AIR SAMPLING LOGBOOK€¦ · US EPA Region 4 Yell ow Bluff Air Study Wilcox County, Alabama SESD...

US EPA Region 4 Yell ow Bluff Air Study

Wilcox County, Alabama SESD Project Identification Number: 11-0068

November 2010- December 2010

H2S CALIBRATION/ VERIFICATION

AIR SAMPLING LOGBOOK

LOGBOOK_/_OF j_

DATES: THRU:

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US EPA Region 4 Yellow Bluff Air Study



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H2S Calibration I Verification

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Station I.D. 'fe£ ------

Site Description \ZoLAND eocVdC S~- 9~(~~~)

Date: \jt}j}ll Time: \O:ol Operator: ~6 ~

CALIBRATION SYSTEM

Gas Calibrator ID: E(?A llo'-1 5

MFC(s) Calibrated: I 0 I 7_ I I I b

Gas Cylinder Mfg.: 'SCon--twc UO.iJ\Dt

H2S MONITOR

Monitor ID: ~ A111'UJ

SETTINGS: TEMPERATURES:

COEF: l.ooz INT.: ·3~.3 c AfOu::_\Cf.\

Cylinder ID: ~ 4 z Z) BKG: ~LA PPB CHAMBER: \...{ 4 .1 C

Concentration: 5:1 (]) H2S PPM RANGE: Zoo PPB CONVERTER: 3-z.2..c Cert Date: ~ 1 'LI I IO A VG. TIME: G 0 sec

CALIBRATION SYSTEM H2S MONITOR I DATA LOGGER

Total Flow Concentration Zero Air Cal. Gas Monitor Data Logger Setting Setting Flow Flow cc/min. H2S (PPB) cc/min cc/min H2S (PPB) H2S (PPB)

\9t~ ZERO \ q <6<6 0.00 0. \0 a.3

\ q 1<6 \bD \q 3~ s~~cr7 \s~.Y \S'S 5 '

\q~'{ lO lql?-z. Z.Ll .. Y(o &7. 1 Co~ .. )

[N l1l8L CAU\3~ CATlO~

SETTINGS CHANGED? OR NO (CIRLCE ONE)

NEW SETTINGS: Note: If calibration setting changed, then you must re-verify.

COEF: 0 .Cf. ~ L. BKG: ._j /As PPB RANGE: WO PPB AVG. TIME: (:,0 sec

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Continuation of field record for salnple YfSJ • fA iS ···cR.\ ~Lt>~

Other Notes/Sketch (Include North and Scale)

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Station I.D. 'i t:E -~:....=:.._ __ _

Site Description ~l/:1ND C()()Ptil ~" ~~~ CIY3 rr-4$6

d~h~

Date: .J.J: 33 Time: \\:'53 Operator:~ N~ ~ \ \'V'Ihl

CALIBRATION SYSTEM H2S MONITOR

Gas Calibrator 10: Ff.\ 1\ "llo'1.5

MFC(s) Calibrated: \0 1 1...{ 1 Jo Gas Cylinder Mfg.: SC6r fl..~ UQv\~E

c. ~c.A Cylinder ID: ~ f" Y ZZ \

Concentration: S :/ (!) H2S PPM

Cert Date: ~ I G J I I 0

CALIBRATION SYSTEM

Monitor 10: ~ f}..ll\Zh

SETTINGS:

COEF: C. 9~"2._

BKG: 'tJ J ~ PPB

TEMPERATURES:

INT.: 31..) C

CHAMBER: \..{ 4 • 9 C

RANGE: L..oO PPB CONVERTER: 372 .. C

AVG. TIME: ~([) sec

H2S MONITOR I DATA LOGGER

Total Flow Concentration Zero Air Cal. Gas Monitor Data Logger Setting Setting Flow Flow

cc/min. H2S cc/min cc/min H2S (PPB) H2S (PPB)

\'1~5 ZERO \'1g5 0.00 G, \ (2). \

l(oO \Cf(_g' S<; .C{lf \~~.<D \ (o (l).,. ('])

CHANGED? YES OR (CIRLCE ONE)

Note: If calibration setting changed, then you must re-verify.

