Martin Peng Oak Ridge National Laboratory, UT-Battelle, LLC For NSTX National Research Team
Scissortail Laboratory, LLC
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Scissortail Laboratory, LLC OMMA Lic. No.: PAAA-N15H-TGDI (405) 788-0247 SAP Resources Received On: 8/12/2019 GAAA-VYAA-TW2Y Reported On: 8/17/2019 BootLegger Flower 852-03 N/A N/A Potency Ref. Method(s): J AOAC 2015 V98-6 Extraction Date: 8/13/2019 ASTM Method D2216-10 Mass Extracted (g): 0.2042 Final Volume (mL): 20 Dry wt. corr. mass (g): 0.1842 Moisture Content (%): 9.8 mg/L Dilution Factor Conc. In Sample - dry (mg/g) Potency % Potency LOQ (%) Analytical Date Analyst CBDV 0 5 0.000 0.00 0.05 8/16/2019 SIF CBDA 1.04 5 0.565 0.06 0.05 8/16/2019 SIF CBGA 16.711 5 9.073 0.91 0.05 8/16/2019 SIF CBG 0 5 0.000 0.00 0.05 8/16/2019 SIF CBD 0 5 0.000 0.00 0.05 8/16/2019 SIF THCV 0 5 0.000 0.00 0.05 8/16/2019 SIF CBN 0 5 0.000 0.00 0.05 8/16/2019 SIF d9-THC 12.986 5 7.050 0.71 0.05 8/16/2019 SIF d8-THC 0 5 0.000 0.00 0.05 8/16/2019 SIF CBC 0 5 0.000 0.00 0.05 8/16/2019 SIF THCA 39.183 50 212.733 21.27 0.54 8/16/2019 SIF Total Cannabanoid: 22.94 % Total THC: 19.36 % Total CBD: 0.05 % Approved By: All associated batch QC passed within acceptable limits. Total THC is calculated as [(THCA x 0.8770) + d9-THC]. Total CBD is calculated as [(CBDA x 0.8770) + CBD]. These samples were run in accordance with current ISO 17025 standards. Lab Director Sample: Matrix: STL Number: Batch Number: Harvest/Process Date: 1 of 6
Transcript of Scissortail Laboratory, LLC
Scissortail Laboratory, LLCOMMA Lic. No.: PAAA-N15H-TGDI (405) 788-0247
SAP Resources Received On: 8/12/2019GAAA-VYAA-TW2Y Reported On: 8/17/2019
BootLegger
Flower
852-03
N/A
N/A
Potency
Ref. Method(s): J AOAC 2015 V98-6 Extraction Date: 8/13/2019ASTM Method D2216-10
Mass Extracted (g): 0.2042 Final Volume (mL): 20Dry wt. corr. mass (g): 0.1842 Moisture Content (%): 9.8
mg/LDilution Factor
Conc. In Sample -
dry (mg/g) Potency %Potency LOQ (%) Analytical Date Analyst
CBDV 0 5 0.000 0.00 0.05 8/16/2019 SIFCBDA 1.04 5 0.565 0.06 0.05 8/16/2019 SIFCBGA 16.711 5 9.073 0.91 0.05 8/16/2019 SIFCBG 0 5 0.000 0.00 0.05 8/16/2019 SIFCBD 0 5 0.000 0.00 0.05 8/16/2019 SIFTHCV 0 5 0.000 0.00 0.05 8/16/2019 SIFCBN 0 5 0.000 0.00 0.05 8/16/2019 SIFd9-THC 12.986 5 7.050 0.71 0.05 8/16/2019 SIFd8-THC 0 5 0.000 0.00 0.05 8/16/2019 SIFCBC 0 5 0.000 0.00 0.05 8/16/2019 SIFTHCA 39.183 50 212.733 21.27 0.54 8/16/2019 SIF
Total Cannabanoid: 22.94 %Total THC: 19.36 %Total CBD: 0.05 %
Approved By:
All associated batch QC passed within acceptable limits.Total THC is calculated as [(THCA x 0.8770) + d9-THC]. Total CBD is calculated as [(CBDA x 0.8770) + CBD].
These samples were run in accordance with current ISO 17025 standards.
