semspub.epa.gov• March 26,2015 U.S Environmental Protection Agency Water Enforcement OES4-SMR 5...

• March 26,2015

U.S Environmental Protection Agency Water Enforcement OES4-SMR 5 Post Office Square, Suite 100 Boston, MA 02109-3912

GE Global Operations - EHS

159 Plastics Avenue Pittsf.eld, MA 01201

Massachusetts Department of Environmental Protection Division of Watershed Management Surface Water Discharge Permit Program 8 New Bond Street Worcester, MA 01606

Massachusetts Department of Environmental Protection Western Regional Office- Bureau of Resource Protection 436 Dwight Street Springfield, MA 01103

Permit Number: MA0003891

Dear Sir or Madam et al:

The February 2015 Discharge Monitoring Reports and list of comments are enclosed. There were no exceedances during this month.

- _(/ 1.~

Y?Z;urs uly,

JXndrew T. Silfer P.E. Leader, Housatonic/Pittsfield

cc: M. Calacone, GE S. Coyle, Veolia Water E. Cullen, GE CSSO (cover only)

OneEHS

February 2015 DMR Comments

1. Rule for Associating Flow/Precipitation Data with Sample Date.

A typical NPDES Sampling Day is defined as the 24-hour period starting at 7 AM on the first day and ending at 7 AM the following day. The date associated with this time period is the date of the following day. For example, 4/3/09 7:00 AM - starts the time period and 4/4/09 7:00AM ends the 24-hour period; the associated date for this 24-hour day is 4/4/09. Because of this definition, all grab samples and composite samples taken between 7:00AM and 12:00 Midnight will have its associated flow or precipitation reported on the following day. Grab samples and composite samples taken between 12:00 Midnight and 7:00AM will have the same date as its associated flow and/or precipitation.

2. Reports attached to DMRs

As required by the NPDES Permit, the February 2015 VOC/SVOC analytical results are attached to the 64G-A DMR.

As required by the NPDES Permit, the February 2015 VOC/SVOC analytical results are attached to the 0006-A DMR.

3. Explanation of NODI Codes Entered on DMRs

WOOS-A, WOSA-A, WOOS-A, 098-A and W009·A NODI(9) codes were entered where Rainfall, Flow Total, pH, analytical results (mg/L and/or ug/L), and the associated loadings are not required to be reported in the February 2014 Report.

OOSA·A, W058-A, WOSA-A, SROS-A, 098-A, 0009-A, W009-A There were no discharges during February 2015; therefore a 'C' was entered into the No Discharge box, and "No Discharge" was written in the Comments section on the associated DMR Forms per 2015 DMR Report Forms Instructions.

Page 1 of 1

NAIIUNAL t'ULLU IAN I UI~L.HAHllt: t:LIMINAIIUN ~y~ I t:M \NI-'Ut:~J

DISCHARGE MONITORING REPORT (OMR)

PERMITTEE NAME/ADDRESS (fnclude Facility Name/Location if Different)

NAME: GENERAL ELECTRIC PITTSFIELD ADDRESS: 159 PLASTICS AVE

PITTSFIELD, MA 01201

FACILITY: GENERAL ELECTRIC COMPANY LOCATION: 159 PLASTICS AVE


ATTN: Andrew T. Silfer, Exec Mgr. En

I 64G·A

151§r!RAI=i~E AD~U~EI!i

MONITORING PERIOD

MM/DD!YYYY I MM/DD!YYYY

02/01/2015 02/28/2015

QUANTITY OR LOADING QUALITY OR CONCENTRATION PARAMETER VALUE VALUE UNITS VALUE VALUE VALUE

pH SAMPLE ........ ........ ........ ........ MEASUREMENT -r .oo I . G;;.O

004001 0 PERMIT ........ ........ - 6.5 ........ 9 Effluent Gross REQUIREMENT MINIMUM MAXIMUM Solids, total suspended SAMPLE --- *****" - -MEASUREMENT 0 0 005301 0 PERMIT ****** - ****** Req. Mon. - Req.Mon. Effluent Gross REQUIREMENT MOAVG DAILYMX Oil & Grease SAMPLE ****** ****** ****** ******

MEASUREMENT 0 0 005561 0 PERMIT - - - Req. Mon. ****** Req. Mon. Effluent Gross REQUIREMENT MOAVG DAILYMX Polychlorinated biphenyls IPCBs) SAMPLE ........ - - ******

MEASUREMENT 0 0 395161 0 PERMIT ****** ****** ****** • 065 ******

I

Req. Mon • Effluent Gross REQUIREMENT MOAVG DAILYMX Flow, in conduit or thru treatment SAMPLE ****** ****** -plant MEASUREMENT 0.1 ZSt.. o.,~...; I M(:,-0

500501 0 PERMIT Req. Mon. Req. Mon. MGD - ****** -Effluent Gross REQUIREMENT MOAVG DAILYMX Volatile Organic Compound [VOC] SAMPLE ****** ****** - ******

MEASUREMENT 0 0 51415 1 0 PERMIT - - ****** Req. Mon. - Req. Mon. Effluent Gross REQUIREMENT MOAVG DAILYMX Volatile fraction organics (EPA 624] SAMPLE ****** - ****** ******

MEASUREMENT t.""l.-""10 t- '"'i OO

787331 0 PERMIT ****** ****** - Req. Mon. ****** Req. Mon. Effluent Gross REQUIREMENT MOAVG DAILYMX

NAME/TITLE PRINCIPAL EXECUnVE OFFICER I eofiiiVUI><Mr per>dy o! ltwlh.lllhis-ond ••-,...,. pr-od ur><Mrmy..._ or

~r. P-.__.,--•• ~ .... --olgnod..,_.lh.ll~~.._,.-.-.... ,.. ... . ... u .... , .. "'"---od. Baoodonmyilquiryo!flopenanot......,.""",.....,. .... ..... 01 ..... po-·~ oespcnsiblo ,., ;.-..mg ..... - .... - .. -od .. co 1M bnl: ot my ~and belef, uue,IICCUfMe, .rid c::ornpMte. I am ..,.,.lhat lhefe are Ugnlficanl

t-orm 1\pprovea

OMS No. 2040-0004

DMR Mailing ZIP CODE: 01201

MAJOR

(SUBR W)

64G INTERNAL THROUGH 005

Internal Outfall

No Discharge 0

NO. FREQUENCY SAMPLE

UNITS EX OF ANALYSIS TYPE

sv 0 c,...~E;IOI'-L '-t ~c.o ... p-

su Twice per GRAB Month

IYI ~ /L 0 -z..f,...o Cb~'Z'"f

mg/L Twice per COMP24 Month

~'1 1'- 0 "l-/MO &ILJ'. 13 I

mg/L Twice per GRAB Month

t..(.q lL 0 Z./tvO t!al'< , "l.. "'i

ug/L Twice per COMP24 Month

****** a c.c,.....,... ~~D,_.

****** Continuous Recorder (auto)

c.cq k .. 0 'Z.(Mo ~ .... A~

ug/L Twice per GRAB Month

'-'"i 4'- 0 -z...lrv.a c,..,._ .... ~ I

ug/L Twice per GRAB Month

TELEPHONE DATE

Wzrl?tJl5 Exec. Mgr, Env. Remediation (413)448·5902 ponallH ,., .. 1m1101g---· O!Wding "" .-.-r o1 ron. ond ~ ro. m.-.g SIGNATURE OF PRINCIPAL EXECUnVE OFFICER OR -.. AUTHORIZED AGENT TYPED OR PRINTED AREA Codo I NUMBER I t.ltottJI).IYVY'II'

COMMENTS AND EXPLANAnON OF ANY VIOLATIONS (Reference all attachments here)

SEE 64GT FOR TOXICITY; FLOW TOTAL SEE FOOTNOTE 4; 51415 IS REPORT SEMI-VOLITILES.

EPA Form 3320.1 (Rev.01106) Previous editions may be used. 12/15/2014 Page 1

PERMITTEE NAME/ADDRESS (Include Facilily Name/location ;t Ditterent)

NAME: GENERAL ELECTRIC PITTSFIELD

ADDRESS: 159 PLASTICS AVE PITTSFIELD, MA 01201

FACILITY: GENERAL ELECTRIC COMPANY

LOCATION: 159 PLASTICS AVE PITTSFIELD, MA 01201

ATTN: Andrew T. Siller, Exec Mgr. En

NA IIUNAL I"'ULLU IAN I UI::OvHAHl:>t:: t::LIMINA IIUN ::OY::OI t::M lNI"'Ut:::OJ

DISCHARGE MONITORING REPORT (DMR)

I MA0003891 II 64G·A I PERMIT NUMBER blscRARGE NUMBER

MONITORING PERIOD

MM!DDIYYYY I MM!DD!YYYY

02/01/2015 02/28/2015


Flow, total SAMPLE - - **'**** MEASUREMENT 0 . 1--i"Z.t t!}./"-1~1 rv.t-o

822201 0 PERMIT Req. Mon. Req. Mon. MGD **'**** **'**** **'**** Effluent Gross REQUIREMENT MOAVG DAILYMX

NAME/TITLE PRINCIPAL EXECUTIVE OFFICER lc.rtllyonlor ponoly clllwlhalltllo doc:umonlandol-.-ro--' ..-my-ar

t.d-.._-lnoaoordonoo wWio aysaom dellgnod Ia --~ponannolpoportygolhor-. ~ ""'int_lon_,od~ -'"'"'Y~cllhoponanarpoqans111lai'IWiago.,.

Exec. Mgr, Env. Remediation ~.ar-poiiGIIodiroellyrwljiOilliiJiol..-gollemglholnlonnollon, lho...,_aulmllodb , lholloololmy~--1.-. ....... -_,... .. _, ......... --. ... ..-

--lor ... ~ IMelnft>rmaDI. inl:t.rdong ... .,.,.._.,of .... - n.plsarmonllor lonGWW~t~ -.. TYPED OR PRINTED

COMMENTS AND EXPLANA110N OF ANY VIOLA110NS (Reference all attachments here)

SEE 64GT FOR TOXICITY; FLOW TOTAL SEE FOOTNOTE 4; 514151S REPORT SEMI-VOUTILES.

EPA Form 3320-1 (Rev.01106I Previous edition• may be used.

r-orm ~pprovea

OMB No. 2040..()004

DMR Mailing ZIP COOE: 01201

MAJOR

(SUBRW)

64G INTERNAL THROUGH 005

Internal Outfall

No DischargeD



....... 0 eo.-rr r2. c:.o ... , .._

**'**** Continuous REH:Order (auto)

TELEPHONE OATE

AIIEACodo

12/15/2014 Page 2

Attachment E • 64G

Weekly Weekly Oil& Grease FN TSS Date Mio- pH Max-pH MGIL MGIL

02/01/15 02/02/15 U4.10 1,G U1.00 02/03/15

02/04/15 02/05/15 02/06/15 02/07/15 7.00 7.20

02/08/15 02/09/15 U4.10 1,G U1.00 02/10/15 02/11/15

02/12/15 02/13/15 02/14/15 7.00 7.10 02/15/15

02/16/15 02/17/15 02/18/15

02/19/15 02/20/15 02/21/15 7.00 7.60 02/22/15

02/23/15

02/24/15 02/25/15

02/26/15

02/27/15 02/28/15 7.40 7.60

FN 1 • (U) Indicates compound analyzed for but oot detected

C - Composite sample G - Grab sample

FN PCB UGIL

1,C

1,C

FN voc FN svoc FN Metered Raln/Precip Raln/Precip Flow- MGD Total-In Peak -In

0.1431 0.00 0.00 0 c 1.400 G 0 G 0.1441 0.20 0.07

0.1392 0.16 0.02 0.1248 0.00 0.00 0.1429 0.15 0.04 0.1399 0.09 0.05 0.1322 0.08 0.08 0.1291 0.06 0.02

0 c 1.140 G 0 G 0.1402 0.19 0.05 0.1265 0.07 0.01 0.1193 0.00 0.00 0.1301 0.08 0.06 0.1375 0.04 0.02 0.1143 0.00 0.00 0.1307 0.13 0.02 0.1318 0.00 0.00 0.1087 0.00 0.00 0.1241 0.00 0.00 0.1233 0.01 0.01 0.1173 0.52 0.08 0.1224 0.36 0.11 0.1106 0.09 0.02 0.1205 0.03 0.02 0.1213 0.52 0.14 0.1089 0.00 0.00 0.1175 0.00 0.00 0.1142 0.00 0.00 0.1025 0.00 0.00

----

February 10, 2015

Mr. Sean Coyle Veolia Water North America

1 000 East Street Pittsfield, MA 01201

Laboratory Results for: GE -Pittsfield 1\'PDES

Dear Mr. Coyle:

ALS Environmental ALS Group USA, Corp 1565 Jefferson Rd, Building 300, Suite 360 Rochester, NY 14623 T: 585-288-5380 F: 585-288-8475 www .alsglobal.com

Analytical Report for Service Request No: Rl500757

Enclosed are the results of the sample(s) submitted to our laboratory on February 3, 2015. For your reference,

these analyses have been assigned our service request number R1500757.

All analyses were performed according to our laboratory's quality assurance program. The test results meet

requirements of the NELAP standards except as noted in the case narrative report. All results are intended to be

considered in their entirety, and ALS Environmental is not responsible for use of less than the complete report.

Results apply only to the items submitted to the laboratory for analysis and individual items (samples) analyzed,

as listed in the report. The measurement uncertainty of the results included in this report is within that expected

when using the prescribed method(s) for analysis of these samples, and represented by Laboratory Control

Sample control limits. Any events, such as QC failures, which may add to the uncertainty are explained in the

report narrative.

Please contact me if you have any questions. My extension is 7473. You may also contact me via email at

[email protected].

Respectfully submitted,

ALS Group USA Corp. dba ALS Environmental

Deb Patton Project Manager

-~··

r, JGHT SOLUTION~

Page 1 of Q\.o

... ::::1"6 ......

R I G H T P .1 f~ TN E P.

•

Client: Service Request No.: Project: Date Received: Sample Matrix: Project/Case No.:

ALS Environmental

General Electric R1500757 GE·Pittsfield NPDES 2/3/15 Water

CASE NARRATIVE

All analyses were perfonned consistent with the quality assurance program of ALS Environmental. This report

contains analytical results for samples designated for Tier II. When appropriate to the method, method blank results have been reported with each analytical test.

Sample Receipt

Three water samples were received for analysis at ALS Environmental on 2/3115. The samples were received in good condition and consistent with the accompanying chain of custody form. The samples were received within the

0-6°C temperature guidelines. The samples were stored in a refrigerator between 1 °C and 6°C upon receipt at the laboratory.

Volatile Organics

All samples were analyzed within the 3 day holding time for Acrolein.

All surrogate standard recoveries were within acceptance limits for the samples.

No other analytical or quality control problems were encountered during analysis.

Extractable Organics

The initial and continuing calibration criteria were met.

Surrogate standard recoveries were within acceptance limits for the samples.

The Method Blank contained a low level hit ofDiethyl Phthalate and has been flagged with a "J". No data was affected.

The Laboratory Control Sample and Duplicate Laboratory Control Sample (LCSD) for Benzidine were outside of

the control limits and have been flagged with a "•". They recovered below the :MRL. There were no hits in the sample for this compound but there may be a low bias.


..

CASE NARRATIVE This report contains analytical results for the following samples:

Service Request Number: R1500757

lablD R1500757-001

R1500757-002

R1500757-003

Client ID 64G-1 Q2M-1 X-GV

64G-1Q2M-1X-GS

Trip Blank

A Enuironmental

u

J

B

E

E

D

•

H

#

REPORT QUALIFIERS AND DEFINITIONS

Analyte was analyzed for but not detected. + Correlation coefficient for MSA is <0.995. The sample quantitation limit has been

N lnorganics- Matrix spike recovery was outside corrected for dilution and for percent moisture, unless otherwise noted in the case

laboratory limits.

narrative. N Organics- Presumptive evidence of a compound

Estimated value due to either being a (reported as a TIC) based on the MS library search.

Tentatively Identified Compound (TIC) or s Concentration has been determined using Method that the concentration is between the MRL of Standard Additions {MSA). and the MDL. Concentrations are not verified w Post-Digestion Spike recovery is outside control within the linear range of the calibration. For DoD: concentration >40% difference between

limits and the sample absorbance is <50% of the

two GC columns (pesticides/Arclors). spike absorbance.

Analyte was also detected in the associated p Concentration >40% (25% for CLP) difference

method blank at a concentration that may between the two GC columns.

have contributed to the sample result. c Confirmed by GCIMS

Inorganics- Concentration is estimated due to Q DoD reports: indicates a pesticide/Aroclor is not the serial dilution was outside control limits. confirmed ~100% Difference between two GC

Organics- Concentration has exceeded the columns).

calibration range for that specific analysis. X See Case Narrative for discussion.

Concentration is a result of a dilution, MRL Method Reporting Limit. Also known as: typically a secondary analysis of the sample LOQ Limit ofQuantitation (LOQ) due to exceeding the calibration range or that The lowest concentration at which the method a surrogate has been diluted out of the sample analyte may be reliably quantified under the and cannot be assessed. method conditions.

Indicates that a quality control parameter has MDL Method Detection Limit. A statistical value derived exceeded laboratory limits. Under the from a study designed to provide the lowest ''Notes" column of the Form I, this qualifier concentration that will be detected 99% of the time. denotes analysis was performed out of Values between the MDL and MRL are estimated Holding Time. (see J qualifier).

Analysis was performed out of hold time for LOD Limit of Detection. A value at or above the MDL tests that have an "immediate" hold time which has been verified to be detectable. criteria.

NO Non-Detect. Analyte was not detected at the Spike was diluted out. concentration listed. Same as U qualifier.

Lab ID #for Massachusetts Certification M-NY032

Analyses were conducted in accordance with Massachusetts Department of Environmental Protection certification standards, except as noted in the laboratory case narrative provided. A copy of the current Department issued parameter list is included in this report .

.... • 1' .. ~ ,;:;..=.~~.-r..;;mz::=,:..;::. .. .v: .. -..;;·.:a.=-~~~"K"t.n.:S-.._~~~=~·'\Ma~~r=~~·~~

·z l G r; '1 ~ '. 1_ 1 T r ~ • · c: 1 r. 1 c; : r T P •\ n T ;-..~ E R

P·\INTRANE'l\QAQC\Forms Conlfolled\QUALlF _routine forMA rJ DOC s1n.e ae e 4

The .CoJnJuonweal~h of Massachus~tts:

Depart1nen,t of Ef!-vb·otunental ProtectioJt Division of Environmental A11alysis

Senator William X Wall Experiment Station

M-NY03l

certifies

' ALS ENVIRONMENTAL ROCHESTER 1565 JEFFERSON RD BUILDING 300, SUITE 3'60 ROCHESTER, l\'Y 14623-0000

' . Laboratory-Director: LARRY LEWIS

for tlte a11alysis of NON POTABLE WATER(CHEMISTRY)

pursuant to 310.CMR 42.00

This certificate supersedes all previous Massachu~ett's certificates issued to this laboratory. The la~oratory is regulated by and shall be resp"onsible for being in compliance with

Massachusetts regiJlations at 310 CMR 42.00.

This certificate is valid only when accompanied by the la,test dated Certified Parameter List.n•••"''" issued by the Massachusetts D.E.P. Contact the Division of Environmental Analysis to verify the current certificaticm status of the labor~;~tory.

Certification is no guarantee of the validity of the data. This certification is subject to unannounced laboratory inspections.

Di're~tor, Division of Environmental Analysis

Issued: 01 JPL 2014

Expires: 30 JiJN 2015

oeoes

COMMONWEALTH OF MASSACHUSETIS DEPARTMENT OF ENVIRONMENTAL PROTECTION

Certified Parameter List as of: 01 JUL2014

M-NY032 ALS El'I'VIRONMENTAL ROCHESTER

ROCHESTER NY

NON POTABLE WATER (CHEMISTRY)

~nalytes

ALUMINUM

ANTIMONY

ANTIMONY

ARSENIC

ARSENIC

BERYlliUM

BERYLLIUM

CADMIUM

CADMIUM

CHROMIUM

CHROMIUM

COBALT

COBALT

COPPE~

COPPER

IRON

LEAD

LEAD

MANGANESE

MANGANESE

MERCURY

MOLYBDENUM

MOLYBDENUM

NICKEL

NICKEL.

SELENIUM

SELENIUM

SILVER

SILVER

THALLIUM

THALLIUM

VANADIUM

VANADIUM

ZINC

ZINC

SPECIFIC CONDUCTIVITY

TOTAL DISSOLVED SOLIDS

HARDNESS (CAC03), TOTAL.

CALCIUM

MAGNESIUM

SODIUM

POTASSIUM

ALKALINITY, TOTAl

June 26,2014

Effective Date

01 JUL2014

*= Provisional Certification

Expiration 30 JUN 2015 Date

Methods

EPA200.7

EPA200.7

EPA200.8

EPA200.7

EPA200.8

EPA200.7

EPA 200.8

EPA200.7

EPA200.8

EPA2pG.7

EPA200.8

EPA200.7

EPA200.8

EPA200.7

EPA200.8

EPA200.7

EPA200.7

EPA20D.8

EPA200.7

EPA200.8

EPA245.1

EPA200.7

EPA200.8

EPA200.7

EPA200.8

EPA200.7

EPA200.8

EPA200.7

EPA200.8

EPA200.7

EPA200.8 '

EPA200.7

EPA200.8

EPA200.7

EPA200.8

EPA 120.1

· SM2540C

SM2340C

EPA200.7

EPA200.7

EPA200.7

EPA200.7

SM2320B

Page 1 of 2

COMMONWEALTH OF MASSACHUSETTS DEPARTMENT OF ENVIRONMENTAL PROTECTION

Certified Parameter List as of:

M~NY032 ALS ENVIRONMENTAL ROCHESTER

ROCHESTER 1\Y

NON POTABLE WATER {CHEMISTRY)

Analytes

CHLORIDE

CHLORIDE

FLUORIDE

SULFATE

AMMON IA-N

NITRATE-N

NITRATE·N

KJELDAHL·N

ORTHOPHOSPHATE

PHOSPHORUS, TOTAL

CHEMICAL OXYGEN DEMAND

BIOCHEMICAL OXYGEN DEMAND

TOTAL ORGANIC CARBON

CYANIDE, TOTAL

NON-FILTERABLE RESIDUE

OIL AND GREASE

PHENOLICS, TOTAL

VOLA TILE HAI.OCARBONS

VOLATILE HALOCARBONS

VOLATILE AROMATICS

VOLA TILE AROMATICS

SVOC.ACID EXTRACT ABLES

SVOC.BASEINEUTRAL EXTRACTABLES

POLYCHLORINATED BIPHENYLS (WATEJ

Effective Date

01 JUL2014

Ol.TUL2014

June 26,2014 *• Provisional Certification

Expiration 30JUNl015 Date

Methods

SM 4500-CL·E

EPA300.0

EPA 300.0

EPA300.0

EPA350.1

EPA300.0

EPA353.2

EPA351.2

EPA365.1

E.PA365.1

EPA410.4

SM5210B

SM5310C

EPA335.4

SM2540D

EPA 1664

EPA420.4

EPA601

EPA624

EPA602

EPA624

EPA625

EPA625

EPA60B

Page l of 2

eaoe7

Client: Project: Sample Matrix:

Sample Name: Lab Code:

ALS Group USA, Corp. dba ALS Environmental

Analytical Report

General Electric Company GE -Pittsfield NPDES Water

64G-I Q2M-1 X-GV RI500757-00I

Service Request: Rl500757 Date Collected: 2f 211 5 0730 Date Received: 2/ 311 5 Date Analyzed: 2/3/ 15 13:50

Units: ~giL Basis: NA

Volatile Organic Compounds by GC/MS with 3 Day Holding Time for Acrolein, Unprcserved

Analytical Method: 624 Analysis Lot: 431315

Data File Name: I:\ACQUDATA\MSVOA6\DATA\020315\M0200.D\ Instrument Name: R-MS-06 Dilution Factor: I

CAS No. Analyte Name Result Q MRL MDL Note

71-55-6 I, 1, 1-Trichloroethane (TCA) 1.0 u 1.0 0 .13

79-34-5 I, I ,2,2-Tetrachloroethane 1.0 u 1.0 0.23

79-00-5 I, I ,2-Trichloroethane 1.0 u 1.0 0.12 ---

75-34-3 I, 1-Dichloroethane (I , I-DCA) 0.46 J 1.0 0.10

75-35-4 I, 1-Dichloroethene (I, 1-DCE) 1.0 u 1.0 0.22

95-50-1 I ,2-Dichlorobenzene 1.0 u 1.0 0.10 -

107-06-2 I ,2-Dichloroethane 1.0 u 1.0 0.18

78-87-5 I ,2-Dichloropropane 1.0 u 1.0 0 . 15

541-73-1 I ,3-Dichlorobenzene 1.0 u 1.0 0.10 ·-

106-46-7 I ,4-Dichlorobenzenc 1.0 u 1.0 0.15

110-75-8 2-Chloroethyl Vinyl Ether IOU 10 0.64

107-02-8 Acrolein 10 u 10 0.73 ---

107-13-1 Acrylonitrile 10 u 10 0.37

71-43-2 Benzene 1.0 u 1.0 0.10

75-27-4 Bromodichloromethane 1.0 u 1.0 0.15 -- ---

75-25-2 Bromoform 1.0 u 1.0 0 .16

74-83-9 Bromomethane 1.0 u 1.0 0 .12

56-23-5 Carbon Tetrachloride 1.0 u 1.0 0.10 - --108-90-7 Chlorobenzene 1.0 u 1.0 0.13

75-00-3 Chloroethane 0.52 J 1.0 0.15

67-66-3 Chloroform 1.0 u 1.0 0.13 --

74-87-3 Chloromethane 1.0 u 1.0 0.16

124-48-1 Chlorodibromomethane 1.0 u 1.0 0.15

75-71-8 Dichlorodilluoromcthanc (CFC 12) 1.0 u 1.0 0.17

75-09-2 Methylene Chloride 0.28 J 1.0 0.18

100-41-4 Ethylbenzene 1.0 u 1.0 0.19

127-18-4 Tetrachloroethene (PCE) 1.0 u 1.0 0.20 ----

108-88-3 Toluene 1.0 u 1.0 0.10

79-01-6 Trichloroethene (TCE) 1.0 u 1.0 0.15

75-69-4 Trichloronuoromcthane (CFC I I} 1.0 u 1.0 0 .13 --- ----

75-01-4 Vinyl Chloride 0.14 J 1.0 0.14

10061-01-5 cis-1 ,3-Dich loropropene 1.0 u 1.0 0.14

156-60-5 trans- I ,2-Dichloroethene 1.0 u 1.0 0.15

10061-02-6 trans- I ,3-Dichloropropene 1.0 u 1.0 0.10

Printed 2/10/1 S 9 36 Form lA

l.alp~wsOO l\st:~~limsS\LIMSRcps\AnalyticalRepol1 rpl SuperSet Refe~nce 1 5..()()()()320289 ~·· 00




Analytical Report


64G-IQ2M-IX-GV RJ500757-00 I

Service Request: R 1500757 Date Collected: 2/ 2!15 0730 Date Received: 2/ 311 5 Date Analyzed: 2/3/ 15 13:50

Units: J.tg/L Basis: NA

Volatile Organic Compounds by GC/MS with 3 Day Holding Time for Acrolein, Unpreserved

Analytical Method: 624 Data File Name: I:\ACQUDATA\MSVOA6\DATA\020315\M0200.D\

Analysis Lot: 4313 I 5 Instrument Name: R-MS-06

Dilution Factor: I

Control Date

Surrogate Name %Rec Limits Analyzed Q

1,2-Dichloroethane-d4 95 81-127 2/3/1 5 13:50

4-Bromotluorobenzene 96 79-123 2f311 5 13:50

Toluene·d8 100 83-120 2/311 5 13:50 ---- ---

Printed 2/10/15 9·36 fonn lA f) 9 tJ fl 9

I .:~lprewsOO I \starlimsS\l..IMSRcps\Analytica!Repon.rpl SupcrScl Reference I S-0000320289 rev 00




Analytical Report

Tentatively Identified Compounds (TIC)

Service Request: Rl500757 Date Collected: 2/2/ 15 Date Received: 2/3/ 15 Date Analyzed: 2/3/1 5 1350

Volatile Organic Compounds by GC/MS with 3 Day Holding Time for Acrolein, Unpresen·ed


64G-IQ2M-IX-GV RI500757-00I

Analytical Method: 624

CAS# Analyte Name RT Result Q

Units: ~giL

Basis: NA

No Tentatively Identified Compounds Detected.

Comments:

Printed 0211012015 9.36 Fonn!B af3919 1\:llprcwsOO llstarlimsS\LIMSRcps\Anal)1icaiTICRcpon rpt SuperSet Reference: I 5.0000320289 rev 00



Analytical Method: Prep Method: Data File Name:

CAS No.

83-32-9 208-96-8 120-12-7 ----92-87-5 56-55-3 50-32-8

205-99-2 191-24-2 207-08-9

85-68-7 84-74-2 193-39-5

111-91-1 111-44-4 91-58-7

95-57-8 108-60-1 218-01-9

53-70-3 91-94-1 120-83-2

84-66-2 131-11-3 105-67-9

51-28-5 121-14-2 606-20-2

-122-66-7 117-81-7 206-44-0

86-73-7 118-74-1 87-68-3

Printed 2110/1 S 9 36


Analyticol Rcpon


64G-IQ2M-IX-GS Rl500757-002

Semivolatilc Organic Compounds by GC/MS

625 EPA 3510C 1:\ACQUDATA\59730\Data\020515\BA 750.0\

Analyte Name Result Q MRL

Acenaphthene 4.7 u 4.7

Acenaphthylene 4.7 u 4.7 Anthracene 4.7 u 4.7

Benzidine 94 u 94

Benz( a }anthracene 4.7 u 4.7 Benzo(a}pyrene 4.7 u 4.7

Benzo(b )fluoranthene 4.7 u 4.7

Bcnzo{g,h, i)perylene 4.7 u 4.7 Benzo{k)fluoranthcnc 4.7 u 4.7 -- - --~-

Butyl Benzyl Phthalate 4.7 u 4.7

Di-n-butyl Phthalate 4.7 u 4.7

lndeno( I ,2,3-cd)pyrene 4.7 u 4.7 -

Bis(2-chloroethoxy)methane 4.7 u 4.7 Bis(2-chloroethyl) Ether 4.7 u 4.7

2-Chloronaphthalene 4.7 u 4.7

2-Chlorophenol 4.7 u 4.7 2,2'-0xybis( 1-chloropropane} 4.7 u 4.7 Chrysene 4.7 u 4.7

Dibenz(a,h)anthracene 4.7 u 4.7 3 ,3'· Dich 1orobenzid ine 4.7 u 4.7

2,4-Dichlorophenol 4.7 u 4.7 -------

Diethyl Phthalate 4.7 u 4.7 Dimethyl Phthalate 4.7 u 4.7 2,4-Dimethylphenol 4.7 u 4.7

2,4-Dinitrophenol 47 u 47 2,4-Dinitrotoluene 4.7 u 4.7 2,6-Dinitrotoluene 4.7 u 4.7

- - --I ,2-D iphenylhydrazine 4.7 u 4.7 B is(2-ethylhexyl) Phthalate 4.7 u 4.7 Fluoranthene 4.7 u 4.7

Fluorene 4.7 u 4.7 Hexachlorobenzene 4.7 u 4.7 Hexachlorobutadiene 4.7 u 4.7

fonn lA

•,\alprewsOO l \starlimsS\l.lMSRcps\AnnlyticalRcpon .rpt

MDL

1.0 1.0 1.0

90 1.0 1.0

1.0 1.0 1.0

2.4 1.0 1.2

2.2 1.3 1.0

1.0 1.0 1.0

1.3 4.5 1.3

1.0 1.0 1.5

20 1.6 1.8

1.0 1.2 1.0

1.0 1.0 1.3

Service Request: R 1500757 Date Collected: 2/ 2115 0730 Date Received: 2/ 311 5

Date Extracted: 214/15 Date Analyzed: 2/5/15 14:24

Units: ).lg/L Basis: NA

Analysis Lot: 431825 Extraction Lot: 228578

Instrument Name: R-MS-54 Dilution Factor: I

Note

- ---

---

SuperSet Reference I S-0000320289 rev 00




CAS No.

