug

. 23

Ju

ly

30

Aug.

31

July

31

A

ug

. 31

S

ept.

7

July

31

A

ug

. 30

A

ug

. 1

Au

g.

24

Au

g.

6 S

ept.

1

Au

g.

6 A

ug

. 29

A

ug

. 7

Au

g.

28

Au

g.

3 A

ug

. 28

Char

ges

(pounds)

.

Cok

e b

ed.

5 190

200

220

210

200

200

220

210

210

220

200

210

220

210

190

200

200

190

190

190

190

190

190

190

190

190

230

220

190

190

190

180

190

200

Pig

ir

on

.

6 570

600

660

630

600

800

880

840

840

880

800

840

880

630

570

600

600

570

570

570

570

570

570

570

570

570

690

660

570

570

570

540

570

600

Scra

p.

7 190

200

220

210

200

210

190

200

200

190

190

190

190

190

190

190

190

190

230

220

190

190

190

180

190

200

Cok

e.

8 60 58

53 55

58 58

70

55

55

70

44

73

38J

55 60

57

58

60

60

60

60

60

60

60

60

60

50

53

' 60

'

60

60

63

60 TQ

Pig

iro

n.

9 420

413

398

405

413

550

530

540

540

530

550

540

530

405

420

412

413

420

420

420

420

420

420

420

420

420

390

398

420

420

420

428

420

413

Scr

ap.

10 140

138

133

135

138

135

140

137

138

140

140

140

140

140

140

140

140

140

130

133

140

140

140

143

140

138

Cok

e.

11 60 58

53 55

58 58

70

55

55

70

44

73

38f

55 60

57

58

60

60

60

60 5°

&)

60

60

60

50

53

60

60

60

63

60

58

Pig

ir

on.

12 420

413

398

405

413

550

530

540

540

530

550

540'

530

405

420

412

413

420

420

420

420

420

420

420

420

420

390

398

420

420

420

428

420

413

Scr

ap.

13 140 13

8 13

313

5 13

8

135

140

137

138

140

140

140

140

140

140

140

140

140

130

133

140

140

140

143

140

138

Cok

e.

14 60 57

52 55 57 57

70

55

55

70

44

72

38f

55 60

58

57

60

60

60

60

60

60

60

60

60

50

52

60

60

60

62

60

57

Pig

ir

on.

15 420

412

397

405

412

550

530

540

540

530

550

540

530

405

420

413

412

420

420

420

420

420

420

420

420

420

390

397

420

420

420

427

420

412

Scr

ap.

16 140

137

.132 13

5 13

7

135

140

138

137

140

140

140

140

140

140

140

140

140

130

132

140

140

140

142

140

137

Cok

e.

17 60 57

52 55

57 57

70

55

55

70

43

72

38f

55 60

58

57

60

60

60

60

60

60

60

60

60

50

52

60

60

60

62

60

57

Pig

ir

on.

18 420

412

397

405

412

550

530

540

540

530

550

540

530

405

420

413

412

420

420

420

420

420

420

420

420

420

390

397

420

420

420

427

420

412

Scr

ap.

19 140

137

132

135

137

,13

5

140

138

137

140

140

140

140

140

140

140

140

140

130

132

140

140

140

142

140

137

Tota

l.

Cok

e.

20 430

430

430

430

430

430

500

430

430

500

375

500

375

430

430

' 43

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0 43

0

Pig

ir

on.

21

2,25

0

2,25

0 2,

250

2,25

0 2,

250

3,00

0 3,

000

3,00

0 3,

000

3,00

0 3,

000

3,00

0 3,

000

2,25

0

2,25

0 2,

250

2,25

0 2,

250

2,

250

2,25

0 2,

250

2,25

0 2,

250

2,25

0 2,

250

2,25

0 2,

250

2,25

0 2,

250

2,

250

2,

250

2,25

0 2,

250

2,25

0

Scr

ap.

22 750

750

750

750

750

(a)

(»)

(°)

(a) a (a)

(«) 75

0

750

750

750

750

750

750

750

750

750

750

750

750

750

750

750

750

750

750

750

750

Rati

o

of i

ron

to c

oke.

23

7 7 7 7 7 7 6 7 7 6 8 6 8 7 7 7

7 7 7 7 7 7 7 7 7. 7 7 7 7 7 7 7 7 7

Page 67: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

Ill

127

144

179

118 97 134

10 (

w.)

.........

10 (

w. )

.-..

....

-11

(w

.)..

....

.--

11 -

(w.)