Lab Director
Sample:
Matrix:
STL Number:
Batch Number:
Harvest/Process Date:
1 of 6
Scissortail Laboratory, LLCOMMA Lic. No.: PAAA-N15H-TGDI (405) 788-0247
SAP Resources Received On: 8/12/2019GAAA-VYAA-TW2Y Reported On: 8/19/2019
BootLegger
Flower
852-03
N/A
N/A
Terpenes
Ref. Method(s): J AOAC 2015 V98-6 Mass Extracted (g): 0.0203Shimadzu Scientific Whitepaper: GCMS-1604Agilent Technologies App Note: 5991-8499EN
From Instrument
(ug/g)
ug on column (10uL) wt % PQL (%) Analytical Date Analyst
.alpha.-Pinene 7638.19 37.63 0.376 0.00192 8/14/2019 IDCCamphene 157.94 0.78 0.008 0.00192 8/14/2019 IDC.beta.-Myrcene 11794.59 58.10 0.581 0.00192 8/14/2019 IDC.beta.-Pinene 2806.00 13.82 0.138 0.00192 8/14/2019 IDC3-Carene 544.65 2.68 0.027 0.00192 8/14/2019 IDCAlpha Terpinene 394.43 1.94 0.019 0.00192 8/14/2019 IDCD-Limonene 2119.13 10.44 0.104 0.00192 8/14/2019 IDCp-Cymene 0.00 0.00 0.000 0.00192 8/14/2019 IDC.beta.-Ocimene 3930.94 19.36 0.194 0.00192 8/14/2019 IDCEucalyptol 62.54 0.31 0.003 0.00192 8/14/2019 IDC.gamma.-Terpinene 230.01 1.13 0.011 0.00192 8/14/2019 IDCTerpinolene 7031.30 34.64 0.346 0.00192 8/14/2019 IDCLinalool 1168.47 5.76 0.058 0.00192 8/14/2019 IDCIsopulegol 0.00 0.00 0.000 0.00192 8/14/2019 IDCGeraniol 51.74 0.25 0.003 0.00192 8/14/2019 IDCCaryophyllene 1047.15 5.16 0.052 0.00192 8/14/2019 IDCHumulene 273.93 1.35 0.013 0.00192 8/14/2019 IDCNerolidol cis 0.00 0.00 0.000 0.00192 8/14/2019 IDCNerolidol trans 109.74 0.54 0.005 0.00192 8/14/2019 IDCGuaiol 671.30 3.31 0.033 0.00192 8/14/2019 IDCCaryophyllene oxide 0.00 0.00 0.000 0.00192 8/14/2019 IDC.alpha.-Bisabolol 261.36 1.29 0.013 0.00192 8/14/2019 IDC
Percent Terpenes by wt: 1.985
Approved By:All associated batch QC passed within acceptable limits.These samples were run in accordance with current ISO 17025 standards.
Lab Director
Sample:
Matrix:
STL Number:
Batch Number:
Harvest/Process Date:
.beta.-Myrcene .alpha.-Pinene
Terpinolene .beta.-Ocimene
.beta.-Pinene D-Limonene
All Other Terpenes
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Scissortail Laboratory, LLCOMMA Lic. No.: PAAA-N15H-TGDI (405) 788-0247
SAP Resources Received On: 8/12/2019GAAA-VYAA-TW2Y Reported On: 8/22/2019
BootLegger
Flower
852-03
N/A
N/A
PesticidesAnalysis Date: 8/19/2019 Analyzed By: Ref Method: LC/MS/MS and GC/MS*
Pass
Action Level (μg/g)
Conc. In Sample (μg/g) Pass
Action Level (μg/g)
Conc. In Sample (μg/g)
Yes 0.5 ND Yes 0.2 NDYes 0.4 ND Yes 0.4 NDYes 2 ND Yes 0.4 NDYes 0.2 ND Yes 0.2 NDYes 0.4 ND Yes 0.2 NDYes 0.2 ND Yes 0.2 NDYes 0.2 ND Yes 0.4 NDYes 0.2 ND Yes 0.2 NDYes 0.4 ND Yes 0.2 NDYes 0.2 ND Yes 0.2 NDYes 0.2 ND Yes 0.5 NDYes 0.2 ND Yes 1 NDYes 1 ND Yes 0.4 NDYes 0.2 ND Yes 0.2 NDYes 0.2 ND Yes 0.2 NDYes 1 ND Yes 2 NDYes 1 ND Yes 0.2 NDYes 1 ND Yes 0.4 NDYes 0.1 ND Yes 0.2 NDYes 0.2 ND Yes 1 NDYes 0.2 ND Yes 0.2 NDYes 0.2 ND Yes 0.2 NDYes 0.4 ND Yes 0.2 NDYes 0.2 ND Yes 0.2 NDYes 0.2 ND Spirotetramat (203313-25-1) Yes 0.2 ND
Etoxazole (153233-91-1) Spiromesifen (283594-90-1)
Dimethoate (60-51-5) Pyridaben* (96489-71-3)
Ethoprophos* (13194-48-4) Spinosad A (168316-95-8)
Etofenprox (80844-07-1) Spinosad D (168316-95-8)
