Background Report Reference - US EPA · Background Report Reference AP-42 Section Number: ... Plant...

Background Report Reference

AP-42 Section Number: 10.6.1

Background Report Section: 4

Reference Number: 68

Title: Result Of The June 2 & 3,1994 Particulate Emission Enginering Testing at the Louisiana Pacific Plant In Hayward, Wisconsin

Interpoll Laboratories, Inc.

July 1994

I

EPA

Text Box

Note: This is a reference cited in AP 42, Compilation of Air Pollutant Emission Factors, Volume I Stationary Point and Area Sources. AP42 is located on the EPA web site at www.epa.gov/ttn/chief/ap42/ The file name refers to the reference number, the AP42 chapter and section. The file name "ref02_c01s02.pdf" would mean the reference is from AP42 chapter 1 section 2. The reference may be from a previous version of the section and no longer cited. The primary source should always be checked.

I I I I I I I I I I I I I I I I I r I

Interpol I Laboratories, I nc. 4500 Ball Road N.E.

Circle Pines, Minnesota 55014-1819

TEL: (612) 786-6020 FAX: (612) 786-7854

ENGI N EERl NG

RESULT OF THE JUNE 2 & 3, 1994 PARTICULATE EMISSION ENGINEERING

TESTING AT THE LOUISIANA PACIFIC PLANT IN HAYWARD, WISCONSIN

Submitted to:

LOUISIANA-PACIFIC CORPORATION Route 8, Box 8263

Hayward, Wisconsin 54843

Attention:

Sue Somers

Approved by:

Report Number 4-3068 July 8, 1994 SP/slp

Q&. Daniel spen

Manager Stationan/ Source Testing Department

.-

TABLE OF CONTENTS

... ABBREVIATIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . III

1 INTRODUCTION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . l

2 SUMMARY AND DISCUSSION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

3 AIR EMISSION RESULTS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11

3.1 Results of Orsat & Moisture Analyses . . . . . . . . . . . . . . . . . . . . . . . . . 12

3.2 Results of Particulate Loading Determinations . . . . . . . . . . . . . . . . . . . 17

I I I

APPENDICES:

A - Volumetric Flow Rate Determination

8 - Field Data Sheets

C - Interpol1 Laboratories Analytical Data

D - Sampling Train Calibration Data

.. II

I I I I I I I I I I 1 I I I I ‘I :I

ACFM cc (ml) DSCFM DSML DEC-F ( O F )

DIA. FP FTISEC g CPM CWACF CWDSCF gldscm HP H RS IN. IN.HC. IN.WC. LB LBIDSCF LBIHR LB/1 06BTU LBIMMBTU LTPD MW mg/Nm’ ug/Nm’ microns (urn) MIN. ng ohmcm PM PPH PPM PPmC PPmd PPmtw PPt PSI SQ. FT. TPD ug v/v WIW

<

AB B REV I AT I 0 N S

actual cubic feet per minute cubic centimeter (milliliter) dry standard cubic foot of dry gas per minute dry standard milliliter degrees Fahrenheit diameter finished product for plant feet per second gram gallons per minute grains per actual cubic foot grains per dry standard cubic foot grams per dry standard cubic meter horsepower hours inches inches of mercury inches of water pound pounds per dry standard cubic foot pounds per hour pounds per million British Thermal Units heat input pounds per million British Thermal Units heat input long tons per day megawatt milligrams per dry standard cubic meter micrograms per dry standard cubic meter micrometer minutes nanograms ohmcentimeter particulate matter pounds per hour parts per million parts per million carbon parts per million, dry parts per million, wet parts per trillion pounds per square inch square feet tons per day micrograms percent by volume percent by weight s (when following a number)

Standard conditions are defined as 68OF (20°C) and 29.92 IN. of mercury pressure.

@Atadhrp\mis&bbr.fm

... 1 1 1

I #I I I I I I I I I I I I I I I I I I

1 INTRODUCTION

On June 2 & 3, 1994 Interpoll Laboratories Personnel conducted a Particulate

Emission Engineering Test on the Line 2 RTO Outlet, Surface Cyclone Exhaust, Core Cyclone

Outlet, and RTO Outlet Duct at the Louisiana Pacific Plant in Hayward, Wisconsin. Gary Hove and Ed Trowbridge performed the on-site portion of the test. Coordination between

testing activities and plant operation was provided by Sue Somers of Louisiana Pacific. A

member of the Wisconsin DeDartment of Natural Resources did not witness the test.

Particulate evaluations were performed in accordance with EPA Methods 1 - 5, CFR

Title 40, Part 60, Appendix A (revised July 1, 1994). A preliminary determination of the gas

linear velocity profile was made before the first particulate determination to allow selection

of the appropriate nozzle diameter required for isokinetic sample withdrawal. An Interpoll

Labs sampling train which meets or exceeds specifications in the above-cited reference was

used to extract particulate samples by means of a heated glass-lined probe. Wet catch

samples were collected in the back half of the Method 5 sampling train and analyzed as per

Wisconsin DNR Protocol.

An integrated flue gas sample was extracted simultaneously with each particulate

sample using a specially designed gas sampling system. Integrated flue gas samples were

collected in 44-liter Tedlar bags housed in a protective aluminum container. After sampling

was complete, the bags were returned to the laboratory for Orsat analysis. Prior to sampling,

the Tedlar bags are leak checked at 15 IN.HG. vacuum with an in-line rotameter. Bags with

any detectable inleakage are discarded.

Testing was conducted from 2 test ports oriented at 90 degrees on the stack. The test

ports are located diameters downstream and diameters upstream of the nearest flow

disturbances. A -point traverse was used to collect representative particulate samples. Each

traverse point was sampled minutes to give a total sampling time of minutes per run.

The important results of the test are summarized in Section 2. Detailed results are

presented in Section 3. Field data and all other supporting information are presented in the

appendices.

1

I I I I I I I I I I I I I I I I I I I

2 SUMMARY AND DISCUSSION

The results of the particulate emission tests are summarized in Tables 1 - 4. An

overview of the results is presented in the table below.

Concentration Emission Rate

Source (CWDSCF) (LBIHR)

Line 2 RTO Outlet Stack 0.0376 20

Surface Cyclone Exhaust 0.175 46

Core Cyclone Outlet 0.146 36

RTO Inlet Duct 0.147 79

No difficulties were encountered in the field or in the laboratory evaluation of the

samples. On the basis of this fact and a complete review of the entire data and results, it is

our opinion that the results reported herein are accurate and closely reflect the actual values

which existed at the time the test was performed.

2

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I I I I 1

I1 I I I I I I I I I I I I I

3 RESULTS

The results of all field and laboratory evaluations are presented in this section. Gas

composition (Orsat and moisture) are presented first followed by the computer printout of

the particulate results. Preliminary measurements including test port locations are given in

the appendices.

The results have been calculated on a personal computer using programs written in

Extended BASIC specifically for source testing calculations. EPA-published equations have

been used as the basis of the calculation techniques in these programs. The particulate

emission rate has been calculated using the product of the concentration times flow method.

11

I I I I 1

I 1 I I I I I I I I I 1 I I I

3.1 Results of Orsat & Moisture Analyses

12

I I I I! I I I I I I I I I I I I I I I

I n t e r p o l l Labs R e p o r t No. 4-3068 L o u i s i a n a P a c i f i c C o r p o r a t i o n

Hayward, W I

T e s t No. 1 L i n e 2 R T O O u t l e t S t a c k

R e s u l t s o f O r s a t S M o i s t u r e Ana lyses - - - - -Me thods 3 S 4 ( 2 v / v )

Date o f r u n

D r y b a s i s ( o r s a t )

c a r b o n d i o x i d e . . . . . . . . . . . . oxygen .................... c a r b o n monoxide . . . . . . . . . . . n i t r o g e n . . . . . . . . . . . . . . . . . .

