Post on 10-Apr-2015
description
ANALYTICAL REPORT
Job Number: 460-13139-1
Job Description: Dumont Fields - Twin Boro
For:Duffield Associates
5400 Limestone RoadWilmington, DE 19808
Attention: Mr. Bradley Summerville
_____________________________________________
Approved for release.Jamie CapaciProject Manager I6/3/2010 3:55 PM
Jamie CapaciProject Manager I
jamie.capaci@testamericainc.com06/03/2010
The test results in this report meet all NELAP requirements unless specified within the case narrative. Pursuant toNELAP, this report may not be reproduced, except in full, without the written approval of the laboratory. All questionsregarding this report should be directed to the TestAmerica Edison Project Manager.
TestAmerica Edison Certifications and Approvals: Connecticut: CTDOH #PH-0200, New Jersey: NJDEP (NELAP)#12028, New York: NYDOH (NELAP) #11452, NYDOH (ELAP) #11452, Pennsylvania: PADEP (NELAP) 68-00522 andRhode Island: RIDOH LAO00132
TestAmerica Laboratories, Inc.
TestAmerica Edison 777 New Durham Road, Edison, NJ 08817
Tel (732) 549-3900 Fax (732) 549-3679 www.testamericainc.com
06/03/2010Page 1 of 623
Table of ContentsCover Title Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Data Summaries . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
Report Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
Executive Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
Method / Analyst Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
Sample Datasheets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62
QC Data Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 66
Data Qualifiers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 95
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 97
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 101
Organic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 106
GC/MS VOA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 106
Method 8260B . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 106Method 8260B QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 107Method 8260B Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 114Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 142
Method 8260B ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 142Method 8260B CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 154
Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 157Method 8260B Tune Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 157Method 8260B Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 165Method 8260B LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 171
Method 8260B Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 185
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Table of ContentsMethod 8260B Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 187
GC/MS Semi VOA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 189
Method 8270C . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 189Method 8270C QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 190Method 8270C Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 202Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 298
Method 8270C ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 298Method 8270C CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 309
Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 312Method 8270C Tune Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 312Method 8270C Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 320Method 8270C LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 329Method 8270C MS/MSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 336
Method 8270C Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 340Method 8270C Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 342
GC Semi VOA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 344
Method 8081A . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 344Method 8081A QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 345Method 8081A Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 360Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 389
Method 8081A ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 389Method 8081A PEM Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 409Method 8081A CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 417
Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 425Method 8081A Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 425Method 8081A LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 431
06/03/2010Page 3 of 623
Table of ContentsMethod 8081A MS/MSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 441
Method 8081A Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 445Method 8081A Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 448
Method 8082 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 450Method 8082 QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 451Method 8082 Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 464Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 488
Method 8082 ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 488Method 8082 CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 538
Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 546Method 8082 Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 546Method 8082 LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 552Method 8082 MS/MSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 563
Method 8082 Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 567Method 8082 Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 570
Inorganic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 572
Metals Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 572
Met Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 573
Met Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 574
Met QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 578Met ICV/CCV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 578Met Blanks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 580Met ICSA/ICSAB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 584Met MS/MSD/PDS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 588Met Duplicates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 589Met LCS/LCSD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 590
06/03/2010Page 4 of 623
Table of ContentsMet Serial Dilution . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 592
Met MDL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 593
Met Linear Ranges . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 595
Met Preparation Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 596
Met Analysis Run Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 598
Met Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 600
General Chemistry Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 603
Gen Chem Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 604
Gen Chem MDL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 605
Gen Chem Analysis Run Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 606
Gen Chem Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 613
Shipping and Receiving Documents . . . . . . . . . . . . . . . . . . . . . . . . . . . 621
Client Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 622
Sample Receipt Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 623
06/03/2010Page 5 of 623
CASE NARRATIVE
Client: Duffield Associates
Project: Dumont Fields - Twin Boro
Report Number: 460-13139-1
This case narrative is in the form of an exception report, where only the anomalies related to this report, method specific performance
and/or QA/QC issues are discussed. If there are no issues to report, this narrative will include a statement that documents that there are
no relevant data issues.
It should be noted that samples with elevated Reporting Limits (RLs) as a result of a dilution may not be able to satisfy customer reporting
limits in some cases. Such increases in the RLs are unavoidable but acceptable consequence of sample dilution that enables
quantification of target analytes or interferences which exceed the calibration range of the instrument.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
RECEIPT
The samples were received on 05/13/2010; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 3.3 C.
Note: All samples which require thermal preservation are considered acceptable if the arrival temperature is within 2C of the required
temperature or method specified range. For samples with a specified temperature of 4C, samples with a temperature ranging from just
above freezing temperature of water to 6C shall be acceptable. Samples that are hand delivered immediately following collection may not
meet these criteria, however they will be deemed acceptable according to NELAC standards, if there is evidence that the chilling process
has begun, such as arrival on ice, etc.
TOTAL METALS
Samples 460-13139-2, 460-13139-4, 460-13139-5 and 460-13139-7 were analyzed for total metals in accordance with EPA SW-846
Method 6010B. The samples were prepared on 05/14/2010 and analyzed on 05/18/2010.
The matrix spike(MS) recoveries for antimony in batch 37477 was outside control limits. The associated laboratory control sample (LCS)
recovery met acceptance criteria.
Samples 460-13139-2(4X), 460-13139-4(4X), 460-13139-5(4X) and 460-13139-7(4X) required dilution prior to analysis. The reporting
limits have been adjusted accordingly.
As a standard practice all soil samples and related QC samples (i.e., MB, LCS, Dup, MS, SD) are diluted 2X-4X prior to analysis. Further
dilutions may be required dependent upon analyte levels in the samples. Refer to the analytical results forms for dilutions.
No other difficulties were encountered during the metals analyses.
All other quality control parameters were within the acceptance limits.
TOTAL MERCURY
Samples 460-13139-2, 460-13139-4, 460-13139-5 and 460-13139-7 were analyzed for total mercury in accordance with EPA SW-846
Method 7471A. The samples were prepared and analyzed on 05/14/2010.
No difficulties were encountered during the mercury analyses.
All quality control parameters were within the acceptance limits.
ORGANOCHLORINE PESTICIDES
Samples 460-13139-2, 460-13139-4, 460-13139-5 and 460-13139-7 were analyzed for organochlorine pesticides in accordance with EPA
SW-846 Method 8081A. The samples were prepared on 05/14/2010 and analyzed on 05/17/2010.
DCB surrogate recovery for the following sample(s) was outside control limits: 460-13139-4 on the primary column. Evidence of matrix
interference is present; therefore, re-extraction and/or re-analysis was not performed.
No other difficulties were encountered during the pesticides analyses.
All other quality control parameters were within the acceptance limits.
06/03/2010Page 6 of 623
POLYCHLORINATED BIPHENYLS (PCBS)
Samples 460-13139-2, 460-13139-4, 460-13139-5 and 460-13139-7 were analyzed for polychlorinated biphenyls (PCBs) in accordance
with EPA SW-846 Method 8082. The samples were prepared and analyzed on 05/14/2010.
No difficulties were encountered during the PCBs analyses.
All quality control parameters were within the acceptance limits.
VOLATILE ORGANIC COMPOUNDS (GC-MS)
Samples 460-13139-2, 460-13139-4, 460-13139-5 and 460-13139-7 were analyzed for volatile organic compounds (GC-MS) in
accordance with EPA SW-846 Method 8260B. The samples were prepared on 05/14/2010 and analyzed on 05/18/2010.
No difficulties were encountered during the volatiles analyses.
All quality control parameters were within the acceptance limits.
SEMIVOLATILE ORGANIC COMPOUNDS (GC-MS)
Samples 460-13139-2, 460-13139-4, 460-13139-5 and 460-13139-7 were analyzed for semivolatile organic compounds (GC-MS) in
accordance with EPA SW-846 Method 8270C. The samples were prepared on 05/17/2010 and analyzed on 05/18/2010.
The laboratory control sample (LCS) for batch 37564 was outside control limits for the following analyte: Benzidine.
The matrix spike / matrix spike duplicate (MS/MSD) precision for batch 37564 was outside control limits for Benzidine.
The matrix spike / matrix spike duplicate (MS/MSD) recoveries for batch 37564 were outside control limits for 2,4-Dinitrophenol,
4,6-Dinitro-2-methylphenol and Benzidine.
No other difficulties were encountered during the semivolatiles analyses.
All other quality control parameters were within the acceptance limits.
PERCENT SOLIDS
Samples 460-13139-1 through 460-13139-8 were analyzed for percent solids in accordance with ASTM D2974-87 Modified. The samples
were analyzed on 05/14/2010 and 05/17/2010.
No difficulties were encountered during the % solids analyses.
All quality control parameters were within the acceptance limits.
06/03/2010Page 7 of 623
SAMPLE SUMMARY
Client: Duffield Associates Job Number: 460-13139-1
Client Sample IDLab Sample ID Client Matrix
Date/Time
Sampled
Date/Time
Received
05/12/2010 0900 05/13/2010 1830TB-3 2-3460-13139-1 Soil
05/12/2010 0945 05/13/2010 1830TB-3 6-7460-13139-2 Soil
05/12/2010 1030 05/13/2010 1830TB-2 2-3460-13139-3 Soil
05/12/2010 1045 05/13/2010 1830TB-2 5-6460-13139-4 Soil
05/12/2010 1125 05/13/2010 1830TB-1 2-3460-13139-5 Soil
05/12/2010 1145 05/13/2010 1830TB-1 5-6460-13139-6 Soil
05/12/2010 1230 05/13/2010 1830TB-5 3-4460-13139-7 Soil
05/12/2010 1340 05/13/2010 1830TB-4 6-7460-13139-8 Soil
TestAmerica Edison
06/03/2010Page 8 of 623
EXECUTIVE SUMMARY - Detections
Client: Duffield Associates Job Number: 460-13139-1
Analyte Result / Qualifier
Reporting
Limit Units Method
Lab Sample ID Client Sample ID
460-13139-1 TB-3 2-3
1.0 % Moisture17.9Percent Moisture
1.0 % Moisture82.1Percent Solids
460-13139-2 TB-3 6-7
41 ug/Kg 8270C28 JBenzo[a]anthracene
410 ug/Kg 8270C120 JBis(2-ethylhexyl) phthalate
1.2 mg/Kg 6010B1.9Arsenic
0.46 mg/Kg 6010B0.20 JBeryllium
2.3 mg/Kg 6010B9.1Chromium
5.8 mg/Kg 6010B13.9Copper
1.2 mg/Kg 6010B17.5Lead
9.3 mg/Kg 6010B7.0 JNickel
7.0 mg/Kg 6010B31.3Zinc
1.0 % Moisture18.8Percent Moisture
1.0 % Moisture81.2Percent Solids
460-13139-3 TB-2 2-3
1.0 % Moisture13.9Percent Moisture
1.0 % Moisture86.1Percent Solids
TestAmerica Edison
06/03/2010Page 9 of 623
EXECUTIVE SUMMARY - Detections
Client: Duffield Associates Job Number: 460-13139-1
Analyte Result / Qualifier
Reporting
Limit Units Method
Lab Sample ID Client Sample ID
460-13139-4 TB-2 5-6
380 ug/Kg 8270C97 JAcenaphthylene
380 ug/Kg 8270C110 JAcenaphthene
380 ug/Kg 8270C150 JFluorene
380 ug/Kg 8270C1500Phenanthrene
380 ug/Kg 8270C240 JAnthracene
380 ug/Kg 8270C1800Fluoranthene
380 ug/Kg 8270C1500Pyrene
38 ug/Kg 8270C710Benzo[a]anthracene
380 ug/Kg 8270C960Chrysene
380 ug/Kg 8270C210 JBis(2-ethylhexyl) phthalate
38 ug/Kg 8270C820Benzo[b]fluoranthene
38 ug/Kg 8270C300Benzo[k]fluoranthene
38 ug/Kg 8270C690Benzo[a]pyrene
38 ug/Kg 8270C610Indeno[1,2,3-cd]pyrene
38 ug/Kg 8270C130Dibenz(a,h)anthracene
380 ug/Kg 8270C680Benzo[g,h,i]perylene
77 ug/Kg 8081A170 pChlordane
7.7 ug/Kg 8081A554,4'-DDD
7.7 ug/Kg 8081A8.6 p4,4'-DDE
7.7 ug/Kg 8081A294,4'-DDT
7.7 ug/Kg 8081A5.5 J pDieldrin
1.1 mg/Kg 6010B4.5Arsenic
0.46 mg/Kg 6010B0.37 JBeryllium
1.1 mg/Kg 6010B0.98 JCadmium
2.3 mg/Kg 6010B17.9Chromium
5.7 mg/Kg 6010B71.8Copper
1.1 mg/Kg 6010B251Lead
9.2 mg/Kg 6010B11.9Nickel
2.3 mg/Kg 6010B4.9 BSilver
6.9 mg/Kg 6010B137Zinc
0.035 mg/Kg 7471A0.22Mercury
1.0 % Moisture12.8Percent Moisture
1.0 % Moisture87.2Percent Solids
460-13139-5 TB-1 2-3
1.0 mg/Kg 6010B1.4Arsenic
2.0 mg/Kg 6010B4.6Chromium
5.0 mg/Kg 6010B7.2Copper
1.0 mg/Kg 6010B7.9Lead
8.1 mg/Kg 6010B5.4 JNickel
6.1 mg/Kg 6010B19.2Zinc
1.0 % Moisture6.5Percent Moisture
1.0 % Moisture93.5Percent Solids
TestAmerica Edison
06/03/2010Page 10 of 623
EXECUTIVE SUMMARY - Detections
Client: Duffield Associates Job Number: 460-13139-1
Analyte Result / Qualifier
Reporting
Limit Units Method
Lab Sample ID Client Sample ID
460-13139-6 TB-1 5-6
1.0 % Moisture11.9Percent Moisture
1.0 % Moisture88.1Percent Solids
460-13139-7 TB-5 3-4
860 ug/Kg 8270C200 JAcenaphthene
860 ug/Kg 8270C440 JFluorene
860 ug/Kg 8270C1800Phenanthrene
860 ug/Kg 8270C260 JAnthracene
860 ug/Kg 8270C1300Fluoranthene
860 ug/Kg 8270C790 JPyrene
86 ug/Kg 8270C380Benzo[a]anthracene
860 ug/Kg 8270C560 JChrysene
860 ug/Kg 8270C190 JBis(2-ethylhexyl) phthalate
86 ug/Kg 8270C590Benzo[b]fluoranthene
86 ug/Kg 8270C230Benzo[k]fluoranthene
86 ug/Kg 8270C410Benzo[a]pyrene
86 ug/Kg 8270C460Indeno[1,2,3-cd]pyrene
860 ug/Kg 8270C460 JBenzo[g,h,i]perylene
17 ug/Kg 8081A16 J pgamma-BHC (Lindane)
170 ug/Kg 8081A1700Chlordane
17 ug/Kg 8081A18 p4,4'-DDE
17 ug/Kg 8081A28Dieldrin
2.5 mg/Kg 6010B3.2Arsenic
2.5 mg/Kg 6010B1.1 JCadmium
5.1 mg/Kg 6010B6.7Chromium
12.7 mg/Kg 6010B22.0Copper
2.5 mg/Kg 6010B222Lead
20.4 mg/Kg 6010B7.0 JNickel
15.3 mg/Kg 6010B152Zinc
0.082 mg/Kg 7471A0.31Mercury
1.0 % Moisture61.5Percent Moisture
1.0 % Moisture38.5Percent Solids
460-13139-8 TB-4 6-7
1.0 % Moisture16.3Percent Moisture
1.0 % Moisture83.7Percent Solids
TestAmerica Edison
06/03/2010Page 11 of 623
METHOD SUMMARY
Job Number: 460-13139-1Client: Duffield Associates
Preparation MethodMethodLab LocationDescription
Matrix: Solid
SW846 8260BVolatile Organic Compounds (GC/MS) TAL EDI
SW846 5035TAL EDIClosed System Purge and Trap
SW846 8270CSemivolatile Compounds by Gas Chromatography/Mass
Spectrometry (GC/MS)
TAL EDI
SW846 3541TAL EDIAutomated Soxhlet Extraction
SW846 8081AOrganochlorine Pesticides (GC) TAL EDI
SW846 3541TAL EDIAutomated Soxhlet Extraction
SW846 8082Polychlorinated Biphenyls (PCBs) by Gas Chromatography TAL EDI
SW846 3541TAL EDIAutomated Soxhlet Extraction
SW846 6010BMetals (ICP) TAL EDI
SW846 3050BTAL EDIPreparation, Metals
SW846 7471AMercury (CVAA) TAL EDI
SW846 7471ATAL EDIPreparation, Mercury
EPA MoisturePercent Moisture TAL EDI
Lab References:
TAL EDI = TestAmerica Edison
Method References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
TestAmerica Edison
06/03/2010Page 12 of 623
METHOD / ANALYST SUMMARY
Client: Duffield Associates Job Number: 460-13139-1
Method Analyst Analyst ID
Boykin, Kenneth KBSW846 8260B
Zhao, Chunxin CZSW846 8270C
Manlangit, Ferdie FMSW846 8081A
Diaz, Carol B CBDSW846 8082
Chang, Churn Der CDCSW846 6010B
Sheikh, Razia B RBSSW846 7471A
Dave, Virendra VDEPA Moisture
TestAmerica Edison
06/03/2010Page 13 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-3 6-7
Client Matrix: % Moisture: 18.8
460-13139-2
Soil
Date Sampled: 05/12/2010 0945
Date Received: 05/13/2010 1830
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
05/14/2010 0850
05/18/2010 0018
1.0
8260B Analysis Batch: 460-37643
Prep Batch: 460-37413
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
o37400.d
5.02 g
5 mL
5035
VOAMS12
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
1.2 U 1.20.78Chloromethane
1.2 U 1.20.50Bromomethane
1.2 U 1.20.29Vinyl chloride
1.2 U 1.20.49Chloroethane
1.2 U 1.20.58Methylene Chloride
1.2 U 1.20.32Trichlorofluoromethane
1.2 U 1.20.451,1-Dichloroethene
1.2 U 1.20.311,1-Dichloroethane
1.2 U 1.20.35trans-1,2-Dichloroethene
1.2 U 1.20.29cis-1,2-Dichloroethene
1.2 U 1.20.29Chloroform
1.2 U 1.20.481,2-Dichloroethane
1.2 U 1.20.231,1,1-Trichloroethane
1.2 U 1.20.12Carbon tetrachloride
1.2 U 1.20.37Bromodichloromethane
1.2 U 1.20.391,2-Dichloropropane
1.2 U 1.20.25cis-1,3-Dichloropropene
1.2 U 1.20.45Trichloroethene
1.2 U 1.20.69Dibromochloromethane
1.2 U 1.20.731,1,2-Trichloroethane
1.2 U 1.20.91Benzene
1.2 U 1.20.27trans-1,3-Dichloropropene
6.1 U 6.11.62-Chloroethyl vinyl ether
1.2 U 1.20.86Bromoform
1.2 U 1.20.40Tetrachloroethene
1.2 U 1.20.931,1,2,2-Tetrachloroethane
1.2 U 1.20.37Toluene
1.2 U 1.20.59Chlorobenzene
1.2 U 1.20.23Ethylbenzene
3.7 U 3.70.96Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
92 70 - 1381,2-Dichloroethane-d4 (Surr)
88 66 - 126Toluene-d8 (Surr)
102 72 - 132Bromofluorobenzene
TestAmerica Edison 06/03/2010Page 14 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-3 6-7
Client Matrix: % Moisture: 18.8
460-13139-2
Soil
Date Sampled: 05/12/2010 0945
Date Received: 05/13/2010 1830
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
05/14/2010 0850
05/18/2010 0018
1.0
8260B Analysis Batch: 460-37643
Prep Batch: 460-37413
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
o37400.d
5.02 g
5 mL
5035
VOAMS12
Tentatively Identified Compounds
QualifierEst. Result (ug/Kg)RTAnalyteCas Number
0Number TIC's Found:
NoneTentatively Identified Compound
TestAmerica Edison 06/03/2010Page 15 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-2 5-6
Client Matrix: % Moisture: 12.8
460-13139-4
Soil
Date Sampled: 05/12/2010 1045
Date Received: 05/13/2010 1830
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
05/14/2010 0854
05/18/2010 0043
1.0
8260B Analysis Batch: 460-37643
Prep Batch: 460-37413
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
o37401.d
3.75 g
5 mL
5035
VOAMS12
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
1.5 U 1.50.97Chloromethane
1.5 U 1.50.63Bromomethane
1.5 U 1.50.36Vinyl chloride
1.5 U 1.50.61Chloroethane
1.5 U 1.50.72Methylene Chloride
1.5 U 1.50.40Trichlorofluoromethane
1.5 U 1.50.561,1-Dichloroethene
1.5 U 1.50.391,1-Dichloroethane
1.5 U 1.50.43trans-1,2-Dichloroethene
1.5 U 1.50.36cis-1,2-Dichloroethene
1.5 U 1.50.36Chloroform
1.5 U 1.50.601,2-Dichloroethane
1.5 U 1.50.291,1,1-Trichloroethane
1.5 U 1.50.15Carbon tetrachloride
1.5 U 1.50.46Bromodichloromethane
1.5 U 1.50.491,2-Dichloropropane
1.5 U 1.50.31cis-1,3-Dichloropropene
1.5 U 1.50.55Trichloroethene
1.5 U 1.50.86Dibromochloromethane
1.5 U 1.50.911,1,2-Trichloroethane
1.5 U 1.51.1Benzene
1.5 U 1.50.34trans-1,3-Dichloropropene
7.6 U 7.61.92-Chloroethyl vinyl ether
1.5 U 1.51.1Bromoform
1.5 U 1.50.50Tetrachloroethene
1.5 U 1.51.21,1,2,2-Tetrachloroethane
1.5 U 1.50.46Toluene
1.5 U 1.50.74Chlorobenzene
1.5 U 1.50.29Ethylbenzene
4.6 U 4.61.2Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
95 70 - 1381,2-Dichloroethane-d4 (Surr)
89 66 - 126Toluene-d8 (Surr)
105 72 - 132Bromofluorobenzene
TestAmerica Edison 06/03/2010Page 16 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-2 5-6
Client Matrix: % Moisture: 12.8
460-13139-4
Soil
Date Sampled: 05/12/2010 1045
Date Received: 05/13/2010 1830
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
05/14/2010 0854
05/18/2010 0043
1.0
8260B Analysis Batch: 460-37643
Prep Batch: 460-37413
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
o37401.d
3.75 g
5 mL
5035
VOAMS12
Tentatively Identified Compounds
QualifierEst. Result (ug/Kg)RTAnalyteCas Number
0Number TIC's Found:
NoneTentatively Identified Compound
TestAmerica Edison 06/03/2010Page 17 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-1 2-3
Client Matrix: % Moisture: 6.5
460-13139-5
Soil
Date Sampled: 05/12/2010 1125
Date Received: 05/13/2010 1830
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
05/14/2010 0855
05/18/2010 0108
1.0
8260B Analysis Batch: 460-37643
Prep Batch: 460-37413
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
o37402.d
3.09 g
5 mL
5035
VOAMS12
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
1.7 U 1.71.1Chloromethane
1.7 U 1.70.71Bromomethane
1.7 U 1.70.41Vinyl chloride
1.7 U 1.70.69Chloroethane
1.7 U 1.70.82Methylene Chloride
1.7 U 1.70.45Trichlorofluoromethane
1.7 U 1.70.641,1-Dichloroethene
1.7 U 1.70.441,1-Dichloroethane
1.7 U 1.70.49trans-1,2-Dichloroethene
1.7 U 1.70.41cis-1,2-Dichloroethene
1.7 U 1.70.41Chloroform
1.7 U 1.70.681,2-Dichloroethane
1.7 U 1.70.321,1,1-Trichloroethane
1.7 U 1.70.17Carbon tetrachloride
1.7 U 1.70.53Bromodichloromethane
1.7 U 1.70.551,2-Dichloropropane
1.7 U 1.70.35cis-1,3-Dichloropropene
1.7 U 1.70.63Trichloroethene
1.7 U 1.70.97Dibromochloromethane
1.7 U 1.71.01,1,2-Trichloroethane
1.7 U 1.71.3Benzene
1.7 U 1.70.38trans-1,3-Dichloropropene
8.7 U 8.72.22-Chloroethyl vinyl ether
1.7 U 1.71.2Bromoform
1.7 U 1.70.57Tetrachloroethene
1.7 U 1.71.31,1,2,2-Tetrachloroethane
1.7 U 1.70.52Toluene
1.7 U 1.70.83Chlorobenzene
1.7 U 1.70.33Ethylbenzene
5.2 U 5.21.4Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
100 70 - 1381,2-Dichloroethane-d4 (Surr)
90 66 - 126Toluene-d8 (Surr)
108 72 - 132Bromofluorobenzene
TestAmerica Edison 06/03/2010Page 18 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-1 2-3
Client Matrix: % Moisture: 6.5
460-13139-5
Soil
Date Sampled: 05/12/2010 1125
Date Received: 05/13/2010 1830
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
05/14/2010 0855
05/18/2010 0108
1.0
8260B Analysis Batch: 460-37643
Prep Batch: 460-37413
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
o37402.d
3.09 g
5 mL
5035
VOAMS12
Tentatively Identified Compounds
QualifierEst. Result (ug/Kg)RTAnalyteCas Number
0Number TIC's Found:
NoneTentatively Identified Compound
TestAmerica Edison 06/03/2010Page 19 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-5 3-4
Client Matrix: % Moisture: 61.5
460-13139-7
Soil
Date Sampled: 05/12/2010 1230
Date Received: 05/13/2010 1830
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
05/14/2010 0858
05/18/2010 0133
1.0
8260B Analysis Batch: 460-37643
Prep Batch: 460-37413
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
o37403.d
2.50 g
5 mL
5035
VOAMS12
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
5.2 U 5.23.3Chloromethane
5.2 U 5.22.1Bromomethane
5.2 U 5.21.2Vinyl chloride
5.2 U 5.22.1Chloroethane
5.2 U 5.22.4Methylene Chloride
5.2 U 5.21.4Trichlorofluoromethane
5.2 U 5.21.91,1-Dichloroethene
5.2 U 5.21.31,1-Dichloroethane
5.2 U 5.21.5trans-1,2-Dichloroethene
5.2 U 5.21.2cis-1,2-Dichloroethene
5.2 U 5.21.2Chloroform
5.2 U 5.22.01,2-Dichloroethane
5.2 U 5.20.971,1,1-Trichloroethane
5.2 U 5.20.53Carbon tetrachloride
5.2 U 5.21.6Bromodichloromethane
5.2 U 5.21.71,2-Dichloropropane
5.2 U 5.21.0cis-1,3-Dichloropropene
5.2 U 5.21.9Trichloroethene
5.2 U 5.22.9Dibromochloromethane
5.2 U 5.23.11,1,2-Trichloroethane
5.2 U 5.23.8Benzene
5.2 U 5.21.1trans-1,3-Dichloropropene
26 U 266.62-Chloroethyl vinyl ether
5.2 U 5.23.6Bromoform
5.2 U 5.21.7Tetrachloroethene
5.2 U 5.24.01,1,2,2-Tetrachloroethane
5.2 U 5.21.6Toluene
5.2 U 5.22.5Chlorobenzene
5.2 U 5.20.99Ethylbenzene
16 U 164.1Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
89 70 - 1381,2-Dichloroethane-d4 (Surr)
73 66 - 126Toluene-d8 (Surr)
92 72 - 132Bromofluorobenzene
TestAmerica Edison 06/03/2010Page 20 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-5 3-4
Client Matrix: % Moisture: 61.5
460-13139-7
Soil
Date Sampled: 05/12/2010 1230
Date Received: 05/13/2010 1830
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
05/14/2010 0858
05/18/2010 0133
1.0
8260B Analysis Batch: 460-37643
Prep Batch: 460-37413
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
o37403.d
2.50 g
5 mL
5035
VOAMS12
Tentatively Identified Compounds
QualifierEst. Result (ug/Kg)RTAnalyteCas Number
3Number TIC's Found:
67-64-1 1.94 1100Acetone
78-93-3 3.23 2202-Butanone (MEK)
10.68 28 T JUnknown
TestAmerica Edison 06/03/2010Page 21 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-3 6-7
Client Matrix: % Moisture: 18.8
460-13139-2
Soil
Date Sampled: 05/12/2010 0945
Date Received: 05/13/2010 1830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
05/17/2010 0900
05/18/2010 1500
1.0
8270C Analysis Batch: 460-37818
Prep Batch: 460-37564
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
p2888.d
15.00 g
1 mL
3541
BNAMS10
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
410 U 41050Phenol
410 U 410542-Chlorophenol
410 U 410672-Nitrophenol
410 U 410652,4-Dimethylphenol
410 U 410652,4-Dichlorophenol
410 U 410684-Chloro-3-methylphenol
410 U 410732,4,6-Trichlorophenol
1200 U 1200862,4-Dinitrophenol
1200 U 12001004-Nitrophenol
1200 U 12001904,6-Dinitro-2-methylphenol
1200 U 1200200Pentachlorophenol
410 U 41041N-Nitrosodimethylamine
41 U 418.5Bis(2-chloroethyl)ether
410 U 410561,3-Dichlorobenzene
410 U 410611,4-Dichlorobenzene
410 U 410651,2-Dichlorobenzene
41 U 415.4N-Nitrosodi-n-propylamine
41 U 416.9Hexachloroethane
41 U 419.1Nitrobenzene
410 U 41047Isophorone
410 U 41058Bis(2-chloroethoxy)methane
41 U 416.71,2,4-Trichlorobenzene
410 U 41060Naphthalene
83 U 8317Hexachlorobutadiene
410 U 410120Hexachlorocyclopentadiene
410 U 410582-Chloronaphthalene
410 U 41055Dimethyl phthalate
410 U 41058Acenaphthylene
83 U 83102,6-Dinitrotoluene
410 U 41058Acenaphthene
83 U 83122,4-Dinitrotoluene
410 U 41055Diethyl phthalate
410 U 410704-Chlorophenyl phenyl ether
410 U 41069Fluorene
410 U 41066N-Nitrosodiphenylamine
410 U 410734-Bromophenyl phenyl ether
41 U 415.7Hexachlorobenzene
410 U 41071Phenanthrene
410 U 41072Anthracene
410 U 41062Di-n-butyl phthalate
410 U 41068Fluoranthene
410 U 41070Pyrene
410 U * 41087Benzidine
410 U 41048Butyl benzyl phthalate
830 U 830903,3'-Dichlorobenzidine
28 J 417.5Benzo[a]anthracene
TestAmerica Edison 06/03/2010Page 22 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-3 6-7
Client Matrix: % Moisture: 18.8
460-13139-2
Soil
Date Sampled: 05/12/2010 0945
Date Received: 05/13/2010 1830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
05/17/2010 0900
05/18/2010 1500
1.0
8270C Analysis Batch: 460-37818
Prep Batch: 460-37564
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
p2888.d
15.00 g
1 mL
3541
BNAMS10
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
410 U 41059Chrysene
120 J 41054Bis(2-ethylhexyl) phthalate
410 U 41048Di-n-octyl phthalate
41 U 416.1Benzo[b]fluoranthene
41 U 415.7Benzo[k]fluoranthene
41 U 415.0Benzo[a]pyrene
41 U 416.5Indeno[1,2,3-cd]pyrene
41 U 414.9Dibenz(a,h)anthracene
410 U 41043Benzo[g,h,i]perylene
410 U 41053bis (2-chloroisopropyl) ether
Surrogate %Rec Acceptance LimitsQualifier
80 38 - 105Nitrobenzene-d5
82 41 - 118Phenol-d5
100 16 - 151Terphenyl-d14
78 10 - 1202,4,6-Tribromophenol
76 37 - 1252-Fluorophenol
78 40 - 1092-Fluorobiphenyl
TestAmerica Edison 06/03/2010Page 23 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-3 6-7
Client Matrix: % Moisture: 18.8
460-13139-2
Soil
Date Sampled: 05/12/2010 0945
Date Received: 05/13/2010 1830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
05/17/2010 0900
05/18/2010 1500
1.0
8270C Analysis Batch: 460-37818
Prep Batch: 460-37564
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
p2888.d
15.00 g
1 mL
3541
BNAMS10
Tentatively Identified Compounds
QualifierEst. Result (ug/Kg)RTAnalyteCas Number
0Number TIC's Found:
NoneTentatively Identified Compound
TestAmerica Edison 06/03/2010Page 24 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-2 5-6
Client Matrix: % Moisture: 12.8
460-13139-4
Soil
Date Sampled: 05/12/2010 1045
Date Received: 05/13/2010 1830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
05/17/2010 0900
05/18/2010 2025
1.0
8270C Analysis Batch: 460-37818
Prep Batch: 460-37564
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
p2900.d
15.05 g
1 mL
3541
BNAMS10
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
380 U 38046Phenol
380 U 380512-Chlorophenol
380 U 380622-Nitrophenol
380 U 380612,4-Dimethylphenol
380 U 380612,4-Dichlorophenol
380 U 380634-Chloro-3-methylphenol
380 U 380682,4,6-Trichlorophenol
1100 U 1100802,4-Dinitrophenol
1100 U 1100974-Nitrophenol
1100 U 11001804,6-Dinitro-2-methylphenol
1100 U 1100180Pentachlorophenol
380 U 38039N-Nitrosodimethylamine
38 U 387.9Bis(2-chloroethyl)ether
380 U 380521,3-Dichlorobenzene
380 U 380561,4-Dichlorobenzene
380 U 380601,2-Dichlorobenzene
38 U 385.0N-Nitrosodi-n-propylamine
38 U 386.4Hexachloroethane
38 U 388.5Nitrobenzene
380 U 38043Isophorone
380 U 38054Bis(2-chloroethoxy)methane
38 U 386.21,2,4-Trichlorobenzene
380 U 38055Naphthalene
77 U 7715Hexachlorobutadiene
380 U 380110Hexachlorocyclopentadiene
380 U 380532-Chloronaphthalene
380 U 38051Dimethyl phthalate
97 J 38054Acenaphthylene
77 U 779.62,6-Dinitrotoluene
110 J 38054Acenaphthene
77 U 77112,4-Dinitrotoluene
380 U 38051Diethyl phthalate
380 U 380654-Chlorophenyl phenyl ether
150 J 38064Fluorene
380 U 38062N-Nitrosodiphenylamine
380 U 380674-Bromophenyl phenyl ether
38 U 385.2Hexachlorobenzene
1500 38066Phenanthrene
240 J 38067Anthracene
380 U 38058Di-n-butyl phthalate
1800 38063Fluoranthene
1500 38065Pyrene
380 U * 38080Benzidine
380 U 38044Butyl benzyl phthalate
770 U 770843,3'-Dichlorobenzidine
710 387.0Benzo[a]anthracene
TestAmerica Edison 06/03/2010Page 25 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-2 5-6
Client Matrix: % Moisture: 12.8
460-13139-4
Soil
Date Sampled: 05/12/2010 1045
Date Received: 05/13/2010 1830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
05/17/2010 0900
05/18/2010 2025
1.0
8270C Analysis Batch: 460-37818
Prep Batch: 460-37564
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
p2900.d
15.05 g
1 mL
3541
BNAMS10
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
960 38055Chrysene
210 J 38050Bis(2-ethylhexyl) phthalate
380 U 38045Di-n-octyl phthalate
820 385.6Benzo[b]fluoranthene
300 385.3Benzo[k]fluoranthene
690 384.7Benzo[a]pyrene
610 386.0Indeno[1,2,3-cd]pyrene
130 384.5Dibenz(a,h)anthracene
680 38040Benzo[g,h,i]perylene
380 U 38050bis (2-chloroisopropyl) ether
Surrogate %Rec Acceptance LimitsQualifier
59 38 - 105Nitrobenzene-d5
60 41 - 118Phenol-d5
74 16 - 151Terphenyl-d14
53 10 - 1202,4,6-Tribromophenol
55 37 - 1252-Fluorophenol
67 40 - 1092-Fluorobiphenyl
TestAmerica Edison 06/03/2010Page 26 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-2 5-6
Client Matrix: % Moisture: 12.8
460-13139-4
Soil
Date Sampled: 05/12/2010 1045
Date Received: 05/13/2010 1830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
05/17/2010 0900
05/18/2010 2025
1.0
8270C Analysis Batch: 460-37818
Prep Batch: 460-37564
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
p2900.d
15.05 g
1 mL
3541
BNAMS10
Tentatively Identified Compounds
QualifierEst. Result (ug/Kg)RTAnalyteCas Number
9Number TIC's Found:
9.23 400 T JC15H12 PAH-1
9.25 440 T JC15H12 PAH-2
9.33 550 T JC15H10/C15H12 PAHs
9.36 320 T JC15H12 PAH-3
84-65-1 9.54 510 T J N9,10-Anthracenedione
9.77 330 T JC16H14 PAH
10.49 370 T JC17H12 PAH-1
10.60 380 T JC17H12 PAH-2
13.25 500 T JC20H12 PAH
TestAmerica Edison 06/03/2010Page 27 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-1 2-3
Client Matrix: % Moisture: 6.5
460-13139-5
Soil
Date Sampled: 05/12/2010 1125
Date Received: 05/13/2010 1830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
05/17/2010 0900
05/18/2010 1152
1.0
8270C Analysis Batch: 460-37818
Prep Batch: 460-37564
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
p2881.d
15.02 g
1 mL
3541
BNAMS10
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
350 U 35043Phenol
350 U 350472-Chlorophenol
350 U 350582-Nitrophenol
350 U 350572,4-Dimethylphenol
350 U 350572,4-Dichlorophenol
350 U 350594-Chloro-3-methylphenol
350 U 350632,4,6-Trichlorophenol
1100 U 1100752,4-Dinitrophenol
1100 U 1100914-Nitrophenol
1100 U 11001704,6-Dinitro-2-methylphenol
1100 U 1100170Pentachlorophenol
350 U 35036N-Nitrosodimethylamine
35 U 357.4Bis(2-chloroethyl)ether
350 U 350481,3-Dichlorobenzene
350 U 350531,4-Dichlorobenzene
350 U 350571,2-Dichlorobenzene
35 U 354.7N-Nitrosodi-n-propylamine
35 U 356.0Hexachloroethane
35 U 357.9Nitrobenzene
350 U 35041Isophorone
350 U 35050Bis(2-chloroethoxy)methane
35 U 355.81,2,4-Trichlorobenzene
350 U 35052Naphthalene
72 U 7214Hexachlorobutadiene
350 U 350100Hexachlorocyclopentadiene
350 U 350502-Chloronaphthalene
350 U 35048Dimethyl phthalate
350 U 35051Acenaphthylene
72 U 729.02,6-Dinitrotoluene
350 U 35050Acenaphthene
72 U 72102,4-Dinitrotoluene
350 U 35047Diethyl phthalate
350 U 350614-Chlorophenyl phenyl ether
350 U 35060Fluorene
350 U 35058N-Nitrosodiphenylamine
350 U 350634-Bromophenyl phenyl ether
35 U 354.9Hexachlorobenzene
350 U 35062Phenanthrene
350 U 35062Anthracene
350 U 35054Di-n-butyl phthalate
350 U 35059Fluoranthene
350 U 35061Pyrene
350 U * 35075Benzidine
350 U 35041Butyl benzyl phthalate
720 U 720783,3'-Dichlorobenzidine
35 U 356.5Benzo[a]anthracene
TestAmerica Edison 06/03/2010Page 28 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-1 2-3
Client Matrix: % Moisture: 6.5
460-13139-5
Soil
Date Sampled: 05/12/2010 1125
Date Received: 05/13/2010 1830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
05/17/2010 0900
05/18/2010 1152
1.0
8270C Analysis Batch: 460-37818
Prep Batch: 460-37564
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
p2881.d
15.02 g
1 mL
3541
BNAMS10
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
350 U 35051Chrysene
350 U 35047Bis(2-ethylhexyl) phthalate
350 U 35042Di-n-octyl phthalate
35 U 355.3Benzo[b]fluoranthene
35 U 354.9Benzo[k]fluoranthene
35 U 354.3Benzo[a]pyrene
35 U 355.7Indeno[1,2,3-cd]pyrene
35 U 354.3Dibenz(a,h)anthracene
350 U 35037Benzo[g,h,i]perylene
350 U 35046bis (2-chloroisopropyl) ether
Surrogate %Rec Acceptance LimitsQualifier
70 38 - 105Nitrobenzene-d5
68 41 - 118Phenol-d5
91 16 - 151Terphenyl-d14
93 10 - 1202,4,6-Tribromophenol
58 37 - 1252-Fluorophenol
69 40 - 1092-Fluorobiphenyl
TestAmerica Edison 06/03/2010Page 29 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-1 2-3
Client Matrix: % Moisture: 6.5
460-13139-5
Soil
Date Sampled: 05/12/2010 1125
Date Received: 05/13/2010 1830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
05/17/2010 0900
05/18/2010 1152
1.0
8270C Analysis Batch: 460-37818
Prep Batch: 460-37564
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
p2881.d
15.02 g
1 mL
3541
BNAMS10
Tentatively Identified Compounds
QualifierEst. Result (ug/Kg)RTAnalyteCas Number
0Number TIC's Found:
NoneTentatively Identified Compound
TestAmerica Edison 06/03/2010Page 30 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-5 3-4
Client Matrix: % Moisture: 61.5
460-13139-7
Soil
Date Sampled: 05/12/2010 1230
Date Received: 05/13/2010 1830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
05/17/2010 0900
05/18/2010 1958
1.0
8270C Analysis Batch: 460-37818
Prep Batch: 460-37564
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
p2899.d
15.01 g
1 mL
3541
BNAMS10
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
860 U 860110Phenol
860 U 8601102-Chlorophenol
860 U 8601402-Nitrophenol
860 U 8601402,4-Dimethylphenol
860 U 8601402,4-Dichlorophenol
860 U 8601404-Chloro-3-methylphenol
860 U 8601502,4,6-Trichlorophenol
2600 U 26001802,4-Dinitrophenol
2600 U 26002204-Nitrophenol
2600 U 26004104,6-Dinitro-2-methylphenol
2600 U 2600420Pentachlorophenol
860 U 86088N-Nitrosodimethylamine
86 U 8618Bis(2-chloroethyl)ether
860 U 8601201,3-Dichlorobenzene
860 U 8601301,4-Dichlorobenzene
860 U 8601401,2-Dichlorobenzene
86 U 8611N-Nitrosodi-n-propylamine
86 U 8614Hexachloroethane
86 U 8619Nitrobenzene
860 U 86099Isophorone
860 U 860120Bis(2-chloroethoxy)methane
86 U 86141,2,4-Trichlorobenzene
860 U 860130Naphthalene
170 U 17035Hexachlorobutadiene
860 U 860250Hexachlorocyclopentadiene
860 U 8601202-Chloronaphthalene
860 U 860120Dimethyl phthalate
860 U 860120Acenaphthylene
170 U 170222,6-Dinitrotoluene
200 J 860120Acenaphthene
170 U 170252,4-Dinitrotoluene
860 U 860120Diethyl phthalate
860 U 8601504-Chlorophenyl phenyl ether
440 J 860150Fluorene
860 U 860140N-Nitrosodiphenylamine
860 U 8601504-Bromophenyl phenyl ether
86 U 8612Hexachlorobenzene
1800 860150Phenanthrene
260 J 860150Anthracene
860 U 860130Di-n-butyl phthalate
1300 860140Fluoranthene
790 J 860150Pyrene
860 U * 860180Benzidine
860 U 860100Butyl benzyl phthalate
1700 U 17001903,3'-Dichlorobenzidine
380 8616Benzo[a]anthracene
TestAmerica Edison 06/03/2010Page 31 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-5 3-4
Client Matrix: % Moisture: 61.5
460-13139-7
Soil