BKG:. ____ PPB RANGE:. ___ PPB AVG. TIME:. __ sec

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Continuation of field record for sample 'fffi \.} z: S (&JI1 ~- Y '?!l-f'Q m-yJo lf1


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Station I.D. 't BA. ___;;_ ____ _

Site Description 'f~\;'J 8LVFF"\V\N N ~

Date: 1/zy ftt Time: lb~ 3\.f Operator: 0~ Nct\.t-l

CALIBRATION SYSTEM

Gas Calibrator ID: "f1?~ P,..!lo"'-15

MFC(s) Calibrated: \0 I Z-1 I \0

Gas Cylinder Mfg.: SC.c\1 A\6(_ UQ\li.t£

H2S MONITOR r:s:-1

~ ~~~ ·l~f\\ , Monitor ID: t. ~iii · 1 ·~ qU4b

SEITINGS: TEMPERATURES:

COEF: \ '() 7_/.p INT.: ·?fo~q c cc -\i.Ll,., __Mtz~v\ ~

Cylinder 10: ~ \ \l'i:55 ~7Z.l Q.l \)-z..t\\ \ S :id> o:t d~h I

&~' \ BKG: ~- ~ PPB CHAMBER: 4 [__. Cf C

Concentration: \ ()"' ~ ~2~&~fv1 Cert Date: ff I ~ I --Z!:) \ 0

RANGE: 1-ob PPB CONVERTER:~-rl C

A VG. TIME: (cO sec

CALIBRATION SYSTEM H2S MONITOR I DATA LOGGER

Total Flow Concentration Zero Air Cal. Gas Monitor Data Logger Setting Setting Flow Flow cc/min. H2S (PPB) cc/min cc/min H2S (PPB) H2S (PPB)

\[\q~ ZERO lC{'bC{ 0.00 ·- (0. "3 -z. - (~ol

\~~0 ) (-,0 \q~Q> .ss. .<\~ \54,~ \SY:l

\qto2_ {D \ q (o\,5.{ L_'-\~'-'~ Co<l ~> Co<t .. 1

{ Ntl (A\- c ~~' ToN

-SETTINGS CHANGED? ~ OR NO (CIRLCE ONE)

NEW SEITINGS: Note: If calibration setting changed, then you must re-verify.

COEF:O..,C\qz_ BKG: tJ { ~ PPB RANGE: (._no PPB AVG. TIME: f.oO sec

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Continuation of field record for sample _'(_8_~_._ __________ _


JL\~j At26 ST ..

'-

(

'----l-------J - - -J

-

~-------..__

Smnple Terun Leodcr/Samplec Signatme!Da~ \ I Z,'l \II

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Station I.D. >{ BA Site Description '-/<i),ij)W BW Ft= ~OVJN \-11rt--L

Date: \{2>-{(1\ Time:~;z..g Operator:-=~=----tJ_· -~-------

CALIBRATION SYSTEM

Gas Calibrator ID: ~ f\\ f 0'-\.S

MFC(s) Calibrated: I 0 I '2-1 1 l D

Gas Cylinder Mfg.: "'Sffi'\T Al(L L1 G0lD ~f.{LJ cA.

Cylinder 10: W ~ '-\ 1Z I &~ I \ S .7(!) '( Ufll ' '2\. \\

Concentration: +o • 0; ~S\f{k.~\ Cert Date: <6 I 56 I '2£> ( 0

CALIBRATION SYSTEM Total Flow Concentration Zero Air Cal. Gas

Setting Setting Flow Flow cc/min. H2S (PPB) cc/min cc/min

\<\q'D ZERO \'\G\0 0.00

\CfCfl. }(oo \q 30 55' '11

CA1.- 8fl.l\T1c N Vfl(J

H2S MOf.J!~ 04 ,,~\\)

MonitoriD: ffA ~ CfZ'l:J


COEF: 1 .. OZ/::> INT.: 2.(o,'3 c

BKG: t-JIA PPB CHAMBER: l1Z~ <6 c

RANGE: 2£fO PPB CONVERTER:.3f<3 C

AVG. TIME: f>O sec


Monitor Data Logger H2S (PPB) H2S (PPB)

-b~C,Co -0 .. 3.\

\S'1.G 1~0~0

tc'~ <A T\trJ

-SETTINGS CHANGED? YES OR ~ (CIRLCE ONE)

NEW SETTINGS: Note: If calib~ ~. · _"' vuaugea, then you mut://4rify. ~

~: COEF: PPB RANGE': ~ u AV<}. TIME: sec '-- I./""'

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Continuation of field record for sample --="'c.....::Bl\=---.l.. ___________ _


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Station I.D.