77-47-4 67-72-1 78-59-1

534-52-l 59-50-7 91-20-3

. --98-95-3 88-75-5 100-02-7


Analytical Report


640- I Q2M-1 X-GS R1500757-002

Scmivolatile Organic Compounds by GCIMS

625 EPA 3510C 1:\ACQUDA T A \59730\Data\0205 I 5\BA 750.0\


Hexachlorocyclopentadiene 4.7 u 4.7 Hexachloroethane 4.7 u 4.7 lsophorone 4.7 u 4.7

4,6-Dinitro-2-methylphenol 47 u 47 4-Chloro-3-methylphenol 4.7 u 4.7 Naphthalene 4.7 u 4.7 --------Nitrobenzene 4.7 u 4.7 2-Nitrophenol 4.7 u 4.7 4-N itrophenol 47 u 47

MDL

1.0 1.2 1.0

II 1.2 1.0 -

1.6 1.4 5.9

Service Request: Rl500757 Date Collected: 2/2/15 0730 Date Received: 2/3/ 15

Date Extracted: 2/4/ 15 Date Analyzed: 2/5/ 15 14:24

Units: J.1g/L Basis: NA



Note

-- ------62-75-9 N-Nitrosodimethylamine 4.7 u 4.7 1.0 86-30-6 N-Nitrosodiphenylamine 4.7 u 4.7 1.0 117-84-0 Di-n-octyl Phthalate 4.7 u 4.7 1.2

87-86-5 Pentachlorophenol (PCP) 47 u 47 6.9 85-01-8 Phenanthrene 4.7 u 4.7 1.0 108-95-2 Phenol 4.7 u 4.7 1.0

101-55-3 4-Bromophenyl Phenyl Ether 4.7 u 4.7 2.2 7005-72-3 4-Chlorophcnyl Phenyl Ether 4.7 u 4.7 1.2 621-64-7 N-Nitrosodi-n-propylamine 4.7 u 4.7 1.3

-----129-00-0 Pyrene 4.7 u 4.7 1.0 120-82-1 I ,2,4-Trichlorobenzene 4.7 u 4.7 1.0 88-06-2 2,4,6-Trichlorophenol 4.7 u 4.7 1.4

- -------Semi Volatile Organic Compounds 4.7 u 4.7 0.68

Control Date Surrogate Name 0/11Rec Limits Analyzed Q

p-Terphenyl-d 14 90 40-133 2/5/ 15 14:24 N i trobenzene-d 5 92 37- 117 2/5/ 15 14:24 Phenol-d6 34 10-107 2/5115 14:24

2-Fiuorobiphenyl 94 39-119 2/5/ 15 14:24 2-Fiuorophenol 51 10-105 2/5/ 15 14:24 2,4,6-Tribromophenol 108 28-157 2/5/ 15 14:24

Printed 2110115 I 3:57 FC1011 lA

\\alpn:wsOO I\st :~rl imsS\LIMSR~ps\An:llytic~IRcport rpt Sup~rS~t R~fen:nc~ 15.0000320289 r~v 00




Analytical Report


Trip Blank R 1500757-003

Service Request: R 1500757 Date Collected: 2/ 2115 0730 Date Received: 2/ 3/15 Date Analyzed: 2/3/ 15 13:19

Units: !Jg/L Basis: NA



Datu File Name: l:\ACQUDATA\MSVOA6\DATA\020315\MO 199.0\ Instrument Name: R-MS-06 Dilution Factor: I

CAS No. Analytc Name Result Q MRL MDL Note

71-55-6 I, I, 1-Trichloroethane (TCA) 1.0 u 1.0 0.13


79-00-5 1,1 ,2-Trichloroethane 1.0 u 1.0 0.12 - -

75-34-3 I, 1-Dichloroethane {I, I-DCA) 1.0 u 1.0 0.10

75-35-4 I, 1-Dichloroethene { 1,1-DCE) 1.0 u 1.0 0.22

95-50-1 1 ,2-Dichlorobenzene 1.0 u 1.0 0.10 --


78-87-5 I ,2-Dichloropropane 1.0 u 1.0 0.15

541-73-1 I ,3-Dichlorobenzene 1.0 u 1.0 0.10 ------

106-46-7 I ,4-Dichlorobcnzene 1.0 u 1.0 0.15

110-75-8 2-Chloroethyl Vinyl Ether 10 u 10 0.64

107-02-8 Acrolein 10 u 10 0.73 - ---107-13-1 Acrylonitrile 10 u 10 0.37

71-43-2 Benzene 1.0 u 1.0 0.10

75-27-4 Bromod ichloromethanc 1.0 u 1.0 0.15 --· ·--

75-25-2 Bromoform 1.0 u 1.0 0.16

74-83-9 Bromomethane 1.0 u 1.0 0.12

56-23-5 Carbon Tetrachloride 1.0 u 1.0 0.10

108-90-7 Chlorobenzene 1.0 u 1.0 0.13

75-00-3 Chloroethane 1.0 u 1.0 0. 15 67-66-3 Chloroform 1.0 u 1.0 0.13

74-87-3 Chloromethane 1.0 u 1.0 0.16


75-71-8 Dichlorodifluoromethanc (CFC 12) 1.0 u 1.0 0.17

75-09-2 Methylene Chloride 1.0 u 1.0 0.18 100-41-4 Ethylbenzene 1.0 u 1.0 0.19

127-18-4 Tetrachloroethene (PCE) 1.0 u 1.0 0.20

108-88-3 Toluene 1.0 u 1.0 0.10 79-01-6 Trichloroethene (TCE) 1.0 u 1.0 0.15

75-69-4 Trichlorofluoromcthane (CFC II) 1.0 u 1.0 0.13

75-01-4 Vinyl Chloride 1.0 u 1.0 0.14

10061-01-5 cis-! ,3-Dichloropropene 1.0 u 1.0 0.14

156-60-5 trans-! ,2-Dichloroethene 1.0 u 1.0 0.15 ---

10061-02-6 trans-! ,3-Dichloropropene 1.0 u 1.0 0.10

Printed 2110/IS 9:36 Form lA 09013 \lalprewsOOI\st;ullmsS\LIMSRcps\AnalytiQJRcport.rpt SuperSet Reference I 5.0000320289 rev 00



ALS Group USA, Corp. dbn ALS Environmental

Analytical Report


Trip Blank R 1500757-003

Service Request: RIS00757 Date Collected: 2/ 2/J 5 0730 Date Received: 2/ 3/J 5 Date Analyzed: 2/3 / 15 13: 19

Units: Jlg/L Basis: NA



Analysis Lot: 43 1315 Instrument Name: R-MS-06

Dilution Factor: I

Control Date


I ,2-Dichloroethane-d4 98 81 - 127 2/3{1 5 13:19

4-Bromofluorobenzene 95 79~ 123 2/311 5 13: 19

Toluene-dB 98 83-120 2/311 5 13: 19

Printed 2110.115 9 36 FormiA 0f3914 \lollprcwsOOI\statlimsS\LIMSRcps\Anal)1icalRcpon rpl SuperSet Reference: 15·0000320289 rc,· 00



General Electric Company GE ·Pittsfield NPDES Water

Anal}1ical Rcpon

Tentatively Identified Compounds (fiC)

Service Request: R 1500757 Date Collected: 212115 Date Received: 2/3/ 15 Date Analyzed: 2/3115 1319


Sample Name: Trip Blank Lab Code: R 1500757-003



Units: Jtg/L Basis: NA


Comments:

Printed 02/ 1012015 9:36 Fonn I B 9 (!) fi} 15 \\alprcwsOOI\st;ulimsS\l..JMSRcps\Analytie~ITICRcport.rpt SuperSet Reren:ncc: IS-0000320289 rev 00



ALS Group USA, Corp.'dba ALS Environmental

Analytical Report


Method Blank RQ1501304-04

Service Request: R 1500757 Date Collected: NA Date Received: NA Date Analyzed: 2/3115 II: II


Volatile Organic: Compounds by GCIMS with 3 Day Holding Time ror Acrolein, Unpreserved


Data File Name: I:\ACQUDATA\MSVOA6\DATA\020315\MO 196.0\ Instrument Name: R-MS-06 Dilution Factor:


71-55-6 I, 1, 1-Trichloroethane (TCA) 1.0 u 1.0 0.13


79-00-5 1, I ,2-Trichloroethane 1.0 u 1.0 0.12

75-34-3 1,1-Dichloroethane (!,I-DCA) 1.0 u 1.0 0.10

75-35-4 1, 1-Dichloroethcne (I, 1-DCE) 1.0 u 1.0 0.22

95-50-1 I ,2-Dichlorobenzene 1.0 u 1.0 0.10

107-06-2 I ,2-Dich loroethane 1.0 u 1.0 0.18

78-87-5 I ,2-Dich loropropane 1.0 u 1.0 0.15

541-73-1 1 ,3-Dichlorobenzene 1.0 u 1.0 0.10 ----106-46-7 1 ,4-Dichlorobenzene 1.0 u 1.0 0.15

110-75-8 2-Chlorocthyl Vinyl Ether 10 u 10 0.64

107-02-8 Acrolein IOU 10 0.73 - - -


71-43-2 Benzene 1.0 u 1.0 0.10

75-27-4 B romod ich loromethane 1.0 u 1.0 0.15

75-25-2 Bromoform 1.0 u 1.0 0.16

74-83-9 Bromomethane 1.0 u 1.0 0.12


108-90-7 Chi oro benzene 1.0 u 1.0 0.13

75-00-3 Chloroethane 1.0 u 1.0 0.15

67-66-3 Chloroform 1.0 u 1.0 0.13

74-87-3 Chloromethane 1.0 u 1.0 0.16


75-71-8 Oichlorodifluoromcthanc (Cfo'C 12) 1.0 u 1.0 0.17 ----75-09-2 Methylene Chloride 1.0 u 1.0 0.18

100-41-4 Ethyl benzene 1.0 u 1.0 0.19

127-18-4 Tctrachloroethene (PCE) 1.0 u 1.0 0.20

108-88-3 Toluene 1.0 u 1.0 0.10

79-01-6 Trichloroethene (TCE) 1.0 u 1.0 0.15 75-69-4 Trichlorofluoromcthanc (CFC II) 1.0 u 1.0 0.13

~---

75-01-4 Vinyl Chloride 1.0 u 1.0 0.14

10061-01-5 cis-! ,3-Dichloropropene 1.0 u 1.0 0.14 156-60-5 trans- I ,2-Dichloroethene 1.0 u 1.0 0.15


Printed 211 0/ l S 9.36 Form lA

\·.;tlprewsOOJ'.st~rlimsSU.IMSRcps\Analy1icaJRcport.rpl SuperSet Reference· I S..()(J()()J20289 rev 00




Analytical Report


Method Blank RQI501304-04

Service Request: Rl500757 Date Collected: NA Date Received: NA Date Analyzed: 2/3/ I 5 II : I I


Volatile Organic Compounds by GC/MS with 3 Day Holding Time for Acrolein, Unprescrved

Analytical Method: 624 Data File Name: I:\ACQUDATA\MSVOA6\DATA\020315\MOJ96.D\

Analysis Lot: 4313 15 Instrument Name: R-MS-06

Dilution Factor: I

Control Date Surrogate Name %Rec Limits Analyzed Q

I ,2·Dichloroethane-d4 95 81-127 213115 II ; II

4-Bromotluorobenzcnc 96 79-123 213115 11: 1 I Toluene-dB 96 83·120 213/ 1 5 I I : I I ---- ~-~-

Printed 2/10/1 S 9;36 Fotm lA e e e 1 7 1lalprews00 I \starlimsS\LIMSReps\AnnlyticnlRcport rpt SuperSet Rc:fcrencc:: IS-0000320289 rc:v 00



Analytical Method:



Analytical Report


Service Request: Rl500757 Date Collected: NA Date Received: NA Date Analyzed: 2/3/ 15 1111


Method Blank Units: f.lg/L RQI501304-04 Basis: NA

624

CAS# Analytc Name RT Result Q


Comments:

Printed 02/101201 S 9.36 Fnnn I D f3 f3 0 1 8 \lalprewsOO I \sl:~rlimsS\LIMSReps\All~1)1ic:IITICReport rpl SupcrScl Reference 15.0000320289 rev 00




CAS No.

83-32-9 208-96-8 120-12·7


Analytical Report


Method Blank RQI501175-0I

Scmivolatile Organic Compounds by GC/MS

625 EPA 3510C 1:\ACQUDA T A \59730\Data\0205 I 5\BA 747 .D\


Acenaphthene 5.0 u 5.0 Acenaphthylene 5.0 u 5.0 Anthracene 5.0 u 5.0

----92-87-5 Benzidine 100 u 100

56-55-3 Benz( a )anthracene 5.0 u 5.0

50-32-8 B enzo( a )pyrene 5.0 u 5.0

205-99·2 B enzo(b )tl uoranthcne 5.0 u 5.0

191-24-2 Benzo(g,h, i)perylene 5.0 u 5.0 207-08-9 Benzo(k)tluoranthene 5.0 u 5.0

85-68-7 Butyl Benzyl Phthalate 5.0 u 5.0 84-74-2 Di-n-butyl Phthalate 5 .0 u 5.0 193-39-5 lndeno( I ,2,3·cd)pyrcne 5 .0 u 5.0 ----111-91-1 B is(2·chloroethoxy)methanc 5.0 u 5.0

111·44-4 Bis(2-chloroethyl) Ether 5.0 u 5.0 91-58-7 2-Chloronaphthalene 5 .0 u 5.0

95-57-8 2-Chlorophcnol 5.0 u 5.0

108·60-1 2,2'-0xybis( 1-chloropropane) 5.0 u 5.0 218-01-9 Chryscne 5.0 u 5.0 -- -- ---53-70-3 Dibenz(a,h)anthracene 5.0 u 5.0

91-94-1 3 ,3'-Dichlorobenzid ine 5.0 u 5.0 120-83-2 2,4-Dichlorophenol 5.0 u 5.0

--84-66-2 Diethyl Phthalate 2.3 J 5.0 131-11-3 Dimethyl Phthalate 5.0 u 5.0 105-67-9 2,4·Dimethylphenol 5.0 u 5.0

51-28-5 2,4-Dinitrophenol 50 u 50 121-14-2 2,4-Dinitrotoluene 5.0 u 5.0 606·20-2 2,6-Dinitrotoluene 5.0 u 5.0

122-66-7 I ,2-Diphenylhydrazine 5.0 u 5.0 117-81-7 Bis(2-ethylhexyl) Phthalate 5.0 u 5.0 206-44·0 Fluoranthene 5.0 u 5.0 -----86-73-7 Fluorene 5.0 u 5.0 118-74-1 Hexachlorobenzene 5 .0 u 5.0

87-68-3 Hexachlorobutadiene 5.0 u 5.0 -- -

Printed 2/10/15 9·36 Foon lA

l.lalprewsOOIIst;ullmsS\l.IMSRc:ps\Analytic3lRcport.flll

Service Request: Rl500757 Date Collected: NA Date Received: NA

Date Extracted: 2/411 5 Date Analyzed: 2/5/ 15 13:07




MDL Note

1.0 1.0 1.0

90 1.0 1.0

1.0 1.0 1.0

2.4 1.0 1.2

2.2 1.3 1.0

1.0 1.0 1.0

1.3 4.5 1.3

1.0 1.0 1.5

20 1.6 1.8

1.0 1.2 1.0

1.0 1.0 1.3

00919 SuperSet Reference I S-0000320289 n:•· 00




CAS No.

77-47-4 67-72-1 78-59-1

534-52-1 59-50-7 91-20-3

98-95-3 88-75-5 100-02-7

62-75-9 86-30-6 117-84-0

87-86-5 85-01-8 108-95-2

101-55-3 7005-72-3 621-64-7

129-00-0 120-82-1 88-06-2

Surrogate Name

p-Terphenyl-dl4 N i trobenzene-d5 Phenol-d6

2-Fluorobiphenyl 2-Fiuorophenol 2,4,6-Tribromophenol

Printed 2/10/15 13:57


Analytical Report


Method Blank RQ1501 175-01

Semivolatilc Organic Compounds by GC/MS

625 EPA3510C 1:\ACQUDATA\59730\Data\020515\BA 747.0 \


Hexachlorocyclopentadiene 5.0 u 5.0

Hexachloroethane 5.0 u 5.0

lsophorone 5.0 u 5.0

4,6-Dinitro-2-methylphenol 50 u 50

4-Chloro-3-methylphenol 5.0 u 5.0 Naphthalene 5.0 u 5.0

N itrobenzenc 5.0 u 5.0

2-N itrophenol 5.0 u 5.0

4-Nitrophenol 50 u 50 ---

N-Nitrosodimethylamine 5 .0 u 5 .0

N-Nitrosodiphenylamine 5.0 u 5.0

Di-n-octyl Phthalate 5.0 u 5.0 -

Pentachlorophenol (PCP) 50 u 50

Phenanthrene 5.0 u 5.0

Phenol 5.0 u 5.0

4-Bromophenyl Phenyl Ether 5.0 u 5.0

4-Chlorophenyl Phenyl Ether 5.0 u 5 .0

N-Nitrosodi-n-propylamine 5.0 u 5.0

Pyrene 5.0 u 5.0

I ,2,4-Trichlorobenzene 5.0 u 5.0

2,4,6-Trichlorophenol 5.0 u 5.0 ----Semi Volatile Organic Compounds 2.3 J 5.0

Control Date %Rec Limits Analyzed

102 40-133 2/5/ 15 13:07

98 37-117 2/5/ 15 13:07 37 10-107 2/5/ 15 13:07

94 39-119 2/5/ 15 13:07

55 10-105 2/5/ 15 13:07 112 28-157 2/511 5 13:07

--- -

Form lA

1\:llprcwsOO I \st~rhmsS\l..IMSRcps\An~l)ticaiRcpol1 rpl

MDL

1.0 1.2 1.0

II 1.2 1.0

1.6 1.4 5.9

1.0 1.0 1.2

6.9 1.0 1.0

2.2 1.2 1.3

1.0 1.0 1.4

0.68

Q

Service Request: RIS00757 Date Collected: NA Date Received: NA

Date Extracted: 2/4/1 5 Date Analyzed: 2/S/ 15 13:07

Units: f.lg/L Basis: NA



Note

0002'3 SuperSet Rcfc~ntc: t S-0000320289 f'C\' 00



QNQC Report

General Electric Company GE -Pinsfield NPDES Water

Lab Control Sample Summary

Service Request: R1 500757 Date Analyzed: 2/ 311 5


Analytical Method: 624 Units: pg/L Basis: NA

Analysis Lot: 431315

Lab Control Sample RQ 150 1304-03

Spike %Rcc

Ana1yte Name Result Amount %Rcc Limits

I, I, I-Trichloroethane (TCA) I8.6 20.0 93 52- I62

I,I ,2,2-Tetrachloroethane 16.6 20.0 83 46- 157

1,1 ,2-Trichloroethane 18.3 20.0 91 52- 150

I, 1-Dichloroethane (1, I-DCA) I8. I 20.0 9I 59- 155

I, I-Dichloroethene (I, 1-DCE) 18.4 20.0 92 10-234

1 ,2-Dichiorobenzene 19.0 20.0 95 18 - I90

I ,2-D ich loroethane 16.8 20.0 84 49- 155

I ,2-Dich loropropane I7.2 20.0 86 10-210

I ,3-Dichlorobenzene 19.0 20.0 95 59- 156

I ,4-Dichlorobenzene 18.8 20.0 94 I8- 190

2-Chloroethyl Vinyl Ether 18.0 20.0 90 10-305

Acrolein 80.3 100 80 10- 186

Acrylonitrile 94.4 100 94 84- I28

Benzene 18.9 20.0 94 37- 15I

Bromod ichloromethane 20.2 20.0 101 35- I55

Bromoform 21.9 20.0 1IO 45- 169

Bromomethane 16.6 20.0 83 10-242

Carbon Tetrachloride 21.1 20.0 105 70- I40

Ch lorobenzene 18.9 20.0 95 37- 160

Chloroethane 16.6 20.0 83 14- 230

Chloroform 19.5 20.0 98 51- 138

Chloromethane 18.7 20.0 94 IO- 273

Chlorodibromomcthane 20.8 20.0 104 53- 149

Dichlorodifluoromcthanc (CFC 12) 20.9 20.0 104 64- I30

Methylene Chloride 18.0 20.0 90 10-221

Ethyl benzene 18.7 20.0 94 37- 162

Tetrachloroethene (PCE) 19.4 20.0 97 64- 148

Toluene 18.9 20.0 95 47- I50

Trichloroethene (TCE) 20.1 20.0 100 71- IS7

Trichlorofluoromcthanc (CFC I I} 19.5 20.0 98 17- 181

Vinyl Chloride I9.2 20.0 96 10- 251

cis- I ,3-Dichloropropene 18.7 20.0 94 10-227

trans- I ,2-Dichloroethene 19.7 20.0 98 54· I 56

Re5ulls fbggtd ~·ith an asterisk(") indicate \'alues outside control criteria.

Percent n:covencs and relative percent dtfTcrenccs (RPD) arc determined by the software using values tn the calc:ulauon which have not been rounded

Printed 2/10!15 9·36 Form3C Oe921 .alprewsOO I \st~rhms$\l.IMSReps\LabControiSamplc 'l'l SuperSet Reference I 5-0000320289 rev 00



QNQC Report



Service Request: R I 500757 Date Analyzed: 213115


Ana lytical Method: 624

Analyte Name

trans-! ,3-Dichloropropene

Lab Control Sample RQ 1501304-03

Spike Result Amount % Rec

20.8 20.0 104

Ruulu flagged with 11n asterisk{*) indic11tc \ ' II lues ouuhlr control cr iteria.

-Jo Rec Limits

I 7 - 183


Analysis Lot: 43 1315

Percent recoveries and relative percent diffe rences (RPD111re dctcrmmcd by the softw3rc usmg values in the calculation wh1ch h3\·e not been rounded.

Prinlcd 2110115 9.36 Form3C 99922

1\alprcwsOOI\storlimsS\l.IMSRcps\LabControlSomplc rpt SuperSet Reference I S.()()()()320289 rev 00


QNQC Report

Clien't: General Electric Company Service Request: Rl500757

Project: GE -Pittsfield NPDES Date Analyzed: 2/ 5115

Sample Matrix: Water

Lab Control Sample Summary Scmivolatilc Organic Compounds by GC/MS

Analytical Method: 625 Units: Jlg/L

Prep Method: EPA 3510C Basis: NA

Extraction Lot: 228578

Lab Control Sample Duplicate Lab Control Sample

RQ1501175-02 RQ1501175-03

Spike Spike %Rcc RPD

Analytc Name Result Amount %Rcc Result Amount %Rcc Limits RPD Limit

Acenaphthene 86.5 100 86 85.6 tOO 86 47- 145 30

Acenaphthylene 89.7 100 90 88.3 100 88 33- 145 2 30

Anthracene 94.5 100 94 93.4 100 93 27- 133 30

Benzidine IOOU 100 0 • IOOU 100 0 • 10- 169 NC 30

Benz( a )anthracene 97.3 100 97 100 100 100 33- 143 3 30

B enzo( a )pyrene 99.3 100 99 103 100 103 17- 163 4 30

Benzo{b )fluoranthene 94.6 100 95 tot tOO 101 24- 159 7 30

Benzo(g,h, i)perylene 103 100 103 104 100 104 10-219 < I 30

Benzo(k )fluoranthcnc 90.2 100 90 90.1 100 90 11 - 162 <I 30

Butyl Benzyl Phthalate 109 100 109 Ill 100 Ill 10- 152 2 30

Di-n-butyl Phthalate 109 100 109 107 100 107 to- II8 2 30

lndeno( I ,2,3-cd)pyrene 103 100 103 104 100 104 10- 171 < I 30

Bis(2-chloroethoxy)methane 90.7 100 91 88.3 100 88 33- 184 3 30

Bis(2-chloroethyl) Ether 76.1 100 76 84.1 100 84 12- 158 10 30

2-Ch loronaphthalene 82.4 100 82 78.8 100 79 60- 118 4 30

2-Ch I oro phenol 83.3 100 83 86.7 100 87 23- 134 4 30

2,2'-0xybis( 1-chloropropane) 84.1 100 84 87.5 tOO 88 36- 166 4 30

Chrysene 98.7 100 99 100 100 100 17- 168 30

Dibenz( a,h)anthracene 105 100 lOS 107 100 107 10-227 2 30

3,3'-Dichlorobenzidine 86.3 100 86 90.1 100 90 10-262 4 30

2,4-Dichlorophenol 93.5 100 93 90.4 100 90 39- 135 3 30

Diethyl Phthalate 100 100 100 104 100 104 to- 114 4 30

Dimethyl Phthalate 95 .6 100 96 95.0 100 95 10- 112 < I 30

2,4-Dimethylphenol 96.2 100 96 90.9 100 91 32- 119 6 30

2,4-Dinitrophenol 91.3 100 91 81.3 100 81 10- 191 12 30

2,4-Dinitrotoluene 97.0 100 97 95.2 100 95 39- 139 2 30

2,6-Dinitrotoluene 96.5 100 97 95.3 100 95 50- 158 30

I ,2-Diphenylhydrazine 99.1 100 99 98.8 100 99 57- 117 < I 30

Bis(2-ethylhexyl) Phthalate Ill 100 Ill 112 tOO 112 10- 158 I 30

Fluoranthene 103 100 103 101 100 101 26- 137 I 30

Fluorene 90.1 100 90 87.8 100 88 59- 121 3 30

Hexachlorobenzene 96.8 100 97 92.4 tOO 92 10- 152 5 30

Hexachlorobutadiene 67.9 100 68 68.7 100 69 24- 116 I 30

Resulls flagged with an Asterisk(*) indiutc v·alu.s outside control criteria.

Percent rctoHric:s and rclau~·c percent dtfTcrcncc:s (RPD} arc: dctcnnmc:d by the sofiwure ustns values in the c:~lculation "hich have not been rounded.

Prinlcd 2110/1 S 9·36 FormJC etH1.123 ' l:llprewsOO 1\starlimsS\LIMSRcps\LabControiS:unplc rpt SuperSet Reference: I 5.0000320289 rev 00


QNQC Report

Clicn"t: General Electric Company Service Request: Rl500757




Analytical Method: 625 Units: ~giL

Prep Method: EPA 3SlOC Basis: NA


Lab Control Sample Duplicate Lab Control Sample RQ150117S-02 RQ1501175-03


Analytc Name Result Amount •;., Rcc Result Amount % Rec Limits RPD Limit

Hexachlorocyc1opentadiene 76.2 100 76 73.8 100 74 28-98 3 30

Hexachloroethane 59.3 100 59 63.9 100 64 40- 113 7 30

Isophorone 92.6 100 93 92.4 100 92 21. 196 <I 30

4,6-Din itro· 2 -methylpheno I 96.1 100 96 95.7 100 96 10- 181 < I 30

4-Chloro-3-methylphenol 99.1 100 99 97.1 100 97 22- 147 2 30

Naphthalene 72.4 100 72 68.5 100 69 21- 133 5 30

Nitrobenzene 92.6 100 93 89.6 100 90 35. 180 3 30

2-Nitrophenol 90.8 100 91 87.4 100 87 29- 182 4 30

4· N itropheno I 65.5 100 65 77.2 100 77 10- 132 16 30

N-N itrosodimethylamine 54.1 100 54 57.4 100 57 33.70 6 30

N-Nitrosodiphenylamine 98 .6 100 99 96.5 100 96 so- 117 2 30

Di-n-octyl Phthalate 106 100 106 I 14 100 I 14 10. 146 7 30

Pentachlorophenol (PCP) 91.8 100 92 98.7 100 99 14- 176 7 30

Phenanthrene 98.7 100 99 98.1 100 98 54. 120 <I 30

Phenol 38.1 100 38 40.8 100 41 10. 112 7 30

4-Bromophenyl Phenyl Ether 94.3 100 94 95.7 100 96 53- 127 30

4-Chlorophenyl Phenyl Ether 92.2 100 92 90.5 100 91 25 • ISS 2 30

N-Nitrosodi-n-propylamine 83.1 100 83 91.7 100 92 10.230 10 30

Pyrene 103 100 103 107 100 107 52· tiS 3 30

1 ,2,4· Trich1orobenzene 65.0 100 65 63.2 100 63 29-85 3 30

2,4,6-Trichlorophenol 96.0 100 96 97.3 100 97 37. 144 30

llc.,uliJ nagged with an U!lcrisk (*)indicate values oullidc control criteria.

Percent recoveries 11nd rel~II\'C percent differences (RPD) nrc detcrmmcd by the sofiw:m: usmc values m the cnlcul~tion which have not been rounded.

Printed 2110115 9.36

1\:llprcwsOOl\statlimsS\LlMSRcps\l.abControlSlllllplc rpt SuperSet Reference l 5.0000320289 rev 00

A ·Enulronmental CHAIN OF CUSTODY/LABORATORY ANALYSIS REQUEST FORM 23155 ·

1565 Jefferson Road, Building 300, Suite 360 • Rochester, NY 14623 I + 1 585 288 5380 + 1 585 288 8475 (fax) PAGE J OF/

l'n>leciName l'n>leciNumbo<

NPDES Permit Pn>jM:IM-0< ReportCC

Sean Covle Company/Addnlsa

VPnlir~ Fnvirnnn- ·• NA lGE CEPl

1nnn J:":~ct <:t

o: ..... r. ... t~ ~~~~~ 01 "l01 -· Ema~

111 'l_IIOJLt:::'70Q ~ 111 ':l-11 all_ 7nr:;.,

ANALYSIS REQUESTED (Include Method Number and Container Preservative)

PRESERVATIVE I t() I 0 Ul a: "' z ~ 8 u. 0

I I Preservative Key 0. NONE 1. HCL 2. HN03 3 . H2S04 4. NaOH 5. Zn. Acetate 6. MeQH 7. NaHS04 8. Other __

I~ '"'X''-·-- h - ·_ ~~~~~.J~~ ~;;~~~#-

~ ~ z

'~1ft,! !.tit ;(r$ ilj//jl 9f/&:?J&!Ji'!/~!/i.sfi.s REMARKS/

ALTERNATE DESCRIPTION ......- -~ "'

CLIENT SAMPLE ID

_L:.Ar.... .1.0~•· a .,."-1 ,..1 U~ ....... -~"'-C.,41WI ..LI' UY

_C..A~ ... ,.....,.&a 4V ,-.r "',.""' .... ~ ...... -~ T .. i ..... ot~..,.t,

SPECIAL INSTRUCTIONS/COMMENTS Metals

FOR OFfiCE USE ONLYLABID

.

~ ~~.:; tl'~~-·-~-~..._!»~: ::t.

I

1 c~~ :'i" :;(i; • 1 ~~/c.t" ....... ~-

~- -~·-101..-"

TURNAROUND REQUIREMENTS

--- RUSH ISURCIIARGES APPLY)

--- 1 day --2 day -----3 dey ---4 day -X day

REPORT REQUIREMENTS

__ I. Resulls Only

_ _ 11. Aes\JIIs + OC Summaries

(LCS. DUP, MSIMSO as requin!<l)

INVOICE INFORMATION

1'0.

BILL TO:

EPA 624 & 625 list included with COC's Samples packed in Ice __ n1. Resuns + oc anc1 Cllibration

Summanes REQUESTED REPORT DATE

_x 11/. Data validation Report with Raw Dala 1----------- ---1 SeeQAPP 0

SQTE WHERE SAMPLES WERE COLLECTED Edata __ Yes __ No

RECEIVED BY REUNQUISHEO BY RECEIVED BY REUNOUISHEO BY RECEIVED BY

.. / / Signal uno Signature Slgnalure Signature

PmtedNamo PMted Name PrintedNamo R1500757 5 f1rm Fi Fim Voolla Water North Amonea

""' GE .Pitlaftold NPOES

Dalalrvne Ootetrvne Datofrvne \\\\\\\\\\\\\\\1\\\\\\\1\\\\\\\\ \ll\\1\\\\\ll\\\\\ ~ 2012 by ALS Group

. A Cooler Receipt and Preservation Check Form

Project/Client ..sfr. ?dtb,i/ FolderNumber 4'1.)- 1.57 .

B,~~9S!Z§.?e. s ~iiil~iWB!!UiiMIJI BIIUU Ill

~~ I Cooler received on .J., l _J·-' by: l1iJ COURIER: ALS UPS ~ VELOCITY CLIENr. "" 1 Were Custody seals d'n outside of cooler? ~N Sa Perchlorate samples have required headspace? y N@)

2 Custody papers properly completed {ink, signed)?( tJ?N Sb Did VOA vials, Alk,or Sulfide have sig* bubbles? Y@NA

3 Did all bottles arrive in good condition (unbroken)? ~N 6 Where did the bottles originate? ("ALSIRO,V CLIENf

4 Circle:(Wet]§i> Dry Ice Gel packs present?, ~N 7 Soil VOA received as: Bulk Encore 5035set ~

8. Temperature Readings Date: z!J~- Time: 10/.~ ID: IR#3~ From: Temp Blank ~ f_

Observed Temp (0C) /.7' Correction Factor (OC) -1)./' Corrected Temp (OC) J./"' Within 0-6°C? (YJN y N y N y N y N y N y N

If out of Temperature, note packing/ice condition: Ice melted Poorly Packed Same Day Rule

&Client Approval to Run Samples: Standing Approval Client aware at drop-off Client notified by:

All samples held in storage location: 5035 samples placed in storage location:

PC Serondary Review:

_ifc.::' ~-,~<.:~:..::z...~- by ~ed;::;.....-- on -""§UJP-'--- at ;ol(, ----- by on at __ _

Cooler Breakdown: Date: Time: fl' (1.1/:, by:_--'1@~--==-----1. Were all bottle labels com te i.e. analysis, prefefVStion, etc.)? i NO 2. Did all bottle labels and tags agree with custody papers? NO 3. Were correct containers used for the tests indicated? NO

4. Air Samples: Cassettes I Tubes Intact Canisters Pressurized Tedlar® Bags Inflated l . ExpJam anv dJscrepancJes:

pH Reagent Yes No Lot Received Exp SampleiD Vol. Lot Added Final Yes:-AU samples OK

>12 NaOH $2 HN03

$2 H:zS04 <4 NaHS04

Residual ForCN Chlorine Phenol (-) and 522

Na2S203 . ZnAcetate . HCI ••

If+, contact PM to add Na1S103 (CN), ascorbic {phenol).

. -**

Added pH

**Not to be tested before analysis -pH tested and recorded by VOAs on a separate worksheet

No=Samples were preserved at The lab as listed

PMOK to Adjust:

Bottle lot numbers:. _ _,f'---!-r?.::.:~~-.fJ.if'-:a>"""""' ... J"<;,..--..,./4-0"'au.t ..... toCJV:(IC::.-...... I.u:1:l.:.LV:~------------------Other Comments:

PC Secondary Review: __ ... ""';::-::r+. _· ___ _ *significant air bubbles: VOA >5-6 mm : WC > 1 in. diameter

P .\INTRANET\QAQC\Forms Controlled\Coolcr Receipt r7.doc S/6114 00926

February 18, 2015


1 000 East Street Pittsfield, MA 0120 1

Laboratory Results for: GE -Pittsfield NPDES

Dear Mr. Coyle:

ALS Environmental ALS Group USA, Corp 1565 Jefferson Rd, Building 300, Suite 360 Rochester, NY 14623 T: 585-288-5380 F: 585-288-8475 www.alsglobal.com

Analytical Report for Service Request No: R1500964

Enclosed are the results of the sample(s) submitted to our laboratory on February 10, 2015. For your reference, these analyses have been assigned our service request number R1500964.

All analyses were performed according to our laboratory's quality assurance program. The test results meet requirements of the NELAP standards except as noted in the case narrative report. All results are intended to be considered in their entirety, and ALS Environmental is not responsible for use of less than the complete report. Results apply only to the items submitted to the laboratory for analysis and individual items (samples) analyzed, as listed in the report. The measurement uncertainty of the results included in this report is within that expected when using the prescribed method(s) for analysis of these samples, and represented by Laboratory Control Sample control limits. Any events, such as QC failures, which may add to the uncertainty are explained in the report narrative.

Please contact me if you have any questions. My extension is 7473. You may also contact me via email at [email protected].



~a:fu)'-Deb Patton Project Manager

Page 1 of Qlo

RIGHT PP.RTNER. 00fll31

Client: Service Request No.: Project: Date Received: Sample Matrix: Project/Case No.:

ALS Environmental

General Electric R1500964 GE-Pittsfield NPDES 2/10/15 Water

CASE NARRATIVE

All analyses were performed consistent with the quality assurance program of ALS Environmental. This report contains analytical results for samples designated for Tier II. When appropriate to the method, method blank results have been reported with each analytical test.

Sample Receipt

Three water samples were received for analysis at ALS Environmental on 2/10115. The samples were received in good condition and consistent with the accompanying chain of custody form. The samples were received within the 0-6°C temperature guidelines. The samples were stored in a refrigerator between l°C and 6°C upon receipt at the laboratory.

Volatile Organics



The Method Blank for Bromomethane contained a low level hit and has been flagged with a "J". No data was affected.





The Method Blank was free of contamination.

The Laboratory Control Sample and Duplicate Laboratory Control Sample (LCSD) for Benzidine and the LCSD for Di-n-butyl Phthalate and Diethyl Phthalate were outside ofthe control limits and have been flagged with a"*". There were no hits in the sample for these compounds. There may be a low bias in the sample for Benzidine.


Approved by __ _,C\'2~t'-1~0Qa-li..---------~Datc. __ .Qld,..._\J.::\~.\l....:<_ aooe2


\lalprews001\starllmsSILIMSReps\CaseNarrative rpt

Service Request Number: R 1500964

LabiO R 1500964-001 R 1500964-002

R 1500964-003

Client 10 64G-1 Q2M-2X-GV

64G-1 Q2M-2X-GS

TRIP BLANK

. A Enuironmental

u

J

B

E

E

D

•

H

#



N Inorganics- Matrix spike recovery was outside corrected for dilution and for percent moisture, unless otherwise noted in the case

laboratory limits.



Tentatively Identified Compound (TIC) or s Concentration has been determined using Method that the concentration is between the MRL of Standard Additions (MSA). and the MDL. Concentrations are not verified

\V Post-Digestion Spike recovery is outside control within the linear range of the calibration. For DoD: concentration >40% difference between

limits and the sample absorbance is <50% of the

two GC columns (pesticides!Arclors). spike absorbance.




Inorganics- Concentration is estimated due to Q DoD reports: indicates a pesticide/Aroclor is not the serial dilution was outside control limits. confirmed ~100% Difference between two GC



Concentration is a result of a dilution, MRL Method Reporting Limit. Also known as: typically a secondary analysis of the sample LOQ Limit of Quantitation (LOQ) due to exceeding the calibration range or that The lowest concentration at which the method a surrogate has been diluted out of the sample analyte may be reliably quantified under the and cannot be assessed. method conditions.


Analysis was performed out of hold time for LOD Limit of Detection. A value at or above the MDL tests that have an "immediate" hold time which has been verified to be detectable. criteria.

ND Non-Detect. Analyte was not detected at the Spike was diluted out. concentration listed. Same as U qualifier.

Lab ID # for Massachusetts Certification M-NY032

Analyses were conducted in accordance with Massachusetts Department of Environmental Protection certification standards, except as noted in the laboratory case narrative provided. A copy of the current Department issued parameter list is included in this report.

·z, G H ·:· 'C• !. J J' f ' •• ' I I l (; H 7 F •', l~ .l :'-i E R

P .\ INTRANE'nQAQC\Forms Controllcd\QUALIF _routine forMA r3.DOC S/1 MJ11) 13 1!J 4

The . Com1nonweal~h of Massa.chus~tts:

Depart1nent of Envi'ronme~tal Protection Division of Environme11tal Analysis

·Senator William X Wall Expefime11( Station

M-NY032

certifies

ALSEmnRONMENTALROCHESTER

1565 JEFFERSON RD BUILDING 300, SUITE 360 ROCHESTER, NY 14613-0000

Laboratory Director: · LARRY LEWIS

.· for the analysis ·of NON POTABLE WA~ER(CHEMISTRY)

pursuant to 310.CMR 42.00

This certificate supersedes all previous Massach~etts certificates issued to this laboratory. The laboratory is regulated by and shall be responsible for being in compliance with Ma.ssachuset~ reiula(io.ns at 310 CMR. 42.00.

This certificate is valid only when accompanied by the la_test dated Certified Parameter List issued by the Massachusetts b.E.P. Contact the Division ofEnvironmental Analysis to verify the."current certificatfqn status of the labpratqry.

Certification is no guarantee.ofthe validity of the data . . This certification is subject to unannounced laboratory inspections.

Issued: 01 JUL 2014

Expires: 30 JON 2015

Director, Division of Environmental Analysis

eooas

COMl\'IONWEALTH OF MASSACHUSETTS DEPARTMENT OF ENVIRONMENTAL PROTECTION

Certified Parameter List as of: 01JUL2014

M-NY032 ALS ENVIRONMENTAL ROCHESTER ·

ROCHESTER NY


Analytes

ALUMINUM

ANTIMONY

ANTIMONY

ARSENIC

ARSENIC

BERYLLIUM

BERYLliUM

CADMIUM

CADMIUM

CHROMIUM

CHROMIUM

COBALT

COBALT

COPPE~

COPPER

IRON

LEAD

LEAD

MANGANESE

MANGANESE

MERCURY

MOLYBDENUM

MOLYBDENUM

NICKEL ·

NICKEL

SELENIUM

SELENIUM

SILVER

SILVER

THALLIUM

THALLIUM

VANADIUM

VANADIUM

ZINC

ZINC




CALCIUM

MAGNESIUM

SODIUM

POTASSIUM

AU<AUNITY, TOTAL

June 26, 2014

Effective Date

01 JUL2014

*"" Provisional Certification


Methods

EPA200.7

EPA200.7

EPA200.B

EPA200.7

EPA200.8

EPA200.7

EPA200.8

EPA200.7

EPA200.B

EPA29Q.7

EPA200.8

EPA200.7

EPA200.8

EPA200.7

EPA200.B

EPA200.7

EPA200.7

EPA200.8

EPA200.7

EPA200.8

EPA245.1

EPA200.7

EPA200.8

EPA200.7

EPA200.8

EPA200.7

EPA200.8

EPA200.7

EPA200.S

EPA200.7

EPA200.8

EPA200.7

EPA200.8

EPA200.7

EPA200.8

EPA 120.1

SM2540C

SM2340C

EPA200.7

EPA200.7

EPA200.7

EPA200.7

SM2320B

Page 1 of 2

013006


CertlOed Parameter List ns of:

M~NY032 ALS ENVIRONMENTAL ROCHESTER

ROCHESTER NY


Analytes

CHLORIDE

CHLORIDE

FLUORIDE

SULFATE

AMMONIA·N

NITRATE·N

NITRATE·N

KJELDAHL·N

ORTHOPHOSPHATE

PHOSPHORUS, TOTAL




CYANIDE, TOTAL

NON·FIL TERABLE RESIDUE

OIL AND GREASE

PHENOLICS, TOTAL

VOLA TILE HALO CARBONS

VOLA TILE HALOCARBONS

VOLA TILE AROMATICS

VOLATILE AROMATICS

SVOC.ACID EXTRACTABLES

SVOC.BASEINEUTRAL EXTRACT ABLES

POL YCHLORINATEO BIPHENYLS (WATEf

Effective Date

01 JUL2014

01 JUL2014

June 26, 2014 *= Provisional Certification

Expiration 30JUN2015 Date

Methods

SM 4500-CL·E

EPA300.0

EPA300.0

EPA300.D

EPA350.1

EPA 300.0

EPA 353.2

EPA351.2

EPA365.1

E.PA365.1

EPA410.4

SM5210B

SM5310C

EPA335.4

SM25400

EPA 1664

EPA420.4

EPA601

EPA624

EPA602

EPA624

EPA625

EPA625

EPA608

Page 2 of 2

eetHJ7



Analytical Method: Data File Name:

CAS No.

