C o w a l G o l d O p e r a t i o n - Evolution Mining...Cowal Gold Project – Dust Management Plan...

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August 2003 Dust Management Plan C o w a l G o l d O p e r a t i o n

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Page 1: C o w a l G o l d O p e r a t i o n - Evolution Mining...Cowal Gold Project – Dust Management Plan COWAL GOLD PROJECT DUST MANAGEMENT PLAN AUGUST 2003 Project No. HAL-02-07/1/15

August 2003

DustManagement Plan

C o w a l G o l d O p e r a t i o n

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Cowal Gold Project – Dust Management Plan

COWAL GOLD PROJECT

DUST MANAGEMENT PLAN

AUGUST 2003

Project No. HAL-02-07/1/15 Document No. DMP01-R

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Cowal Gold Project – Dust Management Plan

HAL-02-07/1/15/00685106.DOC/29/09/03

PREFACE

This Dust Management Plan (DMP) has been prepared to meet the requirements of Condition 6.1 of the Cowal Gold Project Development Consent. Where there is any conflict between the provisions of this DMP and the applicable statutory requirements (i.e. licences, permits, consents and relevant laws) the statutory requirements are to take precedence. In accordance with Development Consent Condition 3.2 this DMP is to be revised/updated at least every five years, or as otherwise directed by the Director-General, in consultation with the relevant government authorities. Relevant current regulatory guidelines and Australian Standards are appended to this DMP to provide guidance to Barrick employees and its contractors. It is the responsibility of Barrick to ascertain whether these guidelines or Australian Standards have been updated since the production of this DMP, and to conform with any new versions of these guidelines or standards as required by Development Consent Conditions. Similarly, it is the responsibility of Barrick to refer to the latest versions of statutory instruments or guidelines that are referenced in this DMP, but have not been appended.

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TABLE OF CONTENTS Section Page

1 INTRODUCTION 1 1.1 OBJECTIVES AND SCOPE 4

2 AIR QUALITY CRITERIA 5

3 BASELINE AIR QUALITY 6 3.1 EIS BASELINE DUST MONITORING 6

3.1.1 Dust Deposition 6 3.1.2 TSP 8

3.2 CONTINUATION OF BASELINE MONITORING 8 3.2.1 Dust Deposition 8 3.2.2 TSP 8

4 DUST GENERATION SOURCES 8

5 DUST SUPPRESSION AND CONTROL 10 5.1 AIR QUALITY SAFEGUARDS 10 5.2 DUST CONTROL EQUIPMENT 12 5.3 STOCKPILE SURFACE TREATMENT 12 5.4 REHABILITATION 13

6 ADDITIONAL MODIFICATION OF MINING OPERATIONS TO MINIMISE DUST EMISSIONS 14 6.1 REQUIREMENT FOR ADDITIONAL MODIFICATIONS OF OPERATIONS 14 6.2 DUST MANAGEMENT PROCEDURES 16

6.2.1 Standard Management Procedure 16 6.2.2 Amenity Criteria Management Procedure 17

7 AIR QUALITY MONITORING PROGRAMME 19 7.1 METEOROLOGY 19 7.2 DUST DEPOSITION GAUGES 20

7.2.1 Analysis of Metals in Dust Samples 22 7.2.2 Dust Deposition Monitoring within Lake Cowal 22 7.2.3 Surface Water Monitoring Programme 23

7.3 TOTAL SUSPENDED PARTICULATE HIGH VOLUME SAMPLER 24 7.4 REVIEW OF MONITORING PROGRAMMES 25

8 STAKEHOLDER CONSULTATION 26 8.1 COMMUNITY ENVIRONMENTAL MONITORING AND CONSULTATIVE

COMMITTEE 26 9 COMPLAINTS AND PROPERTY ACQUISITION IN THE EVENT OF DUST

AFFECTATION 27

9.1 COMPLAINTS REGISTER 27 9.2 INDEPENDENT INVESTIGATION PROCESS 28 9.3 PROPERTY ACQUISITION DUE TO DUST AFFECTATION 29

10 REPORTING 30

11 REFERENCES 31

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Cowal Gold Project – Dust Management Plan

TABLE OF CONTENTS (continued)

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LIST OF TABLES

Table 1 NSW EPA Impact Assessment Criteria for Dust

Table 2 NSW EPA Impact Assessment Criteria for TSP Matter

Table 3 EIS Baseline Mean Annual Dust Deposition Rates (November 1993 to November 1994)

Table 4 Safeguards and Control Methods for Construction Generated Dust Sources

Table 5 Safeguards and Control Methods for Exposed Area Dust Sources

Table 6 Safeguards and Control Methods for Mining Generated Dust Sources

Table 7 Dust Control Equipment

Table 8 Modifications to Dust Generating Activities

Table 9 Dust Monitoring Sites and Rationale

Table 10 Project Surface Water Monitoring Programme

LIST OF FIGURES

Figure 1 Project Location

Figure 2 Location of Pre-EIS Baseline Dust Monitoring Sites

Figure 3 Location of Dust Monitoring Sites 1999-2003

Figure 4 Dust Management Procedures

Figure 5 Dust Monitoring Locations

LIST OF APPENDICES

Appendix A Approved Methods for the Sampling and Analysis of Air Pollutants in New South Wales

Appendix B AS 2922 Ambient Air - Guide for the Siting of Sampling Units

Appendix C AS 3580.10.1-1991 Methods for Sampling and Analysis of Ambient Air - Determination of Particulates - Deposited Matter - Gravimetric Method

Appendix D AS 2724.3-1984 Ambient Air – Particulate Matter – Determination of Total Suspended Particulates (TSP) – High Volume Sampler Gravimetric Method

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1 INTRODUCTION The Cowal Gold Project (the Project) is located approximately 38 kilometres (km) north-east of West Wyalong, New South Wales (NSW) (Figure 1). The Project is owned by Barrick Gold Australia Ltd (Barrick). Development Consent Conditions 6.1, 6.2, 8.1 and 8.3 for the mine and pipeline require the preparation of the enclosed Dust Management Plan (DMP). The consent conditions and the corresponding sections of this Plan that address the conditions are outlined below:

Consent Condition Section

6.1 Air Quality Management

(a) The Applicant shall prior to the commencement of construction works prepare a dust management plan detailing air quality safeguards and procedures for dealing with dust emissions in consultation with the EPA and to the satisfaction of the Director-General. The management plan shall be updated as required by the Director-General and/or EPA. The plan shall include, but not be limited to, details of: locations for dust monitoring (in accordance with Australian Standard), including location gauges near the Gumbelah residence, and bird breeding and native flora areas determined by the Applicant in consultation with the EPA and NPWS;

Section 5 Section 6

Figures 2, 3 and 5 Table 9

(b) methods to determine when and how the mine operation is to be modified to minimise the potential for dust emissions.

Section 6

(c) measures to continue baseline monitoring undertaken prior to development consent.

(Refer condition 8.3 for air quality monitoring details)

Sections 3 and 7

6.2 Dust Suppression and Control

The Applicant shall:

(i) maintain and use sufficient equipment with the capacity to apply water to all unsealed trafficked areas at a rate which minimises dust emissions;

Section 5.1 and Table 7

(ii) ensure the prompt and effective rehabilitation of all disturbed areas to minimise generation of wind erosion dust, in accordance with the requirements of DMR;

Section 5.1 and Table 5

(iii) keep the surface of all stockpiles sufficiently treated to minimise windblown dust.

Section 5.1 and Table 5

8.1 Meteorological

The Applicant shall continue meteorological monitoring by utilising and maintaining the existing weather station on site. The data shall be particularly used for predicting noise, dust and blasting impacts on nearby residences, and bird breeding areas identified by the Applicant in consultation with NPWS.

Section 7.1

8.3 Air Quality and Dust

The Applicant shall:

(a) undertake monitoring at locations described in the dust management plan (condition 6.1);

Section 7

(b) monitor dust deposition rates and concentrations of total suspended particulates (TSP) for the life of the mine, including monitoring impacts of dust on any surface water within the high water mark of Lake Cowal; and

Sections 7.2 and 7.3 and Figure 5

(c) provide all results and analysis of air quality monitoring in the AEMR including a determination of the dust deposition rate in gm/m2/month, which shall be plotted in the AEMR.

Section 10

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Bland

San

dy

Creek

Cre

ek

Lake

Cowal

Nerang

Cowal

6 300 000 N

540

000

E54

0 00

0 E

6 280 000 N

6 260 000 N

6 280 000 N

6 260 000 N

520

000

E

ML1535

Bogeys

Island

WamboyneMountain

Blow Clear

BillysLookout

COWAL GOLDPROJECT

Wam

boyn

eRo

ad

West Wyalong

Burcher

LakeCargelligo

Railway

Wes

t

Wya

long

Newell

Highway

To Temoraapprox 59km

To Forbesapprox 46km

QuandiallaRoad

McCaskiesLane

Wes

tsLa

ne

Ridleys Lane Websters Lane

Wamboyn

e

Dip

Buttenshaw

Lane

Road

Sullivans

Lane

Lane

LonergansLane

Lane

Cun

ning

tons

Lane

Bodels

Wilsons

Lane

Burc

her

Rai

lway

Websters Road

Burcher Road

Kurb

ooLa

ne

Cootamundra

LEGENDProposed Borefield and Borefield Pipeline

Proposed Site Access Road

Proposed Electricity Transmission Line

Mining Lease Boundary

Relocated Travelling Stock Reserve

0 5

Kilometres

10

FIGURE 1

Project Location

HAL-02-07 RMP Dust_001A

D u s t M a n a g e m e n t P l a n

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In addition: • Consent Condition 3.6 states the requirements for site rehabilitation management. This condition

is addressed in Section 5.4.

• Consent Condition 8.7 establishes the requirements for a Community Consultative Committee and is addressed in Section 8.1.

• Consent Condition 8.8 establishes the requirements for an Independent Environmental Audit (IEA) and an Independent Monitoring Panel (IMP). These conditions are discussed in Section 7.4.

• Consent Condition 9.2 establishes environmental reporting requirements as provided and discussed in Section 10.

• Consent Conditions 10 and 11 outline the requirements for receipt and response to community complaints and Proponent’s obligations with regard to dust affectation. These conditions are provided and discussed in Section 9.

• In accordance with Consent Condition 12.1 the Applicant is obliged to ensure all statutory requirements are fully met.

Conditions of Authority ML 1535 The Department of Mineral Resources (DMR) also has requirements that relate to dust control and rehabilitation as detailed in the Conditions of Authority of the Mining Lease (ML) 2000. Relevant Conditions of Authority include:

Rehabilitation 12. (a) Land disturbed must be rehabilitated to a stable and permanent form suitable for a subsequent

land use acceptable to the Director General and in accordance with the Mining Operations Plan so that:

• there is no adverse environmental effect outside of the disturbed area and that the land

is properly drained and protected from soil erosion.

• the state of the land is compatible with the surrounding land use and land use requirements.

• the landforms,soils, hydrology and flora require no greater maintenance than in the surrounding land.

• in cases where revegetation is required and native vegetation has been removed or damaged, the original species must be re-established with close reference to the flora survey included in the Mining Operations plan. If the original vegetation was not native, any re-established vegetation must be appropriate for the area and at an acceptable density.

• the land does not pose a threat to public safety. (b) Any topsoil that is removed must be stored and maintained in a manner acceptable to the

Director General. 13. The lease holder must comply with any direction given by the Director-General regarding the

stabilisation and revegetation of any mine residues, tailings or overburden dumps situated on the lease area.

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Prevention of Soil erosion and Pollution 14. Operations must be carried out in a manner that does not cause or aggravate air pollution, water

pollution (including sedimentation) or soil contamination or erosion, unless otherwise authorised by a relevant approval, and in accordance with an accepted Mining operation Plan. For the purpose of this condition, water shall be taken to be include any watercourse, waterbody or groundwaters. The lease holder must observe and perform any instruction given by the director general.

These Conditions of Authority are addressed in Section 5, particularly Section 5.4. Annual Environmental Management Report (AEMR) 26. (1) Within 12 months of the commencement of mining operations and thereafter annually or, at

such other times as may be allowed by the Director-General, the lease holder must lodge an Annual Environmental Management Report (AEMR) with the Director-General.

(2) The AEMR must be prepared in accordance with the Director-General's guidelines current at the time of reporting and contain a review and forecast of performance for the preceding and ensuing twelve months in terms of:

(a) the accepted Mining Operations Plan;

(b) development consent requirements and conditions;

(c) Environment Protection Authority and Department of Land and Water Conservation licences and approvals;

(d) any other statutory environmental requirements;

(e) details of any variations to environmental approvals applicable to the lease area; and

(f) where relevant, progress towards final rehabilitation objectives.

(3) After considering an AEMR the Director-General may, by notice in writing, direct the lease holder to undertake operations, remedial actions or supplementary studies in the manner and within the period specified in the notice to ensure that operations on the lease area are conducted in accordance with sound mining and environmental practice.

(4) The lease holder shall, as and when directed by the Minister, cooperate with the Director-General to conduct and facilitate review of the AEMR involving other government agencies and the local council.

This Condition of Authority is addressed in Section 10.

1.1 OBJECTIVES AND SCOPE The primary objective of this DMP is to establish a dust management strategy for the Project that complies with Consent Conditions by providing: • a summary of relevant issues;

• air quality safeguards and procedures for dealing with dust emissions;

• details on how and when the mine operation is to be modified to minimise the potential for dust emissions; and

• dust monitoring locations and measures to continue baseline monitoring.

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As assessed in the Cowal Gold Project Environmental Impact Statement (EIS) (North Limited, 1998) atmospheric dust is the predicted dominant component of air emissions from the Project. Other minor air quality emissions could potentially include exhaust fumes from mobile equipment, blasting fumes and evaporative emissions from processing facilities (Pavel Zib and Associates, 1997). As the EIS air quality assessment of the Project found these other emissions were not environmentally significant, this DMP provides safeguards, controls and management measures relating to dust emissions (both dust deposition and total suspended particulates [TSP]). This approach for the DMP has been agreed by the NSW Environment Protection Authority (EPA) (EPA, pers. comm., 5 June 2003). The DMP is structured as follows: Section 1: Outlines the objectives of the plan and details relevant consent conditions.

Section 2: Identifies relevant air quality criteria that apply to the Project.

Section 3: Outlines baseline air quality monitoring.

Section 4: Identifies potential dust generation sources for which management measures are proposed.

Section 5: Details air quality safeguards and control measures.

Section 6: Presents procedures for modifications to mining operations to minimise dust emissions.

Section 7: Outlines the air quality monitoring programme.

Section 8: Presents stakeholder consultation and notification requirements.

Section 9: Details complaint resolution and property acquisition requirements.

Section 10: Outlines reporting requirements for dust related issues. In accordance with consent condition requirements, EPA and the National Parks and Wildlife Service (NPWS) have been consulted during the preparation of this management plan. The DMP will be prepared to the satisfaction of the Director-General of the Department of Infrastructure, Planning and Natural Resources (DIPNR).

2 AIR QUALITY CRITERIA As set out in Section 1.1, relevant air quality criteria derived from the consent conditions and consultation with the EPA relate to dust deposition and TSP. Other emissions to air arising from the Project are not considered to be environmentally significant. The consent conditions require the management, monitoring and reporting of dust emissions from the Project. Dust is a generic term used to describe fine particles that are suspended in the atmosphere (Environment Australia, 1998). Consent Condition 8.3(b) requires monitoring of both dust deposition rates and concentration of TSP (Section 1). These can be defined as follows (Environment Australia, 1998): • dust deposition (deposited matter) – this term describes any particulate matter that falls out

from suspension in the atmosphere. This measurement is usually expressed in units of mass per area per time (eg. grams per square metre per month - g/m2/month); and

• TSP - the nominal size of this fraction has particles with a diameter up to 50 microns (micrometres or μm). This enables determinations of dust concentrations in units of mass (usually micrograms) per cubic metre (μg/m3).