-------

Site Description '10w"J '\?i-0~ lO\NN ~

Date:~Time: ll:lJS· Operator: ~h ~


Gas Calib tor 10: Monitor 10:

MFC(s) Calibrated. I I SETTINGS: TEMPERATURES:

Gas Cylinder Mf~ COEF: INT.:

Cylinder ID: ~ BKG: PPB CHAMBER:

Concentration: H2S' RANGE: PPB CONVERTER:

/ Cert Date: I I ~ AVG. TIME: sec ""- /

~~ CALIBRATION SYSTEM

""' JI2S MONITOR I DATA LOGGER

Total Flow Concentration Zero Air Cal. Gas ( ~ Monitor Data Logger Setting Setting Flow Flow ~~S (PPB) H2S (PPB) cc/min. H2S (PPB) cc/min cc/min

ZERO 0.00 "\"'-9 ~// ~

" ""' ~

'\

SETTINGS CHANGED? YES OR NO (CIRLCE ONE)


c

c

c

\ COEF: BKG: PPB RANGE: PPB AVG. TIME: se~\.,

'J

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~~~·t't\1~;~cy, ~a~~~at_~~ CPr.11\-~M: }:\ z._S /.50z_ ~~'1?-W-~ : . .

.¥\. ~"~ \ f 'X:"\ II Sample Team Leader/Sampler Signature/Date~ \ c--..>.s

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Station I.D. Yf38 ---=----- ,, ·, ''

Site Description ~ U:Omt -Sl47Ef7A(ti_(~~) ~~N~

Date: \ { ul \ l Time: to·.YY Operator: ..1;...~.-L--· __ N_<:Ati ______ _ ..

--CALIBRATION ~YSTEM

~' ~

Gas Calibrator 10: UA. ~11o'-\5 :, '

MFC(s) Calibrated: \ t) I -z_/ I \0 scu-rr ~' ~ l) <9 u \0~

Gas Cylinder Mfg.: PtMUL\ a

Cylinder 10: ~~ 6{ I ~ 5:.. '-1. 2..1..\ \\\ _. _S:]Q. cRt \\26ll\ (::!} ,\?)o\

Concentration:~2S PPM

Cert Date: <2 I 2..1 1 2.()\6

CALIBRATION SYSTEM Total Flow Concentration Zero Air Cal. Gas

Setting Setting Flow Flow cc/min. H2S cc/min cc/rnin

ZERO \9~9. \ 0.00

ttco t 9. 3o.s ss:q1

l<-tg~.s lo \9(o L.. 0 '24.'---\l

MlO Pfs YES

• <~I

~t.\ ~EITING..S: 6" w·- 0 . ct.~ ~ COEF~

BKG: rJ}A PPB

RANGE: ZDo PPB

AVG. TIME: &,(/) sec

.. ,

.. TEMP.ERA TURES~

INT.: 3 (0 <Z> c

CHAMBER: 44- .Cf C

CONVERTER: 322. C


Monitor Data Logger H2S (PPB) H2S (PPB)

(2). ( 5 <1),7_

f(,l. <t 1~2.b

Co9.~ ~9. cg

(CIRLCE ONE)

Note: If calibratiog seftipg changed, then you must re-verify. I ' ~ '

BKG: ____ PPB RANGE: ___ .PPB AVG. TIME: __ .sec

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Cn,ntinuation of field record for sample _¥--'@,=-=:_~-----------


~~5\ CiAs9Z{) Q\Jfrt_JYJ ~L ct0Yt'2rCt1\ OZSI<Sf'JI'HC() \N &A~ A. St'41l\L ~OVN~ ~ Se>z w~ b2£~ ~"' -r»-£ TLS\ ( s pP6 e 1 C!:O ,, ~ 2-~@}o), ~vs- 0\G tvOT A~ ID . IN~CNCC \1'1Z.-f'l\~\Jf£MWT: ~~a_S ~6~ ~oJu~~T tz~oo.

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Station I.D. _'ft?A~~--~ ,,l.b\11

Site Description A2?t ~~ Bu..>ff' /o'J'l\'\ ~

Date: t I uf ' ' Time: I G,~ lS Operator:~ N~~--i

CALIBRATION SYSTEM

Gas Calibrator 10: A\ l 0 Y 5 MFC(s)Calibrated: )0 I?...,/ I \()

H2S MONITOR

Monitor 10: E\1\ C\.(.lo 4S0

SETTINGS: TEMPERATURES: 'S <..c"l\ N-. u Q.\J\ C{

Gas Cylinder Mfg.: A:MVIJ.CA COEF: Q) ''\~ L INT. : 3~.3

BKG: tJ I A PPB CHAMBER: 4 3. (

c

c Cylinder ID: fF' '1 ZZ.,\ Concentration: 0 ~7 (/) H2S PPM

Cert Date: <6 I G 7 I ( 0

RANGE: 1._;b0 PPB CONVERTER: 3(3 C

AVG. TIME: (oQ> sec

CALIBRATION SYSTEM H2S MONITOR I DATA LOGGER Total Flow Concentration Zero Air Cal. Gas Monitor Data Logger Setting Setting Flow Flow

·. cc/min. H2S (PPB) cc/min cc/min H2S (PPB) H2S (PPB)

\ q <l1 ~'-' ZERO \'\<6q ,4 0.00 -0.70 -0 .. 23 .'···.

