PerformancePLUS Long-Life DeUteriUm Detector LamPSThe only guaranteed, long-lasting, high energy...

4
P erformance PLUS LONG-LIFE DEUTERIUM DETECTOR LAMPS The only guaranteed, long-lasting, high energy lamp designed specifically for Waters 2487 and 996/2996 Detectors Waters PerformancePLUS™ long-life deuterium detector lamps were co-developed by Waters Corporation and Hamamatsu Photonics, K.K. They are exclusively available from Waters and cannot be sourced elsewhere. While it is possible to purchase non-Waters lamps for your Waters detector, there are significant differences in quality and design that can impact detector performance. A PerformancePLUS lamp from Waters represents the modifications and testing that each lamp goes through once it is received from Hamamatsu. UNIQUELY DESIGNED FOR YOUR WATERS DETECTOR Choosing the right lamp for your Waters detector can make a significant difference in overall system performance. Waters PerformancePLUS Long-Life Deuterium Detector Lamps are specifically designed for use with Waters detectors to ensure long-life, cost-effective performance. Waters lamps offer many proprietary features not found in alternative lamps. Exclusive capacitor box design for reliable starting Waters lamp capacitors are built into the cable so it stays cool and does not degrade over time. This construction ensures reliable ignition of the deuterium arc lamp for superior lifetime performance. See Figure 1. Independently certified as part of the detector for safety Waters 2487 Dual-Wavelength Absorbance Detectors and Waters 996/2996 Photodiode Array (PDA) Detectors are certified for Canadian, European, and U.S. safety requirements with the Waters PerformancePLUS Long-Life Deuterium Detector Lamp included as part of the detector design. Certification requires user-accessible wires that experience high voltage to be double insulated. Use of alternative lamps without certification may compromise product safety. See Figure 2. Uniquely designed for your Waters detector: n Exclusive capacitor box for reliable starting n Certified for electronic safety n Precision alignment for maximum performance n Consistent cathode coating for improved stability n Precision machined for optimum interface with Waters detectors n Inorganic ceramic bonding cement for minimal degradation of lamp intensity n Rigorous reliability testing for reliable performance n Guaranteed minimum lifetime for cost savings n Ensured warranty coverage for peace of mind Figure 1. Capacitor Box. Waters’ unique lamp capacitor box design enables reliable ignition. Figure 2. Lamp Connector Comparison. The Waters lamp connector (lower cable) complies with electrical safety codes. Exposed wires in the alternative lamp connector (upper cable) can present a potential electrical shock hazard to users. Ensured warranty coverage for peace of mind Waters lamps are the only lamps approved for Waters warranty replacement. Damage to a Waters system resulting from use of alternative lamps is not covered under the Waters product warranty.

Transcript of PerformancePLUS Long-Life DeUteriUm Detector LamPSThe only guaranteed, long-lasting, high energy...

Page 1: PerformancePLUS Long-Life DeUteriUm Detector LamPSThe only guaranteed, long-lasting, high energy lamp designed specifically for Waters 2487 and 996/2996 Detectors Waters PerformancePLUS™

P e r fo rm an c e P LUS Lo ng - L i f e D eU t e r iUm D e t ec t o r L am P S

The only guaranteed, long-lasting, high energy lamp designed specifically for Waters 2487 and 996/2996 Detectors

Waters PerformancePLUS™ long-life deuterium detector lamps were co-developed by

Waters Corporation and Hamamatsu Photonics, K.K. They are exclusively available from

Waters and cannot be sourced elsewhere. While it is possible to purchase non-Waters

lamps for your Waters detector, there are significant differences in quality and design

that can impact detector performance. A PerformancePLUS lamp from Waters represents the

modifications and testing that each lamp goes through once it is received from Hamamatsu.

UniqUeLy DeSigneD for yoUr WAT erS DeT eCTorChoosing the right lamp for your Waters detector can make a significant difference in overall

system performance. Waters PerformancePLUS Long-Life Deuterium Detector Lamps are

specifically designed for use with Waters detectors to ensure long-life, cost-effective performance.

Waters lamps offer many proprietary features not found in alternative lamps.

exclusive capacitor box design for reliable startingWaters lamp capacitors are built into the cable

so it stays cool and does not degrade over time.

This construction ensures reliable ignition of the

deuterium arc lamp for superior lifetime performance.