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Further detail on applicable criteria for these two aspects of air quality is provided below. Dust Deposition Table 1 details the EPA criteria for deposited dust which seek to limit total annual average levels to 4 grams per square metre per month (g/m2/month) and project related increases to 2 g/m2/month.

Table 1 NSW EPA Impact Assessment Criteria for Dust

Pollutant Averaging Period Maximum Increase in Deposited Dust Level

Maximum Total Deposited Dust Level

Deposited dust Annual 2 g/m2/month 4 g/m2/month

Source: EPA (2001) (Table 3.6) Note: Dust is assessed as insoluble solids as defined by AS 3580.10.1-1991 (AM-19).

Total Suspended Particulates (TSP) Table 2 details the applicable EPA criteria for TSP.

Table 2 NSW EPA Impact Assessment Criteria for TSP Matter

Pollutant Averaging period Concentration

TSP Annual 90 µg/m3 Source: EPA (2001) (Table 3.7)

3 BASELINE AIR QUALITY

3.1 EIS BASELINE DUST MONITORING

3.1.1 Dust Deposition Baseline dust deposition was monitored for a one year period (1993-1994) prior to the release of the Project EIS (North Limited, 1998) at the locations shown on Figure 2. The mean deposition rates at each sampling site are summarised in Table 3.

Table 3 EIS Baseline Mean Annual Dust Deposition Rates

(November 1993 to November 1994)

Site Mean (g/m2/month) Number of Measurements

51 1.61 11

52 1.37 13

54 0.99 13 Source: North Limited (1998)

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Creek

Bland

San

dy

NerangCowal

Wamboyne

Mountain

Burcher

-R

ailway

West

WyalongCOWAL

GOLDPROJECT

Bogeys

Island

Open Pit

Northern

Tailings Storage

Southern

Tailings Storage

NorthernWaste

Emplacement

SouthernWaste

Emplacement

Ore Stockpile andProcess Plant Area

‘Coniston’

‘Gumbelah’

‘Lakeside’

‘Lake Cowal'‘Hillgrove’

Site 52Site 51

Site 54

540

000

E

535

000

E

545

000

E

6 275 000 N

6 270 000 N

6 290 000 N

6 285 000 N

545

000

E

6 280 000 N

6 275 000 N

6 280 000 N

LEGEND

Barrick-owned Land

Mining Lease Boundary

Dust Deposition Gauge

0 2

Kilometres

4

ML1535

FIGURE 2

Location of Pre-EIS BaselineDust Monitoring Sites

S o i l S t r i p p i n g M a n a g e m e n t P l a nD u s t M a n a g e m e n t P l a n

HAL-02-07 RMP Dust_003A

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3.1.2 TSP No baseline monitoring of TSP was undertaken at Lake Cowal prior to the granting of development consent. Given the consistently low recorded levels of dust deposition, the concentrations of TSP are expected to be correspondingly low (Pavel Zib and Associates, 1997). Background mean annual TSP concentrations of 30 micrograms per cubic metre (μg/m3) were adopted for use in the Project EIS (North Limited, 1998).

3.2 CONTINUATION OF BASELINE MONITORING

3.2.1 Dust Deposition Dust deposition monitoring has been conducted at seven sites (Figure 3) since 1999 in a continuation of the baseline monitoring undertaken prior to the issued development consent (Section 3.1.1). In addition to the three baseline sites (51, 52 and 54), monitoring has also been conducted at the general monitoring sites of Lakeside, McLintocks, Site I5 and the Site Office (Figure 3). Continuation of baseline monitoring is further discussed in Section 7.2.

3.2.2 TSP No monitoring of TSP has occurred to date since the granting of development consent as TSP monitoring was not a component of the baseline monitoring programme. The commencement of TSP monitoring is discussed in Section 7.3.

4 DUST GENERATION SOURCES The air quality assessment conducted for the EIS (Pavel Zib and Associates, 1997) concluded that the Project would result in only minor exceedances of the dust deposition and TSP criteria outside of the Project Mining Lease Application (MLA) area. The exceedances that were identified were restricted to small areas adjoining the MLA area. No non-Company owned residences were predicted to exceed the relevant EPA criteria. Potential dust emission sources from mining operations include (Pavel Zib and Associates, 1997): • areas disturbed by construction activities;

• areas disturbed by mining activities, including waste emplacement areas and other portions of the mine site exposed to wind;

• waste rock handling and stockpiling activities (including loading and unloading, spreading and shaping of waste);

• movement of vehicles on unsealed roads for general mining activities;

• topsoil stripping and stockpiling;

• drilling and blasting; and

• crushing, screening, transport and preparation of ore.

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Creek

Bland

San

dy

NerangCowal

Wamboyne

Mountain

Burcher

-R

ailway

West

WyalongCOWAL

GOLDPROJECT

Bogeys

Island

Open Pit

Northern

Tailings Storage

Southern

Tailings Storage

NorthernWaste

Emplacement

SouthernWaste

Emplacement

Ore Stockpile andProcess Plant Area

‘Coniston’

‘Gumbelah’

‘Lakeside’

‘Lake Cowal'‘Hillgrove’

5

Site 52Site 51

Site 54

Site Office

McLintocks

Lakeside

I

540

000

E

535

000

E

545

000

E

6 275 000 N

6 270 000 N

6 290 000 N

6 285 000 N

545

000

E

6 280 000 N

6 275 000 N

6 280 000 N

LEGEND

Barrick-owned Land

Mining Lease Boundary

Dust Deposition Gauge

0 2

Kilometres

4

ML1535

FIGURE 3

Location of DustMonitoring Sites 1999-2003

S o i l S t r i p p i n g M a n a g e m e n t P l a nD u s t M a n a g e m e n t P l a n

HAL-02-07 RMP Dust_004A

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In addition, farming activities could potentially also contribute to local and regional dust levels (Pavel Zib and Associates, 1997).

5 DUST SUPPRESSION AND CONTROL

5.1 AIR QUALITY SAFEGUARDS The Project air quality safeguards and control methods will minimise dust emissions from all sources identified in Section 4 (other than farming activities). These sources can be categorised as follows: (i) construction activities;

(ii) exposed areas (via wind erosion); and

(iii) general mining activities. Barrick will manage dust emissions proactively in a manner that minimises potential air quality impacts in accordance with development consent conditions for the Project. The air quality safeguards and control methods to minimise dust emissions that are detailed in this section have been prepared in consultation with the EPA (EPA, pers. comm., 5 June 2003). Tables 4, 5 and 6 list the air quality safeguards and control methods to minimise sources of construction, exposed area and general mining generated dust, respectively.

Table 4

Safeguards and Control Methods for Construction Generated Dust Sources

Source Control Methods

Disturbed Surfaces • Disturbed surfaces will be watered using water trucks or other methods to suppress dust.

• Areas for soil stripping will be minimised to reduce the area of exposed ground at any one time.

Access Roads • Access roads will be watered (using water trucks or other methods) and regularly maintained.

• Routes will be clearly marked.

• Obsolete roads will be ripped and revegetated.

• The speed of vehicles travelling on unsealed surfaces will be restricted.

Soil Stripping • Access tracks used for soil stripping during the loading and unloading cycle will be watered.

• Soil stripping will be limited to areas required for mining operations. After: North Limited (1998)

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Table 5 Safeguards and Control Methods for Exposed Area Dust Sources

Source Control Methods

General Areas Disturbed by Mining

• Areas for soil stripping will be minimised to reduce the area of exposed ground at any one time.

• Exposed areas will be reshaped, topsoiled and revegetated as soon as practicable in accordance with DMR requirements (DMR, 2002), to minimise the generation of wind erosion dust.

Waste Emplacement Areas

• Exposed active work areas on waste emplacement surfaces will be watered to suppress dust where practicable. Progressive rehabilitation (ie. reshaping, topsoil placement and revegetation) of waste emplacement areas will continue throughout the Project in accordance with DMR requirements (DMR, 2002).

Soil Stockpiles • Long term soil stockpiles will be revegetated with a cover crop.

Material Handling and Stockpiles

• Prevention of truck overloading to reduce spillage during ore loading/unloading and hauling.

• The coarse ore stockpile will be protected by a hood to prevent wind erosion of its surface.

• All conveyors will incorporate wind covers as necessary.

• The surface of all stockpiles will be sufficiently treated to minimise dust emissions. Such treatment may include application of a dust suppressant, regular dust suppression watering or establishment of vegetation on longer term stockpiles (eg. the low grade ore stockpile).

After: North Limited (1998)

Table 6 Safeguards and Control Methods for Mining Generated Dust Sources

Source Control Methods

Haul Road • All roads and trafficked areas will be watered (using water trucks or other methods) and regularly maintained (using graders) to minimise the generation of dust.

• Routes will be clearly marked.

• Obsolete roads will be ripped and re-vegetated.

Minor Roads • Development of minor roads will be limited and the locations of these will be clearly defined.

• Regularly used minor roads will be watered and regularly maintained.

• Obsolete minor roads will be ripped and re-vegetated.

Materials Handling • Prevention of truck overloading to reduce spillage during ore loading/unloading and hauling.

• A water spray dust suppression system will be used at the primary crusher bin during truck dumping of raw ore.

• All conveyors will incorporate wind covers as necessary.

• Freefall height during ore/waste stockpiling will be limited.

Soil Stripping • Access tracks used for soil stripping during the loading and unloading cycle will be watered.

• Soil stripping will be limited to areas required for mining operations.

Drilling • Dust aprons will be lowered during drilling for collection of fine dust.

• Water injection or dust suppression sprays will be used when high levels of dust are being generated.

Blasting • Fine material collected during drilling will not be used for blast stemming.

• Adequate stemming will be used at all times.

Equipment Maintenance

• Emissions from mobile equipment exhausts will be minimised by the implementation of a maintenance programme to service equipment in accordance with the equipment manufacturer specifications.

After: North Limited (1998)

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5.2 DUST CONTROL EQUIPMENT Table 7 presents the equipment that will be used to minimise Project dust generation.

Table 7 Dust Control Equipment

Equipment Type Typical Control Area

Water Trucks • Haul roads and exposed trafficked surfaces and all construction sites

Water Sprays • Ore crusher, product conveyors and conveyor feed points on stockpiles

Dust Collection Systems • Drill rigs

Hoods/Covers • Coarse ore stockpile

• Conveyors After: North Limited (1998)

An additional control measure that has been adopted for the Project is the use of a baghouse and associated collection hood/ducting to filter off-gas emissions (ie. to remove dust particles) from the gold room doré melt furnace. Particulate material collected by the baghouse will be returned to the melt furnace periodically (SNC Lavalin, 2003). This control method reduces the potential for any minor environmental emissions from the gold smelting process and maximises the retention of gold product. In accordance with Consent Condition 6.2(i) Barrick will maintain and use sufficient equipment to apply dust suppression water to unsealed and trafficked areas at a rate which minimises dust emissions (Tables 4, 5 and 6). Dust control equipment will be maintained in accordance with a site maintenance schedule that is based on equipment manufacturer’s specifications. The EPA does not recommend the description of specific rates of dust control watering or treatment of stockpiles in a DMP (EPA, pers. comm., 5 June 2003). Suitable rates of application of dust suppression water will be determined on an ongoing basis through on-site experience and will be largely related to soil types, variability in mine traffic volumes and meteorological conditions (for example, higher watering rates will be applied on hot, dry, windy days when large numbers of vehicles are trafficking massive-structured soil types than on wet days). Specific application rates are not prescribed in this DMP due to the potentially high day to day variability in weather conditions. It will be the responsibility of the Construction or Operational Manager (in co-operation with the Environmental Manager) to assess and implement suitable rates of water application to minimise dust emissions from trafficked and unsealed areas.

5.3 STOCKPILE SURFACE TREATMENT In accordance with Consent Condition 6.2(iii), Barrick will treat all stockpiles (eg. apply dust suppression and/or revegetate) as necessary to minimise windblown dust emissions (Table 5). As above, specific dust suppression activities will be determined by the Construction or Operational Manager in co-operation with the Environmental Manager. Measures to control wind-borne dust and sediment runoff from stockpiles include the following: (i) stripping and placement of soil stockpiles at appropriate moisture conditions whenever possible;

(ii) watering of stockpiles during construction when conditions indicate the need;

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(iii) the application of mulch over completed soil stockpiles and monitoring the rapid revegetation of soil stockpiles (either unassisted or assisted, via the application of seed, fertiliser and water) to promoted rapid cover and as a consequence, erosion control;

(iv) construction of stockpiles of appropriate height and batter angles; and

(v) minimisation of runoff to stockpile areas. The control of wind-borne dust along the pipeline and borefield areas includes the regular inspection of works and any stockpile areas and rapid enactment of any remedial or response measures with respect to dust and soil/sediment control.

5.4 REHABILITATION Further to the above controls, rehabilitation works will be undertaken progressively as construction activities and mining proceed, in accordance with Consent Condition 3.6 and Section 5 of the EIS. Rehabilitation will be undertaken promptly in accordance with a progressive rehabilitation programme. The rehabilitation programme general principles include (North Limited, 1998): (i) The rehabilitation of Project landforms is to be progressive and conducted in accordance with

approved, verified plans which are to be updated annually.

(ii) The stability of newly prepared (ie. topsoiled) landforms prior to the establishment of long term vegetation is to be protected via the construction of moisture-retaining graded drains, water-holding structures (eg. surface depressions) and, where appropriate, the use of authorised hybrid cover crops to provide initial erosion protection.

(iii) Rehabilitation of the outer embankments of the tailings storages to be grassed during processing operational years, reducing habitat opportunities for avifauna.

(iv) Endemic groundcover, understorey, and tree seed and seedlings would be cultivated and utilised.

(v) The annual rehabilitation programme and budget is to be prepared by a site team incorporating the Project’s senior management.

Rehabilitation works will be detailed in the Mining Operations Plan (MOP) in accordance with the requirements of the DMR (DMR, 2002). The MOP describes all mining and mining related activities, rehabilitation plans and land use outcomes over the MOP period (maximum 7 years). The MOP must be in a format endorsed by the DMR and must contain plans and text which identify and define the area(s) proposed to be disturbed, mining and rehabilitation method(s) to be used and progressive rehabilitation schedules. For each area to be rehabilitated, the MOP will describe, where relevant (DMR, 2002): • physical and chemical characteristics of mining and processing waste of emplaced material

relevant to rehabilitation;

• method of land shaping;

• characteristics of all cover material including sealing/drainage layers, subsoil/topsoil;

• thicknesses of cover layers and methods of laying and compaction;

• drainage and erosion control consistent with material characteristics or erosion risk;

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• final landform profile and slopes;

• soil treatment;

• vegetation species and methods of their establishment;

• the extent to which agreed rehabilitation outcomes and land use have been met; and

• maintenance activities/requirements. In accordance with Consent Condition 6.2(ii), effective rehabilitation will be ensured by: • the implementation of the rehabilitation programme in accordance with the above general

principles;

• rehabilitation maintenance work;

• rehabilitation monitoring activities; and

• compliance with DMR’s Mining Rehabilitation and Environmental Management Process (which includes the above DMR MOP and annual reporting requirements [Section 10]) (DMR, 2002).

Where practicable, disturbed areas will be seeded and stabilised with appropriate groundcover immediately following construction, to provide surface stability and an effective means of controlling dust (Tables 4 and 5). Additional DMR requirements relating to rehabilitation and/or dust control are included in the Mining Lease (ML 2000) conditions. Relevant conditions are provided in Section 1.

It will be the responsibility of the Environmental Manager in co-operation with the Construction or Operational Manager to meet the requirements of the DMR with regard to rehabilitation and dust control.