Wet b a s i s ( o r s a t )

c a r b o n d i o x i d e . . . . . . . . . . . .

oxygen .................... c a r b o n monox ide . . . . . . . . . . . n i t r o g e n . . . . . . . . . . . . . . . . . . w a t e r vaDor . . . . . . . . . . . . . . .

D r y m o l e c u l a r w e i g h t . . . . . . . . Wet m o l e c u l a r w e i g h t . . . . . . . . S p e c i f i c g r a v i t y . . . . . . . . . . . . Water mass f l o w . . . . .. (LB/HR)

Run 1 06-02-94

3 . 9 0

16.80

0.00

79.30

3.01

12.95

0.00

61.13

22.91

29.30

26.71

0.923

52915

F O 1 . 0 5 1

I I I, I I I I I I I I I I I I I I

I n t e r p o l 1 Labs R e p o r t No. 4-3068 L o u i s i a n a P a c i f i c C o r p o r a t i o n

Hayward, W I

T e s t No. 2 S u r f a c e C y c l o n e E x h a u s t

R e s u l t s o f O r s a t 8 M o i s t u r e Analyses-----Methods 3 8 4 ( * v / v )

D a t e o f r u n Run 1

06-02 -94


c a r b o n d i o x i d e . . . . . . . . . . . . 3 . 2 0

oxygen .................... 1 7 . 8 0

c a r b o n m o n o x i d e . . . . . . . . . . . 0.00

n i t r o g e n . . . . . . . . . . . . . . . . . . 79.00


c a r b o n d i o x i d e . . . . . . . . . . . . 2.60

oxygen. . . . . . . . . . . . . . . . . . . . 1 4 . 4 4

c a r b o n m o n o x i d e . . . . . . . . . . . 0.00

n i t r o g e n . . . . . . . . . . . . . . . . . . 64.10

w a t e r v a p o r ............... 18.86

D r y m o l e c u l a r w e i g h t . . . . . . . . 29.22

Wet m o l e c u l a r w e i g h t . . . . . . . . 27.11

S p e c i f i c g r a v i t y . . . . . . . . . . . . 0.936

Wate r mass f l o w . . . . . . (LB/HR) 20230

FO 0 . 9 6 9

14

I I I I I I I I I I I I I I I I I I

I n t e r p o l 1 Labs R e p o r t NO. 4-3068 L o u i s i a n a P a c i f i c C o r p o r a t i o n

Hayward, WI

T e s t No. 3 Core C y c l o n e O u t l e t

R e s u l t s o f O r s a t 8 M o i s t u r e Ana lyses - - - - - Me thods 3 B 4 ( 2 v / v )

Date o f r u n Run 1

06-02 -94


c a r b o n d i o x i d e . . . . . . ...... 2.10

o x y g e n . . . . . ............... 18.80

c a r b o n monoxide 0.00

n i t r o g e n . . . . . . . . . . . . . . . . . . 79.10

. . . . . . . . . . .


c a r b o n d i o x i d e . . . . . . . . . . . . 1.78

oxygen .................... 1 5 . 9 3

c a r b o n monox ide . . . . . . . . . . . 0.00

n i t r o g e n . . . . . . . . . . . . . . . . . . 6 7 . 0 1

............... w a t e r v a p o r 1 5 . 2 8

D r y m o l e c u l a r w e i g h t . . . . . . . . 29.09

W e t m o l e c u l a r w e i g h t . . . . . . . . 27.39

S p e c i f i c g r a v i t y . . . . . . . . . . . . 0 . 9 4 6

Water mass f l o w . . . . . . ( LB/HR) 14666

F O 1.000

1 I I I I I I I I I I I I I I I I I

I n t e r p o l 1 L a b s R e p o r t No. 4 - 3 0 6 8 L o u i s i a n a P a c i f i c C o r p o r a t i o n

H a y w a r d , W I

T e s t N o . 4 RTO I n l e t D u c t

R e s u l t s o f O r s a t S M o i s t u r e Analyses----- Methods 3 S 4 ( Z v / v )

D a t e o f run Run 1

0 6 - 0 3 - 9 4

Dry b a s i s ( o r s a t )

c a r b o n d i o x i d e . ........... 3 . 4 0

o x y g e n .................... 1 7 . 5 0

c a r b o n m o n o x i d e . . . . . . . . . . . 0.00

n i t r o g e n . . . . . . . . . . . . . . . . . . 7 9 . 1 0


c a r b o n d i o x i d e . . . . . . . . . . . . 2 . 7 1

o x y g e n .................... 1 3 . 9 6

c a r b o n m o n o x i d e . . . . ....... 0.00

n i t r o g e n . . . . . . . . . . . . . . . . . . 6 3 . 0 9

w a t e r v a D o r . . ............. 2 0 . 2 4

D r y m o l e c u l a r w e l g h t . . . . . . . . 2 9 . 2 4

Wet m o l e c u l a r w e i g h t . . . . . . . . 2 6 . 9 7

S p e c i f i c g r a v i t y . . . . . . . . . . . . 0 . 9 3 2

W a t e r mass f l o w . . . . . . ( L B / H R ) 4 4 6 7 5

F O 1.000

16


3.2 Results of Particulate Determinations

1 7

I I I I I I' I I I I I I I I I I I I I

I n t e r p o l l Labs R e p o r t No. 4 - 3 0 6 8 L o u i s i a n a P a c i f i c C o r p o r a t i o n

Hayward, W I

T e s t No. 1 L i n e 2 RTO O u t l e t S t a c k

R e s u l t s o f P a r t i c u l a t e L o a d i n g D e t e r m i n a t i o n s - - - - - - - Method 5

Date o f r u n

T i m e r u n s t a r t / e n d . . . . . (HRS)

S t a t i c p r e s s u r e . . . . . . ( 1 N . W C ) C r o s s s e c t i o n a l a r e a ( S Q . F T ) P i t o t t u b e c o e f f i c i e n t . . . . . . Wate r in sample gas

c o n d e n s e r . . . . . . . . . . . . . (ML) i m p i n g e r s . . . . . . . . . . ( G R A M S ) d e s i c c a n t . . . . . . . . . . ( G R A M S ) t o t a l . . . . . . . . . . . . . . ( G R A M S )

T o t a l p a r t i c u l a t e m a t e r i a l . . . . . . . . . . . . c o l l e c t e d

Gas m e t e r c o e f f i c i e n t B a r o m e t r i c p r e s s u r e . . Avg. o r i f . p r e s . d r o p . . Avg. gas m e t e r temp. .

g r a m s )

. . . . . . 1 N . H G ) I N . W C ) DEF-F)

Volume t h r o u g h gas m e t e r . . . . a t m e t e r c o n d i t i o n s . . . ( C F ) s t a n d a r d c o n d i t i o n s . ( D S C F )

T o t a l s a m p l i n g t i m e . . . N o z z l e d i a m e t e r . ...... A v g . s t a c k gas temp .. V o l u m e t r i c f l o w r a t e .

a c t u a l . . . . . . . . . . . . . d r y s t a n d a r d . . . . . . .