Date Sampled: 05/12/2010 1230
Date Received: 05/13/2010 1830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
05/17/2010 0900
05/18/2010 1958
1.0
8270C Analysis Batch: 460-37818
Prep Batch: 460-37564
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
p2899.d
15.01 g
1 mL
3541
BNAMS10
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
560 J 860120Chrysene
190 J 860110Bis(2-ethylhexyl) phthalate
860 U 860100Di-n-octyl phthalate
590 8613Benzo[b]fluoranthene
230 8612Benzo[k]fluoranthene
410 8611Benzo[a]pyrene
460 8614Indeno[1,2,3-cd]pyrene
86 U 8610Dibenz(a,h)anthracene
460 J 86091Benzo[g,h,i]perylene
860 U 860110bis (2-chloroisopropyl) ether
Surrogate %Rec Acceptance LimitsQualifier
55 38 - 105Nitrobenzene-d5
41 41 - 118Phenol-d5
54 16 - 151Terphenyl-d14
52 10 - 1202,4,6-Tribromophenol
39 37 - 1252-Fluorophenol
60 40 - 1092-Fluorobiphenyl
TestAmerica Edison 06/03/2010Page 32 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-5 3-4
Client Matrix: % Moisture: 61.5
460-13139-7
Soil
Date Sampled: 05/12/2010 1230
Date Received: 05/13/2010 1830
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
05/17/2010 0900
05/18/2010 1958
1.0
8270C Analysis Batch: 460-37818
Prep Batch: 460-37564
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
p2899.d
15.01 g
1 mL
3541
BNAMS10
Tentatively Identified Compounds
QualifierEst. Result (ug/Kg)RTAnalyteCas Number
25Number TIC's Found:
12.11 5400 T JUnknown-1
12.22 13000 T JUnknown Alkane-1
13.16 23000 T JUnknown Alkane-2
13.86 4200 T JUnknown-2
7616-22-0 13.96 8500 T J N.gamma.-Tocopherol
14.13 16000 T JUnknown Alkane-3
59-02-9 14.36 11000 T J NVitamin E
15.02 3800 T JUnknown-3
15.21 6500 T JUnknown-4
15.37 10000 T JUnknown-5
15.62 30000 T JUnknown-6
15.72 10000 T JUnknown Sterol
1000194-62-4 15.77 30000 T J N4,4,6a,6b,8a,11,11,14b-Octamethyl-1,4,4a
15.81 4700 T JUnknown-7
15.86 9800 T JUnknown-8
15.98 22000 T JUnknown-9
16.11 36000 T JUnknown-10
16.27 11000 T JUnknown-11
16.32 23000 T JUnknown-12
16.37 10000 T JUnknown-13
16.44 10000 T JUnknown-14
16.55 13000 T JUnknown-15
16.75 3400 T JUnknown-16
16.86 5100 T JUnknown-17
17.40 4500 T JUnknown-18
TestAmerica Edison 06/03/2010Page 33 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-3 6-7
Client Matrix: % Moisture: 18.8
460-13139-2
Soil
Date Sampled: 05/12/2010 0945
Date Received: 05/13/2010 1830
Method:
8081A Organochlorine Pesticides (GC)
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8081A
3541
1.0
05/17/2010 0800
05/14/2010 0915
Analysis Batch: 460-37575
Prep Batch: 460-37420
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type: PRIMARY
15.00 g
10 mL
1 uL
PESTGC1
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
8.3 U 8.31.8Aldrin
8.3 U 8.31.5alpha-BHC
8.3 U 8.31.1beta-BHC
8.3 U 8.31.3delta-BHC
8.3 U 8.30.96gamma-BHC (Lindane)
83 U 8318Chlordane
8.3 U 8.30.994,4'-DDD
8.3 U 8.31.64,4'-DDE
8.3 U 8.31.04,4'-DDT
8.3 U 8.31.6Dieldrin
8.3 U 8.31.7Endosulfan I
8.3 U 8.31.2Endosulfan II
8.3 U 8.31.1Endosulfan sulfate
8.3 U 8.31.2Endrin
8.3 U 8.32.1Endrin aldehyde
8.3 U 8.31.2Heptachlor
8.3 U 8.31.7Heptachlor epoxide
83 U 8317Toxaphene
Surrogate %Rec Acceptance LimitsQualifier
115 22 - 141Tetrachloro-m-xylene
125 10 - 165DCB Decachlorobiphenyl
TestAmerica Edison 06/03/2010Page 34 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-3 6-7
Client Matrix: % Moisture: 18.8
460-13139-2
Soil
Date Sampled: 05/12/2010 0945
Date Received: 05/13/2010 1830
Method:
8081A Organochlorine Pesticides (GC)
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8081A
3541
1.0
05/17/2010 0800
05/14/2010 0915
Analysis Batch: 460-37575
Prep Batch: 460-37420
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type: SECONDARY
15.00 g
10 mL
1 uL
PESTGC1
Surrogate %Rec Acceptance LimitsQualifier
112 22 - 141Tetrachloro-m-xylene
105 10 - 165DCB Decachlorobiphenyl
TestAmerica Edison 06/03/2010Page 35 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-2 5-6
Client Matrix: % Moisture: 12.8
460-13139-4
Soil
Date Sampled: 05/12/2010 1045
Date Received: 05/13/2010 1830
Method:
8081A Organochlorine Pesticides (GC)
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8081A
3541
1.0
05/17/2010 0827
05/14/2010 0915
Analysis Batch: 460-37575
Prep Batch: 460-37420
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type: PRIMARY
15.01 g
10 mL
1 uL
PESTGC1
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
7.7 U 7.71.7Aldrin
7.7 U 7.71.4alpha-BHC
7.7 U 7.71.0beta-BHC
7.7 U 7.71.2delta-BHC
7.7 U 7.70.89gamma-BHC (Lindane)
170 p 7717Chlordane
55 7.70.924,4'-DDD
8.6 p 7.71.54,4'-DDE
29 7.70.964,4'-DDT
5.5 J p 7.71.5Dieldrin
7.7 U 7.71.6Endosulfan I
7.7 U 7.71.2Endosulfan II
7.7 U 7.70.99Endosulfan sulfate
7.7 U 7.71.1Endrin
7.7 U 7.71.9Endrin aldehyde
7.7 U 7.71.1Heptachlor
7.7 U 7.71.5Heptachlor epoxide
77 U 7716Toxaphene
Surrogate %Rec Acceptance LimitsQualifier
121 22 - 141Tetrachloro-m-xylene
168 10 - 165XDCB Decachlorobiphenyl
TestAmerica Edison 06/03/2010Page 36 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-2 5-6
Client Matrix: % Moisture: 12.8
460-13139-4
Soil
Date Sampled: 05/12/2010 1045
Date Received: 05/13/2010 1830
Method:
8081A Organochlorine Pesticides (GC)
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8081A
3541
1.0
05/17/2010 0827
05/14/2010 0915
Analysis Batch: 460-37575
Prep Batch: 460-37420
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type: SECONDARY
15.01 g
10 mL
1 uL
PESTGC1
Surrogate %Rec Acceptance LimitsQualifier
106 22 - 141Tetrachloro-m-xylene
155 10 - 165DCB Decachlorobiphenyl
TestAmerica Edison 06/03/2010Page 37 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-1 2-3
Client Matrix: % Moisture: 6.5
460-13139-5
Soil
Date Sampled: 05/12/2010 1125
Date Received: 05/13/2010 1830
Method:
8081A Organochlorine Pesticides (GC)
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8081A
3541
1.0
05/17/2010 0841
05/14/2010 0915
Analysis Batch: 460-37575
Prep Batch: 460-37420
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type: PRIMARY
15.00 g
10 mL
1 uL
PESTGC1
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
7.2 U 7.21.6Aldrin
7.2 U 7.21.3alpha-BHC
7.2 U 7.20.97beta-BHC
7.2 U 7.21.1delta-BHC
7.2 U 7.20.83gamma-BHC (Lindane)
72 U 7216Chlordane
7.2 U 7.20.864,4'-DDD
7.2 U 7.21.44,4'-DDE
7.2 U 7.20.904,4'-DDT
7.2 U 7.21.4Dieldrin
7.2 U 7.21.5Endosulfan I
7.2 U 7.21.1Endosulfan II
7.2 U 7.20.92Endosulfan sulfate
7.2 U 7.21.0Endrin
7.2 U 7.21.8Endrin aldehyde
7.2 U 7.21.0Heptachlor
7.2 U 7.21.4Heptachlor epoxide
72 U 7215Toxaphene
Surrogate %Rec Acceptance LimitsQualifier
117 22 - 141Tetrachloro-m-xylene
138 10 - 165DCB Decachlorobiphenyl
TestAmerica Edison 06/03/2010Page 38 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-1 2-3
Client Matrix: % Moisture: 6.5
460-13139-5
Soil
Date Sampled: 05/12/2010 1125
Date Received: 05/13/2010 1830
Method:
8081A Organochlorine Pesticides (GC)
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8081A
3541
1.0
05/17/2010 0841
05/14/2010 0915
Analysis Batch: 460-37575
Prep Batch: 460-37420
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type: SECONDARY
15.00 g
10 mL
1 uL
PESTGC1
Surrogate %Rec Acceptance LimitsQualifier
113 22 - 141Tetrachloro-m-xylene
118 10 - 165DCB Decachlorobiphenyl
TestAmerica Edison 06/03/2010Page 39 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-5 3-4
Client Matrix: % Moisture: 61.5
460-13139-7
Soil
Date Sampled: 05/12/2010 1230
Date Received: 05/13/2010 1830
Method:
8081A Organochlorine Pesticides (GC)
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8081A
3541
1.0
05/17/2010 0909
05/14/2010 0915
Analysis Batch: 460-37575
Prep Batch: 460-37420
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type: PRIMARY
15.00 g
10 mL
1 uL
PESTGC1
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
17 U 173.8Aldrin
17 U 173.2alpha-BHC
17 U 172.4beta-BHC
17 U 172.7delta-BHC
16 J p 172.0gamma-BHC (Lindane)
1700 17038Chlordane
17 U 172.14,4'-DDD
18 p 173.44,4'-DDE
17 U 172.24,4'-DDT
28 173.4Dieldrin
17 U 173.7Endosulfan I
17 U 172.6Endosulfan II
17 U 172.2Endosulfan sulfate
17 U 172.4Endrin
17 U 174.3Endrin aldehyde
17 U 172.5Heptachlor
17 U 173.5Heptachlor epoxide
170 U 17036Toxaphene
Surrogate %Rec Acceptance LimitsQualifier
76 22 - 141Tetrachloro-m-xylene
75 10 - 165DCB Decachlorobiphenyl
TestAmerica Edison 06/03/2010Page 40 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-5 3-4
Client Matrix: % Moisture: 61.5
460-13139-7
Soil
Date Sampled: 05/12/2010 1230
Date Received: 05/13/2010 1830
Method:
8081A Organochlorine Pesticides (GC)
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8081A
3541
1.0
05/17/2010 0909
05/14/2010 0915
Analysis Batch: 460-37575
Prep Batch: 460-37420
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type: SECONDARY
15.00 g
10 mL
1 uL
PESTGC1
Surrogate %Rec Acceptance LimitsQualifier
84 22 - 141Tetrachloro-m-xylene
78 10 - 165DCB Decachlorobiphenyl
TestAmerica Edison 06/03/2010Page 41 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-3 6-7
Client Matrix: % Moisture: 18.8
460-13139-2
Soil
Date Sampled: 05/12/2010 0945
Date Received: 05/13/2010 1830
Method:
8082 Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8082
3541
1.0
05/14/2010 1959
05/14/2010 0719
Analysis Batch: 460-37531
Prep Batch: 460-37391
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type: PRIMARY
15.00 g
10 mL
PESTGC7
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
83 U 8316Aroclor 1016
83 U 8325Aroclor 1221
83 U 8347Aroclor 1232
83 U 8316Aroclor 1242
83 U 8322Aroclor 1248
83 U 8328Aroclor 1254
83 U 839.2Aroclor 1260
83 U 8314Aroclor 1262
83 U 8314Aroclor 1268
Surrogate %Rec Acceptance LimitsQualifier
108 27 - 165DCB Decachlorobiphenyl
TestAmerica Edison 06/03/2010Page 42 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-3 6-7
Client Matrix: % Moisture: 18.8
460-13139-2
Soil
Date Sampled: 05/12/2010 0945
Date Received: 05/13/2010 1830
Method:
8082 Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8082
3541
1.0
05/14/2010 1959
05/14/2010 0719
Analysis Batch: 460-37531
Prep Batch: 460-37391
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type: SECONDARY
15.00 g
10 mL
PESTGC7
Surrogate %Rec Acceptance LimitsQualifier
106 27 - 165DCB Decachlorobiphenyl
TestAmerica Edison 06/03/2010Page 43 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-2 5-6
Client Matrix: % Moisture: 12.8
460-13139-4
Soil
Date Sampled: 05/12/2010 1045
Date Received: 05/13/2010 1830
Method:
8082 Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8082
3541
1.0
05/14/2010 2032
05/14/2010 0719
Analysis Batch: 460-37531
Prep Batch: 460-37391
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type: PRIMARY
15.03 g
10 mL
PESTGC7
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
77 U 7715Aroclor 1016
77 U 7723Aroclor 1221
77 U 7743Aroclor 1232
77 U 7715Aroclor 1242
77 U 7720Aroclor 1248
77 U 7726Aroclor 1254
77 U 778.6Aroclor 1260
77 U 7713Aroclor 1262
77 U 7713Aroclor 1268
Surrogate %Rec Acceptance LimitsQualifier
110 27 - 165DCB Decachlorobiphenyl
TestAmerica Edison 06/03/2010Page 44 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-2 5-6
Client Matrix: % Moisture: 12.8
460-13139-4
Soil
Date Sampled: 05/12/2010 1045
Date Received: 05/13/2010 1830
Method:
8082 Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8082
3541
1.0
05/14/2010 2032
05/14/2010 0719
Analysis Batch: 460-37531
Prep Batch: 460-37391
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type: SECONDARY
15.03 g
10 mL
PESTGC7
Surrogate %Rec Acceptance LimitsQualifier
97 27 - 165DCB Decachlorobiphenyl
TestAmerica Edison 06/03/2010Page 45 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-1 2-3
Client Matrix: % Moisture: 6.5
460-13139-5
Soil
Date Sampled: 05/12/2010 1125
Date Received: 05/13/2010 1830
Method:
8082 Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8082
3541
1.0
05/14/2010 2048
05/14/2010 0719
Analysis Batch: 460-37531
Prep Batch: 460-37391
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type: PRIMARY
15.02 g
10 mL
PESTGC7
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
72 U 7214Aroclor 1016
72 U 7222Aroclor 1221
72 U 7241Aroclor 1232
72 U 7214Aroclor 1242
72 U 7219Aroclor 1248
72 U 7224Aroclor 1254
72 U 728.0Aroclor 1260
72 U 7212Aroclor 1262
72 U 7212Aroclor 1268
Surrogate %Rec Acceptance LimitsQualifier
113 27 - 165DCB Decachlorobiphenyl
TestAmerica Edison 06/03/2010Page 46 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-1 2-3
Client Matrix: % Moisture: 6.5
460-13139-5
Soil
Date Sampled: 05/12/2010 1125
Date Received: 05/13/2010 1830
Method:
8082 Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8082
3541
1.0
05/14/2010 2048
05/14/2010 0719
Analysis Batch: 460-37531
Prep Batch: 460-37391
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type: SECONDARY
15.02 g
10 mL
PESTGC7
Surrogate %Rec Acceptance LimitsQualifier
109 27 - 165DCB Decachlorobiphenyl
TestAmerica Edison 06/03/2010Page 47 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-5 3-4
Client Matrix: % Moisture: 61.5
460-13139-7
Soil
Date Sampled: 05/12/2010 1230
Date Received: 05/13/2010 1830
Method:
8082 Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8082
3541
1.0
05/14/2010 2121
05/14/2010 0719
Analysis Batch: 460-37531
Prep Batch: 460-37391
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type: PRIMARY
15.02 g
10 mL
PESTGC7
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
170 U 17033Aroclor 1016
170 U 17052Aroclor 1221
170 U 17099Aroclor 1232
170 U 17033Aroclor 1242
170 U 17046Aroclor 1248
170 U 17059Aroclor 1254
170 U 17019Aroclor 1260
170 U 17030Aroclor 1262
170 U 17030Aroclor 1268
Surrogate %Rec Acceptance LimitsQualifier
55 27 - 165DCB Decachlorobiphenyl
TestAmerica Edison 06/03/2010Page 48 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-5 3-4
Client Matrix: % Moisture: 61.5
460-13139-7
Soil
Date Sampled: 05/12/2010 1230
Date Received: 05/13/2010 1830
Method:
8082 Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8082
3541
1.0
05/14/2010 2121
05/14/2010 0719
Analysis Batch: 460-37531
Prep Batch: 460-37391
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type: SECONDARY
15.02 g
10 mL
PESTGC7
Surrogate %Rec Acceptance LimitsQualifier
65 27 - 165DCB Decachlorobiphenyl
TestAmerica Edison 06/03/2010Page 49 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-3 6-7
Client Matrix: % Moisture: 18.8
460-13139-2
Soil
Date Sampled: 05/12/2010 0945
Date Received: 05/13/2010 1830
6010B Metals (ICP)
Method: 6010B Analysis Batch: 460-37705 Instrument ID:
Preparation: Prep Batch: 460-37477 Lab File ID: 05182010A.txt
Dilution: 4.0 Initial Weight/Volume: 1.06 g
Date Analyzed: 05/18/2010 1155 Final Weight/Volume: 50 mL
Date Prepared: 05/14/2010 1542
3050B
ICP4
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
2.3 U 2.31.0Antimony
1.9 1.20.81Arsenic
0.20 J 0.460.20Beryllium
1.2 U 1.20.18Cadmium
9.1 2.31.4Chromium
13.9 5.80.95Copper
17.5 1.20.58Lead
7.0 J 9.30.62Nickel
2.3 U 2.31.1Selenium
2.3 U 2.30.18Silver
2.3 U 2.31.1Thallium
31.3 7.01.1Zinc
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 460-37472 Instrument ID:
Preparation: Prep Batch: 460-37424 Lab File ID: 37424hg1.PRN
Dilution: 1.0 Initial Weight/Volume: 0.63 g
Date Analyzed: 05/14/2010 1252 Final Weight/Volume: 100 mL
Date Prepared: 05/14/2010 0925
7471A
LEEMAN5
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
0.039 U 0.0390.030Mercury
TestAmerica Edison 06/03/2010Page 50 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-2 5-6
Client Matrix: % Moisture: 12.8
460-13139-4
Soil
Date Sampled: 05/12/2010 1045
Date Received: 05/13/2010 1830
6010B Metals (ICP)
Method: 6010B Analysis Batch: 460-37705 Instrument ID:
Preparation: Prep Batch: 460-37477 Lab File ID: 05182010A.txt
Dilution: 4.0 Initial Weight/Volume: 1.00 g
Date Analyzed: 05/18/2010 1201 Final Weight/Volume: 50 mL
Date Prepared: 05/14/2010 1542
3050B
ICP4
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
2.3 U 2.31.0Antimony
4.5 1.10.80Arsenic
0.37 J 0.460.20Beryllium
0.98 J 1.10.18Cadmium
17.9 2.31.4Chromium
71.8 5.70.94Copper
251 1.10.57Lead
11.9 9.20.61Nickel
2.3 U 2.31.1Selenium
4.9 B 2.30.17Silver
2.3 U 2.31.1Thallium
137 6.91.1Zinc
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 460-37472 Instrument ID:
Preparation: Prep Batch: 460-37424 Lab File ID: 37424hg1.PRN
Dilution: 1.0 Initial Weight/Volume: 0.64 g
Date Analyzed: 05/14/2010 1255 Final Weight/Volume: 100 mL
Date Prepared: 05/14/2010 0925
7471A
LEEMAN5
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
0.22 0.0350.028Mercury
TestAmerica Edison 06/03/2010Page 51 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-1 2-3
Client Matrix: % Moisture: 6.5
460-13139-5
Soil
Date Sampled: 05/12/2010 1125
Date Received: 05/13/2010 1830
6010B Metals (ICP)
Method: 6010B Analysis Batch: 460-37705 Instrument ID:
Preparation: Prep Batch: 460-37477 Lab File ID: 05182010A.txt
Dilution: 4.0 Initial Weight/Volume: 1.06 g
Date Analyzed: 05/18/2010 1204 Final Weight/Volume: 50 mL
Date Prepared: 05/14/2010 1542
3050B
ICP4
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
2.0 U 2.00.89Antimony
1.4 1.00.70Arsenic
0.40 U 0.400.18Beryllium
1.0 U 1.00.16Cadmium
4.6 2.01.2Chromium
7.2 5.00.82Copper
7.9 1.00.50Lead
5.4 J 8.10.54Nickel
2.0 U 2.00.94Selenium
2.0 U 2.00.15Silver
2.0 U 2.00.98Thallium
19.2 6.10.99Zinc
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 460-37472 Instrument ID:
Preparation: Prep Batch: 460-37424 Lab File ID: 37424hg1.PRN
Dilution: 1.0 Initial Weight/Volume: 0.60 g
Date Analyzed: 05/14/2010 1226 Final Weight/Volume: 100 mL
Date Prepared: 05/14/2010 0925
7471A
LEEMAN5
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
0.035 U 0.0350.028Mercury
TestAmerica Edison 06/03/2010Page 52 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
Client Sample ID:
Lab Sample ID:
TB-5 3-4
Client Matrix: % Moisture: 61.5
460-13139-7
Soil
Date Sampled: 05/12/2010 1230
Date Received: 05/13/2010 1830
6010B Metals (ICP)
Method: 6010B Analysis Batch: 460-37705 Instrument ID:
Preparation: Prep Batch: 460-37477 Lab File ID: 05182010A.txt
Dilution: 4.0 Initial Weight/Volume: 1.02 g
Date Analyzed: 05/18/2010 1210 Final Weight/Volume: 50 mL
Date Prepared: 05/14/2010 1542
3050B
ICP4
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
5.1 U 5.12.2Antimony
3.2 2.51.8Arsenic
1.0 U 1.00.45Beryllium
1.1 J 2.50.40Cadmium
6.7 5.13.0Chromium
22.0 12.72.1Copper
222 2.51.3Lead
7.0 J 20.41.4Nickel
5.1 U 5.12.4Selenium
5.1 U 5.10.39Silver
5.1 U 5.12.5Thallium
152 15.32.5Zinc
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 460-37472 Instrument ID:
Preparation: Prep Batch: 460-37424 Lab File ID: 37424hg1.PRN
Dilution: 1.0 Initial Weight/Volume: 0.63 g
Date Analyzed: 05/14/2010 1259 Final Weight/Volume: 100 mL
Date Prepared: 05/14/2010 0925
7471A
LEEMAN5
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
0.31 0.0820.064Mercury
TestAmerica Edison 06/03/2010Page 53 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
General Chemistry
Client Sample ID:
Lab Sample ID:
TB-3 2-3
Client Matrix:
460-13139-1
Soil
Date Sampled: 05/12/2010 0900
Date Received: 05/13/2010 1830
Analyte Result Qual Units RL RL Dil Method
Percent Moisture 17.9 % 1.0 1.0 1.0 Moisture
Analysis Batch: 460-37508 DryWt Corrected: NDate Analyzed: 05/14/2010 2147
Percent Solids 82.1 % 1.0 1.0 1.0 Moisture
Analysis Batch: 460-37508 DryWt Corrected: NDate Analyzed: 05/14/2010 2147
TestAmerica Edison 06/03/2010Page 54 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
General Chemistry
Client Sample ID:
Lab Sample ID:
TB-3 6-7
Client Matrix:
460-13139-2
Soil
Date Sampled: 05/12/2010 0945
Date Received: 05/13/2010 1830
Analyte Result Qual Units RL RL Dil Method
Percent Moisture 18.8 % 1.0 1.0 1.0 Moisture
Analysis Batch: 460-37508 DryWt Corrected: NDate Analyzed: 05/14/2010 2147
Percent Solids 81.2 % 1.0 1.0 1.0 Moisture
Analysis Batch: 460-37508 DryWt Corrected: NDate Analyzed: 05/14/2010 2147
TestAmerica Edison 06/03/2010Page 55 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
General Chemistry
Client Sample ID:
Lab Sample ID:
TB-2 2-3
Client Matrix:
460-13139-3
Soil
Date Sampled: 05/12/2010 1030
Date Received: 05/13/2010 1830
Analyte Result Qual Units RL RL Dil Method
Percent Moisture 13.9 % 1.0 1.0 1.0 Moisture
Analysis Batch: 460-37508 DryWt Corrected: NDate Analyzed: 05/14/2010 2147
Percent Solids 86.1 % 1.0 1.0 1.0 Moisture
Analysis Batch: 460-37508 DryWt Corrected: NDate Analyzed: 05/14/2010 2147
TestAmerica Edison 06/03/2010Page 56 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
General Chemistry
Client Sample ID:
Lab Sample ID:
TB-2 5-6
Client Matrix:
460-13139-4
Soil
Date Sampled: 05/12/2010 1045
Date Received: 05/13/2010 1830
Analyte Result Qual Units RL RL Dil Method
Percent Moisture 12.8 % 1.0 1.0 1.0 Moisture
Analysis Batch: 460-37508 DryWt Corrected: NDate Analyzed: 05/14/2010 2147
Percent Solids 87.2 % 1.0 1.0 1.0 Moisture
Analysis Batch: 460-37508 DryWt Corrected: NDate Analyzed: 05/14/2010 2147
TestAmerica Edison 06/03/2010Page 57 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
General Chemistry
Client Sample ID:
Lab Sample ID:
TB-1 2-3
Client Matrix:
460-13139-5
Soil
Date Sampled: 05/12/2010 1125
Date Received: 05/13/2010 1830
Analyte Result Qual Units RL RL Dil Method
Percent Moisture 6.5 % 1.0 1.0 1.0 Moisture
Analysis Batch: 460-37508 DryWt Corrected: NDate Analyzed: 05/14/2010 2147
Percent Solids 93.5 % 1.0 1.0 1.0 Moisture
Analysis Batch: 460-37508 DryWt Corrected: NDate Analyzed: 05/14/2010 2147
TestAmerica Edison 06/03/2010Page 58 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
General Chemistry
Client Sample ID:
Lab Sample ID:
TB-1 5-6
Client Matrix:
460-13139-6
Soil
Date Sampled: 05/12/2010 1145
Date Received: 05/13/2010 1830
Analyte Result Qual Units RL RL Dil Method
Percent Moisture 11.9 % 1.0 1.0 1.0 Moisture
Analysis Batch: 460-37508 DryWt Corrected: NDate Analyzed: 05/14/2010 2147
Percent Solids 88.1 % 1.0 1.0 1.0 Moisture
Analysis Batch: 460-37508 DryWt Corrected: NDate Analyzed: 05/14/2010 2147
TestAmerica Edison 06/03/2010Page 59 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
General Chemistry
Client Sample ID:
Lab Sample ID:
TB-5 3-4
Client Matrix:
460-13139-7
Soil
Date Sampled: 05/12/2010 1230
Date Received: 05/13/2010 1830
Analyte Result Qual Units RL RL Dil Method
Percent Moisture 61.5 % 1.0 1.0 1.0 Moisture
Analysis Batch: 460-37639 DryWt Corrected: NDate Analyzed: 05/17/2010 1956
Percent Solids 38.5 % 1.0 1.0 1.0 Moisture
Analysis Batch: 460-37639 DryWt Corrected: NDate Analyzed: 05/17/2010 1956
TestAmerica Edison 06/03/2010Page 60 of 623
Analytical Data
Client: Duffield Associates Job Number: 460-13139-1
General Chemistry
Client Sample ID:
Lab Sample ID:
TB-4 6-7
Client Matrix:
460-13139-8
Soil
Date Sampled: 05/12/2010 1340
Date Received: 05/13/2010 1830
Analyte Result Qual Units RL RL Dil Method
Percent Moisture 16.3 % 1.0 1.0 1.0 Moisture
Analysis Batch: 460-37508 DryWt Corrected: NDate Analyzed: 05/14/2010 2147
Percent Solids 83.7 % 1.0 1.0 1.0 Moisture
Analysis Batch: 460-37508 DryWt Corrected: NDate Analyzed: 05/14/2010 2147
TestAmerica Edison 06/03/2010Page 61 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
Surrogate Recovery Report
8260B Volatile Organic Compounds (GC/MS)
Client Matrix: Solid
Lab Sample ID Client Sample ID
DCA TOL BFB
%Rec %Rec %Rec
460-13139-2 TB-3 6-7 92 88 102
460-13139-4 TB-2 5-6 95 89 105
460-13139-5 TB-1 2-3 100 90 108
460-13139-7 TB-5 3-4 89 73 92
MB 460-37643/5 104 92 107
LCS 460-37643/3 89 90 108
LCSD 460-37643/4 90 95 106
Surrogate Acceptance Limits
DCA = 1,2-Dichloroethane-d4 (Surr) 70-138
TOL = Toluene-d8 (Surr) 66-126
BFB = Bromofluorobenzene 72-132
TestAmerica Edison
06/03/2010Page 62 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
Surrogate Recovery Report
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Client Matrix: Solid
Lab Sample ID Client Sample ID
2FP PHL NBZ FBP TBP TPH
%Rec %Rec %Rec %Rec %Rec %Rec
460-13139-2 TB-3 6-7 76 82 80 78 78 100
460-13139-4 TB-2 5-6 55 60 59 67 53 74
460-13139-5 TB-1 2-3 58 68 70 69 93 91
460-13139-7 TB-5 3-4 39 41 55 60 52 54
MB 460-37564/1-A 76 82 80 78 82 93
LCS 460-37564/2-A 74 78 82 80 99 89
460-13139-5 MS TB-1 2-3 MS 74 79 80 80 67 91
460-13139-5 MSD TB-1 2-3 MSD 72 75 81 82 66 89
Surrogate Acceptance Limits
2FP = 2-Fluorophenol 37-125
PHL = Phenol-d5 41-118
NBZ = Nitrobenzene-d5 38-105
FBP = 2-Fluorobiphenyl 40-109
TBP = 2,4,6-Tribromophenol 10-120
TPH = Terphenyl-d14 16-151
TestAmerica Edison
06/03/2010Page 63 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
Surrogate Recovery Report
8081A Organochlorine Pesticides (GC)
Client Matrix: Solid
Lab Sample ID Client Sample ID
TCX1 TCX2 DCB1 DCB2
%Rec %Rec %Rec %Rec
460-13139-2 TB-3 6-7 115 112 125 105
460-13139-4 TB-2 5-6 121 106 155 168X
460-13139-5 TB-1 2-3 117 113 138 118
460-13139-7 TB-5 3-4 84 76 78 75
MB 460-37420/1-A 76 75 145 118
LCS 460-37420/2-A 75 71 93 92
460-13147-A-2-B MS 107 94 132 123
460-13147-A-2-C
MSD
101 91 147 56p
Surrogate Acceptance Limits
TCX = Tetrachloro-m-xylene 22-141
DCB = DCB Decachlorobiphenyl 10-165
TestAmerica Edison
06/03/2010Page 64 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
Surrogate Recovery Report
8082 Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Client Matrix: Solid
Lab Sample ID Client Sample ID
DCB1 DCB2
%Rec %Rec
460-13139-2 TB-3 6-7 106 108
460-13139-4 TB-2 5-6 110 97
460-13139-5 TB-1 2-3 109 113
460-13139-7 TB-5 3-4 65 55
MB 460-37391/1-A 98 94
LCS 460-37391/2-A 104 110
460-13137-A-1-B MS 108 106
460-13137-A-1-C
MSD
91 91
Surrogate Acceptance Limits
DCB = DCB Decachlorobiphenyl 27-165
TestAmerica Edison
06/03/2010Page 65 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
SolidClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
05/17/2010 2011
Method Blank - Batch: 460-37643
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 460-37643
Prep Batch: N/A o37390.d
5 mL
5 mL
N/A
Units: ug/Kg
Method: 8260B
Preparation: N/A
VOAMS12MB 460-37643/5
Analyte RLMDLQualResult
1.0 U 1.00.63Chloromethane
1.0 U 1.00.41Bromomethane
1.0 U 1.00.23Vinyl chloride
1.0 U 1.00.40Chloroethane
1.0 U 1.00.47Methylene Chloride
1.0 U 1.00.26Trichlorofluoromethane
1.0 U 1.00.371,1-Dichloroethene
1.0 U 1.00.251,1-Dichloroethane
1.0 U 1.00.28trans-1,2-Dichloroethene
1.0 U 1.00.24cis-1,2-Dichloroethene
1.0 U 1.00.24Chloroform
1.0 U 1.00.391,2-Dichloroethane
1.0 U 1.00.191,1,1-Trichloroethane
1.0 U 1.00.10Carbon tetrachloride
1.0 U 1.00.30Bromodichloromethane
1.0 U 1.00.321,2-Dichloropropane
1.0 U 1.00.20cis-1,3-Dichloropropene
1.0 U 1.00.36Trichloroethene
1.0 U 1.00.56Dibromochloromethane
1.0 U 1.00.591,1,2-Trichloroethane
1.0 U 1.00.74Benzene
1.0 U 1.00.22trans-1,3-Dichloropropene
5.0 U 5.01.32-Chloroethyl vinyl ether
1.0 U 1.00.70Bromoform
1.0 U 1.00.33Tetrachloroethene
1.0 U 1.00.761,1,2,2-Tetrachloroethane
1.0 U 1.00.30Toluene
1.0 U 1.00.48Chlorobenzene
1.0 U 1.00.19Ethylbenzene
3.0 U 3.00.79Xylenes, Total
Surrogate % Rec Acceptance Limits
1,2-Dichloroethane-d4 (Surr) 104 70 - 138
Toluene-d8 (Surr) 92 66 - 126
Bromofluorobenzene 107 72 - 132
Method Blank TICs- Batch: 460-37643
Cas Number Analyte RT Est. Result Qual
Tentatively Identified Compound None
TestAmerica Edison 06/03/2010Page 66 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
05/17/2010 1746
05/17/2010 1810
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 460-37643
1.0
1.0
Solid
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Solid
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/Kg
Prep Batch: N/A
Analysis Batch: 460-37643
N/A
o37386.d
5 mL
5 mL
o37387.d
5 mL
5 mL
ug/Kg
Analysis Batch: 460-37643
Prep Batch: N/A
Method: 8260B
Preparation: N/A
N/A
VOAMS12
VOAMS12
LCS 460-37643/3
LCSD 460-37643/4
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
9696 50 - 151 0 30Chloromethane
111110 54 - 142 1 30Bromomethane
9897 67 - 133 0 30Vinyl chloride
10099 56 - 146 0 30Chloroethane
134120 74 - 137 11 30Methylene Chloride
105107 61 - 139 2 30Trichlorofluoromethane
116104 71 - 126 11 301,1-Dichloroethene
10899 76 - 125 8 301,1-Dichloroethane
10899 75 - 122 9 30trans-1,2-Dichloroethene
110100 80 - 120 10 30cis-1,2-Dichloroethene
10999 77 - 120 9 30Chloroform
10898 76 - 118 9 301,2-Dichloroethane
115103 78 - 117 11 301,1,1-Trichloroethane
116107 79 - 118 8 30Carbon tetrachloride
115100 79 - 119 14 30Bromodichloromethane
10598 82 - 122 8 301,2-Dichloropropane
10994 80 - 123 15 30cis-1,3-Dichloropropene
10699 79 - 119 7 30Trichloroethene
9183 68 - 120 9 30Dibromochloromethane
10089 73 - 118 12 301,1,2-Trichloroethane
11099 77 - 117 11 30Benzene
8776 67 - 121 14 30trans-1,3-Dichloropropene
8783 74 - 120 5 302-Chloroethyl vinyl ether
8473 59 - 125 13 30Bromoform
11193 80 - 120 18 30Tetrachloroethene
10195 79 - 122 7 301,1,2,2-Tetrachloroethane
10996 75 - 115 12 30Toluene
110100 80 - 120 9 30Chlorobenzene
111105 81 - 121 5 30Ethylbenzene
112103 82 - 122 8 30Xylenes, Total
Surrogate LCS % Rec LCSD % Rec Acceptance Limits
1,2-Dichloroethane-d4 (Surr) 89 90 70 - 138
Toluene-d8 (Surr) 90 95 66 - 126
TestAmerica Edison 06/03/2010Page 67 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
Surrogate LCS % Rec LCSD % Rec Acceptance Limits
Bromofluorobenzene 108 106 72 - 132
Solid
Date Analyzed: Date Analyzed:05/17/2010 1746 05/17/2010 1810
Dilution: Dilution:1.0 1.0
LCS Lab Sample ID:
Client Matrix:
Date Prepared:
LCSD Lab Sample ID:
Client Matrix: Solid
Date Prepared:N/A N/A
Laboratory Control/
Laboratory Duplicate Data Report - Batch: 460-37643
Method: 8260B
Preparation: N/A
Units: ug/KgLCS 460-37643/3 LCSD 460-37643/4
LCSD
Result/Qual
LCS
Result/Qual
LCSD Spike
Amount
LCS Spike
AmountAnalyte
19.219.220.0 20.0Chloromethane
22.322.020.0 20.0Bromomethane
19.519.520.0 20.0Vinyl chloride
19.919.920.0 20.0Chloroethane
26.823.920.0 20.0Methylene Chloride
21.121.520.0 20.0Trichlorofluoromethane
23.120.820.0 20.01,1-Dichloroethene
21.519.820.0 20.01,1-Dichloroethane
21.619.820.0 20.0trans-1,2-Dichloroethene
22.120.020.0 20.0cis-1,2-Dichloroethene
21.819.920.0 20.0Chloroform
21.519.620.0 20.01,2-Dichloroethane
23.020.520.0 20.01,1,1-Trichloroethane
23.321.520.0 20.0Carbon tetrachloride
23.120.120.0 20.0Bromodichloromethane
21.119.520.0 20.01,2-Dichloropropane
21.818.720.0 20.0cis-1,3-Dichloropropene
21.219.820.0 20.0Trichloroethene
18.316.720.0 20.0Dibromochloromethane
20.017.820.0 20.01,1,2-Trichloroethane
21.919.720.0 20.0Benzene
17.515.220.0 20.0trans-1,3-Dichloropropene
17.416.520.0 20.02-Chloroethyl vinyl ether
16.814.720.0 20.0Bromoform
22.318.620.0 20.0Tetrachloroethene
20.318.920.0 20.01,1,2,2-Tetrachloroethane
21.719.220.0 20.0Toluene
21.920.020.0 20.0Chlorobenzene
22.121.120.0 20.0Ethylbenzene
67.161.960.0 60.0Xylenes, Total
TestAmerica Edison 06/03/2010Page 68 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
SolidClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
05/18/2010 1057
Method Blank - Batch: 460-37564
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Analysis Batch: 460-37818
Prep Batch: 460-37564
05/17/2010 0900
p2879.d
15.02 g
1 mL
Units: ug/Kg
Method: 8270C
Preparation: 3541
BNAMS10MB 460-37564/1-A
Analyte RLMDLQualResult
330 U 33040Phenol
330 U 330442-Chlorophenol
330 U 330542-Nitrophenol
330 U 330532,4-Dimethylphenol
330 U 330532,4-Dichlorophenol
330 U 330554-Chloro-3-methylphenol
330 U 330592,4,6-Trichlorophenol
1000 U 1000702,4-Dinitrophenol
1000 U 1000854-Nitrophenol
1000 U 10001604,6-Dinitro-2-methylphenol
1000 U 1000160Pentachlorophenol
330 U 33034N-Nitrosodimethylamine
33 U 336.9Bis(2-chloroethyl)ether
330 U 330451,3-Dichlorobenzene
330 U 330491,4-Dichlorobenzene
330 U 330531,2-Dichlorobenzene
33 U 334.4N-Nitrosodi-n-propylamine
33 U 335.6Hexachloroethane
33 U 337.4Nitrobenzene
330 U 33038Isophorone
330 U 33047Bis(2-chloroethoxy)methane
33 U 335.41,2,4-Trichlorobenzene
330 U 33048Naphthalene
67 U 6713Hexachlorobutadiene
330 U 33097Hexachlorocyclopentadiene
330 U 330472-Chloronaphthalene
330 U 33045Dimethyl phthalate
330 U 33047Acenaphthylene
67 U 678.42,6-Dinitrotoluene
330 U 33047Acenaphthene
67 U 679.62,4-Dinitrotoluene
330 U 33044Diethyl phthalate
330 U 330574-Chlorophenyl phenyl ether
330 U 33056Fluorene
330 U 33054N-Nitrosodiphenylamine
330 U 330594-Bromophenyl phenyl ether
33 U 334.6Hexachlorobenzene
330 U 33058Phenanthrene
330 U 33058Anthracene
330 U 33051Di-n-butyl phthalate
330 U 33055Fluoranthene
330 U 33057Pyrene
330 U 33070Benzidine
TestAmerica Edison 06/03/2010Page 69 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
SolidClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
05/18/2010 1057
Method Blank - Batch: 460-37564
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Analysis Batch: 460-37818
Prep Batch: 460-37564
05/17/2010 0900
p2879.d
15.02 g
1 mL
Units: ug/Kg
Method: 8270C
Preparation: 3541
BNAMS10MB 460-37564/1-A
Analyte RLMDLQualResult
330 U 33039Butyl benzyl phthalate
670 U 670733,3'-Dichlorobenzidine
33 U 336.1Benzo[a]anthracene
330 U 33048Chrysene
330 U 33044Bis(2-ethylhexyl) phthalate
330 U 33039Di-n-octyl phthalate
33 U 334.9Benzo[b]fluoranthene
33 U 334.6Benzo[k]fluoranthene
33 U 334.1Benzo[a]pyrene
33 U 335.3Indeno[1,2,3-cd]pyrene
33 U 334.0Dibenz(a,h)anthracene
330 U 33035Benzo[g,h,i]perylene
330 U 33043bis (2-chloroisopropyl) ether
Surrogate % Rec Acceptance Limits
Nitrobenzene-d5 80 38 - 105
Phenol-d5 82 41 - 118
Terphenyl-d14 93 16 - 151
2,4,6-Tribromophenol 82 10 - 120
2-Fluorophenol 76 37 - 125
2-Fluorobiphenyl 78 40 - 109
Method Blank TICs- Batch: 460-37564
Cas Number Analyte RT Est. Result Qual
2.30Unknown Aldol Condensate-1 497 T A J
2.72Unknown Aldol Condensate-2 16600 T A J
TestAmerica Edison 06/03/2010Page 70 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
Solid
1.0
05/18/2010 1125Date Analyzed:
Lab Control Sample - Batch: 460-37564
Client Matrix:
Lab Sample ID:
Dilution:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
p2880.d
05/17/2010 0900
Analysis Batch: 460-37818
Prep Batch: 460-37564
15.00 g
1 mL
Units: ug/Kg
Method: 8270C
Preparation: 3541
BNAMS10LCS 460-37564/2-A
Analyte QualLimit% Rec.ResultSpike Amount
6670 4950 74 54 - 115Phenol
6670 5140 77 56 - 1102-Chlorophenol
6670 5640 85 55 - 1012-Nitrophenol
6670 5280 79 56 - 1122,4-Dimethylphenol
6670 5340 80 58 - 1152,4-Dichlorophenol
6670 5690 85 55 - 1174-Chloro-3-methylphenol
6670 5360 80 53 - 1182,4,6-Trichlorophenol
6670 1100 16 10 - 1292,4-Dinitrophenol
6670 6490 97 45 - 1144-Nitrophenol
6670 2180 33 10 - 1104,6-Dinitro-2-methylphenol
6670 4830 72 19 - 113Pentachlorophenol
3330 2550 77 40 - 84N-Nitrosodimethylamine
3330 3020 91 44 - 101Bis(2-chloroethyl)ether
3330 2490 75 47 - 841,3-Dichlorobenzene
3330 2500 75 47 - 851,4-Dichlorobenzene
3330 2570 77 48 - 871,2-Dichlorobenzene
3330 3040 91 42 - 107N-Nitrosodi-n-propylamine
3330 2480 74 45 - 90Hexachloroethane
3330 2640 79 42 - 106Nitrobenzene
3330 2850 86 48 - 97Isophorone
3330 2860 86 51 - 100Bis(2-chloroethoxy)methane
3330 2740 82 48 - 941,2,4-Trichlorobenzene
3330 2710 81 53 - 94Naphthalene
3330 2710 81 45 - 98Hexachlorobutadiene
3330 3110 93 24 - 98Hexachlorocyclopentadiene
3330 2700 81 51 - 1022-Chloronaphthalene
3330 2960 89 52 - 112Dimethyl phthalate
3330 2780 83 51 - 103Acenaphthylene
3330 3130 94 51 - 1152,6-Dinitrotoluene
3330 2840 85 46 - 100Acenaphthene
3330 3200 96 53 - 1102,4-Dinitrotoluene
3330 3000 90 52 - 114Diethyl phthalate
3330 2910 87 50 - 1064-Chlorophenyl phenyl ether
3330 2890 87 51 - 108Fluorene
3330 3110 93 49 - 106N-Nitrosodiphenylamine
3330 2910 87 44 - 1024-Bromophenyl phenyl ether
3330 2940 88 43 - 104Hexachlorobenzene
3330 2850 86 48 - 108Phenanthrene
3330 2870 86 50 - 107Anthracene
3330 2980 89 50 - 108Di-n-butyl phthalate
3330 3040 91 49 - 108Fluoranthene
3330 2850 85 49 - 116Pyrene
3330 169 5 J *10 - 61Benzidine
3330 3010 90 49 - 117Butyl benzyl phthalate
TestAmerica Edison 06/03/2010Page 71 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
Solid
1.0
05/18/2010 1125Date Analyzed:
Lab Control Sample - Batch: 460-37564
Client Matrix:
Lab Sample ID:
Dilution:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
p2880.d
05/17/2010 0900
Analysis Batch: 460-37818
Prep Batch: 460-37564
15.00 g
1 mL
Units: ug/Kg
Method: 8270C
Preparation: 3541
BNAMS10LCS 460-37564/2-A
Analyte QualLimit% Rec.ResultSpike Amount
3330 2870 86 24 - 1053,3'-Dichlorobenzidine
3330 2880 86 46 - 112Benzo[a]anthracene
3330 2900 87 45 - 114Chrysene
3330 3010 90 49 - 119Bis(2-ethylhexyl) phthalate
3330 3130 94 40 - 106Di-n-octyl phthalate
3330 3060 92 33 - 96Benzo[b]fluoranthene
3330 2990 90 35 - 115Benzo[k]fluoranthene
3330 2590 78 36 - 89Benzo[a]pyrene
3330 2870 86 43 - 109Indeno[1,2,3-cd]pyrene
3330 2900 87 43 - 107Dibenz(a,h)anthracene
3330 2980 89 43 - 106Benzo[g,h,i]perylene
3330 2700 81 45 - 102bis (2-chloroisopropyl) ether
Surrogate % Rec Acceptance Limits
Nitrobenzene-d5 82 38 - 105
Phenol-d5 78 41 - 118
Terphenyl-d14 89 16 - 151
2,4,6-Tribromophenol 99 10 - 120
2-Fluorophenol 74 37 - 125
2-Fluorobiphenyl 80 40 - 109
TestAmerica Edison 06/03/2010Page 72 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
05/18/2010 1218
05/18/2010 1246
Solid
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 460-37564
1.0
1.0
MS Lab Sample ID:
MSD Lab Sample ID:
Client Matrix:
Date Prepared:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Client Matrix: Solid
Analysis Batch: 460-37818
Analysis Batch: 460-37818
05/17/2010 0900
05/17/2010 0900
Prep Batch: 460-37564
Prep Batch: 460-37564
p2882.d
15.04 g
1 mL
p2883.d
15.03 g
1 mL
Method: 8270C
Preparation: 3541
BNAMS10
BNAMS10
460-13139-5
460-13139-5
Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS
% Rec.
76 73 54 - 115 5 30Phenol
76 75 56 - 110 1 302-Chlorophenol
81 79 55 - 101 3 302-Nitrophenol
78 75 56 - 112 4 302,4-Dimethylphenol
80 76 58 - 115 4 302,4-Dichlorophenol
86 80 55 - 117 7 304-Chloro-3-methylphenol
67 66 53 - 118 2 302,4,6-Trichlorophenol
0 0 10 - 129 NC 30 U F U F2,4-Dinitrophenol
65 65 45 - 114 0 304-Nitrophenol
3 0 10 - 110 NC 30 J F U F4,6-Dinitro-2-methylphenol
22 21 19 - 113 4 30Pentachlorophenol
74 75 40 - 84 1 30N-Nitrosodimethylamine
90 88 44 - 101 2 30Bis(2-chloroethyl)ether
66 67 47 - 84 2 301,3-Dichlorobenzene
69 69 47 - 85 0 301,4-Dichlorobenzene
71 72 48 - 87 1 301,2-Dichlorobenzene
91 87 42 - 107 5 30N-Nitrosodi-n-propylamine
66 68 45 - 90 2 30Hexachloroethane
76 76 42 - 106 0 30Nitrobenzene
84 81 48 - 97 3 30Isophorone
85 83 51 - 100 3 30Bis(2-chloroethoxy)methane
78 78 48 - 94 0 301,2,4-Trichlorobenzene
77 78 53 - 94 1 30Naphthalene
74 76 45 - 98 3 30Hexachlorobutadiene
85 89 24 - 98 4 30Hexachlorocyclopentadiene
79 80 51 - 102 1 302-Chloronaphthalene
85 86 52 - 112 1 30Dimethyl phthalate
82 83 51 - 103 1 30Acenaphthylene
90 90 51 - 115 0 302,6-Dinitrotoluene
84 83 46 - 100 0 30Acenaphthene
87 88 53 - 110 1 302,4-Dinitrotoluene
85 85 52 - 114 1 30Diethyl phthalate
TestAmerica Edison 06/03/2010Page 73 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
05/18/2010 1218
05/18/2010 1246
Solid
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 460-37564
1.0
1.0
MS Lab Sample ID:
MSD Lab Sample ID:
Client Matrix:
Date Prepared:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Client Matrix: Solid
Analysis Batch: 460-37818
Analysis Batch: 460-37818
05/17/2010 0900
05/17/2010 0900
Prep Batch: 460-37564
Prep Batch: 460-37564
p2882.d
15.04 g
1 mL
p2883.d
15.03 g
1 mL
Method: 8270C
Preparation: 3541
BNAMS10
BNAMS10
460-13139-5
460-13139-5
Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS
% Rec.