See Figure 1.

independently certified as part of the detector for safetyWaters 2487 Dual-Wavelength Absorbance

Detectors and Waters 996/2996 Photodiode

Array (PDA) Detectors are certified for Canadian,

European, and U.S. safety requirements with the

Waters PerformancePLUS Long-Life Deuterium

Detector Lamp included as part of the detector

design. Certification requires user-accessible wires

that experience high voltage to be double insulated.

Use of alternative lamps without certification may

compromise product safety. See Figure 2.

Uniquely designed for your Waters detector:

n exclusive capacitor box for

reliable starting

n Certified for electronic safety

n Precision alignment for

maximum performance

n Consistent cathode coating

for improved stability

n Precision machined for

optimum interface with

Waters detectors

n inorganic ceramic bonding

cement for minimal

degradation of lamp intensity

n rigorous reliability testing

for reliable performance

n guaranteed minimum lifetime

for cost savings

n ensured warranty coverage for

peace of mind

Figure 1. Capacitor Box. Waters’ unique lamp capacitor box design enables reliable ignition.

Figure 2. Lamp Connector Comparison. The Waters lamp connector (lower cable) complies with electrical safety codes. Exposed wires in the alternative lamp connector (upper cable) can present a potential electrical shock hazard to users.

ensured warranty coverage for peace of mindWaters lamps are the only lamps approved for Waters warranty replacement. Damage to a Waters

system resulting from use of alternative lamps is not covered under the Waters product warranty.

Page 2: PerformancePLUS Long-Life DeUteriUm Detector LamPSThe only guaranteed, long-lasting, high energy lamp designed specifically for Waters 2487 and 996/2996 Detectors Waters PerformancePLUS™

P reCiSion DeSign for SUPerior PerformAnC e

Waters’ lamp design continues to evolve and currently includes

these differentiating features:

n Precision alignment and tolerances applied to arc point

within the lamp housing, based on optical analysis of the

detector, to provide maximum performance. No other lamp

manufacturer has knowledge of Waters proprietary optical

design characteristics.

n Directly heated cathode for greater stability in single beam

instruments (996/2996 PDA Detector lamps).

n Consistent cathode coating for improved stability.

n Precision-machined base and proprietary design to interface

with Waters detector lamp housing for optimum performance.

n Inorganic ceramic bonding cement to minimize degradation

of lamp intensity. Alternative lamps often use epoxy adhesives

that can damage optics, resulting in very costly repairs.

See Figure 3.

Over time, the heat generated from a lamp can cause inferior bond-

ing materials to outgas, leaving a coating of contaminants on the

lamp housing window and optics bench mirror. These contaminants

can lead to premature failure of the mirrors and other optical

components due to corrosion from these contaminants interacting

with moisture and chemical vapors in the environment. See Figures

4 and 5.

Figure 4a. Undamaged Lamp Housing Mirror.

Figure 4b. Damaged Lamp Housing Mirror. Note the corrosion which can reduce reflectance and affect sensitivity.

Figure 5b. Damaged Optics Bench Mirror. Note the dull spot which reduces reflectivity.

Figure 5a. Undamaged Optics Bench Mirror.

Figure 3. Alternative Lamp. Epoxy adhesive tends to degrade over time. Note the brown discoloration.

Page 3: PerformancePLUS Long-Life DeUteriUm Detector LamPSThe only guaranteed, long-lasting, high energy lamp designed specifically for Waters 2487 and 996/2996 Detectors Waters PerformancePLUS™

rigoroUS T eST ing for reLiAbLe PerformAnC eWaters conducts extensive testing to better understand lamps

and lamp life. Waters selects a specific lamp design and then

initiates Lamp Robustness Testing, which includes life, shock,

internal lamp structure, ignition reliability, and radiant intensity

distribution testing.

Lamps also go through additional assembly and Quality Assurance

(QA) tests, including lamp alignment, intensity, and signal-to-

noise. This testing ensures an overall field failure rate of <0.1%

and an unmatchable fit for Waters instruments.

Lamp robustness TestingWaters dedicates extensive reliability resources to perform lamp

lifetime studies. In partnership with our lamp manufacturer, all

possible scenarios that can happen in your lab are tested to provide

you with optimum performance you need to succeed. Waters

development and testing has led to lamp advancements that

improve robustness and life. Degradation from shock and vibration

has been reduced due to lamp improvements. Figures 6 and 7 illus-

trate the longer lifetime, increased light intensity, and decreased

noise resulting from Waters lamps cathode improvements.

Long L ife for CoST-effeCT iv e PerformAnC eWaters PerformancePLUS Long-Life Deuterium

Detector Lamps have a guaranteed minimum life-

time of 2000 hours; however, data shows that these

lamps can perform up to 3000 hours.