\g<&"G..5 )0 <7> \qz<g. Y SS;1l \05.3 1Co3 ,.

\qg-c,.'= (0 \'llo?)oJ ZY,Y~ Coq.l foCf

:: '

ll z(p/ ',: \,-_..

Mtt D S1\JD' ~ ~ ' '··· // >.

"' 1 'SETTINGS CHANGED? ~ (CIRLCE ONE)

.·_::·:· ,, YES OR

NEW SETTINGS: Note: If calibration setting changed, then you must re-verify. < . '• ' '•i:<·l'X.'; ,, .. I:·'COEF: AVG. TIME: ·. ·see ' BKG: PPB RANGE: PPB

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Continuation of field record for sample _..:.Y-2:B::::::..:A~-----------


~T ~~SO G~ ~~2-/P{S ~ UiZA~ ~FI a) \N (yAfl? ~IN~lj ~\ \3~l'L CNUNf_ ~\ ~~ti'MTdJ1 S~ 6 .. ~ t::o'NNU1f'-t~St>~ SLQ/~ /x-JfJt-'YZ~

}NCUJOtrJG ~Y, 'fv\INV\Z_, ~ Po'WW~\UJO(

~A,

Sample Team Lead"/Samplcr Signature/Date~~ ~ \ \ 'l~ \II of40

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Station I.D. '{~

Site Description '-!1A.JJ:Jw lSVJff? \t)Wt-J ~

Date: \ {L..l { l \ ·~ Time: il.' ;3l> · · Operator: ~· , tJoPsf} ' ,t._ '~

CALIBRATION SYSTEM

Gas 10: Monitor 10: ----------

MFC(s) Cali I I

Gas Cylinder

Cylinder 10:

Concentration:

Cert Date: I I

CALIBRATION SYSTEM

Setting cc/min.

Concentration Zero Air Setting Flow

H2S cc/min

ZERO

CHANGED? YES

0.00

OR


COEF: ___ _ INT.: _____ c

BKG: ____ .PPB CHAMBER: ___ C

RANGE: ___ .PPB CONVERTER: __ C

AVG. TIME: sec


NO (CIRLCE ONE)

Data Logger H2S (PPB)

Note: If calibration setting changed, then you must re-verify.

BKG: ____ PPB RANGE: ___ PPB AVG. TIME: ___ .sec

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Station I.D. YB8 Site Description (Lo~ Coa~ ~ ~Lt(. l~ ~rtJ~0

Date:~tzlll I Time: l/:SD Operator:~ ~


Gas ' librator ID: Monitor ID:

MFC(s) Calibr d: I I SETTINGS: TEMPERATURES:

Gas Cylinder Mf . COEF: INT.: c . Cylinder ID: ~ A r

BKG: PPB CHAMBER: c

,~ Concentration: H2S ~ RANGE: PPB CONVERTER: c

Cert Date: I I ,~/) AVG. TIME: sec

Y"A CALIBRATION SYSTEM \ ~ H2S MONITOR I DATA LOGGER

Total Flow Concentration Zero Air cru~ ~ Monitor Data Logger Setting Setting Flow Flow cc/min. H2S (PPB) cc/min cc/min H2S (PPB) H2S (PPB)

ZERO 0.00 ~<< ~

~. ~"" ~

SETTINGS CHANGED? YES OR NO (CIRLCE ONE) ~ NEW SETTINGS: Note: If calibration setting changed, then you must re-verify. '\

\ COEF: BKG: PPB RANGE: PPB AVG. TIME: sec

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Continuation of field record for sample ___ "j.t...--.::8:._8:::..<..--________ _


Sample Temn LeodedSmnpl« Signature!Dat~ \ \z:J l \ \ of40

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Station I.D. _"{_._~_~ _·_~~---

Site Description ~~ UrJ-~ --srnJ't: ~, (~LOJND') C~}f\)ttG

Date: \/2£/11 Time: 9 ~ 00 Operator: @f,h ~

CALIBRATION SYSTEM

Gas Calibrator ID:S.()A A-Tlo'{S'