85 86 50 - 106 1 304-Chlorophenyl phenyl ether
84 85 51 - 108 2 30Fluorene
93 93 49 - 106 0 30N-Nitrosodiphenylamine
88 88 44 - 102 1 304-Bromophenyl phenyl ether
87 87 43 - 104 1 30Hexachlorobenzene
82 85 48 - 108 3 30Phenanthrene
84 85 50 - 107 2 30Anthracene
84 89 50 - 108 6 30Di-n-butyl phthalate
85 91 49 - 108 6 30Fluoranthene
87 84 49 - 116 4 30Pyrene
3 4 10 - 61 38 30 J F J FBenzidine
87 88 49 - 117 1 30Butyl benzyl phthalate
87 89 24 - 105 2 303,3'-Dichlorobenzidine
85 85 46 - 112 1 30Benzo[a]anthracene
87 87 45 - 114 0 30Chrysene
87 88 49 - 119 1 30Bis(2-ethylhexyl) phthalate
87 88 40 - 106 2 30Di-n-octyl phthalate
89 91 33 - 96 2 30Benzo[b]fluoranthene
87 89 35 - 115 3 30Benzo[k]fluoranthene
75 77 36 - 89 2 30Benzo[a]pyrene
88 88 43 - 109 1 30Indeno[1,2,3-cd]pyrene
84 85 43 - 107 1 30Dibenz(a,h)anthracene
87 89 43 - 106 2 30Benzo[g,h,i]perylene
78 79 45 - 102 0 30bis (2-chloroisopropyl) ether
Surrogate MS % Rec MSD % Rec Acceptance Limits
Nitrobenzene-d5 80 81 38 - 105
Phenol-d5 79 75 41 - 118
Terphenyl-d14 91 89 16 - 151
2,4,6-Tribromophenol 67 66 10 - 120
2-Fluorophenol 74 72 37 - 125
2-Fluorobiphenyl 80 82 40 - 109
TestAmerica Edison 06/03/2010Page 74 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
TestAmerica Edison 06/03/2010Page 75 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
Solid
Date Analyzed: Date Analyzed:05/18/2010 1218 05/18/2010 1246
Dilution: Dilution:1.0 1.0
MS Lab Sample ID:
Client Matrix:
Date Prepared:
MSD Lab Sample ID:
Client Matrix: Solid
Date Prepared:05/17/2010 0900 05/17/2010 0900
Matrix Spike/
Matrix Spike Duplicate Data Report - Batch: 460-37564
Method: 8270C
Preparation: 3541
Units: ug/Kg460-13139-5 460-13139-5
MSD
Result/Qual
MS
Result/Qual
MSD Spike
Amount
MS Spike
Amount
Sample
Result/QualAnalyte
350 U 7110 7120 5410 5170Phenol
350 U 7110 7120 5430 53502-Chlorophenol
350 U 7110 7120 5770 56202-Nitrophenol
350 U 7110 7120 5560 53702,4-Dimethylphenol
350 U 7110 7120 5660 54402,4-Dichlorophenol
350 U 7110 7120 6080 56904-Chloro-3-methylphenol
350 U 7110 7120 4770 46702,4,6-Trichlorophenol
1100 U 7110 7120 1100 1100U F U F2,4-Dinitrophenol
1100 U 7110 7120 4630 46304-Nitrophenol
1100 U 7110 7120 191 1100J F U F4,6-Dinitro-2-methylphenol
1100 U 7110 7120 1600 1530Pentachlorophenol
350 U 3560 3560 2620 2660N-Nitrosodimethylamine
35 U 3560 3560 3190 3150Bis(2-chloroethyl)ether
350 U 3560 3560 2340 23901,3-Dichlorobenzene
350 U 3560 3560 2440 24401,4-Dichlorobenzene
350 U 3560 3560 2530 25601,2-Dichlorobenzene
35 U 3560 3560 3240 3100N-Nitrosodi-n-propylamine
35 U 3560 3560 2360 2420Hexachloroethane
35 U 3560 3560 2690 2700Nitrobenzene
350 U 3560 3560 2980 2900Isophorone
350 U 3560 3560 3020 2950Bis(2-chloroethoxy)methane
35 U 3560 3560 2760 27701,2,4-Trichlorobenzene
350 U 3560 3560 2740 2780Naphthalene
72 U 3560 3560 2630 2720Hexachlorobutadiene
350 U 3560 3560 3040 3150Hexachlorocyclopentadiene
350 U 3560 3560 2820 28602-Chloronaphthalene
350 U 3560 3560 3030 3060Dimethyl phthalate
350 U 3560 3560 2920 2940Acenaphthylene
72 U 3560 3560 3210 32002,6-Dinitrotoluene
350 U 3560 3560 2980 2970Acenaphthene
72 U 3560 3560 3110 31502,4-Dinitrotoluene
350 U 3560 3560 3010 3030Diethyl phthalate
350 U 3560 3560 3010 30504-Chlorophenyl phenyl ether
350 U 3560 3560 2970 3020Fluorene
350 U 3560 3560 3310 3320N-Nitrosodiphenylamine
350 U 3560 3560 3110 31304-Bromophenyl phenyl ether
35 U 3560 3560 3080 3110Hexachlorobenzene
350 U 3560 3560 2930 3030Phenanthrene
350 U 3560 3560 2970 3040Anthracene
350 U 3560 3560 2980 3160Di-n-butyl phthalate
350 U 3560 3560 3030 3230Fluoranthene
TestAmerica Edison 06/03/2010Page 76 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
Solid
Date Analyzed: Date Analyzed:05/18/2010 1218 05/18/2010 1246
Dilution: Dilution:1.0 1.0
MS Lab Sample ID:
Client Matrix:
Date Prepared:
MSD Lab Sample ID:
Client Matrix: Solid
Date Prepared:05/17/2010 0900 05/17/2010 0900
Matrix Spike/
Matrix Spike Duplicate Data Report - Batch: 460-37564
Method: 8270C
Preparation: 3541
Units: ug/Kg460-13139-5 460-13139-5
MSD
Result/Qual
MS
Result/Qual
MSD Spike
Amount
MS Spike
Amount
Sample
Result/QualAnalyte
350 U 3560 3560 3110 2980Pyrene
350 U 3560 3560 89.3 131J F J FBenzidine
350 U 3560 3560 3090 3120Butyl benzyl phthalate
720 U 3560 3560 3100 31803,3'-Dichlorobenzidine
35 U 3560 3560 3010 3030Benzo[a]anthracene
350 U 3560 3560 3100 3080Chrysene
350 U 3560 3560 3100 3130Bis(2-ethylhexyl) phthalate
350 U 3560 3560 3080 3150Di-n-octyl phthalate
35 U 3560 3560 3160 3220Benzo[b]fluoranthene
35 U 3560 3560 3090 3180Benzo[k]fluoranthene
35 U 3560 3560 2660 2720Benzo[a]pyrene
35 U 3560 3560 3110 3150Indeno[1,2,3-cd]pyrene
35 U 3560 3560 3000 3030Dibenz(a,h)anthracene
350 U 3560 3560 3110 3170Benzo[g,h,i]perylene
350 U 3560 3560 2780 2800bis (2-chloroisopropyl) ether
TestAmerica Edison 06/03/2010Page 77 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
SolidClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
05/17/2010 0937
Method Blank - Batch: 460-37420
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Analysis Batch: 460-37575
Prep Batch: 460-37420
05/14/2010 0915
xr108835.d
15.00 g
10 mL
1 uL
Units: ug/Kg
Column ID: PRIMARY
Method: 8081A
Preparation: 3541
PESTGC1MB 460-37420/1-A
Analyte RLMDLQualResult
6.7 U 6.71.5Aldrin
6.7 U 6.71.2alpha-BHC
6.7 U 6.70.91beta-BHC
6.7 U 6.71.0delta-BHC
6.7 U 6.70.78gamma-BHC (Lindane)
67 U 6715Chlordane
6.7 U 6.70.804,4'-DDD
6.7 U 6.71.34,4'-DDE
6.7 U 6.70.844,4'-DDT
6.7 U 6.71.3Dieldrin
6.7 U 6.71.4Endosulfan I
6.7 U 6.71.0Endosulfan II
6.7 U 6.70.86Endosulfan sulfate
6.7 U 6.70.94Endrin
6.7 U 6.71.7Endrin aldehyde
6.7 U 6.70.96Heptachlor
6.7 U 6.71.4Heptachlor epoxide
67 U 6714Toxaphene
Surrogate % Rec Acceptance Limits
Tetrachloro-m-xylene 76 22 - 141
DCB Decachlorobiphenyl 145 10 - 165
Surrogate % Rec Acceptance Limits
Tetrachloro-m-xylene 75 22 - 141
DCB Decachlorobiphenyl 118 10 - 165
TestAmerica Edison 06/03/2010Page 78 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
Solid
1.0
05/17/2010 0543Date Analyzed:
Lab Control Sample - Batch: 460-37420
Client Matrix:
Lab Sample ID:
Dilution:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
xf108820.d
05/14/2010 0915
Analysis Batch: 460-37575
Prep Batch: 460-37420
15.00 g
10 mL
1 uL
Units: ug/Kg
Column ID: PRIMARY
Method: 8081A
Preparation: 3541
PESTGC1LCS 460-37420/2-A
Analyte QualLimit% Rec.ResultSpike Amount
133 88.9 67 32 - 152Aldrin
133 96.3 72 41 - 145alpha-BHC
133 104 78 28 - 155beta-BHC
133 121 91 31 - 154delta-BHC
133 98.6 74 33 - 152gamma-BHC (Lindane)
133 94.7 71 50 - 1544,4'-DDD
133 98.1 74 47 - 1504,4'-DDE
133 99.1 74 39 - 1544,4'-DDT
133 89.6 67 40 - 147Dieldrin
133 93.6 70 42 - 147Endosulfan I
133 101 76 32 - 150Endosulfan II
133 103 77 37 - 143Endosulfan sulfate
133 104 78 44 - 149Endrin
133 104 78 34 - 142Endrin aldehyde
133 93.0 70 32 - 152Heptachlor
133 97.0 73 33 - 149Heptachlor epoxide
Surrogate % Rec Acceptance Limits
Tetrachloro-m-xylene 75 22 - 141
DCB Decachlorobiphenyl 93 10 - 165
Solid
1.0
05/17/2010 0543Date Analyzed:
Lab Control Sample - Batch: 460-37420
Client Matrix:
Lab Sample ID:
Dilution:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
xr108820.d
05/14/2010 0915
Analysis Batch: 460-37575
Prep Batch: 460-37420
15.00 g
10 mL
1 uL
Units: ug/Kg
Column ID: SECONDARY
Method: 8081A
Preparation: 3541
PESTGC1LCS 460-37420/2-A
Analyte QualLimit% Rec.ResultSpike Amount
133 82.2 62 32 - 152Aldrin
133 89.0 67 41 - 145alpha-BHC
133 102 76 28 - 155beta-BHC
133 109 82 31 - 154delta-BHC
133 90.2 68 33 - 152gamma-BHC (Lindane)
133 93.4 70 50 - 1544,4'-DDD
133 94.8 71 47 - 1504,4'-DDE
133 97.2 73 39 - 1544,4'-DDT
133 88.6 66 40 - 147Dieldrin
TestAmerica Edison 06/03/2010Page 79 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
Solid
1.0
05/17/2010 0543Date Analyzed:
Lab Control Sample - Batch: 460-37420
Client Matrix:
Lab Sample ID:
Dilution:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
xr108820.d
05/14/2010 0915
Analysis Batch: 460-37575
Prep Batch: 460-37420
15.00 g
10 mL
1 uL
Units: ug/Kg
Column ID: SECONDARY
Method: 8081A
Preparation: 3541
PESTGC1LCS 460-37420/2-A
Analyte QualLimit% Rec.ResultSpike Amount
133 93.3 70 42 - 147Endosulfan I
133 101 75 32 - 150Endosulfan II
133 101 76 37 - 143Endosulfan sulfate
133 101 76 44 - 149Endrin
133 103 78 34 - 142Endrin aldehyde
133 87.2 65 32 - 152Heptachlor
133 93.5 70 33 - 149Heptachlor epoxide
Surrogate % Rec Acceptance Limits
Tetrachloro-m-xylene 71 22 - 141
DCB Decachlorobiphenyl 92 10 - 165
TestAmerica Edison 06/03/2010Page 80 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
05/17/2010 0636
05/17/2010 0650
Solid
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 460-37420
1.0
1.0
MS Lab Sample ID:
MSD Lab Sample ID:
Client Matrix:
Date Prepared:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Column ID:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Column ID:
Client Matrix: Solid
Analysis Batch: 460-37575
Analysis Batch: 460-37575
05/14/2010 0915
05/14/2010 0915
Prep Batch: 460-37420
Prep Batch: 460-37420
xf108822.d
15.01 g
10 mL
1 uL
PRIMARY
xf108823.d
15.00 g
10 mL
1 uL
PRIMARY
Method: 8081A
Preparation: 3541
PESTGC1
PESTGC1
460-13147-A-2-B MS
460-13147-A-2-C MSD
Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS
% Rec.
99 95 32 - 152 4 30Aldrin
100 94 41 - 145 6 30alpha-BHC
100 94 28 - 155 6 30beta-BHC
109 103 31 - 154 5 30delta-BHC
101 96 33 - 152 5 30gamma-BHC (Lindane)
104 102 50 - 154 2 304,4'-DDD
110 105 47 - 150 5 304,4'-DDE
102 94 39 - 154 8 304,4'-DDT
98 91 40 - 147 7 30Dieldrin
94 89 42 - 147 5 30Endosulfan I
99 95 32 - 150 5 30Endosulfan II
96 96 37 - 143 0 30Endosulfan sulfate
109 106 44 - 149 3 30Endrin
95 89 34 - 142 6 30Endrin aldehyde
91 82 32 - 152 10 30Heptachlor
97 92 33 - 149 6 30Heptachlor epoxide
Surrogate MS % Rec MSD % Rec Acceptance Limits
Tetrachloro-m-xylene 107 101 22 - 141
DCB Decachlorobiphenyl 132 56 10 - 165p
TestAmerica Edison 06/03/2010Page 81 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
05/17/2010 0636
05/17/2010 0650
Solid
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 460-37420
1.0
1.0
MS Lab Sample ID:
MSD Lab Sample ID:
Client Matrix:
Date Prepared:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Column ID:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Column ID:
Client Matrix: Solid
Analysis Batch: 460-37575
Analysis Batch: 460-37575
05/14/2010 0915
05/14/2010 0915
Prep Batch: 460-37420
Prep Batch: 460-37420
xr108822.d
15.01 g
10 mL
1 uL
SECONDARY
xr108823.d
15.00 g
10 mL
1 uL
SECONDARY
Method: 8081A
Preparation: 3541
PESTGC1
PESTGC1
460-13147-A-2-B MS
460-13147-A-2-C MSD
Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS
% Rec.
83 80 32 - 152 4 30Aldrin
85 80 41 - 145 6 30alpha-BHC
84 82 28 - 155 2 30beta-BHC
93 87 31 - 154 6 30delta-BHC
85 79 33 - 152 7 30gamma-BHC (Lindane)
87 77 50 - 154 13 304,4'-DDD
88 79 47 - 150 11 304,4'-DDE
82 74 39 - 154 10 304,4'-DDT
83 78 40 - 147 7 30Dieldrin
88 82 42 - 147 7 30Endosulfan I
80 74 32 - 150 8 30Endosulfan II
77 71 37 - 143 8 30Endosulfan sulfate
96 87 44 - 149 10 30Endrin
76 63 34 - 142 19 30Endrin aldehyde
90 79 32 - 152 12 30Heptachlor
86 79 33 - 149 8 30Heptachlor epoxide
Surrogate MS % Rec MSD % Rec Acceptance Limits
Tetrachloro-m-xylene 94 91 22 - 141
DCB Decachlorobiphenyl 123 147 10 - 165
TestAmerica Edison 06/03/2010Page 82 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
Solid
Date Analyzed: Date Analyzed:05/17/2010 0636 05/17/2010 0650
Dilution: Dilution:1.0 1.0
MS Lab Sample ID:
Client Matrix:
Date Prepared:
MSD Lab Sample ID:
Client Matrix: Solid
Date Prepared:05/14/2010 0915 05/14/2010 0915
Matrix Spike/
Matrix Spike Duplicate Data Report - Batch: 460-37420
Method: 8081A
Preparation: 3541
Units: ug/Kg460-13147-A-2-B MS 460-13147-A-2-C MSD
MSD
Result/Qual
MS
Result/Qual
MSD Spike
Amount
MS Spike
Amount
Sample
Result/QualAnalyte
7.7 U 153 153 151 145Aldrin
7.7 U 153 153 154 145alpha-BHC
7.7 U 153 153 153 144beta-BHC
7.7 U 153 153 167 159delta-BHC
7.7 U 153 153 155 147gamma-BHC (Lindane)
7.7 U 153 153 159 1564,4'-DDD
7.7 U 153 153 169 1614,4'-DDE
6.4 J 153 153 162 1504,4'-DDT
7.7 U 153 153 150 140Dieldrin
7.7 U 153 153 144 137Endosulfan I
7.7 U 153 153 152 145Endosulfan II
7.7 U 153 153 147 147Endosulfan sulfate
7.7 U 153 153 168 163Endrin
7.7 U 153 153 145 137Endrin aldehyde
7.7 U 153 153 139 125Heptachlor
7.7 U 153 153 149 140Heptachlor epoxide
TestAmerica Edison 06/03/2010Page 83 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
Solid
Date Analyzed: Date Analyzed:05/17/2010 0636 05/17/2010 0650
Dilution: Dilution:1.0 1.0
MS Lab Sample ID:
Client Matrix:
Date Prepared:
MSD Lab Sample ID:
Client Matrix: Solid
Date Prepared:05/14/2010 0915 05/14/2010 0915
Matrix Spike/
Matrix Spike Duplicate Data Report - Batch: 460-37420
Method: 8081A
Preparation: 3541
Units: ug/Kg460-13147-A-2-B MS 460-13147-A-2-C MSD
MSD
Result/Qual
MS
Result/Qual
MSD Spike
Amount
MS Spike
Amount
Sample
Result/QualAnalyte
7.7 U 153 153 127 122Aldrin
7.7 U 153 153 129 122alpha-BHC
7.7 U 153 153 128 125beta-BHC
7.7 U 153 153 142 134delta-BHC
7.7 U 153 153 130 121gamma-BHC (Lindane)
7.7 U 153 153 134 1184,4'-DDD
7.7 U 153 153 135 1224,4'-DDE
4.8 J 153 153 131 1184,4'-DDT
7.7 U 153 153 128 120Dieldrin
7.7 U 153 153 135 126Endosulfan I
7.7 U 153 153 123 113Endosulfan II
7.7 U 153 153 118 109Endosulfan sulfate
7.7 U 153 153 148 133Endrin
7.7 U 153 153 116 95.9Endrin aldehyde
7.7 U 153 153 137 122Heptachlor
7.7 U 153 153 132 122Heptachlor epoxide
TestAmerica Edison 06/03/2010Page 84 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
SolidClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
05/14/2010 1820
Method Blank - Batch: 460-37391
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Analysis Batch: 460-37531
Prep Batch: 460-37391
05/14/2010 0719
or077395.d
15.00 g
10 mL
Units: ug/Kg
Column ID: PRIMARY
Method: 8082
Preparation: 3541
PESTGC7MB 460-37391/1-A
Analyte RLMDLQualResult
67 U 6713Aroclor 1016
67 U 6720Aroclor 1221
67 U 6738Aroclor 1232
67 U 6713Aroclor 1242
67 U 6718Aroclor 1248
67 U 6723Aroclor 1254
67 U 677.5Aroclor 1260
67 U 6712Aroclor 1262
67 U 6712Aroclor 1268
Surrogate % Rec Acceptance Limits
DCB Decachlorobiphenyl 98 27 - 165
Surrogate % Rec Acceptance Limits
DCB Decachlorobiphenyl 94 27 - 165
TestAmerica Edison 06/03/2010Page 85 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
Solid
1.0
05/14/2010 1837Date Analyzed:
Lab Control Sample - Batch: 460-37391
Client Matrix:
Lab Sample ID:
Dilution:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
of077396.d
05/14/2010 0719
Analysis Batch: 460-37531
Prep Batch: 460-37391
15.00 g
10 mL
Units: ug/Kg
Column ID: PRIMARY
Method: 8082
Preparation: 3541
PESTGC7LCS 460-37391/2-A
Analyte QualLimit% Rec.ResultSpike Amount
333 316 95 62 - 148Aroclor 1016
333 328 98 58 - 145Aroclor 1260
Surrogate % Rec Acceptance Limits
DCB Decachlorobiphenyl 110 27 - 165
Solid
1.0
05/14/2010 1837Date Analyzed:
Lab Control Sample - Batch: 460-37391
Client Matrix:
Lab Sample ID:
Dilution:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
or077396.d
05/14/2010 0719
Analysis Batch: 460-37531
Prep Batch: 460-37391
15.00 g
10 mL
Units: ug/Kg
Column ID: SECONDARY
Method: 8082
Preparation: 3541
PESTGC7LCS 460-37391/2-A
Analyte QualLimit% Rec.ResultSpike Amount
333 278 83 62 - 148Aroclor 1016
333 314 94 58 - 145Aroclor 1260
Surrogate % Rec Acceptance Limits
DCB Decachlorobiphenyl 104 27 - 165
TestAmerica Edison 06/03/2010Page 86 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
05/14/2010 1909
05/14/2010 1926
Solid
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 460-37391
1.0
1.0
MS Lab Sample ID:
MSD Lab Sample ID:
Client Matrix:
Date Prepared:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Column ID:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Column ID:
Client Matrix: Solid
Analysis Batch: 460-37531
Analysis Batch: 460-37531
05/14/2010 0719
05/14/2010 0719
Prep Batch: 460-37391
Prep Batch: 460-37391
of077398.d
15.03 g
10 mL
PRIMARY
of077399.d
15.02 g
10 mL
PRIMARY
Method: 8082
Preparation: 3541
PESTGC7
PESTGC7
460-13137-A-1-B MS
460-13137-A-1-C MSD
Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS
% Rec.
104 106 62 - 148 2 30Aroclor 1016
106 110 58 - 145 4 30Aroclor 1260
Surrogate MS % Rec MSD % Rec Acceptance Limits
DCB Decachlorobiphenyl 108 91 27 - 165
TestAmerica Edison 06/03/2010Page 87 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
05/14/2010 1909
05/14/2010 1926
Solid
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 460-37391
1.0
1.0
MS Lab Sample ID:
MSD Lab Sample ID:
Client Matrix:
Date Prepared:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Column ID:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Column ID:
Client Matrix: Solid
Analysis Batch: 460-37531
Analysis Batch: 460-37531
05/14/2010 0719
05/14/2010 0719
Prep Batch: 460-37391
Prep Batch: 460-37391
or077398.d
15.03 g
10 mL
SECONDARY
or077399.d
15.02 g
10 mL
SECONDARY
Method: 8082
Preparation: 3541
PESTGC7
PESTGC7
460-13137-A-1-B MS
460-13137-A-1-C MSD
Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS
% Rec.
94 98 62 - 148 4 30Aroclor 1016
96 100 58 - 145 4 30Aroclor 1260
Surrogate MS % Rec MSD % Rec Acceptance Limits
DCB Decachlorobiphenyl 106 91 27 - 165
TestAmerica Edison 06/03/2010Page 88 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
Solid
Date Analyzed: Date Analyzed:05/14/2010 1909 05/14/2010 1926
Dilution: Dilution:1.0 1.0
MS Lab Sample ID:
Client Matrix:
Date Prepared:
MSD Lab Sample ID:
Client Matrix: Solid
Date Prepared:05/14/2010 0719 05/14/2010 0719
Matrix Spike/
Matrix Spike Duplicate Data Report - Batch: 460-37391
Method: 8082
Preparation: 3541
Units: ug/Kg460-13137-A-1-B MS 460-13137-A-1-C MSD
MSD
Result/Qual
MS
Result/Qual
MSD Spike
Amount
MS Spike
Amount
Sample
Result/QualAnalyte
69 U 343 343 357 364Aroclor 1016
69 U 343 343 362 376Aroclor 1260
Solid
Date Analyzed: Date Analyzed:05/14/2010 1909 05/14/2010 1926
Dilution: Dilution:1.0 1.0
MS Lab Sample ID:
Client Matrix:
Date Prepared:
MSD Lab Sample ID:
Client Matrix: Solid
Date Prepared:05/14/2010 0719 05/14/2010 0719
Matrix Spike/
Matrix Spike Duplicate Data Report - Batch: 460-37391
Method: 8082
Preparation: 3541
Units: ug/Kg460-13137-A-1-B MS 460-13137-A-1-C MSD
MSD
Result/Qual
MS
Result/Qual
MSD Spike
Amount
MS Spike
Amount
Sample
Result/QualAnalyte
69 U 343 343 321 335Aroclor 1016
69 U 343 343 331 343Aroclor 1260
TestAmerica Edison 06/03/2010Page 89 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
SolidClient Matrix:
2.0Dilution:
Date Analyzed:
Lab Sample ID:
05/18/2010 1120
Method Blank - Batch: 460-37477
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 460-37705
Prep Batch: 460-37477
05/14/2010 1542
05182010A.txt
1.00 g
50 mL
Units: mg/Kg
Method: 6010B
Preparation: 3050B
ICP4MB 460-37477/1-A ^2
Analyte RLMDLQualResult
1.0 U 1.00.44Antimony
0.50 U 0.500.35Arsenic
0.20 U 0.200.088Beryllium
0.50 U 0.500.078Cadmium
1.0 U 1.00.59Chromium
2.5 U 2.50.41Copper
0.50 U 0.500.25Lead
4.0 U 4.00.27Nickel
1.0 U 1.00.47Selenium
0.0811 J 1.00.076Silver
1.0 U 1.00.48Thallium
3.0 U 3.00.49Zinc
Solid
4.0
05/18/2010 1123Date Analyzed:
LCS-Standard Reference Material - Batch:
Client Matrix:
Lab Sample ID:
Dilution:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
05182010A.txt
05/14/2010 1542
Analysis Batch: 460-37705
Prep Batch: 460-37477
1.02 g
50 mL
Units: mg/Kg
Method: 6010B
Preparation: 3050B
ICP4LCSSRM 460-37477/2-A ^4
Analyte QualLimit% Rec.ResultSpike Amount
66.1 68.57 104 32.0 - 353Antimony
102 93.00 91 69.7 - 131Arsenic
76.1 73.49 97 74.0 - 126Beryllium
59.5 53.69 90 73.3 - 127Cadmium
231 228.8 99 70.8 - 129Chromium
171 171.5 101 75.3 - 124Copper
84.3 86.10 102 69.8 - 130Lead
131 123.8 94 73.2 - 127Nickel
280 249.4 89 69.6 - 130Selenium
29.5 29.73 101 65.1 - 135Silver
119 124.3 105 67.8 - 133Thallium
582 538.2 92 73.6 - 127Zinc
TestAmerica Edison 06/03/2010Page 90 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
SolidClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
05/14/2010 1222
Method Blank - Batch: 460-37424
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 460-37472
Prep Batch: 460-37424
05/14/2010 0925
37424hg1.PRN
0.60 g
100 mL
Units: mg/Kg
Method: 7471A
Preparation: 7471A
LEEMAN5MB 460-37424/1-A
Analyte RLMDLQualResult
0.033 U 0.0330.026Mercury
Solid
10
05/14/2010 1224Date Analyzed:
LCS-Standard Reference Material - Batch:
Client Matrix:
Lab Sample ID:
Dilution:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
37424hg1.PRN
05/14/2010 0925
Analysis Batch: 460-37472
Prep Batch: 460-37424
0.60 g
100 mL
Units: mg/Kg
Method: 7471A
Preparation: 7471A
LEEMAN5LCSSRM 460-37424/2-A ^10
Analyte QualLimit% Rec.ResultSpike Amount
8.46 9.15 108 51.3 - 149Mercury
Solid
1.0
05/14/2010 1231Date Analyzed:
Matrix Spike - Batch: 460-37424
Lab Sample ID:
Client Matrix:
Dilution:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
05/14/2010 0925
37424hg1.PRN
Analysis Batch: 460-37472
Prep Batch: 460-37424
0.60 g
100 mL
Units: mg/Kg
Method: 7471A
Preparation: 7471A
LEEMAN5460-13139-5
QualLimit% Rec.ResultSpike AmountSample Result/QualAnalyte
0.035 U 0.178 0.214 120 75 - 125Mercury
TestAmerica Edison 06/03/2010Page 91 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
mg/KgUnits:
Solid
Dilution: 1.0
Date Analyzed:
Duplicate - Batch: 460-37424
Lab Sample ID:
Client Matrix:
Date Prepared:
05/14/2010 1228
05/14/2010 0925
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 460-37472
Prep Batch: 460-37424 37424hg1.PRN
0.60 g
100 mL
Method: 7471A
Preparation: 7471A
LEEMAN5460-13139-5
Analyte QualLimitRPDResultSample Result/Qual
0.0350.035 U NC 20 UMercury
TestAmerica Edison 06/03/2010Page 92 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
%Units:
Solid
Dilution: 1.0
Date Analyzed:
Duplicate - Batch: 460-37508
Lab Sample ID:
Client Matrix:
Date Prepared:
05/14/2010 2147
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 460-37508
Prep Batch: N/A
N/A
Method: Moisture
Preparation: N/A
N/A
No Equipment Assigned460-13146-A-1 DU
Analyte QualLimitRPDResultSample Result/Qual
16.116.2 1 20Percent Moisture
83.983.8 0 20Percent Solids
TestAmerica Edison 06/03/2010Page 93 of 623
Quality Control Results
Job Number: 460-13139-1Client: Duffield Associates
%Units:
Solid
Dilution: 1.0
Date Analyzed:
Duplicate - Batch: 460-37639
Lab Sample ID:
Client Matrix:
Date Prepared:
05/17/2010 1956
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 460-37639
Prep Batch: N/A
N/A
Method: Moisture
Preparation: N/A
N/A
No Equipment Assigned460-13237-A-4 DU
Analyte QualLimitRPDResultSample Result/Qual
16.215.8 2 20Percent Moisture
83.884.2 0 20Percent Solids
TestAmerica Edison 06/03/2010Page 94 of 623
DATA REPORTING QUALIFIERS
Client: Duffield Associates Job Number: 460-13139-1
Lab Section Qualifier Description
GC/MS VOA
Indicates an Estimated Value for TICsJ
Indicates the analyte was analyzed for but not detected.U
Result is a tentatively identified compound (TIC) and an
estimated value.
T
GC/MS Semi VOA
Indicates an Estimated Value for TICsJ
Indicates the analyte was analyzed for but not detected.U
MS/MSD Recovery or RPD exceeds the control limitsF
Recovery or RPD exceeds control limits*
Result is a tentatively identified compound (TIC) and an
estimated value.
T
Result is less than the RL but greater than or equal to the MDL
and the concentration is an approximate value.
J
The tentatively identified compound is a suspected
aldol-condensation product.
A
This flag indicates the presumptive evidence of a compound.N
GC Semi VOA
Indicates the analyte was analyzed for but not detected.U
Result is less than the RL but greater than or equal to the MDL
and the concentration is an approximate value.
J
Surrogate is outside control limitsX
The %RPD between the primary and confirmation
column/detector is >40%. The lower value has been reported.
p
TestAmerica Edison
06/03/2010Page 95 of 623
DATA REPORTING QUALIFIERS
Client: Duffield Associates Job Number: 460-13139-1
Lab Section Qualifier Description
Metals
Compound was found in the blank and sample.B
Indicates the analyte was analyzed for but not detected.U
Result is less than the RL but greater than or equal to the MDL
and the concentration is an approximate value.