. ( M I N ) . . ( I N ) DEG-F)

. . . . . . ( A C F M ) DSCFM)

I s o k i n e t i c v a r i a t i o n . . . . . ( 5 )

P a r t i c u l a t e c o n c e n t r a t i o n . . . a c t u a l . . . . . . . . . . . . (GR/ACF) d r y s t a n d a r d . . . . . ( G R / D S C F )

P a r t i c l e mass r a t e . .. (LB/HR)

18

Run 1 0 6 - 0 2 - 9 4

L 6 0 4 / 1 7 1 0

- 0 . 6 7 3 6 . 2 3

. a 4 0

0.0 2 2 7 . 0

1 2 . 0 2 3 9 . 0

0 . 0 9 2 3

0 . 9 9 6 1 2 8 . 9 9

1 . 1 8 8 5 . 5

4 0 . 4 8 3 7 . 9 1

6 4 . 0 0 . 2 4 9

3 2 9

1 2 7 2 4 4 6 3 4 6 8

100.1

0 . 0 1 8 7 3 0 . 0 3 7 5 6

2 0 . 4 4

1 I 'I P 'I I II I I I I I I I I I

I n t e r p o l 1 La.bs R e p o r t No. 4-3068 L o u i s i a n a P a c i f i c C o r p o r a t i o n

Hayward, W I

T e s t No. 2 S u r f a c e C y c l o n e E x h a u s t

R e s u l t s o f P a r t l c u l a t e L o a d l n g Detern inat lons-- - - - - - Method 5

D a t e o f r u n Run 1

06-02-94

Time run s t a r t / e n d . . . . . (HRS) 1844/2000

S t a t l c p r e s s u r e . ..... ( 1 N . W C ) C r o s s s e c t i o n a l a r e a (SQ.FT) P i t o t t u b e c o e f f i c i e n t . . . . . . Water i n sample gas

c o n d e n s e r . . . . . . . . . . . . .( M L ) i m p i n g e r s . . . . . . . . . . (GRAMS) d e s i c c a n t . . . . . . . . . . (GRAMS) t o t a l . . . . . . . . . . . . . . (GRAMS)

T o t a l p a r t i c u l a t e m a t e r i a l . . .......... c o l l e c t e d

Gas m e t e r c o e f f i c i e n t B a r o m e t r i c p r e s s u r e . . Avg. o r i f . p r e s . d r o p . . Avg. gas m e t e r temp..

g r a m s )

. . . . . . I N . H G ) I N . W C ) DEF-F)

Volume t h r o u g h gas m e t e r . . . . a t m e t e r c o n d i t i o n s . ..( CF) s t a n d a r d c o n d i t i o n s . (DSCF)

T o t a l s a m p l i n g t i m e . . . . ( M I N ) N o z z l e d i a m e t e r . ........( I N ) A v g . s t a c k gas temp ..(DEG-F)

V o l u m e t r i c f l o w r a t e . . . . . . . . d r y s t a n d a r d . . . . . . . (DSCFM)

I s o k i n e t i c v a r i a t i o n . . . . . ('i) P a r t i c u l a t e c o n c e n t r a t i o n . . .

a c t u a l . . . . . . . . . . . . (GR/ACF) d r y s t a n d a r d . . . . . ( GR/DSCF)

P a r t i c l e mass r a t e . . . ( LB/HR)

a c t u a l . . . . . . . . . . . . . . (ACFM)

-14.00 9.62 .040

0.0 118.0 46.0

164.0

0.3763

0.9961

1.03 80.3

28.99

35.20 33.27

60.00 .18S 214

52239 31034

92.2

0.10363 0.17451

46.42

I I I I I I' I I I I I I I I I I I I I

I n t e r p o l 1 Labs R e p o r t No. 4 - 3 0 6 8 L o u i s i a n a P a c i f i c C o r p o r a t i o n

Hayward. W I


R e s u l t s o f P a r t i c u l a t e L o a d i n g D e t e r m i n a t i o n s - - - - - - - Method 5

Date o f r u n Run 1

0 6 - 0 2 - 9 4

Time r u n s t a r t / e n d ..... ( H R S ) 2 1 3 0 / 2 2 3 5

S t a t i c p r e s s u r e . . . . . . ( 1 N . W C ) C r o s s s e c t i o n a l a r e a (SQ.FT) P i t o t t u b e c o e f f i c i e n t . . . . . . Wate r i n sample gas

c o n d e n s e r . . . . . . . . . . . . . (ML) i m p i n g e r s . . . . . . . . . . ( G R A M S ) d e s i c c a n t . . . . . . . . . . ( G R A M S ) t o t a l . . . . . . . . . . . . . . ( G R A M S )

T o t a l p a r t i c u l a t e m a t e r i a l . . . . . . . . . . . . c o l l e c t e d ( g r a m s )

Gas m e t e r c o e f f i c i e n B a r o m e t r i c p r e s s u r e . Avg. o r l f . p r e s . d r o p . Avg. gas m e t e r temp. .

. . ..... ( IN.HG) ( 1 N . W C ) ( D E F - F )

Volume t h r o u g h gas m e t e r . . . . a t m e t e r c o n d i t i o n s . . . ( C F ) s t a n d a r d c o n d l t i o n s . ( D S C F )

T o t a l s a m p l i n g t i m e . . . . ( M I N ) N o z z l e d i a m e t e r . . ...... . ( I N ) A v g . s t a c k gas temp . . ( D E G - F )

V o l u m e t r i c f l o w r a t e . . . . . . . . a c t u a l . . . . . . . . . . . . . . (ACFM) d r y s t a n d a r d . . . . . . . ( D S C F M )

I s o k i n e t i c v a r i a t i o n . . . . . ( % )

P a r t i c u l a t e c o n c e n t r a t i o n . . . a c t u a l . . .......... ( G R / A C F ) d r y s t a n d a r d . . . . . ( G R / D S C F )

P a r t i c l e mass r a t e . . . ( L B / H R )

20

- 1 4 . 0 0 9 . 6 2 . 8 4 0

0 .0 1 1 5 . 0

9 . 0 1 2 4 . 0

0 .3058

0 . 9 9 6 1

0 . 9 5 7 1 . 0

2 8 . 9 9

3 3 . 7 0 3 2 . 4 1

60.00 . 1 8 5

2 1 9

4 7 0 4 7 2 8 9 8 1

9 6 . 1

0 . 0 8 9 6 6 0 . 1 4 5 6 0

3 6 . 1 7

I I I I I I I I I I I I I I I I I

I n t e r p o l 1 L a b s R e p o r t No. 4 - 3 0 6 8 L o u i s i a n a P a c i f i c C o r p o r a t i o n

H a y w a r d . W I

T e s t No. 4 RTO I n l e t D u c t

R e s u l t s o f P a r t l c u l a t e Loading D e t e r m i n a t i o n s - - - - - - - M e t h o d 5

D a t e o f r u n

T i me r u n s t a r t / e n d . . . . . (HRS)

S t a t i c p r e s s u r e . . . . . . (1N.WC) C r o s s s e c t i o n a l a r e a ( S Q . F T ) P i t o t t u b e c o e f f i c i e n t . . .... W a t e r i n s a m p l e g a s

c o n d e n s e r . . . . . . . . . . . . . ( M L ) i m p i n g e r s . . . . . . . . . . ( G R A M S ) d e s i c c a n t . . . . . . . . . . (GRAMS) t o t a l . . ............ (GRAMS)

T o t a l D a r t i c u l a t e m a t e r i a l . . . . . . . . . . . . c o l l e c t e d

Gas m e t e r c o e f f i c i e n t B a r o m e t r i c p r e s s u r e . . A v g . o r i f . p r e s . d r o p . . A v g . g a s m e t e r t e m p . .

g r a m s )

. . . . . . I N . H G ) I N . W C ) DEF-F)

Vo lume t h r o u g h g a s m e t e r . . . . a t m e t e r c o n d i t i o n s ... ( C F ) s t a n d a r d c o n d i t i o n s . (DSCF)

T o t a l s a m p l i n g t i m e . . . . ( M I N ) N o z z l e d i a m e t e r . . . ...... ( I N ) A v g . s t a c k g a s t e m p . . (DEG-F)

V o l u m e t r i c f l o w r a t e . . . . . . . . a c t u a l . . . . . . . . . . . . . . (ACFM) d r y s t a n d a r d . . . . . . .( DSCFM)

I s o k i n e t i c v a r i a t i o n . . . . . ( % )

P a r t i c u l a t e c o n c e n a c t u a l . . ........ d r y s t a n d a r d . . . .

