Initial Site Characterization Albro Estate 102 Prouty Hill ...

42
TYPE OF SUBMITTAL PETROLEUM REIMBURSEMENT FUND PHASE Workscope/Budget Technical Report X Reimbursement Request Monitoring Result (Pre-permit) Monitoring Result (Post-permit) Initial Response Action Free product Removal Initial Site Characterization X Supplemental Site Investigation Remedial Action Plan Remedial Design Plan Remedial Implementation/O+M Groundwater Management Permit Initial Site Characterization Albro Estate 102 Prouty Hill Road Sunderland, VT Prepared For: Patricia Ludwig Executor, George W Albro 3 rd Estate 1416 Sunderland Hill Road Arlington, VT 05250 Phone: (802) 375-6965 Prepared By: Harper Environmental Associates, Inc. 1811 Hale Hollow Road, Bridgewater Corners, VT 05035 (802) 672-6112 fax (802) 672-6227 Cliff Harper, Principal April 1, 2009

Transcript of Initial Site Characterization Albro Estate 102 Prouty Hill ...

TYPE OF SUBMITTAL PETROLEUM REIMBURSEMENT FUND PHASE

Workscope/Budget Technical Report X Reimbursement Request Monitoring Result (Pre-permit) Monitoring Result (Post-permit)

Initial Response Action Free product Removal Initial Site Characterization X Supplemental Site Investigation Remedial Action Plan Remedial Design Plan Remedial Implementation/O+M Groundwater Management Permit

Initial Site Characterization

Albro Estate 102 Prouty Hill Road

Sunderland, VT

Prepared For: Patricia Ludwig

Executor, George W Albro 3rd Estate 1416 Sunderland Hill Road

Arlington, VT 05250 Phone: (802) 375-6965

Prepared By: Harper Environmental Associates, Inc.

1811 Hale Hollow Road, Bridgewater Corners, VT 05035 (802) 672-6112 fax (802) 672-6227 Cliff Harper, Principal

April 1, 2009

April 1, 2009 Mr. Chuck Schwer, Section Chief Sites Management Section, VTDEC Waste Management Division 103 S. Main St./West Building Waterbury, Vermont 05671-0404 SUBJECT: Results of the Subsurface Investigation at the Albro Estate Residential Property, 102 Prouty Hill Road, Sunderland, VT. (Expressway Form Submitted) Dear Mr. Schwer, An intrusive field investigation was completed at the Albro Residence in Sunderland Vermont on March 17, 2009. Harper Environmental Associates, Inc. (HEA) is pleased to submit a summary of our field procedures, and the results from the groundwater & soil sampling event due to a release of fuel oil from a leaking underground storage tank (LUST). This report is subject to the limitations found in the Appendices. Site BackgroundAlan Hess of Able Realty, Arlington, VT, contracted Harper Environmental Associates (HEA) to oversee the removal of one 1,000-gallon UST from the above referenced site. Jason Homes of Home Property Maintenance completed all the excavation work and all environmental field activities were conducted by HEA on March 12, 2009. During the UST closure, by removal, petroleum hydrocarbon contamination was discovered in soils below the base of the UST. The tank was found to be in poor condition with multiple, corrosion holes along the bottom and welded end seams of the tank. Onsite soil screening for volatile organic compounds (VOCs) using a Photoionization Detector (PID) indicated soil readings as high a 185 parts per million (ppm) at approximately 6 feet below grade along the center line of the UST. Free product was not encountered in the excavation. The excavation was extended to a depth of approximately 9 feet below grade and no groundwater was encountered. Bedrock was not encountered during the excavation. The full extent of the contamination was not identified at the time of removal. The site was surveyed for sensitive receptors. Potential receptors included indoor air, soil, groundwater, nearby drinking water well and Peters Brook approximately 150 feet north of the UST. During the UST closure, contaminated soil was encountered below the bottom of the UST. Contaminated soil was excavated from the pit and placed on a dump truck. Excavated soils from below the UST cradle were visually impacted by fuel oil and exhibited a strong fuel oil odor, with PID readings greater than 100 ppm at nine feet below grade. Approximately 1.5 yards of contaminated soil was removed from the excavation.

2

An Expressway Investigation form was sent to VTDEC dated March 16, 2009, which indicated the need for further investigation at the site based on the contamination observed during the UST removal activities. Six-Geoprobe borings were completed at the site on March 17, 2009. All extracted soil samples were screened on site using a PID. Groundwater was encountered during the advancement of one of the borings and damp/saturated soils were encountered during the advancement of two other borings. Three one-inch diameter-monitoring wells were installed into the deeper soil borings to a depth of 8.1-10 feet below grade. No groundwater samples were collected on the day of drilling for laboratory analysis. Soil samples were collected from GP-1 and SB-3 during the installation of the soil borings. The locations of the monitoring wells and soil borings can be seen on the Figure 2: Site Map. General Site Description The Albro Estate is located at 102 Prouty Hill Road, Sunderland, VT (Figure 1: Site Location Map). One residential building and one two bay garage building are located on site. The former UST was positioned between the residential building and the septic tank as indicated in Figure 2: Site Map The properties surrounding the site are residential properties, and Prouty Hill Road is a quiet residential dead end street. Overhead electrical lines service the residential building. The property uses a private drinking water well and septic system. The drinking water well is located approximately 25 feet west of the residential building. The septic system is located between the former UST and Peters Brook. For more accurate locations see Figure 2, Site Map. Preliminary Activities Prior to field activities, HEA prepared a site-specific Health and Safety Plan in accordance with OSHA 29 Code of Federal Regulations 1910 and 1929. During the investigation, the plan was kept on-site and signed by all field staff. HEA walked the site prior to field activities and located the potential sampling locations. All subsurface utilities were marked-out prior to drilling through Vermont’s dig-safe services and the owner. Geoprobe Soil Boring/Monitoring Well Installation On March 17, 2009, HEA supervised the completion of six soil borings and three monitoring well installations at the site. The location of each of the soil borings and monitoring wells are depicted on Figure 2, Site Map. All borings (GP-1, 2, and 3, and SB-1, 2, and 3) were completed into the field around the site of the former UST. Drill logs were completed for each of the borings and can be found attached to this report. T+K drilling of Troy, NH installed the borings. A truck mounted Geoprobe drill rig was used for this project due to the position of the former tank cradle and the desired soil boring locations close to the septic tank and leach field.