Lamps can suffer damage when started or running.

Waters lamp design ensures that multiple lamp

strikes will not harm the lamp. As a result, you

can turn off a Waters lamp when not acquiring

data, significantly reducing the cost per sample

analyzed. Figure 8 illustrates the high sensitivity

that can be achieved with a Waters lamp.

Figure 6. Signal Degradation. Waters lamps provide 2000 hours of warranty life; however, data shows that these lamps can provide up to 3000 hours of lamp life.

Waters Lamps Energy Remaining (%) Over Time @ 254nm

5060708090

100

0 1000 2000 3000 4000

Time (Hours)

% Energy Remaining

% E

nerg

y R

em

ain

ing

WATerS LAmPS: energy remaining (%) over Time @ 254 nm

Figure 7. Average Peak-to-Peak Noise. Low noise tends to decrease slightly as lamp energy decreases. We know of no alternative lamps that perform better than Waters lamps.

0.0

1.0

2.0

3.0

4.0

5.0

6.0

7.0

8.0

0 1000 2000 3000

2487 Lamp HoursAverage Noise 2487 Noise Spec

Ave

rage

Pea

k-to

-Pea

k N

oise

(µAU

)

Waters Lamps Average Peak-to-Peak Noise

WATerS LAmPS: Average Peak-to-Peak noise

Figure 8. Sensitivity. The high sensitivity of the Waters 2996 Photodiode Array Detector with a PerformancePLUS Deuterium Lamp enables the detection of an API’s related compounds to levels as low as 0.006% (Paroxetine @ 1.0AU Full Scale).

Peak Retention Time(min)

% Area Signal-to-Noise

Impurity 1 1.80 0.011 5

Impurity 2 2.19 0.006 3

Impurity 3 2.69 0.013 7

Impurity 4 12.45 0.072 32

Paroxetine 13.27 99.751 32540

Impurity 5 15.39 0.027 12

Impurity 6 17.63 0.010 3

Impurity 7 17.91 0.009 5

Impurity 8 21.71 0.071 26

Impurity 9 22.36 0.017 5

Impurity 10 24.58 0.012 4

WATerS LAmPS: optimized for High Sensitivity

Page 4: PerformancePLUS Long-Life DeUteriUm Detector LamPSThe only guaranteed, long-lasting, high energy lamp designed specifically for Waters 2487 and 996/2996 Detectors Waters PerformancePLUS™

Waters Corporation 34 Maple Street Milford, MA 01757 U.S.A. T: 1 508 478 2000 F: 1 508 872 1990 www.waters.com

Waters and Waters Quality Parts are registered trademarks of Waters Corporation. PerformancePLUS and The Science of What’s Possible are trademarks of Waters Corporation. All other trademarks are the property of their respective owners.

©2009 Waters Corporation. Produced in the U.S.A.October 2009 720003118EN LB-PDF

exPerienCeD, WorLDWiDe ServiCe – iT’S more THAn jUST rePLACing A LAmPDuring Performance Maintenance visits, your Waters Field Service Engineer replaces

PerformancePLUS Long-Life Deuterium Detector Lamps as needed. Additionally, the

engineerverifies and maintains your Waters detector for optimal performance.

order nowTo order a Waters PerformancePLUS Long-Life Deuterium Detector Lamp,

go to www.waters.com/wqp.

be ASSUreD

CHooSe WATerS gLobAL ServiCeS

Waters global Services focuses

on optimizing Waters products

with superior service, support,

upgrades, training, and

Waters quality Parts.

Proven SATiSfACTion

for the eighth consecutive year,

an independent quality auditing

firm ranked Waters global

Services best-in-class in

providing expert technical

knowledge, quick resolution

of system issues, and

process support1.

for more information, go to

www.waters.com/custsat.

1 Achievement in Customer Excellence Award, CustomerSat, Inc., 2007-2008; NorthFace ScoreBoard Award sm, Omega Management Group Corporation, 2000-2006.

for Trouble-free System operation, Use only Waters quality PartsWaters designs and manufactures Waters Quality Parts® to the same strict regulatory

standards as your high-performance Waters systems to ensure:

n Continued system compliance

n Maximum lifetime and reliability of both the spare part and your instrument

n Contamination free environment

n Accurate and reproducible results

For more information or to order parts, go to www.waters.com/wqp.

Waters Detector Lamp Kit Part Number

2487 Dual-Wavelength Absorbance Detector WAS081142

996/2996 PDA Detector WAT052586