MFC(s)Calibrated: lo 1 Z/ 1 2o10 "SC:01T AIQ.. u Q\) tb2:

Gas Cylinder Mfg.: ~~CA.. c~- ,(z'bi~<

Cylinder ID: ~p -l:::f-1-73..5 Lt Zc l

H2S MONITOR

Monitor 10: ~ Al/121o SETTINGS: TEMPERATURES:

COEF: G.:I<g2_ INT.: 31,5 BKG: Nl:ft- PPB CHAMBER: y lJ · Cf

c

c

Concentration: 5 :7rz;, H2S PPM

Cert Date: 0 I -z·7 I I(!)

RANGE: Z£.tz> PPB CONVERTER: 32.2 C

AVG. TIME: (0<() sec

CALIBRATION SYSTEM H2S MONITOR I DATA LOGGER Total Flow Concentration Zero Air Cal. Gas Monitor Data Logger

Setting Setting Flow Flow cc/min. H2S (PPB) cc/min cc/min H2S (PPB) H2S (PPB)

\9qi,'L ZERO l9'9L'l 0.00 GV~0Y (7),(])

\<icte __ fo j (pQ' 1<-tsz_. s ss ,\7 /01J., 0 l~®.b

\ q¥(,. y J(b ~~ SCL 9 ZY,L{~ ~~. tf ~g~S

fJJD a;:: ~TVD'J 7_/f Is Ct1D ~ SETTINGS CHANGED? YES OR (CIRLCE ONE)


COEF: ---- BKG: ____ PPB RANGE: ___ PPB AVG. TIME: __ sec

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Continuation of field record for sample _·y~e£.c::..!.... __________ _


~·~ (85S£0 Q:.- C41-z:e-i/ dJ-5 DCSCfZ'G£0 11\]

~.. ~~-rzaz_ ~ ~-~\Jt 1\T ~'f~M~'i \') ~ 00 ~ bAJA '1}:)\J'JN~ ~,.~to&~->

Sample Team Leader/Sampler Signature/Date-~~~---\ __ · ~-__j_--ll )r-:~=· +-/_:_{1.!._____ ___ _ Qj i

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Station I.D. "feJ\ Site Description Y ~ tSLJJfP To'l\l'J ~

Date: tl 6.-tlt \ Time: 1 3; '15 Operator: -'-~----..:.==-=:...__~:...__..:..:.._H_L_ __ ~--

CALIBRATION SYSTEM

Gas Calibrator ID: tfA .P.ll O'-t5

MFC(s)Calibrated: lO t 'Lr I ~ld scatr Ali U G$v tO£ ~

Gas Cylinder Mfg.: FPf2CZ.~ 01' ''~)J

H2S MONITOR

Monitor ID: Ef'A~2Co~.S~ - :k .


COEF: "· C} 9 "2_ INT.: )([). (/) c

Cylinder ID: ~r L( ZZ ( BKG: N lA- PPB CHAMBER: 4 S ,?_ C

Concentration: S .:/e>H2S PPM RANGE: 2..::)0 PPB CONVERTER: 3 79 C

Cert Date: '6 I y I l0 AVG. TIME: b({) sec

CALIBRATION SYSTEM H2S MONITOR I DATA LOGGER Total Flow Concentration Zero Air Cal. Gas

Data Logger H2S Setting Setting Flow Flow Monitor H2S (PPB) cc/min. H2S (PPB) cc/min cc/min (PPB)

tq~~ .l ZERO \q<rt. \ 0.00 -0. Lf -([). s I ern.? [(p~ jq?J.Lf 5S.ct5 /01 j(or:D_ 7 l ~%~.? 7t/J [q~Q5. (/J Z4.Y6 ~7. ~ (,~, (/)

t)~( D~S ~cY\ c II(J[S ~'

SETTINGS CHANGED? YES OR <(_NO \ (CIRLCE ONE)

NEW SETTINGS: Note: If calibration setting changed, then you must re-verifY.

COEF: BKG: PPB RANGE: PPB AVG. TIME: sec

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Continuation of field record for sample YBA.. · ~ ----~----------~---------


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AIR SAMPLING LOGBOOK€¦ · US EPA Region 4 Yell ow Bluff Air Study Wilcox County, Alabama SESD...

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Transcript of AIR SAMPLING LOGBOOK€¦ · US EPA Region 4 Yell ow Bluff Air Study Wilcox County, Alabama SESD...