71-55-6 79-34-5 79-00-5 -----75-34-3 75-35-4 95-50-1

107-06-2 78-87-5 541-73-1

106-46-7 110-75-8 107-02-8

107-13-1 71-43-2 75-27-4

75-25-2 74-83-9 56-23-5

108-90-7 75-00-3 67-66-3

74-87-3 124-48-1 75-71-8

75-09-2 100-41-4 127-18-4

108-88-3 79-01-6 75-69-4 ----75-01-4 10061-01-5 156-60-5

10061-02-6

Printed 211 8fJ 5 9 SS


Analytical Report


64G-I Q2M-2X-GV RI500964-00 I

Service Request: R 1500964 Date Collected: 2/ 9/ 15 0710 Date Received: 211 Oil 5 Date Analyzed: 2ft 2/15 I I :32

Units: ~giL

Basis: NA


624 Analysis Lot: 432507

1:\ACQUDAT A \MSVOA6\DA T A \021215\M0368.D\ Instrument Name: R-MS-06 Dilution Factor: 1

Analyte Name Result Q MRL MDL Note

1,1, 1-Trichloroethane (TCA) 1.0 u 1.0 0.13

1, 1 ,2,2-Tetrachloroethane 1.0 u 1.0 0.23

I, I ,2-Trichloroethane 1.0 u 1.0 0.12 -I, 1-Dichloroethane (I 1 I-DCA) 0.49 J 1.0 0.10

I, 1-Dichloroethene (I I 1-DCE) 1.0 u 1.0 0.22

I ,2-Dichlorobenzene 1.0 u 1.0 0.10 --I ,2-Dichloroethanc 1.0 u 1.0 0.18

I ,2-Dichloropropane 1.0 u 1.0 0.15

I ,3-Dichlorobenzenc 1.0 u 1.0 0.10 ---I ,4-Dichlorobcnzene 1.0 u 1.0 0.15

2-Chloroethyl Vinyl Ether 10 u 10 0.64

Acrolein 10 u 10 0.73 --- ~- --

Acrylonitrile 10 u 10 0.37

Benzene 1.0 u 1.0 0.10

Bromodichloromethane 1.0 u 1.0 0.15

Bromoform 1.0 u 1.0 0.16

Bromomethane 1.0 u 1.0 0.12

Carbon Tetrachloride 1.0 u 1.0 0.10

Chlorobenzene 1.0 u 1.0 0.13

Chloroethane 0.65 J 1.0 0.15

Chloroform 1.0 u 1.0 0.13

Chloromethane 1.0 u 1.0 0.16

Chlorod ibromomethane 1.0 u 1.0 0.15 Dichlorodifluoromcthanc (CFC 12) 1.0 u 1.0 0.17

Methylene Chloride 1.0 u 1.0 0.18

Ethylbenzene 1.0 u 1.0 0.19

Tetrachloroethene (PCE) 1.0 u 1.0 0.20 ----Toluene 1.0 u 1.0 0.10

Trichloroethene (TCE) 1.0 u 1.0 0.15 Trichlorofluoromcthanc (CFC II) 1.0 u 1.0 0. 13

Vinyl Chloride 1.0 u 1.0 0.14

cis- I 13-Dichloropropene 1.0 u 1.0 0.14

trans- I 12-Dichloroethene 1.0 u 1.0 0. 15 -- -

trans- I 13-Dichloropropene 1.0 u 1.0 0. 10

Fonn lA eoeos 1\alprcwsOO llstarhmsS\LIMSRcps\Annl)1icn1Rcpon rpt Su~rSct Reference: IS·000032127S rcv OO




Analytical Report


64G-I Q2M-2X-GV R 1500964-00 1

Sen·ice Request: Rl500964 Date Collected: 21911 5 0710 Date Received: 2/10/1 5 Date Analyzed: 2/12fl 5 II :32


Volatile Organic Compounds by GC/MS with 3 Day Holding Time for Acrolein, Unprescrvcd


Analysis Lot: 432507 Instrument Name: R-MS-06

Dilution Factor: I

Control Date Surrogate Name %Rcc Limits Analyzed Q

I ,2-D ich lorocthane-d4 90 81-127 2/1211 5 11:32

4-Bromonuorobenzenc 99 79-123 2112115 II :32

Toluene-dB 100 83-120 2/12115 II :32

Printed 2/18/1 S 9.55 Form lA 0 0 0 f3 9

\lalpn:wsOOIIstnrlimsS\LlMSRcps\AnnlyticnlRcpon.rpt SuperSet Reference IS·000032\27S rcvOO




Analytical Report


Service Request: R1500964 Date Collected: 2/9/15 Date Received: 2/ I 0/1 5 Date Analyzed: 211211 5 1132

Volatile Organic Compounds by GC/MS with 3 Day Holding Time ror Acrolein, Unprcserved


64G-IQ2M-2X-GV R I 500964-00 I



Units: jlg/L Basis: NA


Comments:

Printed 0211812015 9.55 Form IB 00910 \\alprews001\stilflimsS\liMSReps\Ana1)1icalTICRepon.rpt SuperSet Reference 15-0000321275 rcv OO


Analytical Report




64G-1 Q2M-2X-GS R 1500964-002

Semivolatile Organic Compounds by GC/MS

Analytical Method: 625 Prep Method: EPA 3510C Data File Name: I:\ACQUDATA\5973D\Data\021215\BA827.D\

CAS No. Annlyte Name Result Q MRL

83-32-9 Acenaphthene 4.7 u 4.7 208-96-8 Acenaphthylene 4 .7 u 4.7

120-12·7 Anthracene 4.7 u 4.7 -92-87-5 Benzidine 94 u 94 56-55-3 Benz( a)anthracene 4.7 u 4.7 50-32-8 Benzo(a)pyrene 4.7 u 4.7

--205-99-2 Benzo(b )fluoranthene 4.7 u 4.7 \91-24-2 Benzo(g,h, i)perylene 4.7 u 4.7 207-08-9 B enzo(k) n uoranthene 4.7 u 4.7

85-68-7 Butyl Benzyl Phthalate 4.7 u 4.7 84-74-2 Di-n-butyl Phthalate 4.7 u 4.7 193-39-5 Indcno( 1,2,3-cd)pyrene 4.7 u 4.7

111-91-1 B is(2-chloroethoxy )methane 4.7 u 4.7 111-44-4 Bis(2-chloroethyl) Ether 4.7 u 4.7 91-58-7 2-Chloronaphthalene 4.7 u 4.7

95-57-8 2-Chlorophenol 4.7 u 4.7 108-60-1 2,2'-0xybis( 1-chloropropane) 4.7 u 4.7 218-01-9 Chrysene 4.7 u 4.7

--53-70-3 Dibenz(a,h)anthracene 4.7 u 4.7 91-94-1 3,3'-Dichlorobenzidine 4.7 u 4.7 120-83-2 2,4-Dichlorophenol 4.7 u 4.7 -- -84-66-2 Diethyl Phthalate 4.7 u 4.7 131-11-3 Dimethyl Phthalate 4.7 u 4.7 105-67-9 2,4-Dimethylphenol 4.7 u 4.7

----51-28-5 2,4-Dinitrophenol 47 u 47 121-14-2 2,4-Dinitrotoluene 4.7 u 4.7 606-20-2 2,6-Dinitroto\uene 4.7 u 4.7 -- --122-66-7 1,2-Diphenylhydrazine 4.7 u 4.7 117-81-7 Bis(2-ethylhexyl) Phthalate 4.7 u 4.7 206-44-0 Fluoranthene 4.7 u 4.7 - --86-73-7 Fluorene 4.7 u 4.7 118-74-1 Hexachlorobenzcne 4.7 u 4.7 87-68-3 Hexachlorobutadiene 4.7 u 4.7 - -- -77-47-4 Hexachlorocyclopentadiene 4.7 u 4.7

Printed 2118/15 9.55 Fonn lA.

\WprewsOOl\starlimsS\LlMSRcps\Anni)1Jco1Repon rpl

MDL

1.0 1.0 1.0

90 1.0 1.0

1.0 1.0 1.0

2.4 1.0 1.2

2.2 1.3 1.0

1.0 1.0 1.0

1.3 4.5 1.3

1.0 1.0 1.5

20 1.6 1.8

1.0 1.2 1.0

1.0 1.0 1.3

1.0

Service Request: Rl500964 Date Collected: 2/9/ 15 0710 Date Received: 2/ I 0/ 15

Date Extracted: 2/10115 Date Analyzed: 2112115 12:24

Units: J!g/L Basis: NA



Note

eao:t1 SuperSet Reference IS.0000l2127S rev 00




CAS No.

67-72-1 78-59-1 534-52-1

59-50-7 91-20-3 98-95-3

88-75-5 100-02-7 62-75-9

86-30-6 I I 7-84-0 87-86-5

85-01-8 108-95-2 101-55-3

7005-72-3 621 -64-7 129-00-0

120-82- 1 88-06-2

Surrogate Name

p-Terphenyl-d 14 N itrobenzene-d5 Phenol-d6

2-Fiuorobiphcnyl 2-Fluorophenol 2,4,6-Tribromophenol

Printed 2118/JS )4·39


Analytical Report


64G-I Q2M-2X-GS R 1500964-002


625 EPA 3510C 1:\ACQUDA T A \5973 D\Data\021215\BA827.0\


Hexachloroethane 4.7 u 4.7 lsophoronc 4.7 u 4.7 4,6-Dinitro-2-methylphcnol 47 u 47

4-Chloro-3-mcthylphenol 4.7 u 4.7 Naphthalene 4.7 u 4.7 Nitrobenzene 4.7 u 4.7

-2-N itrophenol 4.7 u 4.7 4-Nitrophenol 47 u 47 N-Nitrosodimcthylamine 4.7 u 4.7

N-Nitrosodiphenylamine 4.7 u 4.7 Di-n-octyl Phthalate 4.7 u 4.7 Pentachlorophenol (PCP) 47 u 47

Phenanthrene 4.7 u 4.7 Phenol 4.7 u 4.7 4-Bromophenyl Phenyl Ether 4.7 u 4.7

-4-Chlorophenyl Phenyl Ether 4.7 u 4.7 N-N itrosodi-n-propylamine 4.7 u 4.7 Pyrene 4.7 u 4.7

1 ,2,4-Trichlorobenzene 4.7 u 4.7 2,4,6-Trichlorophenol 4.7 u 4.7 Semi Volatile Organic Compounds 4.7 u 4.7 --- ---

Control Date % Rec Limits Analyzed

87 40-133 2/12/ 15 12:24 83 37-117 211 2/ 15 12:24 34 10-107 2/12/ 15 12:24

84 39- 119 211 2/ 15 12:24 47 10-105 2/ 12/ 15 12:24

113 28-157 2/ 12/ 15 12:24

Foon l A

\l:!lprews00 1 1s1arl•msSILIMSRcps\An~lyticalRcpon.rpl

MDL

1.2 1.0 II

1.2 1.0 1.6

1.4 5.9 1.0

1.0 1.2 6.9

1.0 1.0 2.2

1.2 1.3 1.0

1.0 1.4

0.68

Q

Sen•ice Request: Rl500964 Date Collected: 2/ 9/ 15 0710 Date Recei\'ed: 2/ 10/ 15

Date Extracted: 2/ 10/15 Date Analyzed: 2/ 12/ 15 12:24


Anal)'sis Lot: 432653 Extraction Lot: 228975

Instrument Name: R-MS-54 Dilution Factor:

Note

----

60012 Supc:rSc1 Rcfcrcnc:c: IS.000032ll7S N\' 00


Sample Name: Lnb Code:


Analytical Report


TRIP BLANK R 1500964-003

Service Request: RIS00964 Date Collected: 219/ 15 0710 Date Received: 2/1 Oil S Date Analyzed: 2/12/15 11 :00

Units: flg/L Basis: NA

Volatile Organic Compounds by GC/ MS with 3 Day Holding Time for Acrolein, Unpreserved


Data File Name: 1:\ACQUDATA\MSVOA6, DATA\021215\M0367.D\ Instrument Name: R-MS-06 Dilution Factor:

CAS No. Analytc Nnme Result Q MRL MDL Note

71-55-6 I, 1,1-Trichloroethanc (TCA) 1.0 u 1.0 0 .13

79-34-5 I, I ,2,2-Tetrachloroethane 1.0 u 1.0 0 .23

79-00-5 I, 1,2-Trichloroethane 1.0 u 1.0 0.12

75-34-3 1,1-Dichloroethane (\,I-DCA) 1.0 u 1.0 0.10


95-50-1 I ,2-Dichlorobenzene 1.0 u 1.0 0.10 --- --- --107-06-2 I ,2-Dichloroethane 1.0 u 1.0 0.18

78-87-5 I ,2-Dichloropropanc 1.0 u 1.0 0.15

541-73-1 I ,3-Dichlorobcnzene 1.0 u 1.0 0.10 - ------106-46-7 I ,4-Dich\orobenzene 1.0 u 1.0 0.15


107-02-8 Acrolein 10 u 10 0.73 - ------107-13-1 Acrylonitrile 10 u to 0.37

71-43-2 Benzene 1.0 u 1.0 0. 10

75-27-4 Bromodichloromethane 1.0 u 1.0 0.15

75-25-2 Bromofonn 1.0 u 1.0 0.16

74-83-9 Bromomcthane 1.0 u 1.0 0.12


108-90-7 Chlorobenzene 1.0 u 1.0 0.13

75-00-3 Chloroethanc 1.0 u 1.0 0.15

67-66-3 Chlorofonn 1.0 u 1.0 0.13 ---- -

74-87-3 Chloromethane 1.0 u 1.0 0.16

124-48-1 Chlorod ibromomethane 1.0 u 1.0 0.15

75-71-8 DichlorodiOuoromcthane (CFC 12) 1.0 u 1.0 0.17 -


127-18-4 Tetrachloroethene (PCE) 1.0 u 1.0 0.20 -108-88-3 Toluene 1.0 u 1.0 0 .10


75-69-4 TrichloroOuoromcthllnc (CFC II) 1.0 u 1.0 0 . 13 --- --75-01-4 Vinyl Chloride 1.0 u 1.0 0 .14

10061-01-5 cis- I ,3-Dichloropropene 1.0 u 1.0 0. 14 156-60-5 trans- I ,2-Dichloroethene 1.0 u 1.0 0.15

10061-02-6 trans-! ,3-Dichloropropenc 1.0 u 1.0 0 .10

Printed 2/18115 9 55 Foon lA 00'313 1\.llprewsOO llsrarlimsS\LIMSRcps\AnnlyiJcalReport rp1 Supc:rScr Reference: 15.0000321275 revOO




Analytical Report



Service Request: Rl500964 Date Collected: 2/ 9/ 15 0710 Date Received: 211 Oil 5 Date Analyzed: 2112/ 15 11:00

Units: !lg/L Basis: NA

Volatile Organic Compounds by GC/MS with 3 Day Holding Time for Acrolein, Unprescrvcd



Dilution Factor: I

Control Date Surrogate Name o/. Rcc Limits Analyzed Q

I ,2-Dichloroethane-d4 94 81-127 2112/ 15 11:00 4-B romofluorobenzcne 97 79-123 211211 5 I I :00 Toluene-d8 100 83-120 2112/ 15 11:00

Printed 2118115 9 55 Form lA t.lJ t.lJ Q 14

\\alprcwsOOI\st~rlirnsS\LIMSRcps\AnalyticaiRcpoll .lllt SuperSet Reference: 15.0000321275 rev 00




Anal}1ical Report


Service Request: R1500964 Date Collected: 219/ 15 Date Received: 2!1 0/15 Date Analyzed : 2fl 211 5 1100






Units: ~giL

Basis: NA

No Tentati\.cly Identified Compounds Detected.

Commt nts:

Printed 02/18/2015 9:55 Form In 0 0 0 15

llalprewsOOIIsl~rlimsS\LIMSReps\An~l)11taiTICRcpon.tpt SuperSet Reference. IS-0000321275 revOO




CAS No.

7 I -55-6 79-34-5 79-00-5 -75-34-3 75-35-4 95-50-1 -----107-06-2 78-87-5 541-73-1

106-46-7 II 0-75-8 107-02-8 --107-13-1 71-43-2 75-27-4

75-25-2 74-83-9 56-23-5

--108-90-7 75-00-3 67-66-3

74-87-3 124-48-1 75-71-8

75-09-2 100-41-4 127-18-4

108-88-3 79-01-6 75-69-4

75-01-4 10061-01-5 156-60-5

10061-02-6

Printed 2118/IS 9.55


Analytical Report


Service Request: R 1500964 Date Collected: NA Date Received: NA Date Analyzed: 2112/15 10:26

Method Blank RQJ501575-04



624 Analysis Lot: 432507 I:\ACQUDATA\MSVOA6\DATA\021215\M0366.D\ Instrument Name: R-MS-06

Dilution Factor:


1,1, !-Trichloroethane (TCA) 1.0 u 1.0 0.13 I, 1 ,2,2-Tetrachloroethane 1.0 u 1.0 0.23 I, I ,2-Trichloroethane 1.0 u 1.0 0.12

I, 1-Dichloroethane (I, I-DCA) 1.0 u 1.0 0.10 I, 1-Dichlorocthene (I, I -DCE) 1.0 u 1.0 0.22 I ,2-Dichlorobenzene 1.0 u 1.0 0.10 -- -I ,2-Dichloroethane 1.0 u 1.0 0.18 I ,2-D ichl oropropane 1.0 u 1.0 0.15 I ,3-Dichlorobenzene 1.0 u 1.0 0.10

I ,4-Dichlorobcnzene 1.0 u 1.0 0.15 2-Chloroethyl Vinyl Ether 10 u 10 0.64 Acrolein 10 u 10 0.73 -- --Acrylonitrile 10 u 10 0.37 Benzene 1.0 u 1.0 0.10 Bromod ichloromethanc 1.0 u 1.0 0.15

Bromoform 1.0 u 1.0 0.16 Bromomethane 0.16 J 1.0 0.12 Carbon Tetrachloride 1.0 u 1.0 0.10 ----Chi oro benzene 1.0 u 1.0 0.13 Chloroethane 1.0 u 1.0 0.15 Chloroform 1.0 u 1.0 0.13 -----Chloromethane 1.0 u 1.0 0.16 Chlorodibromomethane 1.0 u 1.0 0.15 Dichlorodifluoromcthanc (CFC 12) 1.0 u 1.0 0.17

~----

Methylene Chloride 1.0 u 1.0 0.18 Ethyl benzene 1.0 u 1.0 0.19 Tetrachloroethene (PCE) 1.0 u 1.0 0.20

Toluene 1.0 u 1.0 0.10 Trichloroethcne (TCE) 1.0 u 1.0 0.15 Trichlorofiuoromcthanc (CFC II) 1.0 u 1.0 0.13 - ---Vinyl Chloride 1.0 u 1.0 0.14 cis- I ,3-Dichloropropene 1.0 u 1.0 0.14 trans-1 ,2-Dichloroethene 1.0 u 1.0 0.15 -- -trans- I ,3-Dichloropropene 1.0 u 1.0 0.10

Fonn lA

-

\lalprewsOOl\starlimsS\LIMSRers\Anol)11tlliRcpon.rpt SuperSet Reference: 15..0000321275 revOO




Analytical Report


Method Blank RQ 1501575-04

Service Request: R 1500964 Date Collected: NA Date Received: NA Date Analyzed: 211 211 5 10:26

Units: Percent Basis: NA




Dilution Factor:


I ,2-Dichloroethane-d4 91 81-127 2/ 12/ 15 10:26 4-B romofluorobenzenc 93 79-123 2/ 12/15 10:26 Tolucne-d8 97 83-120 2/ 12/15 10:26

---

Printed 2/18/l S 9 S S Form I A f3 f3 13 1 7 •,\nJpn:wsOO l\s!~rhmsS\LIMSRcps\Analyti':~IRcport rpl SuperSet Reference JS.000032127S revOO

Client: Project: Sa mple Matrix:

ALS Group USA, Corp. dba ALS Environmenta l


Anal}1ical Report

Tentath·e1y Identified Compounds (TIC)

Service Request: R 1500964 Date Collected: NA Date Received: NA Date Analyzed: 2/12115 1026



Method Blank RQ 150 I 575-04



Units: jJg/L Basis: NA


Comments:

Printed 02/181201 s 9-55 Form IB 130018

1\DiprewsOO 1\starhmsS\l.IMSReps\AnalytiCOIITICReport rpt SuperSet Reference IS--0000321275 revOO


Analytical Report




Method Blank RQ1501387-0I

Scmi\'olatile Organic Compounds by GC/MS

Analytical Method: 625 Prep Method: EPA 35JOC Data File Name: 1:\ACQUDA T A \5973 D\Data\02 I 215\BA822.D\

CAS No. Analyte Name Result Q MRL

83-32-9 Acenaphthene 5.0 u 5.0

208-96-8 Acenaphthylene 5.0 u 5.0 120-12-7 Anthracene 5.0 u 5.0 ----92-87-5 Benzidine 100 u 100 56-55-3 Benz( a)anthracene 5.0 u 5.0 50-32-8 B enzo( a )pyrene 5.0 u 5.0

--- ~--

205-99-2 Benzo(b )tluoranthene 5.0 u 5.0 191-24-2 B enzo(g,h, i )perylene 5.0 u 5.0 207-08-9 Bcnzo(k)tluoranthene 5.0 u 5.0 ---85-68-7 Butyl Benzyl Phthalate 5.0 u 5.0 84-74-2 Di-n-butyl Phthalate 5.0 u 5.0 193-39-5 lndeno( I ,2,3-cd)pyrene 5.0 u 5.0

111-91-1 B is(2-ch loroethoxy )methane 5.0 u 5.0 111-44-4 Bis(2-chloroethyl) Ether 5.0 u 5.0 91-58-7 2-Ch Joronaphthalene 5.0 u 5.0

95-57-8 2-Chlorophenol 5.0 u 5.0 108-60-1 2,2'-0xybis( 1-chloropropanc) 5.0 u 5.0 218-01-9 Chrysene 5.0 u 5.0

53-70-3 Dibenz(a,h)anthracene 5.0 u 5.0 91-94-1 3,3'-Dichlorobenzid ine 5.0 u 5.0 120-83-2 2,4-Dichlorophcnol 5.0 u 5.0

~--

84-66-2 Diethyl Phthalate 5.0 u 5.0 131-11-3 Dimethyl Phthalate 5.0 u 5.0 105-67-9 2,4-Dimethylphcnol 5.0 u 5.0

--51-28-5 2,4-Dinitrophenol 50 u 50 121-14-2 2,4-Dinitrotoluene 5.0 u 5.0 606-20-2 2,6-Din itrotoluene 5.0 u 5.0 ----122-66-7 I ,2-Diphenylhydrazine 5.0 u 5.0 117-81-7 Bis(2-ethylhcxyl) Phthalate 5.0 u 5.0 206-44-0 Fluoranthene 5.0 u 5.0 --- ----86-73-7 Fluorene 5.0 u 5.0 118-74-1 Hexachlorobenzene 5.0 u 5.0 87-68-3 Hexachlorobutadiene 5.0 u 5.0

77-47-4 H exach lorocyclopentad iene 5.0 u 5.0

Printed 2/18/15 9.55 Form lA

\\alprewsOOI\s1;alimsS\!.IMSReps\Anal~11caiRepon.rp1

MDL

1.0 1.0 1.0

90 1.0 1.0

1.0 1.0 1.0

2.4 1.0 1.2

2.2 1.3 1.0

1.0 1.0 1.0

1.3 4.5 1.3

1.0 1.0 1.5

20 1.6 1.8

1.0 1.2 1.0

1.0 1.0 1.3

1.0

Service Request: Rl500964 Date Collected: NA Date Received: NA

Date Extracted: 211 0115 Date Analyzed: 2112115 10:15

Units: ~giL

Basis: NA



Note

eoo1s SuperSet Refen:nce 15·000032127 S rev 00




Analytical Report


Method Blank RQJ501387-0l

Semivolatile Organic Compounds by GCIMS

Analytical Method: 625 Prep Method: EPA 35JOC Data File Name: I:\ACQUDATA\5973D\Data\021215\BA822.D\

CAS No. Analyte Name Result Q MRL

67-72-1 Hexachloroethane 5.0 u 5.0 78-59-1 lsophoronc 5.0 u 5.0 534-52-1 4 ,6-D initro-2-mcthy I p he no l 50 u 50

--- ---59-50-7 4-Chloro-3-methylphenol 5.0 u 5.0 91-20-3 Naphthalene 5.0 u 5.0 98-95-3 Nitrobenzene 5.0 u 5.0 ----- -----88-75-5 2-Nitrophenol 5.0 u 5.0 100-02-7 4-Nitrophenol 50 u 50 62-75-9 N -N itrosod imethylamine 5.0 u 5.0

MDL

1.2 1.0 II

1.2 1.0 1.6

Service Request: R 1500964 Date Collected: NA Date Received: NA

Date Extracted: 2/10/15 Date Analyzed: 2/12115 10:15




Note

----1.4 5.9 1.0

-- ------- ---- - - --86-30-6 N-Nitrosod iphenylamine 5.0 u 5.0 1.0 117-84-0 Di-n-octyl Phthalate 5.0 u 5.0 1.2 87-86-5 Pentachlorophenol (PCP) 50 u 50 6.9

85-01-8 Phenanthrene 5.0 u 5.0 1.0 108-95-2 Phenol 5.0 u 5.0 1.0 101-55-3 4-Bromopheny\ Phenyl Ether 5.0 u 5.0 2.2 -----'7005-72-3 4-Ch\orophcny\ Phenyl Ether 5.0 u 5.0 1.2 621-64-7 N -N itrosod i-n-propylaminc 5.0 u 5.0 1.3 129-00-0 Pyrcne 5.0 u 5.0 1.0

)20-82-1 I ,2,4-Trichlorobenzene 5.0 u 5.0 1.0 88-06-2 2,4,6-Trichlorophenol 5.0 u 5.0 1.4

Semi Volatih! Oreonic Compounds 5.0 u 5.0 0.68 -- ---- ----- --- ----


p-Terphcnyl-d 14 99 40-133 2/12115 10:15 N itrobenzene-d5 84 37-11 7 2/1211 5 10:15 Phenol-d6 32 10-107 2/ 12/ 15 10:15 --- - -- -2-Fiuorobipheny\ 79 39-119 2/12/ 15 10:15 2-Fiuorophenol 46 10-105 2/1211 5 10:15 2,4,6-Tribromophenol 106 28 6 157 2/ 12/ 15 10:15

----

Printed 2118115 14:39 Fonn li\ 0 13 Q 2 f3 \lalprcwsOO 1 \starhmsS\LIMSRcps\Annl)1i,alRcpon Ill! SuperSet Rcfcrcn'c I 5-000032127 S rev 00


ALS Group USA9 Corp. dba ALS Environmental

QNQCReport



Service Request: Rl500964 Date Analyzed: 2/ 12115

Volatile Organic Compounds by GC/MS with 3 Day Holding Time for Acrolein9 Unpreserved

Analytical Method: 624 Units: J!g/L Basis: NA



Spike % Rec Analyte Name Result Amount % Rec Limits

1,1 , 1-Trichloroethane (TCA) 19.3 20.0 96 52- 162 I, 1 ,2,2-Tetrachloroethane 17.1 20.0 86 46- 157 I, 1 ,2-Trichloroethane 18.8 20.0 94 52- 150

I, 1-Dichloroethane (1, I-DCA) 17.9 20.0 89 59- 155 I, 1-Dichloroethene ( 1, 1-DCE) 19.3 20.0 97 10-234 I ,2-Dichlorobenzenc 19.9 20.0 100 18 - 190

1 ,2-Dich loroethane 17.8 20.0 89 49- 155 I ,2-Dich loropropanc 17.3 20.0 86 10-210 I ,3 -Dich I oro benzene 20.0 20.0 100 59 - 156

I ,4-D ich I oro benzene 19.9 20.0 100 18- 190 2-Chloroethyl Vinyl Ether 16.2 20.0 81 10-305 Acrolein 73. 1 100 73 10- 186

Acrylonitrile 95.6 100 96 84- 128 Benzene 19.1 20.0 95 37- 151 Bromodichloromethanc 20.2 20.0 101 35- 155

Bromoform 21.4 20.0 107 45- 169 Bromomethane 17.5 20.0 87 10-242 Carbon Tetrachloride 21.9 20.0 109 70- 140

Ch lorobenzene 19.9 20.0 99 37- 160 Chloroethane 17.9 20.0 90 14-230 Chloroform 19.8 20.0 99 51 - 138

Chloromethane 20.2 20.0 101 10-273 Chlorodibromomethane 20.4 20.0 102 53- 149 Dichlorodifluoromethnnc (CFC 12) 20.8 20.0 104 64- 130

Methylene Chloride 19.3 20.0 97 10-221 Ethylbenzene 18.8 20.0 94 37- 162 Tetrachloroethene (PCE) 21.5 20.0 108 64- 148

Toluene 19.3 20.0 96 47- 150 Trichloroethene (TCE) 21.1 20.0 105 71 - 157 Trichlorofluoromcthane (CFC II) 20.4 20.0 102 17- 181

Vinyl Chloride 19.5 20.0 98 10- 251 cis- I ,3-Dichloropropene 18.9 20.0 94 10-227 trans- I ,2-Dichloroethene 20.6 20.0 103 54- 156

Results nallttl'tl with an 11Jicrisk (")indicate nlurs outsillc control criteria.

Percent reco\·cries and relative percent difTcrcnccs (RPD) arc determined by the softw:~re usmg v:~lues in the calculatiOn which ha\'c not been rounded

Printed 2/18115 9 55 form3C eee21 \lalprc:wsOOllstarlrmsS\LIMSRcpsllolbControiS:unple.rpt SuperSet Rcrercncc 15.0000321275 rcvOO



QAJQC Report General Electric Company GE -Pittsfield NPDES Water


Service Request: R 1500964 Date Analyzed: 211211 5



Analyte Name

trans-1,3-Dichloropropene

Lab Control Sample RQ 150 I 575-03


20.1 20.0 101

Results fbj!gcd with nn u terisk ( •) indicntc •·nlucs outside coni rol criteria.

%Rec Limits

17- 183



Percent recoveries and relative percent differences (RPD) arc determined by the sofiwnrc using \'Blues in the calculation which have not been rounded

Printed 2/18/1 S 9 55 Fonn JC {!) 0 0 2 2 \l:llprcwsOO I \starhmsS\liMSRcpsllnbControiSamplc rpt SuperSet Rcrcrencc 15.000032127 S rev 00


QNQC Report

Client: General Electric Company Service Request: R1500964

Project: GE -Pittsfield NPDES Date Analyzed: 2112/15


Lab Control Sample Summary Semivolatilc Organic Compounds by GC/MS




Lab Control Sample Duplicate Lab Control Sample RQISOI387-02 RQ1501387-03

Spike Spike % Rec RPD

Analyte Name Result Amount % Rcc Result Amount % Rec Limits RPD Limit

Acenaphthene 95.2 100 95 98.5 100 98 47. 145 3 30

Acenaphthylene 97.6 100 98 101 100 101 33. 145 4 30

Anthracene 99.1 100 99 lOS 100 lOS 27. 133 6 30

Benzidine 100 u 100 0 • 100 u 100 0 • 10. 169 NC 30

Benz(a)anthracene 101 100 101 106 100 106 33. 143 4 30

Benzo(a)pyrene 103 100 103 109 100 109 17. 163 6 30

Benzo(b )fluoranthene 101 100 101 107 100 107 24- 159 6 30

Benzo{g,h, i)perylene 103 100 103 109 100 109 10-219 6 30

Benzo(k)fluoranthene 92.6 100 93 101 100 101 II- 162 8 30

Butyl Benzyl Phthalate Ill 100 Ill 116 100 116 I 0- 152 4 30

Di-n-butyl Phthalate 114 100 114 120 100 120 • 10- 118 5 30

Indeno( I ,2,3-cd)pyrene 103 100 103 108 100 108 10- 171 5 30

B is(2-chl oroethoxy )methane 91.3 100 91 92.2 100 92 33- 184 < I 30

Bis(2-chloroethyl) Ether 82.2 100 82 84.4 100 84 12 - 158 3 30

2-Chloronaphthalene 85.6 100 86 90.6 100 91 60- ll8 6 30

2-Chlorophenol 90.6 100 91 89.1 100 89 23- 134 2 30

2,2'-0xybis( 1-chloropropane) 84.0 tOO 84 82.2 100 82 36- 166 2 30

Chrysene 99.6 100 100 105 100 lOS 17- 168 6 30

Dibenz(a,h)anthracene 103 100 103 109 100 109 10-227 6 30

3,3'-Dichlorobenzidine 92.5 100 92 106 100 106 10-262 14 30

2,4-Dichlorophenol 93.2 100 93 97.4 100 97 39- 135 4 30

Diethyl Phthalate 112 100 112 118 100 118 • 10 . 114 5 30

Dimethyl Phthalate 103 100 103 109 100 109 10- 112 6 30

2,4-Dimethylphenol 99.1 100 99 103 100 103 32- 119 4 30

2,4-Dinitrophenol 86.0 100 86 80.3 100 80 10 - 191 7 30

2,4-Dinitrotoluene 101 100 101 115 100 I 15 39- 139 13 30

2, 6-D in itrotol uene 105 100 lOS 110 100 110 so- 158 5 30

I ,2-Diphenylhydrazine 104 100 104 105 100 105 57 - 117 < I 30

Bis(2-ethylhexyl) Phthalate I 18 100 118 120 100 120 10 - 158 2 30

Fluoranthene lOS 100 108 118 too 118 26- 137 9 30

Fluorene 95.6 100 96 99.3 100 99 59- 121 4 30

Hexachlorobenzene 103 100 103 104 100 104 10 - 152 30

Hexachlorobutadiene 74.3 100 74 73.3 100 73 24- ll6 30

Results Ra~:~:cd willa an asterisk (0 ) lnclil'ale \'Diues outside control criteriA.

Percent recoveries and ~lath-e percent d•fTcrcnccs (RPD) 1uc dctcnnined by the sofiw:uc using values m the calculation which ha\·c not been rounded.

Printed 2118/1 S 9 55 FonnlC 66023 \lalprcwsOO 1\starlirns$\l.IMSRcps\L;JbControiSamplc.rpl SuperSet Reference IS·000032127S ~vOO


QA/QC Report

Client: General Electric Company Service Request: Rl500964

Project: GE -Pittsfield NPDES Date Analyzed: 2/1 2115



Scmivolatilc Organic Compounds by GC/MS

Analytical Method: 625 Units: J.lg/L



Lab Control Sample Duplicate Lab Control Sample

RQI501387-02 RQI501387-03

Spike Spike %Rec RPD

Analyte Name Result Amount %Rcc Result Amount o/o Rcc Limits RPD Limit

Hexach lorocyclopentadiene 83.2 100 83 81.0 100 81 28-98 3 30

Hexach lorocthane 63.7 100 64 68.0 100 68 40- 113 6 30

Isophorone 97.9 100 98 103 100 103 21 - 196 5 30

4,6-Dinitro-2-methylphenol 97.0 100 97 107 100 107 to- 181 10 30

4-Chloro-3-methylphenol 105 100 105 Ill 100 Ill 22- 147 6 30

Naphthalene 72.2 100 72 75.0 100 75 21- 133 4 30

Nitrobenzene 94.8 100 95 96.2 100 96 35- 180 30

2-Nitrophenol 93.0 100 93 92.6 100 93 29- 182 <I 30

4-Nitrophenol 64.4 100 64 70.1 100 70 10- 132 9 30

N-Nitrosodimethylamine 62.5 100 62 65.4 100 65 33 -70 5 30

N-Nitrosodiphenylaminc 101 100 101 106 100 106 50- 117 5 30

Di-n-octyl Phthalate I 17 100 117 124 100 124 10- 146 5 30


Phenanthrene 103 100 103 108 100 108 54- 120 4 30

Phenol 42.9 100 43 46.6 100 47 10- 112 8 30

4-Bromophenyl Phenyl Ether 102 100 102 103 100 103 53- 127 <I 30

4-Chlorophenyl Phenyl Ether 100 100 100 105 \00 105 25- 158 5 30

N-N itrosod i·n-propylamine 91.3 100 91 95.8 100 96 10-230 5 30

Pyrene 108 100 108 112 100 112 52 - 115 3 30

I ,2,4-Trichlorobenzene 69.2 100 69 69.2 100 69 29-85 <I 30

2,4 ,6-Trichlorophenol 99.5 100 100 108 100 108 37- 144 8 30

Results flagged with an asterisk(") Indicate\ a lues outside control criteri11.