J
TestAmerica Edison
06/03/2010Page 96 of 623
Quality Control Results
Client: Duffield Associates Job Number: 460-13139-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
GC/MS VOA
Prep Batch: 460-37413
SolidTB-3 6-7 5035460-13139-2 T
SolidTB-2 5-6 5035460-13139-4 T
SolidTB-1 2-3 5035460-13139-5 T
SolidTB-5 3-4 5035460-13139-7 T
Analysis Batch:460-37643
Lab Control Sample Solid 8260BLCS 460-37643/3 T
Lab Control Sample Duplicate Solid 8260BLCSD 460-37643/4 T
Method Blank Solid 8260BMB 460-37643/5 T
Solid 460-37413TB-3 6-7 8260B460-13139-2 T
Solid 460-37413TB-2 5-6 8260B460-13139-4 T
Solid 460-37413TB-1 2-3 8260B460-13139-5 T
Solid 460-37413TB-5 3-4 8260B460-13139-7 T
Report Basis
T = Total
GC/MS Semi VOA
Prep Batch: 460-37564
Lab Control Sample Solid 3541LCS 460-37564/2-A T
Method Blank Solid 3541MB 460-37564/1-A T
SolidTB-3 6-7 3541460-13139-2 T
SolidTB-2 5-6 3541460-13139-4 T
SolidTB-1 2-3 3541460-13139-5 T
Matrix Spike Solid 3541460-13139-5MS T
Matrix Spike Duplicate Solid 3541460-13139-5MSD T
SolidTB-5 3-4 3541460-13139-7 T
Analysis Batch:460-37818
Lab Control Sample Solid 460-375648270CLCS 460-37564/2-A T
Method Blank Solid 460-375648270CMB 460-37564/1-A T
Solid 460-37564TB-3 6-7 8270C460-13139-2 T
Solid 460-37564TB-2 5-6 8270C460-13139-4 T
Solid 460-37564TB-1 2-3 8270C460-13139-5 T
Matrix Spike Solid 460-375648270C460-13139-5MS T
Matrix Spike Duplicate Solid 460-375648270C460-13139-5MSD T
Solid 460-37564TB-5 3-4 8270C460-13139-7 T
Report Basis
T = Total
TestAmerica Edison
06/03/2010Page 97 of 623
Quality Control Results
Client: Duffield Associates Job Number: 460-13139-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
GC Semi VOA
Prep Batch: 460-37391
Lab Control Sample Solid 3541LCS 460-37391/2-A T
Method Blank Solid 3541MB 460-37391/1-A T
Matrix Spike Solid 3541460-13137-A-1-B MS T
Matrix Spike Duplicate Solid 3541460-13137-A-1-C MSD T
SolidTB-3 6-7 3541460-13139-2 T
SolidTB-2 5-6 3541460-13139-4 T
SolidTB-1 2-3 3541460-13139-5 T
SolidTB-5 3-4 3541460-13139-7 T
Prep Batch: 460-37420
Lab Control Sample Solid 3541LCS 460-37420/2-A T
Method Blank Solid 3541MB 460-37420/1-A T
SolidTB-3 6-7 3541460-13139-2 T
SolidTB-2 5-6 3541460-13139-4 T
SolidTB-1 2-3 3541460-13139-5 T
SolidTB-5 3-4 3541460-13139-7 T
Matrix Spike Solid 3541460-13147-A-2-B MS T
Matrix Spike Duplicate Solid 3541460-13147-A-2-C MSD T
Analysis Batch:460-37531
Lab Control Sample Solid 460-373918082LCS 460-37391/2-A T
Method Blank Solid 460-373918082MB 460-37391/1-A T
Matrix Spike Solid 460-373918082460-13137-A-1-B MS T
Matrix Spike Duplicate Solid 460-373918082460-13137-A-1-C MSD T
Solid 460-37391TB-3 6-7 8082460-13139-2 T
Solid 460-37391TB-2 5-6 8082460-13139-4 T
Solid 460-37391TB-1 2-3 8082460-13139-5 T
Solid 460-37391TB-5 3-4 8082460-13139-7 T
Analysis Batch:460-37575
Lab Control Sample Solid 460-374208081ALCS 460-37420/2-A T
Method Blank Solid 460-374208081AMB 460-37420/1-A T
Solid 460-37420TB-3 6-7 8081A460-13139-2 T
Solid 460-37420TB-2 5-6 8081A460-13139-4 T
Solid 460-37420TB-1 2-3 8081A460-13139-5 T
Solid 460-37420TB-5 3-4 8081A460-13139-7 T
Matrix Spike Solid 460-374208081A460-13147-A-2-B MS T
Matrix Spike Duplicate Solid 460-374208081A460-13147-A-2-C MSD T
Report Basis
T = Total
TestAmerica Edison
06/03/2010Page 98 of 623
Quality Control Results
Client: Duffield Associates Job Number: 460-13139-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
Metals
Prep Batch: 460-37424
LCS-Standard Reference Material Solid 7471ALCSSRM 460-37424/2-A ^10 T
Method Blank Solid 7471AMB 460-37424/1-A T
SolidTB-3 6-7 7471A460-13139-2 T
SolidTB-2 5-6 7471A460-13139-4 T
SolidTB-1 2-3 7471A460-13139-5 T
Duplicate Solid 7471A460-13139-5DU T
Matrix Spike Solid 7471A460-13139-5MS T
SolidTB-5 3-4 7471A460-13139-7 T
Analysis Batch:460-37472
LCS-Standard Reference Material Solid 460-374247471ALCSSRM 460-37424/2-A ^10 T
Method Blank Solid 460-374247471AMB 460-37424/1-A T
Solid 460-37424TB-3 6-7 7471A460-13139-2 T
Solid 460-37424TB-2 5-6 7471A460-13139-4 T
Solid 460-37424TB-1 2-3 7471A460-13139-5 T
Duplicate Solid 460-374247471A460-13139-5DU T
Matrix Spike Solid 460-374247471A460-13139-5MS T
Solid 460-37424TB-5 3-4 7471A460-13139-7 T
Prep Batch: 460-37477
LCS-Standard Reference Material Solid 3050BLCSSRM 460-37477/2-A ^4 T
Method Blank Solid 3050BMB 460-37477/1-A ^2 T
SolidTB-3 6-7 3050B460-13139-2 T
SolidTB-2 5-6 3050B460-13139-4 T
SolidTB-1 2-3 3050B460-13139-5 T
SolidTB-5 3-4 3050B460-13139-7 T
Analysis Batch:460-37705
LCS-Standard Reference Material Solid 460-374776010BLCSSRM 460-37477/2-A ^4 T
Method Blank Solid 460-374776010BMB 460-37477/1-A ^2 T
Solid 460-37477TB-3 6-7 6010B460-13139-2 T
Solid 460-37477TB-2 5-6 6010B460-13139-4 T
Solid 460-37477TB-1 2-3 6010B460-13139-5 T
Solid 460-37477TB-5 3-4 6010B460-13139-7 T
Report Basis
T = Total
TestAmerica Edison
06/03/2010Page 99 of 623
Quality Control Results
Client: Duffield Associates Job Number: 460-13139-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
General Chemistry
Analysis Batch:460-37508
SolidTB-3 2-3 Moisture460-13139-1 T
SolidTB-3 6-7 Moisture460-13139-2 T
SolidTB-2 2-3 Moisture460-13139-3 T
SolidTB-2 5-6 Moisture460-13139-4 T
SolidTB-1 2-3 Moisture460-13139-5 T
SolidTB-1 5-6 Moisture460-13139-6 T
SolidTB-4 6-7 Moisture460-13139-8 T
Duplicate Solid Moisture460-13146-A-1 DU T
Analysis Batch:460-37639
SolidTB-5 3-4 Moisture460-13139-7 T
Duplicate Solid Moisture460-13237-A-4 DU T
Report Basis
T = Total
TestAmerica Edison
06/03/2010Page 100 of 623
Quality Control Results
Client: Duffield Associates Job Number: 460-13139-1
Laboratory Chronicle
05/13/2010 18:30
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time: Received Date/Time:05/12/2010 09:00
460-13139-1 TB-3 2-3
A:Moisture 460-13139-D-1 460-37508 05/14/2010 21:47 VDTAL EDI1
05/13/2010 18:30
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time: Received Date/Time:05/12/2010 09:45
460-13139-2 TB-3 6-7
P:5035 460-13139-B-2-A 460-37643 460-37413 05/14/2010 08:50 MMDTAL EDI1
A:8260B 460-13139-B-2-A 460-37643 460-37413 05/18/2010 00:18 KBTAL EDI1
P:3541 460-13139-E-2-E 460-37818 460-37564 05/17/2010 09:00 cmTAL EDI1
A:8270C 460-13139-E-2-E 460-37818 460-37564 05/18/2010 15:00 CZTAL EDI1
P:3541 460-13139-E-2-B 460-37575 460-37420 05/14/2010 09:15 hpTAL EDI1
A:8081A 460-13139-E-2-B 460-37575 460-37420 05/17/2010 08:00 FMTAL EDI1
P:3541 460-13139-E-2-A 460-37531 460-37391 05/14/2010 07:19 ARATAL EDI1
A:8082 460-13139-E-2-A 460-37531 460-37391 05/14/2010 19:59 CBDTAL EDI1
P:3050B 460-13139-E-2-D ^4 460-37705 460-37477 05/14/2010 15:42 ARCTAL EDI4
A:6010B 460-13139-E-2-D ^4 460-37705 460-37477 05/18/2010 11:55 CDCTAL EDI4
P:7471A 460-13139-E-2-C 460-37472 460-37424 05/14/2010 09:25 RBSTAL EDI1
A:7471A 460-13139-E-2-C 460-37472 460-37424 05/14/2010 12:52 RBSTAL EDI1
A:Moisture 460-13139-D-2 460-37508 05/14/2010 21:47 VDTAL EDI1
05/13/2010 18:30
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time: Received Date/Time:05/12/2010 10:30
460-13139-3 TB-2 2-3
A:Moisture 460-13139-D-3 460-37508 05/14/2010 21:47 VDTAL EDI1
A = Analytical Method P = Prep Method TestAmerica Edison
06/03/2010Page 101 of 623
Quality Control Results
Client: Duffield Associates Job Number: 460-13139-1
Laboratory Chronicle
05/13/2010 18:30
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time: Received Date/Time:05/12/2010 10:45
460-13139-4 TB-2 5-6
P:5035 460-13139-B-4-A 460-37643 460-37413 05/14/2010 08:54 MMDTAL EDI1
A:8260B 460-13139-B-4-A 460-37643 460-37413 05/18/2010 00:43 KBTAL EDI1
P:3541 460-13139-E-4-E 460-37818 460-37564 05/17/2010 09:00 cmTAL EDI1
A:8270C 460-13139-E-4-E 460-37818 460-37564 05/18/2010 20:25 CZTAL EDI1
P:3541 460-13139-E-4-B 460-37575 460-37420 05/14/2010 09:15 hpTAL EDI1
A:8081A 460-13139-E-4-B 460-37575 460-37420 05/17/2010 08:27 FMTAL EDI1
P:3541 460-13139-E-4-A 460-37531 460-37391 05/14/2010 07:19 ARATAL EDI1
A:8082 460-13139-E-4-A 460-37531 460-37391 05/14/2010 20:32 CBDTAL EDI1
P:3050B 460-13139-E-4-D ^4 460-37705 460-37477 05/14/2010 15:42 ARCTAL EDI4
A:6010B 460-13139-E-4-D ^4 460-37705 460-37477 05/18/2010 12:01 CDCTAL EDI4
P:7471A 460-13139-E-4-C 460-37472 460-37424 05/14/2010 09:25 RBSTAL EDI1
A:7471A 460-13139-E-4-C 460-37472 460-37424 05/14/2010 12:55 RBSTAL EDI1
A:Moisture 460-13139-D-4 460-37508 05/14/2010 21:47 VDTAL EDI1
05/13/2010 18:30
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time: Received Date/Time:05/12/2010 11:25
460-13139-5 TB-1 2-3
P:5035 460-13139-B-5-A 460-37643 460-37413 05/14/2010 08:55 MMDTAL EDI1
A:8260B 460-13139-B-5-A 460-37643 460-37413 05/18/2010 01:08 KBTAL EDI1
P:3541 460-13139-E-5-G 460-37818 460-37564 05/17/2010 09:00 cmTAL EDI1
A:8270C 460-13139-E-5-G 460-37818 460-37564 05/18/2010 11:52 CZTAL EDI1
P:3541 460-13139-E-5-B 460-37575 460-37420 05/14/2010 09:15 hpTAL EDI1
A:8081A 460-13139-E-5-B 460-37575 460-37420 05/17/2010 08:41 FMTAL EDI1
P:3541 460-13139-E-5-A 460-37531 460-37391 05/14/2010 07:19 ARATAL EDI1
A:8082 460-13139-E-5-A 460-37531 460-37391 05/14/2010 20:48 CBDTAL EDI1
P:3050B 460-13139-E-5-F ^4 460-37705 460-37477 05/14/2010 15:42 ARCTAL EDI4
A:6010B 460-13139-E-5-F ^4 460-37705 460-37477 05/18/2010 12:04 CDCTAL EDI4
P:7471A 460-13139-E-5-C 460-37472 460-37424 05/14/2010 09:25 RBSTAL EDI1
A:7471A 460-13139-E-5-C 460-37472 460-37424 05/14/2010 12:26 RBSTAL EDI1
A:Moisture 460-13139-D-5 460-37508 05/14/2010 21:47 VDTAL EDI1
05/13/2010 18:30
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time: Received Date/Time:05/12/2010 11:25
460-13139-5 MS TB-1 2-3
P:3541 460-13139-E-5-H MS 460-37818 460-37564 05/17/2010 09:00 cmTAL EDI1
A:8270C 460-13139-E-5-H MS 460-37818 460-37564 05/18/2010 12:18 CZTAL EDI1
P:7471A 460-13139-E-5-E MS 460-37472 460-37424 05/14/2010 09:25 RBSTAL EDI1
A:7471A 460-13139-E-5-E MS 460-37472 460-37424 05/14/2010 12:31 RBSTAL EDI1
A = Analytical Method P = Prep Method TestAmerica Edison
06/03/2010Page 102 of 623
Quality Control Results
Client: Duffield Associates Job Number: 460-13139-1
Laboratory Chronicle
05/13/2010 18:30
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time: Received Date/Time:05/12/2010 11:25
460-13139-5 MSD TB-1 2-3
P:3541 460-13139-E-5-I MSD 460-37818 460-37564 05/17/2010 09:00 cmTAL EDI1
A:8270C 460-13139-E-5-I MSD 460-37818 460-37564 05/18/2010 12:46 CZTAL EDI1
05/13/2010 18:30
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time: Received Date/Time:05/12/2010 11:25
460-13139-5 DU TB-1 2-3
P:7471A 460-13139-E-5-D DU 460-37472 460-37424 05/14/2010 09:25 RBSTAL EDI1
A:7471A 460-13139-E-5-D DU 460-37472 460-37424 05/14/2010 12:28 RBSTAL EDI1
05/13/2010 18:30
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time: Received Date/Time:05/12/2010 11:45
460-13139-6 TB-1 5-6
A:Moisture 460-13139-D-6 460-37508 05/14/2010 21:47 VDTAL EDI1
05/13/2010 18:30
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time: Received Date/Time:05/12/2010 12:30
460-13139-7 TB-5 3-4
P:5035 460-13139-B-7-A 460-37643 460-37413 05/14/2010 08:58 MMDTAL EDI1
A:8260B 460-13139-B-7-A 460-37643 460-37413 05/18/2010 01:33 KBTAL EDI1
P:3541 460-13139-E-7-E 460-37818 460-37564 05/17/2010 09:00 cmTAL EDI1
A:8270C 460-13139-E-7-E 460-37818 460-37564 05/18/2010 19:58 CZTAL EDI1
P:3541 460-13139-E-7-B 460-37575 460-37420 05/14/2010 09:15 hpTAL EDI1
A:8081A 460-13139-E-7-B 460-37575 460-37420 05/17/2010 09:09 FMTAL EDI1
P:3541 460-13139-E-7-A 460-37531 460-37391 05/14/2010 07:19 ARATAL EDI1
A:8082 460-13139-E-7-A 460-37531 460-37391 05/14/2010 21:21 CBDTAL EDI1
P:3050B 460-13139-E-7-D ^4 460-37705 460-37477 05/14/2010 15:42 ARCTAL EDI4
A:6010B 460-13139-E-7-D ^4 460-37705 460-37477 05/18/2010 12:10 CDCTAL EDI4
P:7471A 460-13139-E-7-C 460-37472 460-37424 05/14/2010 09:25 RBSTAL EDI1
A:7471A 460-13139-E-7-C 460-37472 460-37424 05/14/2010 12:59 RBSTAL EDI1
A:Moisture 460-13139-E-7 460-37639 05/17/2010 19:56 VDTAL EDI1
05/13/2010 18:30
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time: Received Date/Time:05/12/2010 13:40
460-13139-8 TB-4 6-7
A:Moisture 460-13139-D-8 460-37508 05/14/2010 21:47 VDTAL EDI1
A = Analytical Method P = Prep Method TestAmerica Edison
06/03/2010Page 103 of 623
Quality Control Results
Client: Duffield Associates Job Number: 460-13139-1
Laboratory Chronicle
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time: N/A Received Date/Time: N/A
MB N/A
A:8260B MB 460-37643/5 460-37643 05/17/2010 20:11 KBTAL EDI1
P:3541 MB 460-37564/1-A 460-37818 460-37564 05/17/2010 09:00 cmTAL EDI1
A:8270C MB 460-37564/1-A 460-37818 460-37564 05/18/2010 10:57 CZTAL EDI1
P:3541 MB 460-37420/1-A 460-37575 460-37420 05/14/2010 09:15 hpTAL EDI1
A:8081A MB 460-37420/1-A 460-37575 460-37420 05/17/2010 09:37 FMTAL EDI1
P:3541 MB 460-37391/1-A 460-37531 460-37391 05/14/2010 07:19 ARATAL EDI1
A:8082 MB 460-37391/1-A 460-37531 460-37391 05/14/2010 18:20 CBDTAL EDI1
P:3050B MB 460-37477/1-A ^2 460-37705 460-37477 05/14/2010 15:42 ARCTAL EDI2
A:6010B MB 460-37477/1-A ^2 460-37705 460-37477 05/18/2010 11:20 CDCTAL EDI2
P:7471A MB 460-37424/1-A 460-37472 460-37424 05/14/2010 09:25 RBSTAL EDI1
A:7471A MB 460-37424/1-A 460-37472 460-37424 05/14/2010 12:22 RBSTAL EDI1
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time: N/A Received Date/Time: N/A
LCS N/A
A:8260B LCS 460-37643/3 460-37643 05/17/2010 17:46 KBTAL EDI1
P:3541 LCS 460-37564/2-A 460-37818 460-37564 05/17/2010 09:00 cmTAL EDI1
A:8270C LCS 460-37564/2-A 460-37818 460-37564 05/18/2010 11:25 CZTAL EDI1
P:3541 LCS 460-37420/2-A 460-37575 460-37420 05/14/2010 09:15 hpTAL EDI1
A:8081A LCS 460-37420/2-A 460-37575 460-37420 05/17/2010 05:43 FMTAL EDI1
P:3541 LCS 460-37391/2-A 460-37531 460-37391 05/14/2010 07:19 ARATAL EDI1
A:8082 LCS 460-37391/2-A 460-37531 460-37391 05/14/2010 18:37 CBDTAL EDI1
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time: N/A Received Date/Time: N/A
LCSD N/A
A:8260B LCSD 460-37643/4 460-37643 05/17/2010 18:10 KBTAL EDI1
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time: N/A Received Date/Time: N/A
LCSSRM N/A
P:3050B LCSSRM
460-37477/2-A ^4
460-37705 460-37477 05/14/2010 15:42 ARCTAL EDI4
A:6010B LCSSRM
460-37477/2-A ^4
460-37705 460-37477 05/18/2010 11:23 CDCTAL EDI4
P:7471A LCSSRM
460-37424/2-A ^10
460-37472 460-37424 05/14/2010 09:25 RBSTAL EDI10
A:7471A LCSSRM
460-37424/2-A ^10
460-37472 460-37424 05/14/2010 12:24 RBSTAL EDI10
A = Analytical Method P = Prep Method TestAmerica Edison
06/03/2010Page 104 of 623
Quality Control Results
Client: Duffield Associates Job Number: 460-13139-1
Laboratory Chronicle
05/13/2010 18:00
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time: Received Date/Time:05/12/2010 15:30
MS N/A
P:3541 460-13147-A-2-B MS 460-37575 460-37420 05/14/2010 09:15 hpTAL EDI1
A:8081A 460-13147-A-2-B MS 460-37575 460-37420 05/17/2010 06:36 FMTAL EDI1
P:3541 460-13137-A-1-B MS 460-37531 460-37391 05/14/2010 07:19 ARATAL EDI1
A:8082 460-13137-A-1-B MS 460-37531 460-37391 05/14/2010 19:09 CBDTAL EDI1
05/13/2010 18:00
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time: Received Date/Time:05/12/2010 15:30
MSD N/A
P:3541 460-13147-A-2-C
MSD
460-37575 460-37420 05/14/2010 09:15 hpTAL EDI1
A:8081A 460-13147-A-2-C
MSD
460-37575 460-37420 05/17/2010 06:50 FMTAL EDI1
P:3541 460-13137-A-1-C
MSD
460-37531 460-37391 05/14/2010 07:19 ARATAL EDI1
A:8082 460-13137-A-1-C
MSD
460-37531 460-37391 05/14/2010 19:26 CBDTAL EDI1
05/13/2010 18:00
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time: Received Date/Time:05/13/2010 00:00
DU N/A
A:Moisture 460-13146-A-1 DU 460-37508 05/14/2010 21:47 VDTAL EDI1
A:Moisture 460-13237-A-4 DU 460-37639 05/17/2010 19:56 VDTAL EDI1
Lab References:TAL EDI = TestAmerica Edison
A = Analytical Method P = Prep Method TestAmerica Edison
06/03/2010Page 105 of 623
Method 8260BVolatile Organic Compounds (GC/MS)
by Method 8260B
06/03/2010Page 106 of 623
FORM II
GC/MS VOA SURROGATE RECOVERY
Lab Name: Job No.: 460-13139-1
SDG No.:
Matrix: Solid Level: Low
TestAmerica Edison
GC Column (1): DB-624 ID: 0.18(mm)
#Lab Sample IDClient Sample ID # #DCA TOL BFB
460-13139-2TB-3 6-7 92 88 102
460-13139-4TB-2 5-6 95 89 105
460-13139-5TB-1 2-3 100 90 108
460-13139-7TB-5 3-4 89 73 92
MB 460-37643/5 104 92 107
LCS 460-37643/3 89 90 108
LCSD 460-37643/4 90 95 106
QC LIMITSQC LIMITSDCA = 1,2-Dichloroethane-d4 (Surr) 70-138
TOL = Toluene-d8 (Surr) 66-126BFB = Bromofluorobenzene 72-132
FORM II 8260B
# Column to be used to flag recovery values
06/03/2010Page 107 of 623
GC/MS VOA LAB CONTROL SAMPLE RECOVERY
FORM III
Job No.:Lab Name:
SDG No.:
Level:Matrix:Matrix:
Low
460-13139-1
Lab File ID: o37386.dSolid
Lab ID: LCS 460-37643/3 Client ID:
TestAmerica Edison
REC
%
REC
QC
LIMITSCONCENTRATION
(ug/Kg)
SPIKE
ADDED
(ug/Kg)
#
LCS LCS
COMPOUND
Chloromethane 20.0 19.2 50-15196
Bromomethane 20.0 22.0 54-142110
Vinyl chloride 20.0 19.5 67-13397
Chloroethane 20.0 19.9 56-14699
Methylene Chloride 20.0 23.9 74-137120
Trichlorofluoromethane 20.0 21.5 61-139107
1,1-Dichloroethene 20.0 20.8 71-126104
1,1-Dichloroethane 20.0 19.8 76-12599
trans-1,2-Dichloroethene 20.0 19.8 75-12299
cis-1,2-Dichloroethene 20.0 20.0 80-120100
Chloroform 20.0 19.9 77-12099
1,2-Dichloroethane 20.0 19.6 76-11898
1,1,1-Trichloroethane 20.0 20.5 78-117103
Carbon tetrachloride 20.0 21.5 79-118107
Bromodichloromethane 20.0 20.1 79-119100
1,2-Dichloropropane 20.0 19.5 82-12298
cis-1,3-Dichloropropene 20.0 18.7 80-12394
Trichloroethene 20.0 19.8 79-11999
Dibromochloromethane 20.0 16.7 68-12083
1,1,2-Trichloroethane 20.0 17.8 73-11889
Benzene 20.0 19.7 77-11799
trans-1,3-Dichloropropene 20.0 15.2 67-12176
2-Chloroethyl vinyl ether 20.0 16.5 74-12083
Bromoform 20.0 14.7 59-12573
Tetrachloroethene 20.0 18.6 80-12093
1,1,2,2-Tetrachloroethane 20.0 18.9 79-12295
Toluene 20.0 19.2 75-11596
Chlorobenzene 20.0 20.0 80-120100
Ethylbenzene 20.0 21.1 81-121105
Xylenes, Total 60.0 61.9 82-122103
FORM III 8260B
# Column to be used to flag recovery and RPD values
06/03/2010Page 108 of 623
GC/MS VOA LAB CONTROL SAMPLE DUPLICATE RECOVERY
FORM III
Job No.:Lab Name:
SDG No.:
Level:Matrix:Matrix:
Low
460-13139-1
Lab File ID: o37387.dSolid
Lab ID: LCSD 460-37643/4 Client ID:
TestAmerica Edison
COMPOUND
SPIKE
ADDED CONCENTRATION %
REC
%
RPD
QC LIMITS
RPD REC (ug/Kg) (ug/Kg)
#
LCSD LCSD
20.0 19.2 30 50-151Chloromethane 096
20.0 22.3 30 54-142Bromomethane 1111
20.0 19.5 30 67-133Vinyl chloride 098
20.0 19.9 30 56-146Chloroethane 0100
20.0 26.8 30 74-137Methylene Chloride 11134
20.0 21.1 30 61-139Trichlorofluoromethane 2105
20.0 23.1 30 71-1261,1-Dichloroethene 11116
20.0 21.5 30 76-1251,1-Dichloroethane 8108
20.0 21.6 30 75-122trans-1,2-Dichloroethene 9108
20.0 22.1 30 80-120cis-1,2-Dichloroethene 10110
20.0 21.8 30 77-120Chloroform 9109
20.0 21.5 30 76-1181,2-Dichloroethane 9108
20.0 23.0 30 78-1171,1,1-Trichloroethane 11115
20.0 23.3 30 79-118Carbon tetrachloride 8116
20.0 23.1 30 79-119Bromodichloromethane 14115
20.0 21.1 30 82-1221,2-Dichloropropane 8105
20.0 21.8 30 80-123cis-1,3-Dichloropropene 15109
20.0 21.2 30 79-119Trichloroethene 7106
20.0 18.3 30 68-120Dibromochloromethane 991
20.0 20.0 30 73-1181,1,2-Trichloroethane 12100
20.0 21.9 30 77-117Benzene 11110
20.0 17.5 30 67-121trans-1,3-Dichloropropene 1487
20.0 17.4 30 74-1202-Chloroethyl vinyl ether 587
20.0 16.8 30 59-125Bromoform 1384
20.0 22.3 30 80-120Tetrachloroethene 18111
20.0 20.3 30 79-1221,1,2,2-Tetrachloroethane 7101
20.0 21.7 30 75-115Toluene 12109
20.0 21.9 30 80-120Chlorobenzene 9110
20.0 22.1 30 81-121Ethylbenzene 5111
60.0 67.1 30 82-122Xylenes, Total 8112
FORM III 8260B
# Column to be used to flag recovery and RPD values
06/03/2010Page 109 of 623
FORM IV
GC/MS VOA METHOD BLANK SUMMARY
Lab Name:
SDG No.:
Job No.: 460-13139-1TestAmerica Edison
Date Analyzed:
GC Column: ID:
Instrument ID: 05/17/2010 20:11
DB-624
YHeated Purge:(Y/N)
VOAMS12
o37390.dLab File ID: Lab Sample ID: MB 460-37643/5
SolidMatrix:
0.18(mm)
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:
LAB SAMPLE ID
LAB
FILE ID DATE ANALYZEDCLIENT SAMPLE ID
05/17/2010 17:46o37386.dLCS 460-37643/3
05/17/2010 18:10o37387.dLCSD 460-37643/4
05/18/2010 00:18o37400.d460-13139-2TB-3 6-7
05/18/2010 00:43o37401.d460-13139-4TB-2 5-6
05/18/2010 01:08o37402.d460-13139-5TB-1 2-3
05/18/2010 01:33o37403.d460-13139-7TB-5 3-4
FORM IV 8260B
06/03/2010Page 110 of 623
FORM V
BROMOFLUOROBENZENE (BFB)
Lab Name:
SDG No.:
Job No.: 460-13139-1
Lab File ID:
Instrument ID:
o36289.d
VOAMS12
04/15/2010
13:12
BFB Injection Date:
BFB Injection Time:
M/E ION ABUNDANCE CRITERIA% RELATIVEABUNDANCE
Analysis Batch No.: 34969
50 15.0 - 40.0 % of mass 95 15.8
75 30.0 - 60.0 % of mass 95 47.6
95 Base Peak, 100% relative abundance 100.0
96 5.0 - 9.0 % of mass 95 6.5
173 Less than 2.0 % of mass 174 0.0 (0.0)1
174 50.0 - 120.00 % of mass 95 74.4
175 5.0 - 9.0 % of mass 174 6.1 (8.2)1
176 95.0 - 101.0 % of mass 174 73.8 (99.2)1
177 5.0 - 9.0 % of mass 176 5.0 (6.8)2
1-Value is % mass 174 2-Value is % mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:
GC/MS VOA INSTRUMENT PERFORMANCE CHECK
TestAmerica Edison
CLIENT SAMPLE IDLAB
FILE IDLAB SAMPLE IDDATE
ANALYZEDTIME
ANALYZED
o36292.d 04/15/2010 14:24IC 460-34969/2
o36294.d 04/15/2010 15:13IC 460-34969/3
o36295.d 04/15/2010 15:38ICIS 460-34969/19
o36296.d 04/15/2010 16:03IC 460-34969/20
o36297.d 04/15/2010 16:27IC 460-34969/6
o36298.d 04/15/2010 16:52IC 460-34969/7
FORM V 8260B 06/03/2010Page 111 of 623
FORM V
BROMOFLUOROBENZENE (BFB)
Lab Name:
SDG No.:
Job No.: 460-13139-1
Lab File ID:
Instrument ID:
o37384.d
VOAMS12
05/17/2010
16:42
BFB Injection Date:
BFB Injection Time:
M/E ION ABUNDANCE CRITERIA% RELATIVEABUNDANCE
Analysis Batch No.: 37643
50 15.0 - 40.0 % of mass 95 16.0
75 30.0 - 60.0 % of mass 95 49.0
95 Base Peak, 100% relative abundance 100.0
96 5.0 - 9.0 % of mass 95 6.5
173 Less than 2.0 % of mass 174 0.6 (0.9)1
174 50.0 - 120.00 % of mass 95 68.7
175 5.0 - 9.0 % of mass 174 5.2 (7.6)1
176 95.0 - 101.0 % of mass 174 66.0 (96.2)1
177 5.0 - 9.0 % of mass 176 3.6 (5.5)2
1-Value is % mass 174 2-Value is % mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:
GC/MS VOA INSTRUMENT PERFORMANCE CHECK
TestAmerica Edison
CLIENT SAMPLE IDLAB
FILE IDLAB SAMPLE IDDATE
ANALYZEDTIME
ANALYZED
o37385.d 05/17/2010 17:02CCVIS 460-37643/2
o37386.d 05/17/2010 17:46LCS 460-37643/3
o37387.d 05/17/2010 18:10LCSD 460-37643/4
o37390.d 05/17/2010 20:11MB 460-37643/5
TB-3 6-7 o37400.d 05/18/2010 00:18460-13139-2
TB-2 5-6 o37401.d 05/18/2010 00:43460-13139-4
TB-1 2-3 o37402.d 05/18/2010 01:08460-13139-5
TB-5 3-4 o37403.d 05/18/2010 01:33460-13139-7
FORM V 8260B 06/03/2010Page 112 of 623
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY
Lab Name: Job No.:
SDG No.:
FORM VIII
TestAmerica Edison 460-13139-1
Sample No.: CCVIS 460-37643/2 Date Analyzed: 05/17/2010 17:02
Lab File ID (Standard): o37385.d
Instrument ID: VOAMS12 GC Column: DB-624 ID: 0.18(mm)
Heated Purge: (Y/N) Y
Calibration ID: 5832
AREA # RT # AREA RT # AREA # RT ##
FB CBZ DCB
UPPER LIMIT
LOWER LIMIT
2954680
738670 542177
2168708
292159
1168634
4.26 8.05 11.7312/24 HOUR STD
4.76
3.76
8.55
7.55
12.23
11.23
1477340 1084354 584317
LAB SAMPLE ID CLIENT SAMPLE ID
LCS 460-37643/3 1596386 1094145 577641 4.26 8.05 11.73
LCSD 460-37643/4 1620590 1107274 586808 4.26 8.05 11.74
MB 460-37643/5 1237424 1154369 545686 4.26 8.05 11.73
460-13139-2 TB-3 6-7 1493462 1272951 616746 4.26 8.05 11.74
460-13139-4 TB-2 5-6 1437887 1144265 567459 4.26 8.05 11.73
460-13139-5 TB-1 2-3 1396875 1243273 600118 4.26 8.05 11.73
460-13139-7 TB-5 3-4 1175155 1039684 426343 4.26 8.05 11.73
FB = Fluorobenzene
CBZ = Chlorobenzene-d5
DCB = 1,4-Dichlorobenzene-d4
Area Limit = 50%-200% of internal standard area
RT Limit = ± 0.5 minutes of internal standard RT
# Column used to flag values outside QC limits
FORM VIII 8260B
06/03/2010Page 113 of 623
FORM IForm 1GC/MS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-3 6-7
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-2
Matrix: o37400.dLab File ID:
Date Collected:8260BAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 09:45
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:
18.8
1
Level: (low/med) Low
5.02(g)
0.18(mm)
Date Analyzed: 05/18/2010 00:18
ID:DB-624
Analysis Batch No.: 37643 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Chloromethane74-87-3 1.2 1.2 0.78U
Bromomethane74-83-9 1.2 1.2 0.50U
Vinyl chloride75-01-4 1.2 1.2 0.29U
Chloroethane75-00-3 1.2 1.2 0.49U
Methylene Chloride75-09-2 1.2 1.2 0.58U
Trichlorofluoromethane75-69-4 1.2 1.2 0.32U
1,1-Dichloroethene75-35-4 1.2 1.2 0.45U
1,1-Dichloroethane75-34-3 1.2 1.2 0.31U
trans-1,2-Dichloroethene156-60-5 1.2 1.2 0.35U
cis-1,2-Dichloroethene156-59-2 1.2 1.2 0.29U
Chloroform67-66-3 1.2 1.2 0.29U
1,2-Dichloroethane107-06-2 1.2 1.2 0.48U
1,1,1-Trichloroethane71-55-6 1.2 1.2 0.23U
Carbon tetrachloride56-23-5 1.2 1.2 0.12U
Bromodichloromethane75-27-4 1.2 1.2 0.37U
1,2-Dichloropropane78-87-5 1.2 1.2 0.39U
cis-1,3-Dichloropropene10061-01-5 1.2 1.2 0.25U
Trichloroethene79-01-6 1.2 1.2 0.45U
Dibromochloromethane124-48-1 1.2 1.2 0.69U
1,1,2-Trichloroethane79-00-5 1.2 1.2 0.73U
Benzene71-43-2 1.2 1.2 0.91U
trans-1,3-Dichloropropene10061-02-6 1.2 1.2 0.27U
2-Chloroethyl vinyl ether110-75-8 6.1 6.1 1.6U
Bromoform75-25-2 1.2 1.2 0.86U
Tetrachloroethene127-18-4 1.2 1.2 0.40U
1,1,2,2-Tetrachloroethane79-34-5 1.2 1.2 0.93U
Toluene108-88-3 1.2 1.2 0.37U
Chlorobenzene108-90-7 1.2 1.2 0.59U
Ethylbenzene100-41-4 1.2 1.2 0.23U
Xylenes, Total1330-20-7 3.7 3.7 0.96U
FORM I 8260B
06/03/2010Page 114 of 623
FORM IForm 1GC/MS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-3 6-7
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-2
Matrix: o37400.dLab File ID:
Date Collected:8260BAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 09:45
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:
18.8
1
Level: (low/med) Low
5.02(g)
0.18(mm)
Date Analyzed: 05/18/2010 00:18
ID:DB-624
Analysis Batch No.: 37643 ug/KgUnits:
SURROGATE %RECCAS NO. LIMITS Q
17060-07-0 1,2-Dichloroethane-d4 (Surr) 92 70-138
2037-26-5 Toluene-d8 (Surr) 88 66-126
460-00-4 Bromofluorobenzene 102 72-132
FORM I 8260B
06/03/2010Page 115 of 623
FORM IForm 1GC/MS VOA ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Client Sample ID:
Lab Name: Job No.:
TB-3 6-7
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-2
Matrix: o37400.dLab File ID:
Date Collected:8260BAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 09:45
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:
18.8
1
Level: (low/med) Low
5.02(g)
0.18(mm)
Date Analyzed: 05/18/2010 00:18
ID:DB-624
Analysis Batch No.: 37643 ug/KgUnits:
Number TICs Found: TIC Result Total: 00
QRTCOMPOUND NAME RESULTCAS NO.
Tentatively Identified Compound None
FORM I-TIC 8260B
06/03/2010Page 116 of 623
Data File: /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37400.dReport Date: 18-May-2010 09:27
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37400.dLab Smp Id: 460-13139-B-2-A Client Smp ID: TB-3 6-7Inj Date : 18-MAY-2010 00:18 Operator : VOAMS 9 Inst ID: VOAMS12.iSmp Info : 460-13139-B-2-A;;;5.02;5Misc Info : 460-13139-B-2-AComment : Method : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/8260L_10.mMeth Date : 17-May-2010 18:29 ken Quant Type: ISTDCal Date : 15-APR-2010 16:52 Cal File: o36298.dAls bottle: 16 Dil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd2
Concentration Formula: Amt * DF * ((Vt/Ws)/((100-M)/100)) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 5.00000 Volume of final extract (mL)Ws 5.02000 Weight of sample extracted (g)M 18.78882 % Moisture (not decanted)
Cpnd Variable Local Compound Variable
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE ( ug/L) (ug/Kg)
========================== ==== == ====== ====== ======== ======= =======
$ 16 1,2-Dichloroethane-d4 (SUR) 65 3.933 3.933 (0.923) 308316 45.9493 56
* 69 Fluorobenzene 96 4.262 4.262 (1.000) 1493462 50.0000
$ 37 Toluene-d8 (SUR) 98 6.072 6.073 (0.754) 1191531 43.8335 54
* 32 Chlorobenzene-d5 117 8.054 8.054 (1.000) 1272951 50.0000
$ 41 Bromofluorobenzene (SUR) 174 9.913 9.913 (0.845) 400760 50.9986 62
* 91 1,4-Dichlorobenzene-d4 152 11.736 11.730 (1.000) 616746 50.0000
06/03/2010Page 117 of 623
Data File: /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37400.dReport Date: 18-May-2010 09:27
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37400.dLab Smp Id: 460-13139-B-2-A Client Smp ID: TB-3 6-7Inj Date : 18-MAY-2010 00:18 Operator : VOAMS 9 Inst ID: VOAMS12.iSmp Info : 460-13139-B-2-A;;;5.02;5Misc Info : 460-13139-B-2-AComment : Method : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/8260L_10.mMeth Date : 17-May-2010 18:29 ken Quant Type: ISTDCal Date : 15-APR-2010 16:52 Cal File: o36298.dAls bottle: 16 Dil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd2
- NO TENTATIVELY IDENTIFIED COMPOUNDS -
06/03/2010Page 118 of 623
Data File: o37400.d
Date: 18-MAY-2010 00:18
Client ID: TB-3 6-7 Instrument: VOAMS12.i
Sample Info: 460-13139-B-2-A;;;5.02;5 Operator: VOAMS 9
06/03/2010Page 119 of 623
FORM IForm 1GC/MS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-2 5-6
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-4
Matrix: o37401.dLab File ID:
Date Collected:8260BAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 10:45
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:
12.8
1
Level: (low/med) Low
3.75(g)
0.18(mm)
Date Analyzed: 05/18/2010 00:43
ID:DB-624
Analysis Batch No.: 37643 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Chloromethane74-87-3 1.5 1.5 0.97U
Bromomethane74-83-9 1.5 1.5 0.63U
Vinyl chloride75-01-4 1.5 1.5 0.36U
Chloroethane75-00-3 1.5 1.5 0.61U
Methylene Chloride75-09-2 1.5 1.5 0.72U
Trichlorofluoromethane75-69-4 1.5 1.5 0.40U
1,1-Dichloroethene75-35-4 1.5 1.5 0.56U
1,1-Dichloroethane75-34-3 1.5 1.5 0.39U
trans-1,2-Dichloroethene156-60-5 1.5 1.5 0.43U
cis-1,2-Dichloroethene156-59-2 1.5 1.5 0.36U
Chloroform67-66-3 1.5 1.5 0.36U
1,2-Dichloroethane107-06-2 1.5 1.5 0.60U
1,1,1-Trichloroethane71-55-6 1.5 1.5 0.29U
Carbon tetrachloride56-23-5 1.5 1.5 0.15U
Bromodichloromethane75-27-4 1.5 1.5 0.46U
1,2-Dichloropropane78-87-5 1.5 1.5 0.49U
cis-1,3-Dichloropropene10061-01-5 1.5 1.5 0.31U
Trichloroethene79-01-6 1.5 1.5 0.55U
Dibromochloromethane124-48-1 1.5 1.5 0.86U
1,1,2-Trichloroethane79-00-5 1.5 1.5 0.91U
Benzene71-43-2 1.5 1.5 1.1U
trans-1,3-Dichloropropene10061-02-6 1.5 1.5 0.34U
2-Chloroethyl vinyl ether110-75-8 7.6 7.6 1.9U
Bromoform75-25-2 1.5 1.5 1.1U
Tetrachloroethene127-18-4 1.5 1.5 0.50U
1,1,2,2-Tetrachloroethane79-34-5 1.5 1.5 1.2U
Toluene108-88-3 1.5 1.5 0.46U
Chlorobenzene108-90-7 1.5 1.5 0.74U
Ethylbenzene100-41-4 1.5 1.5 0.29U
Xylenes, Total1330-20-7 4.6 4.6 1.2U
FORM I 8260B
06/03/2010Page 120 of 623
FORM IForm 1GC/MS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-2 5-6
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-4
Matrix: o37401.dLab File ID:
Date Collected:8260BAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 10:45
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:
12.8
1
Level: (low/med) Low
3.75(g)
0.18(mm)
Date Analyzed: 05/18/2010 00:43
ID:DB-624
Analysis Batch No.: 37643 ug/KgUnits:
SURROGATE %RECCAS NO. LIMITS Q
17060-07-0 1,2-Dichloroethane-d4 (Surr) 95 70-138
2037-26-5 Toluene-d8 (Surr) 89 66-126
460-00-4 Bromofluorobenzene 105 72-132
FORM I 8260B
06/03/2010Page 121 of 623
FORM IForm 1GC/MS VOA ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Client Sample ID:
Lab Name: Job No.:
TB-2 5-6
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-4
Matrix: o37401.dLab File ID:
Date Collected:8260BAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 10:45
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:
12.8
1
Level: (low/med) Low
3.75(g)
0.18(mm)
Date Analyzed: 05/18/2010 00:43
ID:DB-624
Analysis Batch No.: 37643 ug/KgUnits:
Number TICs Found: TIC Result Total: 00
QRTCOMPOUND NAME RESULTCAS NO.
Tentatively Identified Compound None
FORM I-TIC 8260B
06/03/2010Page 122 of 623
Data File: /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37401.dReport Date: 18-May-2010 09:28
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37401.dLab Smp Id: 460-13139-B-4-A Client Smp ID: TB-2 5-6Inj Date : 18-MAY-2010 00:43 Operator : VOAMS 9 Inst ID: VOAMS12.iSmp Info : 460-13139-B-4-A;;;3.75;5Misc Info : 460-13139-B-4-AComment : Method : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/8260L_10.mMeth Date : 17-May-2010 18:29 ken Quant Type: ISTDCal Date : 15-APR-2010 16:52 Cal File: o36298.dAls bottle: 17 Dil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd2
Concentration Formula: Amt * DF * ((Vt/Ws)/((100-M)/100)) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 5.00000 Volume of final extract (mL)Ws 3.75000 Weight of sample extracted (g)M 12.77533 % Moisture (not decanted)
Cpnd Variable Local Compound Variable
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE ( ug/L) (ug/Kg)
========================== ==== == ====== ====== ======== ======= =======
$ 16 1,2-Dichloroethane-d4 (SUR) 65 3.933 3.933 (0.923) 306931 47.5108 73
* 69 Fluorobenzene 96 4.262 4.262 (1.000) 1437887 50.0000
$ 37 Toluene-d8 (SUR) 98 6.073 6.073 (0.754) 1088814 44.5595 68
* 32 Chlorobenzene-d5 117 8.054 8.054 (1.000) 1144265 50.0000
$ 41 Bromofluorobenzene (SUR) 174 9.913 9.913 (0.845) 380967 52.6906 80
* 91 1,4-Dichlorobenzene-d4 152 11.730 11.730 (1.000) 567459 50.0000
06/03/2010Page 123 of 623
Data File: /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37401.dReport Date: 18-May-2010 09:28
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37401.dLab Smp Id: 460-13139-B-4-A Client Smp ID: TB-2 5-6Inj Date : 18-MAY-2010 00:43 Operator : VOAMS 9 Inst ID: VOAMS12.iSmp Info : 460-13139-B-4-A;;;3.75;5Misc Info : 460-13139-B-4-AComment : Method : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/8260L_10.mMeth Date : 17-May-2010 18:29 ken Quant Type: ISTDCal Date : 15-APR-2010 16:52 Cal File: o36298.dAls bottle: 17 Dil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd2
- NO TENTATIVELY IDENTIFIED COMPOUNDS -
06/03/2010Page 124 of 623
Data File: o37401.d
Date: 18-MAY-2010 00:43
Client ID: TB-2 5-6 Instrument: VOAMS12.i
Sample Info: 460-13139-B-4-A;;;3.75;5 Operator: VOAMS 9
06/03/2010Page 125 of 623
FORM IForm 1GC/MS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-1 2-3
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-5
Matrix: o37402.dLab File ID:
Date Collected:8260BAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 11:25
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:
6.5
1
Level: (low/med) Low
3.09(g)
0.18(mm)
Date Analyzed: 05/18/2010 01:08
ID:DB-624
Analysis Batch No.: 37643 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Chloromethane74-87-3 1.7 1.7 1.1U
Bromomethane74-83-9 1.7 1.7 0.71U
Vinyl chloride75-01-4 1.7 1.7 0.41U
Chloroethane75-00-3 1.7 1.7 0.69U
Methylene Chloride75-09-2 1.7 1.7 0.82U
Trichlorofluoromethane75-69-4 1.7 1.7 0.45U
1,1-Dichloroethene75-35-4 1.7 1.7 0.64U
1,1-Dichloroethane75-34-3 1.7 1.7 0.44U
trans-1,2-Dichloroethene156-60-5 1.7 1.7 0.49U
cis-1,2-Dichloroethene156-59-2 1.7 1.7 0.41U
Chloroform67-66-3 1.7 1.7 0.41U
1,2-Dichloroethane107-06-2 1.7 1.7 0.68U
1,1,1-Trichloroethane71-55-6 1.7 1.7 0.32U
Carbon tetrachloride56-23-5 1.7 1.7 0.17U
Bromodichloromethane75-27-4 1.7 1.7 0.53U
1,2-Dichloropropane78-87-5 1.7 1.7 0.55U
cis-1,3-Dichloropropene10061-01-5 1.7 1.7 0.35U
Trichloroethene79-01-6 1.7 1.7 0.63U
Dibromochloromethane124-48-1 1.7 1.7 0.97U
1,1,2-Trichloroethane79-00-5 1.7 1.7 1.0U
Benzene71-43-2 1.7 1.7 1.3U
trans-1,3-Dichloropropene10061-02-6 1.7 1.7 0.38U
2-Chloroethyl vinyl ether110-75-8 8.7 8.7 2.2U
Bromoform75-25-2 1.7 1.7 1.2U
Tetrachloroethene127-18-4 1.7 1.7 0.57U
1,1,2,2-Tetrachloroethane79-34-5 1.7 1.7 1.3U
Toluene108-88-3 1.7 1.7 0.52U
Chlorobenzene108-90-7 1.7 1.7 0.83U
Ethylbenzene100-41-4 1.7 1.7 0.33U
Xylenes, Total1330-20-7 5.2 5.2 1.4U
FORM I 8260B
06/03/2010Page 126 of 623
FORM IForm 1GC/MS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-1 2-3
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-5
Matrix: o37402.dLab File ID:
Date Collected:8260BAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 11:25
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:
6.5
1
Level: (low/med) Low
3.09(g)
0.18(mm)
Date Analyzed: 05/18/2010 01:08
ID:DB-624
Analysis Batch No.: 37643 ug/KgUnits:
SURROGATE %RECCAS NO. LIMITS Q
17060-07-0 1,2-Dichloroethane-d4 (Surr) 100 70-138
2037-26-5 Toluene-d8 (Surr) 90 66-126
460-00-4 Bromofluorobenzene 108 72-132
FORM I 8260B
06/03/2010Page 127 of 623
FORM IForm 1GC/MS VOA ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Client Sample ID:
Lab Name: Job No.:
TB-1 2-3
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-5
Matrix: o37402.dLab File ID:
Date Collected:8260BAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 11:25
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:
6.5
1
Level: (low/med) Low
3.09(g)
0.18(mm)
Date Analyzed: 05/18/2010 01:08
ID:DB-624
Analysis Batch No.: 37643 ug/KgUnits:
Number TICs Found: TIC Result Total: 00
QRTCOMPOUND NAME RESULTCAS NO.
Tentatively Identified Compound None
FORM I-TIC 8260B
06/03/2010Page 128 of 623
Data File: /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37402.dReport Date: 18-May-2010 09:29
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37402.dLab Smp Id: 460-13139-B-5-A Client Smp ID: TB-1 2-3Inj Date : 18-MAY-2010 01:08 Operator : VOAMS 9 Inst ID: VOAMS12.iSmp Info : 460-13139-B-5-A;;;3.09;5Misc Info : 460-13139-B-5-AComment : Method : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/8260L_10.mMeth Date : 17-May-2010 18:29 ken Quant Type: ISTDCal Date : 15-APR-2010 16:52 Cal File: o36298.dAls bottle: 18 Dil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd2
Concentration Formula: Amt * DF * ((Vt/Ws)/((100-M)/100)) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 5.00000 Volume of final extract (mL)Ws 3.09000 Weight of sample extracted (g)M 6.50888 % Moisture (not decanted)
Cpnd Variable Local Compound Variable
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE ( ug/L) (ug/Kg)
========================== ==== == ====== ====== ======== ======= =======
$ 16 1,2-Dichloroethane-d4 (SUR) 65 3.933 3.933 (0.923) 312712 49.8269 86
* 69 Fluorobenzene 96 4.262 4.262 (1.000) 1396875 50.0000
$ 37 Toluene-d8 (SUR) 98 6.073 6.073 (0.754) 1200401 45.2140 78
* 32 Chlorobenzene-d5 117 8.054 8.054 (1.000) 1243273 50.0000
$ 41 Bromofluorobenzene (SUR) 174 9.913 9.913 (0.845) 414392 54.1944 94
* 91 1,4-Dichlorobenzene-d4 152 11.730 11.730 (1.000) 600118 50.0000
06/03/2010Page 129 of 623
Data File: /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37402.dReport Date: 18-May-2010 09:29
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37402.dLab Smp Id: 460-13139-B-5-A Client Smp ID: TB-1 2-3Inj Date : 18-MAY-2010 01:08 Operator : VOAMS 9 Inst ID: VOAMS12.iSmp Info : 460-13139-B-5-A;;;3.09;5Misc Info : 460-13139-B-5-AComment : Method : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/8260L_10.mMeth Date : 17-May-2010 18:29 ken Quant Type: ISTDCal Date : 15-APR-2010 16:52 Cal File: o36298.dAls bottle: 18 Dil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd2
- NO TENTATIVELY IDENTIFIED COMPOUNDS -
06/03/2010Page 130 of 623
Data File: o37402.d
Date: 18-MAY-2010 01:08
Client ID: TB-1 2-3 Instrument: VOAMS12.i
Sample Info: 460-13139-B-5-A;;;3.09;5 Operator: VOAMS 9
06/03/2010Page 131 of 623
FORM IForm 1GC/MS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-5 3-4
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-7
Matrix: o37403.dLab File ID:
Date Collected:8260BAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 12:30
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:
61.5
1
Level: (low/med) Low
2.50(g)
0.18(mm)
Date Analyzed: 05/18/2010 01:33
ID:DB-624
Analysis Batch No.: 37643 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Chloromethane74-87-3 5.2 5.2 3.3U
Bromomethane74-83-9 5.2 5.2 2.1U
Vinyl chloride75-01-4 5.2 5.2 1.2U
Chloroethane75-00-3 5.2 5.2 2.1U
Methylene Chloride75-09-2 5.2 5.2 2.4U
Trichlorofluoromethane75-69-4 5.2 5.2 1.4U
1,1-Dichloroethene75-35-4 5.2 5.2 1.9U
1,1-Dichloroethane75-34-3 5.2 5.2 1.3U
trans-1,2-Dichloroethene156-60-5 5.2 5.2 1.5U
cis-1,2-Dichloroethene156-59-2 5.2 5.2 1.2U
Chloroform67-66-3 5.2 5.2 1.2U
1,2-Dichloroethane107-06-2 5.2 5.2 2.0U
1,1,1-Trichloroethane71-55-6 5.2 5.2 0.97U
Carbon tetrachloride56-23-5 5.2 5.2 0.53U
Bromodichloromethane75-27-4 5.2 5.2 1.6U
1,2-Dichloropropane78-87-5 5.2 5.2 1.7U
cis-1,3-Dichloropropene10061-01-5 5.2 5.2 1.0U
Trichloroethene79-01-6 5.2 5.2 1.9U
Dibromochloromethane124-48-1 5.2 5.2 2.9U
1,1,2-Trichloroethane79-00-5 5.2 5.2 3.1U
Benzene71-43-2 5.2 5.2 3.8U
trans-1,3-Dichloropropene10061-02-6 5.2 5.2 1.1U
2-Chloroethyl vinyl ether110-75-8 26 26 6.6U
Bromoform75-25-2 5.2 5.2 3.6U
Tetrachloroethene127-18-4 5.2 5.2 1.7U
1,1,2,2-Tetrachloroethane79-34-5 5.2 5.2 4.0U
Toluene108-88-3 5.2 5.2 1.6U
Chlorobenzene108-90-7 5.2 5.2 2.5U
Ethylbenzene100-41-4 5.2 5.2 0.99U
Xylenes, Total1330-20-7 16 16 4.1U
FORM I 8260B
06/03/2010Page 132 of 623
FORM IForm 1GC/MS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-5 3-4
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-7
Matrix: o37403.dLab File ID:
Date Collected:8260BAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 12:30
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:
61.5
1
Level: (low/med) Low
2.50(g)
0.18(mm)
Date Analyzed: 05/18/2010 01:33
ID:DB-624
Analysis Batch No.: 37643 ug/KgUnits:
SURROGATE %RECCAS NO. LIMITS Q
17060-07-0 1,2-Dichloroethane-d4 (Surr) 89 70-138
2037-26-5 Toluene-d8 (Surr) 73 66-126
460-00-4 Bromofluorobenzene 92 72-132
FORM I 8260B
06/03/2010Page 133 of 623
FORM IForm 1GC/MS VOA ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Client Sample ID:
Lab Name: Job No.:
TB-5 3-4
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-7
Matrix: o37403.dLab File ID:
Date Collected:8260BAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 12:30
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:
61.5
1
Level: (low/med) Low
2.50(g)
0.18(mm)
Date Analyzed: 05/18/2010 01:33
ID:DB-624
Analysis Batch No.: 37643 ug/KgUnits:
Number TICs Found: TIC Result Total: 13483
QRTCOMPOUND NAME RESULTCAS NO.
67-64-1 Acetone 1100 1.94
78-93-3 2-Butanone (MEK) 220 3.23
Unknown 28 10.68 T J
FORM I-TIC 8260B
06/03/2010Page 134 of 623
Data File: /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37403.dReport Date: 18-May-2010 09:53
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37403.dLab Smp Id: 460-13139-B-7-A Client Smp ID: TB-5 3-4Inj Date : 18-MAY-2010 01:33 Operator : VOAMS 9 Inst ID: VOAMS12.iSmp Info : 460-13139-B-7-A;;;2.50;5Misc Info : 460-13139-B-7-AComment : Method : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/8260L_10.mMeth Date : 17-May-2010 18:29 ken Quant Type: ISTDCal Date : 15-APR-2010 16:52 Cal File: o36298.dAls bottle: 19 Dil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd2
Concentration Formula: Amt * DF * ((Vt/Ws)/((100-M)/100)) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 5.00000 Volume of final extract (mL)Ws 2.50000 Weight of sample extracted (g)M 0.00000 % Moisture (not decanted)
Cpnd Variable Local Compound Variable
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE ( ug/L) (ug/Kg)
========================== ==== == ====== ====== ======== ======= =======
7 Acetone 43 1.939 1.939 (0.455) 364133 218.087 440
8 Carbon Disulfide 76 2.043 2.037 (0.479) 79922 3.20859 6.4
18 2-Butanone 72 3.226 3.213 (0.757) 38209 42.9502 86
$ 16 1,2-Dichloroethane-d4 (SUR) 65 3.933 3.933 (0.923) 233909 44.3025 89
* 69 Fluorobenzene 96 4.262 4.262 (1.000) 1175155 50.0000
$ 37 Toluene-d8 (SUR) 98 6.073 6.073 (0.754) 809402 36.4566 73
* 32 Chlorobenzene-d5 117 8.054 8.054 (1.000) 1039684 50.0000
$ 41 Bromofluorobenzene (SUR) 174 9.913 9.913 (0.845) 250805 46.1697 92
112 n-Propylbenzene 91 10.377 10.377 (0.885) 41788 0.89175 1.8(a)
* 91 1,4-Dichlorobenzene-d4 152 11.730 11.730 (1.000) 426343 50.0000
70 Naphthalene 128 14.016 14.016 (1.195) 59928 2.13807 4.3
06/03/2010Page 135 of 623
Data File: /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37403.dReport Date: 18-May-2010 09:53
QC Flag Legend
a - Target compound detected but, quantitated amountBelow Limit Of Quantitation(BLOQ).