6 ADDITIONAL MODIFICATION OF MINING OPERATIONS TO MINIMISE DUST EMISSIONS

6.1 REQUIREMENT FOR ADDITIONAL MODIFICATIONS OF OPERATIONS With the implementation of the air quality safeguards and controls outlined above, the distance from operational areas of any bird breeding or native flora areas and given extent of Barrick-owned land surrounding the Project (Figure 2), negligible air quality impacts are anticipated at non-Company owned residences or at bird breeding or native flora areas. Notwithstanding, there may be occasions when additional modifications to mining operations may be required to further minimise Project dust emissions due to a particular emission issue. For example: • a short term dust generation event – eg. excessive dust emissions under unfavourable

meteorological conditions such as a hot, dry and windy day; or

• an amenity criteria exceedance – eg. in the event that the air quality monitoring programme indicates a continuing or episodic Project related exceedance of EPA amenity criteria at a non-Company owned residence or a bird breeding/native flora monitoring area.

Management procedures for modifying the mining operation to address these issues are provided below and are illustrated on Figure 4. Examples of applicable control methods which would be implemented during these procedures to minimise potential dust emissions are provided in Tables 4, 5 and 6.

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SOURCE IDENTIFICATION & PREDICTION

Identification of the mining activities to be conducted andthe potential for dust generation issues given the

meteorological and general environmental conditions.Review of wind speed and direction trigger for modification

(5.6m/s and southerly wind)

MODIFICATION STRATEGY

Determination of the appropriate modificationto be implemented.(Refer to Table 9)

IMPLEMENTATION

Implementation of dust control modification selected inthe modification strategy phase.

REVIEW

The effectiveness of the dust control modification will beassessed utilising visual assessment and components ofthe air quality monitoring programme and assessment

against air quality criteria.

AMENITY CRITERIA ASSESSMENT

Assessment of the results of the dust depositionmonitoring programme against EPA amenity criteria

and potential causes of any elevated dust levels.

STANDARD PROCEDURE AMENITY CRITERIA PROCEDURE

If further controls are required

FIGURE 4

Dust Management Procedures

S o i l S t r i p p i n g M a n a g e m e n t P l a nD u s t M a n a g e m e n t P l a n

HAL-02-07 RMP Dust_005A

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6.2 DUST MANAGEMENT PROCEDURES

6.2.1 Standard Management Procedure The standard management procedure is to be implemented to minimise dust emissions from day-to-day Project activities. Implementation of the procedure will be the responsibility of the Construction or Operational Manager in cooperation with the Environmental Manager. When considering potential dust generation issues at the Project, the following should be considered by the Operational Manager in cooperation with the Environmental Manager: • The nearest non-company owned residence is located approximately 3.5 km north of the Project

ML at “Coniston” (Figure 3).

• The major bird breeding areas associated with Lake Cowal occur in the wooded and vegetated parts to the north of the lake viz. in the Lignum/River red Gum expanses some 4.5 km to the north of the Project area (Resource Strategies et. al., 1997).

• Soil erosion or erosion of stockpiles by winds begins to occur at windspeeds in excess of 5.4 metres per second (m/s) (Quality Urban Air Review Group [QUARG], 1996).

• Baseline meteorological data which indicates that the Project area is strongly influenced by winds from the south-west. Wind speeds during the year are generally moderate and usually range between 6 and 10 kilometres per hour (km/hr) (1.67 to 2.77 m/s), increasing up to 20 km/hr (5.54 m/s) in summer during the afternoons (North Limited, 1998). The Project air quality safeguards and control measures outlined in Section 5 were developed to achieve suitable dust control under this range of conditions.

The standard management procedure includes the following: Source Identification and Prediction The first step of the standard management procedure involves identification of the mining activities that will be conducted and the potential for dust generation. The following should be considered: • the methods and types of equipment that will be used;

• the timing of the dust generating activity;

• the location of the activity (in relation to surrounding topography and landuse);

• the prevailing climatic conditions, including current conditions (Section 7.1) and weather forecasts; and

• the environmental conditions Including lake water levels, season and bird breeding activities.

In addition, if hourly average wind speeds on site are greater than 5.6 m/s (20 km/hr) from the south and general environmental conditions are conducive to dust generation (eg. hot and dry), the Environmental Manager or his/her delegate will be required to review dust generation levels on-site, and assess the requirement for implementing additional modifications to the mining operation to minimise dust emissions, particularly from exposed areas. If the source identification and prediction step indicates a requirement to modify the operation to reduce dust emissions, a modification strategy will be required.

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Modification Strategy This component involves determination of how the mining operation will be modified to include additional dust control and management methods to minimise dust emissions, based on the results of the identification stage. The Operational Manager in cooperation with the Environmental Manager may adopt a range of modifications to the mining operation. Typical modifications that can be adopted are outlined in Table 8, however, additional modification measures may also be adopted as required.

Table 8 Modifications to Dust Generating Activities

Project Component Modification

General Exposed Areas Increased watering of exposed surfaces via water trucks or other methods as required.

Stockpiles Activating or increasing rates of water application at fixed water sprays on stockpiles and/or transfer points.

Ancillary Activities Temporary cessation of ancillary or non essential on-site dust generating activities (eg. soil stripping).

Notwithstanding the modification to activities, the general air quality safeguards and controls described in Section 5 (Tables 4, 5 and 6) should continue to be implemented. Implementation This stage of the procedure involves implementation of the measures selected in the modification strategy phase. Review The Operational Manager in cooperation with the Environmental Manager would continue to implement these modifications until the conditions that led to the requirement for the modification improve (eg. wind speeds drop sufficiently). An important component of the procedure is the assessment of the effectiveness of the modifications. The Construction or Operational Manager will regularly review the effectiveness of dust controls using visual assessment of dust generation at source (eg. dust generation levels behind vehicles on haul roads) as well as review of general environmental and meteorological conditions and any results that may be available from the dust monitoring programme (Section 7). The review will be conducted daily or more often as determined by the Environmental Manager. If required, the manager will return to the modification strategy phase of the procedure to implement further controls as necessary.

6.2.2 Amenity Criteria Management Procedure The objective of the amenity criteria procedure is to identify longer term strategies for mitigating dust levels if EPA amenity criteria for dust deposition are exceeded at non-Company owned residences or bird breeding or native flora areas. It is the responsibility of the Environmental Manager to implement the strategy in cooperation with the Construction or Operational Manager. The procedure includes the following components:

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Amenity Criteria Assessment The results of the dust deposition monitoring programme will be assessed against EPA criteria (Section 2) and reported in the AEMR (Section 10). In the event that the EPA criteria is exceeded, an assessment will be conducted to determine: • the timing of elevated dust levels;

• the general location of the elevated dust levels;

• the climatic conditions at the time of the elevated dust levels;

• potential contributing factors to the elevated dust levels; and

• whether the elevated dust levels are attributable to Project activities. The results of this assessment will be provided to the EPA (and NPWS in the event of exceedances at bird breeding or native flora monitoring sites). Modification Strategy This component involves determination of the modification to operations to minimise dust emissions in the medium to long term, based on the results of the amenity criteria assessment stage of the procedure. The additional dust control, management and modification measures to be adopted (Sections 5 and 6.2.1) will be selected with consideration of: • mine activities scheduled for the next phase of construction/operation;

• possible reasons for previous elevated dust levels;

• additional modifications in the form of control methods or operational changes which could be adopted;

• control equipment that will be utilised; and

• the location of current and future dust generating activities. Implementation This stage of the procedure involves implementation of the dust control and management methods selected in the modification strategy process. Review The effectiveness of the additional dust control and management measures adopted will continue to be assessed against the EPA criteria in accordance with the monitoring programme (Section 7). If required, the Environmental Manager will return to the management strategy phase of the procedure in consultation with the EPA (and NPWS if required). This DMP presents management procedures to minimise potential dust related impacts at the outset of the Project. The development of any additional dust control measures (including modifications to Project activity) is expected to be an iterative process, based on specific issues, observations and empirical data.

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7 AIR QUALITY MONITORING PROGRAMME The existing Project air quality monitoring programme utilises a network of dust deposition gauges (Figure 3). Dust deposition gauges are analysed monthly for ash content, combustible matter and insoluble solids. Levels of metals in the dust (ie. aluminium, arsenic, cadmium, lead, selenium, zinc and copper) are also analysed at six monthly intervals. Additionally dust levels outside of the Project MLA area will be monitored to aid in the continued improvement of dust control methods. The primary objective of dust control at the Project is to limit the Project air quality emissions to within acceptable levels as defined by the air quality criteria detailed in Section 2. It will be the responsibility of the Environmental Manager to implement the monitoring programme prior to the commencement of construction and to ensure monitoring is conducted in accordance with applicable standards and guidelines as described in Sections 7.2 and 7.3. The air quality monitoring programme for the Project has been formulated from: • consent condition requirements; • results of baseline studies conducted for the EIS; and

• consideration of the potential impacts resulting from the Project. The monitoring programme will be used to assess compliance with consent conditions and to review dust management strategies. In accordance with Consent Condition 6.1(a) the location of all monitoring sites (dust deposition and TSP) has been determined in consultation with the EPA (EPA, pers. comm., 5 June 2003) and NPWS (NPWS, pers. comm., 21 May 2003). In accordance with Consent Condition 8.3, the following monitoring programme has been developed to “monitor dust deposition rates and concentrations of total suspended particulates (TSP) for the life of the mine, including monitoring impacts of dust on any surface water within the high water mark of Lake Cowal.” In accordance with Consent Condition 8, the air monitoring programme will be “revised/updated annually, unless otherwise directed by the Director-General, to reflect changing environmental requirements, significant changes in technology/operational practices and results from monitoring conducted”.

7.1 METEOROLOGY In accordance with Consent Condition 8.1, an on-site meteorological station will provide data to be used for predicting dust impacts on nearby residences and bird breeding areas. An automated meteorological station is currently located at the exploration office and records rainfall, wind speed, wind direction and temperature. The station will be relocated to continue to monitor meteorological conditions during Project operations. When used in conjunction with the air quality monitoring results, meteorological data (in particular, wind speed, wind direction and rainfall) will provide useful information for the management of dust emissions (Section 6) and review of dust management practices.

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7.2 DUST DEPOSITION GAUGES A network of 15 static dust gauges will be used to monitor dust deposition in the vicinity of the Project during construction and operations (Figure 5). In accordance with Consent Condition 6.1(a) and (c), 8.3(a) and 8.3(b) dust deposition monitoring sites will be located: • at Gumbelah Homestead (DG6) (Consent Condition 6.1(a));

• within the high water mark of Lake Cowal (DG4 and DG5) (Consent Condition 8.3(b));

• proximal to known bird breeding areas in the north of Lake Cowal (DG2 and DG3) (Consent Condition 6.1(a)); and

• within native flora areas (DG4, DG8, DG9 and DG10) (Consent Condition 6.1(a)). These dust monitoring sites have been located and agreed in consultation with the EPA (EPA, pers. comm., 5 June 2003) and NPWS (NPWS, pers. comm., 21 May 2003). In addition, dust deposition monitoring will be continued at Site 52. Site 52 is the only EIS baseline monitoring site which is not located directly within Project infrastructure disturbance areas. Sites 51 and 54 are located within disturbance areas and continued monitoring at these locations is not practical or required given the range of monitoring sites proposed. Dust deposition monitoring at the sites established to continue the EIS baseline monitoring programme (Section 3.2.1 and Figure 3) will continue (excluding sites 51 and 54). A summary of the dust deposition monitoring sites agreed in consultation with EPA (EPA, pers. comm., 5 June 2003) and NPWS (NPWS, pers. comm., 21 May 2003) is provided in Table 9 along with the rationale for site location.

Table 9 Dust Monitoring Sites and Rationale

Dust Gauge Site Location Rationale

DG 1 Coniston residence

DG 2 Bird breeding area

DG 3 General Monitoring Site (proximal to bird breeding area)

DG 4 Native flora area and Bird Breeding Area (Lake Cowal)

DG 5 Lake Cowal

DG 6 Gumbelah residence

DG 7 Lake Cowal residence

DG 8 Native flora area

DG 9 Hillgrove residence, native flora area

DG 10 Native flora area

McLintock’s Shed General monitoring site

Site Office General monitoring site

Site 52 Continuation of baseline monitoring prior to development consent

Lakeside General monitoring site

I5 General monitoring site

Dust deposition monitoring will continue to be conducted for the life of the mine in accordance with procedures established by the EPA (eg. EPA (2000) Approved Methods for the Sampling and Analysis of Air Pollutants in New South Wales) which sets out the methods to be used for sampling and analysing air pollutants in NSW for statutory purposes (Appendix A).

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Creek

Bland

San

dy

NerangCowal

Wamboyne

Mountain

Burcher

-R

ailway

West

WyalongCOWAL

GOLDPROJECT

Bogeys

Island

Open Pit

Northern

Tailings Storage

Southern

Tailings Storage

NorthernWaste

Emplacement

SouthernWaste

Emplacement

Ore Stockpile andProcess Plant Area

‘Coniston’

‘Gumbelah’

‘Lakeside’

‘Lake Cowal'

‘Hillgrove’

McLintock's

Shed

T3

DG5

DG1

DG2

DG3

DG6

DG7DG9

DG8

HV1

DG10

5I

Site 52

Site Office

DG4

540

000

E

535

000

E

545

000

E

6 275 000 N

6 270 000 N

6 290 000 N

6 285 000 N

545

000

E

6 280 000 N

6 275 000 N

6 280 000 N

ML1535

DG4

LEGEND

Barrick-owned Land

Mining Lease Boundary

Dust Deposition Gauge

TSP High Volume Sampler

Meteorological Station

Transect Area used in Waterbird

Monitoring Surveys �

0 2

Kilometres

4

S o i l S t r i p p i n g M a n a g e m e n t P l a nD u s t M a n a g e m e n t P l a n

T3

Note: T3 is a monitoring transect used for�

waterbird monitoring. The main birdbreeding areas are located in the northernparts of Lake Cowal.

FIGURE 5

Dust Monitoring Locations

HAL-02-07 RMP Dust_002A

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The siting of individual dust monitoring sites will be undertaken in accordance with Australian Standard (AS) 2922 Ambient Air - Guide for the Siting of Sampling Units (Appendix B) which sets out the process for selection of monitoring sites and positioning the sampling units, and AS 3580.10.1-1991 - Methods for sampling and analysis of ambient air - Determination of particulates - Deposited matter - Gravimetric method (Appendix C). For dust gauges Sections 8 and 9 of AS 2922 and Section 7 of AS 3580.10.1 relevantly require: • The site shall be level ground, free, as far as practicable, from foreign sources of pollution such

as chimneys, traffic, incinerators, trees, dusty ground and road traffic. If a local foreign source exists in the area, it shall be noted and mapped.

• The gauge to be located at least 5 m from the nearest obstacle.

• There should be unrestricted airflow of 360o around the sampling site.

• There should be a clear sky angle of 120o above the sampling inlet.

• The height of the funnel aperture above the surface of the immediate surrounding area shall be 2 m (±0.2 m) and the funnel aperture plane should be horizontal.

• In general, the period of exposure shall be 30 (±2) days. All collection and analysis of dust gauge samples will be conducted in accordance with AS 3580.10.1 which sets out the principles, reagents, apparatus, sampling procedures, results calculations and precision, test report format and diagrams of sampling equipment for dust deposition monitoring (Appendix C). Dust deposition samples will be analysed monthly for ash content, combustible matter and insoluble solids. The dust deposition results will be compared with the criteria presented in Section 2. All dust deposition monitoring results will be reported in the AEMR (Section 10).