Percent recovcnes and rc:lnti\c pcrtent differences (RPD) are determined by the softw;ue using values in the calculation wh1ch hllve not been rounded

Primed 2/1811 S 9 55 ronn JC

\lalprewsOO I\starlimsS\LIMSReps\LabControiSample.rpt SuperSet Reference: 1~..0000321275 TevOO

A Enulronmental CHAIN OF CUSTODY/LABORATORY ANALYSIS REQUEST FORM 19389

I OF 1565 Jefferson Road, Building 300, Suite 360 • Rochester, NY 146231 + 1 585 288 5380 + 1 585 288 8475 (fax) PAGE I l'loject Number

. l'loject!Wne NPDES Permit ANALYSIS REQUESTED (Include Method Number and Container Preservative}

l'lojectMonog• Sean Coyle ~cc PRESERVATIVE 1 1 Canpenyr-.ov r e ·

Lt ~ltl Preservative Key

eo 1a nv1ronnement NA (GE CEP) &! 0. NONE 1. HCL

1000 East St. ~ 2. HN03

~ 3. H2S04 4. NaOH

8 5. Zn. Acetate Pittsfield MA 01201 ~

6. MeQH

'/.; ff.~ J; $I I !!J lf; 7. NaHS04 Phone I Emal ffi 413-494-6709 413-494-7052 m !/ "'!'~!Go o !J" ~· B. Other __

/-Signalln e: ~--.A ~I'MiedName ~ IJ!i. 'It ~ t:: .. rGf. tl ~ li] ~ REMARKS/ z <1 0 !Y&!fJ!tPo ~<J~~ ...5EA ,.J c?: . C:0 '7 l~ ALTERNATE DESCRIPTION

FOR OFfiCE USE I SAMPUNG CLIENT SAMPLE ID OHLYLAaiD DATE TIME 'MATRIX .

o .. u-.lU.£M·£~-uV ... - .. _ ... ·- l./9/15 10 H20 3 X I -~. ~·-"" • ~- -A.'"-:!'i -,AM

U"tU • ..L~I"o·'-"-'-"-' - ~,~,.~,.;) -. 7:9 .. M2U l X .. -. -II II-' UtCII U\

---~- !~ ...... ~, :7{ ~::J

-·~? .... H2u .) 1\ o:--.o:;<.• - --:-I'~

- ~ ---=- . -"*--------:!1

.~ ... :. ,7-r,-, -~ '

:.M~ _......,_ 'II;•..--.. ~

~Me.." .-............. .._

~- - • ... .T~- ..... ....

';"" --~ i _,. -~ 1-. ..., r .. , - . - -~.,...-.

~ ---. -~ .... -.,.. ... .... ,.....t\.J·-* ' t ' ~ .. -

SPECIAL INSTRUCTIONSICOMMENTS TURNAROUND REQUIREMENTS REPORT REQUIREMENTS INVOICE INFORMATION Metals

-- RUSH (SURCHARGES APPLY) _I. Rasulls Only

11. Results + ac &rnmal18s POl --1 day -1(-2 day ---3 day -

(t.CS, CUP, MSIMSO as requited)

PA 624 & 625 list included with COC's Samples packed in ice --· day_5day Bill TO: _ m. Results + ac anct Calibrallon

&rnmal18s REQUESTED REPORT DATE ~ rl Oa!a Validation Repcrt with Raw Oa!a

SeeOAPP D

I ~ATE WHERE SAMPLES WERE COLLECTED Edata __ Yes _No

,._, REUNOUISHED BY RECEIVED BY REUNOUISHEO BY RECEIVED BY AEUNOUISHED BY RECEIVED BY

~ --7~ 1 .. .._ l_ '-- ,..

I~A.-l Signa~- ..-lC I Siplln Siplln ~ R1500964 e. <' o ·~ c... ~ 5

Printed!Wne " ~~"" ~-~J l'llnled Noma Printed Nama Printed Name VeoU• W•ter North Amenc•

l/ 15 f'J h. Ce .Pntsfttld NPOES

Fim Fim .._, fn.-J f'lrn Fkm ~

11111111111/llllllllllllllllllllllllllllllllllllll ·;:_ /9//\ Dat&'TIII8 z: a::;_;n n"' Oa!e!rrmez l_,ls_ a1,-£ Datelline DatafTlme Pate/Tine

I

Distribution: White - lab Copy; Yellow • Return lo Ortgfoator C1 2012 by ALS Group

A Cooler Receipt and Preservation Check Form

R1500964 5 Vtolla Water North Amert~a

ljli[iiiiiUIIililiiiiiiiU II~IIIIIIIID 1111

Project/Client bf.. O. 'ii..JWJ FolderNwnber I?J~,.qtf_ -· Cooler received on _ILl_ofl.(_ by: .H~ COURIER: ALS UPS ~ VELOCITY CLIENI'

1 Were Custody seals on outside of cooler? [!)N 5a Perchlorate samples have required beadspace? y N~

2 Custody papers properly completed (ink, signed}? P'>N Sb Did VOA vials, Alk,or Sulfide have sig* bubbles? .0.

YQV~

3 Did all bottles arrive in good condition (unbroken}? P.JN 6 Where did the bottles originate? -~- CLIENT -4 Circle: W~ Dry Ice Gel packs present? P'N 7 Soil VOA received as: Bulk Encore 5035set -~

8. TemperatureReadings Date: 2-/ 1 .. 1 1 '\ Time: lu ~~ ID: IR#3~ From: Temp Blank ~e I

Observed Temp COC} tf.o Correction Factor COC} -l.D

Co~ected Temp (0 C} z..D Within 0·6°C? ('!) N y N y N y N y N y N y N



All samples held in storage location: ~ by ~'a on . at 1 ;>\'b 5035 samples placed In storage lo ation: by on at __ _

PC Sedondary Review:

c1

oole:Brweakdoalwnlb: ttlDatelab: Is 1

(' alTi~e: , I(Jy )? by: @i NO . ere o e e co p e 1.e. an ysiS, preservation, etc.

2. Did all bottle labels and tags agree with custody papers? NO 3. Were correct containers used for the tests indicated? NO 4. Air Samples: Cassettes I Tubes Intact Canisters Pressurized Tedlar® Bags Inflated E 1 ' cU ~xp1runan screpanc1es: pH Reagent Yes No Lot Received Exp SampleiD Vol. Lot Added Final

Added pH >12 NaOH S2 HNO] S2 lilS~ <4 NaHso. Residual ForCN If+, contact PM to Chlorine Phenol add Na1SlOJ (CN), (-) and 522 ascorbic (phenol).

Na2S20l . -ZnAcetate . - **Not to be tested before analysis -pH tested and HCl •• ** recorded by VOAs on a separate worksheet

Yes= All samples OK

NcrSamples were preserved at The lab as listed

PMOKto Adjust:

Bottle lot numbers:'---Lr'..Jc.?!!!..:l.!i.a.it'i.:;-a.210e:!.1+-....J.":J.ot:k>IU{,.oi~'L/.z.;W~t.u:~u.V~---------------------Other Comments: "'

tl.

PC Secondary Review:----.~~-·:\....-_· __

P:\INTRANE'I\QAQC\Porms Conttolled\Cooler Receipt 17.doe

*significant air bubbles: VOA >5-6 mm : WC > 1 in. diameter ee e2s

S/6/14

PERMITTEE NAME/ADDRESS (Include Facility Name/location if Different)

NAME: GENERAL ELECTRIC PITISFIELD

ADDRESS: 159 PLASTICS AVE PITISFIELD, MA 01201




NA IIUNAL 1-'ULLU IAN I Ulb\.,HJ.\Hut: t:LIMINAIIUN bYb I t:M \Nt-'Ut::J)

DISCHARGE MONITORING REPORT (DMR}

I MA0003891 II 064T -A I PERMIT NUMBER DiSCHARGE NUMBER

MONITORING PERIOD

MM/ODNYYY I MM/ODNYYY

02/01/2015 02/28/2015

QUANTITY OR LOADING QUALITY OR CONCENTRATION PARAMETER VALUE VALUE UNITS VALUE

pH SAMPLE ...... - -MEASUREMENT ..., . ~s

00400 IMO PERMIT - - - 6 .5 Internal Monitoring Point REQUIREMENT MINIMUM Solids, total suspended SAMPLE

MEASUREMENT 0 0 lbr/ o1 0

00530 IM 0 PERMIT Req. Mon. Req. Mon. lb/d Req. Mon. Internal Monitoring Point REQUIREMENT MOAVG DAILYMX MOAVG Oil &Grease SAMPLE -MEASUREMENT 0 0 lh s { ol 00556 IMO PERMIT Req. Mon. Req. Mon. lb/d ****** Internal Monitoring Point REQUIREMENT MOAVG DAILYMX

Polychlorinated biphenyls [PCBsl SAMPLE MEASUREMENT 0 .000003 0-000001 Uu I cJ o .o.rzgo

39516IM 0 PERMIT Req. Mon. Req. Mon. lb/d Req. Mon. Internal Monitoring Point REQUIREMENT MOAVG DAILYMX MOAVG Flow, in conduit or thru treatment SAMPLE -plant MEASUREMENT o .oo3~ CJ . OOJ<g M~~

50050 IM 0 PERMIT Req. Mon. Req.Mon .. MGD -Internal Moniloring Point REQUIREMENT MOAVG DAILYMX

Flow, total SAMPLE ****** MEASUREMENT 0. 00 'if 'Z.. o.oo8~ ,...,&-0

82220 IMO PERMIT Req. Mon. Req. Mon. MGD -liltl:)rnal Monitoring Point REQUIREMENT MOAVG DAILYMX

NAME/TITLE PRINCIPAL EXECUTIVE OFFICER l~lnlorpondyolbwlllatlhlodoc:umonlondal-..-swo<w~lnlot..,d-O< .._wton O.~wilh • ..,...., dnlgnod to-.lllatquOlillod po.-~ .-r 01101

tho ntOITIIII!ion -od. Baed ... my oqur, otlho- .. --..._tho

Exec. Mgr, Env. Remediation syslom .................. dif.aly.......,.. lotvotherWig lho ... -.lho--od io. tolho beSC ot my ldlawlodgo ond -~. 111>0, -··-~-1-...,. 11\atlhote are olgnificant .....-.tor .. ~m~~o.g false --.lrd.ldng ... ~ ot 11no-~roo ~~n<r~mg .-..

TYPED OR PRINTED ~~~~

COMMENTS AND EXPLANATION OF ANY VIOLATIONS (Reference all attachments hare)

FLOW TOTAL SEE FOOTNOTE 4.

EPA Form 3320.1 (Rav.01/06) Previous adlllona may be used.

VALUE VALUE - 1 .30 - 9 MAXIMUM --

0

****** Req. Mon. DAILYMX

****** 0 - 15

DAILYMX -0 . IOSi&J

****** Req. Mon. DAILYMX - -

- -****** ******

- ******

.-orm 1\pproveo

OMB No. 2040-0004


MAJOR

(SUBR W)

INTERNAL TO 005

Internal Outfall

No DischargeD



su 0 'Z-/1'-to 6-.A-AI3


""51~ 0 7.-fMo GOMjP'l.Li

mg/L I

Twice per COMP24 Month

t'l1 c, '._ 0 -z.(I'W;J t..-.A-Iar3

rng/L Twice per GRAB Month

I..A 'J I'- 0 'l..IIY\o ~O,...JO"l.'-1

ug/L Twice per COMP24 Month -

0 (.Ni!>~/(.l..'7 E r"L•!'-<A - Weekly ESTIMA

****** 0 Z.lfLfo t:rr7-MA - Weekly ESTIMA

TELEPHONE DATE

AREA~

12/15/2014 Page 1

Attachment E- Outfaii64T

Date pH TSS FN Oil & Grease FN MG/l MG/l

02/01/15 02/02/15 02/03/15 02/04/15 02/05/15 02/06/15 02/07/15 7.25 U1.00 1,C U4.10 1,G 02/08/15 02/09/15 02/10/15 02/11/15 02/12/15 7.30 U4.00 1,G 02/13/15 U1.00 1,C 02/14/15 02/15/15 02/16/15 02/17/15 02/18/15 02/19/15 02/20/15 02/21/15 02/22/15 02/23/15 02/24/15 02/25/15 02/26/15 02/27/15 02/28/15

FN 1 - (U) Indicates compound analyzed for but not detected C - Composite sample G - Grab sample

PCB FN Estimated Metered Rain/Precip Raln/Precip UG/l Flow- MGD Flow- MGD Total-In Peak -In

(50050 IM O) (82220 IM 0) 0.0029 0.00 0.00

0.20 0.07 0.16 0.02 0.00 0.00 0.15 0.04 0.09 0.05

0.1056 c 0.0076 0.08 0.08 0.0007 0.06 0.02

0.19 0.05 0.07 0.01 0.00 0.00 0.08 0.06

0.0208 c 0.0088 0.04 0.02 0.00 0.00

0.0058 0.13 0.02 0.00 0.00 0.00 0.00 0.00 0.00 O.Q1 0.01 0.52 0.08 0.36 0.11

0.0043 0.08 0.02 0.03 0.02 0.52 0.14 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

-·

PERMITIEE NAME/ADDRESS (Include Facility Name.1.ocation if Different}

NAME: GENERAL ELECTRIC PITISFIELD ADDRESS: 159 PLASTICS AVE

PITISFIELD, MA 01201



ATIN: Andrew T. Sitfer, Exec Mgr. En

NAIIUNAL 1-'ULLU IAN I Ul:>l.HAHbc cLIMINAIIUN :>T::JI eM \NI"'Uc::.J


MA0003891 005-A ~-- ---1 PERMIT NUMBER I DISCHARGE NUMBER I

MONITORING PERIOD

MM/DDNYYY I MMIDDNYYY

02/01/2015 02/28/2015


pH SAMPLE ****** - - ****** MEASUREMENT ....., , , t 1 . 8'~

004001 0 PERMIT ****** ****** ****** 6.5 ****** 9 Effluent Gross REQUIREMENT MINIMUM MAXIMUM Solids, total suspended SAMPLE ******

MEASUREMENT 0 0 lhs/ d 0 0 005301 0 PERMIT 188 270 Ibid Req. Mon. ****** Req.Mon. Effluent Gross REQUIREMENT MOAVG DAILYMX MOAVG DAILYMX 011 & Grease SAMPLE ****** ****** ******

MEASUREMENT c. "=' ~ llu /d L-4.50

005561 0 PERMIT - 135 Ibid ****** ****** 15 Effluent Gross REQUIREMENT DAILYMX DAILYMX Polychlorinated biphenyls (PCBs] SAMPLE

I

****** MEASUREMENT 0 0 lh sf of 0 0

395161 0 PERMIT .01 .03 Ibid Req. Mon. ****** Req. Mon. Effluent Gross REQUIREMENT MOAVG DAILYMX MOAVG DAILYMX Rainfall SAMPLE ****** ****** ******

MEASUREMENT o .zo o . z.o lA/

465291 0 PERMIT I Req. Mon. Req. Mon. in ****** ****** ****** Effluent Gross REQUIREMENT MOAVG DAILYMX Flow, in conduit or thru treatment SAMPLE ****** ****** ****** plant MEASUREMENT 0,1"30'1 o . 11..90 r.-,L,D

500501 0 PERMIT Req.Mon. Req. Mon. MGD ****** ****** ****** Effluent Gross REQUIREMENT MOAVG DAILYMX Flow, total SAMPLE ****** ****** ******

MEASUREMENT 0.1-zg~ O,I'Z.~Z... f\,o(sf)

82220 1 0 PERMIT Req. Mon. Req. Mon. MGD ****** ****** ****** Effluent Gross REQUIREMENT MOAVG DAILYMX

l~underponalyallawlhallfl!o-onddllllaclwnenb_n_oduncler mydirodlonor

I bhiiUSUG,. _ IIUIPJ. PP lu::=:.~=::e~:'~de=.:.r--=-:~~..!o~rlrld NAME/TITLE PRINCIPAl. EXECUTIVE OFFICER

r-utm ~ppruvea

OMB No. 2040-0004


MAJOR

(SUBRW)

OUTFALL005

External Outfall No DischargeD

NO. FREQUENCY SAMPLE UNITS EX OF ANALYSIS TYPE

5u 0 ~I IVJO 61\.~fJ

su Twice per GRAB ' '

Month

,...., ~ ,._ 0 7,/ J\o<O .:_a,..~ Z"' mg/L Twice per COMP24

Month

"""'4._. 0 -z./Mo b~A1'3


~~ I'- 0 ZIMo "',.._,p7.}1 ugtl Twice per COMP24

Month

****** 0 (!Oi»T"' tz.c:o ... D-..


**"*** 0 t!.O,.., ~C.O,._f>-.-- Continuous Record !

(manual) 1 - I

CJ co.-...r !Z-C..O"-C"-

****** Continuous Record '

(manual) •

TELEPHONE DATE

Exec. Mgr, Env. Remediation sya.n, or IIOH po ...... dirocdy nljJOJ1SI>Io lorgalhotmQ lho i\-. lho lllolmalion llllmill«! b. tohbnto1 my knowlldge8Jid~t.trw.~•.R~w. •.-n ... ,.'*lhtt..,•~l V ..- -'4,.,..... # • < ( <rt1<Yv - 1 pendln lor .,~ laiM i\._. ~ ltlo poo.-y ol 1no ond mprioawnon1 1ot lln-"".1

I TYPED OR PRINTED I-..·

COMMENTS AND EXPLANATION OFANYVIOLATlONS (Reference all attachments here)

SEE PAGE 4 OF PERMIT, FLOW TOTAL SEE FOOTNOTE 4.

EPA Fonn 3320.1 (Rev.01106) Previous editions may be used.

AREACOcl4o

12/15/2014 Page 1

Attachment E - Outfall 005

TSS FN Oil &Grease FN PCB Date pH MG/L MG/L UG/L

02/01!15

02/02/15 7.71 U1.00 1,C U4.10 1,G 0.0000

02/03/15

02/04/15

02/05/15 02/06/15

02/07/15

02/08/15

02/09/15 7.84 U1.00 1,C 4.50 G 0.0079

02/10/15

02/11/15

02/12/15

02/13/15

02/14/15

02/15/15

02/16/15

02/17/15

02/18/15

02/19/15

02/20/15 02/21/15 02/22/15

02/23/15

02/24/15

02/25/15

02/26/15

02/27/15

02/28/15

FN 1 • (U) Indicates compound analyzed for but not detected

C · Composite sample G - Grab sample

FN Metered Aooded Raln/Preclp Raln/Precip I Flow-MGD Condition Total-In Peak -In

0.1230 NO 0.00 0.00

c 0.1292 NO 0.20 0.07 0.1162 NO 0.16 0.02 0.1143 NO 0.00 0.00 0.1220 NO 0.15 0.04

0.1210 NO 0.09 0.05

0.1167 NO 0.08 0.08

0.1302 NO 0.06 0.02 c 0.1284 NO 0.19 0.05

0.1423 NO 0.07 0.01 0.1229 NO 0.00 0.00 0.1183 NO 0.08 0.06 0.1257 NO 0.04 0.02 0.1070 NO 0.00 0.00

0.1301 NO 0.13 0.02 0.1305 NO 0.00 0.00

0.1300 NO 0.00 0.00

0.1257 NO 0.00 0.00

0.1397 NO O.Q1 0.01

0.1116 NO 0.52 0.08

0.1426 NO 0.36 0.11 0.1504 NO 0.08 0.02 0.1690 NO 0.03 0.02 0.1493 NO 0.52 0.14 0.1225 NO 0.00 0.00 0.1535 NO 0.00 0.00 0.1589 NO 0.00 0.00

0.1350 NO 0.00 0.00

PERMITIEE NAME/ADDRESS (Include Facility Name/Location if Different}



FACIUTY: GENERAL ELECTRIC COMPANY LOCATION: 159 PLASTICS AVE



NAIIUNAL t'ULLU IAN I UI::,\.,HAHb~ ~LIMINAIIUN ::,y::,I~M \Nt'U~::,I


I MA0003891 II W005·A I PERMIT NUMBER DISCHARGE NUMBER

-------- - --- ---

MONITORING PERIOD

MMIDD/YVYV I I MMIDDIYYYY

02/01/2015 I I 02/28/2015


r-um1 ,.ppruvea

OMS No. 2040.()()()4


MAJOR (SUBRW)

OUTFALL 005 WET WEATHER

External Outfall No DischargeD


pH SAMPLE MEASUREMENT - - - Goor( qV - 10Dr(qf) I

004001 0 PERMIT - - - 6.5 - 9 su Quarterly GRAB I Effluent Gross REQUIREMENT MINIMUM MAXIMUM I Solids, total suspended SAMPLE

MEASUREMENT ~ 0o•(9J) c;op,(q]) 00530 1 0 PERMIT Req. Mon. Req. Mon. Ibid Req. Mon. Effluent Gross REQUIREMENT MOAVG DAILYMX MOAVG 0 11 & Grease SAMPLE - ....... ****** ******

MEASUREMENT

00556 1 0 PERMIT ....... ....... ....... ....... Effluent Gross REQUIREMENT

Polychlorinated biphenyls (PCBs) SAMPLE MEASUREMENT c0·(0 (£"oo, ( q J) ~~(~£>

395161 0 PERMIT Req. Mon. Req. Mon. lb/d Req. Mon. Effluent Gross REQUIREMENT MOAVG DAILVMX MOAVG Rainfall SAMPLE IGoD, <ry ~Ol('lj) ******

MEASUREMENT

465291 0 PERMIT Req. Mon. Req. Mon. In ****** Effluent Gross REQUIREMENT MOAVG DAILYMX Flow, total SAMPLE leo•('~V IGor:. (<jv ******

MEASUREMENT

82220 1 0 PERMIT Req. Mon. Req. Mon. MGD -Effluent Gross REQUIREMENT MOAVG DAILYMX

NAME/TITLE PRINCIPAL EXECUTIVE OFFICER I cenll't ..... r ponu, ol lo•lhallhis ............ andaiOII8Chmonls-re _...under my........,"' .............,In accordance - • ay&lom do signed to_. 11ot qualiflod ponome4 property gdlor-lho "*>nnotion ..-od. !!aMd on my lnquOy of.,. poBon"' P"'"""" wl>o,.,.. 1l1e

Exec. Mgr, Env. Remediation '"*"· or_po....,. ~,._.-l"'galhomg fle n-. .,. n-. ..-odls, IOiho-olmy~and-.lrue.ococ:uro!a, -ccmplelo. l.,_.,.lhallhafa••llgnilic:8nl

ponallu foltllbmillilg Ieise illoi!Miion. ncllcr"'l ... poosibilly of lint - ~ too knowi'lg -... TYPED OR PAINTED

COMMENTS AND EXPLANATION OF ANY VIOLATIONS (Reference all aHachments here)

SEE PAGE 5 OF PERMIT. FLOW TOTAL SEE FOOTNOTE 4.

EPA Form 3320.1 (Rev.01/D6) Previous editions may be used.

....... 1000o ( '}_V - Req.Mon. mgll. Three per COMPOS

DAILYMX Quarter

****** ~(qy ....... 15 mg/L Quarterly GRAB

DAILVMX

****** 0_oor ('>Y ....... Req. Mon. ug/L Three per COMPOS

DAILYMX Quarter ****** ****** ....... ****** ....... ....... Continuous Recorder

(auto) ****** ....... ....... ....... - ****** Continuous Recorder

(auto)

TELEPHONE DATE

(413)448-5902

AREA C..

12/15/2014 Page 1

PERMITIEE NAME/ADDRESS (Include Facility Name/local/on if Differenl)






NAI IUNAL I"ULLU IAN I Ul::>l.HAHut I:LIMINPd IUN ::>Y::> II:M (NI"Ut:::>J


I MA0003891 II DOSA-A I PERMIT NUMBER DISCHARGE NUMBER

MONITORING PERIOD

MMIOD/YYYY I MMIOD/YYYY

02/01/2015 02/28/2015


pH SAMPLE MEASUREMENT - - - -

00400YO PERMIT - - - 6.5 - 9 Effluent Gross (Supplementary} REQUIREMENT MINIMUM MAXIMUM Solids, total suspended SAMPLE

MEASUREMENT -00530Y 0 PERMIT Req. Mon. Req.Mon. lb/d Req. Mon. - Req. Mon. Effluent Gross (Supplementary) REQUIREMENT MOAVG DAILYMX MOAVG DAILYMX Oil& Grease SAMPLE ****** ******

MEASUREMENT

005561 0 PERMIT Req. Mon. Req. Mon. lb/d - - 15 Effluent Gross REQUIREMENT MOAVG DAILYMX DAILYMX Polychlorinated biphenyls (PCBs] SAMPLE

MEASUREMENT -39516 y 0 PERMIT Req. Mon. Req. Mon. lb/d Req. Mon. ****** Req. Mon. Effluent Gross (Supplementary) REQUIREMENT MOAVG DAILYMX MOAVG DAILYMX Flow, total SAMPLE ****** ****** ******

MEASUREMENT

822201 0 PERMIT Req. Mon. Req. Mon. MGD ****** "'***** -Effluent Gross REQUIREMENT MOAVG DAILYMX ------

NAME/TITLE PRINCIPAL EXECUTIVE OFFICER I corlify ..mr ponaly ollowthollhio ~ ORI al-....... '""'pr-od ..-my d-or oupoMI!onln llllCIO<IIonco will o oyst., dellgnod to ........... ~ ponomol propor!r v-f>or..,

lho--od.BosedCOirnylr'quiryollhoPifiUIOI.,.......who-lho

Exec. Mgr, Env. Remediation llyslorn.or.,...ptrsonsdndt,....,.,- lo<galhomglholnlocmalion,lho--11. lo hi best of my knowlldgeand betlf, trul, accurate, and amplele. I., iNBNth&l:lhef• ... ~ ponolln tot .,-.g !aile lnfomallon, lnc:llcmg lho pouil>illy ol h .., imprll<lrmerd 1otllncrwW>g --TYPED OR PRINTED

COMMENTS AND EXPLANATION OF ANY VIOLATIONS (Reference all attachments here)

TOTAL FLOW SEE FOOTNOTE 4. Na 01 sctJAf!.~

EPA Form 3320-1 (Rev.D1/06) Prevloua edlllona may be used.

r-unn o'\ppruvea

OMB No 2040-Q004


MAJOR

(SUBRW)

DRYWEATHER 05A

Internal Outfall No Discharge~

NO. FREQUENCY SAMPLE I



mg/L Twice per COMP24 Month



******

- Weekly ESTIMA

TELEPHONE DATE

AREA~

-

12/15/2014 Page 1

Attachment E - Outfall 05A Dry

Date pH TSS FN Oil & Grease FN PCB MG/L MG/L UG/L

02/01/15

02/02/15

02/03/15 02/04/15

02/05/15 02/06/15

02/07/15

02/08/15

02/09/15

02/10/15

02/11/15

02/12/15 02/13/15

02/14/15

02/15/15

02/16/15

02/17/15

02/18/15

02/19/15

02/20/15

02/21115 02/22/15 02/23/15

02/24/15

02/25/15

02/26/15

02/27/15

02/28/15

FN 1 - (U) Indicates compound analyzed for but not detected C -Composite sample

G - Grab sample

FN Estimated Rain/Precip Rain/Precip Flooded Flow- MGD Total-In Peak -In Condition (82220 1 0)

0.00 0.00 NO

0.20 0.07 NO

0.16 0.02 NO 0.00 0.00 NO 0.15 0.04 NO

0.09 0.05 NO

0.08 0.08 NO

0.06 0.02 NO

0.19 0.05 NO

0.07 0.01 NO

0.00 0.00 NO 0.08 0.06 NO 0.04 0.02 NO

0.00 0.00 NO

0.13 0.02 NO

0.00 0.00 NO

0.00 0.00 NO

0.00 0.00 NO

0.01 0.01 NO 0.52 0.08 NO 0.36 0.11 NO 0.08 0.02 NO

0.03 0.02 NO

0.52 0.14 NO

0.00 0.00 NO

0.00 0.00 NO

0.00 0.00 NO

0.00 0.00 NO

----

PERMITIEE NAME/ADDRESS (Include Facility NlllfKIA..ocation if Different)





ATIN: AndrewT. Silfer, Exec Mgr. En

NAIIUNAL 1-'ULLUIANI Ul::,l,;MAHut I:LIMINAIIUN ::,y::, 11:M lNI"UI:::,)


I MA0003891 II W05A-A I PERMIT NUMBER DiscHARGE NUMBER

MONITORING PERIOD

MMIDD!YYYY I MMIDD!YYYY

Q2/01/2015 02/281201 5

r-urrn 11ppruveo

OMB No 2040.()004


MAJOR (SUBR W)

OUTFALL 05A WET WEATHER External Outfall

No DischargeD

I

QUANTITY OR LOADING QUAUTY OR CONCENTRATION NO. FREQUENCY SAMPLE PARAMETER VALUE VALUE UNITS VALUE VALUE VALUE UNITS EX OF ANALYSIS TYPE

pH SAMPLE - - - 0o·(~V - GoD•<9V MEASUREMENT

004001 0 PERMIT ****** I ****** ****** 6.5 ****** 9 su Quarterly GRAB Effluent Gross REQUIREMENT MINIMUM MAXIMUM Solids, total suspended SAMPLE

~DI('ly c;i_o, ( q) 0_o•{1V - IGoo,{V MEASUREMENT

005301 0 PERMIT Req.Mon. Req. Mon. lb/d Req. Mon. - Req. Mon. mg/L Three per COMPOS Effluent Gross REQUIREMENT MOAVG DAILYMX MOAVG DAILYMX Quarter Oil &Grease SAMPLE c;t>()l ( 9)) ~OI{~u ****** ******

!(..ao•(?) MEASUREMENT

005561 0 PERMIT Req. Mon. Req. Mon. lb/d ****** ****** 15 mg/L Quarterly GRAB Effluent Gross REQUIREMENT MOAVG DAILYMX DAILYMX Polychlorinaled biphenyls [PCBs] SAMPLE CNODt( ?}) ~ooroj) I( NOD•( 0 - ~o·cvv MEASUREMENT i 3951610 PERMIT Req. Mon. Req. Mon. lb/d Req. Mon. - Req.Mon. ug/L Three per COMPOS .. Effluent Gross REQUIREMENT MOAVG DAILYMX MOAVG DAILYMX Quarter Rainfall SAMPLE

~('1i) c:Foo,(9V ****** - ****** ****** MEASUREMENT

465291 0 PERMIT Req. Mon. Req. Mon. in ****** ****** ****** ****** Dally when Effluent Gross REQUIREMENT MOAVG DAILYMX Discharging Flow, in conduit or thru treatment SAMPLE - ****** ****** ****** plant MEASUREMENT o . 001 z_ o.ooz 3 ""'~ , 0 f!,O,...J~

500501 0 PERMIT Req. Mon. Req. Mon. MGD ****** ****** ****** - Continuous Effluent Gross REQUIREMENT MOAVG DAILYMX Number of Events SAMPLE ****** - - ****** - , ...... '1

MEASUREMENT -z. ~ 0 ""'H'f~

t) IS"CMIV-'-t""""-

514841 0 PERMIT Req. Mon. ****** fl - ****** - ****** Dally when Effluent Gross REQUIREMENT TOTAL ~ Disch~rgif!g -- > --

'I '*"Y ontor penally o! laowlhal lhol doalrnonl anclal.aac:lmonts _,. -od ..-my dirodiiOI or I ~~In ll<lCCIIIanc:e -· oys~ .. dnignod lo ....... lhal,.-...,_. prope!ly galher ond AtLdlt!W Y. ] ]Iff!; . •r•;~ lhe Wormalion ~ed. ~ Cl'l"" itquiry ot lhe person or pen.ant who manage ...

TELEPHONE NAME/TITLE PRINCIPAL EXECUTIVE OFFICER

oysWn. or lhooe P""""•direc:IIV IHpOtlllblolorgolhtmv 11oln-. 11olnlotmollon wtmlloclls, lothebeltolmy~andbellf..UUI, .ante, andcompllte.l.-n...,.1hatlhet'eate~J 1 < .....- -gs,.:y ·- G'C'~..Gzf<-... I pona1iH rouu-.g taM lnlornUon, ilclldng 11o poaillflry olen._. inpllomlltlllor mowng · - · - - ·· · · · · · · · Exec. Mgr, Env. Remediation

l TYPED OR PRINTED 1-.s



EPA Form 3320-1 (Rev.D1106) Previous edlllons may be used.

AAEJ\Codo

12/15/2014

I

II

TOTALZ ~ '

ru.o~- 11 Recorder

(auto)

VISUAl_

VISUAL

-DATE

Page 1

PERMITTEE NAME/ADDRESS (Include Facility Name/location if Different)






NA IIUNAL 1-'ULLU IAN I Ul::>l..MAMbt t:UMINAIIUN ::.Y::> I t:M (NI-'Ut:::.}


MA0003891 W05A·A ~~-PERMit NUMBER lscAAAGE NUMBER I MONITORING PERIOD

MMIDDIVYYY I MMIDDIVYYY

02101/2015 02/28/2015


Flow, total SAMPLE Goo.<~V ICN~Dr(9V MEASUREMENT

822201 0 PERMIT Req. Mon. Req. Mon. MGD Effluent Gross REQUIREMENT MOAVG DAILYMX

NAME/TITLE PRINCIPAL EXECUTIVE OFFICER I cer1ify...._r polldy of law lhallhio doc:umonl ond ol lllllrdmonls wor. propatod .....,...,. dofodlo<\01 supoiYillonln~we. • rplomdollgnod lo.....,. llal qu.w..d-"'"' propooly ijdort..,

t--~mrir.-r'I'~Miorr.-'l!t'-----------lfwrlloo~,.,.lnlonnalion llbnllod. Baod on my lnquilyol.,. ,.._., 01 ""'*"" rr~~o....._lh•

--

VALUE VALUE - -- -

r-urm 1'\ppruvea

OMB No. 2040.0004


MAJOR

(SUBRW)

OUTFALL 05A WET WEATHER

External Outfall

No DischargeD



-- Continuous Recorder

(auto)

TELEPHONE OAT&:

I SysiOm, Of ..... P""""l d"n<oly rnponoiblo lotgdleMg ..... - ...... _ -od It, Exec. Mgr, Env. Remediiltlon ,. ,.,.bntolmy"'--odgoond-1.1rvo,-•.n ....... ,.. ,.,,. ... ,.lhal...,..,.~l ~ · '<V' Y ' · c H.«Y - 1

paldin lot sulmilmg 1olselnlotmolion, lnWdftg lho poooibilly ol•ond ~lor lnoomg

~--------.TY~P~ED~O~R~P=R=I~N=TE=o~-------i'~-



EPA Form 3320-1 (Rev.01106) Previous editions may be used.

AREA~

12/15/2014 Page 2

Attachment E - Outfall 05A Wet

TSS FN 011 & Grease FN PCB

Date pH MG/L MG/L UG/L

02/01/15 02/02/15 02/03/15

02/04/15

02/05/15

02/06/15

02/07/15

02/08/15

02/09/15

02/10/15 02/11/15

02/12/15

02/13/15

02/14/15

02/15/15 02/16/15

02/17/15

02/18/15

02/19/15

02/20/15

02/21/15

02/22/15

02/23/15

02/24/15

02/25/15

02/26/15

02/27/15 02/28/15

FN 1 - (U) Indicates compound analyzed for but not detected

C - Composite sample

G - Grab sample

FN Metered Flooded RalnJPreclp Raln/Preclp

Flow-MGD Condition Total-In Peak -In

NO 0.00 0.00 NO 0.20 0.07

NO 0.16 0.02

NO 0.00 0.00 0.0023 NO 0.15 0.04

NO 0.09 0.05 NO 0.08 0.08 NO 0.06 0.02 NO 0.19 0.05

NO 0.07 0.01

0.0001 NO 0.00 0.00

NO 0.08 0.06

NO 0.04 0.02

NO 0.00 0.00

NO 0.13 0.02 NO 0.00 0.00

NO 0.00 0.00 NO 0.00 0.00 NO 0.01 0.01

NO 0.52 0.08 NO 0.36 0.11

NO 0.08 0.02

NO 0.03 0.02

NO 0.52 0.14

NO 0.00 0.00

NO 0.00 0.00

NO 0.00 0.00

NO 0.00 0.00

PERMITTEE NAME/ADDRESS (Include Facility Name/Location if Different)





ATIN: Andrew T. Silfer, Exec Mgr. En

NAIIUNAL t'ULLUIANI UI;,LHAHl.lt: t:.LIMINAIIUN ;::,y::;lt:M (Nt'Ut:;::,j


I MA0003891 II W05B·A I PERMIT NUMBER DISCHARGE NUMBER

MONITORING PERIOD MM!DD/YYYY I I MM/DD/YYYY

02/01/2015 I 02/28/2015


pH SAMPLE - - -MEASUREMENT

004001 0 PERMIT ****** - - 6.5 Effluent Gross REQUIREMENT MINIMUM Solids, total suspended SAMPLE - - -MEASUREMENT

00530 1 0 PERMIT ****** ****** ****** Req. Mon. Effluent Gross REQUIREMENT MOAVG 011 &Grease SAMPLE - ****** ****** ******

MEASUREMENT

005561 0 PERMIT ****** ****** ****** ****** Effluent Gross REQUIREMENT

Polychlorinated biphenyls [PCBs) SAMPLE ****** - ****** MEASUREMENT

395161 0 PERMIT ****** ****** - Req. Mon. Effluent Gross REQUIREMENT MOAVG Rainfall SAMPLE ******

MEASUREMENT

465291 0 PERMIT Req. Mon. Req. Mon. in ****** Effluent Gross REQUIREMENT MOAVG DAILYMX Flow, In conduit or thru treatment SAMPLE ****** plant MEASUREMENT

500501 0 PERMIT Req. Mon. Req. Mon. MGD ****** Effluent Gross REQUIREMENT MOAVG DAILYMX Number of Events SAMPLE ****** ******

MEASUREMENT

514841 0 PERMIT Req. Mon. ****** i# ****** Effluent Gross REQUIREMENT TOTAL

NAME/TITLE PRINCIPAL. EXECUTIVE OFFICER I cerury Lnlor ponoly olllwlhol lhs- and ••---,. proporocla.- my dir- ar super-. In II<Zlllnlance- • .,....., doo9>odlo ...... o lhol cpJOiillod porsonnol propet1y golhor-

I Atli11PW T~ -~•lfss& _liP I• -w. IMI'lfonnltiDniUtn\lted. BaMdonmynpyotlhepenonorperaonswhonwwge lhe

VALUE VALUE -- 9

MAXIMUM -- Req. Mon.