06/03/2010Page 136 of 623
Data File: /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37403.dReport Date: 18-May-2010 09:53
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37403.dLab Smp Id: 460-13139-B-7-A Client Smp ID: TB-5 3-4Inj Date : 18-MAY-2010 01:33 Operator : VOAMS 9 Inst ID: VOAMS12.iSmp Info : 460-13139-B-7-A;;;2.50;5Misc Info : 460-13139-B-7-AComment : Method : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/8260L_10.mMeth Date : 17-May-2010 18:29 ken Quant Type: ISTDCal Date : 15-APR-2010 16:52 Cal File: o36298.dAls bottle: 19 Dil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd2
Concentration Formula: Amt * DF * ((Vt/Ws)/((100-M)/100)) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 5.00000 Volume of final extract (mL)Ws 2.50000 Weight of sample extracted (g)M 0.00000 % Moisture (not decanted)
Cpnd Variable Local Compound Variable
ISTD RT AREA AMOUNT======== ==== ====== ======
* 91 1,4-Dichlorobenzene-d4 11.730 2775259 50.000
CONCENTRATIONS QUANT
RT AREA ON-COL( ug/L) FINAL(ug/Kg) QUAL LIBRARY LIB ENTRY CPND #
==== ==== ============= ============ ==== ======= ========= ======
Unknown CAS #:
10.675 296942 5.34980704 11 0 0 91
06/03/2010Page 137 of 623
Data File: o37403.d
Date: 18-MAY-2010 01:33
Client ID: TB-5 3-4 Instrument: VOAMS12.i
Sample Info: 460-13139-B-7-A;;;2.50;5 Operator: VOAMS 9
06/03/2010Page 138 of 623
Data File: o37403.d
Date: 18-MAY-2010 01:33
Client ID: TB-5 3-4 Instrument: VOAMS12.i
Sample Info: 460-13139-B-7-A;;;2.50;5 Operator: VOAMS 9
7 Acetone
06/03/2010Page 139 of 623
Data File: o37403.d
Date: 18-MAY-2010 01:33
Client ID: TB-5 3-4 Instrument: VOAMS12.i
Sample Info: 460-13139-B-7-A;;;2.50;5 Operator: VOAMS 9
18 2-Butanone
06/03/2010Page 140 of 623
Data File: o37403.d
Date: 18-MAY-2010 01:33
Client ID: TB-5 3-4 Instrument: VOAMS12.i
Sample Info: 460-13139-B-7-A;;;2.50;5 Operator: VOAMS 9
Retention Time: 10.68
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Unknown
Bicyclo[2.2.1]heptane, 2-ethyl- 2146-41-0 NIST02.l 10368 53 C9H16 124
Bicyclo[2.2.1]heptane, 2,2,3-trime 473-19-8 NIST02.l 16369 49 C10H18 138
06/03/2010Page 141 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC/MS VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
VOAMS12
Analy Batch No.: 34969
5832Calibration Start Date: Calibration End Date:04/15/2010 14:24
Y
04/15/2010 16:52
0.18(mm)DB-624 ID:
INTERNAL STANDARD CURVE EVALUTION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-34969/2 o36292.d2Level IC 460-34969/3 o36294.d3Level ICIS 460-34969/19 o36295.d4Level IC 460-34969/20 o36296.d5Level IC 460-34969/6 o36297.d6Level IC 460-34969/7 o36298.d
ANALYTE RRF
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CURVETYPE
COEFFICIENT
B M1 M2
# %RSD # MAX%RSD
R^2OR COD
# MIN R^2OR COD
MIN RRF
LVL 6
1-Chloropropane +++++ +++++ +++++ +++++ +++++ Ave+++++
15.0
2-Chloropropane +++++ +++++ +++++ +++++ +++++ Ave+++++
15.0
Propene +++++ +++++ +++++ +++++ +++++ Ave+++++
15.0
Dichlorodifluoromethane 0.5422 0.5230 0.4719 0.4493 0.3392 LinF 0.99800.3324
0.99000.3350
Chloromethane 0.7369 0.6514 0.6123 0.5870 0.4788 LinF 0.99750.4445
0.99000.4514
Vinyl chloride 0.6601 0.6229 0.5878 0.5762 0.4739 LinF 0.99770.4412
0.99000.4477
Bromomethane 0.5004 0.4223 0.3596 0.3414 0.2989 LinF 0.99970.3024
0.99000.3024
Chloroethane 0.4318 0.3538 0.3330 0.3191 0.2733 LinF 0.99890.2611
0.1000 0.99000.2636
Trichlorofluoromethane 0.8600 0.7309 0.7035 0.6806 0.5835 LinF 0.99940.5714
0.99000.5744
n-Pentane 0.0786 0.0654 0.0729 0.0691 0.0621 Ave 9.50.0624
15.00.0684
Ethanol 0.0021 0.0025 0.0021 0.0022 0.0019 Ave 11.10.0019
15.00.0021
Ethyl ether 0.3123 0.2860 0.2487 0.2510 0.2423 Ave 11.20.2380
15.00.2631
Isopropene 0.5603 0.5498 0.5790 0.5747 0.5229 Ave 5.40.5045
15.00.5485
Acrolein 0.0326 0.0383 0.0348 0.0342 0.0432 Ave 11.60.0419
15.00.0375
Freon TF 0.4614 0.4173 0.3915 0.3885 0.3381 Ave 12.10.3393
15.00.3893
FORM VI 8260B
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 142 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC/MS VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
VOAMS12
Analy Batch No.: 34969
5832Calibration Start Date: Calibration End Date:04/15/2010 14:24
Y
04/15/2010 16:52
0.18(mm)DB-624 ID:
INTERNAL STANDARD CURVE EVALUTION
ANALYTE RRF
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CURVETYPE
COEFFICIENT
B M1 M2
# %RSD # MAX%RSD
R^2OR COD
# MIN R^2OR COD
MIN RRF
LVL 6
1,1-Dichloroethene 0.3567 0.3868 0.3609 0.3527 0.2925 Ave 12.70.2780
30.00.3379
Acetone 0.2171 0.1630 0.1347 0.1050 0.0764 LinF 0.99740.0705
0.99000.0710
Iodomethane 0.4149 0.4209 0.4047 0.4057 0.3919 Ave 5.40.3611
15.00.3999
Carbon disulfide 1.1556 1.1071 0.9874 0.9904 1.0476 Ave 6.21.0708
15.01.0598
Isopropanol 0.0335 0.0285 0.0263 0.0252 0.0223 QuaF 0.99390.0224
0.990027.334 6.7713
Acetonitrile 0.0797 0.0687 0.0555 0.0514 0.0413 LinF 0.99710.0383
0.99000.0389
Methyl acetate 0.1414 0.1031 0.0986 0.0946 0.0739 LinF 0.99820.0714
0.99000.0721
Methylene Chloride 0.6993 0.4490 0.4137 0.3900 0.3457 LinF 0.99890.3276
0.99000.3310
TBA 0.0449 0.0371 0.0363 0.0324 0.0315 Ave 14.30.0319
15.00.0357
Acrylonitrile 0.1378 0.1573 0.1442 0.1383 0.1202 Ave 10.00.1230
15.00.1368
trans-1,2-Dichloroethene 0.4591 0.3997 0.4069 0.3867 0.3531 Ave 10.80.3413
15.00.3911
MTBE 0.7522 0.7264 0.7701 0.7537 0.8260 Ave 5.40.8293
15.00.7763
Hexane 0.2712 0.2468 0.2783 0.3051 0.2725 Ave 7.00.2879
15.00.2770
1,1-Dichloroethane 0.7985 0.6736 0.6844 0.6636 0.6035 Ave 11.40.5809
0.1000 15.00.6674
Vinyl acetate 0.7102 0.6659 0.6585 0.7316 0.8552 Ave 12.10.8631
15.00.7474
DIPE 0.9238 0.8739 0.9124 0.9208 0.9686 Ave 4.30.9825
15.00.9303
Tert-butyl ethyl ether 0.8043 0.7458 0.7718 0.7954 0.8662 Ave 6.80.8894
15.00.8122
2,2-Dichloropropane 0.4367 0.4241 0.4810 0.4947 0.4619 Ave 5.90.4469
15.00.4576
cis-1,2-Dichloroethene 0.4420 0.4127 0.3905 0.3782 0.3555 Ave 9.40.3441
15.00.3871
2-Butanone (MEK) 0.0402 0.0413 0.0418 0.0358 0.0356 Ave 9.90.0325
15.00.0379
FORM VI 8260B
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 143 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC/MS VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
VOAMS12
Analy Batch No.: 34969
5832Calibration Start Date: Calibration End Date:04/15/2010 14:24
Y
04/15/2010 16:52
0.18(mm)DB-624 ID:
INTERNAL STANDARD CURVE EVALUTION
ANALYTE RRF
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CURVETYPE
COEFFICIENT
B M1 M2
# %RSD # MAX%RSD
R^2OR COD
# MIN R^2OR COD
MIN RRF
LVL 6
Ethyl acetate 0.0343 0.0270 0.0273 0.0270 0.0272 Ave 10.30.0274
15.00.0284
Bromochloromethane 0.1824 0.1690 0.1589 0.1525 0.1433 Ave 10.80.1362
15.00.1570
Chloroform 0.7318 0.6185 0.6128 0.5890 0.5544 Ave 10.90.5499
30.00.6094
1,1,1-Trichloroethane 0.5194 0.4678 0.5175 0.5211 0.4874 Ave 4.90.4747
15.00.4980
Cyclohexane 0.7209 0.7001 0.6953 0.6890 0.6215 Ave 5.90.6323
15.00.6765
Carbon tetrachloride 0.3909 0.3596 0.4181 0.4239 0.4178 Ave 6.10.4124
15.00.4038
1,1-Dichloropropene 0.4333 0.4166 0.4845 0.4915 0.4867 Ave 6.70.4623
15.00.4625
Benzene 1.4368 1.2625 1.4254 1.4012 1.3909 Ave 7.11.2032
15.01.3534
1,2-Dichloroethane 0.5055 0.4206 0.3973 0.3883 0.3803 Ave 11.90.3750
15.00.4112
Isopropyl acetate 0.5114 0.4721 0.4965 0.5065 0.5711 Ave 8.80.5917
15.00.5249
Tert-amyl methyl ether 0.7638 0.6725 0.6680 0.6704 0.7741 Ave 8.70.8091
15.00.7263
2,4,4-Trimethyl-1-pentene 0.1589 0.1533 0.1271 0.1094 0.1244 LinF 0.99860.1145
0.99000.1160
n-Butanol 0.0056 0.0051 0.0049 0.0051 0.0059 Ave 7.9+++++
15.00.0053
Trichloroethene 0.3853 0.2935 0.3554 0.3502 0.3483 Ave 8.70.3348
15.00.3446
Ethyl acrylate 0.2788 0.3205 0.3000 0.2903 0.3398 Ave 11.50.3775
15.00.3178
Methylcyclohexane 0.6899 0.6140 0.6233 0.6729 0.6673 Ave 4.80.6806
15.00.6580
1,2-Dichloropropane 0.3272 0.3162 0.3472 0.3397 0.3525 Ave 4.00.3412
30.00.3373
Dibromomethane 0.2263 0.1838 0.1837 0.1683 0.1706 Ave 12.90.1605
15.00.1822
Methyl methacrylate 0.2304 0.1751 0.1533 0.1547 0.1778 LinF 0.99970.1806
0.99000.1800
1,4-Dioxane 0.0053 0.0050 0.0047 0.0048 0.0040 Ave 10.90.0040
15.00.0046
FORM VI 8260B
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 144 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC/MS VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
VOAMS12
Analy Batch No.: 34969
5832Calibration Start Date: Calibration End Date:04/15/2010 14:24
Y
04/15/2010 16:52
0.18(mm)DB-624 ID:
INTERNAL STANDARD CURVE EVALUTION
ANALYTE RRF
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CURVETYPE
COEFFICIENT
B M1 M2
# %RSD # MAX%RSD
R^2OR COD
# MIN R^2OR COD
MIN RRF
LVL 6
Propyl acetate 0.6412 0.4143 0.3513 0.3249 0.3538 LinF 0.99980.3615
0.99000.3602
Bromodichloromethane 0.3759 0.3509 0.3764 0.3816 0.4128 Ave 5.90.4072
15.00.3841
2-Chloroethyl vinyl ether 0.1481 0.1363 0.1568 0.1534 0.1721 Ave 9.10.1731
15.00.1566
Epichlorohydrin 0.0353 0.0318 0.0313 0.0314 0.0298 Ave 6.90.0291
15.00.0314
cis-1,3-Dichloropropene 0.4131 0.3734 0.4403 0.4623 0.5085 Ave 11.70.5047
15.00.4504
4-Methyl-2-pentanone 0.2698 0.2986 0.2259 0.2063 0.2312 Ave 13.50.2440
15.00.2460
Toluene 2.3018 1.9052 2.1270 2.1672 2.2207 Ave 9.01.8199
30.02.0903
trans-1,3-Dichloropropene 0.3710 0.3293 0.4953 0.6079 0.6839 LinF 0.99940.6555
0.99000.6590
1,1,2-Trichloroethane 0.2547 0.2126 0.2863 0.3296 0.3372 LinF 0.99920.3160
0.99000.3191
Tetrachloroethene 0.4564 0.3454 0.4757 0.5142 0.5068 Ave 13.20.4744
15.00.4622
1,3-Dichloropropane 0.5130 0.4647 0.6361 0.7046 0.7217 LinF 0.99890.6696
0.99000.6775
2-Hexanone 0.2538 0.2803 0.2756 0.2502 0.2560 Ave 4.70.2622
15.00.2630
Dibromochloromethane 0.2869 0.2226 0.3072 0.3707 0.4176 LinF 0.99960.4085
0.99000.4093
Butyl acetate 0.5680 0.5336 0.5756 0.5675 0.5791 Ave 3.40.5902
15.00.5690
1,2-Dibromoethane 0.3063 0.2340 0.3332 0.3706 0.3860 LinF 0.99880.3569
0.99000.3613
Chlorobenzene 1.2679 1.1200 1.2725 1.2968 1.3206 Ave 5.71.2848
0.3000 15.01.2604
1,1,1,2-Tetrachloroethane 0.2799 0.2352 0.3204 0.3925 0.4407 LinF 0.99970.4357
0.99000.4359
Ethylbenzene 0.7265 0.6553 0.8122 0.7992 0.7490 Ave 7.60.7259
30.00.7447
m&p-Xylene 0.8901 0.7708 0.9340 1.0419 0.9389 Ave 9.80.8795
15.00.9092
o-Xylene 0.7751 0.6844 0.8605 0.9569 0.8858 Ave 11.30.8442
15.00.8345
FORM VI 8260B
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 145 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC/MS VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
VOAMS12
Analy Batch No.: 34969
5832Calibration Start Date: Calibration End Date:04/15/2010 14:24
Y
04/15/2010 16:52
0.18(mm)DB-624 ID:
INTERNAL STANDARD CURVE EVALUTION
ANALYTE RRF
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CURVETYPE
COEFFICIENT
B M1 M2
# %RSD # MAX%RSD
R^2OR COD
# MIN R^2OR COD
MIN RRF
LVL 6
Styrene 1.2501 1.2182 1.4946 1.6541 1.5547 Ave 12.01.4868
15.01.4431
Butyl acrylate 1.3787 1.2580 1.4226 1.5065 1.5332 Ave 10.21.6981
15.01.4662
Bromoform 0.1386 0.1208 0.1751 0.2106 0.2513 LinF 0.99940.2460
0.1000 0.99000.2464
Amly acetate 0.4099 0.3020 0.3435 0.3906 0.3512 Ave 10.50.3574
15.00.3591
Isopropylbenzene 2.1964 2.0047 2.4498 2.6946 2.3715 Ave 11.1+++++
15.02.3434
Camphene, Total 2.2489 1.9256 2.1205 2.0478 1.9104 Ave 6.22.1013
15.02.0591
Monobromobenzene 0.9530 0.8847 0.9827 0.9396 0.9594 Ave 3.60.9675
15.00.9478
1,1,2,2-Tetrachloroethane 0.8387 0.8089 0.8413 0.8148 0.9519 Ave 7.70.9550
0.3000 15.00.8684
1,2,3-Trichloropropane 0.2734 0.2262 0.2388 0.2331 0.2634 Ave 7.50.2556
15.00.2484
trans-1,4-Dichloro-2-butene 0.1289 0.1059 0.0854 0.0864 0.0933 LinF 0.99960.0970
0.99000.0964
N-Propylbenzene 5.4669 5.0455 5.9803 5.9824 5.9666 Ave 11.04.5322
15.05.4957
2-Chlorotoluene 2.9808 2.8955 3.1492 3.1611 3.2284 Ave 4.33.2030
15.03.1030
4-Chlorotoluene 3.4495 3.1411 3.6488 3.5594 3.4194 Ave 5.13.3468
15.03.4275
1,3,5-Trimethylbenzene 3.4507 3.2570 3.6512 3.6565 3.9036 Ave 6.13.6355
15.03.5924
Butyl Methacrylate 1.2020 1.1220 1.2390 1.2626 1.3882 Ave 10.61.5005
15.01.2857
tert-Butylbenzene 2.8468 2.9677 3.4949 3.4946 3.4726 Ave 8.93.3642
15.03.2735
1,2,4-Trimethylbenzene 3.8350 3.2180 3.6764 3.6460 3.9729 Ave 7.43.4518
15.03.6334
2-Octanone 1.1732 1.0771 1.1937 1.0591 1.0825 Ave 5.01.0923
15.01.1130
sec-Butylbenzene 4.7292 4.7248 5.5718 5.5007 5.5211 Ave 13.03.9449
15.04.9987
1,3-Dichlorobenzene 2.2056 1.7788 2.0167 1.9751 2.0327 Ave 6.82.0180
15.02.0045
FORM VI 8260B
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 146 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC/MS VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
VOAMS12
Analy Batch No.: 34969
5832Calibration Start Date: Calibration End Date:04/15/2010 14:24
Y
04/15/2010 16:52
0.18(mm)DB-624 ID:
INTERNAL STANDARD CURVE EVALUTION
ANALYTE RRF
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CURVETYPE
COEFFICIENT
B M1 M2
# %RSD # MAX%RSD
R^2OR COD
# MIN R^2OR COD
MIN RRF
LVL 6
2-Octanol 0.2304 0.1953 0.2458 0.2713 0.2585 Ave 14.40.3007
15.00.2503
1,4-Dichlorobenzene 2.2647 1.9081 2.0168 1.9621 2.0857 Ave 6.22.1240
15.02.0602
p-Isopropyltoluene 3.8704 3.7613 4.5046 4.4095 4.6907 Ave 13.03.3025
15.04.0898
Benzyl chloride 1.2846 1.0362 1.3102 1.4331 1.7114 LinF 0.99851.8267
0.99001.8086
1,2-Dichlorobenzene 2.0775 1.8163 1.8876 1.8001 1.8843 Ave 5.31.8495
15.01.8859
n-Butylbenzene 4.0798 3.8435 4.5477 4.4464 4.6438 Ave 14.13.0968
15.04.1097
1,2-Dibromo-3-Chloropropane 0.2351 0.1691 0.1723 0.1811 0.1894 Ave 13.10.1761
15.00.1872
Camphor 0.1451 0.1046 0.1229 0.1290 0.1077 Ave 12.90.1103
15.00.1199
1,2,4-Trichlorobenzene 1.5255 1.3520 1.4523 1.3933 1.4237 Ave 4.91.3351
15.01.4136
Hexachlorobutadiene 0.7886 0.7609 0.8828 0.8772 0.8562 Ave 6.20.8012
15.00.8278
Naphthalene 3.7939 3.3083 3.5240 3.3931 3.3446 Ave 14.82.3591
15.03.2871
1,2,3-Trichlorobenzene 1.4493 1.3285 1.3312 1.3312 1.3144 Ave 5.21.2311
15.01.3309
1,2-Dichloroethane-d4 (Surr) 0.2481 0.2510 0.2240 0.2169 0.2022 Ave 9.30.2056
15.00.2246
Toluene-d8 (Surr) 1.0332 0.9949 1.0658 1.0999 1.0968 Ave 4.31.1157
15.01.0677
Bromofluorobenzene 0.6140 0.6436 0.6675 0.6346 0.6129 Ave 3.30.6497
15.00.6371
FORM VI 8260B
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 147 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC/MS VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
VOAMS12
Analy Batch No.: 34969
5832Calibration Start Date: Calibration End Date:04/15/2010 14:24
Y
04/15/2010 16:52
GC Column: DB-624 ID: 0.18(mm)
INTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-34969/2 o36292.dLevel 2 IC 460-34969/3 o36294.dLevel 3 ICIS 460-34969/19 o36295.dLevel 4 IC 460-34969/20 o36296.dLevel 5 IC 460-34969/6 o36297.dLevel 6 IC 460-34969/7 o36298.d
ANALYTE CURVETYPE
ISREF
RESPONSE
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CONCENTRATION (UG/L)
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5LVL 6 LVL 6
1-Chloropropane AveCBZ +++++ +++++ +++++ +++++ ++++++++++
+++++ +++++ +++++ +++++ ++++++++++
2-Chloropropane AveFB +++++ +++++ +++++ +++++ ++++++++++
+++++ +++++ +++++ +++++ ++++++++++
Propene AveFB +++++ +++++ +++++ +++++ ++++++++++
+++++ +++++ +++++ +++++ ++++++++++
Dichlorodifluoromethane LinFFB 9829 51094 209388 506957 19808165162135
1.00 5.00 20.0 50.0 200500
Chloromethane LinFFB 13358 63632 271705 662255 27957136903964
1.00 5.00 20.0 50.0 200500
Vinyl chloride LinFFB 11966 60847 260836 650079 27674276851705
1.00 5.00 20.0 50.0 200500
Bromomethane LinFFB 9071 41254 159558 385155 17452934696427
1.00 5.00 20.0 50.0 200500
Chloroethane LinFFB 7827 34561 147753 359969 15955594055833
1.00 5.00 20.0 50.0 200500
Trichlorofluoromethane LinFFB 15590 71397 312150 767854 34073618874740
1.00 5.00 20.0 50.0 200500
n-Pentane AveFB 1424 6387 32359 78006 362390968730
1.00 5.00 20.0 50.0 200500
Ethanol AveFB 38307 98550 142293 197624 275689349834
1000 2000 3000 4000 50006000
Ethyl ether AveFB 5662 27938 110374 283184 14150743696360
1.00 5.00 20.0 50.0 200500
Isopropene AveFB 10157 53707 256913 648374 30535577835552
1.00 5.00 20.0 50.0 200500
Acrolein AveFB 59019 149526 231470 308394 629909781848
100 200 300 400 500600
Freon TF AveFB 8364 40760 173734 438279 19741885270220
1.00 5.00 20.0 50.0 200500
1,1-Dichloroethene AveFB 6467 37786 160155 397935 17077694317065
1.00 5.00 20.0 50.0 200500
FORM VI 8260B 06/03/2010Page 148 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC/MS VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
VOAMS12
Analy Batch No.: 34969
5832Calibration Start Date: Calibration End Date:04/15/2010 14:24
Y
04/15/2010 16:52
GC Column: DB-624 ID: 0.18(mm)
INTERNAL STANDARD RESPONSE AND CONCENTRATION
ANALYTE CURVETYPE
ISREF
RESPONSE
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CONCENTRATION (UG/L)
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5LVL 6 LVL 6
Acetone LinFFB 39351 47775 59779 118448 4463382191135
10.0 15.0 20.0 50.0 2001000
Iodomethane AveFB 7522 41118 179591 457708 22886415607660
1.00 5.00 20.0 50.0 200500
Carbon disulfide AveFB 20948 108150 438107 1117367 611712316630794
1.00 5.00 20.0 50.0 200500
Isopropanol QuaFFB 607480 1113792 1749554 2278520 32541834167051
1000 2000 3000 4000 50006000
Acetonitrile LinFFB 28912 134192 492092 1160085 482225511905866
20.0 100 400 1000 400010000
Methyl acetate LinFFB 2564 10076 43755 106674 4317731109552
1.00 5.00 20.0 50.0 200500
Methylene Chloride LinFFB 12677 43858 183554 440031 20185365088257
1.00 5.00 20.0 50.0 200500
TBA AveFB 16289 72467 322329 730139 36831819907107
20.0 100 400 1000 400010000
Acrylonitrile AveFB 124913 307269 479998 624185 8774371146198
50.0 100 150 200 250300
trans-1,2-Dichloroethene AveFB 8322 39047 180556 436305 20619325301198
1.00 5.00 20.0 50.0 200500
MTBE AveFB 13636 70955 341696 850298 482340312880704
1.00 5.00 20.0 50.0 200500
Hexane AveFB 4917 24105 123471 344172 15912144471278
1.00 5.00 20.0 50.0 200500
1,1-Dichloroethane AveFB 14475 65799 303680 748689 35236609022002
1.00 5.00 20.0 50.0 200500
Vinyl acetate AveFB 12875 65052 292196 825367 499389613405213
1.00 5.00 20.0 50.0 200500
DIPE AveFB 16747 85364 404838 1038836 565594115260277
1.00 5.00 20.0 50.0 200500
Tert-butyl ethyl ether AveFB 14581 72855 342469 897352 505802813814023
1.00 5.00 20.0 50.0 200500
2,2-Dichloropropane AveFB 7917 41430 213438 558153 26972996940846
1.00 5.00 20.0 50.0 200500
cis-1,2-Dichloroethene AveFB 8012 40310 173250 426651 20760355343818
1.00 5.00 20.0 50.0 200500
2-Butanone (MEK) AveFB 7281 12096 18549 40377 2076681009784
10.0 15.0 20.0 50.0 2001000
Ethyl acetate AveFB 1244 5268 24213 61001 318096850152
2.00 10.0 40.0 100 4001000
Bromochloromethane AveFB 3306 16505 70511 172015 8368402115548
1.00 5.00 20.0 50.0 200500
FORM VI 8260B 06/03/2010Page 149 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC/MS VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
VOAMS12
Analy Batch No.: 34969
5832Calibration Start Date: Calibration End Date:04/15/2010 14:24
Y
04/15/2010 16:52
GC Column: DB-624 ID: 0.18(mm)
INTERNAL STANDARD RESPONSE AND CONCENTRATION
ANALYTE CURVETYPE
ISREF
RESPONSE
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CONCENTRATION (UG/L)
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5LVL 6 LVL 6
Chloroform AveFB 13266 60420 271900 664487 32370828541410
1.00 5.00 20.0 50.0 200500
1,1,1-Trichloroethane AveFB 9415 45699 229638 587888 28459317373424
1.00 5.00 20.0 50.0 200500
Cyclohexane AveFB 13068 68390 308504 777281 36287769820423
1.00 5.00 20.0 50.0 200500
Carbon tetrachloride AveFB 7086 35128 185522 478191 24396586405906
1.00 5.00 20.0 50.0 200500
1,1-Dichloropropene AveFB 7854 40700 215002 554490 28421917179727
1.00 5.00 20.0 50.0 200500
Benzene AveFB 26047 123328 632459 1580850 812180918688215
1.00 5.00 20.0 50.0 200500
1,2-Dichloroethane AveFB 9163 41087 176271 438030 22205455824849
1.00 5.00 20.0 50.0 200500
Isopropyl acetate AveFB 18542 92236 440643 1142906 667003118380366
2.00 10.0 40.0 100 4001000
Tert-amyl methyl ether AveFB 13847 65690 296423 756316 452019312567064
1.00 5.00 20.0 50.0 200500
2,4,4-Trimethyl-1-pentene LinFFB 2880 14973 56393 123454 7263291778966
1.00 5.00 20.0 50.0 200500
n-Butanol AveFB 50719 100546 163835 229028 433389+++++
500 1000 1500 2000 2500+++++
Trichloroethene AveFB 6984 28668 157706 395065 20335265200531
1.00 5.00 20.0 50.0 200500
Ethyl acrylate AveFB 5054 31305 133126 327562 19841185863032
1.00 5.00 20.0 50.0 200500
Methylcyclohexane AveFB 12506 59982 276571 759186 389657610569957
1.00 5.00 20.0 50.0 200500
1,2-Dichloropropane AveFB 5931 30886 154070 383264 20584975299536
1.00 5.00 20.0 50.0 200500
Dibromomethane AveFB 4103 17950 81516 189900 9963672492277
1.00 5.00 20.0 50.0 200500
Methyl methacrylate LinFFB 4177 17107 68043 174550 10384152804649
1.00 5.00 20.0 50.0 200500
1,4-Dioxane AveFB 95558 194311 311068 430938 587679751736
1000 2000 3000 4000 50006000
Propyl acetate LinFFB 23248 80944 311765 733128 413153211229348
2.00 10.0 40.0 100 4001000
Bromodichloromethane AveFB 6814 34281 167023 430487 24106556324586
1.00 5.00 20.0 50.0 200500
2-Chloroethyl vinyl ether AveFB 2685 13317 69580 173060 10047082689127
1.00 5.00 20.0 50.0 200500
FORM VI 8260B 06/03/2010Page 150 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC/MS VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
VOAMS12
Analy Batch No.: 34969
5832Calibration Start Date: Calibration End Date:04/15/2010 14:24
Y
04/15/2010 16:52
GC Column: DB-624 ID: 0.18(mm)
INTERNAL STANDARD RESPONSE AND CONCENTRATION
ANALYTE CURVETYPE
ISREF
RESPONSE
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CONCENTRATION (UG/L)
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5LVL 6 LVL 6
Epichlorohydrin AveFB 12794 62116 277498 709199 34753469034273
20.0 100 400 1000 400010000
cis-1,3-Dichloropropene AveFB 7489 36479 195348 521566 29692157838898
1.00 5.00 20.0 50.0 200500
4-Methyl-2-pentanone AveFB 48901 87506 100225 232775 13502757579276
10.0 15.0 20.0 50.0 2001000
Toluene AveCBZ 35372 169702 653762 1476565 827436719110155
1.00 5.00 20.0 50.0 200500
trans-1,3-Dichloropropene LinFCBZ 5701 29332 152245 414159 25481866883355
1.00 5.00 20.0 50.0 200500
1,1,2-Trichloroethane LinFCBZ 3914 18939 87997 224539 12562863317800
1.00 5.00 20.0 50.0 200500
Tetrachloroethene AveCBZ 7013 30765 146217 350365 18884034981279
1.00 5.00 20.0 50.0 200500
1,3-Dichloropropane LinFCBZ 7884 41392 195511 480075 26892197031925
1.00 5.00 20.0 50.0 200500
2-Hexanone AveCBZ 39000 74898 84694 170489 9540335507288
10.0 15.0 20.0 50.0 2001000
Dibromochloromethane LinFCBZ 4409 19824 94435 252590 15560834289334
1.00 5.00 20.0 50.0 200500
Butyl acetate AveCBZ 17457 95060 353843 773295 431534112396122
2.00 10.0 40.0 100 4001000
1,2-Dibromoethane LinFCBZ 4707 20839 102404 252470 14381853748152
1.00 5.00 20.0 50.0 200500
Chlorobenzene AveCBZ 19484 99759 391122 883565 492042813491058
1.00 5.00 20.0 50.0 200500
1,1,1,2-Tetrachloroethane LinFCBZ 4301 20949 98481 267402 16421794574855
1.00 5.00 20.0 50.0 200500
Ethylbenzene AveCBZ 11165 58368 249628 544539 27908627622609
1.00 5.00 20.0 50.0 200500
m&p-Xylene AveCBZ 27357 137315 574126 1419678 699687518471786
2.00 10.0 40.0 100 4001000
o-Xylene AveCBZ 11912 60960 264498 651941 33005128864989
1.00 5.00 20.0 50.0 200500
Styrene AveCBZ 19210 108506 459380 1126968 579281615613202
1.00 5.00 20.0 50.0 200500
Butyl acrylate AveDCB 11389 56933 233518 610553 31154079103920
1.00 5.00 20.0 50.0 200500
Bromoform LinFCBZ 2130 10756 53806 143454 9364692583583
1.00 5.00 20.0 50.0 200500
Amly acetate AveCBZ 6299 26904 105586 266112 13083853753042
1.00 5.00 20.0 50.0 200500
FORM VI 8260B 06/03/2010Page 151 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC/MS VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
VOAMS12
Analy Batch No.: 34969
5832Calibration Start Date: Calibration End Date:04/15/2010 14:24
Y
04/15/2010 16:52
GC Column: DB-624 ID: 0.18(mm)
INTERNAL STANDARD RESPONSE AND CONCENTRATION
ANALYTE CURVETYPE
ISREF
RESPONSE
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CONCENTRATION (UG/L)
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5LVL 6 LVL 6
Isopropylbenzene AveCBZ 33753 178564 752969 1835860 8836094+++++
1.00 5.00 20.0 50.0 200+++++
Camphene, Total AveDCB 18577 87150 348075 829962 388182911265636
1.00 5.00 20.0 50.0 200500
Monobromobenzene AveDCB 7872 40040 161302 380811 19493385186993
1.00 5.00 20.0 50.0 200500
1,1,2,2-Tetrachloroethane AveDCB 6928 36609 138101 330226 19341665119877
1.00 5.00 20.0 50.0 200500
1,2,3-Trichloropropane AveDCB 2258 10239 39196 94478 5352431370300
1.00 5.00 20.0 50.0 200500
trans-1,4-Dichloro-2-butene LinFFB 2337 10349 37887 97438 5449651506749
1.00 5.00 20.0 50.0 200500
N-Propylbenzene AveDCB 45159 228351 981644 2424606 1212370324298694
1.00 5.00 20.0 50.0 200500
2-Chlorotoluene AveDCB 24623 131044 516934 1281161 655983017172189
1.00 5.00 20.0 50.0 200500
4-Chlorotoluene AveDCB 28494 142158 598938 1442568 694807017942950
1.00 5.00 20.0 50.0 200500
1,3,5-Trimethylbenzene AveDCB 28504 147405 599323 1481917 793181119490914
1.00 5.00 20.0 50.0 200500
Butyl Methacrylate AveDCB 9929 50780 203371 511721 28207928044647
1.00 5.00 20.0 50.0 200500
tert-Butylbenzene AveDCB 23516 134310 573676 1416333 705616818036505
1.00 5.00 20.0 50.0 200500
1,2,4-Trimethylbenzene AveDCB 31679 145642 603459 1477665 807272818506249
1.00 5.00 20.0 50.0 200500
2-Octanone AveDCB 9691 48748 195932 429220 21996455855978
1.00 5.00 20.0 50.0 200500
sec-Butylbenzene AveDCB 39065 213837 914577 2229359 1121849821149703
1.00 5.00 20.0 50.0 200500
1,3-Dichlorobenzene AveDCB 18219 80505 331029 800495 413024510819131
1.00 5.00 20.0 50.0 200500
2-Octanol AveDCB 1903 8840 40343 109959 5252051612316
1.00 5.00 20.0 50.0 200500
1,4-Dichlorobenzene AveDCB 18707 86359 331056 795221 423799311387121
1.00 5.00 20.0 50.0 200500
p-Isopropyltoluene AveDCB 31971 170228 739407 1787116 953128917705621
1.00 5.00 20.0 50.0 200500
Benzyl chloride LinFDCB 10611 46895 215067 580809 34774279793596
1.00 5.00 20.0 50.0 200500
1,2-Dichlorobenzene AveDCB 17161 82204 309841 729557 38287579915717
1.00 5.00 20.0 50.0 200500
FORM VI 8260B 06/03/2010Page 152 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC/MS VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
VOAMS12
Analy Batch No.: 34969
5832Calibration Start Date: Calibration End Date:04/15/2010 14:24
Y
04/15/2010 16:52
GC Column: DB-624 ID: 0.18(mm)
INTERNAL STANDARD RESPONSE AND CONCENTRATION
ANALYTE CURVETYPE
ISREF
RESPONSE
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CONCENTRATION (UG/L)
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5LVL 6 LVL 6
n-Butylbenzene AveDCB 33701 173948 746484 1802086 943599716602685
1.00 5.00 20.0 50.0 200500
1,2-Dibromo-3-Chloropropane AveDCB 1942 7653 28277 73411 384903944195
1.00 5.00 20.0 50.0 200500
Camphor AveDCB 5993 23678 100851 261323 10946122957724
5.00 25.0 100 250 10002500
1,2,4-Trichlorobenzene AveDCB 12601 61188 238386 564686 28929087158001
1.00 5.00 20.0 50.0 200500
Hexachlorobutadiene AveDCB 6514 34437 144905 355509 17396844295340
1.00 5.00 20.0 50.0 200500
Naphthalene AveDCB 31339 149725 578445 1375171 679593912647892
1.00 5.00 20.0 50.0 200500
1,2,3-Trichlorobenzene AveDCB 11972 60124 218509 539501 26708096600362
1.00 5.00 20.0 50.0 200500
1,2-Dichloroethane-d4 (Surr) AveFB 224919 245158 248478 244690 295209319383
50.0 50.0 50.0 50.0 50.050.0
Toluene-d8 (Surr) AveCBZ 793858 886156 818959 749412 10216651171616
50.0 50.0 50.0 50.0 50.050.0
Bromofluorobenzene AveDCB 253605 291292 273931 257206 311348348336
50.0 50.0 50.0 50.0 50.050.0
Curve Type Legend:Ave = Average ISTDLinF = Linear ISTD forced zeroQuaF = Quadratic ISTD forced zero
FORM VI 8260B 06/03/2010Page 153 of 623
FORM VII
Lab Name: Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC/MS VOA CONTINUING CALIBRATION DATA
0.18(mm)
460-13139-1
VOAMS12
05/17/2010 17:02
04/15/2010 14:24
04/15/2010 16:52
CCVIS 460-37643/2
DB-624
TestAmerica Edison
Lab File ID: o37385.d Heated Purge: (Y/N) YConc. Units: ug/L
ANALYTE CURVE AVE RRF RRF MIN RRF CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
Dichlorodifluoromethane LinF 0.41800.4430 25.0 20.0 24.8 50.0
Chloromethane LinF 0.48360.5852 0.1000 21.4 20.0 7.1 50.0
Vinyl chloride LinF 0.47800.5604 21.4 20.0 6.8 20.0
Bromomethane LinF 0.37510.3708 24.8 20.0 24.0 50.0
Chloroethane LinF 0.28350.3287 21.5 20.0 7.5 50.0
Trichlorofluoromethane LinF 0.65520.6883 22.8 20.0 14.1 50.0
n-Pentane Ave 0.07170.0684 20.9 20.0 4.7 50.0
Ethanol Ave 0.00180.0021 2500 3000 -16.6 50.0
Ethyl ether Ave 0.23550.2631 17.9 20.0 -10.5 50.0
Isopropene Ave 0.52120.5485 19.0 20.0 -5.0 50.0
Acrolein Ave 0.02350.0375 188 300 -37.4 99.0
1,1-Dichloroethene Ave 0.33320.3379 19.7 20.0 -1.4 20.0
Freon TF Ave 0.40410.3893 20.8 20.0 3.8 50.0
Acetone LinF 0.07800.1278 22.0 20.0 9.8 50.0
Iodomethane Ave 0.42010.3999 21.0 20.0 5.1 50.0
Carbon disulfide Ave 1.0841.060 20.5 20.0 2.3 50.0
Isopropanol QuaF 0.01920.0264 2030 3000 -32.5 50.0
Acetonitrile LinF 0.03930.0558 404 400 0.9 50.0
Methyl acetate LinF 0.06270.0972 17.4 20.0 -13.1 50.0
Methylene Chloride LinF 0.37850.4375 22.9 20.0 14.3 50.0
TBA Ave 0.02740.0357 307 400 -23.3 50.0
Acrylonitrile Ave 0.11640.1368 128 150 -14.9 50.0
trans-1,2-Dichloroethene Ave 0.37090.3911 19.0 20.0 -5.2 50.0
MTBE Ave 0.66530.7763 17.1 20.0 -14.3 50.0
Hexane Ave 0.23940.2770 17.3 20.0 -13.6 50.0
1,1-Dichloroethane Ave 0.61940.6674 0.1000 18.6 20.0 -7.2 50.0
Vinyl acetate Ave 0.58000.7474 15.5 20.0 -22.4 50.0
DIPE Ave 0.80570.9303 17.3 20.0 -13.4 50.0
Tert-butyl ethyl ether Ave 0.66770.8122 0.0100 16.4 20.0 -17.8 50.0
2,2-Dichloropropane Ave 0.46630.4576 20.4 20.0 1.9 50.0
cis-1,2-Dichloroethene Ave 0.37420.3871 19.3 20.0 -3.4 50.0
2-Butanone (MEK) Ave 0.03720.0379 19.6 20.0 -1.7 50.0
Ethyl acetate Ave 0.02090.0284 29.5 40.0 -26.3 50.0
Bromochloromethane Ave 0.15780.1570 20.1 20.0 0.5 50.0
Chloroform Ave 0.59640.6094 19.6 20.0 -2.1 20.0
1,1,1-Trichloroethane Ave 0.48570.4980 19.5 20.0 -2.5 50.0
Cyclohexane Ave 0.62250.6765 18.4 20.0 -8.0 50.0
1,1-Dichloropropene Ave 0.42070.4625 18.2 20.0 -9.0 50.0
Carbon tetrachloride Ave 0.41010.4038 20.3 20.0 1.6 50.0
Benzene Ave 1.2271.353 18.1 20.0 -9.3 50.0
1,2-Dichloroethane Ave 0.38750.4112 18.9 20.0 -5.7 50.0
FORM VII 8260B
06/03/2010Page 154 of 623
FORM VII
Lab Name: Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC/MS VOA CONTINUING CALIBRATION DATA
0.18(mm)
460-13139-1
VOAMS12
05/17/2010 17:02
04/15/2010 14:24
04/15/2010 16:52
CCVIS 460-37643/2
DB-624
TestAmerica Edison
Lab File ID: o37385.d Heated Purge: (Y/N) YConc. Units: ug/L
ANALYTE CURVE AVE RRF RRF MIN RRF CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
Isopropyl acetate Ave 0.40850.5249 31.1 40.0 -22.2 50.0
Tert-amyl methyl ether Ave 0.53480.7263 14.7 20.0 -26.4 50.0
2,4,4-Trimethyl-1-pentene LinF 0.11040.1313 19.0 20.0 -4.8 50.0
n-Butanol Ave 0.00340.0053 950 1500 -36.7 50.0
Trichloroethene Ave 0.29620.3446 17.2 20.0 -14.0 50.0
Ethyl acrylate Ave 0.24840.3178 15.6 20.0 -21.9 50.0
Methylcyclohexane Ave 0.51820.6580 15.8 20.0 -21.2 50.0
1,2-Dichloropropane Ave 0.29020.3373 17.2 20.0 -14.0 20.0
Dibromomethane Ave 0.17910.1822 19.7 20.0 -1.7 50.0
1,4-Dioxane Ave 0.00360.0046 2360 3000 -21.3 50.0
Methyl methacrylate LinF 0.12180.1787 13.5 20.0 -32.3 50.0
Propyl acetate LinF 0.27590.4078 30.6 40.0 -23.4 50.0
Bromodichloromethane Ave 0.37080.3841 19.3 20.0 -3.5 50.0
2-Chloroethyl vinyl ether Ave 0.12090.1566 15.4 20.0 -22.8 50.0
Epichlorohydrin Ave 0.02650.0314 337 400 -15.7 50.0
cis-1,3-Dichloropropene Ave 0.39650.4504 17.6 20.0 -12.0 50.0
4-Methyl-2-pentanone Ave 0.18510.2460 15.0 20.0 -24.8 50.0
Toluene Ave 1.7372.090 16.6 20.0 -16.9 20.0
trans-1,3-Dichloropropene LinF 0.42640.5238 12.9 20.0 -35.3 50.0
1,1,2-Trichloroethane LinF 0.24440.2894 15.3 20.0 -23.4 50.0
Tetrachloroethene Ave 0.36340.4622 15.7 20.0 -21.4 50.0
1,3-Dichloropropane LinF 0.53000.6183 15.6 20.0 -21.8 50.0
2-Hexanone Ave 0.21450.2630 16.3 20.0 -18.5 50.0
Dibromochloromethane LinF 0.29310.3356 14.3 20.0 -28.4 50.0
Butyl acetate Ave 0.49720.5690 35.0 40.0 -12.6 50.0
1,2-Dibromoethane LinF 0.29370.3312 16.3 20.0 -18.7 50.0
Chlorobenzene Ave 1.1681.260 0.3000 18.5 20.0 -7.4 50.0
1,1,1,2-Tetrachloroethane LinF 0.28210.3507 12.9 20.0 -35.3 50.0
Ethylbenzene Ave 0.72790.7447 19.6 20.0 -2.2 20.0
m&p-Xylene Ave 0.87690.9092 38.6 40.0 -3.5 50.0
o-Xylene Ave 0.81620.8345 19.6 20.0 -2.2 50.0
Styrene Ave 1.4011.443 19.4 20.0 -2.9 50.0
Butyl acrylate Ave 1.2691.466 17.3 20.0 -13.4 50.0
Bromoform LinF 0.16450.1904 0.1000 13.4 20.0 -33.2 50.0
Amly acetate Ave 0.55200.3591 30.7 20.0 53.7* 50.0
Isopropylbenzene Ave 2.2832.343 19.5 20.0 -2.6 50.0
Camphene, Total Ave 1.9722.059 19.2 20.0 -4.2 50.0
Monobromobenzene Ave 0.94120.9478 19.9 20.0 -0.7 50.0
1,1,2,2-Tetrachloroethane Ave 0.72320.8684 0.3000 16.7 20.0 -16.7 50.0
1,2,3-Trichloropropane Ave 0.20330.2484 16.4 20.0 -18.2 50.0
trans-1,4-Dichloro-2-butene LinF 0.07820.0995 16.2 20.0 -18.9 50.0
FORM VII 8260B
06/03/2010Page 155 of 623
FORM VII
Lab Name: Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC/MS VOA CONTINUING CALIBRATION DATA
0.18(mm)
460-13139-1
VOAMS12
05/17/2010 17:02
04/15/2010 14:24
04/15/2010 16:52
CCVIS 460-37643/2
DB-624
TestAmerica Edison
Lab File ID: o37385.d Heated Purge: (Y/N) YConc. Units: ug/L
ANALYTE CURVE AVE RRF RRF MIN RRF CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
N-Propylbenzene Ave 5.4005.496 19.7 20.0 -1.7 50.0
2-Chlorotoluene Ave 2.9613.103 19.1 20.0 -4.6 50.0
4-Chlorotoluene Ave 3.3363.427 19.5 20.0 -2.7 50.0
1,3,5-Trimethylbenzene Ave 3.2513.592 18.1 20.0 -9.5 50.0
Butyl Methacrylate Ave 1.1141.286 17.3 20.0 -13.4 50.0
tert-Butylbenzene Ave 3.1293.273 19.1 20.0 -4.4 50.0
1,2,4-Trimethylbenzene Ave 3.3353.633 18.4 20.0 -8.2 50.0
2-Octanone Ave 0.87981.113 15.8 20.0 -21.0 50.0
sec-Butylbenzene Ave 4.9924.999 20.0 20.0 -0.1 50.0
1,3-Dichlorobenzene Ave 1.8752.004 18.7 20.0 -6.5 50.0
2-Octanol Ave 0.15030.2503 12.0 20.0 -40.0 50.0
1,4-Dichlorobenzene Ave 1.9352.060 18.8 20.0 -6.1 50.0
p-Isopropyltoluene Ave 3.9804.090 19.5 20.0 -2.7 50.0
Benzyl chloride LinF 1.3721.434 15.2 20.0 -24.1 50.0
1,2-Dichlorobenzene Ave 1.7731.886 18.8 20.0 -6.0 50.0
n-Butylbenzene Ave 4.0244.110 19.6 20.0 -2.1 50.0
1,2-Dibromo-3-Chloropropane Ave 0.14400.1872 15.4 20.0 -23.1 50.0
Camphor Ave 0.08880.1199 74.0 100 -26.0 50.0
1,2,4-Trichlorobenzene Ave 1.4201.414 20.1 20.0 0.5 50.0
Hexachlorobutadiene Ave 0.80380.8278 19.4 20.0 -2.9 50.0
Naphthalene Ave 3.1203.287 19.0 20.0 -5.1 50.0
1,2,3-Trichlorobenzene Ave 1.2891.331 19.4 20.0 -3.1 50.0
1,2-Dichloroethane-d4 (Surr) Ave 0.21560.2246 48.0 50.0 -4.0 50.0
Toluene-d8 (Surr) Ave 0.94631.068 44.3 50.0 -11.4 50.0
Bromofluorobenzene Ave 0.69300.6371 54.4 50.0 8.8 50.0
FORM VII 8260B
06/03/2010Page 156 of 623
Data File: /chem/VOAMS12.i/8260L_10/04-15-10/15apr10.b/o36289.d Report Date: 15-Apr-2010 13:20
TestAmerica
Data file : /chem/VOAMS12.i/8260L_10/04-15-10/15apr10.b/o36289.dLab Smp Id: BFB-VMBFB Inj Date : 15-APR-2010 13:12 Operator : VOAMS 1 Inst ID: VOAMS12.iSmp Info : BFB-VMBFBMisc Info : Comment : Method : /chem/VOAMS12.i/8260L_10/04-15-10/15apr10.b/VOABFB.mMeth Date : 24-Feb-2010 18:04 ken Quant Type: ISTDCal Date : Cal File: Als bottle: 2 QC Sample: BFBDil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Sample Matrix: WATERProcessing Host: hpd2
Concentration Formula: Amt * DF * Uf * Vf * VI * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorUf 1.00000 ng unit correction factorVf 1.00000 Volumetric correction factorVI 1.00000 Injection Volume
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT (REL RT) MASS RESPONSE ( ug/L) ( ug/L) TARGET RANGE RATIO
== ====== ======== ==== ======== ======= ======= ============ =====
1 BFB CAS #: 460-00-4
2.700 2.700 (0.000) 95 84592 0.00- 100.00 100.00
2.700 2.700 (0.000) 50 13379 15.00- 40.00 15.82
2.700 2.700 (0.000) 75 40224 30.00- 60.00 47.55
2.700 2.700 (0.000) 96 5536 5.00- 9.00 6.54
2.700 2.700 (0.000) 173 0 0.00- 2.00 0.00
2.700 2.700 (0.000) 174 62952 50.00- 100.00 74.42
2.700 2.700 (0.000) 175 5162 5.00- 9.00 8.20
2.700 2.700 (0.000) 176 62464 95.00- 101.00 99.22
2.700 2.700 (0.000) 177 4244 5.00- 9.00 6.79
-------------------------------------------------------------------------------
06/03/2010Page 157 of 623
Data File: o36289.d
Date: 15-APR-2010 13:12
Client ID: Instrument: VOAMS12.i
Sample Info: BFB-VMBFB Operator: VOAMS 1
06/03/2010Page 158 of 623
Data File: o36289.d
Date: 15-APR-2010 13:12
Client ID: Instrument: VOAMS12.i
Sample Info: BFB-VMBFB Operator: VOAMS 1
1 BFB
% RELATIVE m/e ION ABUNDANCE CRITERIA ABUNDANCE
+-----+------------------------------------------+---------------------+| | | || 95 | Base Peak, 100% relative abundance | 100.00 || 50 | 15.00 - 40.00% of mass 95 | 15.82 || 75 | 30.00 - 60.00% of mass 95 | 47.55 || 96 | 5.00 - 9.00% of mass 95 | 6.54 || 173 | Less than 2.00% of mass 174 | 0.00 ( 0.00) || 174 | 50.00 - 100.00% of mass 95 | 74.42 || 175 | 5.00 - 9.00% of mass 174 | 6.10 ( 8.20) || 176 | 95.00 - 101.00% of mass 174 | 73.84 ( 99.22) || 177 | 5.00 - 9.00% of mass 176 | 5.02 ( 6.79) |+-----+------------------------------------------+---------------------+
06/03/2010Page 159 of 623
Data File: o36289.d
Date: 15-APR-2010 13:12
Client ID: Instrument: VOAMS12.i
Sample Info: BFB-VMBFB Operator: VOAMS 1
Data File: /chem/VOAMS12.i/8260L_10/04-15-10/15apr10.b/o36289.dSpectrum: Avg. Scans 101-103 ( 2.70), Background Scan 95
Location of Maximum: 95.00Number of points: 114
m/z Y m/z Y m/z Y m/z Y+------------------+------------------+------------------+------------------+| 36.00 736 | 70.00 557 | 109.00 124 | 149.00 118 || 37.00 3445 | 72.00 728 | 110.00 73 | 150.00 155 || 38.00 3000 | 73.00 3066 | 111.00 134 | 152.00 43 || 39.00 1397 | 74.00 12308 | 113.00 44 | 155.00 118 || 40.00 53 | 75.00 40224 | 114.00 36 | 157.00 118 |+------------------+------------------+------------------+------------------+| 41.00 36 | 76.00 3465 | 115.00 125 | 158.00 66 || 43.00 179 | 77.00 698 | 116.00 187 | 159.00 44 || 44.00 345 | 78.00 448 | 117.00 502 | 171.00 60 || 45.00 613 | 79.00 1486 | 118.00 350 | 172.00 305 || 47.00 1041 | 80.00 447 | 119.00 377 | 174.00 62952 |+------------------+------------------+------------------+------------------+| 48.00 406 | 81.00 1625 | 121.00 61 | 175.00 5162 || 49.00 3190 | 82.00 448 | 123.00 34 | 176.00 62464 || 50.00 13379 | 83.00 37 | 125.00 52 | 177.00 4244 || 51.00 4498 | 85.00 37 | 126.00 84 | 178.00 172 || 52.00 299 | 86.00 118 | 128.00 254 | 182.00 82 |+------------------+------------------+------------------+------------------+| 53.00 37 | 87.00 3555 | 129.00 219 | 186.00 44 || 55.00 348 | 88.00 2888 | 130.00 265 | 191.00 46 || 56.00 1150 | 89.00 64 | 131.00 37 | 192.00 49 || 57.00 1781 | 91.00 187 | 134.00 156 | 193.00 62 || 58.00 33 | 92.00 2154 | 136.00 37 | 207.00 46 |+------------------+------------------+------------------+------------------+| 59.00 97 | 93.00 3190 | 137.00 40 | 208.00 41 || 60.00 516 | 94.00 8659 | 141.00 570 | 232.00 43 || 61.00 3467 | 95.00 84592 | 142.00 49 | 241.00 42 || 62.00 3370 | 96.00 5536 | 143.00 628 | 253.00 82 || 63.00 2925 | 97.00 214 | 144.00 38 | 258.00 40 |+------------------+------------------+------------------+------------------+| 64.00 357 | 104.00 199 | 145.00 58 | 280.00 34 || 67.00 458 | 105.00 172 | 146.00 47 | 281.00 90 || 68.00 7550 | 106.00 219 | 147.00 106 | || 69.00 8092 | 107.00 56 | 148.00 108 | |+------------------+------------------+------------------+------------------+
06/03/2010Page 160 of 623
Data File: /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37384.dReport Date: 17-May-2010 17:56
TestAmerica
Data file : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37384.dLab Smp Id: BFB-VMBFB Inj Date : 17-MAY-2010 16:42 Operator : VOAMS 1 Inst ID: VOAMS12.iSmp Info : BFB-VMBFBMisc Info : Comment : Method : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/VOABFB.mMeth Date : 24-Feb-2010 18:04 ken Quant Type: ISTDCal Date : Cal File: Als bottle: 2 QC Sample: BFBDil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Sample Matrix: WATERProcessing Host: hpd2
Concentration Formula: Amt * DF * Uf * Vf * VI * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorUf 1.00000 ng unit correction factorVf 1.00000 Volumetric correction factorVI 1.00000 Injection Volume
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT (REL RT) MASS RESPONSE ( ug/L) ( ug/L) TARGET RANGE RATIO
== ====== ======== ==== ======== ======= ======= ============ =====
1 BFB CAS #: 460-00-4
2.688 2.700 (0.000) 95 177984 0.00- 100.00 100.00
2.688 2.700 (0.000) 50 28472 15.00- 40.00 16.00
2.688 2.700 (0.000) 75 87240 30.00- 60.00 49.02
2.688 2.700 (0.000) 96 11563 5.00- 9.00 6.50
2.688 2.700 (0.000) 173 1134 0.00- 2.00 0.93
2.688 2.700 (0.000) 174 122192 50.00- 100.00 68.65
2.688 2.700 (0.000) 175 9308 5.00- 9.00 7.62
2.688 2.700 (0.000) 176 117512 95.00- 101.00 96.17
2.688 2.700 (0.000) 177 6472 5.00- 9.00 5.51
-------------------------------------------------------------------------------
06/03/2010Page 161 of 623
Data File: o37384.d
Date: 17-MAY-2010 16:42
Client ID: Instrument: VOAMS12.i
Sample Info: BFB-VMBFB Operator: VOAMS 1
06/03/2010Page 162 of 623
Data File: o37384.d
Date: 17-MAY-2010 16:42
Client ID: Instrument: VOAMS12.i
Sample Info: BFB-VMBFB Operator: VOAMS 1
1 BFB
% RELATIVE m/e ION ABUNDANCE CRITERIA ABUNDANCE
+-----+------------------------------------------+---------------------+| | | || 95 | Base Peak, 100% relative abundance | 100.00 || 50 | 15.00 - 40.00% of mass 95 | 16.00 || 75 | 30.00 - 60.00% of mass 95 | 49.02 || 96 | 5.00 - 9.00% of mass 95 | 6.50 || 173 | Less than 2.00% of mass 174 | 0.64 ( 0.93) || 174 | 50.00 - 100.00% of mass 95 | 68.65 || 175 | 5.00 - 9.00% of mass 174 | 5.23 ( 7.62) || 176 | 95.00 - 101.00% of mass 174 | 66.02 ( 96.17) || 177 | 5.00 - 9.00% of mass 176 | 3.64 ( 5.51) |+-----+------------------------------------------+---------------------+
06/03/2010Page 163 of 623
Data File: o37384.d
Date: 17-MAY-2010 16:42
Client ID: Instrument: VOAMS12.i
Sample Info: BFB-VMBFB Operator: VOAMS 1
Data File: /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37384.dSpectrum: HP MS o37384.d, Scan 100: 2.688 min.