7.2.1 Analysis of Metals in Dust Samples In the majority of situations, dust produced by mining operations is chemically inert, consisting of particles of exposed soil and rock (Environment Australia, 1998). However, there is a perception that dust generated from the Project could potentially contain elevated levels of heavy metals that could adversely impact the water quality of Lake Cowal. This issue arose in submissions to the EIS and at the Commission of Inquiry. In order to address the concern and as a continuation of baseline analysis, composite dust samples will be analysed for select metals (ie. aluminium, arsenic, cadmium, lead, selenium, zinc and copper) at six monthly intervals for comparison to average crustal abundance levels (Bowen, 1979). The concentrations of metals collected in dust gauges during mining operations will be compared to the baseline dust monitoring metals results (Section 3).

7.2.2 Dust Deposition Monitoring within Lake Cowal In accordance with Consent Condition 8.3(b), Site DG5 has been initially positioned near the centre of Lake Cowal so that it remains within the surface water area under a range of lake water level conditions (currently dry). However, if access to this site for collection of data proves difficult under high water levels, an alternative site would be agreed with regulatory authorities. Monitoring at DG5 and other dust deposition gauges located in and around the lake (Figure 5) will provide results representative of potential dust impacts on any surface waters within the high water mark of Lake Cowal.

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7.2.3 Surface Water Monitoring Programme In addition to the dust monitoring programme outlined above, surface water quality monitoring in Lake Cowal will be undertaken to assess the impacts of the Project on lake waters. Analysis of surface water monitoring results in conjunction with dust deposition monitoring data will provide for monitoring of the potential impacts of dust on any surface water within the high water mark of Lake Cowal in accordance with Consent Condition 8.3(b). For example, the relative dust deposition results at sites DG3 and Site 52 (Figure 5) will allow comparison of dust deposition levels within the high water mark of Lake Cowal, both immediately adjacent to the mine and at the opposite side of the lake. If surface water is present, water monitoring results from water quality monitoring sites adjacent to the mine and at the opposite side of the lake can similarly be compared and any differences in water quality examined in light of the dust monitoring data (including metals concentrations in dust and surface waters). A description of the surface water monitoring programme components relevant to monitoring of potential dust impacts on Lake Cowal waters is presented below. The locations, frequency and parameters/analytes of surface water monitoring within Lake Cowal at its associated watercourses that are relevant to the dust monitoring programme are summarised in Table 10. The full surface water monitoring programme is outlined in the Surface Water, Groundwater, Climate and Aquatic Biological Monitoring Programme (SGWMP) and is consistent with the EIS (North Limited, 1998).

Table 10

Project Surface Water Monitoring Programme

Site Project Phase Monitoring Frequency Relevant Parameter/Analyte

Construction Operation

Lake Cowal transect sampling sites (including the Lachlan floodway, irrigation channel, Bland Creek, east shore, Project and control transects

Monthly (when possible) throughout filling and drying cycles

Suspended Solids, Total Dissolved Solids, Turbidity, Depth and Lake water level.

Metals- Aluminium, Arsenic, Cadmium, Copper, Lead, Selenium and Zinc.

Lake inflow sites (including the Lachlan floodway, irrigation channel, Bland Creek and Sandy Creek inflow sites)

Monthly (when possible)

After: North Limited (1998)

Given the ephemeral nature of Lake Cowal, surface water monitoring will not be possible at all times. If Lake Cowal is dry, surface water monitoring will commence after a significant inflow occurs at any of the four inflow sites (Bland Creek, Sandy Creek, irrigation channel and/or Lachlan floodway) or when sufficient water collects in the lake and enables water quality monitoring.

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Water quality monitoring samples will be subject to laboratory analysis at a NATA registered laboratory, with a field test used to determine turbidity. Surface water sample collection, preservation and general maintenance will be in accordance with AS 5667:1998 Water quality – Samples and the SWGMP. The surface water monitoring data will be reported in the AEMR and will be reviewed and revised annually as part of the AEMR review process. Should analysis of relevant surface water monitoring data (Table 10) and data from the dust gauge network indicate adverse effects of Project dust on surface waters within the high water mark of Lake Cowal, additional dust suppression and control measures will be implemented in accordance with the procedures detailed in Section 6.2.

7.3 TOTAL SUSPENDED PARTICULATE HIGH VOLUME SAMPLER The proposed TSP monitoring site is shown on Figure 5. Monitoring will be conducted at HV1 at the ‘Coniston’ Homestead to the north of the Project. The location and selection of a single TSP monitor has been agreed by the EPA (EPA pers. comm., 5 June 2003). The TSP monitor is located at the nearest non-Company owned residence to the Project as the TSP criteria adopted by the EPA were recommended by the National Health and Medical Research Council of Australia as the maximum permissible level of TSP in the air to protect public health in residential environments (Pavel Zib and Associates, 1997). All other non-company owned residences are more than 3.5 km from the Project and monitoring at these distant locations is not warranted given the EIS predicted that the Project would result in only minor exceedances of the dust deposition and TSP criteria outside of the Project MLA area (Pavel Zib and Associates, 1997). The monitoring of TSP will be conducted by high volume sampler in accordance with procedures established with the EPA namely Approved Methods for the Sampling and Analysis of Air Pollutants in New South Wales (Appendix A). TSP will continue to be monitored for the life of the mine unless otherwise agreed by the Director-General. The siting of the monitoring unit will be undertaken in accordance with AS 2922. For TSP high volume samplers Sections 8 and 9 of AS 2922 relevantly require that: • There should be unrestricted airflow of 360O around the sampling site.

• There should be a clear sky angle of 120O above the sampling inlet.

• The sampler shall be 1 to 1.5 m above the ground surface.

• Sampler located at least 20 m from trees.

• No boiler or incinerator flues nearby.

• Located at least 50 m from roads.

• Power supply and vehicular access should be available. TSP will be measured to assess fluctuations in particulate matter concentrations on a six day cycle (ie. a 24 hour sample is collected every six days). The high volume sampler will be fenced if necessary to exclude stock. All sample collection and analysis will be conducted in accordance with AS 2724.3-1984: Ambient Air – Particulate Matter – Determination of Total Suspended Particulates (TSP) – High Volume Sampler Gravimetric Method (Appendix D). AS 2724.3 sets out the principles, apparatus, calibration, procedures, results calculations and accuracy, test report format and diagrams of sampling equipment for TSP high volume samplers. In addition to the dust deposition and TSP monitoring programmes, visual assessments of dust generating activities will be periodically conducted by the Environmental Manager or his/her delegate to identify the major dust generating activities on-site (Section 6).

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7.4 REVIEW OF MONITORING PROGRAMMES

The results of the meteorological, TSP and dust deposition monitoring will continue to be maintained in a database for examination and assessment. This data will be used to analyse relationships between short-term variations in dust levels and the number and distribution of any dust-related complaints. Results of the analysis will then be used in the review of the monitoring programme to determine if further monitoring is necessary (eg. additional dust deposition gauges) or whether the programme can be modified in consultation with the EPA to monitor dust deposition only (no TSP). The results of this review process will be reported annually in the AEMR (Section 10). An IEA will be conducted in accordance with Consent Condition 8.8. The condition is reproduced below:

8.8 Third Party Monitoring/Auditing (a) An Independent Environmental Audit shall be completed:

• six monthly during construction;

• 12 months after commencement of ore processing;

• then every three years thereafter until decommissioning of the mine and ore processing operations respectively, or as otherwise directed by the Director-General.

The Applicant shall conduct an environmental audit of the mining and infrastructure areas of the development in accordance with ISO 14010 - Guidelines and General Principles for Environmental Auditing, and ISO 14011 - Procedures for Environmental Auditing (or the current versions), and in accordance with any specifications required by the Director-General. Copies of the report shall be submitted by the Applicant to the Director-General, BSC, EPA, DLWC, DMR, NPWS and CEMCC within two weeks of the report’s completion for comment.

(i) The audit shall:

a. assess compliance with the requirements of this consent, licences and approvals; b. in the event of any non-compliance, report on the effectiveness of the environmental

management of the mine as it may relate to the area of non-compliance; c. be carried out at the Applicant’s expense; and d. be conducted by a duly qualified independent person or team approved by the Director-

General in consultation with BSC and CEMCC. (ii) The Director-General may, after considering any submission made by the relevant

government agencies, BSC and CEMCC on the report, notify the Applicant of any requirements with regard to any recommendations in the report. The Applicant shall comply with those reasonable requirements within such time as the Director-General may require.

(b) Independent Monitoring Panel

(i) The Applicant shall at its own cost establish an Independent Monitoring Panel prior to commencement of construction. The Applicant shall contribute $30,000 per annum for the functioning of the Panel, unless otherwise agreed by the Director-General. The annual payment shall be indexed according to the Consumer Price Index (CPI) at the time of payment. The first payment shall be paid by the date of commencement of construction and annually thereafter. Selection of the Panel representatives shall be agreed by the Director-General in consultation with relevant government agencies and the CEMCC. The Panel shall at least comprise two duly qualified independent environmental scientists and a representative of the Director-General.

(ii) The panel shall:

a. provide an overview of the independent audits required by condition 8.9 above;

b. regularly review all environmental monitoring procedures undertaken by the Applicant, and monitoring results; and

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c. provide an Annual State of the Environment Report for Lake Cowal with particular reference to the on-going interaction between the mine and the Lake and any requirements of the Director-General. The first report shall be prepared one year after commencement of construction. The report shall be prepared annually thereafter unless otherwise directed by the Director-General. Copies of the report shall be provided to those parties which receive the AEMR (condition 9.2) and shall be made publicly available at Bland Shire Council within two weeks of the report’s completion.

8 STAKEHOLDER CONSULTATION

8.1 COMMUNITY ENVIRONMENTAL MONITORING AND CONSULTATIVE COMMITTEE A Community Environmental Monitoring and Consultative Committee (CEMCC) will be set up for the Project in accordance with Consent Condition 8.7. The condition is reproduced below:

8.7 Community Consultative Committee Community Environmental Monitoring and Consultative Committee (CEMCC) The Applicant shall: (i) establish a Community Environmental Monitoring and Consultative Committee and ensure that the

first meeting is held before the commencement of construction works. Selection of representatives shall be agreed by the Director-General and the appointment of an independent Chairperson shall be to the satisfaction of the Director-General in consultation with the Applicant and BSC. The Committee shall comprise two (2) representatives of the Applicant (including the Environmental Officer), one (1) representative of BSC, one (1) representative of the Lake Cowal Environmental Trust (but not a Trust representative of the Applicant), four community representatives (including one member of the Lake Cowal Landholders Association), to monitor compliance with conditions of this consent and other matters relevant to the operation of the mine during the term of the consent.

Representatives from relevant government agencies (including DUAP) may be invited to attend meetings as required by the Chairperson. The Committee may make comments and recommendations about the implementation of the development and environmental management plans. The Applicant shall ensure that the Committee has access to the necessary plans for such purposes. The Applicant shall consider the recommendations and comments of the Committee and provide a response to the Committee and Director-General.

(ii) The Applicant shall, at its own expense:

a) nominate two (2) representatives to attend all meetings of the Committee;

b) provide to the Committee regular information on the progress of work and monitoring results;

c) promptly provide to the Committee such other information as the Chair of the Committee may reasonably request concerning the environmental performance of the development;

d) provide access for site inspections by the Committee;

e) provide meeting facilities for the Committee, and take minutes of Committee meetings. These minutes shall be available for public inspection at BSC within 14 days of the meeting.

(iii) The Applicant shall establish a trust fund to be managed by the Chair of the Committee to facilitate the functioning of the Committee, and pay $2000 per annum to the fund for the duration of gold processing operations. The annual payment shall be indexed according to the Consumer Price Index (CPI) at the time of payment. The first payment shall be made by the date of the first Committee meeting. The Applicant shall also contribute to the Trust Fund reasonable funds for payment of the independent Chairperson, to the satisfaction of the Director-General.

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(ix) By year 5 of mining operations the Applicant shall, in consultation with CEMCC, identify and discuss post mining issues, particularly in relation to reduced employment and consequent impacts on West Wyalong, and develop a plan for the phase out of the mine workforce. The plan will be reviewed during the year of mining operations following the scale down of the year 8 mining operation workforce. The impacts of the year 8 scale down shall be monitored by the Applicant and results used in planning for full mine closure.

(x) The Applicant shall, in consultation with the CEMCC, develop appropriate strategies to support activities which promote special interest tourism related to the co-existence of mining and the Lake Cowal environment.

The CEMCC will comprise representatives of Bland Shire Council (BSC), Lake Cowal Environmental Foundation (LCEF), two Barrick representatives and four community representatives including one from the Lake Cowal Landholders Association. The CEMCC will provide opportunities for members of the community to attend CEMCC meetings to discuss specific issues relevant to them, including dust-related issues. This will be achieved by landholders making a request to the CEMCC regarding a particular issue, or by the landowner registering a complaint in the complaints register. Landowners who register complaints will be invited to join in discussion of the issue at the next CEMCC meeting. Items of discussion at these meetings will include mine progress, reporting on environmental monitoring, complaints, rehabilitation activities and any environmental assessments undertaken.

9 COMPLAINTS AND PROPERTY ACQUISITION IN THE EVENT OF DUST AFFECTATION

A process for the handling of complaints, resolution of disputes and land acquisition in the event of affectation is provided below in accordance with the requirements of Project consent conditions and to facilitate prompt and comprehensive responses to any community concerns that relate to dust.

9.1 COMPLAINTS REGISTER A complaints register will be maintained by the Environmental Manager in accordance with Consent Condition 10.1(a). The condition is reproduced below:

10.1 Community Consultation (including Aboriginal community) (a) Complaints The Environmental Officer (refer condition 3.1) shall be responsible:

(i) for receiving complaints with respect to construction works and mine operations on a dedicated and publicly advertised telephone line, 24 hours per day 7 days per week, entering complaints or comments in an up to date log book, and ensuring that a response is provided to the complainant within 24 hours; and

(ii) providing a report of complaints received every six months throughout the life of the project to the Director-General, BSC, EPA, DMR, and CEMCC, or as otherwise agreed by the Director-General. A summary of this report shall be included in the AEMR (condition 9.2(a)).

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Information recorded in the complaints register with respect to each complaint will include: • date of complaint;

• name, address and telephone number of complainant;

• nature of complaint; and

• response action taken to date. An initial response will be provided to the complainant within 24 hours. Preliminary investigations into the complaint will commence within 48 hours of complaint receipt. In the event that the complainant is not satisfied with Barrick’s response to the complaint, or exceedance of EPA criteria has been demonstrated, an independent investigation will be undertaken (Section 9.2).

9.2 INDEPENDENT INVESTIGATION PROCESS Consent Condition 11.1(a) outlines the independent investigation process in the event that a landowner considers dust levels are in excess of relevant EPA criteria at their dwelling. The consent condition is reproduced below. Consent Conditions 11.1(b) to (e) are reproduced in Section 9.3.

11.1 Area of Affectation - Land Acquisition (including resolution of disputes)

Note: In Condition 11.1 (a)-(e) "land" means the whole of a lot in a current plan registered at the Land Titles Office as at the date of this consent.

(a) (i) In the event that landowners consider that noise and/or dust from the Cowal Gold mining

operations at their dwelling(s) is in excess of the criteria set out in this consent or the relevant EPA amenity criteria for noise and/or dust levels, and the Director-General, in consultation with the EPA, is satisfied that an investigation is required, the Applicant shall upon receipt of a written request:

• appoint a qualified independent person to undertake direct discussions with the landowners affected to ascertain their concerns and to plan and implement an investigation to quantify the impact and determine the sources of the effect, and

• bear the cost of the independent investigation and make available plans, programmes and other information necessary for the independent person to form an appreciation of the past, present and future mining operations and their effects on noise and/or dust emissions.