DAILYMX ******

****** 15 DAILYMX

******

****** Req. Mon. DAILYMX

****** ******

- -- ******

- ******

****** ******

****** ****** ----

r-orm Approveo

OMB No. 2040.()004


MAJOR (SUBRW)

OUTFALL 058 WET WEATHER External Outfall

No Discharge~



su Quarterly GRAB

' mg/L Quarterly COMPOSj

I i

mg/L Quarterly GRAB

I ug/L Quarterly COMPOS

******

- Dallywhan TOTALZ Discharging

******


******

- Dally when VISUAL Discharging

TELEPHONE DATE

..,..... . .,-f'O....,•c~Hdfyoo_,-ror;olhomgt>oln-.t>olnrormolion-il. ...- •• ~ lo lhe best ar mr knowledge and bellt, ttue.lalnie, Wid con'lp6N. I.wn_,. thal1hefe are~ I b < Z1Ce' ?id,MF v I pono1iH ror tu"'"""'9 loiH lnlannollon,lncbmg 11o J101111*Y o11no.., ~ ror ..,~ · · · - ·

Exec. Mgr, Env. Remediation

l TYPED OR PRINTED 1..-.s.



EPA Fonn 3320.1 (Rev.01106) Prevlou1 editions may be used.

tva o,sc..tJAFl..~

AAEA~

12/15/2014 Page 1

PERMITIEE NAME/ADDRESS (Include Facility Name/Location if Different)






NAIIUNAL t""ULLU IAN I Ul::>l,;HAHut t:LIMINAIIUN ::>Y::>I t:M (Nt""Ut:::>J


I MA0003891 II W05B·A I PERMIT NUMBER DiscHARGE NUMBER

MONITORING PERIOD

MM!DD!YYYY I I MM/DD!YYYY

Q2J01 /201 5 J L 02/2812015


Flow, total SAMPLE MEASUREMENT - *****"' ******

822201 0 PERMIT Req. Mon. Req. Mon. MGD - ****** *****"' Effluent Gross REQUIREMENT MOAVG DAILYMX . -·

NAME/TITl.E PRINCIPAL EXECUTIVE OFFICER I 1 . .,.....,unde. ponolly ot .... -lhil--.. -.... ..... _ .. p-od..-...,-..... IUpOI\'illon In 8llCIIIdonoo - o 1plom del9>od lo ......., 11\o! quallliod penomoi.--"Y golhor..... m I! " 'f- ~iJhs & . , ,.. ......... the ~ ltDnllld. BaMd on ""' nquary ot .,. person Of penon~ who rnlft808 h

r-urm 1\ppruvea

OMB No. 2040-0004


MAJOR

(SUBR W)

OUTFALL 058 WET WEATHER External Outfall

No Discharge rn


******


TELEPHONE DATE

Exec. Mgr, Env. Remediation lptem,OIIIOU po1>GIIIdireci'I~IOI!IIIhomgllolnlonnollon,llolnlonnolion-odls. r , , _

lolho-ol"'''~--l. lnle , -o.-complole. I..,IIWOntlhol_o.,...,_l V ..,.....,... • !&44/l/ 1(413)448·5902 .,.,_"" .. ~m~~ng- -.lrd.ldlng ... poo-.y olllne-in~ for g,ow~ng

I TYPED OR PRINTED 1.-s.



EPA Form 3320-1 (Rev.01/D6) Previous editions may be used.

AREACodo

NO OI:YC..tU:..I'--<.r-C

12/15/2014 Page 2

Attachment E • Outfall OSB Wet

TSS FN Oil & Grease FN PCB Dale pH MG/L MG/L UG/L

02!01/15 02/02/15 02/03/15 02/04/15 02/05/15 02!06/15 02/07/15 02/08/15 02/09/15 02/10/15 02/11/15 02/12/15 02/13/15 02/14/15 02/15/15

02/16/15 02/17/15 02/18/15 02/19/15 02/20/15 02/21/15 02/22/15 02/23/15 02/24/15 02/25/15 02/26/15 02/27/15 02/28/15

FN 1 • (U) Indicates compound analyzed for but not detected C • Composite sample G - Grab sample

FN Metered Rain/Precip Raln/Preclp Flow· MGD Total-In Peak ·In

0.00 0.00 0.20 0.07 0.16 0.02 0.00 0.00 0.15 0.04 0.09 0.05 0.08 0.08 0.06 0.02 0.19 0.05 0.07 0.01 0.00 0.00 0.08 0.06 0.04 0.02 0.00 0.00 0.13 0.02 0.00 0.00 0.00 0.00 0.00 0.00 0.01 0,01

0.52 0.08 0.36 0.11 0.08 0.02 0.03 0.02 0.52 0.14 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00

- -··

PERMITTEE NAME/ADDRESS (Include Facl.lify NamB/l.ocation if Different)





ATTN: AndrewT. Silfer, Exec Mgr. En

NAIIUNAL t""ULLU I AN I Ul::ivHAHI;;t: t:LIMINA IIUN :;y:; I t:M INt""Ut::;)


I MA0003891 ~ I 0006-A

I I PERMIT NUMBER DISCRARGE t;I(Jga~i!l

MONITORING PERIOD I

MMIOD!YYYY I I MMIDD/YYYY

02/01/2015 I 02/28/2015


pH SAMPLE - - - -MEASUREMENT (,. . ~ i.' -r . ', 004001 0 PERMIT - - - 6.5 - 9 Effluent Gross REQUIREMENT MINIMUM MAXIMUM Solids, total suspended SAMPLE .........

MEASUREMENT o.oz. o.oz. lloS"I ~ ~.30 '?.'-10

005301 0 PERMIT Req. Mon. Req. Mon. lb/d Req. Mon. - Req. Mon. Effluent Gross REQUIREMENT MOAVG DAILYMX MOAVG DAILYMX Oil &Grease SAMPLE - - ****** - -MEASUREMENT 0

005561 0 PERMIT - - ****** - - 15 Effluent Gross REQUIREMENT DAILYMX Polychlorinated b iphenyls IPCBs] SAMPLE ******

MEASUREMENT 0 0 1 b,-/ d 0 0 39516 1 0 PERMIT Req. Mon. Req. Mon. lb/d Req. Mon. - Req. Mon. Effluent Gross REQUIREMENT MOAVG DAILYMX MOAVG DAILYMX Flow, in conduit orthru treatment SAMPLE ****** - -plant MEASUREMENT 0 . 0001 C'J. ooo I M&D

500501 0 PERMIT Req. Mon. Req. Mon. MGD - ****** ****** Effluent Gross REQUIREMENT MOAVG DAILYMX

r-urm 1\ppruveu

OMB No 2040.()()()4


MAJOR

(SUBRW)

OUTFALL 006 DRY WEATHER

External Outfall

No DischargeD

NO. FREQUENCY I SAMPLE


su 0 7.-l f\'10 ~~AB

sv Twice per GRAB Month

"" Clj t '- 0 -z./Mo UJ,...p z.n mg/L Twice per COMP24

Month

f"'q /~ 0 -z,l f'V\0 6t--l\.f3


~9"-- 0 7../rno U3"'JA' Z.4


****** I O Wf'lrtL~o. "f E~,._.A

****** Weekly ESTIMA

'

Volatile Organic Compound [VOC] SAMPLE ****** ****** ****** ******

l lr~G I MEASUREMENT 0 0 Lt')ll._ 0 -z. f,.o 514151 0 I PERMIT - - ****** Req. Mon. - Req. Mon. ug/L Twice per GRAB Effluent Gross REQUIREMENT MOAVG DAILYMX . Month Volatile fraction organics [EPA 624] SAMPLE ****** ****** ****** --MEASUREMENT 3.L1 so ~ . 3,0 \.( <ji {'- 0 7../f)AO (,. "'I> 13. 78733 1 0 PERMIT ****** ****** ****** Req. Mon. ****** Req. Mon. ug/L Twice per GRAB Effluent Gross REQUIREMENT MOAVG DAILYMX Month

I cenll'f unoer ponoay olio" thatll1is -lind d-.,...,. prepared onlor my dir-. or

I Aittll i!w 'f. !mt•L fJl l~'"n~..=e~"'~~~-=-~~.:=:::,.~·-::".;.':~':~~===:.=::;..~·~~=.'::':':,~. ~ -JIOftMM lor .,lllnilmg -lnlomoollon. ilWding lllo ~ orlino lind""""""""..,.,., -..g IGNATURE OF PRINCIPAL EXECUTIVE OFFICER OR

Exec. Mgr, Env. Remediation

NAME/TITLE PRINCIPAL EXECUTIVE OFFICER TELEPHONE DATE

I TYPED OR PRINTED 1-... AUTHORIZED AGENT AREA c-. -


SEE PAGE 9 OF PERMIT; FLOW TOTAL SEE FOOTNOTE 4. SEMIVOLATILES UNDER 51415.

EPA Fonn 3320-1 (Rev.D1106) Previous editions may be used. 12115/2014 Page 1

PERMITTEE NAMEJADDRESS (Include FaCJiity Namrt/l.ocation if Different)




LOCATION: 159 PLASTICS AVE PITISFIELD, MA 01201

ATIN: Andrew T. Silfer, Exec Mgr. En

NA IIUNAL t'ULLU I AN I UI~.._MAHul: t:LIMINA II UN ~ Y:::, I t::M lNt'Ut::~l


I MA0003891 II 0006-A I PERMIT NUMBER DISCHARGE NUMBER

MONITORING PERIOD

MMIDDIYYYY I MM/DDIYYYY

02/01/2015 02/28/2015


Flow, total SAMPLE - - -MEASUREMENT O . OOO'Z. ".0003 ""'G. I?

822201 0 PERMIT Req. Mon. Req. Mon. MGD - ****** -Effluent Gross REQUIREMENT MOAVG DAILYMX

I NAME/TITLE PRINCIPAL EXECUTIVE OFFICER I' ~lftlorpona.., Dllaw_lll.ol IIlii ---··--,.pr-od &nlo<"" d-0< IU- lo ..-danoewWI a syot-<IHignod lo ......... quoiliod ponMnOI"'""""' g<llhof and

llbidiEW 'f. !ilfe. ,! ,_.,. __ od Basod'"''"'ini!UOYDI ... ponanor ____ ...

rorm /o\pproveo

OMB No. 2040.0004


MAJOR

(SUBRW)


External Oulfall No DischargeD

NO. FREQUENCY SAMPLE I

UNITS EX OF ANALYSIS TYPE - 0 'Z/""o ~~1'-<.A - Weekly ESTIMA

TELEPHONE DATE

Exec. Mgr, Env. Remediation oyo!Om. 01"""" P""""'dired¥....,.....,.. lor Qlllllomg.,. ..,....,__.,.-_..,II, to ~he bnlc4mybxMtldgeaNMitf, true. 80C&nle . ..t~Je. l.-n...,.thM#Mrlla~eUgl~ rl K v V"'""' r' ' (I<YY t< - I ponalln ... ~-lnl-.~ ... poo--,ot--~,.,~ -·-··· - --·-·--- ----- ---- -

I TYPED OR PRINTED I-..- AREA~


SEE PAGE9 OF PERMIT; FLOW TOTAL SEE FOOTNOTE 4. SEMIVOLATILES UNDER 51415.

EPA Form 3320.1 (Rev.01106) Previous editions may be used. 12/15/2014 Page 2

Attachment E - Outfall 006 Dry

Date pH Oil &Grease FN TSS FN PCB FN MG/l MG/L UG/l

02/01/15 02/02/15 02/03/15 02/04/15 02/05/15 02/06/15 02/07/15 6.98 U4.10 8.40 0.0542 02/08/15 02/09/15 02/10/15 02111/15 02/12/15 7.17 U4.00 02/13/15 8.20 0.0192

io2114/15 io2115/15 lo2116/15 02/17/15 02/18/15 02/19/15 02120/15 02/21/15 02/22/15 02/23/15 02/24/15 02/25/15 02/26/15 02/27/15 02/28/15



G - Grab sample

voc FN svoc FN Estimated Estimated Raln/Preclp Rain/Precip Flow-MGD Flow-MGD Total-In Peak -In

(50050 1 0) (82220 1 0) 0.0001 0.00 0.00

0.20 0.07 0.16 0.02 0.00 0.00 0.15 0.04 0.09 0.05

0 0.0003 0.08 0.08 0.0001 0.06 0.02

0.19 0.05 0.07 0.01 0.00 0.00

4.370 0 0.08 0.06 0.0002 0.04 0.02

0.00 0.00 0 .0001 0.13 0.02

0.00 0.00 2.530 0.00 0.00

0.00 0.00 0,01 O.D1 0.52 0.08 0.36 0.11

0.0001 0.08 0.02 0.03 0.02 0.52 0.14 0.00 0.00 0.00 0.00

0.00 0.00 0.00 0.00

February 18, 2015


1000 East Street Pittsfield, MA 01201


Dear Mr. Coyle:


Analytical Report for Service Request No: R1500963

Enclosed are the results of the sample(s) submitted to our laboratory on February 10, 2015. For your reference,

these analyses have been assigned our service request number Rl500963.

All analyses were performed according to our laboratory's quality assurance program. The test results meet

requirements of the NELAP standards except as noted in the case narrative report. All results are intended to be

considered in their entirety, and ALS Environmental is not responsible for use of less than the complete report.

Results apply only to the items submitted to the laboratory for analysis and individual items (samples) analyzed,

as listed in the report. The measurement uncertainty of the results included in this report is within that expected

when using the prescribed method(s) for analysis ofthese samples, and represented by Laboratory Control

Sample control limits. Any events, such as QC failures, which may add to the uncertainty are explained in the

report narrative.

Please contact me ifyou have any questions. My extension is 7473. You may also contact me via email at

[email protected].



~\_ I


"" .. RIGHT SOLUTIONS

Page 1 of 15

RIGHT PARTNER

tt·

Client: Service Request No.: Project: Date Received: Sample Matrix: ProjecUCase No.:

ALS Environmental

General Electric R1500963 GE-Pittsfield NPDES 2/10115 Water

CASE NARRATIVE

All analyses were performed consistent with the quality assurance program of ALS Envirorunental. This report contains analytical results for samples designated for Tier H. When appropriate to the method, method blank results have been reported with each analytical test.

Sample Receipt

One water sample was received for analysis at ALS Environmental on 2/10/15. The sample was received in good condition and consistent with the accompanying chain of custody form. The sample was received within the 0-6°C

temperature guidelines. The sample was stored in a refrigerator between l°C and 6°C upon receipt at the laboratory.





The Laboratory Control Sample and Duplicate Laboratory Control Sample (LCSD) for Benzidine and the LCSD for Di-n-butyl Phthalate and Diethyl Phthalate were outside ofthe control limits and have been flagged with a"*". There were no hits in the sample for these compounds. There may be a low bias in the sample for Benzidine.


Approved by___,~~---------------D. ate __ ~_\ ..... 18_\"-t-~--

'


l\alprews001\starlimsSILIMSRepsiCaseNarrative,rpt


LabiD R 1500963-001

Client 10 006D-1Q2M-1X-GS

oaeea

A Enuoronmental

u

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B

E

E

D

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H

#


Analyte was analyzed for but not detected. + Correlation coefficient for MSA is <0.995. The sample quantitation limit has been N Inorganics· Matrix spike recovery was outside corrected for dilution and for percent moisture, unless otherwise noted in the case laboratory limits.



Tentatively Identified Compound (TIC) or s Concentration has been determined using Method that the concentration is between the MRL of Standard Additions (MSA). and the MDL. Concentrations are not verified

\V Post-Digestion Spike recovery is outside control within the linear range of the calibration. For DoD: concentration >40% difference between limits and the sample absorbance is <50% of the





Inorganics· Concentration is estimated due to Q DoD reports: indicates a pesticide/Aroclor is not the serial dilution was outside control limits. confirmed ~ 100% Difference between two GC

Organics· Concentration has exceeded the columns).


Concentration is a result of a dilution, MRL Method Reporting Limit. Also known as: typically a secondary analysis of the sample LOQ Limit of Quantitation (LOQ) due to exceeding the calibration range or that The lowest concentration at which the method a surrogate has been diluted out of the sample analyte may be reliably quantified under the and cannot be assessed. method conditions .

Indicates that a quality control parameter has MDL Method Detection Limit. A statistical value derived exceeded laboratory limits. Under the from a study designed to provide the lowest "Notes" column of the Form 1, this qualifier concentration that will be detected 99% of the time. denotes analysis was performed out of Values between the MDL and MRL are estimated Holding Time. (see J qualifier).

Analysis was performed out of hold time for LOD Limit of Detection. A value at or above the MDL tests that have an "immediate" hold time which has been verified to be detectable. criteria. ND Non· Detect. Analyte was not detected at the Spike was diluted out. concentration listed. Same as U qualifier.

Lab ID # for Massachusetts Certification M-l\TY032

Analyses were conducted in accordance with Massachusetts Department of Environmental Protection certification standards, except as noted in the laboratory case narrative provided. A copy of the current Department issued parameter list is included in this report.

'T • ~.:.J:""~7~":;r.."'~·~..m:-;::~£:.•-..... 'l,l!'-!Z:::!.:Z::::-=:lD.-:ow!...,c::s;:u: .... '2.~W"AICIG:L.~\~~-rs::&.===coo="'"""--='=

.i< f G H T S 0 1. Jl T i :,: ~~r S F I C H T Pi\ f( TN E R

P:\INTRANE1\QAQC\Fonns Controlled\QUALIF _routine forMA rJ.DOC stlln f3 a e 4

The . Com1nonwealth of Massachus~tts·

1Jepart1nent of E~vb·onmental Protection Division of Environmental ~nalysis

Senator William X Wall Experiment Station

M-li.'Y032

certifies

ALSE~ONMENTALROCHESTER 1565 JEFFERSON RD BUILDING 300, SUITE 360 ROCHESTER, NY 14623-0000

Laboratory Director: LARRY LEWIS

for the a11aly~isoj NON POTABLE WA~ER(CHEMJSTRY)

prn-sua11t to 310.CMR 42.00

This certificate supersedes all previous Massachu~ett's certificates issued to this laboratory. The laboratory is regulated by and shall be responsible for being in compliance with Massachusetts regulations at 310 CMR 42.00. · · ·

This cert(ftcaie is valid O~Jiy when accompanied by the latest dated Certified Parameter List issued by the Massachusetts b.E.P. Contact the Division o/Environmental Analysis to verify th~. current certiflcaffqrJ status of the laborqtory.

Certification is ·no guarantee 'of the validity of the data . . This certification is subject to unannounced laboratt?ry inspections.

Issued: 01 JPL 2014

Expires: 30 JiJN 2015

Director, pivuion of Environmental Analysis

eeues



M-NY031 ALS ENVIRONMENTAL ROCHESTER.·

ROCHESTER NY


Analytes

ALUMINUM

ANTIMONY

ANTIMONY

ARSENIC

ARSENIC BERYLLIUM

BERYLLIUM

CADMIUM

CADMIUM

CHROMIUM

CHROMIUM

COBALT

COBALT

COPPER

COPPER

IRON

LEAD

LEAD

MANGANESE

MANGANESE

MERCURY

MOLYBDENUM

MOLYBDENUM

NICKEL·

NICKEL

SELENIUM

SELENIUM

SILVER

SILVER

THALLIUM

THALLIUM

VANADIUM

VANADIUM

ZINC

ZINC SPECIFIC CONDUCTIVITY



CALCIUM

MAGNESIUM

SODIUM

POTASSIUM

ALKALINITY, TOTAL

June 26, 2014

Effective Date

01 JUL2014

*= Provisional CertlficatJon


Methods

EPA200.7

EPA200.7

EPA200.B

EPA200.7

EPA200.8

EPA200.7

EPA200.8

EPA 200.7

EPA200.8

EPA200.7

EPA200.8

EPA200.7

EPA200.B

EPA200.7

EPA200.8

EPA200.7

EPA200.7

EPA200.B

EPA200.7

EPA200.8

EPA245.1

EPA200.7

EPA200.8

EPA200.7

EPA200.8

EPA200.7

EPA200.8

EPA200.7

EPA200.B

EPA200.7

EPA200.8

EPA200.7

EPA200.6

EPA200.7

EPA200.8

EPA 120.1

SM2540C

SM2340C

EPA200.7

EPA200.7

EPA200.7

EPA200.7

SM2320B

Page 1 of 1

eeoos


Certified Parameter List as of:

M-NY032 ALS ENVIRONMENTAL ROCHESTER

ROCHESTER l't'Y

NON POTABLE WATER {CHEMISTRY)

Analytes

CHLORIDE

CHLORIDE

FLUORIDE

SULFATE

AMMONIA·N

NITRATE-N

NITRATE-N

KJELOAHL-N

ORTI-IOPHOSPHA TE

PHOSPHORUS, TOTAL




CYANIDE, TOTAL


OIL AND GREASE

PHENOLICS, TOTAL

VOLA TILE HALOCARBONS


VOLATILE AROMATICS

VOLA TILE AROMATICS

SVOC-ACID EXTRACT ABLES

SVOC.BASEINEUTRAL EXTRACT ABLES

POLYCHLORINATED BIPI-ENYLS r;NA TEF

Effective Date

01JUL2014

01 JUL2014

June 16, 2014 *= Provisional Certlncatlon


Methods

SM 4500-CL·E

EPA300.0

EPA300.0

EPA300.0

EPA350.1

EPA300.0

EPA353.2

EPA351.2

EPA365.1

EPA365.1

EPA410.4

SM5210B

SM5310C

EPA 335.4

SM2540D

EPA 1664

EPA420.4

EPA601

EPA624

EPA602

EPA624

EPA625

EPA625

EPA608

Page 1 of 2

oeoe7




CAS No.

83-32-9 208-96-8 120-12-7

92-87-5 56-55-3 50-32-8

205-99-2 191-24-2 207-08-9

85-68-7 84-74-2 193-39-5

111-91-1 111-44-4 91-58-7

95-57-8 108-60-1 218-01-9 -53-70-3 91-94-1 120-83-2

84-66-2 131-11-3 105-67-9

51-28-5 121-14-2 606-20-2

122-66-7 117-81-7 206-44-0 --86-73-7 118-74-1 87-68-3

77-47-4

Printed 2/18/15 9 52


Analytical Report


0060-1 Q2M-I X-GS R 1500963-001

Scmi\'olatilc Organic Compounds by GC/MS

625 EPA 3510C I :\ACQUDA T A \5973 D\Data\021215\BA826.D\

Annlytc Name Result Q MRL

Acenaphthcne 4.7 u 4.7

Acenaphthylene 4.7 u 4.7

Anthracene 4.7 u 4.7

Benzidine 94 u 94 Benz( a)anthracene 4.7 u 4.7

Benzo(a)pyrene 4.7 u 4.7

Benzo(b )t1uoranthene 4.7 u 4.7 Benzo(g,h,i)perylene 4.7 u 4.7

Benzo(k)t1uoranthcne 4.7 u 4.7

Butyl Benzyl Phthalate 4.7 u 4.7 Di-n-butyl Phthalate 4.7 u 4.7

lndeno( I ,2,3-cd)pyrenc 4.7 u 4.7 -- -

B is(2-chloroethoxy )methane 4.7 u 4.7 8 is(2-chloroethyl) Ether 4 .7 u 4.7

2-Chloronaphtha\ene 4.7 u 4.7

2-Ch\oropheno\ 4.7 u 4.7 2,2'-0xybis( 1-chloropropane) 4 .7 u 4.7

Chrysene 4.7 u 4.7

Dibenz(a,h)anthracene 4.7 u 4.7 3,3'-Dichlorobenzidine 4.7 u 4.7 2,4-Dichlorophenol 4.7 u 4.7 --Diethyl Phthalate 4.7 u 4.7 Dimethyl Phthalate 4.7 u 4.7 2,4-Dimethylphenol 4 .7 u 4.7

2,4-Dinitrophenol 47 u 47 2,4-Dinitrotoluene 4.7 u 4.7 2,6-Dinitrotoluene 4.7 u 4.7

-I ,2-Diphenylhydrazine 4.7 u 4.7 8is(2·ethylhexyl) Phthalate 4.7 u 4.7 Fluoranthene 4.7 u 4.7

Fluorene 4.7 u 4.7 Hexachlorobenzene 4.7 u 4.7

Hexachlorobutadiene 4.7 u 4.7

Hexachlorocyc lopentadiene 4.7 u 4.7

Fonn lA

llollprcwsOOI\st~rlimsS\LIMSReps\An31yttc31Rcport rpt

MDL

1.0 1.0 1.0

90 1.0 1.0

1.0 1.0 1.0

2.4 1.0 1.2

2.2 1.3 1.0

1.0 1.0 1.0

1.3 4.5 1.3

1.0 1.0 1.5

20 1.6 1.8

1.0 1.2 1.0

1.0 1.0 1.3

1.0

Service Request: Rl500963 Date Collected: 2/7/15 0945 Date Received: 2110115

Date Extracted: 2/10115 Date Analyzed: 2/12/15 II :58

Units: J.lg/L Basis: NA



Note

- --

oeees SuperSet Rcrercncc 15.0000321339 rev 00


Sample Name: Lnb Code:


CAS No.

67-72-1 78-59-1 534-52-1

59-50-7 91-20-3 98-95-3

88-75-5 100-02-7 62-75-9

86-30-6 117-84-0 87-86-5

85-01-8 108-95-2 101-55-3

7005-72-3 621-64-7 129-00-0

120-82-1 88-06-2

Surrogate Name

p· Terphenyl-d 14 N i trobenzene-d5 Phenol-d6


Printed 2118/15 14:39


Anal) tical Report General Electric Company GE -Pittsfield NPDES Water

006D-IQ2M-IX-GS R 1500963-00 I


625 EPA3510C I:\ACQUDATA\5973D\Data\021215\BA826.D\


Hexachloroethane 4.7 u 4.7 Isophorone 4.7 u 4.7 4,6-Dinitro-2-methylphenol 47 u 47

4-Chloro-3-methylphenol 4.7 u 4.7 Naphthalene 4.7 u 4.7 Nitrobenzene 4.7 u 4.7 --2-Nitrophenol 4.7 u 4.7 4-Nitrophcnol 47 u 47 N-Nitrosodimethylamine 4.7 u 4.7

N-Nitrosodiphenylamine 4.7 u 4.7 Di-n-octyl Phthalate 4.7 u 4.7 Pentachlorophenol (PCP) 47 u 47 ----Phenanthrene 4.7 u 4.7 Phenol 4.7 u 4.7 4-Bromophenyl Phenyl Ether 4.7 u 4.7

4-Chlorophenyl Phenyl Ether 4.7 u 4.7 N-Nitrosodi-n-propylamine 4.7 u 4.7 Pyrene 4.7 u 4.7

I ,2,4-Trichlorobenzene 4.7 u 4.7 2,4,6-Trichlorophenol 4.7 u 4.7 Semi Volatile Organic Compounds 4.7 u 4.7


94 40-133 2/12/ 15 11:58 85 37-117 2112115 11:58 32 10-107 2112115 11:58

-84 39-119 2/12115 11:58 45 10-105 2112/ 15 11 :58 110 28-157 2/12/ 15 II :58

form lA

'.lolprewsOOI\starltmsS\I.IMSReps\Anal)ticaiRepon rpl

MDL

1.2 1.0 II

1.2 1.0 1.6

1.4 5.9 1.0

Service Request: Rl500963 Date Collected: 2/ 7/15 0945 Date Received: 2110115

Date Extracted: 2110/15 Date Analyzed: 2/12/15 II :58

Units: J.!g/L Basis: NA



Note

---1.0 1.2 6.9

1.0 1.0 2.2

1.2 1.3 1.0

1.0 1.4

0.68

Q

eoees SuperSet Reference· I S-0000321339 rev 00




CAS No.

83-32-9 208-96-8 120-12-7

92-87-5 56-55-3 50-32-8

205-99-2 191-24-2 207-08-9

85-68-7 84-74-2 193-39-5

111-91-1 111-44-4 91-58-7 - - -

95-57-8 108-60-1 218-01-9 -

53-70-3 91-94-1 120-83-2 -84-66-2 131-11-3 105-67-9

51-28-5 121-14-2 606-20-2

122-66-7 117-81-7 206-44-0

---86-73-7 118-74-1 87-68-3

77-47-4

Printed 2118115 9.52


Analytical Report


Method Blank RQI 501387-01

Semivolntilc Organic Compounds by GC/MS

625 EPA 3510C 1:\ACQUDA T A \5973D\Data\021215\BA822.D\

Analytc Name Result Q MRL

Acenaphthene 5.0 u 5.0

Acenaphthylene 5.0 u 5.0

Anthracene 5.0 u 5.0 ---Benzidine 100 u 100

Benz(a)anthracene 5.0 u 5.0

B enzo( a )py rene 5.0 u 5.0 ------Benzo(b )fluoranthene 5.0 u 5.0

Bcnzo(g, h, i )pery lene 5.0 u 5.0

Benzo(k)fluoranthene 5.0 u 5.0

Butyl Benzyl Phthalate 5.0 u 5.0

Di-n-butyl Phthalate 5.0 u 5.0

Indeno( I ,2,3-cd)pyrenc 5.0 u 5.0 --Bis(2-chloroethoxy)methanc 5.0 u 5.0

B is(2-chloroethyl) Ether 5.0 u 5.0

2-Chloronaphthalene 5.0 u 5.0

2-Chlorophenol 5.0 u 5.0

2,2'-0xybis( 1-chloropropane) 5.0 u 5.0

Chrysene 5.0 u 5.0

Dibenz(a,h)anthracene 5.0 u 5.0

3,3'-Dichlorobenzidine 5 .0 u 5.0

2,4-Dich lorophenol 5.0 u 5.0

Diethyl Phthalate 5.0 u 5.0

Dimethyl Phthalate 5.0 u 5.0

2,4-Dimethylphenol 5.0 u 5.0

2,4-Dinitrophenol 50 u 50

2,4-Dinitrotoluene 5.0 u 5 .0

2,6-Dinitrotoluene 5.0 u 5.0

I ,2-Diphenylhydrazine 5.0 u 5.0

Bis(2-ethylhexyl) Phthalate 5.0 u 5.0 Fluoranthene 5.0 u 5.0

Fluorene 5.0 u 5.0

Hexachlorobenzene 5.0 u 5.0

Hexachlorobutadiene 5.0 u 5.0

Hexachlorocyclopentadiene 5.0 u 5 .0

Form lA

1\:JiprcwsOO I \$tarlimsS\LIMSReps\Anal)1ica1Rcport rpt

MDL

1.0 1.0 1.0

90 1.0 1.0

1.0 1.0 1.0

2.4 1.0 1.2

2 .2 1.3 1.0

1.0 1.0 1.0

1.3 4.5 1.3

1.0 1.0 1.5

20 1.6 1.8

1.0 1.2 1.0

1.0 1.0 1.3

1.0

Service Request: R I 500963 Date Collected: NA Date Received: NA

Date Extracted: 2/10115 Date Analyzed: 2/ 12/ 15 10:15




Note

00'310 SuperSet Rcfcrcntc 15-0000321339 rcvOO

Client: Project: Sa mple Matrix:


Analytical Report


Scn·ice Request: Rl500963 Date Collected: NA Date Received: NA

Date Extracted: 2/1011 5 Date Analyzed: 2/ 12/ 15 10:15



Units: JJg/L Basis: NA






67-72-1 Hexachloroethane 5.0 u 5.0 1.2

78-59-1 lsophorone 5.0 u 5.0 1.0

534-52-1 4,6-Dinitro-2-methylphenol 50 u 50 II ---- - ---59-50-7 4-Chloro-3-methylphenol 5.0 u 5.0 1.2

91-20-3 Naphthalene 5.0 u 5.0 1.0

98-95-3 Nitrobenzene 5.0 u 5.0 1.6 - ---88-75-5 2-N itrophenol 5.0 u 5.0 1.4

100-02-7 4-Nitrophenol 50 u 50 5.9

62-75-9 N-Nitrosodimethylamine 5.0 u 5.0 1.0 -- ---- - --

86-30-6 N-Nitrosodiphenylamine 5.0 u 5.0 1.0

117-84-0 Di-n-octyl Phthalate 5.0 u 5.0 1.2

87-86-5 Pentachlorophenol (PCP) 50 u 50 6.9 ----- -- -85-01-8 Phenanthrene 5.0 u 5.0 1.0

108-95-2 Phenol 5.0 u 5.0 1.0

101-55-3 4-Bromophenyl Phenyl Ether 5.0 u 5.0 2.2 ----- --- ---7005-72-3 4-Chlorophenyl Phenyl Ether 5.0 u 5.0 1.2

621-64-7 N-N itrosod i-n-propyl amine 5.0 u 5.0 1.3

129-00-0 Pyrene 5.0 u 5.0 1.0 -

120-82-1 I ,2,4-Trichlorobenzene 5.0 u 5.0 1.0

88-06-2 2,4,6-Trichlorophenol 5.0 u 5.0 1.4 Semi Volatile Organic Compounds 5.0 u 5.0 0.68

Control Date Surrogate Name % Rec Limits Analyzed Q

p-Terphcny 1-d 14 99 40-133 2/12/ 15 10:15

N i trobenzene-d5 84 37-11 7 2/1 2/ 1510:15 Phenol-d6 32 10- 107 2/1211 5 10:1 5

- ---2-Fluorobiphenyl 79 39-119 2/12/ 15 10:15

2-Fiuorophenol 46 10-105 2/1211 5 10:15

2,4 ,6-Tribromophenol 106 28-157 2/12/ 15 10:15 -----

Prinh:d 2/18/15 14 39 Fonn lA o e e 11

\l:llpn:wsOOI\sl:~tlimsS\l.IMSR¢ps\AnalyticaiR¢por1 .rpt SuperSet Reference: 15.0000321339 rev 00

-


QAJQC Report




Lab Control Sample Summary Scmivolatile Organic Compounds by GC/MS




Lab Control Sample Duplicate Lab Control Sample RQ 1501387-02 RQI501387-03


Analytc Name Result Amount %Rec Result Amount 0/e Rcc Limits RPD Limit

Acenaphthene 95.2 100 95 98.5 100 98 47- 145 3 30

Acenaphthylene 97.6 100 98 101 100 101 33- 145 4 30

Anthracene 99.1 100 99 105 100 105 27- 133 6 30

Benzidine 100U 100 0 • 100 u 100 0 • 10- 169 NC 30

Benz(a)anthracene 101 100 101 106 100 106 33- 143 4 30

Benzo(a)pyrene 103 100 103 109 100 109 17- 163 6 30

Benzo(b )tluoranthene 101 100 101 107 100 107 24- 159 6 30

Benzo(g,h, i)pery1ene 103 100 103 109 100 109 10-219 6 30

Benzo(k)fluoranthene 92.6 100 93 101 100 101 II- 162 8 30

Butyl Benzyl Phthalate Ill 100 Ill 116 100 116 I 0- 152 4 30

Di-n-butyl Phthalate 114 100 114 120 100 120 • 10- 118 5 30

lndeno( I ,2,3-cd)pyrene 103 100 103 108 100 108 10- 171 5 30

B is(2 -ch loroethoxy )methane 91.3 100 91 92.2 100 92 33- 184 < I 30

Bis(2-chloroethyl) Ether 82.2 100 82 84.4 100 84 12- 158 3 30

2-Ch loronaphthalcnc 85.6 100 86 90.6 100 91 60- I 18 6 30

2-Ch lorophenol 90.6 100 91 89.1 100 89 23- 134 2 30

2 ,2'-0xybis( 1-ch loropropane) 84.0 100 84 82.2 100 82 36- 166 2 30

Chrysenc 99.6 100 100 105 100 105 17- 168 6 30

Dibenz( a,h )anthracene 103 100 103 109 100 109 10-227 6 30

3,3 '-Dichlorobenzidine 92.5 100 92 106 100 106 10-262 14 30

2,4-Dichlorophcnol 93.2 100 93 97.4 100 97 39- 135 4 30

Diethyl Phthalate I 12 tOO I 12 118 tOO 118 • 10- 114 5 30

Dimethyl Phthalate 103 100 103 109 100 109 10- 112 6 30

2,4-Dimethylphenol 99.1 100 99 103 100 103 32- 119 4 30

2,4-Dinitrophenol 86.0 100 86 80.3 100 80 10- 191 7 30

2,4-Dinitrotoluene 101 100 101 liS 100 115 39- 139 13 30

2,6-Dinitrotoluene lOS 100 105 110 100 110 50- I 58 5 30

1,2-Diphenylhydrazine 104 100 104 lOS 100 105 57- 117 <I 30

Bis(2-ethylhexyl) Phthalate 118 100 I 18 120 100 120 10- 158 2 30

Fluoranthene 108 100 108 118 100 118 26- 137 9 30

Fluorene 95.6 100 96 99.3 100 99 59- 121 4 30

Hexachlorobenzene 103 100 103 104 100 104 10- 152 I 30

Hexachlorobutad iene 74.3 100 74 73.3 100 73 24- 116 I 30

Results Oog.:cd wilh an aslcrisk (•) indicate \"a lues out~idc control crilcri:t.

Percent recoveries ~nd rel~tivc perrenl diiTcrcnccs (RPD) ~redetermined by lhe software using \':llues in lhe calculalion which ha\'C nol been rounded.