Harper Environmental Associates April 1, 2009 Albro Estate, Sunderland, VT

3

The monitoring wells were located in the following three positions: • GP-1, located approximately 5 feet west of the former UST cradle. • GP-2, located approximately 30 northwest of the former UST cradle. • GP-3, located into the tank cradle between the center and the easterly end of the

former UST. The soil borings were located in the following three positions:

• SB-1, located between GP-1 and GP-2, approximately 8-10 feet south of GP-2. • SB-2, located between GP-1 and GP-2, approximately 10 feet north west of GP-1 • SB-3, located approximately 30 feet northeast of GP-3, on the easterly side of the

chain link fence. During boring installation, continuous soil samples were collected using a 3-foot plastic lined sampler. All down hole drilling equipment was cleaned with water between holes. The soil samples were brought to the surface and visually classified by an engineer/geologist. All soil samples were screened in the field for volatile organic compounds (VOC) using a Mini Rae 2000 photoionization detector (PID). Field soil samples were collected in a sealed plastic bag or glass jars. The tip of the PID was inserted into the bag or jar to measure VOC content. Soils consisted of silty loam above sandy silts with pebbles, clay silts were detected between 3 and 6 feet below grade in GP-1 and GP-2. The site is located on a slope topographically gently sloping north towards Peters Brook. Refusal was encountered during the installation of the all six soil borings. The deepest boring extended to 10 feet below grade and the shallowest was installed to 5 feet below grade. Groundwater was detected in two of the three monitoring wells between 7.51 and 8.95 feet below grade. From visual interpretation of surface elevations, groundwater gradient would be expected to move in a northerly direction towards Peters Brook. Only two of the three monitoring wells contained water, consequently no groundwater gradient map could be generated. The two wells that contained groundwater, GP-2 and GP-3, had groundwater elevation of 89.95 and 89.9 feet respectively. One-inch PVC well screen + blank were installed into the three deepest boreholes. Sand was filled around the wells to an elevation above the top of the screen. Bentonte was used to seal a two-foot section of the borehole above the sand fill. Native fill was used to backfill the remainder of the well boring. A flush mounted road box was installed around each of the monitoring wells. Potential Receptors Identification of the potential receptors in proximity to the site was determined during this investigation. A relative degree of risk, from the contamination identified during this study, was assigned to each receptor. The potential receptors include groundwater, soil, surface water, indoor air, drinking water and subsurface utilities.

Harper Environmental Associates April 1, 2009 Albro Estate, Sunderland, VT

4

Soil Soil screening data from the March, 2009 UST removal event indicated the presence of VOC’s in the soils beneath the former UST. The UST excavation extended to a depth of 9 feet below grade where PID readings were recorded greater than 100 ppm. Soils were screened using the PID during the installation of the soil borings on March 17, 2009. No PID readings were detected in any of the soil borings. Soil impacted by fuel oil-type hydrocarbons was not found in GP 1, 2, 3 or SB-1, 2, and 3. No visual indication of hydrocarbon impacts of soil was noted in any of the soil borings. Based on visual observation and PID measurements, the impacted soil zone appears to be concentrated proximate to the former LUST cradle and the bulk of the contaminated soils appear to have been removed during the soil excavation activities. Approximately 1.5 yards of soil was removed loaded directly onto a dump truck, for transportation to a treatment facility. High levels of petroleum-type hydrocarbon impact to soil represent a potential threat to human and environmental receptors including nearby buildings, children playing in the vicinity, and utility corridors. The routes of exposure would include direct contact during excavation, vapors emanating from uncovered soil and vapors entering utility corridors and basements. Since soil contamination was encountered well below the ground surface, exposure to humans through direct contact with soil is minimized. There is a potential risk of exposure to workers who may excavate the soil and have direct contact with the soil or breath vapors emanating from uncovered soil. Soil Analytical Results Two soil samples were collected during the completion of the soil borings and sent for laboratory analysis. One soil sample from GP-1, collected from 7 feet below grade, was analyzed for volatile organic compounds (VOC’s) and total petroleum hydrocarbons (TPH’s). The second soil sample was collected from SB-3, at 6 feet below grade, was analyzed for TPH only. No soil sample contained petroleum hydrocarbon contamination above the respective detection limits. Groundwater Groundwater was observed in two of the three monitoring wells during the groundwater sampling event. No groundwater was detected during the UST closure activities. A groundwater gradient map was not produced due to only two depth to water readings being available. Topographic slope and the position of Peters Brook suggests that groundwater would likely from in a northerly direction. Groundwater samples were collected from the two monitoring wells that contained water (GP-2 and GP-3) on March 20, 2009. The groundwater samples were analyzed for volatile organic compounds (VOC’s) using EPA Method 8021/8260. Not enough water could be collected for TPH analysis. No level of groundwater contamination was detected in any of the groundwater samples, consequently exposure from groundwater is minimal.

Harper Environmental Associates April 1, 2009 Albro Estate, Sunderland, VT

6

Attachments: Figure 1: Site Location Map Figure 2: Site Map Appendix: Well Logs Photos

Phoenix Environmental Laboratory Report Expressway Notification Form Limitations

Harper Environmental Associates April 1, 2009 Albro Estate, Sunderland, VT

Sample Information Custody Information

Matrix:Location Code:

Rush Request:

P.O.#:

Collected by:Received by:

Analyzed by:

DRINKING WATER

HARPER

03/12/09

LDF

see "By" below

AW

Laboratory DataClient ID: SUNDERLAND LUST TAP

Phoenix I.D.: AR45698

03/17/09

0:00

10:30

Parameter Result RL Units Date By Reference

FOR: Attn: Mr. Cliff HarperHarper Environmental Associates1811 Hale Hollow RdBridgewater Corners, VT 05035

Analysis ReportMarch 20, 2009

Time

Date Time

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06040 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG I.D.: GAR45698

Volatiles (524.2)ND1,1,1,2-Tetrachloroethane 0.50 03/17/09 HM 524.2ug/LND1,1,1-Trichloroethane 0.50 03/17/09 HM 524.2ug/LND1,1,2,2-Tetrachloroethane 0.50 03/17/09 HM 524.2ug/LND1,1,2-Trichloroethane 0.50 03/17/09 HM 524.2ug/LND1,1-Dichloroethane 0.50 03/17/09 HM 524.2ug/LND1,1-Dichloroethene 0.50 03/17/09 HM 524.2ug/LND1,1-Dichloropropene 0.50 03/17/09 HM 524.2ug/LND1,2,3-Trichlorobenzene 0.50 03/17/09 HM 524.2ug/LND1,2,3-Trichloropropane 0.50 03/17/09 HM 524.2ug/LND1,2,4-Trichlorobenzene 0.50 03/17/09 HM 524.2ug/LND1,2,4-Trimethylbenzene 0.50 03/17/09 HM 524.2ug/LND1,2-Dibromo-3-chloropropane 0.50 03/17/09 HM 524.2ug/LND1,2-Dichlorobenzene 0.50 03/17/09 HM 524.2ug/LND1,2-Dichloroethane 0.50 03/17/09 HM 524.2ug/LND1,2-Dichloropropane 0.50 03/17/09 HM 524.2ug/LND1,3,5-Trimethylbenzene 0.50 03/17/09 HM 524.2ug/LND1,3-Dichlorobenzene 0.50 03/17/09 HM 524.2ug/LND1,3-Dichloropropane 0.50 03/17/09 HM 524.2ug/LND1,4-Dichlorobenzene 0.50 03/17/09 HM 524.2ug/LND2,2-Dichloropropane 0.50 03/17/09 HM 524.2ug/LND2-Chlorotoluene 0.50 03/17/09 HM 524.2ug/LND4-Chlorotoluene 0.50 03/17/09 HM 524.2ug/LNDBenzene 0.50 03/17/09 HM 524.2ug/LNDBromobenzene 0.50 03/17/09 HM 524.2ug/LNDBromochloromethane 0.50 03/17/09 HM 524.2ug/LNDBromodichloromethane 0.50 03/17/09 HM 524.2ug/LNDBromoform 0.50 03/17/09 HM 524.2ug/LNDBromomethane 0.50 03/17/09 HM 524.2ug/L

Page 1 of 2

SUNDERLAND LUST TAP Phoenix I.D.: AR45698

Parameter Result RL Units Date By ReferenceTimeClient ID:

NDCarbon tetrachloride 0.50 03/17/09 HM 524.2ug/LNDChlorobenzene 0.50 03/17/09 HM 524.2ug/LNDChloroethane 0.50 03/17/09 HM 524.2ug/LNDChloroform 0.50 03/17/09 HM 524.2ug/LNDChloromethane 0.50 03/17/09 HM 524.2ug/LNDcis-1,2-Dichloroethene 0.50 03/17/09 HM 524.2ug/LNDcis-1,3-Dichloropropene 0.50 03/17/09 HM 524.2ug/LNDDibromochloromethane 0.50 03/17/09 HM 524.2ug/LNDDibromoethane 0.50 03/17/09 HM 524.2ug/LNDDibromomethane 0.50 03/17/09 HM 524.2ug/LNDDichlorodifluoromethane 0.50 03/17/09 HM 524.2ug/LNDEthylbenzene 0.50 03/17/09 HM 524.2ug/LNDHexachlorobutadiene 0.50 03/17/09 HM 524.2ug/LNDIsopropylbenzene 0.50 03/17/09 HM 524.2ug/LNDm&p-Xylene 1.0 03/17/09 HM 524.2ug/LNDMethyl Ethyl Ketone 5.0 03/17/09 HM 524.2ug/LNDMethyl t-butyl ether (MTBE) 1.0 03/17/09 HM 524.2ug/LNDMethylene chloride 0.50 03/17/09 HM 524.2ug/LNDNaphthalene 0.50 03/17/09 HM 524.2ug/LNDn-Butylbenzene 0.50 03/17/09 HM 524.2ug/LNDn-Propylbenzene 0.50 03/17/09 HM 524.2ug/LNDo-Xylene 0.50 03/17/09 HM 524.2ug/LNDp-Isopropyltoluene 0.50 03/17/09 HM 524.2ug/LNDsec-Butylbenzene 0.50 03/17/09 HM 524.2ug/LNDStyrene 0.50 03/17/09 HM 524.2ug/LNDtert-Butylbenzene 0.50 03/17/09 HM 524.2ug/LNDTetrachloroethene 0.50 03/17/09 HM 524.2ug/LNDToluene 0.50 03/17/09 HM 524.2ug/LNDTotal Trihalomethanes 0.50 03/17/09 HM 524.2ug/LNDTotal Xylenes 1.0 03/17/09 HM 524.2ug/LNDtrans-1,2-Dichloroethene 0.50 03/17/09 HM 524.2ug/LNDtrans-1,3-Dichloropropene 0.50 03/17/09 HM 524.2ug/LNDTrichloroethene 0.50 03/17/09 HM 524.2ug/LNDTrichlorofluoromethane 0.50 03/17/09 HM 524.2ug/LNDVinyl chloride 0.50 03/17/09 HM 524.2ug/L

QA/QC Surrogates114% 1,2-dichlorobenzene-d4 03/17/09 HM 524.2%

82% Bromofluorobenzene 03/17/09 HM 524.2%

102% Dibromofluoromethane 03/17/09 HM 524.2%

95% Toluene-d8 03/17/09 HM 524.2%

Comments:

ND=Not detected BDL=Below Detection Level RL=Reporting Level

Phyllis Shiller, Laboratory Director

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.

March 20, 2009

Page 2 of 2

QA/QC Data

Parameter BlankMS

Rec %MS DupRec % RPD

QA/QC ReportMarch 20, 2009

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06040 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG I.D.: GAR45698

LCS%

LCSD%

LCSRPD

QA/QC Batch 123101, QC Sample No: AR45818 (AR45698)

Volatiles100 981,1,1,2-Tetrachloroethane ND 2.0100 98 2.0

97 981,1,1-Trichloroethane ND 1.093 98 5.2

97 931,1,2,2-Tetrachloroethane ND 4.2101 94 7.2

101 961,1,2-Trichloroethane ND 5.1103 99 4.0

93 921,1-Dichloroethane ND 1.192 92 0.0

94 921,1-Dichloroethene ND 2.285 91 6.8

93 931,1-Dichloropropene ND 0.089 92 3.3

105 881,2,3-Trichlorobenzene ND 17.6114 82 32.7

108 1001,2,3-Trichloropropane ND 7.7117 117 0.0

101 961,2,4-Trichlorobenzene ND 5.1112 85 27.4

101 1051,2,4-Trimethylbenzene ND 3.9104 100 3.9

92 841,2-Dibromo-3-chloropropane ND 9.1108 79 31.0

97 961,2-Dichlorobenzene ND 1.0102 97 5.0

100 961,2-Dichloroethane ND 4.1102 100 2.0

98 961,2-Dichloropropane ND 2.1100 94 6.2

99 1031,3,5-Trimethylbenzene ND 4.0101 99 2.0

98 981,3-Dichlorobenzene ND 0.0101 97 4.0

103 991,3-Dichloropropane ND 4.0106 100 5.8

92 921,4-Dichlorobenzene ND 0.095 90 5.4

78 822,2-Dichloropropane ND 5.088 71 21.4

99 1002-Chlorotoluene ND 1.098 96 2.1

94 882-Hexanone ND 6.698 84 15.4

99 1012-Isopropyltoluene ND 2.098 99 1.0

99 1024-Chlorotoluene ND 3.0103 100 3.0

103 984-Methyl-2-pentanone ND 5.0108 103 4.7

110 96Acetone ND 13.6105 116 10.0

96 87Acrolein ND 9.896 94 2.1

100 92Acrylonitrile ND 8.3101 100 1.0

94 96Benzene ND 2.195 94 1.1

99 96Bromobenzene ND 3.1101 96 5.1

97 94Bromochloromethane ND 3.197 97 0.0

101 97Bromodichloromethane ND 4.0107 104 2.8

108 100Bromoform ND 7.7112 105 6.5

95 94Bromomethane ND 1.188 81 8.3

89 88Carbon Disulfide ND 1.183 80 3.7

99 97Carbon tetrachloride ND 2.092 99 7.3

97 96Chlorobenzene ND 1.097 94 3.1

89 89Chloroethane ND 0.086 82 4.8

Page 1 of 2

QA/QC Data

Parameter BlankMS

Rec %MS Dup Rec % RPD

SDG I.D.: GAR45698

LCS%

LCSD%

LCSRPD

95 94Chloroform ND 1.194 95 1.1

89 90Chloromethane ND 1.190 88 2.2

95 94cis-1,2-Dichloroethene ND 1.192 95 3.2

103 99cis-1,3-Dichloropropene ND 4.0108 93 14.9

103 99Dibromochloromethane ND 4.0107 99 7.8

107 101Dibromoethane ND 5.8111 105 5.6

102 95Dibromomethane ND 7.1103 99 4.0

91 85Dichlorodifluoromethane ND 6.8101 100 1.0

98 100Ethylbenzene ND 2.098 96 2.1

88 89Hexachlorobutadiene ND 1.190 84 6.9

98 101Isopropylbenzene ND 3.094 93 1.1

100 101m&p-Xylene ND 1.0100 98 2.0

94 88Methyl ethyl ketone ND 6.691 101 10.4

98 93Methyl t-butyl ether (MTBE) ND 5.298 93 5.2

95 91Methylene chloride ND 4.393 93 0.0

98 135Naphthalene ND 31.8110 <70 NC

100 104n-Butylbenzene ND 3.9104 99 4.9

98 100n-Propylbenzene ND 2.0100 97 3.0

102 102o-Xylene ND 0.0102 102 0.0

100 102p-Isopropyltoluene ND 2.0104 99 4.9

96 99sec-Butylbenzene ND 3.197 96 1.0

102 102Styrene ND 0.0104 102 1.9

100 102tert-Butylbenzene ND 2.0100 99 1.0

93 95Tetrachloroethene ND 2.191 89 2.2

92 89Tetrahydrofuran (THF) ND 3.396 96 0.0

95 96Toluene ND 1.096 94 2.1

93 94trans-1,2-Dichloroethene ND 1.191 90 1.1

100 96trans-1,3-Dichloropropene ND 4.1110 95 14.6

98 98trans-1,4-dichloro-2-butene ND 0.0112 92 19.6

95 97Trichloroethene ND 2.193 91 2.2

95 91Trichlorofluoromethane ND 4.394 102 8.2

95 89Trichlorotrifluoroethane ND 6.585 98 14.2

91 90Vinyl chloride ND 1.192 87 5.6

99 99% 1,2-dichlorobenzene-d4 111 0.0101 100 1.0

99 101% Bromofluorobenzene 80 2.0100 100 0.0

97 101% Dibromofluoromethane 98 4.0100 103 3.0

99 97% Toluene-d8 97 2.099 99 0.0

A blank MS/MSD was analzyed with this batch.