-.. ..

....

.U

tah: 1..

....

....

....

..W

ashin

gto

n:

2..

....

....

....

..2.

...

....

....

....

156

156

160

160

130

135

135

Aug

. 27

230

250

240

220

200

190

200

690

960

660

600

600

230

220

200

200

50 48 53 58 60 58

390

398

413

420

413

130

133

138

138

50 48 53 58 60 58

390

398

413

420

413

130

133

138

140

138

50 47 52 57 60 57

39O

397

412

42O

412

130

132

137

137

50 52 57.

60 57

390

397

412

420

412

130

132

137

137

430

430

430

430

430

2,25

0

3,00

02,

250

2,25

0

2,25

0

750

750

750

750

750

7 7 7 7 7 7

Pig

iro

n u

sed

fro

m c

ar 2

7633

.&

Pig

iro

n u

sed f

rom

car

1319

43.

c!90

7.

O5

Page 68: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

Cup

ola

test

s o

f co

ke fro

m c

oals

rec

eive

d fr

om

Jan

uary

1,

1906

, to

Ju

ne

30,

19

07

Con

tinu

ed.

OO

M Cupola test

No. 107

131

132

101

108

103

124

109

133 96

115

116

142 95

11

7

125

150

157

164

121

148

122

147

155

156

149

162

163

Des

ignat

ion o

f co

ke.

Fie

ld N

o. o

f co

al.

2

Ala

bam

a:

2B

(w

.)......

2B

(w

.) .

....

.3

..........

....

3(w

.} .

....

...

3(w

.) .

....

...

.4

....

....

....

..

4(w

.) .

....

...

4(w

.) .

....

...

Ark

ansa

s:

IB (

w.)

&.....

IB (

w.)

&.....

7B

(w

.)c.....

7B

(w

.)c..

...

9(w

.)&

. ..

....

Illi

nois

: 22

B (

w.)

.....

OQ

/w

\

29 (

w.)

...

....

29 (

w.)

...

....

India

na :

12 (

w.)

...

....

17 (

w.)

...

....

Kan

sas:

6(w

.) .

....

...

Ken

tuck

y:

8..............

8..............

8..............

9 A

(w

)

9 A

(w

.)..

....

6

fc s 0 O 3 142

142

138

139

139

131

131

136

136 97

97

105

105

102

102

118

170

170

170

110

163

115

164

164

164

167

167

167

Ana

lysi

s of

cok

e (p

erce

nt)

."

S B '3

3 24 3.04

.

3.04

2.

03

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2.

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! o d % £ 26 82.1

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1.

16

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7

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0

1.6

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1.0

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3.6

5

2.4

9

2.4

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2.4

9

2.8

9

3.3

9

2.4

9

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.93

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1.9

6

1.9

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A 03 a

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Specific

gravity.

31

1.88

1.

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1.91

1.

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1.95

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95

1.95

1.96

1.

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1.97

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04

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1.

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1.83

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83

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1.90

1.90

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90

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'

1.86

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86

1.86

0> Si S 4

J ^

CO 4

J

>>9

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T3 3 fe 32 99

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99.9

97

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98.6

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.

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Maximum

blast pres­

sure (ounces).

33

7 7 7 7 7 7 ' 7 7 7 7 7 7 7 7 6§ 7 7 7 7 7 7 7 7 7 7 7 7 7

Rec

ord

of

melt

.

Po

un

ds

of i

ron.

. -d

2 g PI 34

2,25

7 1,

852

740

1,69

5 1,

822

1,45

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00

Page 69: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

123

119

120 98 130

143

161

145

146

151

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154

190

1?6 99 ra 100

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05

Page 70: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

Cup

ola

test

s of c

oke f

rom

coa

ls r

ecei

ved fr

om

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uary

1,

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o. 1 107

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132

101

108

103

124

109

133 96

115

116

142 95

117

125

150

157

164

121

148

122

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156

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163

123

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164

164

164

167

167

167

116

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Page 71: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

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Page 74: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

Cup

ola

test

s of

coke

fro

m c

oals

rec

eive

d fro

m J

anua

ry 1

, 19

06,

to J

une

SO,

1907 C

onti

nued

.

Cu­

po

la

test

N

o. 1 107

131

132

101

108

103

124

109

133 96

115

116

142 95

11

7

125

150

157

164

121

148

122

147

155

156

149

162

163

123

Des

igna

tion

of

coke

.

Fie

ld N

o. o

f co

al.

2

Ala

bam

a:

2 B

(w

.) .