Prinlcd 2/18/1 S 9:52 Form 3C 00f.:J12 1\alprcwsOO l\slOU'hmsSU..IMSReps\LabConcroiSamplc.rpl SuperSet Reference 15..()()00321339 rcvOO


QNQC Rcpon


Project: GE -Pittsfield NPDES Date Analyzed: 2112115


Lab Control Sample Summary Semivolatile Organic Compounds by GC/MS

Analytical Method: 625 Units: llg/L



Lab Control Sample Duplicate Lab Control Sample RQ1501387-02 RQ1501387-03

Spike Spike %Rec RPD

Analyte Name Result Amount %Rec Result Amount % Rec Limits RPD Limit

Hexachlorocyclopentadiene 83.2 100 83 81.0 100 81 28-98 3 30


Isophorone 97.9 100 98 103 100 103 21- 196 5 30

4,6-Dinitro-2-methylphenol 97.0 100 97 107 100 107 10- 181 10 30

4-Chloro-3-mcthylphenol 105 100 105 Ill 100 Ill 22- 147 6 30

Naphthalene 72.2 100 72 75.0 100 75 21- 133 4 30

Nitrobenzene 94.8 100 95 96.2 100 96 35- 180 30

2-Nitrophcno1 93.0 100 93 92.6 100 93 29- 182 <1 30

4-Nitrophenol 64.4 100 64 70.1 100 70 10- 132 9 30

N-Nitrosodimethylamine 62.5 100 62 65.4 100 65 33 -70 5 30

N-Nitrosodiphenylamine 101 100 101 106 100 106 50- 117 5 30

Di-n-octyl Phthalate 117 100 117 124 100 124 10- 146 5 30


Phenanthrene 103 100 103 108 100 108 54- 120 4 30

Phenol 42.9 100 43 46.6 100 47 10- 112 8 30

4-Bromophenyl Phenyl Ether 102 100 102 103 100 103 53- 127 <1 30

4-Chlorophenyl Phenyl Ether 100 100 100 105 100 105 25- 158 5 30

N-Nitrosodi-n-propylamine 91.3 100 91 95.8 100 96 10-230 5 30

Pyrene 108 100 108 112 100 112 52- 115 3 30

I ,2,4-Trichlorobenzene 69.2 100 69 69.2 100 69 29-85 <I 30

2,4,6-Trichlorophenol 99.5 100 100 108 100 108 37- 144 8 30

Rcsull$ Rng~rd with an asterisk(*) indicate \ 'A lues outshlc control criteria.

Percent recO\·ericund relative percent differences (RPD}a re detcnnmcd by the softw<~re using \alucs in the calculauon which hnvc not been rounded.

Printed 2118115 9.52 FOfTTI3c e e a 13

\\alprcwsOOI\starlimsS\LIMSRcps\l.abConlroiSample.rpt SuperSet Reference I 5-0000321339 rev 00

Aenulranmental CHAIN OF CUSTODY/LABORATORY ANALYSIS REQUEST FORM J.~j~U

1565 Jefferson Road, Building 300, Suite 360 • Rochester, NY 146231 +1 585 288 5380 +1 585 288 8475 (fax) PAGE i OF I

Project-- ProjectNt.mber ANALYSIS REQUESTED (Include Method Number and Container Presetvatlve) .

N PD~ <; PISF- H t I Project~ llepart cc PRESERVATIVE ¢ I I J 1 .:5£ArJ c.o ..,J Compcly/AddreM I

/; hi;; Preservative Key

V60L.tf\. cNV t !Gc:."'>r-J,..,:)c; H_,c; .-:Y1 NA. ffi 0. NONE 1. HCL

~ 2. HN03

LOOO 8,' A "7-r "'-= ~ 3. H2S04 4. NaOH

0 5. Zn. Acetate

Ot"Z..6 ( u

J ~~'!~ 6. MeOH P •-rrs F •C• ,.-, MA ~ ll'i 'l.i } 1!1~ 6 "'/t!!J 7. NaHS04 -· Email ffi

( 4 I ~) Lf 9 t..l - G, I 0 'i' 51iEA~. CC> <,l f." ~ V :O C'l \.. •A, <"..J:I "'"' m 6. Other __

~ '!iif:l,/cli ~i ~~ ~~ ~h.wee..~ Sampler'a Prinlecl Name ::J REMARKS/ _.,~"' .) C! . C.d .., t.-1 z

o a ~ o q: o .P. ~<2 ~;3 ALTERNATE DESCRIPTION

FOR OmCE USE SAMPLING

CUENT SAMPLE ID ONLYLABIO DATE 11ME MATRIX

00<., D ·· f ((;) Z M • I )I" ~ (r ~ .,._,... - z{, / 1 s· 4 ~~ ot; A ~Jt. H ~.. n I t ·-------~~ ~ ~·~- . ..L ' •· ·- """' -~ ... ~. .. 4·-..t......:.'l. .··•· •'

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-~ .&l.......:·. ~-. - . .-~ :. =' . . . . ,. """"'- -.

' I ' · '

SPECIALINSlllUCTIONSICOMMENTS TURNAROUND REQUIREMENTS REPORT REQUIREMENTS INVOICE INFORMATION

Metals __ RUSH (SURCHARGES APPlY) __ I. ResiA!s Only

P. ~ + OC Summaries POt - - 1 clay-2day ----3 day --__ 4clay X 5day (I..CS, DUP, MS/MSO as II!QUinldl

' BILL TO: __ IU. Resdls + CC and Calibrallon

Summaries REQUESTED REPORT DATE

)(' IV. Data Vaildallon Repoot with Raw Data '

I SeeOAPP D

I MATE WHERE SAMPLES WERE COLLECTED Edata __ VIIS __ No

0 REUNOUISHEO BY RECEIVED BY REUNOUISHEO SY RECEIVED BY REUNOUISHED BY RECEIVED BY

Q,...<::__ (!_ (' J BJJr,Jogsa s ~ .

~- (' .- i~1 .. g_ Slgnabn Slgnall.re ~~--. -~ 11.....:1 -· C.O <.., U. CE -I'Htanol<t~h Amottca

~~t<"",VA. .,-\ j.s..,.,., l_ PmtedName Prilled Name Printed Name

IIIII/III Ill lflltlilillll\\lllllllllllllllllll\111 flnn ~/7 ( '"" z ·.o cp f'-< Aim._.. A-1..~. Arm F"rm lrnn

I Date/line l~t.eJ'-~ t)!}_r;(" Da!ei'Tine Oatelrlllfl jo.llllrtme 1Dalalllme . . OlsUibullon: White - lab Cow. Yal1ow - Return to Originator e 2012 by AlS Group

.

A B~1~9!!rt~~.~. s mtiiii~ffiiif 11m 11~1 1111 fl/JIIW Ill

Cooler Receipt and Preservation Check Form

Project/Client b<.. g·1bfW.J FolderNumber 'Rir--~3 Cooler received on ~t..lt 0 It<"

_I I by: ~h. COURIER: ALS UPS ~ VELOCITY CLIENT

1 Were Custody seals on outside of cooler? ~N 5a Perchlorate samples have required headspace? y N if:BA)

2 Custody papers properly completed (ink, signed)? ~N 5b Did VOA vials, Alk,or Sulfide have sig* bubbles? ...... YOJ>~

3 Did all bottles arrive in good condition (unbroken)? p)N 6 Where did the bottles originate? ~ CLIENI' -4 Circle: W~ Dry Ice Gel packs present? p?N 7 Soil VOA received as: Bulk Encore 5035set ~

8. Temperature Readings Date: z.L .. 1 '" Time: lu ~J ID: IR#3 d'J!ii) From: Temp Blank ~e -·-Observed Temp eC) '/.0

Correction Factor CCC) - l..t>

Corrected Temp (0 C) 'Z-· D Within 0·6°Cl (Y') N y N y N y N y N y N y N



All samples held in storage location: IWtn.e by ~b on at 1 ;>\~ 5035 samples placed in storage location: by on at __ _

PC Serondary Review:

Cooler Breakdown: Date : Time: IlK by: ~

2. Did all bottle labels and tags agree with custody papers? NO 3. Were correct containers used for the tests indicated? NO

1. Were all bottle labels com et (i.e_ analysis, preseivation, etc.)? ·--or.,~~~~---::-:N:-::0-

4. Air Samples: Cassettes I Tubes Intact Canisters Pressurized edlar® Bags Inflated Explain anv discrepancies: pH Reagent Yes No Lot Received

>12 NaOH $2 HN03 $2 H2so. <4 NaHSO. Residual ForCN If+, contact PM to Chlorine Phenol add Na2S103 (CN),

(-) and 522 ascorbic (phenol).

Na2S203 - . ZnAcetate - . HCl ** ••

Bottle lot numbers: tatJf.'l I/':- 1/jJ Other Comments:

~

Exp SampleiD Vol. Lot Added Final Added pH

**Not to be tested before analysis -pH tested and recorded by VOAs on a separate worksheet

Yes-AU samples OK


PM OK to Adjust:

PC Secondary Review: L\,, ) *significant air bubbles: VOA > 5-6 mm : WC > 1 in. diameter

P:\INTRANET\QAQC\Forms ConlrOlled\Coo~ipt t7.doe S/6/14 081315

,

February 23, 2015


1 000 East Street Pittsfield, MA 0120 I


Dear Mr. Coyle:


Analytical Report for Service Request No: R150 1073

Enclosed are the results of the sample(s) submitted to our laboratory on February 13, 2015. For your reference, these analyses have been assigned our service request number Rl501073.






I I ~ •J ~ .. i i 'i 1 ... ,. , ..

I'·' I'

Page 1 of O,.e

T' I t, t: T I · ": r 1

Client: Service Request No.: Project: Date Received: Sample Matrix: ProjecUCase No.:

ALS Environmental

General Electric Rl501073 GE-Pittsfield NPDES 2/13/15 Water

CASE NARRATIVE

All analyses were performed consistent with the quality assurance program of ALS Environmental. This report contains analytical results for samples designated for Tier II. When appropriate to the method, method blank results have been reported with each analytical test.

Sample Receipt

Three water samples were received for analysis at ALS Environmental on 2/13/15. The samples were received in good condition and consistent with the accompanying chain of custody form. The samples were received within the 0-6"C temperature guidelines. The samples were stored in a refrigerator between 1 °C and 6°C upon receipt at the laboratory.

Volatile Organics




Extractable Orgonics




The Laboratory Control Sample and Duplicate Laboratory Control Sample (LCSD) for Benzidine and the DLCS for Diethyl Phthalate were outside ofthe control limits and has been flagged with a"*". The Laboratory Control Limit for Benzidine recovered below the MRL. There were no hits in the sample for these compounds but there may be a low bias for Benzidine.


Approved by __ _..~~~1..6L1J""-=-----------Date. __ _,IJ...~\')3-=_..,\t,_...S""_


\\alprews001 \starilms$\LIMSReps\CaseNarraUve .rpt

Service Request Number: R1501073

LabiO R1501 073-001 R1501073-002

R1501073-003

Client 10 0060-1 Q2M-1 X-GV 0060-1 Q2M-2X-GS TRIP BLANK

• A Enu~rcnmental u

J

B

E

E

D

•

H

#


Analyte was analyzed for but not detected. + Correlation coefficient for MSA is <0.995.

The sample quantitation limit has been N Inorganics- Matrix spike recovery was outside corrected for dilution and for percent laboratory limits. moisture, unless otherwise noted in the case narrative. N Organics- Presumptive evidence of a compound


Tentatively Identified Compound (TIC) or s Concentration has been determined using Method

that the concentration is between the MRL of Standard Additions (MSA).

and the MDL. Concentrations are not verified w Post-Digestion Spike recovery is outside control within the linear range of the calibration. For DoD: concentration >40% difference between

limits and the sample absorbance is <SO% of the

two GC columns (pesticides/Ardors). spike absorbance.




lnorganics- Concentration is estimated due to Q DoD reports: indicates a pesticidc/Aroclor is not

the serial dilution was outside control limits. confirmed ~ 100% Difference between two GC



Concentration is a result of a dilution, MRL Method Reporting Limit. Also known as:

typically a second31)' analysis of the sample LOQ Limit of Quantitation (LOQ)

due to exceeding the calibration range or that The lowest concentration at which the method

a surrogate has been diluted out of the sample analyte may be reliably quantified under the

and cannot be assessed. method conditions.

Indicates that a quality control parameter has MDL Method Detection Limit. A statistical value derived

exceeded laboratory limits. Under the from a study designed to provide the lowest

"Notes" column of the Form I, this qualifier concentration that will be detected 99% of the time.

denotes analysis was performed out of Values between the MDL and MRL are estimated

Holding Time. (see 1 qualifier).

Analysis was performed out of hold time for LOD Limit of Detection. A value at or above the MDL

tests that have an "immediate" hold time which has been verified to be detectable.

criteria. ND Non-Detect. Analyte was not detected at the

Spike was diluted out. concentration listed. Same as U qualifier.


Analyses were conducted in accordance with Massachusetts Department of Environmental Protection certification

standards, except as noted in the laboratory case narrative provided. A copy of the current Department issued

parameter list is included in this report.

i ~~ ! C H '! P i\ R T :'-1 E R

P:\INTRANE1\QAQ0Fomu Controlled\QUALIF _routine for MA r3 DOC s11~pea4

•

The Com1nonweal~h of Massa.chusetts

Depart1nent of ~nvironmental Protection Division of E11vironmental A11alysis

Senatm· William X Wall Experimen( Station

M-NY032

certifies

ALS ENVIRONMENTAL ROCHESTER 1565 JEFFERSON RD BUILDING 300, SUITE 360 ROCHESTER, NY 14623-0000


for tlte analysis ·of NON POTABLE WATER (CHEMISTRY)

pursua11t to 310 CMR 42.00

This certificate supersedes all previous Massachusetts certificates issued to this laboratory. The laboratory is regulated by and shall be responsible for being in compliance with Massachusetts regulations at 310 CMR. 42.00. · ·

This certificate is valid only when accompa11ied by the Ja.testdated Certified Parameter List nr.l·:ftll.t:~' issued by the Massachusetts .b.E.P. Contact the Division of Environmental Analysis to verify the current certiftcafjqn status of the labprqt~ry.

Certification is no guarantee of the validity of the data. ThiS certification is subject to unannounced laboratory inspections.

Director, Division of Environmental Analysis

Issued: 01 JUL 2014

Expires: 30 JON 2015

eeoes

COMMOl\'WEALTH OF MASSACHUSETTS DEPARTMENT OF ENVIRONMENTAL PROTECTION . .

Certified Parameter List as of: 01 JUL 2014


ROCHESTER NY


Analytes

ALUMINUM

ANTIMONY

ANTIMONY

ARSENIC

ARSENIC

BERYLLIUM

BERYLLIUM

CADMIUM

CADM~UM

CHROMIUM

CHROMUM

COBALT

COBALT

COPPER

COPPER

IRON

LEAD

LEAD

MANGANESE

MANGANESE

MERCURY

MOLYBDENUM

MOLYBDENUM

NICKEL

NICKEL

SELENIUM

SELENIUM

SILVER

SILVER

THALLIUM

THALLIUM

VANADIUM

VANADIUM

ZINC

ZINC



HARDNESS (CAC03), TOTAL

CALCIUM

MAGNESIUM

SODIUM

POTASSIUM

ALKALINITY, TOTAL

June 26, 2014

Effective Date

01 JUL 2014

*=Provisional Certification


Metbods

EPA200.7

EPA200.7

EPA200.B

EPA200.7

EPA200.8

EPA200.7

EPA200.B

EPA200.7

EPA200.B

EPA200.7

EPA200.8

EPA200.7

EPA200.B

EPA200.7

EPA200.8

EPA200.7

EPA200.7

EPA200.8

EPA200.7

EPA200.8

EPA 245.1

EPA200.7

EPA200.8

EPA200.7

EPA200.8

EPA200.7

EPA 200.S

EPA200.7

EPA200.8

EPA200.7

EPA200.8 '

EPA200.7

EPA200.8

EPA200.7

EPA200.8

EPA 120.1

· SM2540C

SM2340C

EPA200.7

EPA200.7

EPA200.7

EPA200.7

SM2320B

Page 1 of 2

oooes

• COMMONWEALTH OF MASSACHUSETTS

DEPARTMENT OF ENVIRONMENTAL PROTECTION

Certified Parameter List as or:


ROCHESTER NY


Analytes

CHLORIDE

CHLORIDE

FLUORIDE

SULFATE

AMMONIA·N

NITRATE·N

NITRATE·N

KJELDAHL·N

ORTHOPHOSPHATE

PHOSPHORUS, TOTAL




CYANIDE, TOTAL


OIL AND GREASE

PHENOLICS, TOTAL



VOLA TILE AROMATICS

VOLATILE AROMATICS

SVOC-ACID EXTRACTABLES

SVOC-BASE/NEUTRAL EXTRACT ABLES

POL YCHLORJNA TED BIPHENYLS \'IVA TEf

Effective Date

01 JUL2014

01 JUL2014

June 26, 2014 *= Provisional Certification

Expiration 30JUN 2015 Date

Methods

SM 4500-CL·E

EPAJOO.O

EPAJOO.O

EPA300.0

EPA350.1

EPA300.0

EPA353.2

EPA351.2

EPA365.1

EfA365.1

EPA410.4

SM 52106

SM5310C

EPA335.4

SM2540D

EPA 1664

EPA420.4

EPA601

EPA624

EPA602

EPA624

EPA625

EPA625

EPA608

Page 1 of 2

ooea?




CAS No.

71-55-6 79·34·5 79-00·5

75-34-3 75-35-4 95-50-1

107-06-2 78-87-5 541-73-1

106-46-7 110-75-8 107-02-8 -I 07-13-1 71-43-2 75-27-4

75-25-2 74-83-9 56-23-5

108-90-7 75-00-3 67-66-3

74-87-3 124-48-1 75-71-8

75-09-2 100-41-4 127-18-4

108-88-3 79-01-6 75-69-4

75-01-4 10061-01-5 156-60-5

10061-02-6

Printed 2123115 9·30


Analytical Report General Electric Company GE ·Pittsfield NPDES Water

006D·1Q2M·IX·GV Rl501 073·001

Service Request: R1501073 Date Collected: 2/12/15 1245 Date Received: 2113115 Date Analyzed: 2/13115 13:52



624 Analysis Lot: 432696 I :\ACQUDA T A \MS VOA6\DA T A \0213 15\M0402.0\ Instrument Name: R·MS-06

Dilution Factor:


I, 1, 1-Trichloroethane (TCA) 1.0 u 1.0 0.13 I, 1 ,2,2· Tetrachloroethane 1.0 u 1.0 0.23 I, I ,2-Trichloroethane 1.0 u 1.0 0.12

I, t-Dich1oroethane (1, I-DCA) 1.0 u 1.0 0.10 I, 1-Dichloroethene ( 1,1-DCE) 1.0 u 1.0 0 .22 I ,2-Dichlorobenzene 1.0 u 1.0 0.10 ---I ,2-Dichloroethane 1.0 u 1.0 0.18 I ,2-Dichloropropane 1.0 u 1.0 0.15 1 ,3-Dichlorobenzene 0.18 J 1.0 0.10 - - .. --I ,4-Dichlorobenzene 1.5 1.0 0.15 2-Chlorocthyl Vinyl Ether 10 u 10 0.64 Acrolein 10 u 10 0.73

Acrylonitrile 10 u 10 0.37 Benzene 1.0 u 1.0 0.10 Bromodichloromethane 1.0 u 1.0 0.15

Bromoform 1.0 u 1.0 0.16 Bromomethane 1.0 u 1.0 0.12 Carbon Tetrachloride 1.0 u 1.0 0.10

Chlorobenzene 0.17 J 1.0 0.13 Chloroethane 1.0 u 1.0 0.15 Chloroform 0.92 J 1.0 0.13

Chloromethane 1.0 u 1.0 0.16 Chlorodibromomethane 1.0 u 1.0 0.15 Dichlorodifluoromcthanc (CFC 12) 1.0 u 1.0 0.17

Methylene Chloride 0.20 J 1.0 0.18 Ethylbenzene 1.0 u 1.0 0.19 Tetrachloroethene (PCE) 1.0 u 1.0 0.20 ---Toluene 1.4 1.0 0.10 Trichloroethene (TCE) 1.0 u 1.0 0.15 Trichlorofluoromethane (CFC l 1) 1.0 u 1.0 0.13

Vinyl Chloride 1.0 u 1.0 0.14 cis-! ,3-Dichloropropene 1.0 u 1.0 0.14 trans-1 ,2-Dich1oroethene 1.0 u 1.0 0.15

------trans- I ,3-Dichloropropene 1.0 u 1.0 0.10

FCl111111A

\lnlprewsOOI\slarlims$\l.IMSReps\AnalycicaiReport.rpl SuperSet Reference: ,Q&i8~6BiJrSoo




Analytical Report


0060-1 Q2M-1 X-GV Rl501073-001

Service Request: Rl501073 Date Collected: 2/12/15 1245 Date Received: 2/1311 5 Date Analyzed: 2/13/ 15 13:52

Units: j..tg/L Basis: NA

Volatile Organic Compounds by GCIMS with 3 Day Holding Time for Acrolein, Unpreserved


Control Surrogate Name 0/oRec Limits

I ,2-Dichloroethane-d4 91 81-127 4-Bromofluorobenzene 96 79-123 Toluene-dB 96 83-120

Pri ntcd 2123/1 S 9:3 0 Fo!:m1A

1\alprewsOO l \starlimsS\LIMSReps\Anal)1icalRepon .rpl

Date Analyzed

2/13/ 15 13:52 2/1311 5 13:52 2/13/ 15 13:52

Q


Dilution Factor: 1




Analytical Report


Service Request: R I SO I 073 Date Collected: 2/12/15 Date Received: 2/ 13/15 Date Analyzed: 2/13/15 1352



006D-1Q2M-IX-GV RI501073-00I




Comments:

Printed 02/23/20 15 9 ;30 Form IB

\l:llprewsOOI\st;ulimsS\LIMSRcps\AnalyticaiTICRepol1 rpt


SuperSet Reference. 1Jlos.J~




CAS No.

83-32-9 208-96-8 120-12-7

92-87-5 56-55-3 50-32-8


Analytical Report

General Electric Company GE -Pittsfield NPOES Water

0060-1 Q2M-2X-GS R 150 1 073-002

Semivo1atile Organic Compounds by GC/MS

625 EPA3510C 1:\ACQUOAT A \59730\Data\021815\BA85 I .D\


Acenaphthene 4.7 u 4.7 Acenaphthylene 4.7 u 4.7 Anthracene 4.7 u 4.7

Benzidine 94 u 94 Benz( a )anthracene 4.7 u 4.7 Benzo(a)pyrene 4.7 u 4.7

-- ---205-99-2 Benzo(b )fluoranthene 4.7 u 4.7 191-24-2 Benzo(g,h, i)perylene 4.7 u 4.7 207-08-9 Benzo(k)fluoranthene 4.7 u 4.7

85-68-7 Butyl Benzyl Phthalate 4.7 u 4.7 84-74-2 Di-n-butyl Phthalate 4.7 u 4.7 193-39-5 Indeno( I ,2,3-cd)pyrene 4.7 u 4.7 -- ----111-91-I B is(2-chloroethoxy )methane 4.7 u 4.7 111-44-4 Bis(2-chloroethyl) Ether 4.7 u 4.7 91-58-7 2-Chloronaphthalene 4.7 u 4.7 --------- -95-57-8 2-Chlorophenol 4.7 u 4.7 108-60-1 2,2'-0xybis( 1-chloropropane) 4.7 u 4.7 218-01-9 Chrysene 4.7 u 4.7

53-70-3 Dibenz( a,h )anthracene 4.7 u 4.7 91-94-1 3 ,3'-Dichlorobenzidine 4.7 u 4.7 120-83-2 2,4-Dichlorophenol 4.7 u 4.7

84-66-2 Diethyl Phthalate 4.7 u 4.7 131-11-3 Dimethyl Phthalate 4.7 u 4.7 105-67-9 2,4-Dimethylphenol 4.7 u 4.7 --51-28-5 2,4-Dinitrophenol 47 u 47 121-14-2 2,4-Dinitrotoluene 4.7 u 4.7 606-20-2 2,6-Dinitrotoluene 4.7 u 4.7 ---122-66-7 I ,2-Diphenylhydrazine 4.7 u 4.7 117-81-7 Bis(2-ethylhexyl) Phthalate 4.7 u 4.7 206-44-0 Fluoranthene 4.7 u 4.7

86-73-7 Fluorene 4.7 u 4.7 118-74-1 Hexachlorobenzene 4.7 u 4.7 87-68-3 Hexachlorobutadiene 4.7 u 4.7

--- -77-47-4 Hexachlorocyclopentadiene 4.7 u 4.7

Printed 2123/ 15 9.:30 Fonni A

\lalprewsOO 1\slllrlmuS\l.IMSReps\AnalyticaiReport.!pl

Service Request: Rl501073 DateCollected: 2/12/15 1245 Date Received: 2/13115

Date Extracted: 2/13/15 Date Analyzed: 2/18/15 13:03




MDL Note

1.0 1.0 1.0 ---90 1.0 1.0

1.0 1.0 1.0

2.4 1.0 1.2

2.2 1.3 1.0

1.0 1.0 1.0

1.3 4.5 1.3

1.0 1.0 1.5

20 1.6 1.8

1.0 1.2 1.0

1.0 1.0 1.3

1.0

SuperSet Reference: IDI<Qil~rl.oo

. Client: Project: Sample Matrix:



CAS No.

67-72-l 78-59-l 534-52-1

59-50-7 91-20-3 98-95-3

88-75-5 100-02-7 62-75-9

86-30-6 117-84-0 87-86-5

85-01-8 108-95-2 101-55-3

7005-72-3 621-64-7 129-00-0

120-82-1 88-06-2

Surrogate Name

p-Terphenyl-d 14 Nitrobenzene-d5 Phenol-d6

2-Fiuorobiphenyl 2-Fluorophenol 2,4,6-Tribromophenol

Printed 2123115 9:30


Analytical Report General Electric Company GE -Pittsfield NPDES Water

0060-1 Q2M-2X-GS R1501073-002

Semivolatlle Organic Compounds by GC/MS

625 EPA3510C I:\ACQUDATA\5973D\Data\021815\BA851.D\


Hexachloroethane 4.7 u 4.7 lsophorone 4.7 u 4.7 4,6-Dinitro-2-methylphenol 47 u 47 -4-Chloro-3-methylphenol 4.7 u 4.7 Naphthalene 4.7 u 4.7 Nitrobenzene 4.7 u 4.7 ---2-Nitrophenol 4.7 u 4.7 4-Nitrophenol 47 u 47 N-N itrosodimethylamine 4.7 u 4.7

N-Nitrosodiphenylamine 4.7 u 4.7 Di-n-octyl Phthalate 4.7 u 4.7 Pentachlorophenol (PCP) 47 u 47

Phenanthrene 4.7 u 4.7 Phenol 4.7 u 4.7 4-Bromophenyl Phenyl Ether 4.7 u 4.7

4-Chlorophenyl Phenyl Ether 4.7 u 4.7 N-Nitrosodi-n-propylamine 4.7 u 4.7 Pyrene 4.7 u 4.7 ---I ,2,4-Trichlorobenzene 4.7 u 4.7 2,4,6-Trichlorophenol 4.7 u 4.7 Semi Volatile Organic Compounds 4.7 u 4.7


94 40-133 2/ 18115 13:03 97 37-117 2/ 18115 13:03 38 10-107 2/ 18/ 15 13:03

90 39-119 2/ 18/ 15 13:03 57 10-105 2/ 18/ 15 13:03 118 28-157 2/ 18/15 13 :03

Form lA

\\alprcwsOO 1 lslarlimsS\LIMSRepsiAnal)1icalRcpon.rpl

MDL

1.2 1.0 II

1.2 1.0 1.6

1.4 5.9 1.0

1.0 1.2 6.9

1.0 1.0 2.2

1.2 1.3 1.0

1.0 1.4

0.68

Q

Service Request: Rl50l073 Date Collected: 2/12115 1245 Date Received: 2/13115





Note

SuperSet Reference: 1 $JGJfiM!re2Jo




CAS No.

71-55-6 79-34-5 79-00-5

75-34-3 75-35-4 95-50-1

107-06-2 78-87-5 541-73-1

106-46-7 110-75-8 107-02-8


Analytical Report


TRIP BLANK Rl501073-003

Service Request: Rl501073 Date Collected: 2/12/15 1245 Date Received: 2/13115 Date Analyzed: 2113115 13:20



624 Analysis Lot: 432696 1:\ACQUDA T A \MSVOA6\DA T A \021315\M040 1.0\ Instrument Name: R-MS-06

Dilution Factor: I


1, 1 , 1-Trichloroethane (TCA) 1.0 u 1.0 0.13 I, 1 ,2,2-Tetrachloroethane 1.0 u 1.0 0.23 l, 1 ,2-Trichloroethane 1.0 u 1.0 0.12

I, 1-Dichloroethane (1, I-DCA) 1.0 u 1.0 0.10 I, 1-Dich1oroethene (I, 1-DCE) 1.0 u 1.0 0.22 I ,2-Dich1orobenzene 1.0 u 1.0 0.10

--l ,2-Dichloroethane 1.0 u 1.0 0.18 I ,2-Dichloropropane 1.0 u 1.0 0.15 I ,3-Dichlorobenzene 1.0 u 1.0 0.10

I ,4-Dichlorobenzene 1.0 u 1.0 0.15 2-Chloroethyl Vinyl Ether 10 u 10 0.64 Acrolein 10 u 10 0.73

- -- ---- ----- ··---- - ------107-13-1 Acrylonitrile 10 u 10 0.37 71-43-2 Benzene 1.0 u 1.0 0.10 75-27-4 Bromodichloromethane 1.0 u 1.0 0.15

- ----- -----75-25-2 Bromofonn 1.0 u 1.0 0.16 74-83-9 Bromomethane 1.0 u 1.0 0.12 56-23-5 Carbon Tetrachloride 1.0 u 1.0 0.10 -- -108-90-7 Chlorobenzene 1.0 u 1.0 0.13 75-00-3 Chloroethane 1.0 u 1.0 0.15 67-66-3 Chlorofonn 1.0 u 1.0 0.13

74-87-3 Chloromethane 1.0 u 1.0 0.16 124-48-1 Chlorodibromomethane 1.0 u 1.0 0.15 75-71-8 Dichlorodifluoromcthanc (CFC 11} 1.0 u 1.0 0.17

75-09-2 Methylene Chloride 1.0 u 1.0 0.18 100-41-4 Ethylbenzene 1.0 u 1.0 0.19 127-18-4 Tetrachloroethene (PCE) 1.0 u 1.0 0.20

108-88-3 Toluene 1.0 u 1.0 0.10 79-01-6 Trichloroethene (TCE) 1.0 u 1.0 0.15 75-69-4 Trichlorotluoromcthane (CFC I t ) 1.0 u 1.0 0.13 -- -------75-01-4 Vinyl Chloride 1.0 u 1.0 0.14 10061-01-5 cis- I ,3-Dichloropropene 1.0 u 1.0 0.14 156-60-5 trans- I ,2-Dichloroethene 1.0 u 1.0 0.15

10061-02-6 trans-! ,3-Dichloropropene 1.0 u 1.0 0.10

Printed 2123JI S 9:30 FotmiA

1\alprewsOO l \s!arlimsS\LIMSReps\AnalyticaiRepol1 rp!





TRIP BLANK Rl501073-003

Service Request: Rl501073 Date Collected: 2/1211 5 1245 Date Received: 2/13/ 15 Date Analyzed: 2/13/1 5 13;20



Analytical Method: 624 Data File Name: I:\ACQUDA T A \MSVOA6\DA T A \021315\M040 J.D\

Control Surrogate Name %Rec Limits

I ,2-Dichloroethane-d4 96 81-127 4-Bromofluorobenzene 94 79-123 Toluene-d8 96 83-120

Printed 2123/15 9 ;30 Fmm1A

\lalp~wsOO 1\starlimsS\LIMSRcps\AnnlyticaiRcport rpt

Date Analyzed

2{)3/ 15 13:20 2!13/ 15 13:20 2/ 13/ 15 13:20

Q


Dilution Factor: I

SuperSet Reference; tD>8:1.i)6'!1!.raoo




Analytical Report


Service Request: Rl501073 Date Collected: 2112/1 S Date Received: 2/13/15 Date Analyzed: 2/13/15 1320

Volatile Organic Compounds by GC/MS with 3 Day Holding Time for Acrolein, Unpreservcd


TRIP BLANK R I 50 I 073-003


CAS# Analytc Name RT Result Q


Comments:

Printed 02/2312015 9;30 Fonn IB

•l;tlpn:wsOO 1\starlinuS\LtMSRcpsiAnalyticaiTICReport.rpl


SuperSet Reference; ~~ ~ ~ 00

. Client: Project: Sample Matrix:



CAS No.

71-55-6 79-34-5 79-00-5

75-34-3 75-35-4 95-50-1 -- -107-06-2 78-87-5 541-73-1

106-46-7 110-75-8 107-02-8

107-13-1 71-43-2 75-27-4

75-25-2 74-83-9 56-23-5

108-90-7 75-00-3 67-66-3

74-87-3 124-48-1 75-71-8

75-09-2 100-41-4 127-18-4

108-88-3 79-01-6 75-69-4

75-01-4 10061-01-5 156-60-5

10061-02-6

Printed 2123/15 9.30


Analytical Report



Service Request: Rl501073 Date Collected: NA Date Received: NA Date Analyzed: 2/ 13/ 15 12:46



624 Analysis Lot: 432696

I:\ACQUDATA\MSVOA6\DATA\021315\M0400.D\ Instrument Name: R-MS-06 Dilution Factor: I


1, I, 1-Trichloroethane (TCA) 1.0 u 1.0 0. 13

I, I ,2,2-Tetrachloroethane 1.0 u 1.0 0.23 I, I ,2-Trichloroethane 1.0 u 1.0 0.12

-l, 1-Dichloroethane (I , I-DCA) 1.0 u 1.0 0.10

I, 1-Dichloroethene (1 , 1-DCE) 1.0 u 1.0 0 .22

I ,2-Dichlorobenzene 1.0 u 1.0 0.10 ---I ,2-Dichloroethane 1.0 u 1.0 0.18

1 ,2-Dichloropropane 1.0 u 1.0 0.15 1 ,3-Dichlorobenzene 1.0 u 1.0 0.10

I ,4-Dichlorobenzene 1.0 u 1.0 0.15

2-Chloroethyl Vinyl Ether 10 u 10 0.64

Acrolein 10 u 10 0.73

Acrylonitrile 10 u 10 0.37

Benzene 1.0 u 1.0 0.10

Bromodichloromethane 1.0 u 1.0 0.15 - --·-

Bromoform 1.0 u 1.0 0.16

Bromomethane 1.0 u 1.0 0.12

Carbon Tetrachloride 1.0 u 1.0 0.10 ---- -----Chlorobenzene 1.0 u 1.0 0 .13

Chloroethane 1.0 u 1.0 0.15

Chloroform 1.0 u 1.0 0.13 ---Chloromethane 1.0 u 1.0 0.16 Chlorodibromomethane 1.0 u 1.0 0.15 Dichlorodifluoromcthnnc (CFC 12) 1.0 u 1.0 0 .17

Methylene Chloride 1.0 u 1.0 0.18

Ethylbenzene 1.0 u 1.0 0.19

Tetrachloroethene (PCE) 1.0 u 1.0 0.20

Toluene 1.0 u 1.0 0.10

Trichloroethene (TCE) 1.0 u 1.0 0.15 Trichlorofluoromethanc (CFC II) 1.0 u 1.0 0.13

Vinyl Chloride 1.0 u 1.0 0.14

cis-1 ,3-Dichloropropene 1.0 u 1.0 0.14

trans-1 ,2-Dich1oroethene 1.0 u 1.0 0.15

trans- I ,3-Dich1oropropene 1.0 u 1.0 0.10

Form lA

\\alpn:wsOO I \st<~rlimsS\LIMSRcps\AnalytlcaiReport rpt SuperSet Reference I @c(I3U611b rf.Soo





Method Blank RQJ501553-04

Service Request: R 1 50 I 073 Date Collected: NA Date Received: NA Date Analyzed: 2/13/ 15 12:46



Analytical Method: 624 Data File Name: l:\ACQUDATA\MSVOA6\DATA\021315\M0400.D\

Control Surrogate Name •IoRee Limits

1,2-Dichloroethane-d4 95 81-127 4-Bromofluorobenzene 97 79-123 Toluene-dB 99 83-120

Printed 2123/15 9·30 Fo1m lA

\\nlprewsOOI\st:ulimsS\LIMSRcps\AnalytitaiRcpor1.rpl

Date Analyzed

2/ 13/ 15 12:46 2/ 13/ 15 12:46 2/ 13/ 15 12:46

Q


Dilution Factor: I

SuperSet Rercn:ntc: 1 sQotiJ2~~o



Analytical Method:



Analytical Report


Service Request: RISOI073 Date Collected: NA Date Received: NA Date Analyzed: 2/13/ 15 1246


Method Blank Units: flg/L RQISOIS53-04 Basis: NA

624



Comments:

Printed 02123/20 IS 9·30 Form IB

~lalprcwsOOI\st:arlimsS\liMSRcps\Anal}1icalTICRcport tpt SuperSet Reference: Wij'~ 8' 00


Analytical Report




Method Blank RQI501530-0I

Service Request: R 150 I 073 Date Collected: NA Date Received: NA

Date Extracted: 2/ 13/ 15 Date Analyzed: 2/ 18/15 II :20

Units: J..lg/L Basis: NA

Semivolatile Organic: Compounds by GCIMS


CAS No. Analyte Name Result Q

83-32-9 Acenaphthene 5.0 u 208-96-8 Acenaphthylene 5.0 u 120-12-7 Anthracene 5.0 u 92-87-5 Benzidine 100 u 56-55-3 Benz( a )anthracene 5.0 u 50-32-8 Benzo(a)pyrene 5.0 u -- -- ---205-99-2 Benzo(b )fluoranthene 5.0 u 191-24-2 Benzo(g,h, i)perylene 5.0 u 207-08-9 Benzo(k)fluoranthene 5.0 u 85-68-7 Butyl Benzyl Phthalate 5.0 u 84-74-2 Di-n-butyl Phthalate 5.0 u 193-39-5 lndeno( 1 ,2,3-cd)pyrene 5.0 u 111-91-1 Bis(2-chloroethoxy)methane 5.0 u 111-44-4 Bis(2-chloroethyl) Ether 5.0 u 91-58-7 2-Chloronaphthalene 5.0 u 95-57-8 2-Chlorophenol 5.0 u 108-60-1 2,2'-0xybis( 1-chloropropane) 5.0 u 218-0J-9 Chrysene 5.0 u 53-70-3 Dibenz( a,h )anthracene 5.0 u 91-94-1 3 ,3 '-Dichlorobenzidine 5.0 u 120-83-2 2,4-Dichlorophenol 5.0 u 84-66-2 Diethyl Phthalate 5.0 u 131-11-3 Dimethyl Phthalate 5.0 u 105-67-9 2,4-Dimethylphenol 5.0 u 51-28-5 2,4-Dinitrophenol 50 u 121-14-2 2,4-Dinitroto1uene 5.0 u 606-20-2 2,6-Dinitrotoluene 5.0 u -----122-66-7 I ,2-Diphenylhydrazine 5.0 u 117-81-7 Bis(2-ethylhexyl) Phthalate 5.0 u 206-44-0 Fluoranthene 5.0 u 86-73-7 Fluorene 5.0 u 118-74-1 Hexach1orobenzene 5.0 u 87-68-3 Hexachlorobutadiene 5.0 u 77-47-4 Hexachlorocyclopentadiene 5.0 u

Printed 2/23(\ S 9.30 Fonn lA

1\alprc:wsOO 1 lstarlinuS\LlMSRcps\Analytica!Report rpt



MRL MDL Note

5.0 1.0 5.0 1.0 5.0 1.0 ---

100 90 5.0 1.0 5.0 1.0 ----5.0 1.0 5.0 1.0 5.0 1.0

5.0 2.4 5.0 1.0 5.0 1.2

5.0 2.2 5.0 1.3 5.0 1.0

5.0 1.0 5.0 1.0 5.0 1.0

5.0 1.3 5.0 4.5 5.0 1.3

5.0 1.0 5.0 1.0 5.0 1.5 - -50 20 5.0 1.6 5.0 1.8 ----5.0 1.0 5.0 1.2 5.0 1.0

5.0 1.0 5.0 1.0 5.0 1.3

5.0 1.0

SuperSet Reference: ~~~~ rsoo




CAS No.

