AZPES/APP Permit Field Method Training Fall 2016
Transcript of AZPES/APP Permit Field Method Training Fall 2016
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AZPES/APP Permit Field Method Training
Fall 2016
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Not Approved Methods
Color Wheels
Test Strips
Pool Kits
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Approved Methods
Standard Methods – 22nd Edition -4500-Cl B (2011) - Iodometric Method I
-4500-Cl C (2011) - Iodometric Method II
-4500-Cl D (2011) - Amperometric Titration
-4500-Cl E (2011) - LL Amperometric Titr.
-4500-Cl F (2011) - DPD Ferrous Titration
-4500-Cl G (2011) - DPD Colorimetric*
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Most other meters by non-Hach companies are also acceptable
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Calibration
Most meters (including Hach) are
factory calibrated and do not need
routine calibration.
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General Procedure
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General Procedure
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General Procedure
*
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General Procedure
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General Procedure
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Method Required QC Method Blank (or RB): 1 daily. If at or above Reporting Level, immediate corrective action. [DI water + DPD] LFB: At reporting level (control charts 1020B.13 or ADHS will allow recovery ± 10%). At least monthly (Goal – each run). [ADHS will allow 2° Stds, e.g. Spec√s APP Permits only] Duplicates: 1 for each matrix type daily or with each batch of 20 or fewer samples. Control Charts 1020B. Need Record for Each
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NSI Solutions, Inc.
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HACH
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0.5 ml Pipetman
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(0.5 ml of standard added) X (25-30 mg/L Cl2)
10.5 ml (sample cell volume + standard added)
= 1.19-1.43 mg/L
(12 ml sample cell volume + 0.5 ml standard added = 1.00-1.2 mg/L)
Formula for Hach Standard
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Questions?