........

2 B

(w

.) ..........

Q 3(w

.)..

.. ........

3(w

.)..

....

...

...

4..

....

....

....

....

4..................

4(w

.).. ...

....

...

4(w

.)..... ..

....

.A

rkan

sas:

IB

(w

.)0-

-- -

----

-IB

(w

.)0

-. -

----

--

7B

(w

.)6-

- .......

7B (

w.)

6--

----

-- -

9(w

.)»

--.-

...

....

Illi

nois

: 22

B (

w.)

...

....

..90 (w

~l

9Q (w

\

29 (

w.)

...........

Indi

ana:

12

(w

.)...........

17 (

w.)

- ..........

Kan

sas:

. 6

(w.)

... .........

Ken

tuck

y:

8..................

8..................

8..................

9 A

(w

)Q

A

fiv\

Q

A

f-or

S

Mis

sour

i:

5(w

.)... ..

....

...

Cok

e te

st

No. 3 14

2 14

2 13

813

9 13

9101

131

136

136 97

97 105

105

102

118

170

170

170

110

163

115

164

164

164

167

167

167

116

Rec

ord

of

mel

t C

onti

nued

.W

eigh

t an

d ti

me

of e

ach

ladl

e of

mel

ted

iron

C

onti

nued

.

21.

Lbs

.

88 102 20 65 96

52 80 58 88

10

9 94 66

85

78

79

88 90

At-

-

89

2.30

4 11

.144

12.0

0

11.0

3 11

.29

4.31

11.3

4

11.4

1 3.

524

11.1

8

4.23

11

.36

3.39

4 11

.24

4.26

3.49

22.

Lbs.

90 79

86 49 80

103 41 40 92

85 12

6 64

100 97

66

98 70

At

91 2.31

11

.15

12.0

2

11. 0

3J

11.3

2

4.34

11.3

6

11.4

3 3.

53

11.1

9

4.2

11.3

6%

3.4

011

.25

4.2

7

3.5O

23.

Lbs.

92 69

53 109 40 67

83 85

10

3 97

130 56

At

93 2.31

J 11

.154

11.0

4 11

.33

11.4

4 3.

55

4.24

11

.37

3.41

11

.26

3.51

24.

Lbs.

94 83

86 20

93 65

75

67

69 90

At

95 2.33

11

.16

11.4

5 3.

56

4.25

11

.39

3.43

11

.27

3.52

25.

Lbs.

96

103 82 v 55 85 45

At

97 2.33

4 11

.17

4.25

4

3.45

3.52

4

26.

Lbs.

98 52

131 25 69

At

99 2.34

11

.18

4.26

3.53

Mel

ting

tim

e (m

in­

ute

s) .

10

0

31

29

26

35

33 33 27

27

32 36

25

....

..

33 35 28

25 34

34

31

30 25

32 33 31

38

32

28

32

42 34

Rem

arks.

101

Iron v

ery h

ot an

d f

luid

; 2

7th

lad

le 97

po

un

ds at

2.35

.

Iro

n h

ot.

Ir

on h

ot;

sl

ag f

illed

up

tuye

res

afte

r 20

th l

adle

and

b

ott

om

had

to b

e dr

oppe

d.

Tem

pera

ture

of

iron

med

ium

. Ir

on

slu

ggis

h.

Iron v

ery

hot

and

flui

d.

Iron h

ot.

Iron h

ot.

Bed

bur

ned

out

and

char

ges

hung

; bo

tom

had

to

be d

ropp

ed a

fter

lot

h la

dle.

Ir

on h

ot.

Cha

rges

hun

g an

d bo

ttom

dro

pped

aft

er

llth

lad

le.

Tem

pera

ture

of

iron

med

ium

. Ir

on c

old

and

dull

. Ir

on h

ot

and

flui

d.

Iron h

ot.

Tem

pera

ture

of

iron

med

ium

. Ir

on

hot

. Ir

on c

old.

Iro

n d

ull.

Tem

pera

ture

of

iron

med

ium

.

Tem

pera

ture

of

iron

med

ium

. D

o.

Do.

Ir

on

hot

. T

empe

ratu

re o

f ir

on m

ediu

m.

Do.

Tem

pera

ture

of

ir

on

med

ium

; 27

th

ladl

e 92

po

unds

at

3.54

; 28

th l

adle

52

po

unds

at

3.54

4;

29th

lad

le 3

9 po

unds

at

3.55

.