Comment:

MS - Matrix SpikePhyllis Shiller, Laboratory Director

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.

March 20, 2009MS Dup - Matrix Spike Duplicate

RPD - Relative Percent DifferenceLCS - Laboratory Control SampleLCSD - Laboratory Control Sample Duplicate

NC - No Criteria

Page 2 of 2

Sample Information Custody Information

Matrix:Location Code:

Rush Request:

P.O.#:

Collected by:Received by:

Analyzed by:

SOIL

HARPER

03/20/09

LB

see "By" below

Laboratory DataClient ID: ALBRO SUNDERLAND LUST GP-1 7 FT

Phoenix I.D.: AR47697

03/24/09

0:00

10:50

Parameter Result RL Units Date By Reference

FOR: Attn: Mr. Cliff HarperHarper Environmental Associates1811 Hale Hollow RdBridgewater Corners, VT 05035

Analysis ReportMarch 31, 2009

Time

Date Time

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06040 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG I.D.: GAR47697

64Percent Solid 03/24/09 M-JL E160.3%< 31Tot.Petroleum HC 31 03/25/09 LK E418.1mg/Kg 1

Volatile Organic CompoundsND1,1,1,2-Tetrachloroethane 8.7 03/25/09 R/J 8021/8260ug/KgND1,1,1-Trichloroethane 8.7 03/25/09 R/J 8021/8260ug/KgND1,1,2,2-Tetrachloroethane 8.7 03/25/09 R/J 8021/8260ug/KgND1,1,2-Trichloroethane 8.7 03/25/09 R/J 8021/8260ug/KgND1,1-Dichloroethane 8.7 03/25/09 R/J 8021/8260ug/KgND1,1-Dichloroethene 8.7 03/25/09 R/J 8021/8260ug/KgND1,1-Dichloropropene 8.7 03/25/09 R/J 8021/8260ug/KgND1,2,3-Trichlorobenzene 8.7 03/25/09 R/J 8021/8260ug/KgND1,2,3-Trichloropropane 8.7 03/25/09 R/J 8021/8260ug/KgND1,2,4-Trichlorobenzene 8.7 03/25/09 R/J 8021/8260ug/KgND1,2,4-Trimethylbenzene 8.7 03/25/09 R/J 8021/8260ug/KgND1,2-Dibromo-3-chloropropane(DBCP) 8.7 03/25/09 R/J 8021/8260ug/KgND1,2-Dibromoethane(EDB) 8.7 03/25/09 R/J 8021/8260ug/KgND1,2-Dichlorobenzene 8.7 03/25/09 R/J 8021/8260ug/KgND1,2-Dichloroethane 8.7 03/25/09 R/J 8021/8260ug/KgND1,2-Dichloropropane 8.7 03/25/09 R/J 8021/8260ug/KgND1,3,5-Trimethylbenzene 8.7 03/25/09 R/J 8021/8260ug/KgND1,3-Dichlorobenzene 8.7 03/25/09 R/J 8021/8260ug/KgND1,3-Dichloropropane 8.7 03/25/09 R/J 8021/8260ug/KgND1,4-Dichlorobenzene 8.7 03/25/09 R/J 8021/8260ug/KgND2,2-Dichloropropane 8.7 03/25/09 R/J 8021/8260ug/KgND2-Chlorotoluene 8.7 03/25/09 R/J 8021/8260ug/KgND2-Hexanone 87 03/25/09 R/J 8021/8260ug/KgND2-Isopropyltoluene 8.7 03/25/09 R/J 8021/8260ug/KgND4-Chlorotoluene 8.7 03/25/09 R/J 8021/8260ug/KgND4-Methyl-2-pentanone 87 03/25/09 R/J 8021/8260ug/Kg

Page 1 of 10

ALBRO SUNDERLAND LUST GP-1 7 FT Phoenix I.D.: AR47697

Parameter Result RL Units Date By ReferenceTimeClient ID:

NDAcetone 100 03/25/09 R/J 8021/8260ug/KgNDAcrylonitrile 17 03/25/09 R/J 8021/8260ug/KgNDBenzene 8.7 03/25/09 R/J 8021/8260ug/KgNDBromobenzene 8.7 03/25/09 R/J 8021/8260ug/KgNDBromochloromethane 8.7 03/25/09 R/J 8021/8260ug/KgNDBromodichloromethane 8.7 03/25/09 R/J 8021/8260ug/KgNDBromoform 8.7 03/25/09 R/J 8021/8260ug/KgNDBromomethane 8.7 03/25/09 R/J 8021/8260ug/KgNDCarbon Disulfide 8.7 03/25/09 R/J 8021/8260ug/KgNDCarbon tetrachloride 8.7 03/25/09 R/J 8021/8260ug/KgNDChlorobenzene 8.7 03/25/09 R/J 8021/8260ug/KgNDChloroethane 8.7 03/25/09 R/J 8021/8260ug/KgNDChloroform 8.7 03/25/09 R/J 8021/8260ug/KgNDChloromethane 8.7 03/25/09 R/J 8021/8260ug/KgNDcis-1,2-Dichloroethene 8.7 03/25/09 R/J 8021/8260ug/KgNDcis-1,3-Dichloropropene 8.7 03/25/09 R/J 8021/8260ug/KgNDDibromochloromethane 8.7 03/25/09 R/J 8021/8260ug/KgNDDibromomethane 8.7 03/25/09 R/J 8021/8260ug/KgNDDichlorodifluoromethane 8.7 03/25/09 R/J 8021/8260ug/KgNDEthylbenzene 8.7 03/25/09 R/J 8021/8260ug/KgNDHexachlorobutadiene 8.7 03/25/09 R/J 8021/8260ug/KgNDIsopropylbenzene 8.7 03/25/09 R/J 8021/8260ug/KgNDMethyl Ethyl Ketone 87 03/25/09 R/J 8021/8260ug/KgNDMethyl tert-butyl ether (MTBE) 17 03/25/09 R/J 8021/8260ug/KgNDMethylene chloride 17 03/25/09 R/J 8021/8260ug/KgNDNaphthalene 8.7 03/25/09 R/J 8021/8260ug/KgNDn-Butylbenzene 8.7 03/25/09 R/J 8021/8260ug/KgNDn-Propylbenzene 8.7 03/25/09 R/J 8021/8260ug/KgNDo-Xylene 8.7 03/25/09 R/J 8021/8260ug/KgNDp&m-Xylene 8.7 03/25/09 R/J 8021/8260ug/KgNDp-Isopropyltoluene 8.7 03/25/09 R/J 8021/8260ug/KgNDsec-Butylbenzene 8.7 03/25/09 R/J 8021/8260ug/KgNDStyrene 8.7 03/25/09 R/J 8021/8260ug/KgNDtert-Butylbenzene 8.7 03/25/09 R/J 8021/8260ug/KgNDTetrachloroethene 8.7 03/25/09 R/J 8021/8260ug/KgNDTetrahydrofuran(THF) 17 03/25/09 R/J 8021/8260ug/KgNDToluene 8.7 03/25/09 R/J 8021/8260ug/KgNDtrans-1,2-Dichloroethene 8.7 03/25/09 R/J 8021/8260ug/KgNDtrans-1,3-Dichloropropene 8.7 03/25/09 R/J 8021/8260ug/KgNDtrans-1,4-dichloro-2-butene 8.7 03/25/09 R/J 8021/8260ug/KgNDTrichloroethene 8.7 03/25/09 R/J 8021/8260ug/KgNDTrichlorofluoromethane 8.7 03/25/09 R/J 8021/8260ug/KgNDTrichlorotrifluoroethane 8.7 03/25/09 R/J 8021/8260ug/KgNDVinyl chloride 8.7 03/25/09 R/J 8021/8260ug/Kg