(ii) The investigation is to be carried out by a qualified independent person in accordance with a documented Plan. The Plan shall be designed and implemented to measure and/or compute (with appropriate calibration by measurement) the relevant noise and/or dust levels at the complainant’s dwelling emitted by the current normal mining operations.

(iii) The independent person, the Plan and the timing of its implementation shall be approved by the Director-General, in consultation with BSC, the EPA, the affected landowner and the Applicant. A report of the investigation shall be provided to the Director-General, the EPA, the Applicant and the affected landowner.

(iv) The results of the investigation shall be assessed and reported by the independent person in the light of the mine’s current operations and proposed short, medium and long term development plans.

(v) If the independent noise and/or dust investigation finds that the relevant criteria are being exceeded by noise and/or dust emission from normal mining operations, the Applicant shall:

• modify those areas of the mining operation which are causing the exceedances; or

• undertake other measures, as agreed with the affected landowner, to ameliorate the effects of the impact, within three (3) months or as otherwise directed by the EPA.

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(vi) Within two (2) months after the expiry of the three (3) month period in sub-clause (v) above, and upon written request from the landowner, the Applicant shall arrange for a further independent noise and/or dust investigation to be completed.

(vii) If the investigation in sub-clause (vi) above finds that the relevant noise and/or dust emission levels from normal mine operations exceed relevant amenity criteria, the Applicant shall purchase the property within six months of receipt of a written request from the owner of the affected property.

(viii) Further independent investigations shall cease if the Director-General, in consultation with the EPA is satisfied that the relevant consent limits or EPA amenity criteria are not being exceeded and are unlikely to be exceeded in the future.

In the event that a request to purchase a property is received by Barrick in respect to Consent Condition 11.1(a)(vii) property acquisition would occur (Section 9.3).

9.3 PROPERTY ACQUISITION DUE TO DUST AFFECTATION Consent Condition 11.1(b),(c),(d) and (e) outlines the process for acquisition of a property in the event of demonstrated dust affectation (Section 9.2). The consent condition is reproduced below:

(b) In respect of a request to purchase land arising under Condition 11.1(a), the Applicant shall pay the owner the acquisition price which shall take into account and provide payment for:

(i) a sum not less than the current market value of the owner's interest in the land used for its existing use at the date of this consent who is the occupier and all improvements thereon at this date as if the land was unaffected by the development proposal.

(ii) the owner's reasonable compensation for disturbance allowance and relocation costs within the Bland or Forbes Local Government Areas.

(iii) the owner's reasonable costs for obtaining legal advice and expert witnesses for the purposes of determining the acquisition price of the land and the terms upon which it is to be acquired.

(c) In the event that the Applicant and any owner referred to in Condition 11.1(a) cannot agree within the time limit upon the acquisition price of the land and/or the terms upon which it is to be acquired, then:

(i) either party may refer the matter to the Director-General, who shall request the President of the Australian Institute of Valuers and Land Economists to appoint a qualified independent valuer, suitably qualified in compensation issues, who shall determine, after consideration of any submissions from the land owner and the Applicant, the acquisition price.

(ii) in the event that the independent valuer requires guidance on any contentious legal, planning or other issues, the independent valuer shall refer the matter to the Director-General, who if satisfied that there is need for a qualified panel, shall arrange for the constitution of the panel. The panel shall consist of:

1) the appointed independent valuer,

2) the Director-General, and/or

3) the President of the Law Society of NSW or his/her nominee.

The qualified panel shall, on the advice of the valuer, determine the issue referred to it and advise the valuer.

(d) The Applicant shall bear the costs of any valuation or survey assessment requested by the Director-General in accordance with Conditions 11.1(a) - 11.1(c).

(e) Upon receipt of a valuation, the Applicant shall offer to acquire the relevant land at a price not less than the said valuation. Should the Applicant's offer to acquire not be accepted by the owner within six (6) months of the date of such offer, the Applicant's obligations to such owner and in respect of that property under Conditions 11.1(a) - 11.1(e) above shall cease.

The General Manager or Environmental Manager will manage the above process if required.

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10 REPORTING An AEMR will be prepared in accordance with the requirements of the DMR (Condition of Authority 26 – Section 1) and Project Consent Condition 9.2 and submitted to the Director-General. Consent Condition 9.2 is reproduced below:

9.2 Environmental Reporting Annual Environmental Management Report (AEMR) (i) The Applicant shall, throughout the life of the mine and for a period of at least five years after the

completion of ore processing operations, prepare and submit an Annual Environmental Management Report (AEMR) to the Director-General. The AEMR shall review the performance of the mine against the environmental management plans (refer condition 3.2), Mining Operations Plan (refer condition 2.1), the conditions of this consent, and other licences and approvals relating to the mine. To enable ready comparison with EIS predictions, diagrams and tables, the report shall include, but not be limited to, the following matters:

a) an annual compliance audit of the performance of the project against conditions of this consent and statutory approvals;

b) a review of the effectiveness of the environmental management of the mine in terms of EPA, DLWC, DMR, NPWS, NSW Fisheries, and BSC requirements;

c) results of all environmental monitoring required under this consent or other approvals, which includes interpretation and discussion by a suitably qualified person;

d) from results of fauna monitoring, records of any fauna deaths due to mine operations;

e) a listing of any variations obtained to approvals applicable to the subject area during the previous year;

f) the outcome of the water budget for the year and the quantity of water used from water storages and Bland Creek palaeochannel borefield;

g) rehabilitation report;

h) environmental management targets and strategies for the next year. (ii) In preparing the AEMR, the Applicant shall:

a) consult with the Director-General during preparation of each report for any additional requirements;

b) comply with any requirements of the Director-General or other relevant government agency; and

c) ensure that the first report is completed and submitted within twelve (12) months of this consent, or at a date determined by the Director-General in consultation with DMR.

(iii) The Applicant shall ensure that copies of each AEMR are submitted at the same time to the

Director-General, EPA, DLWC, DMR, DSC, NPWS, NSW Fisheries, the BSC and CEMCC, and be available for public information at the BSC within 14 days of submission to these authorities.

The AEMR will report on the following dust-related issues: • annual average dust deposition results (plotted in g/m2/month) and comparison to the amenity

criteria (Section 2;

• TSP monitoring results and comparison to the EPA criteria (Section 2);

• measures employed to minimise/prevent excessive dust emissions;

• dust-related complaints and amelioration measures undertaken in the event of any confirmed exceedances of EPA criteria;

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• review of the performance of dust control measures and the monitoring programme;

• interpretation and discussion of the air quality monitoring programme results and management measures by a suitably qualified person; and

• CEMCC decisions relating to Project dust issues. The AEMR will be made available to DIPNR, EPA, Department of Sustainable Natural Resources (formerly Department of Land and Water Conservation), DMR, NPWS, NSW Fisheries, BSC the CEMCC and any other interested stakeholders on request.

11 REFERENCES

Bowen, H.J.M. (1979). Environmental Chemistry of the Elements. Academic Press, New York.

Department of Mineral Resources (DMR) (2002). Guidelines to Mining, Rehabilitation and Environmental Management Plans.

Environment Australia (1998). Dust Control – Best Practise Environmental Management in Minning.

North Limited (1998) Cowal Gold Project Environmental Impact Statement. Prepared by Resource Strategies Pty Ltd.

NSW Environment Protection Authority (2000) Approved Methods for the Sampling and Analysis of Air Pollutants in New South Wales.

NSW Environment Protection Authority (2001) Approved Methods and Guidance for the Modelling and Assesment of Air Pollutants in New South Wales.

Pavel Zib and Associates (1997) Assessment of Air Quality for the Proposed Cowal Gold Project at Lake Cowal, NSW. Report prepared for North Limited.

Quality of Urban Air Review Group (1996) Airborne Particulate Matter in the United Kingdom. Third report of the Quality of the Urban Air Review Group, report prepared at the request of the Department of the Environment.

Resource Strategies, CSIRO Wildlife and Ecology, Goldney. D. and Greg Richards and Associates (1997) Cowal Gold Project Species Impact Statement. Report prepared for North Limited.

SNC Lavalin (2003). Cowal Gold Project 6 MTPA Development Plan.

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APPENDIX A

APPROVED METHODS FOR THE SAMPLING AND ANALYSIS OF AIR POLLUTANTS IN NEW SOUTH WALES

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NSW Environment Protection Authority

Approved methods for the samplingand analysis of air pollutants

in New South Wales

About this publicationFor technical inquiries about this document, contact the Science Management Unit of theEPA.

Published by Environment Protection Authority, 59–61 Goulburn Street, Sydney NSW 2000(PO Box A290, Sydney South NSW 1232). Tel: (02) 9995 5000 (switch), 131 555(information & publications); Fax: (02) 9995 5999; E-mail: [email protected]; WWW:http://www.epa.nsw.gov.au/

This document is available on the EPA's website at http://www.epa.nsw.gov.au/air/amsaap/.

It can also be downloaded from this site in PDF format: amsaap.pdf (106 Kb)

The EPA is pleased to allow this material to be reproduced in whole or in part, provided themeaning is unchanged and the EPA is acknowledged as the source, publisher and author ofthe material.

Revision historyFirst published in NSW Gov Gazette 24 December 1998, p10320, see also NSW Gov Gazette15 January 1999, p141.

Revised version NSW Gov Gazette 28 January 2000, p498; further revised version NSW GovGazette 20 July 2001, p5566

EPA 2001/55ISBN 0 7313 2780 2July 2001

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Contents1. Introduction

2. Sample collection and handling

Stationary source monitoring

Ambient air monitoring

3. Methods for sampling and analysis

Table 1: Methods for the sampling and analysis of air pollutants from stationary sources inNSW

A: Test methods prescribed for the purposes of the Clean Air (Plant and Equipment)Regulation 1997B: Other approved methods (OM)C: Continuous emission monitoring system (CEMS) protocols

Table 2: Methods for the sampling and analysis of air pollutants from mobile sources andmotor vehicle fuels in NSW

Table 3: Methods for the sampling and analysis of ambient air pollutants in NSW

A: General methodsB: Specific methods

4. Analytical report

Stationary source monitoring

Ambient air monitoring

5. References

APPENDICES

Generic procedures and definitions that apply to stationary source monitoring andreporting

Test method 17—Determination of soot

Test method 19—Determination of total mass of unburnt organic vapours from vapourdisposal units

Test method 20—Determination of total mass of unrecovered organic vapours from vapourrecovery units

Test method 21—Calculation of vapour pressure

Test method 26—Exhaust and evaporative emissions from spark-ignition motor vehicles

Test method 27—Lead concentration in leaded and unleaded petrol

Test method 31—Observation procedure for excessive air impurities: visible emissions

Other approved method 9—Determination of “coarse” particulates

Test method sources

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1. IntroductionThis document lists the methods to be used for sampling and analysing air pollutants in NewSouth Wales for statutory purposes. The document covers:

• pollutants in emissions from stationary sources, including continuous monitoring ofsuch emissions

• pollutant emissions from motor vehicles

• components in and properties of petroleum products

• pollutants in ambient air.

This document is referred to in:

• the Clean Air (Plant and Equipment) Regulation 1997

• the Clean Air (Motor Vehicles and Motor Vehicle Fuels) Regulation 1997.

It may also be referred to in conditions attached to statutory instruments, such as licences ornotices, issued under environment protection legislation, as defined in the Protection of theEnvironment Administration Act 1991.

Industry has an obligation to ensure compliance with limits specified in the Clean Air (Plantand Equipment) Regulation 1997, the Clean Air (Motor Vehicles and Motor Vehicle Fuels)Regulation 1997 and certain statutory instruments. All monitoring to show compliance mustbe done in one of three ways:

• in accordance with the methods specified in this document

• in accordance with the methods specified in the relevant statutory instrument

• if no method is specified in either this document or the statutory instrument, in amanner approved by the EPA in writing before any tests are conducted.

In exceptional circumstances, the EPA may approve the use of alternative methods to thoseprovided here. An application for approval of a test method as an equivalent alternative to atest method in this document (the 'approved method') must be made in writing to the ChiefScientist, Environment Protection Authority.

The application must:

1. show that there are exceptional circumstances that justify the use of a method otherthan the approved method

2. give details of the alternative method for which approval is sought

3. show that the alternative method is scientifically sound

4. show that the alternative method would produce results comparable to those producedby the approved method.

The EPA will not approve an alternative test method unless it is satisfied that the applicationfor approval gives adequate details of the proposed alternative method as listed above.

Any other method, which has been approved by the EPA in accordance with the approvalprocedures set out above as an equivalent alternative to a test method of a particular numberin this document, is prescribed as a test method of that same number.

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2. Sample collection and handling

Stationary source monitoring

Collect, handle and preserve samples according to the relevant test method. Collect them atthe locations determined in accordance with the relevant regulation or specified in thestatutory instrument, as the case may be. If the regulation does not provide for determinationof the locations or if no locations are specified in the instrument, collect them from suchlocations that they are representative of the total or known portion of the source emissions.

Whenever a United States Environmental Protection Agency (USEPA) test method refers toMethod 1—Sample and Velocity Traverses for Stationary Sources, Standards Association ofAustralia, AS 4323.1-1995 must be substituted. Whenever a USEPA test method refers toMethod 5—Determination of Particulate Emissions from Stationary Sources, AS 4323.2-1995must be substituted.

When determining compliance with the emission limits for oxides of nitrogen in the CleanAir (Plant and Equipment) Regulation 1997, sample during the normal operation of the plantor equipment being tested, not during start-up or shutdown operations. (Start-up is when theplant or equipment is brought up to its normal operating conditions from inactivity byfollowing a prescribed series of steps or operations. Shutdown is when the plant orequipment is taken out of service from normal operation to inactivity by following aprescribed series of steps or operations.)

Ambient air monitoring

When siting ambient air sampling units, follow AS 2922-1987. Monitoring sites are classifiedinto three types: peak, neighbourhood or background. When selecting a monitoring site, youneed to consider many parameters, including possible chemical or physical interference,locality, terrain, services and local activities. Try to locate wind speed and direction meterswith the ambient air monitoring instruments unless appropriate wind data are available fromanother nearby source.

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3. Methods for sampling and analysisAnalyses should be carried out by a laboratory accredited to perform them by an independentaccreditation body acceptable to the EPA, such as the National Association of TestingAuthorities (NATA).

Methods approved by the EPA for specific analytes and parameters are listed in Tables 1 to 3.In most cases, standard methods are referenced, with additional guidance or clarificationgiven if needed. Where there is no suitable published method, a complete description of theapproved method is given. Refer to Test method sources, for the organisations that publish theapproved methods.

Refer to Generic procedures and definitions that apply to stationary source monitoring andreporting.

Table 1: Methods for the sampling and analysis of air pollutants from stationary sources inNSW

A: Test methods prescribed for the purposes of the Clean Air (Plant and Equipment)Regulation 1997B: Other approved methods (OM)C: Continuous emission monitoring system (CEMS) protocols

Table 2: Methods for the sampling and analysis of air pollutants from mobile sources andmotor vehicle fuels in NSW

Table 3: Methods for the sampling and analysis of ambient air pollutants in NSW

A: General methodsB: Specific methods

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Table 1: Methods for the sampling and analysis of air pollutants from stationary sourcesin NSW

A. Test methods (TM) prescribed for the purposes of the Clean Air (Plant andEquipment) Regulation 1997

MethodNo.