Q

Page 75: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

119

120 98 143

161

145

146

151

152

153

154

190

126 99 128

100

140

104

139

102

' 10

513

810

612

911

2

141

113

137

114

135

110

136

111

127

144

179

118

197

134

New

Mex

ico:

4

B (

w.)

..........

5(w

.)--

-.-

....

.-..

r g

\ 4

B(w

.) ..........

1 5

....

....

....

....

..P

ennsy

lvan

ia:

11.................

11.................

12.................

12 (

w.)

...

....

....

12

....

....

.........

12. .

...............

12 (

w.)

... ........

12 (

w.)

...

....

....

21..

....

...........

Ten

nes

see:

1.

...

....

....

....

..l(

w.)

...-

...

....

.l(

w.)

.........-

-.

2..

....

......

....

..2.

.................

3..

....

....

....

....

4..................

4..................

4..

....

....

....

....

5(w

.). ...........

5(w

.)...... ...

...

6..................

6..

....

....

....

....

7B

(w.)

. ..

....

...

7 B

(w

.)..- -.

..-.

.8

B (

w.)

..........

SB

(w

.)- ..

....

...

9(w

.). ...........

9(w

.)... .........

10 (

w.)

.. .........

10 (

w.)

...........

11 (

w.)

. ..........

11 (

w.)

.. .........

Uta

h: 1..

....

....

....

....

Was

hin

gto

n:

2..

....

......

....

..2

....

....

....

....

..

147

I 15

2

159

161

162

161

161

162

162

187

133

153

153

127

127

128

128

125

129

129

154

154

122

122

123

123

134

124

156

156

160

160

130

135

135

70 86 S3 109

OS 70 100

111 CO 71 QQ

i?7 ?6 74 Qft

00

Q9

91

no ss

9 29

4

3.5

3|

2.33

4.

3A

f\

11.3

54.

11.3

8

9O

fi

1.55

9.44

3A

O

4

**

9i

9 46

4.07

*

nQ

Cl

4.06

4. 1

14

5.04

101 99 71 SS OO as 49 77 74 105 75 90 74 no

108

3.54

9

14

4. 1

1

4ft

l

11.3

611

. 38*

.

Q

97

1.5

5J

3.23

9A

Ai.

4.35

9. 4

6*.

10.2

4

4.08

nO

Q

4.07

A.

11

8?,

57 37 10S

103 17 S7 39 49 101 ?,4 27 S3 57

9.32

3.55

2.36

4.11

11.3

7n

QQ

9.27

£

3.23

4.

4.3

5i

9 47

4.0S

J

11. 3

94.

A

IQi

65 109 89 17 100 60 ?9 4P 50 84 65

9.32

$

4.11

J

3.43

11.3

9

9-28

3.24

9.48

4.40

69 66 58 as as 9« 57

9.33

4.15

2.00

3.26

4.9.

484.

4.09

4

14?, 43 ?,7

79 67

-

9.34

_

3.27

9.49

4.11

01 28 28 34 28 41 34 35 00 36 31 25 33 S4 34 * *

34 35 32 32 31 40 11 34 30 30 34 36 27 OA 26 20 29 30

Do.

Do

.

Do.

in a

sh a

nd d

irty

.

over

tro

ug

h.

Iron h

ot.

'

coke

wou

ld n

ot

ignit

e; b

ott

om

dro

pped

wit

ho

ut

chan

gin

g i

ron.

B

last

on

32 m

inute

s; n

o ir

on m

elte

d.

out.

o P

lus

10 p

er c

ent

pit

ch.

Plu

s 5

per

cen

t p

itch

.

Page 76: WASHING AND COKING TESTS OF COAL AND CUPOLA TESTS OF …

76 WASHING, COKING, AND CUPOLA TESTS.

Chemical effect on iron in cupola tests of coke from coals received from January 1, 1905,to June 30, 1907.

Cupola test No.

1

150 157 164

187 173174 148

47 156 147 155 162 149 163

165 166

143 161 152 145 151 154 146 153

158 171 172 52

159 53

160 167

51 168

49 169 170 50

Designation of coke.

Field No. of coal.

2

Illinois: 29 (w.) ......29 (w.)......29 (w.) ......

Indiana: 5............99............17 (w.)......

Kentucky: 7............8............8............8............9 A (w.)..... 9 A (w.)..... 9 A (w.).....

Ohio: 9............9............

Pennsylvania: 11...........11...........12...........12...........12...........12 (w.)......12 (w.)......19 f\v ~\

Virginia: 2............2(w.).......9 r w ~\IS?.:::::::

West Virginia: 4(w.).......4B (w.)..... 4(w.). ...:..15...........15...........15...........15...........16...........16...........