QA/QC Surrogates104% 1,2-dichlorobenzene-d4 03/25/09 R/J 8021/8260%

94% Bromofluorobenzene 03/25/09 R/J 8021/8260%

96% Dibromofluoromethane 03/25/09 R/J 8021/8260%

98% Toluene-d8 03/25/09 R/J 8021/8260%

Page 2 of 10

ALBRO SUNDERLAND LUST GP-1 7 FT Phoenix I.D.: AR47697

Parameter Result RL Units Date By ReferenceTimeClient ID:

Comments:

ND=Not detected BDL=Below Detection Level RL=Reporting Level

Phyllis Shiller, Laboratory Director

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.

March 31, 2009

1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters.

Page 3 of 10

Sample Information Custody Information

Matrix:Location Code:

Rush Request:

P.O.#:

Collected by:Received by:

Analyzed by:

GROUND WATER

HARPER

03/20/09

LB

see "By" below

Laboratory DataClient ID: ALBRO SUNDERLAND LUST GP-3

Phoenix I.D.: AR47698

03/24/09

0:00

10:50

Parameter Result RL Units Date By Reference

FOR: Attn: Mr. Cliff HarperHarper Environmental Associates1811 Hale Hollow RdBridgewater Corners, VT 05035

Analysis ReportMarch 31, 2009

Time

Date Time

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06040 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG I.D.: GAR47697

Volatile Organic CompoundsND1,1,1,2-Tetrachloroethane 1.0 03/27/09 HM 8021/8260ug/LND1,1,1-Trichloroethane 1.0 03/27/09 HM 8021/8260ug/LND1,1,2,2-Tetrachloroethane 1.0 03/27/09 HM 8021/8260ug/LND1,1,2-Trichloroethane 1.0 03/27/09 HM 8021/8260ug/LND1,1-Dichloroethane 1.0 03/27/09 HM 8021/8260ug/LND1,1-Dichloroethene 1.0 03/27/09 HM 8021/8260ug/LND1,1-Dichloropropene 1.0 03/27/09 HM 8021/8260ug/LND1,2,3-Trichlorobenzene 1.0 03/27/09 HM 8021/8260ug/LND1,2,3-Trichloropropane 1.0 03/27/09 HM 8021/8260ug/LND1,2,4-Trichlorobenzene 1.0 03/27/09 HM 8021/8260ug/LND1,2,4-Trimethylbenzene 1.0 03/27/09 HM 8021/8260ug/LND1,2-Dibromo-3-chloropropane 1.0 03/27/09 HM 8021/8260ug/LND1,2-Dichlorobenzene 1.0 03/27/09 HM 8021/8260ug/LND1,2-Dichloroethane 1.0 03/27/09 HM 8021/8260ug/LND1,2-Dichloropropane 1.0 03/27/09 HM 8021/8260ug/LND1,3,5-Trimethylbenzene 1.0 03/27/09 HM 8021/8260ug/LND1,3-Dichlorobenzene 1.0 03/27/09 HM 8021/8260ug/LND1,3-Dichloropropane 1.0 03/27/09 HM 8021/8260ug/LND1,4-Dichlorobenzene 1.0 03/27/09 HM 8021/8260ug/LND2,2-Dichloropropane 1.0 03/27/09 HM 8021/8260ug/LND2-Chlorotoluene 1.0 03/27/09 HM 8021/8260ug/LND2-Hexanone 5.0 03/27/09 HM 8021/8260ug/LND2-Isopropyltoluene 1.0 03/27/09 HM 8021/8260ug/LND4-Chlorotoluene 1.0 03/27/09 HM 8021/8260ug/LND4-Methyl-2-pentanone 5.0 03/27/09 HM 8021/8260ug/LNDAcetone 50 03/27/09 HM 8021/8260ug/LNDAcrylonitrile 5.0 03/27/09 HM 8021/8260ug/LNDBenzene 1.0 03/27/09 HM 8021/8260ug/L

Page 4 of 10

ALBRO SUNDERLAND LUST GP-3 Phoenix I.D.: AR47698

Parameter Result RL Units Date By ReferenceTimeClient ID:

NDBromobenzene 1.0 03/27/09 HM 8021/8260ug/LNDBromochloromethane 1.0 03/27/09 HM 8021/8260ug/LNDBromodichloromethane 1.0 03/27/09 HM 8021/8260ug/LNDBromoform 1.0 03/27/09 HM 8021/8260ug/LNDBromomethane 1.0 03/27/09 HM 8021/8260ug/LNDCarbon Disulfide 5.0 03/27/09 HM 8021/8260ug/LNDCarbon tetrachloride 1.0 03/27/09 HM 8021/8260ug/LNDChlorobenzene 1.0 03/27/09 HM 8021/8260ug/LNDChloroethane 1.0 03/27/09 HM 8021/8260ug/LNDChloroform 1.0 03/27/09 HM 8021/8260ug/LNDChloromethane 1.0 03/27/09 HM 8021/8260ug/LNDcis-1,2-Dichloroethene 1.0 03/27/09 HM 8021/8260ug/LNDDibromochloromethane 1.0 03/27/09 HM 8021/8260ug/LNDDibromoethane 1.0 03/27/09 HM 8021/8260ug/LNDDibromomethane 1.0 03/27/09 HM 8021/8260ug/LNDDichlorodifluoromethane 1.0 03/27/09 HM 8021/8260ug/LNDEthylbenzene 1.0 03/27/09 HM 8021/8260ug/LNDHexachlorobutadiene 1.0 03/27/09 HM 8021/8260ug/LNDIsopropylbenzene 1.0 03/27/09 HM 8021/8260ug/LNDm&p-Xylene 1.0 03/27/09 HM 8021/8260ug/LNDMethyl ethyl ketone 5.0 03/27/09 HM 8021/8260ug/LNDMethyl t-butyl ether (MTBE) 2.0 03/27/09 HM 8021/8260ug/LNDMethylene chloride 1.0 03/27/09 HM 8021/8260ug/LNDNaphthalene 1.0 03/27/09 HM 8021/8260ug/LNDn-Butylbenzene 1.0 03/27/09 HM 8021/8260ug/LNDn-Propylbenzene 1.0 03/27/09 HM 8021/8260ug/LNDo-Xylene 1.0 03/27/09 HM 8021/8260ug/LNDp-Isopropyltoluene 1.0 03/27/09 HM 8021/8260ug/LNDsec-Butylbenzene 1.0 03/27/09 HM 8021/8260ug/LNDStyrene 1.0 03/27/09 HM 8021/8260ug/LNDtert-Butylbenzene 1.0 03/27/09 HM 8021/8260ug/LNDTetrachloroethene 1.0 03/27/09 HM 8021/8260ug/LNDTetrahydrofuran (THF) 5.0 03/27/09 HM 8021/8260ug/LNDToluene 1.0 03/27/09 HM 8021/8260ug/LNDtrans-1,2-Dichloroethene 1.0 03/27/09 HM 8021/8260ug/LNDtrans-1,4-dichloro-2-butene 5.0 03/27/09 HM 8021/8260ug/LNDTrichloroethene 1.0 03/27/09 HM 8021/8260ug/LNDTrichlorofluoromethane 1.0 03/27/09 HM 8021/8260ug/LNDTrichlorotrifluoroethane 1.0 03/27/09 HM 8021/8260ug/LNDVinyl chloride 1.0 03/27/09 HM 8021/8260ug/L