P a r t i c l e mass r a t e

r a t i o n . . . . (GR/ACF) (GR/DSCF)

. . ( L B / H R )

2 1

R u n 1 0 6 - 0 3 - 9 4

4 5 / 1 4 7

-6.00 2 3 . 7 6

. 8 4 0

0.0 1 5 3 . 0

1 5 . 0 1 6 8 . 0

0 . 2 9 6 4

0 . 9 9 6 1 2 8 . 9 9

0 . 8 8 70 .7

3 2 . 4 5 3 1 . 2 2

60.00

2 0 9 . la5

1 0 4 4 1 8 6 2 7 6 6

1 0 5 . 6

0 . 0 8 8 0 3 0 . 1 4 6 5 1

1 8 . 8 2

'I 1 I I 'I 'I <I :I 'I I 'I I

'I I

'I I

I I

I I I I

APPENDIX A

VOLUMETRIC FLOW RATE DETERMINATIONS

I I I I I 1 I I I I I I I 1 I I I I I!

I n t e r p o l 1 Labs R e p o r t No. 4-3068 L o u i s i a n a P a c i f i c C o r p o r a t i o n

Hayward, W I

T e s t No. 1 L i n e 2 RTO O u t l e t S t a c k

R e s u l t s o f Volumetr ic F l o w Rate Determinat ion- - - - - - - Method 2

D a t e o f D e t e r m i n a t i o n . . . . . . . . . . . . Time o f D e t e r m i n a t i o n . . . . . . . (HRS)

B a r o m e t r i c p r e s s u r e . ...... ( 1 N . H G )

P i t o t t u b e c o e f f i c i e n t . . . . . ......

Number o f s a m p l i n g p o r t s ......... T o t a l number o f p o i n t s . . . . . . . . . . . Shape o f d u c t . . . ................. S t a c k d i a m e t e r . . . . . . . . . . . . . . . ( I N )

Duct a r e a . . . . . . . . . . . . . . . . . (SQ.FT)

D i r e c t i o n o f f l o w . . . . . . . . . . . . . . . .

S t a t i c p r e s s u r e . . . . . . . . . . . (1N.WC)

Avg. gas temp . . . . . . . . . . . . . (DEG-F)

M o i s t u r e c o n t e n t . . . . . . . . . . ( 8 V / V )

Avg. l i n e a r v e l o c i t y ..... (FT/SEC)

Gas d e n s i t y . . . . . . . . . . . . . . (LB/ACF)

M o l e c u l a r w e i g h t . . . . . . (LB/LBMOLE)

Mass f l o w o f gas . . . . . . . . . . (LB/HR)

V o l u m e t r i c f l o w r a t e . . . . . . . . . . . . . a c t u a l . . ................. (ACFM) d r y s t a n d a r d . . . . . . . . . . . . (DSCFM)

06-02-94

1520

28.99

.84

2

16

Round

81.5

36.23

UP

-. 67 326

22.91

59.9

.04507

29.30

352131

130227 65230

A- 1


Hayward, W I

T e s t No. 2 S u r f a c e C y c l o n e Exhaust

R e s u l t s o f V o l u r n e t r l c F l o w R a t e D e t e r r n l n a t i o n - - - - - - - H e t h o d 2

D a t e o f D e t e r m i n a t i o n . . . . . . . . . . . . Time o f D e t e r m i n a t i o n . . . . . . . ( H R S )

0 6 - 0 2 - 9 4

1815

B a r o m e t r i c p r e s s u r e . . . . . . . ( I N .

P i t o t t u b e c o e f f i c i e n t . . . . . . . .

Number o f s a m p l i n g p o r t s . . . . . T o t a l number o f p o i n t s . ...... Shape o f d u c t . . .............. S t a c k d i a m e t e r . . . . . . . . . . . . . . . D u c t a r e a . ................ (SQ

2 9 . 2 2

. 8 4

2

24

Round

42

9 . 6 2

D i r e c t i o n o f f l o w ................

S t a t i c p r e s s u r e . . . . ....... (1N.WC)

DOWN

-14

Avg. gas temp. . . . . M o i s t u r e c o n t e n t .

Avg. l i n e a r v e l o c

Gas d e n s i t y . . . . .. M o l e c u l a r w e i g h t .

. . . . . . . . (DEG-F)

........ ( % V / V )

t y . . . . . (FT/SEC)

. ...... (LB/ACF)

. . . . ILB/LBMOLE)

2 0 9

18.86

9 1 . 6

. o s 2 3 5

2 9 . 2 2

Mass f l o w o f g a s . . . . . . . . . .

V o l u m e t r i c f l o w r a t e . . . . . . a c t u a l . . . . . . . . . . . . . . . . . . d r y s t a n d a r d . . . . . . . . . . . .

A-2

LB/HR)

. . . . . . ( A C F M ) DSCFM)

1 6 5 9 9 5

5 2 8 5 1 3 1 8 9 0

I' I I I I I I I I I I I I I I I I I I

I I I I I I I I I I I I 1 I I I I I


Hayward, W I


R e s u l t s o f V o l u m e t r i c F l o w R a t e D e t e r m i n a t i o n - - - - - - - M e t h o d 2

Date o f D e t e r m i n a t i o n . . . . . . . . . . . . Time o f D e t e r m i n a t i o n . . . . . . . ( H R S )

B a r o m e t r i c p r e s s u r e . . . . ... ( I N . H G )

P i t o t t u b e c o e f f i c i e n t . . . . . . . . . . .

Number o f s a m p l i n g p o r t s . . . . . . . . . T o t a l number o f p o i n t s . . . . . . . . . . . Shape o f d u c t .................... S t a c k d i a m e t e r . . . . . . . . . . . . . . . ( I N )

D u c t a r e a . ................ (SQ.FT)

D i r e c t i o n o f f l o w . . . . . . . . . . . . . . . .

S t a t i c p r e s s u r e . . . . . . . . . . . ( 1 N . W C )

Avg. gas temp . . . . . . . . . . . . . ( D E G - F )

M o i s t u r e c o n t e n t . . . . . . . . . . ( % V / V )

Avg. l i n e a r v e l o c i t y . . . . . ( F T / S E C )


M o l e c u l a r w e i g h t . . . . . . (LB/LBMOLE)

Mass flow o f gas . . . . . . . . . . ( L B / H R )

V o l u m e t r i c f l o w r a t e . . . . . . . . . . . . . a c t u a l . . . . . . . . . . . . . . . . . . . ( A C F M ) d r y s t a n d a r d . ........... ( D S C F M )

0 6 - 0 2 - 9 4

2 0 0 0

2 8 . 9 9

. 8 4

2

2 4

Round

42

9 . 6 2

UP

- 1 4

2 2 0

1 5 . 2 8

8 1 . 5

. 0 5 1 6 2

2 9 . 0 9

1 4 5 7 3 1

4 7 0 5 4 2 8 9 2 5

A-3

I n t e r p o l 1 Labs R e p o r t No. 4-3068 Lou1 s i a n a P a c i f i c C o r p o r a t i o n

Hayward, W I

T e s t No. 4 RTO I n l e t Duc t

R e s u l t s o f V o l u m e t r i c F l o w R a t e D e t e r m i n a t i o n - - - - - - - Method 2

D a t e o f D e t e r m i n a t i o n . . . . . . . . . . . . Time o f D e t e r m i n a t i o n . . . . . . . ( H R S )

B a r o m e t r i c p r e s s u r e . . ..... (1N.HG)

P i t o t t u b e c o e f f i c i e n t . . . . . . . . . . .

