MIT 2 SUMMARY NIST2000 LAO-NNO STO-STCO NOV DEC 2014 1-30-15

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Transcript of MIT 2 SUMMARY NIST2000 LAO-NNO STO-STCO NOV DEC 2014 1-30-15

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Table of Contents: Slide #

1. The Bragg XRD Microscope ……………… 32. Specifications ……………………… 43. SDD & Resolution Chart…………………….. 54. Principle of Operation……………………….. 65. Experimental Set-up Bruker D8…………. 76. Incident Beam ……………………….. 97. NIST2000SRM XRR + LEPTOS….………….. 118. NIST2000SRM (004) SYMMETRIC RC…… 16

i. OMEGA-2THETA SCAN…………… 18ii. PHI SCAN …………… 60 iii. CHI SCAN …………… 63

9. NIST2000SRM (224) ASYMMETRIC RC… 70 10.LAO-NNO RC ………………………. 7811.STO-STCO RC ……………………….. 9712. Comparing data ……………………….. 116

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Incident Beam

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Incident Beam

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(004) Diffracted Beam

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(004) Diffracted Beam

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Om-2Th Phi Chi

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30.884 Arc Sec

117.3592 Arc Sec

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NDE XRD Section Topographs from Individual Coherently Reflecting Domains in Depth

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Sto Pitc 1

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