QA/QC Surrogates102% 1,2-dichlorobenzene-d4 03/27/09 HM 8021/8260%

91% Bromofluorobenzene 03/27/09 HM 8021/8260%

100% Dibromofluoromethane 03/27/09 HM 8021/8260%

101% Toluene-d8 03/27/09 HM 8021/8260%

Page 5 of 10

ALBRO SUNDERLAND LUST GP-3 Phoenix I.D.: AR47698

Parameter Result RL Units Date By ReferenceTimeClient ID:

Comments:

ND=Not detected BDL=Below Detection Level RL=Reporting Level

Phyllis Shiller, Laboratory Director

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.

March 31, 2009

Page 6 of 10

Sample Information Custody Information

Matrix:Location Code:

Rush Request:

P.O.#:

Collected by:Received by:

Analyzed by:

GROUND WATER

HARPER

03/20/09

LB

see "By" below

Laboratory DataClient ID: ALBRO SUNDERLAND LUST GP-2

Phoenix I.D.: AR47699

03/24/09

0:00

10:50

Parameter Result RL Units Date By Reference

FOR: Attn: Mr. Cliff HarperHarper Environmental Associates1811 Hale Hollow RdBridgewater Corners, VT 05035

Analysis ReportMarch 31, 2009

Time

Date Time

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06040 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG I.D.: GAR47697

Volatile Organic CompoundsND1,1,1,2-Tetrachloroethane 1.0 03/27/09 HM 8021/8260ug/LND1,1,1-Trichloroethane 1.0 03/27/09 HM 8021/8260ug/LND1,1,2,2-Tetrachloroethane 1.0 03/27/09 HM 8021/8260ug/LND1,1,2-Trichloroethane 1.0 03/27/09 HM 8021/8260ug/LND1,1-Dichloroethane 1.0 03/27/09 HM 8021/8260ug/LND1,1-Dichloroethene 1.0 03/27/09 HM 8021/8260ug/LND1,1-Dichloropropene 1.0 03/27/09 HM 8021/8260ug/LND1,2,3-Trichlorobenzene 1.0 03/27/09 HM 8021/8260ug/LND1,2,3-Trichloropropane 1.0 03/27/09 HM 8021/8260ug/LND1,2,4-Trichlorobenzene 1.0 03/27/09 HM 8021/8260ug/LND1,2,4-Trimethylbenzene 1.0 03/27/09 HM 8021/8260ug/LND1,2-Dibromo-3-chloropropane 1.0 03/27/09 HM 8021/8260ug/LND1,2-Dichlorobenzene 1.0 03/27/09 HM 8021/8260ug/LND1,2-Dichloroethane 1.0 03/27/09 HM 8021/8260ug/LND1,2-Dichloropropane 1.0 03/27/09 HM 8021/8260ug/LND1,3,5-Trimethylbenzene 1.0 03/27/09 HM 8021/8260ug/LND1,3-Dichlorobenzene 1.0 03/27/09 HM 8021/8260ug/LND1,3-Dichloropropane 1.0 03/27/09 HM 8021/8260ug/LND1,4-Dichlorobenzene 1.0 03/27/09 HM 8021/8260ug/LND2,2-Dichloropropane 1.0 03/27/09 HM 8021/8260ug/LND2-Chlorotoluene 1.0 03/27/09 HM 8021/8260ug/LND2-Hexanone 5.0 03/27/09 HM 8021/8260ug/LND2-Isopropyltoluene 1.0 03/27/09 HM 8021/8260ug/LND4-Chlorotoluene 1.0 03/27/09 HM 8021/8260ug/LND4-Methyl-2-pentanone 5.0 03/27/09 HM 8021/8260ug/LNDAcetone 50 03/27/09 HM 8021/8260ug/LNDAcrylonitrile 5.0 03/27/09 HM 8021/8260ug/LNDBenzene 1.0 03/27/09 HM 8021/8260ug/L

Page 7 of 10

ALBRO SUNDERLAND LUST GP-2 Phoenix I.D.: AR47699

Parameter Result RL Units Date By ReferenceTimeClient ID:

NDBromobenzene 1.0 03/27/09 HM 8021/8260ug/LNDBromochloromethane 1.0 03/27/09 HM 8021/8260ug/LNDBromodichloromethane 1.0 03/27/09 HM 8021/8260ug/LNDBromoform 1.0 03/27/09 HM 8021/8260ug/LNDBromomethane 1.0 03/27/09 HM 8021/8260ug/LNDCarbon Disulfide 5.0 03/27/09 HM 8021/8260ug/LNDCarbon tetrachloride 1.0 03/27/09 HM 8021/8260ug/LNDChlorobenzene 1.0 03/27/09 HM 8021/8260ug/LNDChloroethane 1.0 03/27/09 HM 8021/8260ug/LNDChloroform 1.0 03/27/09 HM 8021/8260ug/LNDChloromethane 1.0 03/27/09 HM 8021/8260ug/LNDcis-1,2-Dichloroethene 1.0 03/27/09 HM 8021/8260ug/LNDDibromochloromethane 1.0 03/27/09 HM 8021/8260ug/LNDDibromoethane 1.0 03/27/09 HM 8021/8260ug/LNDDibromomethane 1.0 03/27/09 HM 8021/8260ug/LNDDichlorodifluoromethane 1.0 03/27/09 HM 8021/8260ug/LNDEthylbenzene 1.0 03/27/09 HM 8021/8260ug/LNDHexachlorobutadiene 1.0 03/27/09 HM 8021/8260ug/LNDIsopropylbenzene 1.0 03/27/09 HM 8021/8260ug/LNDm&p-Xylene 1.0 03/27/09 HM 8021/8260ug/LNDMethyl ethyl ketone 5.0 03/27/09 HM 8021/8260ug/LNDMethyl t-butyl ether (MTBE) 2.0 03/27/09 HM 8021/8260ug/LNDMethylene chloride 1.0 03/27/09 HM 8021/8260ug/LNDNaphthalene 1.0 03/27/09 HM 8021/8260ug/LNDn-Butylbenzene 1.0 03/27/09 HM 8021/8260ug/LNDn-Propylbenzene 1.0 03/27/09 HM 8021/8260ug/LNDo-Xylene 1.0 03/27/09 HM 8021/8260ug/LNDp-Isopropyltoluene 1.0 03/27/09 HM 8021/8260ug/LNDsec-Butylbenzene 1.0 03/27/09 HM 8021/8260ug/LNDStyrene 1.0 03/27/09 HM 8021/8260ug/LNDtert-Butylbenzene 1.0 03/27/09 HM 8021/8260ug/LNDTetrachloroethene 1.0 03/27/09 HM 8021/8260ug/LNDTetrahydrofuran (THF) 5.0 03/27/09 HM 8021/8260ug/LNDToluene 1.0 03/27/09 HM 8021/8260ug/LNDtrans-1,2-Dichloroethene 1.0 03/27/09 HM 8021/8260ug/LNDtrans-1,4-dichloro-2-butene 5.0 03/27/09 HM 8021/8260ug/LNDTrichloroethene 1.0 03/27/09 HM 8021/8260ug/LNDTrichlorofluoromethane 1.0 03/27/09 HM 8021/8260ug/LNDTrichlorotrifluoroethane 1.0 03/27/09 HM 8021/8260ug/LNDVinyl chloride 1.0 03/27/09 HM 8021/8260ug/L