06 -0 3 -9 4

10

29.22

.84

Number o f s a m p l i n g p o r t s . . . . . . . . . 2

T o t a l number o

Shape o f d u c t .

S t a c k d i a m e t e r

D u c t a r e a . . ...

p o i n t s . . . . . . . . . . . .................. . . . . . . . . . . . . . . ( I N )

. . . . . . . . . . . (SQ.FT)

D i r e c t i o n o f f l o w . . . . . . . . .

S t a t i c p r e s s u r e . . . . . . . . . . . Avg. gas temp . . . . . . . . . . . . . M o i s t u r e c o n t e n t . . . . . .....

. . . . . .

I N . W C )

D E G - F )

ta V / V )

Avg. l i n e a r v e l o c i t y ..... (FT/SEC)


M o l e c u l a r w e i g h t . . . . . . ( LB/LBMOLE)

Mass f l o w o f gas .......... (LB/HR)

V o l u m e t r i c f l o w r a t e . . . . . . . . . . . . . a c t u a l . . ................. (ACFM) d r y s t a n d a r d . . . . . . . . . . . . ( D S C F M )

24

Round

66

23.76

HORIZONTAL

-6

199

20.24

72.6

.05397

29.24

335119

103486 63611

A14

I I I I I 1 I I I I 1 I I I I I I I .I


APPENDIX B

FIELD DATA SHEETS

I I I I I I I I I I #I I I I I I I I I

INTERPOLL LABORATORIES, INC. 16 12) 786-6020

EPA Method 2 Field Data Sheet Drawing of Test Site

Cross-section Elevation Job

Test / Run-Date 6 - a - ?f View View Stack Dimen. Zf .s- IN.

Manometer i3 Reg. fi €.up f i f lec. 3arometric Pressure J?.2Z IN.HC Static Pressure IN.WC Operators 0H Pitot No. C.

C N Buib O F Wet bulb O F

032594C:~TACKlWP\FORMS\S-392.1 B-1

lob Source Test Stack Dimen.

INTERPOLL LABORATORIES, INC. (6 12) 786-6020

Data Sheet Drawing of Test Site

Cross-section Elevation

I I

~

O F

IN.HC IN.WC 1 EElec.

Wet bulb E Exp

=s*99 Static Pressure -.I 7 Operators k 7 - - D M Pitot So. z9v-g. c

G O F

Dry Bulb ibIanometer Barometric Pressure

Time End:/C(jO HRS 1 Temp. Meas. Oevice & SIN:

I I I I I I I I I I I I I I I I I

I I I I I I I I I I I

I I I I I I I

i

INTERPOLL LABORATORIES, I N C (612) 786-6020

Interpoll Laboratories EPA Method 5/17 Sample Log Sheet

Job Da~ef$-Z-& Ten / Run <& Source No. of traverse points

Sample Train Leak Check Method Filter p: 4// p$.!lg/)c

Pretesr: $ 0.02 cfm ar 15 in. Hg. (vac) k os tm a cim at ,A in. ~ g . (vac) & Paniculate Catch Data:

Xo. of filters used: Recovery soivent(s)

3/ad-?/

No. of probe wash borrles: Sample recovered by:

M e t o n e G other(s)

Condensate Data:

Weighr e) Final TaR Difference

d Z

I

Integrated Gas Sampling Data:

Bag Pump No. Z$w- Box No. & B q N 0 . L

Pretest leak check: cdmin ar Time s u n : Sampling me:

S/N of 0, Analyzer used to monitor train outlet:

4*L 0% Material: Slaver Aluminized Tedlar Size: - (HRS) Time end

,g * cdmin Operator:

:.

!?.

.. r

I

Cross-section View


EPA Method 2 Field Data Sheet

Elevation View

I I I

I I

Stack Dimen. 4a’- IN. Dry Bulb R / . P F Wet bulb /&L,‘ O F

Manometer Reg. c! Exp GEL. Barometric Pressure SPA 7 IN.HG Static Pressure - / y & IN.WC Operators C=kc F7- Pitot No. 29 v c/ c. - s 4

R or nothing - reg. manometer; 5 - expanded, E - e earonic

032594-C:\STACI<\WFlFORMS\S-392.1

5-5


Final Tare

/ / @ \

-5 Ig

1454 1 %B

1 a (


Difference

I / $'

46


Bag Pump No. z.9 le- Box No. 2-9 B a g N 0 . k

Pretest leak check: cdmin at 1 K n . Hg. Bag Material: Slaver Aluminized Tedlar Size: 44L

Time start: (HRS) Time end (HRS) Sampling rate: y m cdmin Operator: e/ SM of 0, Analyzer used to monitor train outlet: 9

P


I I

I

I I I I I I

I I I

8-7

INTERPOLL LABORATORIES - EPA METHOD 2 FIELD DATA SHEET

C r o s s - s e c t i o n /#Ad G .

s o u r c e ede <JMIH Qdzw7- T e s t __ 3 Run - D a t e k - Z - f / S t a c k d i m e n . 1/= IN.

M a n o m e t e r : s g . o ~ x p . o E l e c .

Barome t r i c p r e s s u r e Z&49 i n Hg

S t a t i c p r e s s u r e -/dd i n wc O p e r a t o r s b-7- P i t o t No.Rqf- '! C p I

D r y b u l b __ O F Wet b u l b __ OF

E l e v a t i o n View V i e w

5-3921 ~~~ ~~~ - R-R R o r n o t h i n g - r e g . manometer ; S- e x p a n d e d ; € - e l e c t r o n i c

D r a w i n g o f T e s t S i t e -

I I I I I I I

INTERPOLL LAROHATOHIES EPA METHOD 5/17 SAMPLE LOG SHEET

Final

I I I

Tare Difference

I I I

Sample Train Leak Check:

Pretest: ( 0.02 cfm at 15 in. Hg. (vac) $( Postest: - 3 cfm at 3 in. Hg. (vac )

Particulate Catch Data:

No.5 of filters used: Recovery solvent ( 5 )

acetone 0 other(s)

44.0 /

No. of probe wash bottles: Sample recovered by:

Condensate Data:

/;.@\ ' Impinger NO. 1

Impinger No. 2

Y

I , 6 4 //f Impinger No. 3 w

I I I] Condenser

.......... _ _ _ _ ................. ...... ...... __ .. _ _ ... ._ .. _ _ _ ....... . ----- -,~- -.... ..... ........................... ." Total I _.


Rag Pump No. Z ~ A 50,: No. x?' Bag No. 3 Bag Material: 5-layer Aluminized Tedlar Size:

Pretest leal: check: ,& cc/min at /c in. Hq.

Time start: AI3/ (HRS) Time end: C?23if (HRS)

Sampling rate: q& cc/min Operator: 67- e S/N of 0, Analyzer used to monitor train outlet:

CF-t:iZZ

..