Location of Maximum: 95.00Number of points: 134
m/z Y m/z Y m/z Y m/z Y+------------------+------------------+------------------+------------------+| 36.10 1183 | 71.90 685 | 111.70 258 | 155.80 121 || 37.00 6748 | 73.00 6936 | 112.60 142 | 156.90 521 || 37.90 5948 | 74.00 28936 | 114.60 174 | 159.40 260 || 39.00 2292 | 75.00 87240 | 115.10 126 | 160.90 349 || 39.80 286 | 76.00 7153 | 115.80 549 | 169.40 287 |+------------------+------------------+------------------+------------------+| 43.30 431 | 76.70 1061 | 116.80 1311 | 170.10 246 || 44.10 953 | 77.10 900 | 117.80 598 | 170.50 285 || 44.70 669 | 77.90 381 | 118.90 869 | 171.00 200 || 45.10 872 | 78.80 4831 | 119.70 169 | 171.70 408 || 46.20 198 | 80.00 1427 | 124.60 402 | 172.70 1134 |+------------------+------------------+------------------+------------------+| 47.00 1409 | 80.80 4094 | 126.00 146 | 173.90 122192 || 48.00 788 | 81.90 840 | 127.20 179 | 174.90 9308 || 49.00 6150 | 82.90 272 | 128.10 610 | 175.90 117512 || 50.00 28472 | 86.10 317 | 128.80 106 | 177.00 6472 || 51.00 10415 | 87.00 8860 | 129.90 793 | 178.00 563 |+------------------+------------------+------------------+------------------+| 52.00 280 | 88.00 8092 | 130.80 544 | 204.30 177 || 55.00 706 | 89.00 105 | 133.70 173 | 207.10 109 || 55.90 2362 | 90.40 629 | 134.70 215 | 209.00 159 || 57.00 4501 | 90.90 624 | 135.80 155 | 218.20 120 || 57.70 138 | 91.90 5401 | 139.20 239 | 230.70 160 |+------------------+------------------+------------------+------------------+| 58.20 122 | 93.00 7018 | 139.70 234 | 231.90 103 || 58.90 145 | 94.00 19008 | 140.80 1482 | 252.40 167 || 60.00 1563 | 95.00 177984 | 141.80 211 | 266.10 139 || 60.90 7246 | 96.00 11563 | 142.70 1970 | 267.20 136 || 62.00 7224 | 96.80 601 | 144.00 196 | 270.80 110 |+------------------+------------------+------------------+------------------+| 63.00 6053 | 100.10 128 | 145.00 317 | 274.80 155 || 64.00 607 | 102.90 280 | 145.70 253 | 277.70 129 || 64.70 223 | 103.80 966 | 146.80 125 | 280.80 168 || 66.50 320 | 105.20 140 | 147.80 624 | 281.20 104 || 68.00 15623 | 105.80 521 | 148.40 236 | 282.30 102 |+------------------+------------------+------------------+------------------+| 69.00 13446 | 106.40 140 | 149.10 210 | 294.80 175 || 70.00 2010 | 106.80 249 | 152.50 113 | 299.60 134 || 70.70 183 | 109.80 104 | 153.70 217 | || 71.10 156 | 111.00 148 | 154.80 610 | |+------------------+------------------+------------------+------------------+
06/03/2010Page 164 of 623
FORM IForm 1GC/MS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: MB 460-37643/5
Matrix: o37390.dLab File ID:
Date Collected:8260BAnalysis Method:
Solid
TestAmerica Edison
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol: 1
Level: (low/med) Low
5(mL)
0.18(mm)
Date Analyzed: 05/17/2010 20:11
ID:DB-624
Analysis Batch No.: 37643 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Chloromethane74-87-3 1.0 1.0 0.63U
Bromomethane74-83-9 1.0 1.0 0.41U
Vinyl chloride75-01-4 1.0 1.0 0.23U
Chloroethane75-00-3 1.0 1.0 0.40U
Methylene Chloride75-09-2 1.0 1.0 0.47U
Trichlorofluoromethane75-69-4 1.0 1.0 0.26U
1,1-Dichloroethene75-35-4 1.0 1.0 0.37U
1,1-Dichloroethane75-34-3 1.0 1.0 0.25U
trans-1,2-Dichloroethene156-60-5 1.0 1.0 0.28U
cis-1,2-Dichloroethene156-59-2 1.0 1.0 0.24U
Chloroform67-66-3 1.0 1.0 0.24U
1,2-Dichloroethane107-06-2 1.0 1.0 0.39U
1,1,1-Trichloroethane71-55-6 1.0 1.0 0.19U
Carbon tetrachloride56-23-5 1.0 1.0 0.10U
Bromodichloromethane75-27-4 1.0 1.0 0.30U
1,2-Dichloropropane78-87-5 1.0 1.0 0.32U
cis-1,3-Dichloropropene10061-01-5 1.0 1.0 0.20U
Trichloroethene79-01-6 1.0 1.0 0.36U
Dibromochloromethane124-48-1 1.0 1.0 0.56U
1,1,2-Trichloroethane79-00-5 1.0 1.0 0.59U
Benzene71-43-2 1.0 1.0 0.74U
trans-1,3-Dichloropropene10061-02-6 1.0 1.0 0.22U
2-Chloroethyl vinyl ether110-75-8 5.0 5.0 1.3U
Bromoform75-25-2 1.0 1.0 0.70U
Tetrachloroethene127-18-4 1.0 1.0 0.33U
1,1,2,2-Tetrachloroethane79-34-5 1.0 1.0 0.76U
Toluene108-88-3 1.0 1.0 0.30U
Chlorobenzene108-90-7 1.0 1.0 0.48U
Ethylbenzene100-41-4 1.0 1.0 0.19U
Xylenes, Total1330-20-7 3.0 3.0 0.79U
FORM I 8260B
06/03/2010Page 165 of 623
FORM IForm 1GC/MS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: MB 460-37643/5
Matrix: o37390.dLab File ID:
Date Collected:8260BAnalysis Method:
Solid
TestAmerica Edison
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol: 1
Level: (low/med) Low
5(mL)
0.18(mm)
Date Analyzed: 05/17/2010 20:11
ID:DB-624
Analysis Batch No.: 37643 ug/KgUnits:
SURROGATE %RECCAS NO. LIMITS Q
17060-07-0 1,2-Dichloroethane-d4 (Surr) 104 70-138
2037-26-5 Toluene-d8 (Surr) 92 66-126
460-00-4 Bromofluorobenzene 107 72-132
FORM I 8260B
06/03/2010Page 166 of 623
FORM IForm 1GC/MS VOA ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: MB 460-37643/5
Matrix: o37390.dLab File ID:
Date Collected:8260BAnalysis Method:
Solid
TestAmerica Edison
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol: 1
Level: (low/med) Low
5(mL)
0.18(mm)
Date Analyzed: 05/17/2010 20:11
ID:DB-624
Analysis Batch No.: 37643 ug/KgUnits:
Number TICs Found: TIC Result Total: 00
QRTCOMPOUND NAME RESULTCAS NO.
Tentatively Identified Compound None
FORM I-TIC 8260B
06/03/2010Page 167 of 623
Data File: /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37390.dReport Date: 17-May-2010 23:27
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37390.dLab Smp Id: MB Inj Date : 17-MAY-2010 20:11 Operator : VOAMS 9 Inst ID: VOAMS12.iSmp Info : MBMisc Info : Comment : Method : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/8260L_10.mMeth Date : 17-May-2010 18:29 ken Quant Type: ISTDCal Date : 15-APR-2010 16:52 Cal File: o36298.dAls bottle: 6 QC Sample: BLANKDil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd2
Concentration Formula: Amt * DF * ((Vt/Ws)/((100-M)/100)) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 5.00000 Volume of final extract (mL)Ws 5.00000 Weight of sample extracted (g)M 0.00000 % Moisture (not decanted)
Cpnd Variable Local Compound Variable
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE ( ug/L) (ug/Kg)
========================== ==== == ====== ====== ======== ======= =======
$ 16 1,2-Dichloroethane-d4 (SUR) 65 3.933 3.933 (0.923) 290019 52.1656 52
* 69 Fluorobenzene 96 4.262 4.262 (1.000) 1237424 50.0000
$ 37 Toluene-d8 (SUR) 98 6.073 6.073 (0.754) 1133872 45.9973 46
* 32 Chlorobenzene-d5 117 8.054 8.054 (1.000) 1154369 50.0000
$ 41 Bromofluorobenzene (SUR) 174 9.913 9.913 (0.845) 372960 53.6413 54
* 91 1,4-Dichlorobenzene-d4 152 11.730 11.730 (1.000) 545686 50.0000
06/03/2010Page 168 of 623
Data File: /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37390.dReport Date: 17-May-2010 23:27
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37390.dLab Smp Id: MB Inj Date : 17-MAY-2010 20:11 Operator : VOAMS 9 Inst ID: VOAMS12.iSmp Info : MBMisc Info : Comment : Method : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/8260L_10.mMeth Date : 17-May-2010 18:29 ken Quant Type: ISTDCal Date : 15-APR-2010 16:52 Cal File: o36298.dAls bottle: 6 QC Sample: BLANKDil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd2
- NO TENTATIVELY IDENTIFIED COMPOUNDS -
06/03/2010Page 169 of 623
Data File: o37390.d
Date: 17-MAY-2010 20:11
Client ID: Instrument: VOAMS12.i
Sample Info: MB Operator: VOAMS 9
06/03/2010Page 170 of 623
FORM IForm 1GC/MS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: LCS 460-37643/3
Matrix: o37386.dLab File ID:
Date Collected:8260BAnalysis Method:
Solid
TestAmerica Edison
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol: 1
Level: (low/med) Low
5(mL)
0.18(mm)
Date Analyzed: 05/17/2010 17:46
ID:DB-624
Analysis Batch No.: 37643 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Chloromethane74-87-3 19.2 1.0 0.63
Bromomethane74-83-9 22.0 1.0 0.41
Vinyl chloride75-01-4 19.5 1.0 0.23
Chloroethane75-00-3 19.9 1.0 0.40
Methylene Chloride75-09-2 23.9 1.0 0.47
Trichlorofluoromethane75-69-4 21.5 1.0 0.26
1,1-Dichloroethene75-35-4 20.8 1.0 0.37
1,1-Dichloroethane75-34-3 19.8 1.0 0.25
trans-1,2-Dichloroethene156-60-5 19.8 1.0 0.28
cis-1,2-Dichloroethene156-59-2 20.0 1.0 0.24
Chloroform67-66-3 19.9 1.0 0.24
1,2-Dichloroethane107-06-2 19.6 1.0 0.39
1,1,1-Trichloroethane71-55-6 20.5 1.0 0.19
Carbon tetrachloride56-23-5 21.5 1.0 0.10
Bromodichloromethane75-27-4 20.1 1.0 0.30
1,2-Dichloropropane78-87-5 19.5 1.0 0.32
cis-1,3-Dichloropropene10061-01-5 18.7 1.0 0.20
Trichloroethene79-01-6 19.8 1.0 0.36
Dibromochloromethane124-48-1 16.7 1.0 0.56
1,1,2-Trichloroethane79-00-5 17.8 1.0 0.59
Benzene71-43-2 19.7 1.0 0.74
trans-1,3-Dichloropropene10061-02-6 15.2 1.0 0.22
2-Chloroethyl vinyl ether110-75-8 16.5 5.0 1.3
Bromoform75-25-2 14.7 1.0 0.70
Tetrachloroethene127-18-4 18.6 1.0 0.33
1,1,2,2-Tetrachloroethane79-34-5 18.9 1.0 0.76
Toluene108-88-3 19.2 1.0 0.30
Chlorobenzene108-90-7 20.0 1.0 0.48
Ethylbenzene100-41-4 21.1 1.0 0.19
Xylenes, Total1330-20-7 61.9 3.0 0.79
FORM I 8260B
06/03/2010Page 171 of 623
FORM IForm 1GC/MS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: LCS 460-37643/3
Matrix: o37386.dLab File ID:
Date Collected:8260BAnalysis Method:
Solid
TestAmerica Edison
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol: 1
Level: (low/med) Low
5(mL)
0.18(mm)
Date Analyzed: 05/17/2010 17:46
ID:DB-624
Analysis Batch No.: 37643 ug/KgUnits:
SURROGATE %RECCAS NO. LIMITS Q
17060-07-0 1,2-Dichloroethane-d4 (Surr) 89 70-138
2037-26-5 Toluene-d8 (Surr) 90 66-126
460-00-4 Bromofluorobenzene 108 72-132
FORM I 8260B
06/03/2010Page 172 of 623
Data File: /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37386.dReport Date: 17-May-2010 20:07
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37386.dLab Smp Id: LCS Inj Date : 17-MAY-2010 17:46 Operator : VOAMS 9 Inst ID: VOAMS12.iSmp Info : LCSMisc Info : Comment : Method : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/8260L_10.mMeth Date : 17-May-2010 18:29 ken Quant Type: ISTDCal Date : 15-APR-2010 16:52 Cal File: o36298.dAls bottle: 2 QC Sample: BSDil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd2
Concentration Formula: Amt * DF * ((Vt/Ws)/((100-M)/100)) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 5.00000 Volume of final extract (mL)Ws 5.00000 Weight of sample extracted (g)M 0.00000 % Moisture (not decanted)
Cpnd Variable Local Compound Variable
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE ( ug/L) (ug/Kg)
========================== ==== == ====== ====== ======== ======= =======
M 14 1,2-Dichloroethene (total) 100 495021 39.8435 40
90 Dichlorodifluoromethane 85 1.012 1.013 (0.238) 241035 22.5387 22
1 Chloromethane 50 1.141 1.147 (0.268) 276534 19.1871 19
4 Vinyl Chloride 62 1.183 1.183 (0.278) 278276 19.4693 19
3 Bromomethane 94 1.372 1.372 (0.322) 212412 22.0007 22
5 Chloroethane 64 1.451 1.445 (0.341) 167312 19.8808 20
9 Trichlorofluoromethane 101 1.573 1.574 (0.369) 393716 21.4673 21
121 n-Pentane 72 1.616 1.616 (0.379) 42637 19.5222 20
127 Ethanol 46 1.707 1.708 (0.401) 161075 2378.15 2400
46 Ethyl Ether 59 1.756 1.756 (0.412) 144204 17.1687 17
119 Isoprene 67 1.762 1.762 (0.414) 324026 18.5014 18
47 Acrolein 56 1.835 1.836 (0.431) 191273 159.847 160
10 1,1-Dichloroethene 96 1.896 1.897 (0.445) 224018 20.7623 21
48 Freon TF 101 1.896 1.897 (0.445) 238620 19.1956 19
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Data File: /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37386.dReport Date: 17-May-2010 20:07
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE ( ug/L) (ug/Kg)
========================== ==== == ====== ====== ======== ======= =======
7 Acetone 43 1.939 1.939 (0.455) 53210 23.4599 23
142 Iodomethane 142 2.000 2.000 (0.469) 254463 19.9308 20
8 Carbon Disulfide 76 2.037 2.037 (0.478) 641152 18.9482 19
50 Acetonitrile 41 2.128 2.128 (0.499) 507349 408.034 410
125 Methyl acetate 74 2.153 2.159 (0.505) 42999 18.6780 19
6 Methylene Chloride 84 2.226 2.226 (0.522) 252844 23.9265 24
51 TBA 59 2.323 2.323 (0.545) 318591 279.598 280
52 Acrylonitrile 53 2.402 2.403 (0.564) 500440 114.570 110
12 trans-1,2-Dichloroethene 96 2.415 2.415 (0.567) 247497 19.8181 20
53 MTBE 73 2.421 2.421 (0.568) 434306 17.5230 18
49 Isopropanol 45 2.043 2.043 (0.479) 1993860 2235.11 2200(A)
54 Hexane 56 2.616 2.616 (0.614) 152512 17.2476 17
11 1,1-Dichloroethane 63 2.726 2.726 (0.640) 422554 19.8302 20
57 Vinyl Acetate 43 2.787 2.787 (0.654) 369414 15.4800 15
55 DIPE 45 2.793 2.793 (0.655) 512977 17.2699 17
149 tert-Butyl ethyl ether 59 3.085 3.085 (0.724) 420393 16.2122 16
104 2,2-Dichloropropane 77 3.189 3.189 (0.748) 311135 21.2972 21
13 cis-1,2-Dichloroethene 96 3.195 3.195 (0.750) 247523 20.0254 20
18 2-Butanone 72 3.225 3.213 (0.757) 20665 17.1005 17
56 Ethyl Acetate 70 3.280 3.274 (0.770) 26897 29.6978 30
108 Bromochloromethane 128 3.402 3.402 (0.798) 104478 20.8377 21
15 Chloroform 83 3.475 3.476 (0.815) 386341 19.8565 20
20 1,1,1-Trichloroethane 97 3.634 3.634 (0.853) 326415 20.5297 20
59 Cyclohexane 56 3.683 3.677 (0.864) 386708 17.9041 18
21 Carbon Tetrachloride 117 3.786 3.787 (0.888) 277101 21.4941 21
92 1,1-Dichloropropene 75 3.786 3.787 (0.888) 289303 19.5922 20
$ 16 1,2-Dichloroethane-d4 (SUR) 65 3.927 3.933 (0.921) 319986 44.6139 45
28 Benzene 78 3.981 3.982 (0.934) 852061 19.7194 20
17 1,2-Dichloroethane 62 4.000 4.000 (0.938) 257436 19.6110 20
61 Isopropyl Acetate 43 4.091 4.091 (0.960) 542308 32.3590 32
140 tert-Amylmethyl Ether 73 4.109 4.116 (0.964) 342824 14.7832 15(R)
* 69 Fluorobenzene 96 4.262 4.262 (1.000) 1596386 50.0000
156 2,4,4-Trimethyl-1-pentene 112 4.603 4.603 (1.080) 66928 18.0764 18
25 Trichloroethene 95 4.640 4.640 (1.089) 217624 19.7816 20
63 n-Butanol 43 4.634 4.634 (1.087) 192947 1132.63 1100
96 Ethyl Acrylate 55 4.798 4.798 (1.126) 165126 16.2730 16
126 Methyl cyclohexane 83 4.841 4.847 (1.136) 355777 16.9350 17
23 1,2-Dichloropropane 63 4.884 4.884 (1.146) 210327 19.5281 20
109 Dibromomethane 93 5.012 5.012 (1.176) 111801 19.2186 19
95 1,4-Dioxane 88 5.067 5.061 (1.189) 385825 2612.67 2600
146 Methyl methacrylate 69 5.060 5.061 (1.187) 86806 15.1057 15(R)
64 Propyl Acetate 43 5.140 5.140 (1.206) 364108 31.6625 32
22 Bromodichloromethane 83 5.207 5.207 (1.222) 246277 20.0800 20
30 2-Chloroethyl Vinyl Ether 63 5.597 5.597 (1.313) 82665 16.5291 16
118 Epichlorohydrin 57 5.652 5.652 (1.326) 318383 317.201 320
24 cis-1,3-Dichloropropene 75 5.749 5.750 (1.349) 269574 18.7467 19
33 4-Methyl-2-Pentanone 43 5.969 5.969 (1.401) 112446 14.3186 14
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Data File: /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37386.dReport Date: 17-May-2010 20:07
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE ( ug/L) (ug/Kg)
========================== ==== == ====== ====== ======== ======= =======
$ 37 Toluene-d8 (SUR) 98 6.072 6.073 (0.754) 1047591 44.8363 45
38 Toluene 91 6.158 6.158 (0.765) 879315 19.2234 19
29 trans-1,3-Dichloropropene 75 6.475 6.475 (0.804) 219864 15.2470 15
27 1,1,2-Trichloroethane 83 6.707 6.707 (0.833) 124315 17.8033 18
35 Tetrachloroethene 166 6.871 6.871 (0.853) 188075 18.5970 18
103 1,3-Dichloropropane 76 6.926 6.926 (0.860) 267074 18.0146 18
34 2-Hexanone 43 7.103 7.103 (0.882) 89741 15.5918 16
26 Dibromochloromethane 129 7.231 7.231 (0.898) 149446 16.6837 17
65 Butyl Acetate 43 7.322 7.322 (0.909) 414275 33.2711 33
66 1,2-Dibromoethane 107 7.359 7.359 (0.914) 145193 18.3664 18
* 32 Chlorobenzene-d5 117 8.054 8.054 (1.000) 1094145 50.0000
39 Chlorobenzene 112 8.096 8.097 (1.005) 550809 19.9701 20
97 1,1,1,2-Tetrachloroethane 131 8.243 8.243 (1.023) 149108 15.6317 16
40 Ethylbenzene 106 8.298 8.298 (1.030) 343579 21.0836 21
43 m+p-Xylene 106 8.487 8.487 (1.054) 817376 41.0826 41
44 o-Xylene 106 9.084 9.090 (1.128) 379766 20.7963 21
42 Styrene 104 9.115 9.115 (1.132) 652197 20.6530 21
147 Butyl Acrylate 55 9.157 9.157 (0.781) 287824 16.9922 17
31 Bromoform 173 9.358 9.359 (1.162) 79223 14.6906 15
145 Amyl Acetate 43 9.553 9.554 (1.186) 240392 30.5914 30
110 Isopropylbenzene 105 9.700 9.700 (1.204) 1062867 20.7267 21
$ 41 Bromofluorobenzene (SUR) 174 9.913 9.913 (0.845) 395698 53.7634 54
150 Camphene 93 10.066 10.060 (0.858) 438409 18.4295 18
107 Bromobenzene 156 10.114 10.115 (0.862) 235634 21.5195 22
36 1,1,2,2-Tetrachloroethane 83 10.224 10.230 (0.872) 189772 18.9151 19
99 1,2,3-Trichloropropane 110 10.255 10.255 (0.874) 53405 18.6088 19
143 trans-1,4-Dichloro-2-butene 53 10.322 10.322 (2.422) 48569 15.7752 16
112 n-Propylbenzene 91 10.377 10.377 (0.885) 1329321 20.9373 21
105 2-Chlorotoluene 91 10.462 10.462 (0.892) 739182 20.6196 21
106 4-Chlorotoluene 91 10.651 10.651 (0.908) 846941 21.3889 21
102 1,3,5-Trimethylbenzene 105 10.700 10.694 (0.912) 826159 19.9063 20
148 Butyl methacrylate 69 10.974 10.968 (0.936) 247235 16.6447 17
115 tert-Butylbenzene 119 11.218 11.212 (0.956) 793519 20.9826 21
100 1,2,4-Trimethylbenzene 105 11.291 11.291 (0.963) 848702 20.2190 20
151 2-Octanone 43 11.535 11.529 (0.983) 248258 19.3078 19
114 sec-Butylbenzene 105 11.541 11.541 (0.984) 1265453 21.9128 22
67 1,3-Dichlorobenzene 146 11.632 11.633 (0.992) 478397 20.6585 21
153 2-Octanol 45 11.681 11.675 (0.996) 37750 13.0531 13(R)
* 91 1,4-Dichlorobenzene-d4 152 11.730 11.730 (1.000) 577641 50.0000
68 1,4-Dichlorobenzene 146 11.760 11.761 (1.003) 473860 19.9088 20
113 p-Isopropyltoluene 119 11.766 11.767 (1.003) 1014389 21.4689 21
69 1,2-Dichlorobenzene 146 12.212 12.212 (1.041) 441667 20.2717 20
117 Benzyl chloride 91 11.962 11.962 (1.020) 298675 14.2946 14
111 n-Butylbenzene 91 12.272 12.267 (1.046) 1041415 21.9345 22
101 1,2-Dibromo-3-chloropropane 75 13.065 13.059 (1.114) 35475 16.4046 16
152 Camphor 95 13.730 13.736 (1.170) 111841 80.7128 81
93 1,2,4-Trichlorobenzene 180 13.821 13.821 (1.178) 346356 21.2077 21
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CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE ( ug/L) (ug/Kg)
========================== ==== == ====== ====== ======== ======= =======
94 Hexachlorobutadiene 225 13.986 13.986 (1.192) 199223 20.8319 21
70 Naphthalene 128 14.022 14.016 (1.195) 812454 21.3940 21
98 1,2,3-Trichlorobenzene 180 14.223 14.223 (1.213) 313268 20.3736 20
M 45 Xylene (Total) 100 1197143 61.8789 62
QC Flag Legend
A - Target compound detected but, quantitated amountexceeded maximum amount.
R - Spike/Surrogate failed recovery limits.
06/03/2010Page 176 of 623
Data File: o37386.d
Date: 17-MAY-2010 17:46
Client ID: Instrument: VOAMS12.i
Sample Info: LCS Operator: VOAMS 9
06/03/2010Page 177 of 623
FORM IForm 1GC/MS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: LCSD 460-37643/4
Matrix: o37387.dLab File ID:
Date Collected:8260BAnalysis Method:
Solid
TestAmerica Edison
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol: 1
Level: (low/med) Low
5(mL)
0.18(mm)
Date Analyzed: 05/17/2010 18:10
ID:DB-624
Analysis Batch No.: 37643 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Chloromethane74-87-3 19.2 1.0 0.63
Bromomethane74-83-9 22.3 1.0 0.41
Vinyl chloride75-01-4 19.5 1.0 0.23
Chloroethane75-00-3 19.9 1.0 0.40
Methylene Chloride75-09-2 26.8 1.0 0.47
Trichlorofluoromethane75-69-4 21.1 1.0 0.26
1,1-Dichloroethene75-35-4 23.1 1.0 0.37
1,1-Dichloroethane75-34-3 21.5 1.0 0.25
trans-1,2-Dichloroethene156-60-5 21.6 1.0 0.28
cis-1,2-Dichloroethene156-59-2 22.1 1.0 0.24
Chloroform67-66-3 21.8 1.0 0.24
1,2-Dichloroethane107-06-2 21.5 1.0 0.39
1,1,1-Trichloroethane71-55-6 23.0 1.0 0.19
Carbon tetrachloride56-23-5 23.3 1.0 0.10
Bromodichloromethane75-27-4 23.1 1.0 0.30
1,2-Dichloropropane78-87-5 21.1 1.0 0.32
cis-1,3-Dichloropropene10061-01-5 21.8 1.0 0.20
Trichloroethene79-01-6 21.2 1.0 0.36
Dibromochloromethane124-48-1 18.3 1.0 0.56
1,1,2-Trichloroethane79-00-5 20.0 1.0 0.59
Benzene71-43-2 21.9 1.0 0.74
trans-1,3-Dichloropropene10061-02-6 17.5 1.0 0.22
2-Chloroethyl vinyl ether110-75-8 17.4 5.0 1.3
Bromoform75-25-2 16.8 1.0 0.70
Tetrachloroethene127-18-4 22.3 1.0 0.33
1,1,2,2-Tetrachloroethane79-34-5 20.3 1.0 0.76
Toluene108-88-3 21.7 1.0 0.30
Chlorobenzene108-90-7 21.9 1.0 0.48
Ethylbenzene100-41-4 22.1 1.0 0.19
Xylenes, Total1330-20-7 67.1 3.0 0.79
FORM I 8260B
06/03/2010Page 178 of 623
FORM IForm 1GC/MS VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: LCSD 460-37643/4
Matrix: o37387.dLab File ID:
Date Collected:8260BAnalysis Method:
Solid
TestAmerica Edison
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol: 1
Level: (low/med) Low
5(mL)
0.18(mm)
Date Analyzed: 05/17/2010 18:10
ID:DB-624
Analysis Batch No.: 37643 ug/KgUnits:
SURROGATE %RECCAS NO. LIMITS Q
17060-07-0 1,2-Dichloroethane-d4 (Surr) 90 70-138
2037-26-5 Toluene-d8 (Surr) 95 66-126
460-00-4 Bromofluorobenzene 106 72-132
FORM I 8260B
06/03/2010Page 179 of 623
Data File: /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37387.dReport Date: 17-May-2010 20:07
TestAmerica
VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37387.dLab Smp Id: LCSD Inj Date : 17-MAY-2010 18:10 Operator : VOAMS 9 Inst ID: VOAMS12.iSmp Info : LCSDMisc Info : Comment : Method : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/8260L_10.mMeth Date : 17-May-2010 18:29 ken Quant Type: ISTDCal Date : 15-APR-2010 16:52 Cal File: o36298.dAls bottle: 3 QC Sample: BSDDil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd2
Concentration Formula: Amt * DF * ((Vt/Ws)/((100-M)/100)) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 5.00000 Volume of final extract (mL)Ws 5.00000 Weight of sample extracted (g)M 0.00000 % Moisture (not decanted)
Cpnd Variable Local Compound Variable
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE ( ug/L) (ug/Kg)
========================== ==== == ====== ====== ======== ======= =======
M 14 1,2-Dichloroethene (total) 100 551170 43.7014 44
90 Dichlorodifluoromethane 85 1.007 1.013 (0.236) 246011 22.6604 23
1 Chloromethane 50 1.141 1.147 (0.268) 280679 19.1838 19
4 Vinyl Chloride 62 1.183 1.183 (0.278) 283367 19.5293 20
3 Bromomethane 94 1.372 1.372 (0.322) 218172 22.2598 22
5 Chloroethane 64 1.439 1.445 (0.338) 170390 19.9442 20
9 Trichlorofluoromethane 101 1.573 1.574 (0.369) 392325 21.0719 21
121 n-Pentane 72 1.622 1.616 (0.381) 47960 21.6313 22
127 Ethanol 46 1.708 1.708 (0.401) 165851 2412.10 2400
46 Ethyl Ether 59 1.756 1.756 (0.412) 160563 18.8309 19
119 Isoprene 67 1.769 1.762 (0.415) 352393 19.8206 20
47 Acrolein 56 1.836 1.836 (0.431) 193625 159.396 160
10 1,1-Dichloroethene 96 1.897 1.897 (0.445) 253166 23.1134 23
48 Freon TF 101 1.903 1.897 (0.446) 262458 20.7979 21
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CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE ( ug/L) (ug/Kg)
========================== ==== == ====== ====== ======== ======= =======
7 Acetone 43 1.939 1.939 (0.455) 49861 21.6549 22
142 Iodomethane 142 2.000 2.000 (0.469) 280315 21.6277 22
8 Carbon Disulfide 76 2.043 2.037 (0.479) 687938 20.0272 20
50 Acetonitrile 41 2.128 2.128 (0.499) 557084 441.342 440
125 Methyl acetate 74 2.159 2.159 (0.506) 44775 19.1589 19
6 Methylene Chloride 84 2.226 2.226 (0.522) 287754 26.8234 27
51 TBA 59 2.323 2.323 (0.545) 346571 299.611 300
52 Acrylonitrile 53 2.403 2.403 (0.564) 511031 115.248 120
12 trans-1,2-Dichloroethene 96 2.415 2.415 (0.567) 274203 21.6287 22
53 MTBE 73 2.421 2.421 (0.568) 467729 18.5896 18
49 Isopropanol 45 2.043 2.043 (0.479) 2018158 2227.02 2200(A)
54 Hexane 56 2.616 2.616 (0.614) 172880 19.2591 19
11 1,1-Dichloroethane 63 2.726 2.726 (0.640) 465976 21.5413 22
57 Vinyl Acetate 43 2.787 2.787 (0.654) 411856 17.0008 17
55 DIPE 45 2.793 2.793 (0.655) 575539 19.0867 19
149 tert-Butyl ethyl ether 59 3.085 3.085 (0.724) 474276 18.0170 18
104 2,2-Dichloropropane 77 3.195 3.189 (0.750) 348131 23.4738 23
13 cis-1,2-Dichloroethene 96 3.195 3.195 (0.750) 276966 22.0727 22
18 2-Butanone 72 3.226 3.213 (0.757) 23076 18.8101 19
56 Ethyl Acetate 70 3.274 3.274 (0.768) 29035 31.5804 32
108 Bromochloromethane 128 3.402 3.402 (0.798) 119530 23.4837 23
15 Chloroform 83 3.476 3.476 (0.815) 430231 21.7820 22
20 1,1,1-Trichloroethane 97 3.634 3.634 (0.853) 371490 23.0157 23
59 Cyclohexane 56 3.683 3.677 (0.864) 417907 19.0596 19
21 Carbon Tetrachloride 117 3.786 3.787 (0.888) 304647 23.2779 23
92 1,1-Dichloropropene 75 3.786 3.787 (0.888) 321297 21.4338 21
$ 16 1,2-Dichloroethane-d4 (SUR) 65 3.933 3.933 (0.923) 327433 44.9703 45
28 Benzene 78 3.982 3.982 (0.934) 961260 21.9143 22
17 1,2-Dichloroethane 62 4.006 4.000 (0.940) 287138 21.5470 22
61 Isopropyl Acetate 43 4.091 4.091 (0.960) 607798 35.7251 36
140 tert-Amylmethyl Ether 73 4.110 4.116 (0.964) 414461 17.6054 18
* 69 Fluorobenzene 96 4.262 4.262 (1.000) 1620590 50.0000
156 2,4,4-Trimethyl-1-pentene 112 4.603 4.603 (1.080) 67250 17.8921 18
25 Trichloroethene 95 4.646 4.640 (1.090) 236502 21.1765 21
63 n-Butanol 43 4.634 4.634 (1.087) 201766 1166.71 1200
96 Ethyl Acrylate 55 4.798 4.798 (1.126) 190787 18.5211 18
126 Methyl cyclohexane 83 4.847 4.847 (1.137) 410422 19.2443 19
23 1,2-Dichloropropane 63 4.884 4.884 (1.146) 230623 21.0928 21
109 Dibromomethane 93 5.012 5.012 (1.176) 129261 21.8880 22
95 1,4-Dioxane 88 5.067 5.061 (1.189) 386053 2575.17 2600
146 Methyl methacrylate 69 5.055 5.061 (1.186) 95473 16.3658 16
64 Propyl Acetate 43 5.140 5.140 (1.206) 398938 34.1731 34
22 Bromodichloromethane 83 5.207 5.207 (1.222) 287481 23.0894 23
30 2-Chloroethyl Vinyl Ether 63 5.597 5.597 (1.313) 88101 17.3529 17
118 Epichlorohydrin 57 5.652 5.652 (1.326) 334583 328.362 330
24 cis-1,3-Dichloropropene 75 5.750 5.750 (1.349) 318223 21.7994 22
33 4-Methyl-2-Pentanone 43 5.975 5.969 (1.402) 129514 16.2458 16
06/03/2010Page 181 of 623
Data File: /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37387.dReport Date: 17-May-2010 20:07
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE ( ug/L) (ug/Kg)
========================== ==== == ====== ====== ======== ======= =======
$ 37 Toluene-d8 (SUR) 98 6.073 6.073 (0.754) 1121982 47.4508 47
38 Toluene 91 6.158 6.158 (0.765) 1005590 21.7234 22
29 trans-1,3-Dichloropropene 75 6.475 6.475 (0.804) 255319 17.4957 17
27 1,1,2-Trichloroethane 83 6.707 6.707 (0.833) 141364 20.0050 20
35 Tetrachloroethene 166 6.871 6.871 (0.853) 227891 22.2669 22
103 1,3-Dichloropropane 76 6.926 6.926 (0.860) 296838 19.7848 20
34 2-Hexanone 43 7.103 7.103 (0.882) 92348 15.8544 16
26 Dibromochloromethane 129 7.231 7.231 (0.898) 165525 18.2596 18
65 Butyl Acetate 43 7.322 7.322 (0.909) 435485 34.5598 34
66 1,2-Dibromoethane 107 7.359 7.359 (0.914) 169638 21.2041 21
* 32 Chlorobenzene-d5 117 8.054 8.054 (1.000) 1107274 50.0000
39 Chlorobenzene 112 8.097 8.097 (1.005) 612134 21.9303 22
97 1,1,1,2-Tetrachloroethane 131 8.243 8.243 (1.023) 176993 18.3349 18
40 Ethylbenzene 106 8.298 8.298 (1.030) 365157 22.1420 22
43 m+p-Xylene 106 8.487 8.487 (1.054) 897827 44.5911 44
44 o-Xylene 106 9.084 9.090 (1.128) 415434 22.4797 22
42 Styrene 104 9.115 9.115 (1.132) 721987 22.5920 22
147 Butyl Acrylate 55 9.157 9.157 (0.780) 322044 18.7154 19
31 Bromoform 173 9.359 9.359 (1.162) 91554 16.7759 17
145 Amyl Acetate 43 9.554 9.554 (1.186) 264814 33.2997 33(R)
110 Isopropylbenzene 105 9.700 9.700 (1.204) 1157095 22.2966 22
$ 41 Bromofluorobenzene (SUR) 174 9.913 9.913 (0.845) 395096 52.8429 53
150 Camphene 93 10.066 10.060 (0.858) 448780 18.5707 18
107 Bromobenzene 156 10.115 10.115 (0.862) 259509 23.3297 23
36 1,1,2,2-Tetrachloroethane 83 10.224 10.230 (0.871) 206879 20.2981 20
99 1,2,3-Trichloropropane 110 10.255 10.255 (0.874) 60531 20.7624 21
143 trans-1,4-Dichloro-2-butene 53 10.328 10.322 (2.423) 54348 17.3886 17
112 n-Propylbenzene 91 10.377 10.377 (0.884) 1506239 23.3532 23
105 2-Chlorotoluene 91 10.462 10.462 (0.891) 832256 22.8532 23
106 4-Chlorotoluene 91 10.651 10.651 (0.908) 937455 23.3049 23
102 1,3,5-Trimethylbenzene 105 10.700 10.694 (0.912) 937327 22.2321 22
148 Butyl methacrylate 69 10.974 10.968 (0.935) 285817 18.9415 19
115 tert-Butylbenzene 119 11.218 11.212 (0.956) 881519 22.9454 23
100 1,2,4-Trimethylbenzene 105 11.291 11.291 (0.962) 960539 22.5258 22
151 2-Octanone 43 11.529 11.529 (0.982) 242654 18.5772 18
114 sec-Butylbenzene 105 11.541 11.541 (0.983) 1413705 24.0975 24
67 1,3-Dichlorobenzene 146 11.639 11.633 (0.992) 528182 22.4520 22
153 2-Octanol 45 11.675 11.675 (0.995) 39257 13.3621 13(R)
* 91 1,4-Dichlorobenzene-d4 152 11.736 11.730 (1.000) 586808 50.0000
68 1,4-Dichlorobenzene 146 11.761 11.761 (1.002) 539430 22.3096 22
113 p-Isopropyltoluene 119 11.767 11.767 (1.003) 1133180 23.6084 24
69 1,2-Dichlorobenzene 146 12.212 12.212 (1.041) 505359 22.8327 23
117 Benzyl chloride 91 11.962 11.962 (1.019) 327428 15.4259 15
111 n-Butylbenzene 91 12.273 12.267 (1.046) 1169584 24.2492 24
101 1,2-Dibromo-3-chloropropane 75 13.059 13.059 (1.113) 40554 18.4601 18
152 Camphor 95 13.736 13.736 (1.170) 115450 82.0159 82
93 1,2,4-Trichlorobenzene 180 13.821 13.821 (1.178) 396882 23.9218 24
06/03/2010Page 182 of 623
Data File: /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37387.dReport Date: 17-May-2010 20:07
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE ( ug/L) (ug/Kg)
========================== ==== == ====== ====== ======== ======= =======
94 Hexachlorobutadiene 225 13.986 13.986 (1.192) 221832 22.8336 23
70 Naphthalene 128 14.016 14.016 (1.194) 908248 23.5428 24
98 1,2,3-Trichlorobenzene 180 14.223 14.223 (1.212) 356541 22.8256 23
M 45 Xylene (Total) 100 1313261 67.0709 67
QC Flag Legend
A - Target compound detected but, quantitated amountexceeded maximum amount.