Parameter measured Method

TM-1 Selection of sampling positions AS 4323.1-1995

TM-2 Velocity and volumetric flow rate USEPA (1997) Method 2 or 2C (asappropriate)

TM-3 Sulfur (sulfuric acid mist includingsulfur trioxide)

USEPA (1997) Method 8

TM-4 Sulfur (sulfur dioxide) USEPA (1997) Method 6–6C (as appropriate)

TM-5 Sulfur (hydrogen sulfide) USEPA (1997) Method 15

TM-6 Sulfur in petroleum products ASTM (1998) D4294-98 or ASTM (1998)D2622-98 or ASTM (1995) D129-95

TM-7 & 8 Chlorine and hydrogen chloride USEPA (1997) 26A

TM-9 Fluorine USEPA (1997) Method 13A or 13B (asappropriate)

TM-10 Rate of emissions of fluoride fromaluminium smelters

USEPA (1997) Method 14 or 14A (asappropriate)

TM-11 Oxides of nitrogen USEPA (1997) Method 7–7E (as appropriate)(NOx analysers may be substituted in Method7E provided the performance specifications ofthe method are met); or USEPA (1997)Method 20. Both NO and NOx must be directlymeasured.

TM-12, 13& 14

Hazardous substances (antimony,arsenic, beryllium, cadmium, chromium,cobalt, lead, mercury, manganese,nickel, selenium, tin and vanadium)

USEPA (1997) Method 29 (Analysis for tinand vanadium to be done by InductivelyCoupled Argon Plasma EmissionSpectroscopy (ICAP) as defined in Method29.)

TM-15 Total solid particles AS 4323.2-1995

TM-16 Smoke AS 3543-1989

TM-17 Soot Test method 17

TM-18 Dioxins and furans (polychlorinateddibenzo-p-dioxins and polychlorinateddibenzofurans)

USEPA (1997) Method 23 (Duration ofsampling must be between 6 and 16 hours.Several discrete samples may be taken suchthat the total sampling time is within thespecified range.)

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MethodNo.

Parameter measured Method

TM-19 Volatile organic liquids—total mass ofunburnt organic vapours, displaced bythe transfer of volatile organic liquidsfrom vapour disposal units

Test method 19

TM-20 Volatile organic liquids—total mass ofunrecovered organic vapours, displacedby the transfer of volatile organic liquidsfrom vapour recovery units

Test method 20

TM-21 Volatile organic liquids—calculation ofvapour pressure

Test method 21

TM-22 Moisture content in stack gases USEPA (1997) Method 4

TM-23 Dry gas density/molecular weight ofstack gases

USEPA (1997) Method 3

TM-24 Carbon dioxide in stack gases USEPA (1997) Method 3A

TM-25 Oxygen in stack gases USEPA (1997) Method 3A

B. Other approved methods (OM)

MethodNo.

Parameter measured Method

OM-1 Carbon monoxide USEPA (1997) Method 10

OM-2 Volatile organic emissions USEPA (1997) Method 18 or Method 25–25E(as appropriate)

OM-3 Total or hexavalent chromium emissionsfrom decorative and hard chromiumelectroplating and anodising operations

USEPA (1997) Method 306

OM-4 Total and hexavalent chromiumemissions

California EPA Air Resources Board (1997)Method 425; or USEPA (1996) Method 0061(as appropriate). (Method 0061 is validated fordetermination of hexavalent chromium fromhazardous waste incinerators, municipal wasteincinerators, municipal waste combustors andsewage sludge incinerators.)

OM-5 PM10 emissions USEPA (1997) Method 201 or 201A (asappropriate)

OM-6 Polycyclic aromatic hydrocarbons(PAHs)

California EPA Air Resources Board (1997)Method 429

OM-7 Odour (dynamic olfactometry) Standards Association of Australia DR 99306or CEN European Committee forStandardisation (1997)

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MethodNo.

Parameter measured Method

OM-8 Measurement of gaseous emission ratesfrom land surfaces using an emissionisolation flux chamber (for sampling ofodour from diffuse sources)

USEPA (1986) EPA/600/8-8E/008

OM-9 Determination of “coarse” particulates Other Approved Method 9

C. Continuous emission monitoring system (CEMS) protocols

MethodNo.

Parameter measured Method

CEM-1 Opacity USEPA (1997) Performance Specification 1

CEM-2 Sulfur dioxide and nitrogen oxides USEPA (1997) Performance Specification 2

CEM-3 Oxygen and carbon dioxide USEPA (1997) Performance Specification 3

CEM-4 Carbon monoxide USEPA (1997) Performance Specification 4

CEM-5 Total reduced sulfur USEPA (1997) Performance Specification 5

CEM-6 Flow rate USEPA (1997) Performance Specification 6

CEM-7 Hydrogen sulfide USEPA (1997) Performance Specification 7

CEM-8 Volatile organic compounds USEPA (1997) Performance Specification 8

CEM-9 Gas chromatography USEPA (1997) Performance Specification 9

CEM-10 Extractive Fourier transform infra-redradiation

USEPA (1997) Proposed PerformanceSpecification 15

Note: Any other method, which has been approved by the EPA in accordance with theapproval procedures set out in the introduction to this document as an equivalent alternativeto a test method of a particular number in this document, is prescribed as a test method of thatsame number.

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Table 2: Methods for the sampling and analysis of air pollutants from mobile sourcesand motor vehicle fuels in NSW

Test methods (TM) prescribed for the purposes of the Clean Air (Motor Vehicles andMotor Vehicle Fuels) Regulation 1997

MethodNo.

Parameter measured Method

TM-26 Exhaust and evaporative emissions fromspark-ignition motor vehicles

Federal Office of Road Safety ADR 37/00(1989) or ADR 37/01 (1995). Refer to testmethod 26 for additional guidance

TM-27 Lead concentration in leaded andunleaded petrol

Test method 27

TM-28 Phosphorus concentration in unleadedpetrol

ASTM (1994) D3231-94

TM-29 Research octane number of unleadedpetrol

ASTM (1997) D2699-97

TM-30 Motor octane number of unleaded petrol ASTM (1997) D2700-97

TM-31 Observation procedure for excessive airimpurities: visible emissions

Test method 31

Note: Any other method, which has been approved by the EPA in accordance with theapproval procedures set out in the introduction to this document as an equivalent alternativeto a test method of a particular number in this document, is prescribed as a test method of thatsame number.

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Table 3: Methods for the sampling and analysis of ambient air pollutants in NSW

A: General methodsB: Specific methods

A. General methods for ambient air monitoring (AM)

MethodNo.

Parameter measured Method

AM-1 Guide for the siting of sampling units AS 2922-1987

AM-2 Guide for measurement of horizontalwind for air quality applications

AS 2923-1987

AM-3 Preparation of reference testatmospheres

AS 3580.2.1-1990 or AS 3580.2.2-1990

AM-4 On-site meteorological programguidance for regulatory modellingapplications

USEPA (1987) EPA 450/4-87-013

B. Specific methods for ambient air monitoring

MethodNo.

Parameter measured Method

AM-5 Acid gases AS 3580.3.1-1990

AM-6 Carbon monoxide AS 3580.7.1-1992

AM-7 Fluorides—automated, double papertape sampling method

AS 3580.13.1-1993

AM-8 Fluorides—manual, double filter papersampling method

AS 3580.13.2-1991

AM-9 Fluorides—sodium acetate coated tubeabsorption method

AS 3580.13.3-1993

AM-10 Hydrogen sulfide AS 3580.8.1-1990

AM-11 Lead—particulate collection by high-volume sampler

AS 2800-1985

AM-12 Nitrogen oxides AS 3580.5.1-1993

AM-13 Ozone AS 3580.6.1-1990

AM-14 Particulate matter—suspended matter—filter paper soiling method

AS 2724.2-1987

AM-15 Particulate matter—TSP—high-volumesampler method

AS 2724.3-1984

AM-16 Particulate matter—light scattering—integrating nephelometer method

AS 2724.4-1987

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MethodNo.

Parameter measured Method

AM-17 Particulate matter—impinged matter—directional dust gauge method

AS 2724.5-1987

AM-18 Particulate matter—PM10—high-volumesampler with size-selective inlet

AS 3580.9.6-1990

AM-19 Particulates—deposited matter—gravimetric method AS 3580.10.1-1991

AM-20 Sulfur dioxide AS 3580.4.1-1990

AM-21 Volatile organic compounds AS 3580.11.1-1993

Note: Any other method, which has been approved by the EPA in accordance with theapproval procedures set out in the introduction to this document as an equivalent alternativeto a test method of a particular number in this document, is prescribed as a test method of thatsame number.

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4. Analytical report

Stationary source monitoring

The results of any monitoring required by a statutory instrument must be provided as asummary report signed by the licence holder or, where there is no licence, by the personrequired to provide the report. The report must contain at least the following information foreach air contaminant, unless the statutory instrument states otherwise

• name and address of reporting organisation or individual

• date of issue of the report

• date, time and place of measurements

• identification of source tested

• the test method used and details of any deviation from that method

• details of source or process operating conditions during sampling and a statementabout the representativeness of the sample taken

• location of sampling plane, with respect to the nearest upstream and downstream flowdisturbances

• number of sampling points

• period of sampling (start and end times)

• average stack gas velocity in metres per second

• average stack gas temperature in kelvins

• contaminant molecular weight or density in kilograms per cubic metre

• water content of stack gas, expressed as a percentage by volume

• stack gas volumetric flow rate on a dry basis under standard conditions, in cubicmetres per second

• concentration of contaminant on a dry basis under standard conditions, in grams percubic metre

• mass emission rate of contaminant on a dry basis under standard conditions, in gramsper second

• details of sample preservation, if applicable

• any factors that may have affected the monitoring results

• the precision of the results (using AS 2706 as a guide)

• details of the most recent calibration of each instrument used to take measurements.

If an air contaminant cannot be detected, results must not be quoted as zero but as less thanthe method's limit of detection.

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All volumes and concentrations are normally reported as dry at a temperature of 0°C and at anabsolute pressure of 101.3 kilopascals (kPa). The EPA’s monitoring requirements may alsospecify a reference gas level to which the result must be corrected.

Ambient air monitoring

The results of any monitoring required by a statutory instrument must be provided as asummary report signed by the licence holder or, where there is no licence, by the personrequired to provide the report. The report must contain at least the following information foreach air contaminant, unless the statutory instrument states otherwise:

• name and address of reporting organisation or individual

• date of issue of the report

• the test method used and details of any deviation from that method

• period of monitoring (start and end dates and percentage of time the instruments wereon-line)

• location of monitoring points (normal address and Australian Map Grid reference,height above nominal ground level, and a description of the terrain features)

• the air pollutants measured, the monitoring instruments used, and a description of theair sampling system

• maximum hourly average concentration, daily average concentration, and appropriatelonger-term averages

• appropriate statistical information to describe the variability and range of theconcentrations

• any factors that may have affected the monitoring results

• the precision of the results (using AS 2706 as a guide)

• details of the most recent calibration of each instrument used to take measurements.

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5. ReferencesAmerican Society for Testing and Materials

ASTM. 1994. D3231-94: Standard test method for phosphorus in gasoline. American Societyfor Testing and Materials. West Conshohocken, PA.

ASTM. 1995. D129-95: Standard test method for sulfur in petroleum products (general bombmethod). American Society for Testing and Materials. West Conshohocken, PA.

ASTM. 1997. D2699-97: Standard test method for research octane number of spark-ignitionengine fuel. American Society for Testing and Materials. West Conshohocken, PA.

ASTM. 1997. D2700-97: Standard test method for motor octane number of spark-ignitionengine fuel. American Society for Testing and Materials. West Conshohocken, PA.

ASTM. 1997. D3237-97: Standard test method for lead in gasoline by atomic absorptionspectroscopy. American Society for Testing and Materials. West Conshohocken, PA.

ASTM. 1998. D2622-98: Test method for sulfur in petroleum products (X-ray spectrographicmethod). American Society for Testing and Materials. West Conshohocken, PA.

ASTM. 1998. D4294-98: Standard test method for sulfur in petroleum products by energy-dispersive X-ray fluorescence spectroscopy. American Society for Testing and Materials.West Conshohocken, PA.

California Environmental Protection Agency Air Resources Board

California Environmental Protection Agency Air Resources Board. 1997. Method 425:Determination of total chromium emissions from stationary sources. Sacramento, CA.

California Environmental Protection Agency Air Resources Board. 1997. Method 429:Polycyclic aromatic hydrocarbon (PAH) emissions from stationary sources. Sacramento, CA.

CEN European Committee for Standardisation. 1997. European Standard—Air quality—determination of odour concentration by dynamic olfactometry. CEN/TC264/WG2/N222/e.Brussels.

Federal Office of Road Safety

Federal Office of Road Safety. 1989. Australian Design Rule 37/00: Emission control forlight vehicles. Canberra.

Federal Office of Road Safety. 1995. Australian Design Rule 37/01: Emission control forlight vehicles. Canberra.

Standards Association of Australia 1984–1989

Standards Association of Australia. 1984. AS 2724.3-1984: Particulate matter—determinationof total suspended particulates (TSP)—high volume sampler gravimetric method. Homebush,NSW.

Standards Association of Australia. 1985. AS 2800-1985: Particulate lead—high volumesampler gravimetric collection—flame atomic absorption spectrometric method. Homebush,NSW.

Standards Association of Australia. 1987. AS 2724.2-1987: Particulate matter—determination

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of suspended matter expressed as equivalent black smoke by filter paper soiling. Homebush,NSW.

Standards Association of Australia. 1987. AS 2724.4-1987: Particulate matter—determinationof light scattering—integrating nephelometer method. Homebush, NSW.

Standards Association of Australia. 1987. AS 2724.5-1987: Particulate matter—determinationof impinged matter expressed as directional dirtiness, background dirtiness and/or areadirtiness (directional dust gauge method). Homebush, NSW.

Standards Association of Australia. 1987. AS 2922-1987: Guide for the siting of samplingunits. Homebush, NSW.

Standards Association of Australia. 1987. AS 2923-1987: Guide for measurement ofhorizontal wind for air quality applications. Homebush, NSW.

Standards Association of Australia. 1989. AS 3543-1989: Use of standard Ringelmann andAustralian Standard miniature smoke charts. Homebush, NSW.

Standards Association of Australia 1990

Standards Association of Australia. 1990. AS 1876-1990: Petrol (gasoline) for motorvehicles. Homebush, NSW.

Standards Association of Australia. 1990. AS 3580.2.1-1990: Preparation of reference testatmospheres—permeation tube method. Homebush, NSW.

Standards Association of Australia. 1990. AS 3580.2.2-1990: Preparation of reference testatmospheres—compressed gas method. Homebush, NSW.

Standards Association of Australia. 1990. AS 3580.3.1-1990: Acid gases—titrimetric method.Homebush, NSW.

Standards Association of Australia. 1990. AS 3580.4.1-1990: Sulfur dioxide—direct readinginstrumental method. Homebush, NSW.

Standards Association of Australia. 1990. AS 3580.6.1-1990: Ozone—direct-readinginstrumental method. Homebush, NSW.

Standards Association of Australia. 1990. AS 3580.8.1-1990: Hydrogen sulfide—automaticintermittent sampling—gas chromatographic method. Homebush, NSW.

Standards Association of Australia. 1990. AS 3580.9.6-1990: Suspended particulate matter—PM10 high volume sampler with size-selective inlet—gravimetric method. Homebush, NSW.

Standards Association of Australia 1991–1999

Standards Association of Australia. 1991. AS 3580.10.1-1991: Particulates—depositedmatter—gravimetric method. Homebush, NSW.

Standards Association of Australia. 1991. AS 3580.13.2-1991: Fluorides—gaseous and acid-soluble particulate fluorides—manual, double filter paper sampling. Homebush, NSW.

Standards Association of Australia. 1992. AS 3580.7.1-1992: Carbon monoxide—direct-reading instrumental method. Homebush, NSW.

Standards Association of Australia. 1993. AS 3580.5.1-1993: Oxides of nitrogen—chemiluminescence method. Homebush, NSW.

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Standards Association of Australia. 1993. AS 3580.11.1-1993: Volatile organic compounds—methane and non-methane volatile organic compounds—direct-reading instrumental method.Homebush, NSW.