Daminozide (1596-84-5) Propiconazole (60207-90-1)DDVP (62-73-7) Propoxur* (114-26-1)
Diazinon* (333-41-5) Pyrethrins* (8003-34-7)
Clofentezine (74115-24-5) Phosmet* (732-11-6)
Cyfluthrin* (68359-37-5) Piperonyl butoxide* (51-03-6)
Cypermethrin* (52315-07-8) Prallethrins* (2331-36-9)
Chlorantraniliprole (800008-45-7) Oxamyl (23135-22-0)
Chlorfenapyr* (122453-73-0) Paclobutrazol* (76738-62-0)
Chlorpyrifos* (2921-88-2) Permethrins* (52645-53-1)
Boscalid* (188425-85-6) MGK 264* (113-48-4)
Carbaryl (63-25-2) Myclobutanil (88671-89-0)
Carbofuran (1563-66-2) Naled (300-76-5)
Azoxystrobin (131860-33-8) Methiocarb (2032-65-7)
Bifenazate* (149877-41-8) Methomyl (16752-77-5)
Bifenthrin* (82657-04-3) Methyl parathion* (298-0-0)
Acequinocyl (57960-19-7) Kresoxim-methyl* (143390-89-0)
Acetamiprid (135410-20-7) Malathion (121-75-5)
Aldicarb (116-06-3) Metalaxyl* (57837-19-1)
Compound CompoundAbamectin (71751-41-2) Imazalil (35554-44-0)
Acephate (30560-19-1) Imidacloprid (138261-41-3)
F.A.S.T Labs
Sample:
Matrix:
STL Number:
Batch Number:
Harvest/Process Date:
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Scissortail Laboratory, LLCOMMA Lic. No.: PAAA-N15H-TGDI (405) 788-0247
SAP Resources Received On: 8/12/2019GAAA-VYAA-TW2Y Reported On: 8/22/2019
BootLegger
Flower
852-03
N/A
N/A
MycotoxinsAnalysis Date: 8/19/2019 Analyzed By: Ref Method: Hardy Diagnostics CompactDry
Action Level
(μg/kg) PassAflatoxin B1 20 YesAflatoxin B2 20 YesAflatoxin G1 20 YesAflatoxin G2 20 YesOchratoxin A 20 YesND
Action Level* (μg/kg)
ND
Sample:
Matrix:
STL Number:
Batch Number:
Harvest/Process Date:
Compound
Conc. In Sample (If
Above 1/2 Action Level)
(μg/kg)NDNDND
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Scissortail Laboratory, LLCOMMA Lic. No.: PAAA-N15H-TGDI (405) 788-0247
SAP Resources Received On: 8/12/2019GAAA-VYAA-TW2Y Reported On: 8/22/2019
BootLegger
Flower
852-03
N/A
N/A
Heavy MetalsAnalysis Date: 8/19/2019 Analyzed By: Ref Method: ICP/MS
Action Level* (μg/kg) Pass
Arsenic (As) 400 YesCadmium (Cd) 440 YesLead (Pb) 1000 YesMercury (Hg) 200 Yes
*Action Levels based on levels listed in Title 310 Chapter 681 Medical Marijuana Control Program
F.A.S.T Labs
ND
Sample:
Matrix:
STL Number:
Batch Number:
Harvest/Process Date:
Compound
Conc. In Sample (If Above 1/2 Action
Level)
(μg/kg)NDNDND
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Scissortail Laboratory, LLCOMMA Lic. No.: PAAA-N15H-TGDI (405) 788-0247
SAP Resources Received On: 8/12/2019GAAA-VYAA-TW2Y Reported On: 8/22/2019
BootLegger
Flower
852-03
N/A
N/A
MicrobialAnalysis Date: 8/19/2019 Analyzed By: Ref Method: Hardy Diagnostics CompactDry
Action Level* (μg/kg) Pass
1 Yes1 Yes1 Yes
104 Yes104 Yes
1 Yes
*Action Levels based on levels listed in Title 310 Chapter 681 Medical Marijuana Control Program
Salmonella spp. ND
Escherichia Coli (E. Coli) NDMold NDYeast ND
Compound
Conc. In Sample (If
Above 1/2 Action Level)
(CFU/g)Aerobic Plate Count, Total NDColiforms, Total ND
F.A.S.T Labs
Sample:
Matrix:
STL Number:
Batch Number:
Harvest/Process Date:
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