\

B-9 S-0046RR

1

-I

e e W c 2

n

-

B-10

I I I I I I I I I' I E E I I:, I k I 1 it

Traverse ? o m NO.

!

INTERPOL1 LABORATORIES, INC. (61 2) 786-6020

I , ' , , ~ 2 €PA Method 2 Field Data Sheet

Fraction Distance

Diameter Wall (IN.) From End o i POR (IN.1 Velocity Temp. o i Cas (00 o i From Scad Distance

-. .

stack Dimen. IN. O F Dry Bulb O F Wet bulb

.Llanometer %Reg. r i ~ x p cElec. 3arometric Pressure a9. JL Stark Pressure +#I fl IN.WC

-

Operators F7--Q+ Pitot iUo. a4 J G c. - f Y

Drawing o i Test Site R /I



Date,k3+%!est .;/ Run / No. of traverse points

Job 2- Source A%@ &Jy hIethod 4- Filter holder: /‘‘4&S Filter type: Sample Train Leak Check

Pretest: 5 0 0 cfm at 15 in. Hg. (vac)&. Post test: - d ciin at .// in. Hg. (VacA,

Particulate Catch Data:

No. of filters used Recovery solvent(s)

&ketone Clother@)

4@3

/ No. of probe wash bottles: Sample recovered by: r 2 - 7 -

Condensate Data:

Weight (g) Final Tare Difference

(i”

3J-3 1 /BO( /-G-3

/& 7 /& Is-

D /


Bag Pump No. 2 9#- Box No. G? 3 Bag N o . 1

Pretest leak check Time start: Sampling rate:

S / N of 0, Analyzer used to monitor train outlet:

44 L Bag Material: 5-laver Aluminized Tedlar Size: _. a cdmin at / in. Hg. (HRS) Time end: (HRS) 3 z E cclmin Operator: E?

.q 12309 j-G \STACKlWP\blETHODS\S-O046RR

_ _ . - ~. -~

8-12

I I I I I I I I 1 1 I I I I I I I I ‘I

I I E

I I

1

8-13 I

I I I 1 I 1 I I I I I I I I I I I I I

APPENDIX C

INTERPOLL LABORATORIES ANALYTICAL DATA

I I I I 1 I I I I I I I I I I I I

x . . . '

Ambient A i r CIA Check EPCI Method 3 guide lines'.^ Orsat Analyzer System L e a k Check Fuel Type Fe Within EPCI M-3 G u i d e l i n e s . Coal : . . , . for fuel t y p e . A n t h r a c i t e A i g n i t e .'1.016-1i l'Z0' . .

F0 Range ..*:... . . : . . I . . . . . . . - . . .

Bituminous 1. Q83-1 - 250 . ' .

Where F = 20.9-0, O i l : CO, D i s t i 1 late 1.. 260-1.4 1s

Residual :1.210-1. ,370

Natural 1.600-1.936 Praaanc 1.434-1.396

Gas:

F=Flask (250 cc all g l a s s ) B = T e d l a r Bag (Z- layer)

I -r -. . - Butane

C-1 Woad/Wood B a r k

No. Buret Readings ( m l ) Conc. of Co, An. Zero P t . After CO, AIter 0= %v/v D r y

1 0.00 3 . za 21.00 3.- . 2 ,Q&o 3 e 2 0 21.00 3 - 2 0

I I I I I I

0 Ambient 6ir QCI Check 0 Orsat Analyzer System Leak Check 0 Fg Within EPCI M-3 Guidelines

for fuel type. Where F,= 20.9-Oa

CDZ

F=Flask (250 cc all glass) B=Tedl ar Bag (5-1 dyer) c-2

EPCI Method 3 Guidelines '. Fuel TvDe FB Range . . . Coal :

Anthracite/Lignite 1.016-1-1Z0 Bituminous i.oax-i.2;o Oil:

Distillate Residual

1 260-1.4 15 ,1.,210-1.570

I I

Gas:

I Natural 1.6Q0-1- 936.. Propane 1.435-1.596 Butane 1.405-1.553

Wood/WOOd Bark 1.0QQ-l.lJ0

I @Ambient A i r GlcI Check €PA Method 3 Guidel'ines g Orsat Analyzer System Leak Check Fuel Type % F0 Ranqe 0 Fg Within EPA H-3 Guidelines - Coal:

for f u e l type. Anthraci te/Lignite l.Gl16-1.1J0 Bituminous 1. 083-1.230

I I corl

Where F,= 20.9-0= ~. ~ - _ _ _

Oil: Disti 11 ate Residual

1..260-1.413 1.220-1.370

Gas: Natural 1.600-1.856 Propane 1.43-1.336

F=Flask (250 cc all glass) Butane 1.405- 1.55.7 B=Tedl ar B a g (5-1 ayer ) c-3 Wood/Wood Bark 1. 000- 1.150

I

.. T e s t No.

-I I I I I I

I n t e r p o l 1 Labora tor ies (612) 786-6020

T e s t I R u n L Log Number 3Oh+o 2T Comments

T e s t A R u n L Log Number- 031 Comments

EPFI flethod 5 D a t a R e p o r t i n g S h e e t Impinger C a t c h / W i s c o n s i n P r o t o c o l

Job L P//J,- a S o u r c e Team Leader T e s t S i t e 1 D a t e S u b m i t t e d ' D a t e of T e s t

I

I I

T e s t No. I No. of Huns Cam D a t e of A n a l y s i s 6 l 3 F l v Techn ic ian

D i s h No. 20 D i s h No. D i s h T a r e W t . 4'&:3$ D i s h c S a m p l e W t . LI g D i s h t S a m p l e W t . & , a 3 g S a m p l e W t . 0.6082 g S a m p l e W t . 0 . W 3 0 g

D i s h No. 44 D i s h No. g D i s h Tar-; D i s h T a r e W t . 4?./,/91

D i s h c S a m p l e W t . g CishcSample W t . . ~ .5b- g S a m p l e W t . 6.0$09 g S a m p l e W t .

maturi fiqueous Pbaee Sol vent Phase I D1z.h T a r e W t .

T es t -Run 0 F i e l d B l a n k Loq N u m b e r Comment-,

Log ?!umber Comments

D i s h T a r e W t . g D i s h T a r e W t . 9 D i sh+Sampl e W t . g D ish+Sample W t . 9 S a m p l e W t . g S a m p l e W t . 9

47 D i s h No. LZZ D i s h T a r e W t . Yf, uLs3 g D i s h T a r e W t . D i s h + S a m p l e Wt.- S a m p l e W t . O.OZo+ g

Log Number Comments

.- I

...

.)

:_.