67-72-1 78-59-1 534-52-1 -- -59-50-7 91-20-3 98-95-3

88-75-5 100-02-7 62-75-9

86-30-6 117-84-0 87-86-5

85-01-8 108-95-2 101-55-3

7005-72-3 621-64-7 129-00-0

120-82-1 88-06-2

Surrogate Name

p-Terphenyl-d 14 N itrobenzene-d5 Phenol-d6


Printed 2123/1 S 9:30


Amliyticnl Report General Electric Company GE -Pittsfield NPDES Water

Method Blank RQ1501530-0I

Semivolatlle Organic Compounds by GC/MS

625 EPA3510C I :\ACQUDA T A \5973 D\Data\02181 5\BA84 7.0\


Hexachloroethane 5.0 u 5.0 Isophorone 5.0 u 5.0 4,6-Dinitro-2-methylphenol 50 u 50

4-Ch I oro-3-methylphenol 5.0 u 5.0 Naphthalene 5.0 u 5.0 Nitrobenzene 5.0 u 5.0

2-Nitropheno\ 5.0 u 5.0 4-Nitrophenol 50 u 50 N-Nitrosodimethylamine 5.0 u 5.0

N-Nitrosodiphenylamine 5.0 u 5.0 Di-n-octyl Phthalate 5.0 u 5.0 Pentachlorophenol (PCP) 50 u 50 ---Phenanthrene 5.0 u 5.0 Phenol 5.0 u 5.0 4-Bromophenyl Phenyl Ether 5.0 u 5.0

4-Chlorophenyl Phenyl Ether 5.0 u 5.0 N-Nitrosodi-n-propylamine 5.0 u 5.0 Pyrene 5.0 u 5.0 -----I ,2,4-Trichlorobenzene 5.0 u 5.0 2,4,6-Trichlorophenol 5.0 u 5.0 Semi Volatile Organic Compounds 5.0 u 5.0


97 40-133 2/ 18/ 15 II :20 89 37-117 2118/ 15 11:20 37 10-107 2/ 18/ 15 I 1:20

83 39-119 2/18/15 II :20 54 10-105 2/ 18/15 11:20 114 28-157 2/ 18115 11:20

Form1A

1\:llprcwsOO llstarlimsS\LIMSRcps\Anal)1icaiRcport.rpt

MDL

1.2 1.0 11

1.2 1.0 1.6

1.4 5.9 1.0

1.0 1.2 6.9

1.0 1.0 2.2

1.2 1.3 1.0

1.0 1.4

0.68

Q

Service Request: R 150 I 073 Date Collected: NA Date Received: NA




Instrument Name: R-MS-54 Dilution Factor: 1

Note

SuperSet Rcfc~ncc : ~~~2 !l;J 00



QNQC Report General Electric Company GE -Pittsfield NPDES Water


Service Request: R1501073 Date Analyzed: 2/1 3115


Analytical Method: 624 Units: J!g/L Basis: NA



Spike %Rec Analyte Name Result Amount %Rec Limits

I, 1,1-Trichloroethane (TCA) 17.7 20.0 88 52- 162 I, I ,2,2-Tetrachloroethane 17.9 20.0 90 46- 157 I, I ,2-Trichloroethane 19.3 20.0 97 52- 150

I, 1-Dichloroethane (I, I-DCA) 17.4 20.0 87 59- 155 I, 1-Dichloroethene (I, 1-0CE) 18.6 20.0 93 10-234 I ,2-Dichlorobenzene 19.8 20.0 99 18- 190

I ,2-Dichloroethane 17.7 20.0 89 49- 155 I ,2-Dichloropropane 16.8 20.0 84 10-210 1,3-Dichlorobenzene 20.1 20.0 100 59- 156

I ,4-Dichlorobenzene 19.4 20.0 97 18- 190 2-Chloroethyl Vinyl Ether 18.9 20.0 95 10- 305 Acrolein 73.2 100 73 10- 186

Acrylonitrile 103 100 103 84- 128 Benzene 18.3 20.0 91 37- 151 Bromodichloromethane 19.9 20.0 100 35- 155

Bromoform 22.5 20.0 113 45- 169 Bromomethane 17.4 20.0 87 10-242 Carbon Tetrachloride 20.7 20.0 104 70- 140

Chlorobenzene 18.9 20.0 94 37- 160 Chloroethane 17.0 20.0 85 14-230 Chlorofonn 18.8 20.0 94 51 - 138

Chloromethane 18.5 20.0 93 10-273 Chlorodibromomethane 21.7 20.0 108 53- 149 Dichlorodifluoromcthanc (CFC 12) 18.5 20.0 92 64- 130

Methylene Chloride 18.2 20.0 91 10-221 Ethylbenzene 18.1 20.0 91 37- 162 Tetrachloroethene (PCE) 19.8 20.0 99 64- 148

Toluene 18.6 20.0 93 47-150 Trichloroethene (TCE) 20.3 20.0 101 71- 157 Trichlorofluoromethanc (CFC II) 18.8 20.0 94 17- 181

Vinyl Chloride 18.3 20.0 92 10-251 cis-1,3-Dichloropropene 19.2 20.0 96 10-227 trans-1 ,2-Dichloroethene 18.4 20.0 92 54- 156

Resulu Ragged \l'ith a n asterlsk (*)Indicate valu~ ouuide control criteria.

Percent rctO\'Cric! and rcl~tivc percent differences (RPD} arc determined by the sofiware using values in the cal, ulat1on \\hich have not been rounded

Printed 2123/1 S 9:30 Form JC

1\alprcwsOOIIstarlim'$\I..IMSRc:p'll.abConlroiS:unplc.rpl



QNQCRc:port



Service Request: RI501073 Date Analyzed: 2113/ 15



Analyte Name

trans· I ,3-Dichloropropene



20.3 20.0 102

Results flagged with an aSieriJk (")Indicate values outside control criteria.

%Rec Limits

17- 183



Percent recoveries and relative percent differences (RPD) are detenn1ncd by the software us1ng \'lllues in the c:alculation which have not been rounded

Printed 212311 S 9 30 Form JC

'.lalprewsOOIIstarlimsS\LIMSRcps\LabControiSarnplc.rpt SuperSet Reference: I S9~~W


QNQC Report

Client: General Electric Company Service Request: Rl501073 Project: GE -Pittsfield NPDES Date Analyzed: 2/18!15 Sample Matrix: Water

Lab Control Sample Summary Semivolatlle Organic Compounds by GC/MS

Analytical Method: 625 Units: llgiL Prep Method: EPA 3510C Basis: NA


Lab Control Sample Duplicate Lab Control Sample RQ1501530-02 RQ1501530-03

Spike Spike 0/e Rec RPD Analyte Name Result Amount %Rec Result Amount %Rec Limits RPD Limit

Acenaphthene 92.1 100 92 93.6 100 94 47- 145 2 30 Acenaphthylene 93.4 100 93 96.0 100 96 33- 145 3 30 Anthracene 94.3 100 94 98.1 100 98 27- 133 4 30

Benzidine 100 u 100 0 • 100 u 100 0 • 10- 169 NC 30 Benz( a )anthracene 96.9 100 97 99.6 100 100 33- 143 3 30 B enzo( a )pyrene 96.7 100 97 104 100 104 17- 163 7 30

Benzo(b )fluoranthene 95.8 100 96 102 100 102 24- 159 6 30 Benzo(g,h,i)perylene 98.8 100 99 100 100 100 10-219 I 30 Benzo(k)fluoranthene 89.3 100 89 92.8 100 93 II- 162 4 30

Butyl Benzyl Phthalate 104 100 104 113 100 113 10- 152 8 30 Di-n-butyl Phthalate 109 100 109 113 100 113 10- 118 3 30 Indeno( I ,2,3-cd)pyrene 97.6 100 98 100 100 100 10- 171 3 30

Bis(2-chloroethoxy)methane 71.0 100 71 74.3 100 74 33- 184 5 30 Bis(2-chloroethyl) Ether 76.7 100 77 77.2 100 77 12- 158 <I 30 2-Chloronaphthalene 83.2 100 83 82.3 100 82 60- 118 I 30

2-Chlorophenol 85.2 100 85 85.1 100 85 23- 134 < I 30 2,2'-0xybis( 1-chloropropane) 76.4 100 76 75.9 100 76 36- 166 < I 30 Chrysene 95.2 100 95 98.5 100 99 17- 168 3 30

D i benz( a,h )anthracene 97.2 100 97 102 100 102 10-227 5 30 3,3'-Dichlorobenzidine 76.7 100 77 83.1 100 83 10-262 8 30 2,4-D ichloropheno I 76.9 100 77 78.2 100 78 39 - 135 2 30

Diethyl Phthalate 112 100 112 118 100 118 • 10- 114 5 30 Dimethyl Phthalate 105 100 105 107 100 107 10- 112 3 30 2,4-Dimcthylphenol 78.5 100 78 80.6 100 81 32- 119 3 30

2,4-Dinitrophenol 83.9 100 84 74.9 100 75 10- 191 II 30 2,4-Dinitrotoluene 108 100 108 110 100 110 39- 139 2 30 2,6-Dinitrotoluene 101 100 101 104 100 104 50- 158 3 30

I ,2-Diphenylhydrazine 96.1 100 96 96.4 100 96 57- 117 < I 30 B is(2-ethylhexyl) Phthalate 112 100 112 117 100 117 10- 158 5 30 Fluoranthene 103 100 103 106 100 106 26- 137 3 30

Fluorene 96.1 100 96 97.1 100 97 59- 121 30 Hexachlorobenzene 97.5 100 97 97.0 100 97 10- 152 <I 30 Hexach lorobutad iene 50.4 100 50 44.3 100 44 24- 116 13 30

Results n11gged ,.·ith an asterisk (*) Indicate VDiucs outside control criteria.

Percent recoveries and relauvc pcn:cnt diiTcn:nccs (RPD) arc determined by the sofiware using values in the •alculation which ha\·e not been rounded

Printed 2123/1 S 9-30 Form 3C

\lalpn:wsOOI\starlimsS\l.IMSReps\LabControiSamplc.IJlt SuperSet Reren:n•c: I'Jl<e~6?! .goo


QNQC Report


Project: GE -Pittsfield NPDES Date Analyzed: 2/18115



Analytical Method: 625 Units: Jlg/L



Lab Control Sample Duplicate Lab Control Sample RQ1501530-02 RQ 1501530-03


Analytc Name Result Amount % Rec Result Amount 0/o Rec: Limits RPD Limit

Hexachlorocyclopentadiene 68.3 100 68 68.3 100 68 28-98 < I 30


Isophorone 76.5 100 76 80.8 100 81 21 - 196 5 30

4,6-Dinitro-2-methylphenol 90.0 100 90 99.3 100 99 10- 181 10 30

4-Chloro-3-methylphenol 85.1 100 85 87.9 100 88 22- 147 3 30

Naphthalene 54.1 100 54 48.9 100 49 21 - 133 10 30

Nitrobenzene 74.2 100 74 75.8 100 76 35- 180 2 30

2-Nitrophenol 73 .3 tOO 73 74.7 100 75 29- 182 2 30

4-N itrophenol 61.3 100 61 78.8 100 79 10- 132 25 30

N-Nitrosodimethylamine 59.9 100 60 57.8 tOO 58 33-70 4 30

N-Nitrosodiphenylamine 97.0 too 97 99.3 100 99 so-t 17 2 30

Di-n-octyl Phthalate 113 100 113 119 100 119 10- 146 s 30

Pentachlorophenol (PCP) 81.7 tOO 82 84.3 100 84 14- 176 3 30

Phenanthrene 98.9 100 99 104 100 104 54- 120 5 30

Phenol 44.2 too 44 40.4 tOO 40 10. 112 9 30

4-Bromophenyl Phenyl Ether 95.4 100 95 97.8 100 98 53. 127 3 30

4-Chlorophenyl Phenyl Ether 98.7 100 99 lOt 100 101 25. 158 2 30

N-Nitrosodi-n-propylamine 92.3 100 92 92.5 100 93 10.230 <I 30

Pyrene 101 100 101 106 100 106 52- 115 5 30

I ,2,4-Trichlorobenzene 46.6 100 47 41.5 100 41 29.85 12 30

2,4,6-Trichlorophenol 100 tOO 100 102 tOO 102 37- 144 I 30

Rc:sulu naued with an astcruk (*)Indicate values outside control criteria.

Percent recoveries and relative percent diffcrcnc~ (RPO) arc dctcnnincd by the S(lfiw:are using \OIIucs in the calculation which h:a\·e not been rounded.

Printed 2123/1 S 9:30 Form3C

llalprcwsOOIIstarlims$\LIMSRcps\UbControiSamplc rpt SuperSet Reference l Jloti~Jt}c;Q2,~

A enulronmental CHAIN OF CUSTODY/LABORATORY ANALYSIS REQUEST FORM 19391

1565 Jefferson Road, Building 300, Suite 360 • Rochester, NY 14623 1 +1 585 288 5380 +1 585 288 8475 (fax) PAGE / OF /

""'fece_,. NPDES Permit ""'feceNumbet ANALYSIS REQUESTED (Include Method Number end Container Preserva tive)

f'n>lect MaNoer Sean Coyle Ro!>o<1 cc PRESERVATIVE I 0 I 0 l ---r

~~--Veolia Environnement NA (GE CEP}

1000 East St.

Pittsfield MA 01201 -· Email

41~4-6709 ~ 1 413-494-7052 ;.

CUENT SAMPLE 10

(1}006D-1Q2M-1X-GV

_(~)006D-1Q2M-2X·GS

(l)Trip Blank

SP£CIAL INSTRUCT10NSICOMMENTS

Metlls

- ~:;;~1.5X:v71fau /(_ FOROFAC!US!

ONl.YLABID ~w;; ... ,{ Ll • .,

I J; _ £____~~---~

..... . -~

.... -.. ~-fiO"'U- -.... ~

~ .-A.t .. --.~

rv·a·~;i ·~ ...IS.~. --~~

I" ·~-:- ..... -.5"~

:::_~~-~

t:"'?,·'~:!'l

SAMPLING DATE TIME I MATRIX

2/l.UlS I J'J-1/6~ H,Q 13 2/12/iSI a#'5J- I H20 11 2/12/15 I /1//.lf,_ I H20 13

PA 6Z4 & 6Z5 list Included with COC's Samples packed In ice

See OAPP 0

I '!rATE WHERE SAMPLE~ WERE COLI:.fCTED RECEIVEOBY REUNQUISHED BY

Cl)

ffi z

~ 8

i ~~~~9~~-·'~--0"' &~0"' 111:10~ l~-rtt ~ ~ 0<1}', ,IJ:; &~ IJqr tf!g, ~~~~~ eo ""o 0 0 0

X

X X

TURNAROUND REQUIREMENTS

--RUSH (SURCHARGES APPLY}

--1 doy """"X2 cloy -:!day

--~day --!.!.5 day

REQUESTED REPORT DATE

RECEIVED BY

REPORT REQUIREMENTS

__ I. ResUI5 Clrtf

__ n. ReoUts + oc s..mw~es (I..CS, DUP, I.ASIMSD .. rwqui<ed)

--lit R-'ls + OC Mel Calbrallon &.TwNrlcs

Praservatlve Key 0. NONE 1. HCL 2. HNO:J 3. H2SO~ 4. NaOH 5. Zn. Acalale 6. MeOH 7. NaHS04 a. Other __

REMARI<SI ALTERNATE DESCRIPTION

INVOICE INFORMAnON

POt

Bill TO:

~IV: DeJa Varidallon Repclfl wiUI Raw IIIIa I------------......

Edata __ V. _ _ No

REUNOUISHED BY RECEIVED BY

Slgna11n 111nt r """""hn

PmtedName R1501 073 5 ~~~-~~~~~---~-----f:.:::--- VeollaWoltrNorthAmtrtca

F&m :r.;- 0.1~~ Uitil/iiiiilifll~~ IIIII Ulllllll IIIII tm 1111

Olslrlbullon: White - lab Copy; Yelow • Return to Originator 10 2012 by ALS Group

, R1501073 5 Vtolla Water North America

iimiliiiiiliillilillt\111111\ 111111111111111111 A . Co~ler receipt and Preservation Check Form

Project/Client (f- eJJ-1~ d Folder Number .U >-LSI"

Coolerreceivedo:it3··\S by:~ COURIER: ALS UPS QE~VELOCITY CLIENT -1 Were Custody seals on outside of cooler? !)N 5a Perchlorate samples have required headspace? y N~ 2 Custody papers properly completed (ink, signed)? ~N 5b Did VOA vials, Alk,or Sulfide have sig• bubbles? Y~A

3 Did all bottles arrive in good condition (unbroken)? ~N 6 Where did the bottles originate? (ALSIR_s)e CLIENr --4 Circle:~ Dry Ice Gel packs present? I~ 7 Soil VOA received as: Bulk Encore 5035set (. NA )

8. Temperature Readings Date:d-13-15 Time: 1 D: 45 ID: IR#3 @;7 From: Temp Blank ~ample B~ Observed Temp (OC) tl.~ Correction Factor eq -'d. Corrected Temp (0 C) (j, L/

Within 0-6°C? (Y N y N y N y N y N y N y N -


&Client Approval to Run Samples: Standing Approval Client aware at drop-off Client notified by:------

PC Secondary Review:

Cooler Breakdown: Date: ,.~ \S" Time: \1.\(\,} by:_..;;.;l\'-'"1'----:;::!~:-----:-:-=---

1. Were all bottle labels comple e {i.e. analysis, preservation, etc.)? ~ NO 2. Did all bottle labels and tags agree with custody papers? NO 3. Were correct containers used for the tests indicated? S NO 4. Air Samples: Cassettes I Tubes Intact Canisters Pressurized Tedlar® Bags Inflated E I. d' xp.am an tscreoanctes: pH Reagent Yes No Lot Received Exp Sample ID Vol. Lot Added Final

Added pH

~12 NaOH 52 HN01 52 H1S04 <4 NaHS04 Residual ForCN If+, contact PM to Chlorine Phenol add Nalslol (CN),


Na2S20l - -ZnAcetate - - • "'Not to be tested before analysis - pH tested and HCl ... •t recorded by VOAs on a separate worksheet

Yes= All samples OK


PMOK to Adjust:

Bottle lot numbers: __ 94

· :1@1:-~r::~~=· ,._-~~__;IL:\X:H~·:;:;.:..Ij.~,;-;....utP,:.LlLio..l\"._ ____________________ _

Other Comments: I

PC Secondary Review: __ Nl~·-, ___ _ .,.

•significant air bubbles: VOA >5-6 mm : WC > 1 in. diameter

P;\INTRANEl\QAQCIForms Controlled\Cooler Receipt t7 .doc S/6114 0'3026

t

February 25, 2015


1000 East Street Pittsfield, MA 01201


Dear Mr. Coyle:


Analytical Report for Service Request No: Rl501144

Enclosed are the results of the sample(s) submitted to our laboratory on February 18, 2015. For your reference, these analyses have been assigned our service request number R1501144.






F I GI-lT SOLUTIONS

Page 1 of jtj

RIGHT PARTNER



LabiD Client 10 R 1501144-001 0060-1 Q2M-2X-GV

R1501144-002 Trip Blank

All samples were received in good condition unless otherwise noted on the cooler receipt and preservation check form located at the end of this report.

All samples were preserved in accordance with approved analytical methods.

All samples have been analyzed by the approved methods cited on the analytical results pages.

All holding times and associated QC were within limits.

No analytical or QC problems were encountered.

All sampling activities performed by ALS personnel have been in accordance with "ALS Field Procedures and Measurements Manual" or by client specifications.

\lalprews001\starlimsSILIMSReps\CaseNarralive.rpt

A Enuiraflmental

u

J

B

E

E

D

•

H

#



N Inorganics- Matrix spike recovery was outside corrected for dilution and for percent moisture, unless otherwise noted in the case

laboratory limits.



Tentatively Identified Compound (TIC) or s Concentration has been determined using Method that the concentration is between the MRL of Standard Additions (MSA). and the MDL. Concentrations are not verified w Post-Digestion Spike recovery is outside control within the linear range of the calibration. For DoD: concentration >40% difference between

limits and the sample absorbance is <SO% of the



method blank nt a concentration that may between the two GC columns.

have contributed to the sample result. c Confirmed by GC/MS

Inorganics- Concentration is estimated due to Q DoD reports: indicates a pesticide/Aroclor is not the serial dilution was outside control limits. confirmed (:!: I 00% Difference between two GC



Concentration is a result of a dilution, MRL Method Reporting Limit. Also known as: typically a secondary analysis of the sample LOQ Limit ofQuantitation (LOQ) due to exceeding the calibration range or that The lowest concentration at which the method a surrogate has been diluted out ofthe sample analyte may be reliably quantified under the and cannot be assessed. method conditions.


Analysis was performed out of hold time for LOD Limit of Detection. A value at or above the MDL tests that have an "immediate" hold time which has been verified to be detectable. criteria. NO Non-Detect. Analyte was not detected at the Spike was diluted out. concentration listed. Same as U qualifier.


Analyses were conducted in accordance with Massachusetts Department of Environmental Protection certification

standards, except as noted in the laboratory case narrative provided. A copy of the current Department issued parameter list is included in this report.

-~·."t"t:T4S...'\'-".t~·~-=:t"~r.:::.··:.:.;.;-.o;..::.·~::..l=.-s.-=:..~~~.,..1=.::·-n.~~cA-'~~n=..~~~~~

r{! G H l 1

;: Ci L I J ·r f :~ :,; S i F 1 c; H 'f Pi\ f( ·r ~: E H

P.\INTRANE1\QAQOForms Controlled\QUALIF _routine forMA rl.DOC stJ:Iihaaa 3

The . Com1nonweal~h of Massa_chuse,tts

Depart1nent of Envil·on1nental Protection Division of Environmental A~talysis

Senator William X Wall Experimen( Station

M-NY032

certifies

' ALS ENVIRONMENTAL ROCHESTER 1565 JEFFERSON RD BUILDING 300, SUITE 360 ROCHESTER, NY 14623-0000


. for tlte analysis ·of NON· POT ABLE WATER (CHEMISTRY)

pursu~nt to ~10 CMR 42.00

This certificate supersedes all previous Massachuselt"s certificates issued to this laboratory. The laboratory is regulated by and shall be responsible for being in compliance with Ma_ssachusetts regulations at 310 CMR 42.00. ·

This certificate is valid only lflhen accompanied by the l0;test dated Certified Parameter List issued by the Massachusetts b.E.P. Colltact the Division' a/Environmental Analysis to verify the current certification status of the labqrqtory.

Certification is 'no guarantee of the validity of the data. This certification is subject to unannounced laboratory inspections.

Issued: ~~ JUL2014

Expires: 30 JUN 2015

Dtre~tor, Division of Environmental Analysis

00004



M-NY03l ALS ENVIRONMENTAL ROCHESTER ROCHESTER NY


Analytes

ALUMINUM

ANTIMONY

ANTIMONY

ARSENIC

ARSENIC

BERYLLIUM

BERYLLIUM

CADMIUM

CADMIUM

CHROMIUM

CHROM,UM

COBALT

COBALT

COPPER

COPPER

IRON

LEAD

LEAD

MANGANESE

MANGANESE

MERCURY

MOLYBDENUM

MOLYBDENUM

NICKEL

NICKEL

SELENIUM

SELENIUM

SILVER

SILVER

THALLIUM

THALLIUM

VANADIUM

VANADIUM

ZINC

ZINC




CALCIUM

MAGNESIUM

SODIUM

POTASSIUM

ALKALINITY, TOTAL

June 26, 2014

Effective Date

01 JUL2014

*=Provisional Certification


Methods

EPA200.7

EPA200.7

EPA200.B

EPA200.7

EPA200.8

EPA200.7

EPA200.B

EPA200.7

EPA200.8

EPA2PQ.7

EPA200.8

EPA200.7

EPA200.8

EPA200.7

EPA200.8

EPA200.7

EPA200.7

EPA200.8

EPA200.7

EPA200.8

EPA245.1

EPA200.7

EPA200.S

EPA200.7

EPA200.8

EPA200.7

EPA200.8

EPA200.7

EPA200.8

EPA200.7

EPA200.8

EPA200.7

EPA200.8

EPA200.7

EPA200.8

EPA 120.1

SM2540C

SM2340C

EPA200.7

EPA200.7

EPA200.7

EPA200.7

SM2320B

Page 1 of 2

oeaes


CerUned Parameter List as of:


ROCHESTER NY


Analytes

CHLORIDE

CHLORIDE

FLUORIDE

SULFATE

AMMONIA·N

NITRATE-N

NITRATE·N

KJELDAHL-N

ORTHOPHOSPHATE

PHOSPHORUS, TOTAL




CYANIDE, TOTAL


OIL AND GREASE

PHENOLICS, TOTAL


VOLATILEHALOCARBONS

VOLATILE AROMATICS

VOLATILE AROMATICS

SVOC.ACID EXTRACT ABLES

SVOC·BASEINEUTRAL EXTRACT ABLES

POLYCHLORINATED BIPHENYLS {WA TEF

Effective Date

01 JUL2014 -

01 JUL:Z014

June 26, 2014 *=Provisional Certlflcatlon

Expiration 30JUN2015 Date

Metbods

SM 4500-CL·E

EPA300.0

EPA 300.0

EPA300.0

EPA350.1

EPA300.0

EPA353.2

EPA351 .2

EPA365.1

E_PA365.1

EPA410.4

SM 52108

SM5310C

EPA335.4

SM2540D

EPA 1664

EPA420.4

EPA601

EPA624

EPA602

EPA624

EPA625

EPA625

EPA608

Page 1 of 2

0'3006




Analytical Report


0060-1 Q2M-2X-GV RI501144-00J

Service Request: R1501144 Date Collected: 2117/ 15 1315 Date Received: 2118/ 15 Date Analyzed: 2/ 19/1 5 12:40






71-55-6 I, I, 1-Trichloroethane (TCA) 1.0 u 1.0 0.13


79-00-5 I, I ,2-Trichloroethane 1.0 u 1.0 0.12

75-34-3 I, 1-Dichloroethane (I, I-DCA) 1.0 u 1.0 0.10


95-50-1 I ,2-Dichlorobenzene 1.0 u 1.0 0.10

107-06-2 I ,2-Dichloroethanc 1.0 u 1.0 0.18


541-73-1 I ,3-Dichlorobenzenc 0.18 J 1.0 0.10 --

106-46-7 I ,4-Dichlorobenzcne 1.4 1.0 0.15

110-75-8 2-Ch1oroethyl Vinyl Ether 10 u 10 0.64

107-02-8 Acrolein 10 u 10 0.73


71-43-2 Benzene 1.0 u 1.0 0.10

75-27-4 Bromodichloromethane 0.15 J 1.0 0.15 --

75-25-2 Bromoform 1.0 u 1.0 0.16

74-83-9 Bromomethane 1.0 u 1.0 0.12


108-90-7 Chlorobenzene 0.15 J 1.0 0.13

75-00-3 Chloroethane 1.0 u 1.0 0.15

67-66-3 Chloroform 0.85 J 1.0 0.13

74-87-3 Chloromethane 1.0 u 1.0 0.16


75-71-8 Dichlorodifluoromcthanc (CFC 12) 1.0 u 1.0 0.17 ---75-09-2 Methylene Chloride 1.0 u 1.0 0.18 100-41-4 Ethylbenzene 1.0 u 1.0 0.19

127-18-4 Tetrachloroethene (PCE) 1.0 u 1.0 0.20 -108-88-3 Toluene 1.2 1.0 0.10


75-69-4 Trichlorofluoromcthanc (CFC II) 1.0 u 1.0 0.13

75-01-4 Vinyl Chloride 1.0 u 1.0 0.14 10061-01-5 cis- I ,3-Dichloropropene 1.0 u 1.0 0.14

156-60-5 trans-1,2-Dichloroethene 1.0 u 1.0 0.15

10061 -02-6 trans-1,3-Dichloropropene 1.0 u 1.0 0.10

Printed 212511 S 9 46 Foon lA eeoe7 \\:llprcws001\st:ulimsS\LIMSRep5\Analytica1Report.rpt SuperSet Reference: IS..000032214S rcvOO




Analytical Report


0060-1 Q2M-2X-GV R1501144-00l

Service Request: Rl501144 Date Collected: 2/17/1 5 1315 Date Received: 211 8115 Date Analyzed: 2/ 19115 12:40


Volatile Organic Compounds by GC/MS with 3 Day Holding T ime for Acrolein, Unpreserved



Dilution Factor: I


1 ,2-Dichlorocthane-d4 102 81-127 211 9115 12:40 4-Bromo tl uorobenzene 100 79-123 2fl 9115 12:40

Toluene-dB 103 83-120 2/1 9/ 15 12:40 ----

Printed 2125/15 9:46 Focm lA 9 9 9 0 8

1\alprewsOO llsl:~tlimsS\LIMSReps\Analylic:~lReport rpt SuperSet Reference 15..0000322145 n:v 00



General Electric Company GE ·Pins field NPDES Water

Analytical Report


Service Request: R1501 144 Date Collected: 2/17/15 Date Received: 2/18/15 Date Analyzed: 211 9/15 1240

Volatile Organic Compounds by GC/MS with 3 Day Holding Time ror Acrolein, Unpreserved


0060·1 Q2M·2X-GV RISOI 144-001





Comments:

Printed 02/25/2015 9A6 Form lB t:Jf3Q09

\lalprewsOO I \starlimsS\I.IMSR¢1'ls\Anal)1icaiTICReport.rpt SuperSet Rcrcrcncc: IS·000032214S rev 00




Analytical Report


Trip Blank RJ501 144-002

Service Request: Rl501 144 Date Collected: 2/ 17/ 15 1315 Date Received: 2118115 Date Analyzed: 2119115 12:08






71-55-6 I, I, I-Trichloroethane (TCA) 1.0 u 1.0 0.13

79-34-5 1,1 ,2,2-Tetrachloroethane 1.0 u 1.0 0.23

79-00-5 1, I ,2-Trichloroethane 1.0 u 1.0 0.12 - - --

75-34-3 I, I -Dichloroethane (I, I -DCA) 1.0 u 1.0 0.10

75-35-4 1, 1-Dichloroethene (I, I -DCE) 1.0 u 1.0 0.22

95-50-1 1,2-Dichlorobenzene 1.0 u 1.0 0.10



54 t-73-1 1 ,3-Dichlorobenzene 1.0 u 1.0 0.10

106-46-7 1 ,4-Dichlorobenzene 1.0 u 1.0 0.15

I 10-75-8 2-Chloroethyl Vinyl Ether 10 u 10 0.64

107-02-8 Acrolein 10 u 10 0.73

107-13-t Acrylonitrile IOU 10 0.37

71-43-2 Benzene 1.0 u 1.0 0.10


75-25-2 Bromoform 1.0 u 1.0 0.16

74-83-9 Bromomethane 1.0 u 1.0 0.12


108-90-7 Chlorobenzene 1.0 u 1.0 0.13

75-00-3 Chloroethane 1.0 u 1.0 0.15

67-66-3 Chloroform 1.0 u 1.0 0.13

74-87-3 Chloromethane 1.0 u 1.0 0.16

124-48-1 Chlorodibromomethanc 1.0 u 1.0 0.15

75-71-8 DichlorodiOuoromethanc (CFC 12) 1.0 u 1.0 0.17


127-18-4 Tetrachloroethene (PCE) 1.0 u 1.0 0.20 - - ---108-88-3 Toluene 1.0 u 1.0 0.10


75-69-4 Trichloronuoromcthanc (CFC II) 1.0 u 1.0 0.13

75-01-4 Vinyl Chloride 1.0 u 1.0 0. 14

10061-01-5 cis- I ,3-Dichloropropene 1.0 u 1.0 0.14

156-60-5 trans- I ,2-Dichloroethene 1.0 u 1.0 0.15 -


Printed 2125/ 15 9:46 Fotrn lA OI~HJ10

1\alprewsOOI 1st:~rlnnsS\LIMSReps\An31)1Jc31Report . rpt SuperSet Reference. )j.Q00032214S rev 00




Anal}1ical Report


Trip Blank Rl501144-002

Service Request: Rl501144 Date Collected: 211 7/ 15 1315 Date Received: 2118/15 Date Analyzed: 2/ 19/15 12:08


Volatile Organic Compounds by GC/MS with 3 Day Holding Time ror Acrolein, Unpreservcd

Analytical Method: 624 Data File Name: l:\ACQUDATA\MSVOA6\DATA\021915\M0453.D\

Printed 2125115 9.46 Form lA

1.\:llprcwsOOII.st~rlimsS\l.IMSRcps\AnalyticaiRcport rpt


Dilution Factor: I

SuperSet Reference. lj.()00032214S rcvOO




Analytical Report


Service Request: Rl501144 Date Collected: 2/ 17115 Date Received: 2118/ 15 Date Analyzed: 2/J 9/ 15 1208



Trip Blank RISOI144-002




Commt nts:

Printed 0212512015 9:46 Fonn 113

ll:llprcwsOOI\starlimsS\LIMSRcpsiAnal)1ic3ITICReport rpl SuperSet Reference:

Units: pg/L Basis: NA

Oc:J012 15..0000322145 revOO




Analytical Report


Method Blank RQ 1501806-04

Service Request: R1501144 Date Collected: NA Date Received: NA Date Analyzed: 2/ 1911 5 11:34






71-55-6 I, 1,1-Trichloroethane (TCA) 1.0 u 1.0 0.13

79-34-5 1, 1,2,2-Tetrachloroethane 1.0 u 1.0 0.23

79-00-5 1, 1,2-Trichloroethane 1.0 u 1.0 0.12

75-34-3 1, 1-Dichloroethane (I, I-DCA) 1.0 u 1.0 0.10

75-35-4 1,1-Dichloroethene (I, 1-DCE) 1.0 u 1.0 0.22

95-50-1 I ,2-Dichlorobenzene 1.0 u 1.0 0.10 ---107-06-2 I ,2-Dichlorocthane 1.0 u 1.0 0.18

78-87-5 1,2-Dichloropropane 1.0 u 1.0 0.15

541-73-1 I ,3-Dichlorobenzene 1.0 u 1.0 0.10 -.-.-- -106-46-7 I ,4-Dichlorobenzene 1.0 u 1.0 0.15


107-02-8 Acrolein 10 u 10 0.73

107-13-1 Acrylonitrile 10 u 10 0.37 71-43-2 Benzene 1.0 u 1.0 0.10


75-25-2 Bromoform 1.0 u 1.0 0.16

74-83-9 Bromomethane 1.0 u 1.0 0.12


108-90-7 Chi oro benzene 1.0 u 1.0 0.13

75-00-3 Chloroethane 1.0 u 1.0 0.15

67-66-3 Chloroform 1.0 u 1.0 0.13

74-87-3 Chloromethane 1.0 u 1.0 0.16


75-71-8 DichlorodiOuoromcthanc (CFC 12) 1.0 u 1.0 0.17 ---

75-09-2 Methylene Chloride 1.0 u 1.0 0.18

100-41-4 Ethylbenzene 1.0 u 1.0 0.19

127-18-4 Tetrachloroethenc (PCE) 1.0 u 1.0 0.20

108-88-3 Toluene 1.0 u 1.0 0.10


75-69-4 Trichloronuoromcthanc (CFC II) 1.0 u 1.0 0.13

75-01-4 Vinyl Chloride 1.0 u 1.0 0.14

10061-01-5 cis-1,3-Dichloropropene 1.0 u 1.0 0.1 4

156-60-5 trans- I ,2-Dichloroethene 1.0 u 1.0 0.15


Printed 2/2511 S 9 46 Fotm lA

\\:llprcwsOOI\Jt~rlims$\LIMSRcps\AnalyticaiRcpon rpl SuperSet Reference· 15.0000322145 rcvOO




Analytical Report


Method Blank RQ 150 I 806-04

Service Request: R 1501144 Date Collected: NA Date Received: NA Date Analyzed: 211911 5 II :34





Dilution Factor: 1

Control Date


I ,2-Dichloroethane-d4 101 81-127 2/ 19/ 15 11 :34

4-Bromo fluorobenzene 100 79-123 2/ 19/ 15 11:34

Toluene-d8 102 83-120 2/19/ 15 11 :34

Printed 212511 S 9.46 fonn lA Oec:J 14

\lalprcwsOO I \starlimsS\l.IMSRcps\Anal)1icaiRcportrpl SuperSet Rcfc:rcncc IS-0000322145 "'v 00




Analytical Report


Service Request: R1501144 Date Collected: NA Date Received: NA Date Analyzed: 2/19/ 15 1134



Method Blank RQ 1 50 I 806-04



Units: ~giL

Basis: NA


Comments:

Printed 02125120 I 5 9 46 Form I B C) C) C) 15

\\alprcwsOO llstO!tlimsS\l.IMSRcps\An~lytic~ITICReport.rpt SuperSet Reference IS-0000322145 rcvOO



QNQC Report



Service Request: R1501144 Date Analyzed: 2/ 19/ 15


Analytical Method: 624 Units: l!g/L Basis: NA


Lab Control Sample RQ1501806-03

Spike %Rec

Analytc Name Result Amount %Rec Limits

1, 1,1· Trichloroethane (TCA) 20.1 20.0 100 52. 162

1, 1 ,2,2· Tetrachloroethane 19.3 20.0 96 46. 157

I, 1 ,2-Trichloroethane 20.6 20.0 103 52. 150

I, 1-Dichloroethane (I, I -DCA) 20.2 20.0 101 59- 155

1,1-Dichloroethene (I, I -DCE) 21.5 20.0 107 10.234

I ,2-Dich lorobenzene 19.8 20.0 99 18- 190

1,2-Dichloroethane 18.4 20.0 92 49. 155

1,2-Dichloropropane 20.2 20.0 101 10-210

I ,3-Dich lorobenzene 19.7 20.0 98 59. 156

I A-Dichlorobenzene 19.5 20.0 97 18. 190

2-Chloroethyl Vinyl Ether 20.0 20.0 100 10.305

Acrolein 79.6 100 80 10- 186

Acrylonitrile 112 100 112 84. 128

Benzene 21.5 20.0 107 37-151

Bromodichloromethane 22.3 20.0 112 35. 155

Bromoform 22.9 20.0 114 45- 169

Bromomethane 20.2 20.0 101 10-242

Carbon Tetrachloride 22.3 20.0 112 70. 140

Ch lorobenzene 20.5 20.0 102 37. 160

Chloroethane 21.6 20.0 108 14-230

Chloroform 20.3 20.0 101 51- 138

Chloromethane 26.5 20.0 132 10-273

Chlorodibromomethane 22.3 20.0 112 53- 149 Dichlorodilluoromcthanc (CFC 12) 24.3 20.0 121 64- 130

Methylene Chloride 21.5 20.0 107 10-221

Ethyl benzene 20.1 20.0 101 37- 162

Tetrachloroethene (PCE) 19.9 20.0 100 64- 148

Toluene 21.1 20.0 106 47. ISO

Trichloroethene (TCE) 21.0 20.0 105 71 - 157 Trichlorolluoromcthanc {CFC 11) 20.7 20.0 103 17- 181

Vinyl Chloride 24.3 20.0 122 10-251

cis- I ,3-Dichloropropene 22.0 20.0 110 10.227

trans- I ,2-Dichloroethene 21.3 20.0 106 54- 156

Results naggrd 1\'lth An Astrrisk (") lndlcatr \'al~~n outside control critrria.