Standards Association of Australia. 1993. AS 3580.13.1-1993: Fluorides—gaseous and acid-soluble particulate fluorides—automated, double paper tape sampling. Homebush, NSW.

Standards Association of Australia. 1993. AS 3580.13.3-1993: Fluorides—total gaseous andacid-soluble airborne particulate fluoride—sodium acetate coated tube absorption. Homebush,NSW.

Standards Association of Australia. 1995. AS 4323.1-1995: Stationary source emissionmethod 1—selection of sampling positions. Homebush, NSW.

Standards Association of Australia. 1995. AS 4323.2-1995: Stationary source emissionsmethod 2—determination of total particulate matter—isokinetic manual sampling—gravimetric method. Homebush, NSW.

Standards Association of Australia. 1998. AS 3570-1998: Automotive diesel fuel. Homebush,NSW.

Standards Association of Australia. DR 99306 (unpublished) Draft Australian Standard—Airquality—determination of odour concentration by dynamic olfactometry. Homebush, NSW.

United States Environmental Protection Agency 1986–1996

US Environmental Protection Agency. 1986. Measurement of gaseous emission rates fromland surfaces using an emission isolation flux chamber, user's guide. EPA/600/8-8e/008,February 1986.

US Environmental Protection Agency. 1987. On-site meteorological program guidance forregulatory modeling applications. Office of Air Quality Planning and Standards, ResearchTriangle Park, NC. EPA 450/4-87-013.

US Environmental Protection Agency. 1996. Method 0061: Determination of hexavalentchromium emissions from stationary sources (Revision 0, December, 1996). Test methods forevaluating solid waste, 3rd ed., 1986 (SW-846). Office of Solid Waste and EmergencyResponse, Washington, DC.

USEPA Method 201

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 51,Appendix M, Method 201: Determination of PM10 emissions (exhaust gas recycle procedure).US Government Printing Office, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 51,Appendix M, Method 201A: Determination of PM10 emissions (constant sampling rateprocedure). US Government Printing Office, Washington, DC.

USEPA Methods 1–9

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A, Method 1: Sample and velocity traverses for stationary sources. USGovernment Printing Office, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A, Method 2: Determination of stack gas velocity and volumetric flow rate (type Spitot tube). US Government Printing Office, Washington, DC.

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US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A, Method 2C: Determination of stack gas velocity and volumetric flow rate fromsmall stacks or ducts (standard pitot tube). US Government Printing Office, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A, Method 3: Gas analysis for the determination of dry molecular weight. USGovernment Printing Office, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A Method 3A: Determination of oxygen and carbon dioxide concentrations inemissions from stationary sources (instrumental analyzer procedure). US GovernmentPrinting Office, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A. Method 4: Determination of moisture content in stack gases. US GovernmentPrinting Office, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A. Method 5: Determination of particulate emissions from stationary sources. USGovernment Printing Office, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A. Method 6: Determination of sulfur dioxide emissions from stationary sources.US Government Printing Office, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A. Method 6A: Determination of sulfur dioxide, moisture, and carbon dioxideemissions from fossil-fuel combustion sources. US Government Printing Office, Washington,DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A. Method 6B: Determination of sulfur dioxide and carbon dioxide daily averageemissions from fossil-fuel combustion sources. US Government Printing Office, Washington,DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A. Method 6C: Determination of sulfur dioxide emissions from stationary sources(instrumental analyzer procedure). US Government Printing Office, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A. Method 7: Determination of nitrogen oxide emissions from stationary sources.US Government Printing Office, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A. Method 7A: Determination of nitrogen oxide emissions from stationary sources(ion chromatographic method). US Government Printing Office, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A. Method 7B: Determination of nitrogen oxide emissions from stationary sources(ultraviolet spectrophotometry). US Government Printing Office, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A, Method 7C: Determination of nitrogen oxide emissions from stationary sources(alkaline-permanganate/colorimetric method). US Government Printing Office, Washington,DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,

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Appendix A, Method 7D: Determination of nitrogen oxide emissions from stationary sources(alkaline-permanganate/ion chromatographic method). US Government Printing Office,Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A. Method 7E: Determination of nitrogen oxide emissions from stationary sources(instrumental analyzer procedure). US Government Printing Office, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A. Method 8: Determination of sulfuric acid mist and sulfur dioxide emissionsfrom stationary sources. US Government Printing Office, Washington, DC.

USEPA Methods 10–19

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A. Method 13A: Determination of total fluoride emissions from stationary sources(SPADNS zirconium lake method). US Government Printing Office, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A. Method 13B: Determination of total fluoride emissions from stationary sources(specific ion electrode method). US Government Printing Office, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A. Method 14: Determination of fluoride emissions from roof monitors for primaryaluminum plants. US Government Printing Office, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A. Method 14A: Determination of total fluoride emissions from selected sources atprimary aluminum production facilities. US Government Printing Office, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A. Method 15: Determination of hydrogen sulfide, carbonyl sulfide and carbondisulfide emissions from stationary sources. US Government Printing Office, Washington,DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A. Method 18: Measurement of gaseous organic compound emissions by gaschromatography. US Government Printing Office, Washington, DC.

USEPA Methods 20–29

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A. Method 20: Determination of nitrogen oxides, sulfur dioxide and oxygenemissions from stationary gas turbines. US Government Printing Office, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A. Method 23: Determination of polychlorinated dibenzo-p-dioxins andpolychlorinated dibenzofurans from stationary sources. US Government Printing Office,Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A. Method 25: Determination of total gaseous nonmethane organic emissions ascarbon. US Government Printing Office, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A. Method 25A: Determination of total gaseous organic concentrations using aflame ionization analyzer. US Government Printing Office, Washington, DC.

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US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A. Method 25B: Determination of total gaseous organic concentrations using anondispersive infrared analyzer. US Government Printing Office, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A. Method 25C: Determination of nonmethane organic compounds (NMOC) inMSW landfill gases. US Government Printing Office, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A, Method 25D: Determination of the volatile organic concentration of wastesamples. US Government Printing Office, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A, Method 25E: Determination of vapor phase organic concentration in wastesamples. US Government Printing Office, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A, Method 26: Determination of hydrogen chloride emissions from stationarysources—isokinetic method. US Government Printing Office, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A, Method 26A: Determination of hydrogen halide and halogen emissions fromstationary sources—isokinetic method. US Government Printing Office, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix A. Method 29: Determination of metal emissions from stationary sources. USGovernment Printing Office, Washington, DC.

USEPA Performance Specifications 1–9 & 15

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix B, Performance Specification 1—Specifications and test procedures for opacitycontinuous emission monitoring systems in stationary sources. US Government PrintingOffice, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix B, Performance Specification 2—Specifications and test procedures for SO2 andNOx continuous emission monitoring systems in stationary sources. US Government PrintingOffice, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix B, Performance Specification 3—Specifications and test procedures for O2 andCO2 continuous emission monitoring systems in stationary sources. US Government PrintingOffice, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix B, Performance Specification 4—Specifications and test procedures for COcontinuous emission monitoring systems in stationary sources. US Government PrintingOffice, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix B, Performance Specification 5—Specifications and test procedures for TRScontinuous emission monitoring systems in stationary sources. US Government PrintingOffice, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix B, Performance Specification 6—Specifications and test procedures for flow rate

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continuous emission monitoring systems in stationary sources. US Government PrintingOffice, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix B, Performance Specification 7—Specifications and test procedures for H2Scontinuous emission monitoring systems in stationary sources. US Government PrintingOffice, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix B, Performance Specification 8—Specifications and test procedures for VOCcontinuous emission monitoring systems in stationary sources. US Government PrintingOffice, Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 60,Appendix B, Performance Specification 9—Specifications and test procedures for gaschromatographic continuous emission monitoring systems in stationary sources. USGovernment Printing Office, Washington, DC.

US Environmental Protection Agency. 1997. Federal Register, Volume 62, Number 166,August 27, Amendments for Testing and Monitoring Provisions, pp. 45369-45377. ProposedPerformance Specification 15—Performance specification for extractive FTIR continuousemission monitoring systems in stationary sources. US Government Printing Office,Washington, DC.

US Environmental Protection Agency. 1997. Code of Federal Regulations, Title 40, Part 63,Appendix A, Method 306: Determination of chromium emissions from decorative and hardchromium electroplating and anodizing operations. US Government Printing Office,Washington, DC.

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APPENDICESGeneric procedures and definitions that apply to stationary source monitoring andreporting

Test method 17—Determination of soot

Test method 19—Determination of total mass of unburnt organic vapours from vapourdisposal units

Test method 20—Determination of total mass of unrecovered organic vapours from vapourrecovery units

Test method 21—Calculation of vapour pressure

Test method 26—Exhaust and evaporative emissions from spark-ignition motor vehicles

Test method 27—Lead concentration in leaded and unleaded petrol

Test method 31—Observation procedure for excessive air impurities: visible emissions

Other approved method 9—Determination of “coarse” particulates

Test method sources

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Generic procedures and definitions that apply tostationary source monitoring and reporting

Adjustment to reference and equivalent values

1. Oxygen

For adjustment to an oxygen reference, the adjusted concentration of a pollutant, Cb, isdetermined by:

Cb = Ca × (21 – reference oxygen concentration as volume %) ÷ (21 – measured oxygenconcentration as volume %)

where Ca is the measured concentration of the pollutant.

2. Carbon dioxide

For adjustment to a carbon dioxide reference, the adjusted concentration of a pollutant, Cc, isdetermined by:

Cc = Ca × 12 ÷ measured carbon dioxide concentration as volume %

where Ca is the measured concentration of the pollutant.

3. Reference values

For plant currently operating or for which an application for a pollution controlapproval was submitted before 1 September 1997

Equipment Basis Pollutant

Any trade, industry, process,industrial plant, or fuel-burningequipment, except those below

Dry, 273 K, 101.3 kPa All pollutants (except aslisted below)

Boilers and incinerators Dry, 273 K, 101.3 kPa, 12% CO2 Solid particles

Domestic waste incinerators Dry, 273 K, 101.3 kPa, 11% O2 Dioxins and furans

For plant for which an application for a pollution control approval was granted on orafter 1 September 1997

Equipment Basis Pollutant

Any trade, industry, process,industrial plant, or fuel-burningequipment, except those below

Dry, 273 K, 101.3 kPa All pollutants (except aslisted below)

Boilers and incinerators Dry, 273 K, 101.3 kPa, 7% O2 Solid particles

Domestic waste incinerators Dry, 273 K, 101.3 kPa, 11% O2 Dioxins and furans

Gas turbines Dry, 273 K, 101.3 kPa, 15% O2 Oxides of nitrogen

Other fuel-burning equipment Dry, 273 K, 101.3 kPa, 7% O2 Oxides of nitrogen

4. Nitrogen dioxide

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Oxides of nitrogen (NOx) from combustion of fossil fuels consist predominantly of nitricoxide (NO) and nitrogen dioxide (NO2). Oxides of nitrogen concentrations are converted toequivalent NO2 thus:

Equivalent NO2 = calculated NO2 + (measured NO × 46 ÷ 30)

where:

calculated NO2 = measured NOx – measured NO46 = molecular weight of NO2

30 = molecular weight of NO

Both NO and NOx must be measured directly, and all concentrations must be expressed inppm.

Cubic metre (m3)

In this document a cubic metre refers to the volume of dry gas that occupies 1 m3 at atemperature of 0°C (273 K) and at an absolute pressure equivalent to 1 atmosphere (101.3kPa).

Measuring concentrations and volumes in gases

When reporting concentrations of pollutants in gases for comparison with emission standardsor with limits in regulations, licences, approvals, statutory notices, guidelines, codes ofpractice or environmental management plans, you must use the following conversions.However, where any of these conversions are part of the test method used to determine theconcentration, they do not need to be repeated for reporting.

The test method for a pollutant gives the volume of gas sampled at the test conditions(temperature, pressure) at the sample point, Va.

• Determine the moisture content (MC, %) of the gas at the sample point in accordancewith USEPA Method 4.

• Calculate the volume of dry gas at sample point conditions (Vb):

Vb = Va × (100 – MC) ÷ 100 ... (1)

• Calculate the volume of dry gas at standard temperature (273 K) (Vc):

Vc = Vb × 273 ÷ (273 + gas meter temperature in °C) ... (2)

• Calculate the volume of dry gas at standard temperature and pressure (Vd):

Vd = Vc × (gas meter pressure in kPa) ÷ 101.3 ... (3)

• Divide the measured mass of pollutant (Ma ) by Vd to determine the concentration (Ca):

Ca = Ma ÷ Vd ... (4)

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Test method 17—Determination of sootMeasure the concentration of soot emitted from a source with the True Spot Smoke TesterModel RCC-B, the Oil Burner Smoke Scale and the filter paper supplied by Bacharach Inc.,625 Alpha Drive, Pittsburgh, PA, USA. Tel: 0011 1 412 963 2000.

Insert the clean sampling tube, extended if necessary, into the gas stream to be tested. Connectit to the smoke tester. Insert a strip of filter paper into the slot at the end of the tester andtighten the clamp screw. Pull the smoke tester pump handle steadily through 10 full strokes:take 3 to 4 seconds for each pull motion, pause a further 3 seconds at the end of each stroke,then return the pump handle to its original position.

Loosen the clamp screw and examine the paper to see whether any soot has produced a smokespot on the paper. Move the filter paper to a new position in the smoke tester slot. Repeat thetest until consecutive smoke spots on the paper are of equal shading.

Match the colour of the smoke spots on the filter paper to the closest spot on the Oil BurnerSmoke Scale. Hold the scale at arm's length against an opaque white page. Slide the filterpaper behind it so that you can see the spot on the filter paper through the holes in the centresof the colour spots on the scale.

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Test method 19—Determination of total mass of unburntorganic vapours from vapour disposal units

Sampling

Draw the exhaust gases through a 316 stainless steel probe to a sample line of PTFE or 316stainless steel held at a temperature of at least 105°C.

Pass the exhaust gases to a device capable of reducing the moisture content of the gases to adew point of less than 3°C. Filter the sample gases to remove entrained particles.

Analysis

Pass the conditioned sample gases to the following two analysers.

Hydrocarbon analyser (flame ionisation detector type)

Set the analyser to zero with air that has a hydrocarbon concentration of less than 10 ppm byvolume of propane. Calibrate it with a gas of known propane concentration to give adeflection of between 20% and 90% of full scale on the range being used.

The average of the indicated concentration of hydrocarbons in the conditioned sample gasesmust lie between 30% and 90% of full-scale deflection of the analyser. The combined effectsof carbon dioxide and carbon monoxide in the gases must not affect the reading by more than2% of full-scale deflection. The deviation from linear response of the analyser must notexceed 2.5% of full-scale deflection.

Carbon dioxide analyser (non-dispersive infrared type)

Set the analyser to zero with nitrogen that has a carbon dioxide concentration of less than0.05% by volume. Calibrate it with a gas of known carbon dioxide concentration to give adeflection of between 20% and 90% of full scale on the range being used.

The analyser must have a full-scale range for carbon dioxide concentration lying between 0%and 14% and 0% and 20% by volume. The deviation from linear response of the analysermust not exceed 2.5% of full-scale deflection.

Calculation of mass of unburnt organic vapours

The mass of unburnt organic vapours in each cubic metre of the exhaust gases is equal to:

C ÷ (42.3 × L) grams ... (1)

where:

C = the average concentration of hydrocarbons measured as equivalent propane in ppm overthe test period42.3 = a conversion factorL = the average concentration of carbon dioxide content expressed as a percentage of samplegases.

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Test method 20—Determination of total mass ofunrecovered organic vapours from vapour recovery units

Sampling

Draw the exhaust gases through a sample line of PTFE or 316 stainless steel construction.Pass them to a hydrocarbon analyser (flame ionisation detector type).