6 fc -w

1 a>

M83

170 170 170

8 17 17

163

85 164 164 164 167 167 167

72 72

159 159 161 161 161 162 162 162

69 70 70 69

44 44 44 36 36 36 43 45 45 45

Chemical eflect on the iron in melting (per cent) .

Silicon.

§_H

bo 'ft

AW

102

2.12 2.12 2.10

2.10 2.10 2.10 2.12

1.74 2.12 2.12 2.12 2.10 2.12 2.10

2.10 2.10

2.12 2.10 2.12 2.12 2.12 2.12 2.12 2.12

2.12 2.10 2.10 1.89

2.12 1.89 2.12 2.10 1.89 2.10 1.74 2.10 2.10 1.74

a o £ a0>"c

sa

M

103

1.91 1.84 1.68

1.66 1.58 1.71 1.75

1.39 1.82 I'.SO 1.72 1.76 1.83 1.73

1.78 1.74

1.85 1.74 1.86 1.89 1.91 1.81 1.84 1.78

1.77 1.69 1.76 1.55

1.94 1.54 1.90 1.65 1.45 1.71 1.35 1.68 1.67 1.26

i ox . <=« >>oX2£+3

O

A

104

9.90 13.21 20.00

20.96 28.16 18:58 17.47

20.11 14.15 15.12 18.85 16.19 13.68 17.61

15.24 19.06

12.74 17.15 12.28 10.85 9.90

14.62 13.21 16.05

16.52 19.52 17.61 17.77

8.50 18.53 10.38 21.42 23.27 18.57 22.41 20.00 20.47 27.57

Manganese.

a oM

00.'fta i i

105

0.178 .178 .163

.163

.163

.163

.178

.178

.178

.178

.178

.163

.178

.163

.163

.163

.178

.163

.178

.178

.178

.178

.178

.178

.178

.163

.163

.163

.178

.163

.178

.163

.163

.163

.178

.163

.163

.178

a S

"38a i i

106

0.155 .133 .111

.115

.112

.124

.126

.133

.111 .096'

.123

.120

.133

.096

.110

.111

.111

.113

.130

.133

.123

.136

.141

.128

.144

.107

.124 .133

.126

.126

.126

.111

.104

.104

.111

.106

.111

.111

03 0'R °s xo -^+3« o1-1

107

12.93 25.29 31.90

29.44 31.30 23.93 29.20

25.28 37.64 46.06 30.90 26.39 25.29 41.09

34.33 31.89

37.66 30.68 26.97 25.28 30.90 23.59 20.78 28.09

19.09 34.35 23.92 18.42

29.22 22.70 29.21 35.54 36.18 36.19 37:63 34.96 31.90 37.64

Sulphur.

a SM 'ft

ah-t

108

0.059 .059 .098

.098

.098

.098

.059

.051

.059

.059

.059

.098

.059

.098

.098

.098'

.059

.098

.059

.059

.059

.059

.059

.059

.059

.098 .098 .048

.059

.048

.059

.098

.048

.098

.051

.098

.098

.051

o £T3 0> 4J

1aM

109

0.086 .108 .133

.165

.148

.156

.108

.085

.083

.067

.079

.118

.079

.135

.143

.151

.070

.113

.070

.069

.078

.074

.080

.088

.074

.116

.111 .042

.077 -.042

.085

.137

.047

.146

.060

.138

.126

.052

0 COo32 §M

110

0.027 K.049

.035

.067

.050

.058

.049

.034

.024

.008

.020

.020

.020

.037

.045

.053

.011

.015

.011

.010

.019

.016

.021

.029

.015

.018

.013

.018".W

.039"."648"

.009

.040

.028

.001

&0 ft*s

V r-i 3-gg fj w tjO+^~ EH

111

6.59 11.69 6.74

6.13 4.51 7.22 6.88

7.56 19.95 4.65

12.37 7.73 6'.69 8.29

8.16 9.17

4.83 7.57

. 4.92 4.35 5.94

11.13 11.20 15.27

17.10 25.01 12.49

None.

9.41 None. 19.99 9.92

None. 12.79 2.35

16.33 12.94

.26

a oa>M o

si5 J?

112

29 29 29

29 29 29 29

30 30 30 30 30 30 30

31 31

32 32 32 32 32 32 32 32

34 34 34 34

34 34 34 34 34 34 34 34 34 35

O