QA/QC Surrogates100% 1,2-dichlorobenzene-d4 03/27/09 HM 8021/8260%

93% Bromofluorobenzene 03/27/09 HM 8021/8260%

96% Dibromofluoromethane 03/27/09 HM 8021/8260%

100% Toluene-d8 03/27/09 HM 8021/8260%

Page 8 of 10

ALBRO SUNDERLAND LUST GP-2 Phoenix I.D.: AR47699

Parameter Result RL Units Date By ReferenceTimeClient ID:

Comments:

ND=Not detected BDL=Below Detection Level RL=Reporting Level

Phyllis Shiller, Laboratory Director

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.

March 31, 2009

Page 9 of 10

Sample Information Custody Information

Matrix:Location Code:

Rush Request:

P.O.#:

Collected by:Received by:

Analyzed by:

SOIL

HARPER

03/20/09

LB

see "By" below

Laboratory DataClient ID: ALBRO SUNDERLAND LUST SB-3 6 FT

Phoenix I.D.: AR47700

03/24/09

0:00

10:50

Parameter Result RL Units Date By Reference

FOR: Attn: Mr. Cliff HarperHarper Environmental Associates1811 Hale Hollow RdBridgewater Corners, VT 05035

Analysis ReportMarch 31, 2009

Time

Date Time

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06040 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG I.D.: GAR47697

96Percent Solid 03/24/09 M-JL E160.3%< 21Tot.Petroleum HC 21 03/25/09 LK E418.1mg/Kg 1

Comments:

ND=Not detected BDL=Below Detection Level RL=Reporting Level

Phyllis Shiller, Laboratory Director

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.

March 31, 2009

1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters.

Page 10 of 10

QA/QC Data

Parameter BlankMS

Rec %MS DupRec % RPD

QA/QC ReportMarch 31, 2009

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06040 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG I.D.: GAR47697

LCS%

Dup RPD

LCSD%

LCSRPD

QA/QC Batch 123502, QC Sample No: AR47700 (AR47697, AR47700)

96.0Tot.Petroleum HC BDL 102NC

MS - Matrix SpikePhyllis Shiller, Laboratory Director

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.

March 31, 2009MS Dup - Matrix Spike Duplicate

RPD - Relative Percent DifferenceLCS - Laboratory Control SampleLCSD - Laboratory Control Sample Duplicate

NC - No Criteria

Page 1 of 5

QA/QC Data

Parameter BlankMS

Rec %MS DupRec % RPD

QA/QC ReportMarch 31, 2009

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06040 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG I.D.: GAR47697

LCS%

LCSD%

LCSRPD

QA/QC Batch 123723, QC Sample No: AR47576 (ar47698, ar47699)