Analysis

Set the analyser to zero with air that has a hydrocarbon concentration of less than 10 ppm byvolume of propane. Calibrate the analyser with a gas of known propane concentration to givea deflection of between 20% and 90% of full scale on the range being used.

The average of the indicated concentration of hydrocarbons in the exhaust gases must liebetween 30% and 90% of full-scale deflection of the analyser. The combined effects ofcarbon dioxide and carbon monoxide in the gases must not affect the reading by more than2% of full-scale deflection. The deviation from linear response of the analyser shall notexceed 2.5% of full-scale deflection.

Calculation of mass of unrecovered organic vapours

The mass of unrecovered organic vapours emitted for each litre of organic liquid is:

(318 × C × A × M × P × V) ÷ (L × T) milligrams ... (1)

where:

C = the average concentration of hydrocarbons expressed as equivalent propane in ppm overthe test periodA = the cross-sectional area of the exhaust duct at the plane where the measurements aremade, in m2

M = the total time for organic liquid to pass into the tank or out of the industrial plant, inminutesP = the atmospheric pressure in kPaV = the average exhaust gas velocity in metres per secondL = the volume of organic liquid passing into the tank or out of the industrial plant, in litresT = the average exhaust gas temperature in kelvins (273 + temperature in °C)318 = a conversion factor

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Test method 21—Calculation of vapour pressureA volatile organic liquid for which the Reid Vapour Pressure may be ascertained shall bedeemed to have a vapour pressure exceeding 75 kilopascals if the maximum bulk storagetemperature of the liquid is greater than the temperature specified in Column 2 of the tablebelow corresponding to the Reid Vapour Pressure of the liquid specified in Column 1.

Where the Reid Vapour Pressure of the liquid lies between two adjacent values specified inColumn 1 of the table, the corresponding temperature may be calculated as though a linearrelationship existed between the Reid Vapour Pressure and the temperature at and betweenthose two values.

Where the Reid Vapour Pressure of the liquid lies outside the values specified in Column 1 ofthe table or cannot be determined, the vapour pressure of the liquid shall be calculated bysuch methods as the EPA may determine.

Column 1

Reid Vapour Pressure(kPa)

Column 2

Temperature (°C)

50 49

60 43

70 38

80 33

90 29

100 26

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Test method 26—Exhaust and evaporative emissions fromspark-ignition motor vehiclesTesting must be carried out in accordance with the test procedures appropriate for thecategory of vehicle being tested and its date of manufacture specified in ADR 37/00 or ADR37/01, Emission Control for Light Vehicles. Special conditions apply, as detailed below.

A reference here to components applies only to those components related to the emissionperformance of the motor vehicle being tested.

• Compliance testing of new petrol-powered light vehicles

• Compliance testing of in-service petrol-powered light vehicles up to 5 years old orwith 80 000 km accumulated

• Compliance testing of in-service dual-fuel (petrol/LPG) light vehicles up to 5 yearsold or with 80 000 km accumulated, operating on liquefied petroleum gas (LPG)

• Compliance testing of in-service dual-fuel (petrol/LPG) light vehicles up to 5 yearsold or with 80 000 km accumulated, operating on petrol

• Compliance testing of in-service dual-fuel (petrol/CNG) light vehicles up to 5 yearsold or with 80 000 km accumulated, operating on compressed natural gas (CNG)

• Compliance testing of in-service dual-fuel (petrol/CNG) light vehicles up to 5 yearsold or with 80 000 km accumulated, operating on petrol

Compliance testing of new petrol-powered light vehicles

• Test the vehicle in the condition in which it is presented for testing (no tuning orspecial stabilisation distance run-in) unless the manufacturer or its agent requestsspecial preparations to be made before testing.

• In evaporative emissions testing of a vehicle less than 56 days after it wasmanufactured, the Clean Air (Motor Vehicles and Motor Vehicle Fuels) Regulation1997 allows for 1 to 3 g of hydrocarbon emissions emanating from sources other thanthe fuel system of the vehicle.

* Compliance testing of in-service petrol-powered light vehicles up to 5years old or with 80 000 km accumulated

• The engine of the vehicle must be tuned to the manufacturer's specifications.

• Where components originally fitted to the vehicle have been removed, disabled ortampered with, they must be replaced or repaired before testing.

• Components that are faulty or broken through normal use of the vehicle must not bereplaced or repaired before testing.

• Components whose performance has deteriorated through normal use must not bereplaced before testing.

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Compliance testing of in-service dual-fuel (petrol/LPG) light vehicles up to5 years old or with 80 000 km accumulated, operating on liquefiedpetroleum gas (LPG)

• All conditions in * above apply.

• Do not conduct the evaporative emission testing procedure.

• Do not apply any heat source to the vehicle's LPG storage container(s) during testing.

• Use LPG consisting of 50% butane and 50% propane. If this is not available, usecommercially available LPG.

Compliance testing of in-service dual-fuel (petrol/LPG) light vehicles up to5 years old or with 80 000 km accumulated, operating on petrol

• All conditions in * above apply.

• Do not apply any heat source to the vehicle's LPG storage container(s) during testing.

Compliance testing of in-service dual-fuel (petrol/CNG) light vehicles up to5 years old or with 80 000 km accumulated, operating on compressednatural gas (CNG)

• All conditions in * above apply.

• Do not conduct the evaporative emission testing procedure.

• Do not apply any heat source to the vehicle's CNG storage container(s) during testing.

• Use commercially available CNG for this test.

Compliance testing of in-service dual-fuel (petrol/CNG) light vehicles up to5 years old or with 80 000 km accumulated, operating on petrol

• All conditions in * above apply.

• Do not apply any heat source to the vehicle's CNG storage container(s) during testing.

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Test method 27—Lead concentration in leaded andunleaded petrolThe lead in all petrol must be determined with this test method. The method was developedby the EPA from the standard test methods AS 1876-1990 Petrol (Gasoline) for MotorVehicles and ASTM D3237-97 Standard Test Method for Lead in Gasoline by AtomicAbsorption Spectrometry.

Applicability

This method is independent of the lead alkyl type.

Principle

The petrol sample is diluted with methyl isobutyl ketone, and the alkyl lead compounds arestabilised by reaction with iodine and a quaternary ammonium salt. The lead content of thesample is determined by atomic absorption flame spectrophotometry at 283 nm. Standardsprepared from reagent-grade lead chloride are used for calibration.

Range

Lead concentrations in the range 0.005 to 1 g/L can be determined. Higher leadconcentrations require dilution with iso-octane before analysis.

Sampling and storage

Containers for samples from bowsers, tanks, delivery tanks, tank vehicles or pipeline

Sampling containers must be metal cans with welded side seams and a minimum capacity of250 mL. Each container must have an opening at the top of 30 to 50 mm in diameter. The topmust be sealed with a vapour-tight screw cap.

Number of samples

Take two samples of the petrol to be tested and analyse the lead content of each. If requested,leave a third sealed sample with the owner or the person in charge.

Sampling from a bowser

Pour the petrol directly from the nozzle of the bowser hose into the top opening of the samplecontainer. Fill the container to near capacity.

Sampling from a tank, delivery tank, tank vehicle, pipeline, fuel tank or motor vehicle

Take a representative sample. Pour it into a sample container for transport.

Storage

Store samples at 0° to 8°C. Bring them to room temperature before analysis.

Cleaning procedures

Rinse the sampling containers with acetone (propanone) or iso-octane. Dry them in a dryingcabinet at 40°C or higher.

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Reagents

• MIBK: methyl isobutyl ketone (4-methyl-2-pentanone) (AR grade).

• Iodine solution: Dissolve 3.0 g AR grade iodine in AR grade toluene and dilute to 100mL with the toluene. Store in a brown glass bottle.

• Aliquat 336: Tricapryl methyl ammonium chloride.

• 10% Aliquat 336/MIBK solution: Dilute 100 mL of Aliquat 336 to 1 L with MIBK.

• 1% Aliquat 336/MIBK Solution: Dilute 10 mL of Aliquat 336 to 1 L with MIBK.

• Lead chloride: At least 99% pure.

• Stock lead solution (2000 mg/L): Dry lead chloride at 105° ± 5 °C for 3 hours.Dissolve 0.6711 g in about 200 mL of 10% Aliquat 336/MIBK solution. Dilute to themark in 250 mL volumetric flask with 10% Aliquot 336/MIBK solution. Mix well andstore in a brown glass bottle.

• Intermediate stock lead solution (100 mg/L): Transfer accurately by pipette 5 mL ofstock lead solution to a 100 mL volumetric flask. Dilute to the mark with 10% Aliquat336/MIBK solution. Mix well and store in a brown glass bottle.

• Iso-octane: 2,2,4-trimethylpentane (AR grade).

• Nitric acid (1+1): Mix equal volumes of concentrated AR grade nitric acid anddistilled water.

• Acetone (AR grade).

Maximum storage periods for reagents:

iodine solution 30 days

10% Aliquat 336/MIBK 30 days

1% Aliquat 336/MIBK 30 days

stock lead solution 30 days

Standard lead solution 1 day

Grades of reagents other than those indicated may be used on two privisos:

• The reagent is of high enough purity to permit its use without lessening the accuracyof the determination.

• The same source of reagent is used for all standards and blanks.

Analysis

General

Glassware must be de-leaded by rinsing with dilute nitric acid (1+1) and then rinsed withdistilled water. Wash the glassware with acetone and dry it at 50° ± 5°C.

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Preparation of working standards (2, 5, 10, 20 mg/L)

Transfer accurately by pipette 1.0, 2.5, 5.0 and 10.0 mL of the intermediate stock leadsolution (100 mg/L) to four 50 mL volumetric flasks. Adjust the volume of each to 10 mL byadding 1% Aliquat/MIBK solution and add 10 mL of iso-octane. Add 0.1 mL of iodinesolution, mix well and allow to react for at least 1 minute. Dilute to volume with MIBK andmix.

Preparation of the blank

To a 50 mL volumetric flask add 30 mL of MIBK then 10 mL of iso-octane. Add 0.1 mL ofiodine solution, mix well and allow to react for at least 1 minute. Add 5 mL of 1%Aliquat/MIBK solution and mix. Dilute to volume with MIBK and mix.

Preparation of sample

• For petrol with a lead concentration of < 0.1 g/L: To a 50 mL volumetric flaskcontaining 30 mL of MIBK and 10 mL of petrol sample, add 0.1 mL of iodinesolution. Mix well and allow to react for at least 1 minute. Add 5 mL of 1%Aliquat/MIBK solution. Dilute to volume with MIBK and mix.

• For petrol with a lead concentration of 0.1–1 g/L: To a 50 mL volumetric flask add 30mL of MIBK. Add 1–5 mL of petrol sample and enough iso-octane to yield a finalsample volume of 10 mL. Add 0.1 mL of iodide solution, mix well and allow to reactfor at least 1 minute. Add 5 mL of 1% Aliquat/MIBK solution. Dilute to volume withMIBK and mix.

• For petrol with a lead concentration of > 1 g/L, dilute with iso-octane before analysis.

Preparation of the atomic absorption spectrophotometer

Optimise the instrument for lead at 283.3 nm. Using the blank, adjust the gas mixture(acetylene/air) and aspiration rate to obtain an oxidising lean, blue flame. Aspirate the 20mg/L lead working standard and adjust the instrument to achieve maximum response.

Standardisation and analysis

Aspirate the reagent blank and adjust the instrument to zero. Measure the absorbances of the2, 5, 10 and 20 mg/L lead working standards. Aspirate the samples and record the absorbancevalues. Aspirate the blank between each sample measurement.

For instruments without a direct concentration readout, prepare a calibration curve by plottingthe absorbance of the working standards against their concentrations (mg/L) on linear graphpaper.

Calculations

Read the lead concentration in g/L directly from the instrument readout or calculate it byreferring to the appropriate calibration curve:

Lead concentration in petrol sample (g/L) = (C × V1) ÷ (V2 × 1000)

where:

C = lead concentration (mg/L) of sample (as read from graph or instrument readout)V1 = final volume (50 mL)V2 = volume of sample petrol (mL)

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Test method 31—Observation procedure for excessive airimpurities: visible emissionsWhen an observer is determining if a vehicle is being used in breach of the clause limitingvisible emissions, the following principles apply:

• The observer must be satisfied that the vehicle generating the visible emissions iscorrectly identified.

• The observer must be satisfied that the emissions are visible not just because of heat orthe condensation of water vapour.

• The emissions must be continuously visible for more than 10 seconds.

The following details of the observation must be recorded:

• Length of time in seconds that the visible emissions were observed.

• Registration number of the motor vehicle under observation.

• Type of motor vehicle under observation.

• Colour and darkness, in the opinion of the observer, of the air impurities emitted.

• Location, date and approximate time of day that the observation was made.

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Other approved method 9—Determination of “coarse”particulatesTo determine “coarse” particulates:

• determine total solid particles using TM-15;

• simultaneously determine “fine” particulates (PM10 emissions) using OM-5; then

• subtract the result of OM-5 (PM10 or “fine” particulates) from the result of TM-15(Total solid particles) to determine “coarse” particulates.

The two methods must be carried out simultaneously, over the same sampling period toensure the influence of process change does not impact on the results.

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Test method sources

Australian Standard test methods

Available for purchase from Standards Australia, 1 The Crescent, Homebush NSW 2140 (POBox 1055, Strathfield NSW 2135).Tel: 1300 65 46 46; Fax: 1300 65 49 49; E-mail: [email protected]://www.standards.com.au/

American Society for Testing and Materials test methods

Available from Standards Australia (see above) or direct from ASTM, 100 Barr Harbor Drive,West Conshohocken PA 19428-2959, USA.Tel: 0011 1 610 832 9500; Fax: 0015 1 610 832 9500http://www.astm.org/index.html#

United States Environmental Protection Agency test methods

Available from USEPA, National Service Centre for Environmental Publications, PO Box42419, Cincinatti OH 45242, USA.Tel: 0011 1 513 489 8190; Fax: 0015 1 513 489 8695http://www.epa.gov/ttn/emc/ or http://www.epa.gov/ (for on-line ordering)USEPA Method 0061: http://www.epa.gov/epaoswer/hazwaste/test/0061.pdfSW-846 series: http://www.epa.gov/epaoswer/hazwaste/test/main.htm

California Environmental Protection Agency Air Resources Board

Available from Office of Communications, 2020 L Street, Sacramento CA 95814, USA.Tel: 0011 1 916 322 2990; Fax: 0015 1 916 445 5025http://www.arb.ca.gov/testmeth/vol3/vol3.htm

Australian Design Rules test methods

The Federal Office of Road Safety publishes Australian Design Rules for motor vehicles.ADR 37/00 or 37/01, Emission Control for Light Vehicles, is available from the FederalOffice of Road Safety, 15 Mort Street, Canberra ACT 2600 (PO Box 594, Canberra ACT2601).Tel: (02) 6274 7111; Fax: (02) 6274 7922http://www.atsb.gov.au/fors/contact.htm

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APPENDIX B

AS 2922 AMBIENT AIR - GUIDE FOR THE SITING OF SAMPLING UNITS

NOT INCLUDED IN THIS COPY

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APPENDIX C

AS 3580.10.1-1991 METHODS FOR SAMPLING AND ANALYSIS OF AMBIENT AIR - DETERMINATION OF PARTICULATES - DEPOSITED MATTER - GRAVIMETRIC METHOD

NOT INCLUDED IN THIS COPY

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APPENDIX D

AS 2724.3-1984 AMBIENT AIR – PARTICULATE MATTER – DETERMINATION OF TOTAL SUSPENDED PARTICULATES (TSP) – HIGH VOLUME SAMPLER GRAVIMETRIC METHOD

NOT INCLUDED IN THIS COPY