R - Spike/Surrogate failed recovery limits.
06/03/2010Page 183 of 623
Data File: o37387.d
Date: 17-MAY-2010 18:10
Client ID: Instrument: VOAMS12.i
Sample Info: LCSD Operator: VOAMS 9
06/03/2010Page 184 of 623
Lab Name: Job No.:
SDG No.:
Instrument ID:
Analysis Batch Number:
GC/MS VOA ANALYSIS RUN LOG
DILUTION
FACTOR
COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID
TestAmerica Edison 460-13139-1
VOAMS12
34969
Start Date:
End Date: 04/16/2010 00:55
04/15/2010 13:12
BFB 460-34969/1 DB-624 0.18(mm)104/15/2010 13:12 o36289.d
IC 460-34969/2 DB-624 0.18(mm)104/15/2010 14:24 o36292.d
IC 460-34969/3 DB-624 0.18(mm)104/15/2010 15:13 o36294.d
ZZZZZ DB-624 0.18(mm)104/15/2010 15:38
ICIS 460-34969/19 DB-624 0.18(mm)104/15/2010 15:38 o36295.d
ZZZZZ DB-624 0.18(mm)104/15/2010 16:03
IC 460-34969/20 DB-624 0.18(mm)104/15/2010 16:03 o36296.d
IC 460-34969/6 DB-624 0.18(mm)104/15/2010 16:27 o36297.d
IC 460-34969/7 DB-624 0.18(mm)104/15/2010 16:52 o36298.d
ZZZZZ DB-624 0.18(mm)104/15/2010 19:52
ZZZZZ DB-624 0.18(mm)104/15/2010 19:52
ZZZZZ DB-624 0.18(mm)104/15/2010 20:17
ZZZZZ DB-624 0.18(mm)104/15/2010 21:13
ZZZZZ DB-624 0.18(mm)104/15/2010 21:38
ZZZZZ DB-624 0.18(mm)104/15/2010 22:02
ZZZZZ DB-624 0.18(mm)104/15/2010 22:27
ZZZZZ DB-624 0.18(mm)104/15/2010 22:52
ZZZZZ DB-624 0.18(mm)104/15/2010 23:16
ZZZZZ DB-624 0.18(mm)104/15/2010 23:41
ZZZZZ DB-624 0.18(mm)104/16/2010 00:06
ZZZZZ DB-624 0.18(mm)104/16/2010 00:30
ZZZZZ DB-624 0.18(mm)104/16/2010 00:55
8260B
06/03/2010Page 185 of 623
Lab Name: Job No.:
SDG No.:
Instrument ID:
Analysis Batch Number:
GC/MS VOA ANALYSIS RUN LOG
DILUTION
FACTOR
COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID
TestAmerica Edison 460-13139-1
VOAMS12
37643
Start Date:
End Date: 05/18/2010 03:36
05/17/2010 16:42
BFB 460-37643/1 DB-624 0.18(mm)105/17/2010 16:42 o37384.d
CCVIS 460-37643/2 DB-624 0.18(mm)105/17/2010 17:02 o37385.d
LCS 460-37643/3 DB-624 0.18(mm)105/17/2010 17:46 o37386.d
LCSD 460-37643/4 DB-624 0.18(mm)105/17/2010 18:10 o37387.d
MB 460-37643/5 DB-624 0.18(mm)105/17/2010 20:11 o37390.d
ZZZZZ DB-624 0.18(mm)105/17/2010 20:36
ZZZZZ DB-624 0.18(mm)105/17/2010 21:25
ZZZZZ DB-624 0.18(mm)105/17/2010 22:15
ZZZZZ DB-624 0.18(mm)105/17/2010 22:40
ZZZZZ DB-624 0.18(mm)105/17/2010 23:04
ZZZZZ DB-624 0.18(mm)105/17/2010 23:29
ZZZZZ DB-624 0.18(mm)105/17/2010 23:54
460-13139-2 TB-3 6-7 DB-624 0.18(mm)105/18/2010 00:18 o37400.d
460-13139-4 TB-2 5-6 DB-624 0.18(mm)105/18/2010 00:43 o37401.d
460-13139-5 TB-1 2-3 DB-624 0.18(mm)105/18/2010 01:08 o37402.d
460-13139-7 TB-5 3-4 DB-624 0.18(mm)105/18/2010 01:33 o37403.d
ZZZZZ DB-624 0.18(mm)105/18/2010 02:22
ZZZZZ DB-624 0.18(mm)105/18/2010 02:47
ZZZZZ DB-624 0.18(mm)105/18/2010 03:36
8260B
06/03/2010Page 186 of 623
GC/MS VOA Worksheet
Method: 5035
Analyst: D'Almeida, Melissa M
Batch Number: 460-37413 Date Open:
Batch End:
May 14 2010 8:38AM
May 14 2010 9:02AM
Lab ID Client ID Basis Final weight/volume of
sample
Initial weight/volume of
sample
Method Chain
LB3~460-37413/1 5 g 5 mL
460-13119-A-1 T 5.11 g 5 mL
460-13119-A-1 T 5.05 g 5 mL
460-13119-B-3 T 5.18 g 5 mL
460-13119-B-3 T 5.22 g 5 mL
460-13119-B-5 T 5.01 g 5 mL
460-13119-B-5 T 5.01 g 5 mL
460-13147-B-2 T 5.01 g 5 mL
460-13147-B-2 T 5.09 g 5 mL
460-13147-A-1 T 5.20 g 5 mL
460-13147-A-1 T 5.23 g 5 mL
460-13148-C-1 T 5.13 g 5 mL
460-13148-C-1 T 5.08 g 5 mL
460-13139-B-1 TB-3 2-3 T 3.67 g 5 mL
460-13139-C-1 TB-3 2-3 T 3.88 g 5 mL
460-13139-B-2 TB-3 6-7 T 5.02 g 5 mL5035, 8260B
460-13139-C-2 TB-3 6-7 T 5.05 g 5 mL
460-13139-B-3 TB-2 2-3 T 3.80 g 5 mL
460-13139-C-3 TB-2 2-3 T 2.46 g 5 mL
460-13139-B-4 TB-2 5-6 T 3.75 g 5 mL5035, 8260B
460-13139-C-4 TB-2 5-6 T 3.07 g 5 mL
460-13139-B-5 TB-1 2-3 T 3.09 g 5 mL5035, 8260B
460-13139-C-5 TB-1 2-3 T 3.20 g 5 mL
460-13139-B-6 TB-1 5-6 T 4.01 g 5 mL
460-13139-C-6 TB-1 5-6 T 3.02 g 5 mL
06/03/2010Page 187 of 623
GC/MS VOA Worksheet
Method: 5035
Analyst: D'Almeida, Melissa M
Batch Number: 460-37413 Date Open:
Batch End:
May 14 2010 8:38AM
May 14 2010 9:02AM
Lab ID Client ID Basis Final weight/volume of
sample
Initial weight/volume of
sample
Method Chain
460-13139-B-7 TB-5 3-4 T 2.50 g 5 mL5035, 8260B
460-13139-C-7 TB-5 3-4 T 2.73 g 5 mL
460-13139-B-8 TB-4 6-7 T 4.14 g 5 mL
460-13139-C-8 TB-4 6-7 T 4.68 g 5 mL
06/03/2010Page 188 of 623
Method 8270CSemivolatile Organic Compounds
(GC/MS) by Method 8270C
06/03/2010Page 189 of 623
FORM II
GC/MS SEMI VOA SURROGATE RECOVERY
Lab Name: Job No.: 460-13139-1
SDG No.:
Matrix: Solid Level: Low
TestAmerica Edison
GC Column (1): Rtx-5MS ID: 0.25(mm)
#Lab Sample IDClient Sample ID # # # # #2FP PHL NBZ FBP TBP TPH
460-13139-2TB-3 6-7 76 82 80 78 78 100
460-13139-4TB-2 5-6 55 60 59 67 53 74
460-13139-5TB-1 2-3 58 68 70 69 93 91
460-13139-7TB-5 3-4 39 41 55 60 52 54
MB 460-37564/1-A 76 82 80 78 82 93
LCS 460-37564/2-A
74 78 82 80 99 89
460-13139-5 MSTB-1 2-3 MS 74 79 80 80 67 91
460-13139-5 MSDTB-1 2-3 MSD 72 75 81 82 66 89
QC LIMITSQC LIMITS2FP = 2-Fluorophenol 37-125
PHL = Phenol-d5 41-118NBZ = Nitrobenzene-d5 38-105FBP = 2-Fluorobiphenyl 40-109TBP = 2,4,6-Tribromophenol 10-120TPH = Terphenyl-d14 16-151
FORM II 8270C
# Column to be used to flag recovery values
06/03/2010Page 190 of 623
GC/MS SEMI VOA LAB CONTROL SAMPLE RECOVERY
FORM III
Job No.:Lab Name:
SDG No.:
Level:Matrix:Matrix:
Low
460-13139-1
Lab File ID: p2880.dSolid
Lab ID: LCS 460-37564/2-A Client ID:
TestAmerica Edison
REC
%
REC
QC
LIMITSCONCENTRATION
(ug/Kg)
SPIKE
ADDED
(ug/Kg)
#
LCS LCS
COMPOUND
Phenol 6670 4950 54-11574
2-Chlorophenol 6670 5140 56-11077
2-Nitrophenol 6670 5640 55-10185
2,4-Dimethylphenol 6670 5280 56-11279
2,4-Dichlorophenol 6670 5340 58-11580
4-Chloro-3-methylphenol 6670 5690 55-11785
2,4,6-Trichlorophenol 6670 5360 53-11880
2,4-Dinitrophenol 6670 1100 10-12916
4-Nitrophenol 6670 6490 45-11497
4,6-Dinitro-2-methylphenol 6670 2180 10-11033
Pentachlorophenol 6670 4830 19-11372
N-Nitrosodimethylamine 3330 2550 40-8477
Bis(2-chloroethyl)ether 3330 3020 44-10191
1,3-Dichlorobenzene 3330 2490 47-8475
1,4-Dichlorobenzene 3330 2500 47-8575
1,2-Dichlorobenzene 3330 2570 48-8777
N-Nitrosodi-n-propylamine 3330 3040 42-10791
Hexachloroethane 3330 2480 45-9074
Nitrobenzene 3330 2640 42-10679
Isophorone 3330 2850 48-9786
Bis(2-chloroethoxy)methane 3330 2860 51-10086
1,2,4-Trichlorobenzene 3330 2740 48-9482
Naphthalene 3330 2710 53-9481
Hexachlorobutadiene 3330 2710 45-9881
Hexachlorocyclopentadiene 3330 3110 24-9893
2-Chloronaphthalene 3330 2700 51-10281
Dimethyl phthalate 3330 2960 52-11289
Acenaphthylene 3330 2780 51-10383
2,6-Dinitrotoluene 3330 3130 51-11594
Acenaphthene 3330 2840 46-10085
2,4-Dinitrotoluene 3330 3200 53-11096
Diethyl phthalate 3330 3000 52-11490
4-Chlorophenyl phenyl ether 3330 2910 50-10687
Fluorene 3330 2890 51-10887
N-Nitrosodiphenylamine 3330 3110 49-10693
4-Bromophenyl phenyl ether 3330 2910 44-10287
Hexachlorobenzene 3330 2940 43-10488
Phenanthrene 3330 2850 48-10886
Anthracene 3330 2870 50-10786
Di-n-butyl phthalate 3330 2980 50-10889
Fluoranthene 3330 3040 49-10891
Pyrene 3330 2850 49-11685
FORM III 8270C
# Column to be used to flag recovery and RPD values
06/03/2010Page 191 of 623
GC/MS SEMI VOA LAB CONTROL SAMPLE RECOVERY
FORM III
Job No.:Lab Name:
SDG No.:
Level:Matrix:Matrix:
Low
460-13139-1
Lab File ID: p2880.dSolid
Lab ID: LCS 460-37564/2-A Client ID:
TestAmerica Edison
REC
%
REC
QC
LIMITSCONCENTRATION
(ug/Kg)
SPIKE
ADDED
(ug/Kg)
#
LCS LCS
COMPOUND
Benzidine 3330 169 10-615J *
Butyl benzyl phthalate 3330 3010 49-11790
3,3'-Dichlorobenzidine 3330 2870 24-10586
Benzo[a]anthracene 3330 2880 46-11286
Chrysene 3330 2900 45-11487
Bis(2-ethylhexyl) phthalate 3330 3010 49-11990
Di-n-octyl phthalate 3330 3130 40-10694
Benzo[b]fluoranthene 3330 3060 33-9692
Benzo[k]fluoranthene 3330 2990 35-11590
Benzo[a]pyrene 3330 2590 36-8978
Indeno[1,2,3-cd]pyrene 3330 2870 43-10986
Dibenz(a,h)anthracene 3330 2900 43-10787
Benzo[g,h,i]perylene 3330 2980 43-10689
bis (2-chloroisopropyl) ether 3330 2700 45-10281
FORM III 8270C
# Column to be used to flag recovery and RPD values
06/03/2010Page 192 of 623
GC/MS SEMI VOA MATRIX SPIKE RECOVERY
FORM III
Job No.:Lab Name:
SDG No.:
Level:Matrix:Matrix:
Low
460-13139-1
Lab File ID: p2882.dSolid
Lab ID: 460-13139-5 MS Client ID: TB-1 2-3 MS
TestAmerica Edison
LIMITS
COMPOUND
CONCENTRATION %
REC
QC
REC
SAMPLE
CONCENTRATION
SPIKE
ADDED
(ug/Kg) (ug/Kg) (ug/Kg)
#
MS MS
7110 5410 54-115Phenol 76350 U
7110 5430 56-1102-Chlorophenol 76350 U
7110 5770 55-1012-Nitrophenol 81350 U
7110 5560 56-1122,4-Dimethylphenol 78350 U
7110 5660 58-1152,4-Dichlorophenol 80350 U
7110 6080 55-1174-Chloro-3-methylphenol 86350 U
7110 4770 53-1182,4,6-Trichlorophenol 67350 U
7110 1100 10-1292,4-Dinitrophenol 01100 UU F
7110 4630 45-1144-Nitrophenol 651100 U
7110 191 10-1104,6-Dinitro-2-methylphenol 31100 JU F
7110 1600 19-113Pentachlorophenol 221100 U
3560 2620 40-84N-Nitrosodimethylamine 74350 U
3560 3190 44-101Bis(2-chloroethyl)ether 9035 U
3560 2340 47-841,3-Dichlorobenzene 66350 U
3560 2440 47-851,4-Dichlorobenzene 69350 U
3560 2530 48-871,2-Dichlorobenzene 71350 U
3560 3240 42-107N-Nitrosodi-n-propylamine 9135 U
3560 2360 45-90Hexachloroethane 6635 U
3560 2690 42-106Nitrobenzene 7635 U
3560 2980 48-97Isophorone 84350 U
3560 3020 51-100Bis(2-chloroethoxy)methane 85350 U
3560 2760 48-941,2,4-Trichlorobenzene 7835 U
3560 2740 53-94Naphthalene 77350 U
3560 2630 45-98Hexachlorobutadiene 7472 U
3560 3040 24-98Hexachlorocyclopentadiene 85350 U
3560 2820 51-1022-Chloronaphthalene 79350 U
3560 3030 52-112Dimethyl phthalate 85350 U
3560 2920 51-103Acenaphthylene 82350 U
3560 3210 51-1152,6-Dinitrotoluene 9072 U
3560 2980 46-100Acenaphthene 84350 U
3560 3110 53-1102,4-Dinitrotoluene 8772 U
3560 3010 52-114Diethyl phthalate 85350 U
3560 3010 50-1064-Chlorophenyl phenyl ether 85350 U
3560 2970 51-108Fluorene 84350 U
3560 3310 49-106N-Nitrosodiphenylamine 93350 U
3560 3110 44-1024-Bromophenyl phenyl ether 88350 U
3560 3080 43-104Hexachlorobenzene 8735 U
3560 2930 48-108Phenanthrene 82350 U
3560 2970 50-107Anthracene 84350 U
3560 2980 50-108Di-n-butyl phthalate 84350 U
3560 3030 49-108Fluoranthene 85350 U
3560 3110 49-116Pyrene 87350 U
FORM III 8270C
# Column to be used to flag recovery and RPD values
06/03/2010Page 193 of 623
GC/MS SEMI VOA MATRIX SPIKE RECOVERY
FORM III
Job No.:Lab Name:
SDG No.:
Level:Matrix:Matrix:
Low
460-13139-1
Lab File ID: p2882.dSolid
Lab ID: 460-13139-5 MS Client ID: TB-1 2-3 MS
TestAmerica Edison
LIMITS
COMPOUND
CONCENTRATION %
REC
QC
REC
SAMPLE
CONCENTRATION
SPIKE
ADDED
(ug/Kg) (ug/Kg) (ug/Kg)
#
MS MS
3560 89.3 10-61Benzidine 3350 JU F
3560 3090 49-117Butyl benzyl phthalate 87350 U
3560 3100 24-1053,3'-Dichlorobenzidine 87720 U
3560 3010 46-112Benzo[a]anthracene 8535 U
3560 3100 45-114Chrysene 87350 U
3560 3100 49-119Bis(2-ethylhexyl) phthalate 87350 U
3560 3080 40-106Di-n-octyl phthalate 87350 U
3560 3160 33-96Benzo[b]fluoranthene 8935 U
3560 3090 35-115Benzo[k]fluoranthene 8735 U
3560 2660 36-89Benzo[a]pyrene 7535 U
3560 3110 43-109Indeno[1,2,3-cd]pyrene 8835 U
3560 3000 43-107Dibenz(a,h)anthracene 8435 U
3560 3110 43-106Benzo[g,h,i]perylene 87350 U
3560 2780 45-102bis (2-chloroisopropyl) ether 78350 U
FORM III 8270C
# Column to be used to flag recovery and RPD values
06/03/2010Page 194 of 623
GC/MS SEMI VOA MATRIX SPIKE DUPLICATE RECOVERY
FORM III
Job No.:Lab Name:
SDG No.:
Level:Matrix:Matrix:
Low
460-13139-1
Lab File ID: p2883.dSolid
Lab ID: 460-13139-5 MSD Client ID: TB-1 2-3 MSD
TestAmerica Edison
COMPOUND
SPIKE
ADDED CONCENTRATION %
REC
%
RPD
QC LIMITS
RPD REC (ug/Kg) (ug/Kg)
#
MSD MSD
7120 5170 30 54-115Phenol 573
7120 5350 30 56-1102-Chlorophenol 175
7120 5620 30 55-1012-Nitrophenol 379
7120 5370 30 56-1122,4-Dimethylphenol 475
7120 5440 30 58-1152,4-Dichlorophenol 476
7120 5690 30 55-1174-Chloro-3-methylphenol 780
7120 4670 30 53-1182,4,6-Trichlorophenol 266
7120 1100 30 10-1292,4-Dinitrophenol NC0U F
7120 4630 30 45-1144-Nitrophenol 065
7120 1100 30 10-1104,6-Dinitro-2-methylphenol NC0U F
7120 1530 30 19-113Pentachlorophenol 421
3560 2660 30 40-84N-Nitrosodimethylamine 175
3560 3150 30 44-101Bis(2-chloroethyl)ether 288
3560 2390 30 47-841,3-Dichlorobenzene 267
3560 2440 30 47-851,4-Dichlorobenzene 069
3560 2560 30 48-871,2-Dichlorobenzene 172
3560 3100 30 42-107N-Nitrosodi-n-propylamine 587
3560 2420 30 45-90Hexachloroethane 268
3560 2700 30 42-106Nitrobenzene 076
3560 2900 30 48-97Isophorone 381
3560 2950 30 51-100Bis(2-chloroethoxy)methane 383
3560 2770 30 48-941,2,4-Trichlorobenzene 078
3560 2780 30 53-94Naphthalene 178
3560 2720 30 45-98Hexachlorobutadiene 376
3560 3150 30 24-98Hexachlorocyclopentadiene 489
3560 2860 30 51-1022-Chloronaphthalene 180
3560 3060 30 52-112Dimethyl phthalate 186
3560 2940 30 51-103Acenaphthylene 183
3560 3200 30 51-1152,6-Dinitrotoluene 090
3560 2970 30 46-100Acenaphthene 083
3560 3150 30 53-1102,4-Dinitrotoluene 188
3560 3030 30 52-114Diethyl phthalate 185
3560 3050 30 50-1064-Chlorophenyl phenyl ether 186
3560 3020 30 51-108Fluorene 285
3560 3320 30 49-106N-Nitrosodiphenylamine 093
3560 3130 30 44-1024-Bromophenyl phenyl ether 188
3560 3110 30 43-104Hexachlorobenzene 187
3560 3030 30 48-108Phenanthrene 385
3560 3040 30 50-107Anthracene 285
3560 3160 30 50-108Di-n-butyl phthalate 689
3560 3230 30 49-108Fluoranthene 691
3560 2980 30 49-116Pyrene 484
FORM III 8270C
# Column to be used to flag recovery and RPD values
06/03/2010Page 195 of 623
GC/MS SEMI VOA MATRIX SPIKE DUPLICATE RECOVERY
FORM III
Job No.:Lab Name:
SDG No.:
Level:Matrix:Matrix:
Low
460-13139-1
Lab File ID: p2883.dSolid
Lab ID: 460-13139-5 MSD Client ID: TB-1 2-3 MSD
TestAmerica Edison
COMPOUND
SPIKE
ADDED CONCENTRATION %
REC
%
RPD
QC LIMITS
RPD REC (ug/Kg) (ug/Kg)
#
MSD MSD
3560 131 30 10-61Benzidine 384J F
3560 3120 30 49-117Butyl benzyl phthalate 188
3560 3180 30 24-1053,3'-Dichlorobenzidine 289
3560 3030 30 46-112Benzo[a]anthracene 185
3560 3080 30 45-114Chrysene 087
3560 3130 30 49-119Bis(2-ethylhexyl) phthalate 188
3560 3150 30 40-106Di-n-octyl phthalate 288
3560 3220 30 33-96Benzo[b]fluoranthene 291
3560 3180 30 35-115Benzo[k]fluoranthene 389
3560 2720 30 36-89Benzo[a]pyrene 277
3560 3150 30 43-109Indeno[1,2,3-cd]pyrene 188
3560 3030 30 43-107Dibenz(a,h)anthracene 185
3560 3170 30 43-106Benzo[g,h,i]perylene 289
3560 2800 30 45-102bis (2-chloroisopropyl) ether 079
FORM III 8270C
# Column to be used to flag recovery and RPD values
06/03/2010Page 196 of 623
FORM IV
GC/MS SEMI VOA METHOD BLANK SUMMARY
Lab Name:
SDG No.:
Job No.: 460-13139-1TestAmerica Edison
Instrument ID:
Level:(Low/Med)
Date Extracted:
Date Analyzed: 05/18/2010 10:57
05/17/2010 09:00
Low
BNAMS10
Lab File ID: p2879.d Lab Sample ID: MB 460-37564/1-A
Matrix: Solid
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:
LAB SAMPLE ID
LAB
FILE ID DATE ANALYZEDCLIENT SAMPLE ID
05/18/2010 11:25p2880.dLCS 460-37564/2-A
05/18/2010 11:52p2881.d460-13139-5TB-1 2-3
05/18/2010 12:18p2882.d460-13139-5 MSTB-1 2-3 MS
05/18/2010 12:46p2883.d460-13139-5 MSDTB-1 2-3 MSD
05/18/2010 15:00p2888.d460-13139-2TB-3 6-7
05/18/2010 19:58p2899.d460-13139-7TB-5 3-4
05/18/2010 20:25p2900.d460-13139-4TB-2 5-6
FORM IV 8270C
06/03/2010Page 197 of 623
FORM V
DECAFLUOROTRIPHENYLPHOSPHINE (DFTPP)
Lab Name:
SDG No.:
Job No.: 460-13139-1
DFTPP Injection Date: 05/11/2010Lab File ID:
Instrument ID: DFTPP Injection Time: 13:45
p2720.d
BNAMS10
M/E ION ABUNDANCE CRITERIA% RELATIVEABUNDANCE
Analysis Batch No.: 37184
51 30.0 - 60.0 % of mass 198 36.5
68 Less than 2.0 % of mass 69 0.0 (0.0)1
69 Mass 69 relative abundance 42.0
70 Less than 2.0 % of mass 69 0.0 (0.0)1
127 40.0 - 60.0 % of mass 198 58.3
197 Less than 1.0 % of mass 198 0.0
198 Base Peak, 100 % relative abundance 100.0
199 5.0- 9.0 % of mass 198 7.0
275 10.0 - 30.0 % of mass 198 25.9
365 Greater than 1.0 % of mass 198 3.2
441 Present but less than mass 443 12.5
442 Greater than 40.0 % of mass 198 84.3
443 17.0 - 23.0 % of mass 442 16.9 (20.0)2
1-Value is % mass 69 2-Value is % mass 442
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:
GC/MS SEMI VOA INSTRUMENT PERFORMANCE CHECK
TestAmerica Edison
CLIENT SAMPLE IDLAB
FILE IDLAB SAMPLE IDDATE
ANALYZEDTIME
ANALYZED
p2721.d 05/11/2010 14:17ICIS 460-37184/2
p2722.d 05/11/2010 14:43IC 460-37184/3
p2723.d 05/11/2010 15:10IC 460-37184/4
p2724.d 05/11/2010 15:36IC 460-37184/5
p2725.d 05/11/2010 16:03IC 460-37184/6
p2726.d 05/11/2010 16:30IC 460-37184/7
FORM V 8270C 06/03/2010Page 198 of 623
FORM V
DECAFLUOROTRIPHENYLPHOSPHINE (DFTPP)
Lab Name:
SDG No.:
Job No.: 460-13139-1
DFTPP Injection Date: 05/18/2010Lab File ID:
Instrument ID: DFTPP Injection Time: 10:12
p2877.d
BNAMS10
M/E ION ABUNDANCE CRITERIA% RELATIVEABUNDANCE
Analysis Batch No.: 37818
51 30.0 - 60.0 % of mass 198 33.4
68 Less than 2.0 % of mass 69 0.0 (0.0)1
69 Mass 69 relative abundance 37.4
70 Less than 2.0 % of mass 69 0.0 (0.0)1
127 40.0 - 60.0 % of mass 198 54.9
197 Less than 1.0 % of mass 198 0.0
198 Base Peak, 100 % relative abundance 100.0
199 5.0- 9.0 % of mass 198 7.0
275 10.0 - 30.0 % of mass 198 27.1
365 Greater than 1.0 % of mass 198 3.6
441 Present but less than mass 443 14.4
442 Greater than 40.0 % of mass 198 101.8
443 17.0 - 23.0 % of mass 442 19.7 (19.3)2
1-Value is % mass 69 2-Value is % mass 442
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:
GC/MS SEMI VOA INSTRUMENT PERFORMANCE CHECK
TestAmerica Edison
CLIENT SAMPLE IDLAB
FILE IDLAB SAMPLE IDDATE
ANALYZEDTIME
ANALYZED
p2878.d 05/18/2010 10:30CCVIS 460-37818/2
p2879.d 05/18/2010 10:57MB 460-37564/1-A
p2880.d 05/18/2010 11:25LCS 460-37564/2-A
TB-1 2-3 p2881.d 05/18/2010 11:52460-13139-5
TB-1 2-3 MS p2882.d 05/18/2010 12:18460-13139-5 MS
TB-1 2-3 MSD p2883.d 05/18/2010 12:46460-13139-5 MSD
TB-3 6-7 p2888.d 05/18/2010 15:00460-13139-2
TB-5 3-4 p2899.d 05/18/2010 19:58460-13139-7
TB-2 5-6 p2900.d 05/18/2010 20:25460-13139-4
FORM V 8270C 06/03/2010Page 199 of 623
GC/MS SEMI VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY
Lab Name: Job No.:
SDG No.:
FORM VIII
TestAmerica Edison 460-13139-1
Sample No.: CCVIS 460-37818/2 Date Analyzed: 05/18/2010 10:30
Lab File ID (Standard): p2878.d
Instrument ID: BNAMS10 GC Column: Rtx-5MS ID: 0.25(mm)
Heated Purge: (Y/N) N
Calibration ID: 6144
AREA # RT # AREA RT # AREA # RT ##
DCB NPT ANT
UPPER LIMIT
LOWER LIMIT
379576
94894 307798
1231190
149907
599628
4.21 5.51 7.2612/24 HOUR STD
4.71
3.71
6.01
5.01
7.76
6.76
189788 615595 299814
LAB SAMPLE ID CLIENT SAMPLE ID
MB 460-37564/1-A 194268 691224 369280 4.21 5.50 7.26
LCS 460-37564/2-A 175899 596977 306055 4.21 5.50 7.26
460-13139-5 TB-1 2-3 178089 635778 340945 4.21 5.50 7.26
460-13139-5 MS TB-1 2-3 MS 181935 635955 330807 4.21 5.50 7.26
460-13139-5 MSD TB-1 2-3 MSD 176230 597654 296797 4.21 5.50 7.26
460-13139-2 TB-3 6-7 179231 625848 328055 4.21 5.50 7.26
460-13139-7 TB-5 3-4 166401 504685 215742 4.21 5.50 7.26
460-13139-4 TB-2 5-6 184940 594577 269984 4.21 5.50 7.26
DCB = 1,4-Dichlorobenzene-d4
NPT = Naphthalene-d8
ANT = Acenaphthene-d10
Area Limit = 50%-200% of internal standard area
RT Limit = ± 0.5 minutes of internal standard RT
# Column used to flag values outside QC limits
FORM VIII 8270C
06/03/2010Page 200 of 623
GC/MS SEMI VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY
Lab Name: Job No.:
SDG No.:
FORM VIII
TestAmerica Edison 460-13139-1
Sample No.: CCVIS 460-37818/2 Date Analyzed: 05/18/2010 10:30
Lab File ID (Standard): p2878.d
Instrument ID: BNAMS10 GC Column: Rtx-5MS ID: 0.25(mm)
Heated Purge: (Y/N) N
Calibration ID: 6144
AREA # RT # AREA RT # AREA # RT ##
PHN CRY PRY
UPPER LIMIT
LOWER LIMIT
775318
193830 110816
443264
73549
294196
8.73 11.49 13.4012/24 HOUR STD
9.23
8.23
11.99
10.99
13.90
12.90
387659 221632 147098
LAB SAMPLE ID CLIENT SAMPLE ID
MB 460-37564/1-A 486284 267422 185780 8.73 11.48 13.40
LCS 460-37564/2-A 392818 220418 164936 8.73 11.49 13.40
460-13139-5 TB-1 2-3 465487 282918 186032 8.73 11.49 13.40
460-13139-5 MS TB-1 2-3 MS 406314 207230 152357 8.73 11.49 13.40
460-13139-5 MSD TB-1 2-3 MSD 366053 206096 152929 8.73 11.49 13.40
460-13139-2 TB-3 6-7 434676 225779 149045 8.73 11.48 13.40
460-13139-7 TB-5 3-4 245292 175541 185914 8.73 11.49 13.41
460-13139-4 TB-2 5-6 309230 191087 186699 8.73 11.49 13.41
PHN = Phenanthrene-d10
CRY = Chrysene-d12
PRY = Perylene-d12
Area Limit = 50%-200% of internal standard area
RT Limit = ± 0.5 minutes of internal standard RT
# Column used to flag values outside QC limits
FORM VIII 8270C
06/03/2010Page 201 of 623
FORM IForm 1GC/MS SEMI VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-3 6-7
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-2
Matrix: p2888.dLab File ID:
Date Collected:8270CAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 09:45
Level: (low/med)
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Analyzed:
Date Extracted:
Dilution Factor:
Extract. Method: 05/17/2010 09:00
1
3541
05/18/2010 15:00
Low
N
1(mL)
% Moisture: 18.8
Sample wt/vol: 15.00(g)
Analysis Batch No.: 37818 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Phenol108-95-2 410 410 50U
2-Chlorophenol95-57-8 410 410 54U
2-Nitrophenol88-75-5 410 410 67U
2,4-Dimethylphenol105-67-9 410 410 65U
2,4-Dichlorophenol120-83-2 410 410 65U
4-Chloro-3-methylphenol59-50-7 410 410 68U
2,4,6-Trichlorophenol88-06-2 410 410 73U
2,4-Dinitrophenol51-28-5 1200 1200 86U
4-Nitrophenol100-02-7 1200 1200 100U
4,6-Dinitro-2-methylphenol534-52-1 1200 1200 190U
Pentachlorophenol87-86-5 1200 1200 200U
N-Nitrosodimethylamine62-75-9 410 410 41U
Bis(2-chloroethyl)ether111-44-4 41 41 8.5U
1,3-Dichlorobenzene541-73-1 410 410 56U
1,4-Dichlorobenzene106-46-7 410 410 61U
1,2-Dichlorobenzene95-50-1 410 410 65U
N-Nitrosodi-n-propylamine621-64-7 41 41 5.4U
Hexachloroethane67-72-1 41 41 6.9U
Nitrobenzene98-95-3 41 41 9.1U
Isophorone78-59-1 410 410 47U
Bis(2-chloroethoxy)methane111-91-1 410 410 58U
1,2,4-Trichlorobenzene120-82-1 41 41 6.7U
Naphthalene91-20-3 410 410 60U
Hexachlorobutadiene87-68-3 83 83 17U
Hexachlorocyclopentadiene77-47-4 410 410 120U
2-Chloronaphthalene91-58-7 410 410 58U
Dimethyl phthalate131-11-3 410 410 55U
Acenaphthylene208-96-8 410 410 58U
2,6-Dinitrotoluene606-20-2 83 83 10U
Acenaphthene83-32-9 410 410 58U
2,4-Dinitrotoluene121-14-2 83 83 12U
Diethyl phthalate84-66-2 410 410 55U
4-Chlorophenyl phenyl ether7005-72-3 410 410 70U
Fluorene86-73-7 410 410 69U
FORM I 8270C
06/03/2010Page 202 of 623
FORM IForm 1GC/MS SEMI VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-3 6-7
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-2
Matrix: p2888.dLab File ID:
Date Collected:8270CAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 09:45
Level: (low/med)
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Analyzed:
Date Extracted:
Dilution Factor:
Extract. Method: 05/17/2010 09:00
1
3541
05/18/2010 15:00
Low
N
1(mL)
% Moisture: 18.8
Sample wt/vol: 15.00(g)
Analysis Batch No.: 37818 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
N-Nitrosodiphenylamine86-30-6 410 410 66U
4-Bromophenyl phenyl ether101-55-3 410 410 73U
Hexachlorobenzene118-74-1 41 41 5.7U
Phenanthrene85-01-8 410 410 71U
Anthracene120-12-7 410 410 72U
Di-n-butyl phthalate84-74-2 410 410 62U
Fluoranthene206-44-0 410 410 68U
Pyrene129-00-0 410 410 70U
Benzidine92-87-5 410 410 87U *
Butyl benzyl phthalate85-68-7 410 410 48U
3,3'-Dichlorobenzidine91-94-1 830 830 90U
Benzo[a]anthracene56-55-3 28 41 7.5J
Chrysene218-01-9 410 410 59U
Bis(2-ethylhexyl) phthalate117-81-7 120 410 54J
Di-n-octyl phthalate117-84-0 410 410 48U
Benzo[b]fluoranthene205-99-2 41 41 6.1U
Benzo[k]fluoranthene207-08-9 41 41 5.7U
Benzo[a]pyrene50-32-8 41 41 5.0U
Indeno[1,2,3-cd]pyrene193-39-5 41 41 6.5U
Dibenz(a,h)anthracene53-70-3 41 41 4.9U
Benzo[g,h,i]perylene191-24-2 410 410 43U
bis (2-chloroisopropyl) ether108-60-1 410 410 53U
SURROGATE %RECCAS NO. LIMITS Q
4165-60-0 Nitrobenzene-d5 80 38-105
4165-62-2 Phenol-d5 82 41-118
1718-51-0 Terphenyl-d14 100 16-151
118-79-6 2,4,6-Tribromophenol 78 10-120
367-12-4 2-Fluorophenol 76 37-125
321-60-8 2-Fluorobiphenyl 78 40-109
FORM I 8270C
06/03/2010Page 203 of 623
FORM IForm 1GC/MS SEMI VOA ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Client Sample ID:
Lab Name: Job No.:
TB-3 6-7
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-2
Matrix: p2888.dLab File ID:
Date Collected:8270CAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 09:45
Level: (low/med)
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Analyzed:
Date Extracted:
Dilution Factor:
Extract. Method: 05/17/2010 09:00
1
3541
05/18/2010 15:00
Low
N
1(mL)
% Moisture: 18.8
Sample wt/vol: 15.00(g)
Analysis Batch No.: 37818 ug/KgUnits:
Number TICs Found: TIC Result Total: 00
QRTCOMPOUND NAME RESULTCAS NO.
Tentatively Identified Compound None
FORM I-TIC 8270C
06/03/2010Page 204 of 623
Data File: /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2888.d Report Date: 19-May-2010 14:53
TestAmerica
SEMI-VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2888.dLab Smp Id: 460-13139-E-2-E Client Smp ID: TB-3 6-7Inj Date : 18-MAY-2010 15:00 Operator : BNAMS 4 Inst ID: BNAMS10.iSmp Info : 460-13139-E-2-EMisc Info : 460-13139-E-2-EComment : Method : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/8270C_08SP.mMeth Date : 18-May-2010 11:53 czhao Quant Type: ISTDCal Date : 11-MAY-2010 16:30 Cal File: p2726.dAls bottle: 12 Dil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd1
Concentration Formula: Amt * DF * Uf*1000*Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorUf 1.00000 ng unit correction factorVt 1.00000 Volume of final extract (ml)Ws 15.00000 Weight of sample extracted (g)M 18.78882 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE (ug/ml) (ug/Kg)
========================== ==== == ====== ====== ======== ======= =======
$ 16 2-Fluorophenol (SUR) 112 2.963 2.928 (0.704) 455839 75.5200 6200
$ 17 Phenol-d5 (SUR) 99 3.850 3.862 (0.915) 554955 81.5177 6700
* 79 1,4-Dichlorobenzene-d4 152 4.208 4.214 (1.000) 179231 40.0000
$ 76 Nitrobenzene-d5 (SUR) 82 4.767 4.778 (0.867) 243860 39.9973 3300
* 80 Naphthalene-d8 136 5.495 5.507 (1.000) 625848 40.0000
$ 77 2-Fluorobiphenyl (SUR) 172 6.588 6.594 (0.908) 467628 39.0913 3200
* 82 Acenaphthene-d10 164 7.258 7.264 (1.000) 328055 40.0000
$ 18 2,4,6-Tribromophenol (SUR) 330 8.039 8.045 (1.108) 84491 77.7534 6400
* 83 Phenanthrene-d10 188 8.727 8.733 (1.000) 434676 40.0000
52 Phenanthrene 178 8.744 8.756 (1.002) 6679 0.54067 44(a)
56 Fluoranthene 202 9.919 9.925 (1.137) 7957 0.81229 67(a)
57 Pyrene 202 10.143 10.149 (0.883) 7245 0.76175 62(a)
$ 78 Terphenyl-d14 244 10.307 10.307 (0.898) 296258 49.8339 4100
06/03/2010Page 205 of 623
Data File: /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2888.d Report Date: 19-May-2010 14:53
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE (ug/ml) (ug/Kg)
========================== ==== == ====== ====== ======== ======= =======
61 Benzo(a)anthracene 228 11.471 11.476 (0.999) 2160 0.34075 28(aH)
* 81 Chrysene-d12 240 11.482 11.494 (1.000) 225779 40.0000
62 Chrysene 228 11.512 11.524 (1.003) 2636 0.45893 38(a)
63 bis(2-Ethylhexyl)phthalate 149 11.523 11.524 (1.004) 6582 1.40436 120(a)
* 84 Perylene-d12 264 13.398 13.404 (1.000) 149045 40.0000
QC Flag Legend
a - Target compound detected but, quantitated amountBelow Limit Of Quantitation(BLOQ).
H - Operator selected an alternate compound hit.