I I

R e s u l t s Solwen-d : TEs72 Bl$i&Vvent W t . g I F i e l d E l k . R u n 1 R u n 2 R u n 3 R u n R u n 5

I F i e l d E l k . R u n 1 R u n 2 R u n 3 Run 4 R u n 5

I *0688-/1 .Oc/47. I ' O / @ / I .I7203 I I. R e s u l t s Aqueous Phase:

C r - c I .D430 I .040q I - o / q b I . 0 3 3 $ I c J 1LSC-0311YR

I n t e r p o l 1 Labora to r iEs ($12) 75LI-ia=m

EPFI M e t h o d 5 D a t a R e p o r t i n g Sheet P r o b o / C y c l o n e W a s h

o I 1 1

I

- F i e l d Ylank D i s h T a r e U t . &/3L264 9 Log ? J u m t a r A , ( i - - 0 1 P Di s h c S a m p l 2 W t . '.'ol. o f S o l v e n t a m 1 Sample U t . +Solvent Residue=uq/ml

-: T e s t I R u n / D i s h NO. 5 0 / V a l . o f So lven t 45 ml D i s h T a r e W t . 42 W47 q Laq N u m b e r f o L 3- 02-p D i s h + S a m p l e W t . Y7,27b? 4

1' D i s h No. 306

'dol. a+ So lven t 70 m l C i s h Tare U t . Y2.8339 '3 Lag Number 3 o b R - 03-P D i sh+Sampl e W t . rl2.1195 - h 3

T e s t A R u n I

Sample U t . 0.06 17 4 I I c o m m e n t s

I

4 I 1 ' 5 I

D i s h Plo. 4 D i s h T a r s W t . Y7.3?91 a3

~

5 T e s t 4 Run I D i s h NO. 'v'al. a f So lvent i t 5 m l C i s h T a r e U t . 5 6. &IC, 9 Lag NumberJnr . , y - a S - f D i s h c S a m p l e W t . 50.1 155 4 Comments S a m p l e W t . cr,o3iq 9

t.'al. of S o l v e n t m l D i s h T a r e W t . 9 Lag Number D i s h c S a m p l e U t . 9 Caamen t s S a m p l e W t . 9

T e s t R u n C i s h N o .

Lag Number 3 o L D i s h c S a m p l e Wt.yT.51 E9 c; Cornman t s S a m p l e U t . 0.13 92 4'

I I

~

I I I I I I I I 1 I I I I I I I I I I

d , o l v t 0 . ~ ~ 4 7

I n t e r p o l 1 Labora tor ies (612) 796-bQZQ

EPf2 Method 5 Data Report ing Sheet F i l t e r Grav imetr ic5

0.1 289 1 U , t t o 8

Test S i t e Date of Test

617. /d

Job Source Team Leader Fd 7,br .L Date Submitted 61.3 id Test No. Date o f Anal y 5 i s Techni c1 an

~ ~

Test -Run 0 F i l t e r No. 4065

Log Number 3 ~ 1 ~ ~ -01-F F i l t e r Tare W t . (1.6220 F i e l d Blank F i l t e r Type 4" PAi/f(L-*

Comments F i l ter+Sample Wt .C .b? 27 9 Sample W t . 0.40 7 9

9

Test L R u n 1 F i 1 t e r No. 'I O b 1 Log Number 30/. ri - 0 2 - F F i l t e r Type 4" ~ ~ ' c r l ~ / c ~ Comments F i l t e r Tare W t . u . 6 t 5 0 9

F i 1 t er +Sampl e W t -0.6372 9 Sample U t . O . d Y 7 - 9

Test 2 R u n I F i 1 t e r No. 4004 Log Number 30 b g - 0 3 - f F i 1 t e r Type 4" P d J / l c * Comments F i l t e r Tare W t . /I, b 9

Fi l tercSample Wt.QBCIPb g Sample W t . o , r r q 7 9

Test L R u n F i 1 t e r No. 4001 Loq Number 3 0 & ? - O d - F F i l t e r Type 4" LffgM Comments F i l t e r Tare Ut. (J*b265 9

Fi l ter+Sample Wt.O.lSF4 9 Sample W t . 0. I r a 9 9

Test L R u n F i l t e r No. 4 0 0 3 Log Number 3965- O s - I = F i 1 t e r Type qr' PLl14(e% Comments F i l t e r Tare W t . O . b Z 9 0 9

F i 1 ter+Sampl e W t .D.5Ytolgg ; Sample W t . 0. -&LO

Test - R u n - F i 1 t e r No. Log Number F i l t e r Type Comments F i l t e r Tare W t . 9

Fi l ter+Sample W t . 9 Sample W t . 9

Rerul ts: F i e l d Blk. R u n 1 R u n 2 R u n 3 R u n 4 R u n 5

T I C-8

r Y

3 3 E

.

I I I I I I I I I I I 1 I 1 1 1 1 I I -

I I I I I 'I I I . I I I

I I I I I I I

5 4 5

c-9

r 5

> 0

2

I I I I I I I

c-10

z W C CJ .- I C ur

*n 0

c-11

I I I I I I I I I I I I I I I I I I I.

APPENDIX D

SAMPLING TRAIN CALIBRATION DATA

I I I I I I I I I I 1 I I I I I I I

0 C H

- w - -

In S Y c rn 0 UI m VI

V C

8 0 U

L Q

m

a

m

7

m

T r m 0 X 0

L al c al z

m

Q

m 'CT rl m

Q (0

m m

. m m W 8 0 3 z 9

c m

Y L L al 0 rn P W L a al e 0

- "

c)

H al U c VI

c1 : m

L 0

m

"

0 z X 0

L W U

m

H

al

L W

0 z U L 0 P al a

W VI 3 e 0 al U

0 m

8 0 T c m L Q 7 c m 0

c VI m - al 0 8

VI

L al c

T

2

e r 3

.c c al E 3

rn

- 2 c m U 0 c *

0-1

OZH S3H3NI - lVIlN3t13MJIO D- 3

In te rpo l1 Laboratories, I n c .

(612) 786-6020

Nozzle C a l i b r a t i o n

Data Sheet

Date o f Cal ibra t ion: 06-02-94

Technician: Ed Trowbridge

Nozzle Number 10-3

The nozzle i s rotated i n 60 degree increments and the diameter a t each

point i s measured t o the nearest 0.001 inch. The observed readings and

average are shown below.

Pos i t i on Diameter

( i nches 1

1 .185

2 .185

3 .I85

Average: .185

D-4

I I I 1 I I I I I I I I I I I I I I I

I I I I I B I 1 I I I I I I I I I I I

~

~ _ _ 0-5

In terpol 1 Laboratories, Inc .

(612) 786-6020

Nozzle Calibration Data Sheet

Date o f Cal ibrat ion: 06-02-94

Technician: Ed Trowbridge

Nozzle Number 10-4

The nozzle i s rotated i n 60 degree increments and the diameter a t each

point i s measured t o the nearest 0.001 inch. The observed readings and

average are shown below.

Posi t ion Diameter

f inches)

1 .249

2 .249

Average : .249

I n t e r w l l Laboratories. Inc.

Temoerature Measurement Oevice Cal i brat ion Sheet

Temperature of Standard or

Simulated Temp (OF)

u n i t under test :

#-z J vendor OflEGA node1 k d Z / se r ia l Number

Range OF Thermocouple TYW k Date o f Cal ibrat ion //7/9-/ Technician 3 b % d &L?U&k-

Response of Un i t Under Test

(OF1

Method o f Calibrat ion: a Comaartson against AS111 aercurv in glass thermoaeter using a thermostatted and insu16ted alumnull black desrgnec

to provide unifori tenuerature. The teioerature i s adjusted by aa~ustinq the voltaqe on the Block heater cartridge. Onega Model CL-300 Tvoe I Theraocouole Srmulator which Drovides 22 precise teaoerature eouivalent iillivalt signais. The CL-300 i s cold junction coaoensared. Callbratlon accuracy i s f 0.1s af soan ~ Z I O O O F I 1 degree Ifor negative temperatures add t 2 degrees. The CL-300 slnulates exactly the iillivoltage Of a Tvpe L theriocouole at the rndrcated temoerature.