Volatiles121 1151,1,1,2-Tetrachloroethane ND 5.197 101 4.0

118 1141,1,1-Trichloroethane ND 3.494 96 2.1

122 1181,1,2,2-Tetrachloroethane ND 3.396 100 4.1

126 1221,1,2-Trichloroethane ND 3.297 101 4.0

119 1181,1-Dichloroethane ND 0.898 101 3.0

111 1121,1-Dichloroethene ND 0.991 94 3.2

111 1081,1-Dichloropropene ND 2.790 93 3.3

132 1481,2,3-Trichlorobenzene ND 11.4122 130 6.3 3

127 1251,2,3-Trichloropropane ND 1.6111 117 5.3

131 1411,2,4-Trichlorobenzene ND 7.4116 121 4.2 3

126 1251,2,4-Trimethylbenzene ND 0.8107 115 7.2

148 1461,2-Dibromo-3-chloropropane ND 1.4111 113 1.8 3

112 1131,2-Dichlorobenzene ND 0.995 102 7.1

122 1161,2-Dichloroethane ND 5.096 99 3.1

120 1181,2-Dichloropropane ND 1.797 103 6.0

121 1211,3,5-Trimethylbenzene ND 0.0102 110 7.5

116 1161,3-Dichlorobenzene ND 0.098 105 6.9

121 1211,3-Dichloropropane ND 0.0103 107 3.8

117 1191,4-Dichlorobenzene ND 1.7100 105 4.9

<30 <30 2,2-Dichloropropane ND NC84 85 1.2 3

117 1182-Chlorotoluene ND 0.999 105 5.9

136 1432-Hexanone ND 5.0118 125 5.8

119 1192-Isopropyltoluene ND 0.0101 111 9.4

119 1164-Chlorotoluene ND 2.6103 109 5.7

150 1404-Methyl-2-pentanone ND 6.9119 113 5.2

142 124Acetone ND 13.590 90 0.0

98 107Acrolein ND 8.8103 106 2.9

125 124Acrylonitrile ND 0.8106 106 0.0

116 114Benzene ND 1.794 99 5.2

115 113Bromobenzene ND 1.897 102 5.0

122 119Bromochloromethane ND 2.599 101 2.0

127 122Bromodichloromethane ND 4.0102 105 2.9

130 123Bromoform ND 5.598 97 1.0

99 114Bromomethane ND 14.1108 113 4.5

*NC *NC Carbon Disulfide ND NC96 101 5.1

119 112Carbon tetrachloride ND 6.188 92 4.4

112 111Chlorobenzene ND 0.994 99 5.2

93 99Chloroethane ND 6.3106 115 8.1

Page 2 of 5

QA/QC Data

Parameter BlankMS

Rec %MS Dup Rec % RPD

SDG I.D.: GAR47697

LCS%

LCSD%

LCSRPD

121 120Chloroform ND 0.898 101 3.0

108 125Chloromethane ND 14.6113 121 6.8

115 116cis-1,2-Dichloroethene ND 0.9100 101 1.0

104 101cis-1,3-Dichloropropene ND 2.9106 110 3.7

131 125Dibromochloromethane ND 4.7102 103 1.0

127 119Dibromoethane ND 6.5102 105 2.9

115 118Dibromomethane ND 2.696 98 2.1

110 39Dichlorodifluoromethane ND 95.3106 114 7.3 3

116 113Ethylbenzene ND 2.698 105 6.9

104 111Hexachlorobutadiene ND 6.593 102 9.2

122 123Isopropylbenzene ND 0.898 108 9.7

118 115m&p-Xylene ND 2.699 105 5.9

109 111Methyl ethyl ketone ND 1.894 88 6.6

126 123Methyl t-butyl ether (MTBE) ND 2.4102 101 1.0

103 108Methylene chloride ND 4.789 92 3.3

>150 >150 Naphthalene ND NC>130 >130 NC 3

122 122n-Butylbenzene ND 0.0104 114 9.2

117 118n-Propylbenzene ND 0.9100 109 8.6

124 120o-Xylene ND 3.3104 110 5.6

120 119p-Isopropyltoluene ND 0.8106 113 6.4

117 117sec-Butylbenzene ND 0.098 107 8.8

122 120Styrene ND 1.7104 110 5.6

122 121tert-Butylbenzene ND 0.8103 111 7.5

104 105Tetrachloroethene ND 1.089 96 7.6

113 109Tetrahydrofuran (THF) ND 3.693 91 2.2

117 115Toluene ND 1.797 103 6.0

110 114trans-1,2-Dichloroethene ND 3.698 102 4.0

106 102trans-1,3-Dichloropropene ND 3.8107 111 3.7

68 70trans-1,4-dichloro-2-butene ND 2.9112 118 5.2

114 112Trichloroethene ND 1.894 99 5.2

109 106Trichlorofluoromethane ND 2.890 93 3.3

118 106Trichlorotrifluoroethane ND 10.787 90 3.4

114 74Vinyl chloride ND 42.6104 109 4.7

102 101% 1,2-dichlorobenzene-d4 103 1.0100 99 1.0

102 98% Bromofluorobenzene 91 4.0100 99 1.0

103 103% Dibromofluoromethane 99 0.0103 101 2.0

102 100% Toluene-d8 100 2.0100 100 0.0

QA/QC Batch 123501, QC Sample No: AR47728 (ar47697)

Volatiles91 941,1,1,2-Tetrachloroethane ND 3.2100 105 4.9

102 1051,1,1-Trichloroethane ND 2.9110 120 8.7

65 731,1,2,2-Tetrachloroethane ND 11.673 85 15.2 3

101 1021,1,2-Trichloroethane ND 1.0111 112 0.9

103 1081,1-Dichloroethane ND 4.7112 122 8.5

114 1121,1-Dichloroethene ND 1.8124 127 2.4

99 1041,1-Dichloropropene ND 4.9109 122 11.3

77 741,2,3-Trichlorobenzene ND 4.095 101 6.1

88 881,2,3-Trichloropropane ND 0.0107 99 7.8

Page 3 of 5

QA/QC Data

Parameter BlankMS

Rec %MS Dup Rec % RPD

SDG I.D.: GAR47697

LCS%

LCSD%

LCSRPD

71 681,2,4-Trichlorobenzene ND 4.394 102 8.2 3

85 871,2,4-Trimethylbenzene ND 2.398 111 12.4

90 861,2-Dibromo-3-chloropropane ND 4.598 94 4.2

84 841,2-Dichlorobenzene ND 0.096 102 6.1

93 931,2-Dichloroethane ND 0.0108 107 0.9

101 1071,2-Dichloropropane ND 5.8112 120 6.9

85 881,3,5-Trimethylbenzene ND 3.595 109 13.7

81 821,3-Dichlorobenzene ND 1.297 106 8.9

96 961,3-Dichloropropane ND 0.0107 105 1.9

78 791,4-Dichlorobenzene ND 1.394 104 10.1

99 1032,2-Dichloropropane ND 4.0109 122 11.3

88 892-Chlorotoluene ND 1.194 107 12.9

96 932-Hexanone ND 3.2120 108 10.5

90 932-Isopropyltoluene ND 3.393 107 14.0

84 864-Chlorotoluene ND 2.499 110 10.5

107 1034-Methyl-2-pentanone ND 3.8127 119 6.5

112 89Acetone ND 22.9>130 109 NC

127 110Acrolein ND 14.3>130 123 NC

117 114Acrylonitrile ND 2.6130 124 4.7

99 104Benzene ND 4.9110 120 8.7

87 88Bromobenzene ND 1.193 100 7.3

103 110Bromochloromethane ND 6.6113 122 7.7

95 99Bromodichloromethane ND 4.1110 114 3.6

94 95Bromoform ND 1.1106 104 1.9

134 104Bromomethane ND 25.2125 115 8.3

97 94Carbon Disulfide ND 3.1114 120 5.1

92 97Carbon tetrachloride ND 5.3103 115 11.0

92 95Chlorobenzene ND 3.2102 109 6.6

110 108Chloroethane ND 1.8111 129 15.0

100 104Chloroform ND 3.9109 116 6.2

87 108Chloromethane ND 21.5109 >130 NC

108 112cis-1,2-Dichloroethene ND 3.6116 126 8.3

108 106cis-1,3-Dichloropropene ND 1.9118 119 0.8

92 94Dibromochloromethane ND 2.2100 102 2.0

107 102Dibromoethane ND 4.8118 109 7.9

97 99Dibromomethane ND 2.0110 110 0.0

82 85Dichlorodifluoromethane ND 3.6118 >130 NC

95 98Ethylbenzene ND 3.1106 116 9.0

75 77Hexachlorobutadiene ND 2.687 101 14.9

92 95Isopropylbenzene ND 3.296 105 9.0

95 98m&p-Xylene ND 3.1110 120 8.7

102 95Methyl ethyl ketone ND 7.1>130 118 NC

104 92Methyl t-butyl ether (MTBE) ND 12.2118 104 12.6

112 104Methylene chloride ND 7.4119 115 3.4

103 93Naphthalene ND 10.2114 110 3.6

78 79n-Butylbenzene ND 1.399 113 13.2

87 89n-Propylbenzene ND 2.398 108 9.7

96 100o-Xylene ND 4.1106 116 9.0

87 87p-Isopropyltoluene ND 0.0100 114 13.1

Page 4 of 5

QA/QC Data

Parameter BlankMS

Rec %MS Dup Rec % RPD

SDG I.D.: GAR47697

LCS%

LCSD%

LCSRPD

88 91sec-Butylbenzene ND 3.496 110 13.6

99 101Styrene ND 2.0110 117 6.2

92 95tert-Butylbenzene ND 3.296 110 13.6

86 89Tetrachloroethene ND 3.497 112 14.4

118 102Tetrahydrofuran (THF) ND 14.5>130 110 NC

102 105Toluene ND 2.9113 123 8.5

112 101trans-1,2-Dichloroethene ND 10.3128 124 3.2

109 98trans-1,3-Dichloropropene ND 10.6124 115 7.5

101 80trans-1,4-dichloro-2-butene ND 23.2125 100 22.2

112 112Trichloroethene ND 0.0117 124 5.8

93 100Trichlorofluoromethane ND 7.3118 128 8.1

113 110Trichlorotrifluoroethane ND 2.7118 127 7.3

100 108Vinyl chloride ND 7.7120 >130 NC

97 99% 1,2-dichlorobenzene-d4 103 2.0100 99 1.0

103 102% Bromofluorobenzene 91 1.0103 101 2.0

99 98% Dibromofluoromethane 93 1.0100 97 3.0

99 102% Toluene-d8 98 3.0100 102 2.0

MS - Matrix SpikePhyllis Shiller, Laboratory Director

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.

March 31, 2009MS Dup - Matrix Spike Duplicate

RPD - Relative Percent DifferenceLCS - Laboratory Control Sample

LCSD - Laboratory Control Sample Duplicate

NC - No Criteria

3 = This parameter is outside laboratory ms/msd specified limits.

Page 5 of 5