Pcrc:cnt recoveries and relative percent d•ITcrcnc:rs (RPO) arc determined by the software ul ing values in the calculation which ha\·c: not been rounded

Printed 212SfiS 9.46 FonnlC S6016

\\alprewsOOI\starlimsS\l.IMSRcps\LabControiSrunple rp1 SuperSet Reference 15-0000322145 revOO



QNQC Report



Service Request: Rl501144 Date Analyzed: 2/ 19{15

Volatile Organic: Compounds by GC/MS with 3 Day Holding Time for Acrolein, Unpreserved


Analytc Name

trans-1 ,3-Dichloropropene


Spike Result Amount •1o Rec

22.8 20.0 114

Results Oag~:ril " ·lth lin asterisk (•) lndiutr \~lues outside control criteria.

% Rcc Limits

17- 183

Units: J.ig/L Basis: NA


Pen:cnt recoveries and relative percent di!Teren•cs (RPD) arc determined by the softw:~ n: usmg values 1n the colculotion which ha\'e not been rounded

Printed212S/ IS 946 Fonn JC 00017 \\alprcwsOOI\starlimsS'J.IMSReps\l.ilbControiSample rpt SuperSet Reference· 15.0000322145 rev 00

A Enulronmentat CHAIN OF CUSTODY/LABORATORY ANALYSIS REQUEST FORM

1565 Jefferson Road, Building 300, Suite 360 • Rochester, NY 14623 I+ 1 585 288 5380 + 1 585 288 8475 (fax) PAGE J

23575 OF I

Prgfoct Name Project Nl.lllber ANAlYSIS REQUESTED (Include Method Number and Container Preservative)

l'llPDES "· Prgfoct ,..,_ RoponCC PRESERVATIVE 0 J 1 C:o;\n C"nvlo CompanyiAddnlss

f ;£, Preservative Key

\/onlb l=n\ ' NA {(,J: C"I=P\ (/) 0. NONE a: 1. HCL w z 2. HN03

41\1\n ~:: ... , c-.. ~ 3. H2S04

~~~~ ---~ 4. NaOH

0 ilj 5. Zn. Acetate (.)

.... . .t! .• 1....1 a • A n1 'lfl't u. d !\t ~IJ Cl.!! 6. MeOH 0

1,: I~ I (/J~ u ffj; If; 7. NaHS04 Phone' '"•" ,.._,_ ,.. ~ ·-··- Ema~ ffi

,.., ., AnA ,.-.nn / .111 -::~ .. JioJI_ i'n~::-, m I>) zy .p /i ~ .,. .,. 8. Other __

:::!: I>) "' " J? o (.j a ., ...., 0{1 :::J

~ ~~- #- ~~N~~~~db# !_~'!_R oj fij !UI, tJ~ liJ;..~ REMARKS/

• .;.z:_ -{_ z .,~ .... (3! <3!' (3 6 ~ .. <fl., ~;1 ~~ ALTERNATE DESCRIPTION

( FOR OOicE USE " SAMPUNG

CUENT SAMPLE ID ONLYLABID DATE TIME MATRIX

... ,., ., 11 .. 1•1 Cnrn 1"\ :1 v 0'+\J-.L~L.IVI-£1\-u V

-··~tJ·

_,-1•1C:.nrn

'"n 'l v .,,,.,,,r:

ltJ uoaoon. ~ .,,:o. . - ' . .-

.... ' .

.a. '-r

- . ... .XC.-

,• i--__ .... "; ....

SPECIAL INSTRUCTIONS/COMMENTS TURNAROUND REQUIREMENTS REPORT REQUIREMENTS INVOICE INFORMATION

Metal a -- RUSH (SURCHARGES APPLY} __ l Results Only

II. Resulls • OC Summaries POt --1 day -2 doy ----3 day --_ _ 4 day --)(day (LCS. DUP, MS/MSD cs required)

BIUTO: __ Ill. Results + OC and Calibration

EPA 624 & 625 list included with COC's Samples packed In Ice Summaries

REQUESTED REPORT DATE J rv. Data Yalidatlon Ropon with Raw Dala

SeeOAPP 0

sere WHERE SAMPLES WERE COLLECTED Edala __ Yes __ No

Q~~BY ,J r RECEIVED BY REUNOUISHED BY RECEIVED BY REUNOUISHEO BY RECEIVED BY

~-~ -_,~ il/1. ~ / LJ ...

-~ ~./A~ .----u~_.u ... 1~.£1 ..,.Y~ Signal&n Signal 1ft Slgnattn r~~

R1501144 5 Pili led ~~~ Prin~~ # / );/~ Printed Name Printed Name PmleciName V•otlo Wotor North Amort••

GE ..PIIIolleld NPDES

~) -h,; '2_ ·.clr') ~ Film A?_~/ F'rm F'I'ITI ri'ITI llllllllllllllllllllllllllllllllllllllllllllllllll 7I/-,

-~·· l OaterrttJ/Jp-).:j /~J(J Oate/Tlme Oale/Trne Daletrme

, , O!slnbullon: While • Lab Copy; Yel1ow • Return IO Originator e 2012 by ALS Group

J I

l I

I

I

I

A ~ Cooler Receipt and Preservation Check Form

R1501144 5 Voalla Water Nor1h Amorlo:a

lliliifiliiiliillililllllllllllllllllllllllllllll Project/Client-.....,;G:-....E"--~""""-'W::-:::'?F" ..... ·~u,.___ ___ Folder Number td ( - II Yt

Cooler received on w- by· ~ COURIER: ALS UPS ~ VELOCITY CLIENI'

1 Were Custody seals on outside of cooler? C!)N 5a Perchlorate samples have required headspace? Y

2 Custody papers properly completed (ink, signed)? ::!)N 5b Did VOA vials, Allc,or Sulfide have sig* bubbles?

3 Did all bottles arrive in good condition (unbroken)? ~N

4 Circle: (W""et ~ Dry Ice Gel packs present? (!)N - 7 Soil VOA received as: Bulk Encore

8. Temperature Readings Date: ;J JJ)r Time: ~-:3 ID(!Bi8 IR#4 From: Temp Blank ~e BottW ,

Observed Temp (DC) {.2-Correction Factor (0 C) :q.f' Corrected Temp (OC) ~. y.•

Within 0·6°C? (Y)N y N y N y N y N y N y N

If out of Temperature, note packing/lee condition: Ice melted Poorly Packed Same Day Rule

&Client Approval to Run Samples: Standing Approval Client aware at drop·off Client notified by: ------

PC Secondary Review:

Cooler Breakdown: Date : Time: I 'li J by:_..::~:!!f:s'::.-__,=~----

1. Were all bottle labels compl te (i.e. analysis, preservation, etc.)? ro NO

2. Did all bottle labels and tags agree with custody papers? W NO

3. Were correct containers used for the tests indicated? X£S NO

4. Air Samples: Cassettes I Tubes Intact Canisters Pressurized Tedlar® Bags Inflated

I . d' ExpJam any sscrepanc1es: pH Reagent Yes No Lot Received Exp Sample ID Vol. Lot Added Final

Added pH

>12 NaOH $2 HN03 $2 H1so. <4 NaHS04 Residual ForCN If+, contact PM to

Chlorine Phenol add Na1S10 3 (CN),


Na2Sz03 - -ZnAcetate - - .. Not to be tested before analysis -pH tested and

HCl •• •• recorded by VOAs on a separate worksheet

Yes= AU samples OK


PMOK to Adjust:

Bottle lot numbers: ___ .....aL\.:;..' .... v;"'"-.... ~_,· u...,-l~?'-:---------------------------Other Comments:

PC Secondary Review: _ _,,_~.....;:~"------ *significant air bubbles: VOA > 5-6 mm : WC > 1 in. diameter

P:\INTRANE'nQAQC\Fonns Conlrollcd\Cooler Receipt r7.doc 5/6/14

NAIIUNAL t"ULLU IAN I UI::.L.HAHl:H:: t:LIMINAIIUN :)Y:) I t:M lNt"Ut:::.J


r-orm 1\pproveo

OMB No. 2040.0004

PERM ITIEE NAME/ADDRESS (Include Facility Name/Location if Different)

NAME: GENERAL ELECTRIC PITTSFIELD DMR Mailing ZIP CODE: 01201 I MA0003B91 II W006·A I





PERMit NUMBER blscAARGE NUMBER

MONITORING PERIOD

MM/DDIVYYY I I MMIDDIVYYY

02/01/2015 02/28/2015

MAJOR

(SUBRW)


External Outfall

No DischargeD

QUANTITY OR LOADING QUALITY OR CONCENTRATION NO. FREQUENCY SAMPLE PARAMETER VALUE VALUE UNITS VALUE

pH SAMPLE MEASUREMENT - - - Goo.c0

004001 0 PERMIT - - - 6.5 Effluent Gross REQUIREMENT MINIMUM Solids, total suspended SAMPLE

MEASUREMENT ~ ~001('/j) (Eoor (~ CJYODI ( 9j) 005301 0 PERMIT Req. Mon. Req. Mon. lb/d Req. Mon. Effluent Gross REQUIREMENT MOAVG DAILYMX MOAVG Oil & Grease SAMPLE ****** ****** ****** *"****

MEASUREMENT

00556 1 0 PERMIT ****** ****** ****** *"**** Effluent Gross REQUIREMENT

Polychlorinated biphenyls [PCBs) SAMPLE MEASUREMENT K;oo•('ij) ((j_oor (~ 0Dr(~

395161 0 PERMIT Req. Mon. Req. Mon. lb/d Req. Mon. Effluent Gross REQUIREMENT MOAVG DAILYMX MOAVG Rainfall SAMPLE ICNOOo('/]) ~ ~or(?]) -MEASUREMENT

465291 0 PERMIT Req. Mon. Req. Mon. in ****** Effluent Gross REQUIREMENT MOAVG DAILYMX Flow, total SAMPLE

~ IC:oor<!i) -MEASUREMENT

822201 0 PERMIT Req. Mon. Req. Mon. MGD ****** Effluent Gross REQUIREMENT MOAVG DAILYMX

NAME/fiTLE PRINCIPAL EXECUTIVE OFFICER lcortltton!er ponoly ollowlhalthll ~ ond ol-.. ,. -od ondor mrctndion or supoovlllon inaccarolanc:e will\ a ll'f'lom""9>od to......, .... ..-ponomoi-"Y ..,.,., ..r

~~~oint.....-oobnllod.-.., my 1nqu0y ol 111o-or poqa~~ --- 111o

Exec. Mgr, Env. Remediation .,....,. or ..... po....,.dndly ....,.,..._lor lllllhoma ... inlomwllon, ... -- IUimlllod lo, to,. bost otmr 1<now1oc1ge ond bolo!, tnro, """""'"·..., """"*'"· ,..., ...,. ..., ....., anr llignlftcant --lot ou~ ,....lntonnal!on. flclrdng llo~JC~Ri*J or llno ond ~lor mowilg -...

TYPED OR PRINTED



EPA Form 3320-1 (Rev.01106l Previous editions may be used.

VALUE VALUE UNITS EX OF ANALYSIS TYPE

****"'* Goo•('i)

****** 9 su Quarterly GRAB MAXIMUM

****** Goo. ( ,;)) *"**** Req. Mon. mg/L Three per COMPOS

DAILYMX Quarter

*"**** ~·(0 ****** 15 mg/L Quarterly GRAB

DAILYMX - ~o,(!l) ****** Req. Mon. ug/L Three per COMPOS

DAILYMX Quarter ****** ****** ******

****** - - Dally when TOTALZ Discharging

****** ****** ******

****** - - Continuous Recorder - ~ ~~

(auto)

TELEPHONE DATE

AREACodo

12/15/2014 Page 1

PERMITIEE NAME/ADDRESS (Include Fscility Name/Location if Different)





ATTN: Andrew T . Silfer, Exec Mgr. En

I'll-\ IIUNI-\L t'ULLU I 1-\N I Ulbi...HI-\Hl:lt: t:LIMINI-\ IIUN bY b I t:M \Nt'Ut:b}


~ - -II I MA0003891 W06A·A

PERMit NUMBER blscHARGE NUMBER

MONITORING PERIOD

MM/DDNYYY I MM/DDNYYY

02/01/2015 02/28/2015


pH SAMPLE - - - -MEASUREMENT

004001 0 PERMIT ...... ...... ...... 6.5 - 9 Effluent Gross REQUIREMENT MINIMUM MAXIMUM Solids, total suspended SAMPLE

MEASUREMENT -005301 0 PERMIT Req. Mon. Req. Mon. lb/d Req. Mon. - Req.Mon. Effluent Gross REQUIREMENT MOAVG DAILYMX MOAVG DAILYMX Oil &Grease SAMPLE - - - - -MEASUREMENT

0055610 PERMIT - - ****** ****** - 15 Effluent Gross REQUIREMENT DAILYMX Polychlorinated biphenyls [PCBs) SAMPLE -MEASUREMENT

395161 0 PERMIT Req. Mon. Req. Mon. lb/d Req. Mon. ****** Req. Mon. Effluent Gross REQUIREMENT MOAVG DAILYMX MOAVG DAILVMX Rainfall SAMPLE - - -MEASUREMENT

465291 0 PERMIT Req. Mon. Req. Mon. In - - -Effluent Gross REQUIREMENT MOAVG DAILYMX Flow, in conduit or thru treatment SAMPLE - - -plant MEASUREMENT

500501 0 PERMIT Req.Mon. Req. Mon. MGD ...... - -Effluent Gross REQUIREMENT MOAVG DAILYMX Number of Events SAMPLE - - - -MEASUREMENT

514841 0 PERMIT Req. Mon. - II ...... - -Effluent Gross REQUIREMENT TOTAL

NAME/TITLE PRINCIPAL EXECUnVE OFFICER l~undorponallyalla•1hllltob--d-. .. ,.~-mydiroc:tionor

ll.lpOMIIon In~-· ayssomcletigr>odiO -• """~ ..-~golhor8nd ~~>oln!otmMion..-od - mmrlnquoyollho poraon or ponona who..._.,.

Exec. Mgr, Env. Remediation ..,......, orfl_po._,~,.--lofOI'fl'""'"'"il-. lhonr--.-odla. 10 lhe best of,~ and beitl lnle, .a:unde, and CDmJ!Ie'- • .,._.,. ._. t:Nra.,. ....,.. ' .,..- lof Kltmlli'lg- lnlomlolion. lnc:b&lg "" posai'*Y alh 8nd ~tor 11-.g ..-...

TYPED OR PRINTED - ----------

COMMENTS AND EXPLANAnON OF ANY VIOLA nONS (Reference all attachments here)

SEE PAGE 11 OF PERMIT. FLOW TOTAL SEE FOOTNOTE 4. NO OtS"CI~A~

EPA Form 3320.1 (Rev.01/06) Prevloua edltlona may be uaed.

r-urm ~ppruveo

OMB No. 2040-0004


MAJOR

(SUBRW)


External Outfall

No Discharge rc I


su Quarterly GRAB

mg/L Quarterly COMPOS

mg/L Quarterly GRAB

ug/L Quarterly COMPOS

-****** Dally when TOTALZ

Discharging

******


******

****** Dally when VISUAL Discharging

----

TELEPHONE DATE

AREA ~:Me

12/15/2014 Page 1

PERMITTEE NAME/ADDRESS (Include Facility Nam6/Location If Different}






NAIIUNAL I"'ULLU IAN I UI~~HAHut: t:LIMINAIIUN ~Y~ I t:M lNI"'Ut:~j


MA0003891 W06A-A ~ -~ I PERMIT NOMBE I DiSCHARGE NUMBER

MONITORING PERIOD

MMIDDNYYY I MMIDDNYYY

02/01/2015 02/28/2015


Flow, total SAMPLE -MEASUREMENT

822201 0 PERMIT Req. Mon. Req. Mon. MGD -Effluent Gross REQUIREMENT MOAVG DAILYMX

NAME/TlTLE PRINCIPAL EXECUTIVE OFFICER I CO<Iifyundor ponaly of--.,._,..,._ .. _ _ ,. _ _,under my dirodionOf

'lllfiOMIIonlnll<lllllldonc:ewill e optom.........,toeo ... .,...,._.,......,.. -'Y ~~-

VALUE VALUE - -- -

t"urm ~ppruvao

OMB No. 2040-0004


MAJOR

(SUBRW)


External Outfall No Discharge (gJ



-- Continuous Recorder

(auto)_

TELEPHONE DATE

1,--""''llllU~I\tlll'frPE'IIIWI"T!', --SI'IIII .. 'P.,ri"1F,e~---------~, • ..;,,.., .... ,.,.-..-ocr.-""'"' lnqulryollho _., -"""" .,.._""

,..,_,_.,,_.,....,., • ......, .. orpono~~~oforgoo~~omglhotn-.lho--oclll. ' I <v....-e ...,.. ' . c 'I£(':"V V - j . ~~.:=o:!e::.~:;::.:::.:::ld~:...=-1 Exec. Mgr, Env. Remediation

~-------=TY~P~ED~O~R~P~R~IN~TE==D--------i,,'~


SEE PAGE 11 OF PERMIT. FLOW TOTAL SEE FOOTNOTE4.

EPA Form 332D-1 (Rev.01/06) Previous editions mey be und.

NO PI ':)(!IJ Af'Z.Cr;;:-

12/15/2014 Page 2

Attachment E - Outfall 06A Wet

TSS FN Oil &Grease FN PCB Date pH MG/L MG/L UG/L

02/01/15

02/02/15

02/03/15

02/04/15

02/05/15

02/06/15 02/07/15

02/08/15

02/09/15

02/10/15

02/11/15

02/12/15

02/13/15

02/14/15

02/15/15

02/16/15 02/17/15

02/18/15

02/19/15

02/20/15 02121/15

02/22/15

02/23/15

02/24/15

02/25/15

02/26/15 02/27/15 02/28/15



G - Grab sample

FN Metered Rain/Precip Rain/Precip Flow- MGD Total- in Peak- in

0.00 0.00 0.20 0.07 0.16 0.02 0.00 0.00 0.15 0.04

0.09 0.05

0.08 0.08

0.06 0.02 0.19 0.05

0.07 0.01

0.00 0.00

0.08 0.06 0.04 0.02 0.00 0.00

0.13 0.02

0.00 0.00

0.00 0.00

0.00 0.00 O.Q1 0.01

0.52 0.08

0.36 0.11 0.08 0.02 0.03 0.02

0.52 0.14

0.00 0.00

0.00 0.00

0.00 0.00

0.00 0.00

PERM ITIEE NAME/ADDRESS (lncJude Facility Name/Location if Different)






NA IIUNAL t"ULLU, AN I UI:;:,LMAHl:Jt: t:.LIMINA IIUN ::tY::tl t:.M lNI"'Ut:::t)


I MA0003891 II SR05-A I PERMIT NUMBER DISCHARGE NUMBER

MONITORING PERIOD

MMIDD!YYYY I I MMIDD!YYYY

02/01/2015 02/28/2015


Rainfall SAMPLE -MEASUREMENT

46529 1 0 PERMIT Req. Moo. Req. Mon. In ****** Effluent Gross REQUIREMENT MOAVG DAILVMX Number of Events SAMPLE - -MEASUREMENT

514841 0 PERMIT Req. Mon. ****** II ****** Effluent Gross REQUIREMENT TOTAL Flow, total SAMPLE -MEASUREMENT


NAMEJTtTLE PRINCIPAL EXECUTIVE OFFICER 1 ~ lftlot piNIIy at lowlhallhll cloc:lmMI.am •• -......a_,. pnpoowd undO. my dirOction ..-MJpOf\'illon In IIOCOidoncoo -. • oyolom doolgned to ...... that quoliftod ~ pt-'V ~· .-.1

th8infooml-oubmittod. l!aHd ... my""'""'"' ... - ... --......... - ........ .,......,.or.oe~~yrwopconoa.lolorgdlomgtholn-• .,. --odlo,

Exec. Mgr, Env. Remediation b> th8 best of my-...--··--......... .-.leomplole.l---........ ...,_ ponatin lor oubmilh'lg laiH .,,_tion_incW"ong "' posoibllly of lno ondlrnpisamlent tor lnowng -...

TYPED OR PRINTED ----


TOTAL FLOW SEE FOOTNOTE 3.

EPA Form 332G-1 (Rav.01/06) Previous edlllona may be UHd.

VALUE VALUE - -****** ******

- ******

****** -- ******

- -

NO or Sc14AA-~

r-urrn Approvea

OMB No. 2040{1004


MAJOR

(SUBRW)

FlOW FROM 006 EXCEED CAP. OWS64X

External Outfall No Discharge [QJ



-****** Dally when TOTALZ

Discharging ******

****** Dally when VISUAL Discharging

******

****** Dally when Recorder Discharging (auto)

TELEPHONE DATE

AAEACM8

12/15/2014 Page 1

Attachment E - Outfall SR05A

Metered Raln/Precip Raln/Precip

Date Flow-MGD Total-In Peak -In

02/01/15 0.00 0.00

02/02/15 0.20 0.07

02/03/15 0.16 0.02

02/04/15 0.00 0.00 02/05/15 0.15 0.04 02/06/15 0.09 0.05 02/07/15 0.08 0.08 02/08/15 0.06 0.02 02/09/15 0.19 0.05 02/10/15 0.07 0.01

02/11/15 0.00 0.00

02/12/15 0.08 0.06

02/13/15 0.04 0.02

02/14/15 0.00 0.00

02/15/15 0.13 0.02

02/16/15 0.00 0.00

02/17/15 0.00 0.00

02/18/15 0.00 0.00

02/19/15 0.01 O.D1

02/20/15 0.52 0.08 02/21/15 0.36 0.11 02/22/15 0.08 0.02 02/23/15 0.03 0.02 02/24/15 0.52 0.14 02/25/15 0.00 0.00 02/26/15 0.00 0.00 02/27/15 0.00 0.00 02/28/15 0.00 0.00

~

PERMIITEE NAME/ADDRESS (lndudfl Facility Name/Location if Diffflrflnt)





ATTN: AndrewT. Silfer, Exec Mgr. En

NAIIUNAL 1-'ULLU IAN I Ulbl.HAHut tLIMINAIIUN ::.Ybii:M lNI"'UI:::.)


I MA0003B91 II 09B·A I PERMIT NUMBER blscRARGE NUMBER

MONITORING PERIOD

MM!DD!YYYY I I MMIDD!YYYY

02/01/2015 02/28/2015


pH SAMPLE MEASUREMENT

......... - - -004001 0 PERMIT - - - 6.5 - 9 Effluent Gross REQUIREMENT MINIMUM MAXIMUM Solids, total suspended SAMPLE

MEASUREMENT -005301 0 PERMIT 213 876 Ibid Req. Mon. - Req.Mon. Effluent Gross REQUIREMENT MOAVG DAILYMX MOAVG DAILYMX Oil &Grease SAMPLE - - -MEASUREMENT

005561 0 PERMIT - 438 lb/d - - 15 Effluent Gross REQUIREMENT OAILYMX DAILYMX Polychlorinated biphenyls [PCBs] SAMPLE -MEASUREMENT

3951610 PERMIT Req. Mon. Req. Mon. lb/d Req. Mon. - Req. Mon. Effluent Gross REQUIREMENT MOAVG DAILYMX MOAVG DAILYMX Rainfall SAMPLE ****** ****** ******

MEASUREMENT

46529 1 0 PERMIT Req. Mon. Req. Mon. in - - -Effluent Gross REQUIREMENT MOAVG DAILYMX Flow, in conduit or thru treatment SAMPLE - - -plant MEASUREMENT

500501 0 PERMIT Req. Mon. Req. Mon. MGD - - -Effluent Gross REQUIREMENT MOAVG DAILYMX Row, total SAMPLE - - ******

MEASUREMENT

rurm ~o~ppruvea

OMB No. 2040-Q004


MAJOR

(SUBRW)

OUTFALL 098 (119W)

lntemal OUtfall

NO.

UNITS EX

su

mg{L

mg/L

ug/L

******

-******

--

No Discharge 1£]

FREQUENCY SAMPLE OF ANALYSIS TYPE

Quarterly GRAB

Three per COMP24 Quarter

Quarterly GRAB

Three per COMP24 Quarter

Continuous Recorder (auto)

Continuous Recorder (auto)

I I

822201 0 PERMIT Req. Mon. Req. Mon. MGD - - - - Continuous Recorder I Effluent Gross REQUIREMENT MOAVG DAILYMX

NAME/TITLE PRINCIPAL EXECunVE OFFICER l<*lil'y....rorponOIIyotlo.w_thoo __ al...,._.wo,._ocl....ror.,_Of _.-. ... ......,_...,,..,....,.cletianocllo ...... l>al~portC>nllOtprOporlr~r-

1 Alillii!llf. S!III!l. PE 'l - 1helnfonnolion.-.aaoUesoclonmy""*"al.,.,.._.or __ ...._.,. - .or ..... ,.....,,dO.clly.._,.lor~omglloOI-. f>e-...tmaocllo. co1hlbn1ot...,~Mdbelet.we. ecance . .,CICiml*" ,.,.. ... ~.._...,_.,.,~~ er_'V' 4 -~ - '

4 "'l tC'fC' v l !~ro.sutm~MgiiiM-.i'>cllclllgllopouitillyolil>a-mprllonmonllor~;-·.. ·-- -- ·•· ''-.. ·--.. •· - -- -

E~ec. Mgr, Env. Remediation

I TYPED OR PRINTED 1-·


SEE PAGE 12 OF PERMIT; FLOW TOTAL SEE FOOTNOTE 4.

EPA Form 3320.1 (Rev.01/06) Previous editions may be used.

NO DtSC ti.A'-<,-~

(auto) !

TELEPHONE DATE

AREA~

12/15/2014 Page 1

Attachment E - Outfall 098

TSS FN Oil & Grease FN PCB Date pH MG/L MG/l UG/l

02/01/15 02/02/15 02/03/15 02/04/15 02/05/15 02/06/15 02/07/15 02/08/15

02/09/15 02/10/15 02/11/15 02/12/15 02/13{15

02/14/15 02/15/15 02/16/15 02/17/15 02/18/15 02/19/15 02/20/15 02/21/15 02/22/15 02/23/15 02/24/15 02/25/15 02/26/15 02/27/15 02/28/15

FN 1 - (U) Indicates compound analyzed for but not detected C • Composite sample G ~ Grab sample

FN Metered Aaln/Precip Aain/Preclp Flow- MGD Total-In Peak -In

0 0.00 0.00 0 0.20 0.07 0 0.16 0.02 0 0.00 0.00 0 0.15 0.04 0 0.09 0.05 0 0.08 0.08 0 0.06 0.02 0 0.19 0.05 0 0.07 0.01 0 0.00 0.00 0 0.08 0.06 0 0.04 0.02 0 0.00 0.00 0 0.13 0.02 0 0.00 0.00 0 0.00 0.00 0 0.00 0.00 0 0.01 0.01 0 0.52 0.08 0 0.36 0.11 0 0.08 0.02 0 0.03 0.02 0 0.52 0.14 0 0.00 0.00 0 0.00 0.00 0 0.00 0.00 0 0.00 0.00

PERMITTEE NAME/ADDRESS (Include Facility Name/Location if Different)






N~IIUN~L t'ULLU I~NI Ultll..M~Hut:: t::LIMIN~IIUN t.Yt.lt::M \Nt'Ut::tlJ


I D009·A

151§~RAR~~ RDJls~Fi

MM/DD/YYYY MM/DD/YYYY

02/01/2015 02/28/2015


pH SAMPL£ MEASUREMENT

........ ........ .........

00400 1 0 PERMIT - - - 6.5 Effluent Gross REQUIREMENT MINIMUM Solids, total suspended SAMPLE

MEASUREMENT

005301 0 PERMIT Req. Mon. Req. Mon. Ibid Req. Mon. Effluent Gross REQUIREMENT MOAVG DAILYMX MOAVG Oil & Grease SAMPLE - - -MEASUREMENT

005561 0 PERMIT - - - Req. Mon. Effluent Gross REQUIREMENT MOAVG Polychlorinated biphenyls [PCBs) SAMPLE

MEASUREMENT

395161 0 PERMIT Req. Mon. Req.Mon. lb/d Req. Mon. Effluent Gross REQUIREMENT MOAVG DAILYMX MOAVG Flow, in conduit or thru lreatment SAMPLE -plant MEASUREMENT

500501 0 PERMIT Req. Mon. Req. Mon. MGD -Effluent Gross REQUIREMENT MOAVG DAILYMX Flow, total SAMPLE .........

MEASUREMENT

822201 0 PERMIT Req. Mon. Req. Mon. MGD -Effluent Gross REQUIREMENT MOAVG DAILYMX ~-

NAMEJTITLE PRINCIPAL EXECUTIVE OFFICER I~Lnlorponallyollo.,lhol-docurnonlondoi-•Mre~underrf>t- or oupoMslon in acc:ordance wit! • ayolem dollignod to ...... lhal quaiNct ,......... pr-"f ~r ond

II Aiii_4rww I_ ~ililb; ,., I .,_. lhefttom.liansubrniaed. Basedanmtftqt*yotlhepersonat ~whamanagellhe

VALUE VALUE

........

- 9 MAXIMUM ........

........ Req. Mon. DAILYMX -- 15 DAILYMX -- Req. Mon. DAILYMX - -- ........

- -- -

.-orm 1\pprovea

OMB No. 2040·0004


MAJOR

(SUBRW)


External Outfall

No Discharge [gJ




mgfL Twice per COMP24 Month

mgfl Twice per GRAB Month

ug/L Twice per COMP24 Month -

****** Weekly ESTIMA

-- Twice per ESTIMA

Month

TELEPHONE bAT!!.

Exec. Mgr, Env. Remediation =~::-::=.~=:::.:::~~~-!:..~~..:.~1 ( / kRd"'f"=' ' · 4-f<WV'- I ~folwbn-.glal&einlormolion,lr'dldinglho....-.roltnoond~far--.g -·--·- ·- n• • -· • ..

II TYPED OR PAINTED l)'iolaliont.

COMMENTS AND EXPLANATION OF ANY VIOLATIONS (Reference all aHachmenta here)


EPA Form 33211-1 (Rev.D1106) Previous editions may be used.

No 0 r 5' c /-II"',._&-.;-

MEAt-.

12/15/2014 Page 1

Attachment E - Outfall 009 Dry

Date pH TSS FN Oil & Grease FN PCB FN Estimated

MG/L MG/L UG/L Flow- MGD

(50050 1 0)

02101/15

02102115

02/03/15

02/04/15

02/05/15

02/06/15

02/07/15

02/08/15 02/09/15

02/10/15

02/11/15

02/12/15

02/13/15

02/14/15

02/15/15

02/16/15

02/17/15

02/18/15

02/19/15

02/20/15 02/21/15

02122/15 02/23/15

02/24/15

02/25/15

02/26/15 02/27/15

02/28115


2 - Estimated flow observed at the 119W Oil/Water Separator (OWS) Inlet pipe

C • Composite sample

G • Grab sample

Estimated FN Rain/Precip Rain/Precip

Flow-MGD Total-In Peak -In

(82220 1 0)

0 0.00 0.00

0.20 0.07

0.16 0.02

0.00 0.00 0.15 0.04 0.09 0.05

0.08 0.08

0 0.06 0.02

0.19 0.05

0.07 0,01

0.00 0.00

0.08 0.06

0.04 0.02

0.00 o.oo1

0 0.13 0.02!

0.00 o.oo! 0.00 o.oo' 0.00 0.00.

I

O.Q1 O.Q1;

0.52 0.081 0.36 0.11!

0 0.08 0.02

0.03 0.02

0.52 0.141 0.00 o.oo,

I

0.00 0.00 0.00 0.00

0.00 0.00

PERMITIEE NAME/ADDRESS (Include Facility Name/l..ocalion if Ditferenll





ATTN: Andrew T. SiHer, Exec Mgr. En

NAIIUNAL t'ULLU IAN I Ulbi..HAHl:>t: l:t.IMINAIIUN ::>Y::>II:M \NI-'UI:b/


I MA0003891 II W009-A I PERMIT NUMBER blscAARGE NUMBER

MONITORING PERIOD

MM/DD/YYVY I I MM/DD/YYVY

02/01/2015 02/28/2015


pH SAMPLE - - *****'* MEASUREMENT

004001 0 PERMIT - - - 6.5 Effluent Gross REQUIREMENT MINIMUM Solids, total suspended SAMPLE

MEASUREMENT

005301 0 PERMIT Req. Mon. Req. Mon. Ibid Req. Mon. Effluent Gross REQUIREMENT MOAVG DAILYMX MOAVG Oil &Grease SAMPLE - - - -MEASUREMENT

005561 0 PERMIT - - - -Effluent Gross REQUIREMENT

Polychlorinated biphenyls {PCBs] SAMPLE MEASUREMENT

395161 0 PERMIT Req. Mon. Req. Mon. Ibid Req. Mon. Effluent Gross REQUIREMENT MOAVG DAILYMX MOAVG Flow, total SAMPLE -MEASUREMENT


NAME/TITLE PRINCIPAL EXECUTIVE OFFICER lcedJ!y under pondy ot ltwlh&tlhis --d -.....u ,..,. p--od !Oidetmy dQdlon or ...,..-. 01 ~ wllh aoystom deslgnod to ...... llal qualified _...t l'fOPOflrgdMrond

I Attdi 11 ca 1'. ~tth:& . PI! l.,r..-. 1M ntonn.Oon autnaed. Baed on my ~ of he penon Of penona who nanaoe lhe

VALUE VALUE -- 9

MAXIMUM -- Req. Mon. DAILYMX -- 15 DAILYMX -- Req. Mon. DAILYMX - -

- -

r-urm Appruveo

OMB No. 2040-0004


MAJOR (SUBRW)


External Outfall

No Discharge 1£1


su Quarterly GRAB

mgll Three per COMPOS Quarter

mgll Quarterly GRAB

ug/L Three per COMPOS Quarter -

- Continuous Recorder (auto)

TELEPHONE DATE

Exec. Mgr. En11. Remediation - • ..-110Hpor>a~odorodlyrHpOilOillolorljdlomg.,.lntonnacion .... lnlonr-.MIIrnllodlo. I ( / Ut2'/W<' {/ ./fY~ J to.,.beolotmy~and-t,buo.-o . ..,""""""te. l .. _,.,...,.-.., • ..- . . . . . .. .. .. . ' ~tor.,~--. lncWftg.,.~otfneond~torlon-

1 TYPED OR PRINTED 1-..·


SEE PAGE 14 OF PERMIT TOTAL FLOW SEE FOOTNOTE 4

EPA Form 3320.1 (Rev.01106) Previous edlllona may be used.

AREA eo.

1\10 0 ' S" f!../1 ~A-&-,;--

12/15/2014 Page 1

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