Oesi red Temp (OF)

Nomina1

0 100 200 300 400 500 600 700 800 900

1000 1100 1200 1300 1400 1500 1600 1700 1800 1900 2000 2100

I I

I I Averages:

OF = o f f scale. response by u n i t under tes t (OF) X dev = 100 At / (460 + t)

Uni t i n tolerance . _ - ~

~~ Unit- was not in to1ecance:~~recalibrated - See new ca l ib ra t ion sheet. ~~

I I I I 1 1 I I I I I I I I I I I I

5-433 I


J* /.+ ' Interpoll Laboratories. Inc. Y 5 . " ,

Temmratum Measurement Oevic~ Calibration s h e d

Method o f Calibration: 13 Caroariron against ASTll tercury in 9 l a s t k e r i o w t r r using I t h m a s t a t u d and insulated alusinur bloct d s i q n d

ta p r m i d r uai fon teroeraturr. Tha tenperatun ir adjusted by adjustin( the roltaqr 01 the blast heatar cartridqr. Orrgr Ilodrl CL-100 Tvor I Thermcouolr Sirulator rhich oravidar 21 PrKisr teroeraturr Mnivalemt nillivolt rlqnal8. Th a-300 i s cold junction conoensated. Calibration accuracy ir 0.1s a t soan I Z t O O ~ 1 ?. 1 deqrce (for neqatirr teroeratures add Thr CL-100 r i t u l a t e r exactly tha r l i l i v a l t a g e of 1 TyOe L

tharmcouolr a t thr Indlcaced tenneraturr. 1 degrees.

Oesi red Temperature of

N O ~ nal sfmulated Temp (OF) Temp (OF) standard or

I 1 I

0 100 200 300 400 500 600

000 900

1000 1100 1200 1300 1400 1500 1600 1700 1800 1900 2000 2100

roo

I I

~

Response Of Unit Under Test

( O F )

Averages:

OF = o f f scale resoonse by unit under test (OF) X dev = 100 At / (460 + t)

e v i at ion

L h T r

Unit in tolerance Unit was not in tolerance: recalibrated- See new calibration sheet. a

0-7 s-433

Interpoll Laboratories, Inc. (61 2) 786-6020

S-Tvoe Pitot Tube lnsoection Sheet

Pitot Tube No.2Y-h

Pitot tube dimensions:

1, External tubing diameter (DJ I 3)6 IN.

2. Base to Side A opening Plane (PA)

3. Base to Side 8 opening plane (Pd

' qhd IN.

' $68 IN.

Alignment:

4. a, 5. 0, < loo

6. 8, < 5' D 7. 8, < 5' 1

9. W <.0625" &'

Distance from Pitot to Probe ComDonents:

10. Pitot to 0.500 IN. nozzle I .74-.% IN.

I I . Pitot to probe sheath r s o IN.

12. Pitot to thermocouple (parallel to probe) 7% IN.

13. Pitot to thermocouple (perpendicular to probe) 7 d IN.

Meets all EPA design criteria thus C, - 0.84 Does not meet EPA design criteria - thus calibrate in wind tunnel. 0 c, -

Date of Inspection: Inspected by:

5-348

I I I I I I I

.I I I I I I I I I I I I 1 I I I I I I

Interpoll Laboratories, Inc. (612) 786-6020

S-TyDe Pitot Tube lnsoection Sheet

Pitot Tube No.?=

Pitot tube dimensions:

/ .3/6 IN. 1. External tubing diameter (DJ

2. Base to Side A opening plane (PA) : q b d IN,

3. Base to Side B opening plane (Pd 4 &z IN.

Alignmenf:

6. B, < 5' D 7. B, < 5' /3

8 . 2 <.125" 1 8 %

9. w c . 0 6 2 5 " A

Distance from Pitot to Probe Comoonents:

io. Pitot to 0.500 IN. nozzle i 73-d IN.

1 I . Pitot to probe sheath 3.d IN.

12. Pitot to thermocouple (parallel to probe) 3. * IN.

13. Pitot to thermocouple (perpendicular to probe) 7& IN.

,& Meets all €PA design criteria thus C, - 0.84 Does not meet EPA design criteria - thus calibrate in wind tunnel. c, -

Date of Inspection:

CFR Title 40 Part 60 Appenidix A Method 2

Inspected by:

5-348

D-9

Interpoll Laboratories, Inc. I I

(612) 786-6020

S-Tvoe Pitot Tube lnsoection Sheet

Pitot Tube NO.&

pitot tube dimensions:

1. External tubing diameter (DJ 4 37/6 IN. I

Alignment: I

i "k'B IN.

I qk'd IN.

2. Base to Side A opening plane (PA)

3. Base to Side B opening plane (Pd

4. a, < I O 0 3 5. a* < l o o /I

6 . B, < 5' .+ 7. 5, < 5O

8. Z <.125" 3 d 9. W <.0625" b' 2

I I

Distance from Pitot to Probe Comoonents:

I 3. IN. I

I 1

10. Pitot to 0.500 IN. nozzle I 7g3 IN.

1 1. Pitot to probe sheath

12. Pitot to thermocouple (parallel to probe) 3' a IN.

13. Pitot to thermocouple (perpendicular to probe) )76d IN.

0 0

Meets al l €PA design criteria thus Cp - 0.84 Does not meet €PA design criteria - thus calibrate in wind tunnel.

CP -

I I

Date of Inspection: Inspected by:

A$$& 11- 7-4 L/

CFR Title 40 Pan 60 Appenidix A Method 2 5-348 -

~ ~~ ~~ .~ ~ ~~

~ ~~ .~ ~ .~ ~ ~ .~

0-10 ~~ ~~

1 I I I I I I I I I I I I I I I I I I..

Actual Mercury Barometer Read

INTERPOLL LABORATORIES (612)786-6020

Stack Sampling Department - QA Aneroid Barometer Calibration Sheet

Temperature Ambient Correction Adjsted Mercury Initial Aneriod Difference Temp. Factor Barometer Read Barometer Read (Pba-Pbm)

Date /-4-0/,? Technician Q M o d / c Mercury Column Barometer No. Aneroid Barometer No. 63Las

Has this barometer shown any,consistent problems with calibration? Yes/No. If yes, explain. /YO

Has problem been alleviated? Yes/No. How?

d *Note

Aneroid barometers will be calibrated periodically against a mercury column barometer. The aneroid barometer to be calibrated should be placed in close proximity to the mercury barometer and left to equilibrate for 20-30 minutes before calibrating. Aneriod barometer will be calibrated to the adjusted mercury barometer readings. 5-312

D-11

INTERPOLL LABORATORIES (612)786-6020

Stack Sampling Department - QA Aneroid Barometer Ca l i b ra t i on Sheet &-

Date 3-- 3)- 57 4 i

Technician --E=& Mercury Column Barometer No. .L P4f /

Aneroid Barometer No. L4-Y /Zud&P 2 s A f - d / d u 2 - @ N

Temperature Actual Mercury Ambient Correction Adjsted Mercury I n i t i a l Aneriod Di f ference Barometer Read Temp. Factor Barometer Read Barometer Read (Pba-Pbm)

Has t h i s barometer shown any consistent problems w i th ca l ib ra t ion? Yes/No. ' If yes, explain. - Has problem been a l lev ia ted? Yes/No. How?

*Note

Aneroid barometers w i l l be ca l ib ra ted p e r i o d i c a l l y against a mercury column barometer. The aneroid barometer t o be ca l ib ra ted should be placed i n close p rox im i t y t o the mercury barometer and l e f t t o equ i l ib ra te f o r 20-30 minutes before ca l ibrat ing. Aneriod barometer w i l l be ca l ibrated t o the adjusted mercury - barometer readings. 5-312

D-12

7

I I I I I 1 1 .I I I I I I I I I I I -I

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