06/03/2010Page 206 of 623
Data File: /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2888.d Report Date: 19-May-2010 14:53
TestAmerica
SEMI-VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2888.dLab Smp Id: 460-13139-E-2-E Client Smp ID: TB-3 6-7Inj Date : 18-MAY-2010 15:00 Operator : BNAMS 4 Inst ID: BNAMS10.iSmp Info : 460-13139-E-2-EMisc Info : 460-13139-E-2-EComment : Method : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/8270C_08SP.mMeth Date : 18-May-2010 11:53 czhao Quant Type: ISTDCal Date : 11-MAY-2010 16:30 Cal File: p2726.dAls bottle: 12 Dil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd1
- NO TENTATIVELY IDENTIFIED COMPOUNDS -
06/03/2010Page 207 of 623
Data File: p2888.d
Date: 18-MAY-2010 15:00
Client ID: TB-3 6-7 Instrument: BNAMS10.i
Sample Info: 460-13139-E-2-E Operator: BNAMS 4
06/03/2010Page 208 of 623
Data File: p2888.d
Date: 18-MAY-2010 15:00
Client ID: TB-3 6-7 Instrument: BNAMS10.i
Sample Info: 460-13139-E-2-E Operator: BNAMS 4
61 Benzo(a)anthracene
06/03/2010Page 209 of 623
Data File: p2888.d
Date: 18-MAY-2010 15:00
Client ID: TB-3 6-7 Instrument: BNAMS10.i
Sample Info: 460-13139-E-2-E Operator: BNAMS 4
63 bis(2-Ethylhexyl)phthalate
06/03/2010Page 210 of 623
FORM IForm 1GC/MS SEMI VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-2 5-6
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-4
Matrix: p2900.dLab File ID:
Date Collected:8270CAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 10:45
Level: (low/med)
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Analyzed:
Date Extracted:
Dilution Factor:
Extract. Method: 05/17/2010 09:00
1
3541
05/18/2010 20:25
Low
N
1(mL)
% Moisture: 12.8
Sample wt/vol: 15.05(g)
Analysis Batch No.: 37818 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Phenol108-95-2 380 380 46U
2-Chlorophenol95-57-8 380 380 51U
2-Nitrophenol88-75-5 380 380 62U
2,4-Dimethylphenol105-67-9 380 380 61U
2,4-Dichlorophenol120-83-2 380 380 61U
4-Chloro-3-methylphenol59-50-7 380 380 63U
2,4,6-Trichlorophenol88-06-2 380 380 68U
2,4-Dinitrophenol51-28-5 1100 1100 80U
4-Nitrophenol100-02-7 1100 1100 97U
4,6-Dinitro-2-methylphenol534-52-1 1100 1100 180U
Pentachlorophenol87-86-5 1100 1100 180U
N-Nitrosodimethylamine62-75-9 380 380 39U
Bis(2-chloroethyl)ether111-44-4 38 38 7.9U
1,3-Dichlorobenzene541-73-1 380 380 52U
1,4-Dichlorobenzene106-46-7 380 380 56U
1,2-Dichlorobenzene95-50-1 380 380 60U
N-Nitrosodi-n-propylamine621-64-7 38 38 5.0U
Hexachloroethane67-72-1 38 38 6.4U
Nitrobenzene98-95-3 38 38 8.5U
Isophorone78-59-1 380 380 43U
Bis(2-chloroethoxy)methane111-91-1 380 380 54U
1,2,4-Trichlorobenzene120-82-1 38 38 6.2U
Naphthalene91-20-3 380 380 55U
Hexachlorobutadiene87-68-3 77 77 15U
Hexachlorocyclopentadiene77-47-4 380 380 110U
2-Chloronaphthalene91-58-7 380 380 53U
Dimethyl phthalate131-11-3 380 380 51U
Acenaphthylene208-96-8 97 380 54J
2,6-Dinitrotoluene606-20-2 77 77 9.6U
Acenaphthene83-32-9 110 380 54J
2,4-Dinitrotoluene121-14-2 77 77 11U
Diethyl phthalate84-66-2 380 380 51U
4-Chlorophenyl phenyl ether7005-72-3 380 380 65U
Fluorene86-73-7 150 380 64J
FORM I 8270C
06/03/2010Page 211 of 623
FORM IForm 1GC/MS SEMI VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-2 5-6
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-4
Matrix: p2900.dLab File ID:
Date Collected:8270CAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 10:45
Level: (low/med)
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Analyzed:
Date Extracted:
Dilution Factor:
Extract. Method: 05/17/2010 09:00
1
3541
05/18/2010 20:25
Low
N
1(mL)
% Moisture: 12.8
Sample wt/vol: 15.05(g)
Analysis Batch No.: 37818 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
N-Nitrosodiphenylamine86-30-6 380 380 62U
4-Bromophenyl phenyl ether101-55-3 380 380 67U
Hexachlorobenzene118-74-1 38 38 5.2U
Phenanthrene85-01-8 1500 380 66
Anthracene120-12-7 240 380 67J
Di-n-butyl phthalate84-74-2 380 380 58U
Fluoranthene206-44-0 1800 380 63
Pyrene129-00-0 1500 380 65
Benzidine92-87-5 380 380 80U *
Butyl benzyl phthalate85-68-7 380 380 44U
3,3'-Dichlorobenzidine91-94-1 770 770 84U
Benzo[a]anthracene56-55-3 710 38 7.0
Chrysene218-01-9 960 380 55
Bis(2-ethylhexyl) phthalate117-81-7 210 380 50J
Di-n-octyl phthalate117-84-0 380 380 45U
Benzo[b]fluoranthene205-99-2 820 38 5.6
Benzo[k]fluoranthene207-08-9 300 38 5.3
Benzo[a]pyrene50-32-8 690 38 4.7
Indeno[1,2,3-cd]pyrene193-39-5 610 38 6.0
Dibenz(a,h)anthracene53-70-3 130 38 4.5
Benzo[g,h,i]perylene191-24-2 680 380 40
bis (2-chloroisopropyl) ether108-60-1 380 380 50U
SURROGATE %RECCAS NO. LIMITS Q
4165-60-0 Nitrobenzene-d5 59 38-105
4165-62-2 Phenol-d5 60 41-118
1718-51-0 Terphenyl-d14 74 16-151
118-79-6 2,4,6-Tribromophenol 53 10-120
367-12-4 2-Fluorophenol 55 37-125
321-60-8 2-Fluorobiphenyl 67 40-109
FORM I 8270C
06/03/2010Page 212 of 623
FORM IForm 1GC/MS SEMI VOA ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Client Sample ID:
Lab Name: Job No.:
TB-2 5-6
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-4
Matrix: p2900.dLab File ID:
Date Collected:8270CAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 10:45
Level: (low/med)
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Analyzed:
Date Extracted:
Dilution Factor:
Extract. Method: 05/17/2010 09:00
1
3541
05/18/2010 20:25
Low
N
1(mL)
% Moisture: 12.8
Sample wt/vol: 15.05(g)
Analysis Batch No.: 37818 ug/KgUnits:
Number TICs Found: TIC Result Total: 38009
QRTCOMPOUND NAME RESULTCAS NO.
C15H12 PAH-1 400 9.23 T J
C15H12 PAH-2 440 9.25 T J
C15H10/C15H12 PAHs 550 9.33 T J
C15H12 PAH-3 320 9.36 T J
84-65-1 9,10-Anthracenedione 510 9.54 T J N
C16H14 PAH 330 9.77 T J
C17H12 PAH-1 370 10.49 T J
C17H12 PAH-2 380 10.60 T J
C20H12 PAH 500 13.25 T J
FORM I-TIC 8270C
06/03/2010Page 213 of 623
Data File: /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2900.d Report Date: 19-May-2010 16:02
TestAmerica
SEMI-VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2900.dLab Smp Id: 460-13139-E-4-E Client Smp ID: TB-2 5-6Inj Date : 18-MAY-2010 20:25 Operator : BNAMS 4 Inst ID: BNAMS10.iSmp Info : 460-13139-E-4-EMisc Info : 460-13139-E-4-EComment : Method : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/8270C_08SP.mMeth Date : 18-May-2010 11:53 czhao Quant Type: ISTDCal Date : 11-MAY-2010 16:30 Cal File: p2726.dAls bottle: 24 Dil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd1
Concentration Formula: Amt * DF * Uf*1000*Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorUf 1.00000 ng unit correction factorVt 1.00000 Volume of final extract (ml)Ws 15.05000 Weight of sample extracted (g)M 12.77533 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE (ug/ml) (ug/Kg)
========================== ==== == ====== ====== ======== ======= =======
$ 16 2-Fluorophenol (SUR) 112 2.951 2.928 (0.701) 343758 55.1932 4200
$ 17 Phenol-d5 (SUR) 99 3.844 3.862 (0.913) 424868 60.4826 4600
* 79 1,4-Dichlorobenzene-d4 152 4.208 4.214 (1.000) 184940 40.0000
$ 76 Nitrobenzene-d5 (SUR) 82 4.761 4.778 (0.866) 172242 29.7365 2300
* 80 Naphthalene-d8 136 5.495 5.507 (1.000) 594577 40.0000
31 Naphthalene 128 5.513 5.525 (1.003) 10806 0.64724 49(a)
34 2-Methylnaphthalene 142 6.218 6.224 (1.132) 6613 0.66751 51(a)
120 1-Methylnaphthalene 142 6.318 6.324 (1.150) 7956 0.81540 62(a)
$ 77 2-Fluorobiphenyl (SUR) 172 6.588 6.594 (0.908) 327731 33.2894 2500
125 1,3-Dimethylnaphthalene 156 6.923 6.929 (0.954) 8728 1.29127 98(a)
39 Acenaphthylene 152 7.117 7.123 (0.981) 16669 1.27219 97(a)
* 82 Acenaphthene-d10 164 7.258 7.264 (1.000) 269984 40.0000
42 Acenaphthene 154 7.287 7.299 (1.004) 10589 1.44946 110(a)
06/03/2010Page 214 of 623
Data File: /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2900.d Report Date: 19-May-2010 16:02
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE (ug/ml) (ug/Kg)
========================== ==== == ====== ====== ======== ======= =======
43 Dibenzofuran 168 7.463 7.469 (1.028) 7214 0.68263 52(a)
47 Fluorene 166 7.798 7.810 (1.074) 15499 1.99010 150(a)
$ 18 2,4,6-Tribromophenol (SUR) 330 8.039 8.045 (1.108) 47480 53.0919 4000
* 83 Phenanthrene-d10 188 8.727 8.733 (1.000) 309230 40.0000
52 Phenanthrene 178 8.750 8.756 (1.003) 168574 19.1821 1500
53 Anthracene 178 8.797 8.803 (1.008) 27584 3.13888 240(a)
54 Carbazole 167 8.956 8.962 (1.026) 11111 1.50609 110(a)
56 Fluoranthene 202 9.925 9.925 (1.137) 164552 23.6129 1800
57 Pyrene 202 10.148 10.149 (0.883) 161026 20.0043 1500
$ 78 Terphenyl-d14 244 10.307 10.307 (0.897) 185531 36.8743 2800
61 Benzo(a)anthracene 228 11.476 11.476 (0.999) 50160 9.34969 710
* 81 Chrysene-d12 240 11.488 11.494 (1.000) 191087 40.0000
62 Chrysene 228 11.518 11.524 (1.003) 61507 12.6525 960
63 bis(2-Ethylhexyl)phthalate 149 11.523 11.524 (1.003) 10785 2.71890 210(a)
65 Benzo(b)fluoranthene 252 12.881 12.881 (0.961) 56029 10.6991 820
66 Benzo(k)fluoranthene 252 12.916 12.922 (0.963) 22834 3.98923 300(H)
67 Benzo(a)pyrene 252 13.327 13.327 (0.994) 43147 9.00779 690
* 84 Perylene-d12 264 13.409 13.404 (1.000) 186699 40.0000
68 Indeno(1,2,3-cd)pyrene 276 14.908 14.908 (1.112) 31411 8.07262 610
69 Dibenz(a,h)anthracene 278 14.937 14.943 (1.114) 6725 1.70164 130
70 Benzo(g,h,i)perylene 276 15.319 15.319 (1.142) 35090 8.91008 680
QC Flag Legend
a - Target compound detected but, quantitated amountBelow Limit Of Quantitation(BLOQ).
H - Operator selected an alternate compound hit.
06/03/2010Page 215 of 623
Data File: /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2900.d Report Date: 19-May-2010 16:02
TestAmerica
SEMI-VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2900.dLab Smp Id: 460-13139-E-4-E Client Smp ID: TB-2 5-6Inj Date : 18-MAY-2010 20:25 Operator : BNAMS 4 Inst ID: BNAMS10.iSmp Info : 460-13139-E-4-EMisc Info : 460-13139-E-4-EComment : Method : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/8270C_08SP.mMeth Date : 18-May-2010 11:53 czhao Quant Type: ISTDCal Date : 11-MAY-2010 16:30 Cal File: p2726.dAls bottle: 24 Dil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd1
Concentration Formula: Amt * DF * Uf*1000*Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorUf 1.00000 ng unit correction factorVt 1.00000 Volume of final extract (ml)Ws 15.05000 Weight of sample extracted (g)M 12.77533 % Moisture
Cpnd Variable Local Compound Variable
ISTD RT AREA AMOUNT======== ==== ====== ======
* 83 Phenanthrene-d10 8.727 825818 40.000
* 81 Chrysene-d12 11.488 685646 40.000
* 84 Perylene-d12 13.409 567337 40.000
CONCENTRATIONS QUANT
RT AREA ON-COL(ug/ml) FINAL(ug/Kg) QUAL LIBRARY LIB ENTRY CPND #
==== ==== ============= ============ ==== ======= ========= ======
C15H12 PAH-1 CAS #:
9.226 108287 5.24507341 400 0 0 83
06/03/2010Page 216 of 623
Data File: /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2900.d Report Date: 19-May-2010 16:02
CONCENTRATIONS QUANT
RT AREA ON-COL(ug/ml) FINAL(ug/Kg) QUAL LIBRARY LIB ENTRY CPND #
==== ==== ============= ============ ==== ======= ========= ======
C15H12 PAH-2 CAS #:
9.250 120317 5.82777654 440 0 0 83
C15H10/C15H12 PAHs CAS #:
9.332 149704 7.25117045 550 0 0 83
C15H12 PAH-3 CAS #:
9.355 87084 4.21807501 320 0 0 83
9,10-Anthracenedione CAS #: 84-65-1
9.537 136921 6.63203860 500 98 NIST02.l 61654 83
C16H14 PAH CAS #:
9.772 88982 4.31002595 330 0 0 83
C17H12 PAH-1 CAS #:
10.489 82559 4.81641662 370 0 0 81
C17H12 PAH-2 CAS #:
10.601 85236 4.97259894 380 0 0 81
C20H12 PAH CAS #:
13.251 93427 6.58707981 500 0 0 84
06/03/2010Page 217 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
06/03/2010Page 218 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
39 Acenaphthylene
06/03/2010Page 219 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
42 Acenaphthene
06/03/2010Page 220 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
47 Fluorene
06/03/2010Page 221 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
52 Phenanthrene
06/03/2010Page 222 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
53 Anthracene
06/03/2010Page 223 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
56 Fluoranthene
06/03/2010Page 224 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
57 Pyrene
06/03/2010Page 225 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
61 Benzo(a)anthracene
06/03/2010Page 226 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
62 Chrysene
06/03/2010Page 227 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
63 bis(2-Ethylhexyl)phthalate
06/03/2010Page 228 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
65 Benzo(b)fluoranthene
06/03/2010Page 229 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
66 Benzo(k)fluoranthene
06/03/2010Page 230 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
67 Benzo(a)pyrene
06/03/2010Page 231 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
68 Indeno(1,2,3-cd)pyrene
06/03/2010Page 232 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
69 Dibenz(a,h)anthracene
06/03/2010Page 233 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
70 Benzo(g,h,i)perylene
06/03/2010Page 234 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
Retention Time: 9.23
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
C15H12 PAH-1
Anthracene, 2-methyl- 613-12-7 NIST02.l 50612 96 C15H12 192
Phenanthrene, 2-methyl- 2531-84-2 NIST02.l 50626 96 C15H12 192
06/03/2010Page 235 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
Retention Time: 9.25
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
C15H12 PAH-2
1H-Cyclopropa[l]phenanthrene,1a,9b 949-41-7 NIST02.l 50641 94 C15H12 192
Phenanthrene, 1-methyl- 832-69-9 NIST02.l 50623 94 C15H12 192
06/03/2010Page 236 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
Retention Time: 9.33
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
C15H10/C15H12 PAHs
6H-Cyclobuta[jk]phenanthrene 83469-43-6 NIST02.l 49336 46 C15H10 190
Anthracene, 1-methyl- 610-48-0 NIST02.l 50617 46 C15H12 192
06/03/2010Page 237 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
Retention Time: 9.36
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
C15H12 PAH-3
Anthracene, 2-methyl- 613-12-7 NIST02.l 50613 74 C15H12 192
Phenanthrene, 1-methyl- 832-69-9 NIST02.l 50630 72 C15H12 192
06/03/2010Page 238 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
Retention Time: 9.54
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
9,10-Anthracenedione 84-65-1 NIST02.l 61654 98 C14H8O2 208
9,10-Anthracenedione 84-65-1 NIST02.l 61655 92 C14H8O2 208
9,10-Anthracenedione 84-65-1 NIST02.l 61653 90 C14H8O2 208
06/03/2010Page 239 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
Retention Time: 9.77
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
C16H14 PAH
Phenanthrene, 2,5-dimethyl- 3674-66-6 NIST02.l 60352 96 C16H14 206
9,10-Dimethylanthracene 781-43-1 NIST02.l 60343 96 C16H14 206
06/03/2010Page 240 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
Retention Time: 10.49
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
C17H12 PAH-1
11H-Benzo[b]fluorene 243-17-4 NIST02.l 67030 90 C17H12 216
11H-Benzo[a]fluorene 238-84-6 NIST02.l 67031 87 C17H12 216
06/03/2010Page 241 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
Retention Time: 10.60
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
C17H12 PAH-2
Fluoranthene, 2-methyl- 33543-31-6 NIST02.l 67037 93 C17H12 216
Pyrene, 4-methyl- 3353-12-6 NIST02.l 67026 92 C17H12 216
06/03/2010Page 242 of 623
Data File: p2900.d
Date: 18-MAY-2010 20:25
Client ID: TB-2 5-6 Instrument: BNAMS10.i
Sample Info: 460-13139-E-4-E Operator: BNAMS 4
Retention Time: 13.25
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
C20H12 PAH
Perylene 198-55-0 NIST02.l 89813 98 C20H12 252
Perylene 198-55-0 NIST02.l 89814 98 C20H12 252
06/03/2010Page 243 of 623
FORM IForm 1GC/MS SEMI VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-1 2-3
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-5
Matrix: p2881.dLab File ID:
Date Collected:8270CAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 11:25
Level: (low/med)
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Analyzed:
Date Extracted:
Dilution Factor:
Extract. Method: 05/17/2010 09:00
1
3541
05/18/2010 11:52
Low
N
1(mL)
% Moisture: 6.5
Sample wt/vol: 15.02(g)
Analysis Batch No.: 37818 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Phenol108-95-2 350 350 43U
2-Chlorophenol95-57-8 350 350 47U
2-Nitrophenol88-75-5 350 350 58U
2,4-Dimethylphenol105-67-9 350 350 57U
2,4-Dichlorophenol120-83-2 350 350 57U
4-Chloro-3-methylphenol59-50-7 350 350 59U
2,4,6-Trichlorophenol88-06-2 350 350 63U
2,4-Dinitrophenol51-28-5 1100 1100 75U
4-Nitrophenol100-02-7 1100 1100 91U
4,6-Dinitro-2-methylphenol534-52-1 1100 1100 170U
Pentachlorophenol87-86-5 1100 1100 170U
N-Nitrosodimethylamine62-75-9 350 350 36U
Bis(2-chloroethyl)ether111-44-4 35 35 7.4U
1,3-Dichlorobenzene541-73-1 350 350 48U
1,4-Dichlorobenzene106-46-7 350 350 53U
1,2-Dichlorobenzene95-50-1 350 350 57U
N-Nitrosodi-n-propylamine621-64-7 35 35 4.7U
Hexachloroethane67-72-1 35 35 6.0U
Nitrobenzene98-95-3 35 35 7.9U
Isophorone78-59-1 350 350 41U
Bis(2-chloroethoxy)methane111-91-1 350 350 50U
1,2,4-Trichlorobenzene120-82-1 35 35 5.8U
Naphthalene91-20-3 350 350 52U
Hexachlorobutadiene87-68-3 72 72 14U
Hexachlorocyclopentadiene77-47-4 350 350 100U
2-Chloronaphthalene91-58-7 350 350 50U
Dimethyl phthalate131-11-3 350 350 48U
Acenaphthylene208-96-8 350 350 51U
2,6-Dinitrotoluene606-20-2 72 72 9.0U
Acenaphthene83-32-9 350 350 50U
2,4-Dinitrotoluene121-14-2 72 72 10U
Diethyl phthalate84-66-2 350 350 47U
4-Chlorophenyl phenyl ether7005-72-3 350 350 61U
Fluorene86-73-7 350 350 60U
FORM I 8270C
06/03/2010Page 244 of 623
FORM IForm 1GC/MS SEMI VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-1 2-3
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-5
Matrix: p2881.dLab File ID:
Date Collected:8270CAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 11:25
Level: (low/med)
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Analyzed:
Date Extracted:
Dilution Factor:
Extract. Method: 05/17/2010 09:00
1
3541
05/18/2010 11:52
Low
N
1(mL)
% Moisture: 6.5
Sample wt/vol: 15.02(g)
Analysis Batch No.: 37818 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
N-Nitrosodiphenylamine86-30-6 350 350 58U
4-Bromophenyl phenyl ether101-55-3 350 350 63U
Hexachlorobenzene118-74-1 35 35 4.9U
Phenanthrene85-01-8 350 350 62U
Anthracene120-12-7 350 350 62U
Di-n-butyl phthalate84-74-2 350 350 54U
Fluoranthene206-44-0 350 350 59U
Pyrene129-00-0 350 350 61U
Benzidine92-87-5 350 350 75U *
Butyl benzyl phthalate85-68-7 350 350 41U
3,3'-Dichlorobenzidine91-94-1 720 720 78U
Benzo[a]anthracene56-55-3 35 35 6.5U
Chrysene218-01-9 350 350 51U
Bis(2-ethylhexyl) phthalate117-81-7 350 350 47U
Di-n-octyl phthalate117-84-0 350 350 42U
Benzo[b]fluoranthene205-99-2 35 35 5.3U
Benzo[k]fluoranthene207-08-9 35 35 4.9U
Benzo[a]pyrene50-32-8 35 35 4.3U
Indeno[1,2,3-cd]pyrene193-39-5 35 35 5.7U
Dibenz(a,h)anthracene53-70-3 35 35 4.3U
Benzo[g,h,i]perylene191-24-2 350 350 37U
bis (2-chloroisopropyl) ether108-60-1 350 350 46U
SURROGATE %RECCAS NO. LIMITS Q
4165-60-0 Nitrobenzene-d5 70 38-105
4165-62-2 Phenol-d5 68 41-118
1718-51-0 Terphenyl-d14 91 16-151
118-79-6 2,4,6-Tribromophenol 93 10-120
367-12-4 2-Fluorophenol 58 37-125
321-60-8 2-Fluorobiphenyl 69 40-109
FORM I 8270C
06/03/2010Page 245 of 623
FORM IForm 1GC/MS SEMI VOA ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Client Sample ID:
Lab Name: Job No.:
TB-1 2-3
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-5
Matrix: p2881.dLab File ID:
Date Collected:8270CAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 11:25
Level: (low/med)
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Analyzed:
Date Extracted:
Dilution Factor:
Extract. Method: 05/17/2010 09:00
1
3541
05/18/2010 11:52
Low
N
1(mL)
% Moisture: 6.5
Sample wt/vol: 15.02(g)
Analysis Batch No.: 37818 ug/KgUnits:
Number TICs Found: TIC Result Total: 00
QRTCOMPOUND NAME RESULTCAS NO.
Tentatively Identified Compound None
FORM I-TIC 8270C
06/03/2010Page 246 of 623
Data File: /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2881.d Report Date: 19-May-2010 10:39
TestAmerica
SEMI-VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2881.dLab Smp Id: 460-13139-E-5-G Client Smp ID: TB-1 2-3Inj Date : 18-MAY-2010 11:52 Operator : BNAMS 4 Inst ID: BNAMS10.iSmp Info : 460-13139-E-5-GMisc Info : 460-13139-E-5-GComment : Method : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/8270C_08SP.mMeth Date : 18-May-2010 11:53 czhao Quant Type: ISTDCal Date : 11-MAY-2010 16:30 Cal File: p2726.dAls bottle: 5 Dil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd1
Concentration Formula: Amt * DF * Uf*1000*Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorUf 1.00000 ng unit correction factorVt 1.00000 Volume of final extract (ml)Ws 15.02000 Weight of sample extracted (g)M 6.50888 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE (ug/ml) (ug/Kg)
========================== ==== == ====== ====== ======== ======= =======
$ 16 2-Fluorophenol (SUR) 112 2.963 2.928 (0.704) 345245 57.5644 4100
$ 17 Phenol-d5 (SUR) 99 3.850 3.862 (0.915) 461525 68.2284 4800
* 79 1,4-Dichlorobenzene-d4 152 4.209 4.214 (1.000) 178089 40.0000
$ 76 Nitrobenzene-d5 (SUR) 82 4.767 4.778 (0.867) 216296 34.9222 2500
* 80 Naphthalene-d8 136 5.495 5.507 (1.000) 635778 40.0000
$ 77 2-Fluorobiphenyl (SUR) 172 6.588 6.594 (0.908) 430194 34.6024 2500
* 82 Acenaphthene-d10 164 7.258 7.264 (1.000) 340945 40.0000
$ 18 2,4,6-Tribromophenol (SUR) 330 8.039 8.045 (1.108) 105146 93.1031 6600
* 83 Phenanthrene-d10 188 8.727 8.733 (1.000) 465487 40.0000
$ 78 Terphenyl-d14 244 10.307 10.307 (0.897) 337666 45.3279 3200
* 81 Chrysene-d12 240 11.488 11.494 (1.000) 282918 40.0000
* 84 Perylene-d12 264 13.404 13.404 (1.000) 186032 40.0000
06/03/2010Page 247 of 623
Data File: /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2881.d Report Date: 19-May-2010 10:39
TestAmerica
SEMI-VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2881.dLab Smp Id: 460-13139-E-5-G Client Smp ID: TB-1 2-3Inj Date : 18-MAY-2010 11:52 Operator : BNAMS 4 Inst ID: BNAMS10.iSmp Info : 460-13139-E-5-GMisc Info : 460-13139-E-5-GComment : Method : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/8270C_08SP.mMeth Date : 18-May-2010 11:53 czhao Quant Type: ISTDCal Date : 11-MAY-2010 16:30 Cal File: p2726.dAls bottle: 5 Dil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd1
- NO TENTATIVELY IDENTIFIED COMPOUNDS -
06/03/2010Page 248 of 623
Data File: p2881.d
Date: 18-MAY-2010 11:52
Client ID: TB-1 2-3 Instrument: BNAMS10.i
Sample Info: 460-13139-E-5-G Operator: BNAMS 4
06/03/2010Page 249 of 623
FORM IForm 1GC/MS SEMI VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-5 3-4
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-7
Matrix: p2899.dLab File ID:
Date Collected:8270CAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 12:30
Level: (low/med)
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Analyzed:
Date Extracted:
Dilution Factor:
Extract. Method: 05/17/2010 09:00
1
3541
05/18/2010 19:58
Low
N
1(mL)
% Moisture: 61.5
Sample wt/vol: 15.01(g)
Analysis Batch No.: 37818 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Phenol108-95-2 860 860 110U
2-Chlorophenol95-57-8 860 860 110U
2-Nitrophenol88-75-5 860 860 140U
2,4-Dimethylphenol105-67-9 860 860 140U
2,4-Dichlorophenol120-83-2 860 860 140U
4-Chloro-3-methylphenol59-50-7 860 860 140U
2,4,6-Trichlorophenol88-06-2 860 860 150U
2,4-Dinitrophenol51-28-5 2600 2600 180U
4-Nitrophenol100-02-7 2600 2600 220U
4,6-Dinitro-2-methylphenol534-52-1 2600 2600 410U
Pentachlorophenol87-86-5 2600 2600 420U
N-Nitrosodimethylamine62-75-9 860 860 88U
Bis(2-chloroethyl)ether111-44-4 86 86 18U
1,3-Dichlorobenzene541-73-1 860 860 120U
1,4-Dichlorobenzene106-46-7 860 860 130U
1,2-Dichlorobenzene95-50-1 860 860 140U
N-Nitrosodi-n-propylamine621-64-7 86 86 11U
Hexachloroethane67-72-1 86 86 14U
Nitrobenzene98-95-3 86 86 19U
Isophorone78-59-1 860 860 99U
Bis(2-chloroethoxy)methane111-91-1 860 860 120U
1,2,4-Trichlorobenzene120-82-1 86 86 14U
Naphthalene91-20-3 860 860 130U
Hexachlorobutadiene87-68-3 170 170 35U
Hexachlorocyclopentadiene77-47-4 860 860 250U
2-Chloronaphthalene91-58-7 860 860 120U
Dimethyl phthalate131-11-3 860 860 120U
Acenaphthylene208-96-8 860 860 120U
2,6-Dinitrotoluene606-20-2 170 170 22U
Acenaphthene83-32-9 200 860 120J
2,4-Dinitrotoluene121-14-2 170 170 25U
Diethyl phthalate84-66-2 860 860 120U
4-Chlorophenyl phenyl ether7005-72-3 860 860 150U
Fluorene86-73-7 440 860 150J
FORM I 8270C
06/03/2010Page 250 of 623
FORM IForm 1GC/MS SEMI VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-5 3-4
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-7
Matrix: p2899.dLab File ID:
Date Collected:8270CAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 12:30
Level: (low/med)
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Analyzed:
Date Extracted:
Dilution Factor:
Extract. Method: 05/17/2010 09:00
1
3541
05/18/2010 19:58
Low
N
1(mL)
% Moisture: 61.5
Sample wt/vol: 15.01(g)
Analysis Batch No.: 37818 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
N-Nitrosodiphenylamine86-30-6 860 860 140U
4-Bromophenyl phenyl ether101-55-3 860 860 150U
Hexachlorobenzene118-74-1 86 86 12U
Phenanthrene85-01-8 1800 860 150
Anthracene120-12-7 260 860 150J
Di-n-butyl phthalate84-74-2 860 860 130U
Fluoranthene206-44-0 1300 860 140
Pyrene129-00-0 790 860 150J
Benzidine92-87-5 860 860 180U *
Butyl benzyl phthalate85-68-7 860 860 100U
3,3'-Dichlorobenzidine91-94-1 1700 1700 190U
Benzo[a]anthracene56-55-3 380 86 16
Chrysene218-01-9 560 860 120J
Bis(2-ethylhexyl) phthalate117-81-7 190 860 110J
Di-n-octyl phthalate117-84-0 860 860 100U
Benzo[b]fluoranthene205-99-2 590 86 13
Benzo[k]fluoranthene207-08-9 230 86 12
Benzo[a]pyrene50-32-8 410 86 11
Indeno[1,2,3-cd]pyrene193-39-5 460 86 14
Dibenz(a,h)anthracene53-70-3 86 86 10U
Benzo[g,h,i]perylene191-24-2 460 860 91J
bis (2-chloroisopropyl) ether108-60-1 860 860 110U
SURROGATE %RECCAS NO. LIMITS Q
4165-60-0 Nitrobenzene-d5 55 38-105
4165-62-2 Phenol-d5 41 41-118
1718-51-0 Terphenyl-d14 54 16-151
118-79-6 2,4,6-Tribromophenol 52 10-120
367-12-4 2-Fluorophenol 39 37-125
321-60-8 2-Fluorobiphenyl 60 40-109
FORM I 8270C
06/03/2010Page 251 of 623
FORM IForm 1GC/MS SEMI VOA ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Client Sample ID:
Lab Name: Job No.:
TB-5 3-4
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-7
Matrix: p2899.dLab File ID:
Date Collected:8270CAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 12:30
Level: (low/med)
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Analyzed:
Date Extracted:
Dilution Factor:
Extract. Method: 05/17/2010 09:00
1
3541
05/18/2010 19:58
Low
N
1(mL)
% Moisture: 61.5
Sample wt/vol: 15.01(g)
Analysis Batch No.: 37818 ug/KgUnits:
Number TICs Found: TIC Result Total: 32390025
QRTCOMPOUND NAME RESULTCAS NO.
Unknown-1 5400 12.11 T J
Unknown Alkane-1 13000 12.22 T J
Unknown Alkane-2 23000 13.16 T J
Unknown-2 4200 13.86 T J
7616-22-0 .gamma.-Tocopherol 8500 13.96 T J N
Unknown Alkane-3 16000 14.13 T J
59-02-9 Vitamin E 11000 14.36 T J N
Unknown-3 3800 15.02 T J
Unknown-4 6500 15.21 T J
Unknown-5 10000 15.37 T J
Unknown-6 30000 15.62 T J
Unknown Sterol 10000 15.72 T J
1000194-62-4 4,4,6a,6b,8a,11,11,14b-Octamethyl-1,4,4a 30000 15.77 T J N
Unknown-7 4700 15.81 T J
Unknown-8 9800 15.86 T J
Unknown-9 22000 15.98 T J
Unknown-10 36000 16.11 T J
Unknown-11 11000 16.27 T J
Unknown-12 23000 16.32 T J
Unknown-13 10000 16.37 T J
Unknown-14 10000 16.44 T J
Unknown-15 13000 16.55 T J
Unknown-16 3400 16.75 T J
Unknown-17 5100 16.86 T J
Unknown-18 4500 17.40 T J
FORM I-TIC 8270C
06/03/2010Page 252 of 623
Data File: /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2899.d Report Date: 19-May-2010 16:01
TestAmerica
SEMI-VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2899.dLab Smp Id: 460-13139-E-7-E Client Smp ID: TB-5 3-4Inj Date : 18-MAY-2010 19:58 Operator : BNAMS 4 Inst ID: BNAMS10.iSmp Info : 460-13139-E-7-EMisc Info : 460-13139-E-7-EComment : Method : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/8270C_08SP.mMeth Date : 18-May-2010 11:53 czhao Quant Type: ISTDCal Date : 11-MAY-2010 16:30 Cal File: p2726.dAls bottle: 23 Dil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd1
Concentration Formula: Amt * DF * Uf*1000*Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorUf 1.00000 ng unit correction factorVt 1.00000 Volume of final extract (ml)Ws 15.01000 Weight of sample extracted (g)M 61.53846 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE (ug/ml) (ug/Kg)
========================== ==== == ====== ====== ======== ======= =======
$ 16 2-Fluorophenol (SUR) 112 2.957 2.928 (0.703) 221128 39.4595 6800
$ 17 Phenol-d5 (SUR) 99 3.844 3.862 (0.913) 258523 40.9026 7100(R)
* 79 1,4-Dichlorobenzene-d4 152 4.208 4.214 (1.000) 166401 40.0000
$ 76 Nitrobenzene-d5 (SUR) 82 4.767 4.778 (0.867) 135962 27.6539 4800
* 80 Naphthalene-d8 136 5.495 5.507 (1.000) 504685 40.0000
31 Naphthalene 128 5.519 5.525 (1.004) 3709 0.26173 45(a)
34 2-Methylnaphthalene 142 6.218 6.224 (1.132) 2890 0.34367 60(a)
120 1-Methylnaphthalene 142 6.312 6.324 (1.149) 2390 0.28858 50(a)
$ 77 2-Fluorobiphenyl (SUR) 172 6.588 6.594 (0.908) 235629 29.9517 5200
125 1,3-Dimethylnaphthalene 156 6.917 6.929 (0.953) 2136 0.39546 68(a)
* 82 Acenaphthene-d10 164 7.258 7.264 (1.000) 215742 40.0000
42 Acenaphthene 154 7.287 7.299 (1.004) 6749 1.15609 200(a)
43 Dibenzofuran 168 7.458 7.469 (1.028) 7619 0.90221 160(a)
06/03/2010Page 253 of 623
Data File: /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2899.d Report Date: 19-May-2010 16:01
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE (ug/ml) (ug/Kg)
========================== ==== == ====== ====== ======== ======= =======
47 Fluorene 166 7.798 7.810 (1.074) 15977 2.56725 440(a)
$ 18 2,4,6-Tribromophenol (SUR) 330 8.039 8.045 (1.108) 37500 52.4750 9100
* 83 Phenanthrene-d10 188 8.727 8.733 (1.000) 245292 40.0000
52 Phenanthrene 178 8.750 8.756 (1.003) 70548 10.1202 1800
53 Anthracene 178 8.797 8.803 (1.008) 10271 1.47343 260(a)
54 Carbazole 167 8.956 8.962 (1.026) 1635 0.27939 48(aH)
56 Fluoranthene 202 9.919 9.925 (1.137) 41324 7.47562 1300
57 Pyrene 202 10.143 10.149 (0.883) 33542 4.53596 780(a)
$ 78 Terphenyl-d14 244 10.307 10.307 (0.897) 123790 26.7822 4600
61 Benzo(a)anthracene 228 11.471 11.476 (0.998) 10893 2.21024 380
* 81 Chrysene-d12 240 11.488 11.494 (1.000) 175541 40.0000
62 Chrysene 228 11.518 11.524 (1.003) 14455 3.23685 560(a)
63 bis(2-Ethylhexyl)phthalate 149 11.523 11.524 (1.003) 4016 1.10210 190(a)
65 Benzo(b)fluoranthene 252 12.881 12.881 (0.961) 17646 3.38384 590
66 Benzo(k)fluoranthene 252 12.916 12.922 (0.963) 7456 1.30811 230
67 Benzo(a)pyrene 252 13.321 13.327 (0.993) 11271 2.36298 410
* 84 Perylene-d12 264 13.409 13.404 (1.000) 185914 40.0000
68 Indeno(1,2,3-cd)pyrene 276 14.908 14.908 (1.112) 10238 2.65562 460
70 Benzo(g,h,i)perylene 276 15.331 15.319 (1.143) 10400 2.65193 460(a)
QC Flag Legend
a - Target compound detected but, quantitated amountBelow Limit Of Quantitation(BLOQ).
R - Spike/Surrogate failed recovery limits.H - Operator selected an alternate compound hit.
06/03/2010Page 254 of 623
Data File: /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2899.d Report Date: 19-May-2010 16:01
TestAmerica
SEMI-VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2899.dLab Smp Id: 460-13139-E-7-E Client Smp ID: TB-5 3-4Inj Date : 18-MAY-2010 19:58 Operator : BNAMS 4 Inst ID: BNAMS10.iSmp Info : 460-13139-E-7-EMisc Info : 460-13139-E-7-EComment : Method : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/8270C_08SP.mMeth Date : 18-May-2010 11:53 czhao Quant Type: ISTDCal Date : 11-MAY-2010 16:30 Cal File: p2726.dAls bottle: 23 Dil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd1
Concentration Formula: Amt * DF * Uf*1000*Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorUf 1.00000 ng unit correction factorVt 1.00000 Volume of final extract (ml)Ws 15.01000 Weight of sample extracted (g)M 61.53846 % Moisture
Cpnd Variable Local Compound Variable
ISTD RT AREA AMOUNT======== ==== ====== ======
* 81 Chrysene-d12 11.488 536862 40.000
* 84 Perylene-d12 13.409 567669 40.000
CONCENTRATIONS QUANT
RT AREA ON-COL(ug/ml) FINAL(ug/Kg) QUAL LIBRARY LIB ENTRY CPND #
==== ==== ============= ============ ==== ======= ========= ======
Unknown-1 CAS #:
12.111 417217 31.0855978 5400 0 0 81
06/03/2010Page 255 of 623
Data File: /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2899.d Report Date: 19-May-2010 16:01
CONCENTRATIONS QUANT
RT AREA ON-COL(ug/ml) FINAL(ug/Kg) QUAL LIBRARY LIB ENTRY CPND #
==== ==== ============= ============ ==== ======= ========= ======
Unknown Alkane-1 CAS #:
12.223 1043719 77.7643864 13000 0 0 81
Unknown Alkane-2 CAS #:
13.157 1853159 130.580201 23000 0 0 84
Unknown-2 CAS #:
13.856 345601 24.3522478 4200 0 0 84
.gamma.-Tocopherol CAS #: 7616-22-0
13.956 699767 49.3080528 8500 97 NIST02.l 159683 84
Unknown Alkane-3 CAS #:
14.132 1280041 90.1962735 16000 0 0 84
Vitamin E CAS #: 59-02-9
14.361 917147 64.6254471 11000 99 NIST02.l 161945 84
Unknown-3 CAS #:
15.019 312618 22.0281906 3800 0 0 84
Unknown-4 CAS #:
15.207 531423 37.4459666 6500 0 0 84
Unknown-5 CAS #:
15.372 821264 57.8691920 10000 0 0 84
Unknown-6 CAS #:
15.625 2439669 171.907769 30000 0 0 84
Unknown Sterol CAS #:
15.719 849198 59.8375162 10000 0 0 84
4,4,6a,6b,8a,11,11,14b-Octamethyl-1,4,4a CAS #: 1000194-62-4
15.766 2452198 172.790624 30000 86 NIST02.l 160977 84
Unknown-7 CAS #:
15.813 382367 26.9429338 4700 0 0 84
Unknown-8 CAS #:
15.860 803654 56.6283559 9800 0 0 84
Unknown-9 CAS #:
15.983 1834546 129.268630 22000 0 0 84
06/03/2010Page 256 of 623
Data File: /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2899.d Report Date: 19-May-2010 16:01
CONCENTRATIONS QUANT
RT AREA ON-COL(ug/ml) FINAL(ug/Kg) QUAL LIBRARY LIB ENTRY CPND #
==== ==== ============= ============ ==== ======= ========= ======
Unknown-10 CAS #:
16.106 2969630 209.250683 36000 0 0 84
Unknown-11 CAS #:
16.265 876283 61.7460238 11000 0 0 84
Unknown-12 CAS #:
16.324 1905580 134.273981 23000 0 0 84
Unknown-13 CAS #:
16.371 840203 59.2036779 10000 0 0 84
Unknown-14 CAS #:
16.441 839864 59.1797935 10000 0 0 84
Unknown-15 CAS #:
16.553 1046819 73.7626199 13000 0 0 84
Unknown-16 CAS #:
16.753 280252 19.7475552 3400 0 0 84
Unknown-17 CAS #:
16.858 417152 29.3940269 5100 0 0 84
Unknown-18 CAS #:
17.405 372516 26.2488193 4500 0 0 84
06/03/2010Page 257 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
06/03/2010Page 258 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
42 Acenaphthene
06/03/2010Page 259 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
47 Fluorene
06/03/2010Page 260 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
52 Phenanthrene
06/03/2010Page 261 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
53 Anthracene
06/03/2010Page 262 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
56 Fluoranthene
06/03/2010Page 263 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
57 Pyrene
06/03/2010Page 264 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
61 Benzo(a)anthracene
06/03/2010Page 265 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
62 Chrysene
06/03/2010Page 266 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
63 bis(2-Ethylhexyl)phthalate
06/03/2010Page 267 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
65 Benzo(b)fluoranthene
06/03/2010Page 268 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
66 Benzo(k)fluoranthene
06/03/2010Page 269 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
67 Benzo(a)pyrene
06/03/2010Page 270 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
68 Indeno(1,2,3-cd)pyrene
06/03/2010Page 271 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
70 Benzo(g,h,i)perylene
06/03/2010Page 272 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
Retention Time: 12.11
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Unknown-1
2(1H)-Phenanthrenone, 3,4,4a,4b,5, 7715-44-8 NIST02.l 103086 62 C19H30O 274
7H-Furo[3,2-g][1]benzopyran-7-one, 54087-32-0 NIST02.l 102803 58 C15H14O5 274
06/03/2010Page 273 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
Retention Time: 12.22
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Unknown Alkane-1
Hexadecane 544-76-3 NIST02.l 73968 90 C16H34 226
Hexadecane 544-76-3 NIST02.l 73966 68 C16H34 226
06/03/2010Page 274 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
Retention Time: 13.16
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Unknown Alkane-2
Nonacosane 630-03-5 NIST02.l 158131 97 C29H60 408
Tetracosane 646-31-1 NIST02.l 136482 97 C24H50 338
06/03/2010Page 275 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
Retention Time: 13.86
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Unknown-2
1,19-Eicosadiene 14811-95-1 NIST02.l 105307 90 C20H38 278
Oxirane, heptadecyl- 67860-04-2 NIST02.l 107629 70 C19H38O 282
06/03/2010Page 276 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
Retention Time: 13.96
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
.gamma.-Tocopherol 7616-22-0 NIST02.l 159683 97 C28H48O2 416
3,4-Dihydro-3,5,8-trimethyl-3-(4,8 1000105-71-9 NIST02.l 165270 64 C30H50O3 458
Benzenepropanenitrile, 3,4-dimetho 49621-56-9 NIST02.l 49753 55 C11H13NO2 191
06/03/2010Page 277 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
Retention Time: 14.13
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Unknown Alkane-3
Heptadecane 629-78-7 NIST02.l 82607 96 C17H36 240
Hexadecane, 1-iodo- 544-77-4 NIST02.l 141774 95 C16H33I 352
06/03/2010Page 278 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
Retention Time: 14.36
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Vitamin E 59-02-9 NIST02.l 161945 99 C29H50O2 430
Vitamin E 10191-41-0 NIST02.l 161944 99 C29H50O2 430
Vitamin E 10191-41-0 NIST02.l 161942 98 C29H50O2 430
06/03/2010Page 279 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
Retention Time: 15.02
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Unknown-3
2H,8H-Benzo[1,2-b:5,4-b']dipyran-2 55334-39-9 NIST02.l 130818 55 C20H22O4 326
Acetic acid, [2,5-bis(trimethylsil 27798-63-6 NIST02.l 130548 46 C15H26O4Si2 326
06/03/2010Page 280 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
Retention Time: 15.21
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Unknown-4
1,1'-Biphenyl, 2,2',3,4,5-Pentachl 55312-69-1 NIST02.l 129478 90 C12H5Cl5 324
Bis(pentamethylcyclopentadienyl)ir 12126-50-0 NIST02.l 130845 50 C20H30Fe 326
06/03/2010Page 281 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
Retention Time: 15.37
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Unknown-5
Ergostanol 6538-02-9 NIST02.l 157084 90 C28H50O 402
Cholestane, 3-ethoxy-, (3.beta.,5. 2089-02-3 NIST02.l 159710 72 C29H52O 416
06/03/2010Page 282 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
Retention Time: 15.62
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Unknown-6
.beta.-Sitosterol 83-46-5 NIST02.l 159282 98 C29H50O 414
Stigmasterol, 22,23-dihydro- 1000214-20-7 NIST02.l 159291 96 C29H50O 414
06/03/2010Page 283 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
Retention Time: 15.72
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Unknown Sterol
Cholestane, 3-ethoxy-, (3.beta.,5. 2089-02-3 NIST02.l 159710 41 C29H52O 416
Stigmastanol 19466-47-8 NIST02.l 159708 41 C29H52O 416
06/03/2010Page 284 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
Retention Time: 15.77
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
4,4,6a,6b,8a,11,11,14b-Octamethyl- 1000194-62-4 NIST02.l 160977 86 C30H48O 424
Benzenamine, 2,6-dimethyl-N-(4,4-d 281211-68-5 NIST02.l 68040 64 C13H18N2O 218
Urs-12-ene 464-97-1 NIST02.l 158505 58 C30H50 410
06/03/2010Page 285 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
Retention Time: 15.81
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Unknown-7
p-(N-(Dimethylcarbamoylmethyl)acet 92703-70-3 NIST02.l 112574 27 C15H21N3O3 291
Phenol, 2,5-bis(1-methylpropyl)- 54932-77-3 NIST02.l 60195 25 C14H22O 206
06/03/2010Page 286 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
Retention Time: 15.86
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Unknown-8
Androst-5-en-17-ol, 4,4-dimethyl- 1000195-76-3 NIST02.l 118836 43 C21H34O 302
2-Methyl-3-n-heptyl-6-methoxy-1,5- 1000250-74-6 NIST02.l 110925 25 C17H24N2O2 288
06/03/2010Page 287 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
Retention Time: 15.98
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Unknown-9
.alpha.-Amyrin 638-95-9 NIST02.l 161264 91 C30H50O 426
2(1H)Naphthalenone, 3,5,6,7,8,8a-h 1000188-66-5 NIST02.l 68225 89 C15H22O 218
06/03/2010Page 288 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
Retention Time: 16.11
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Unknown-10
4,4,6a,6b,8a,11,12,14b-Octamethyl- 1000194-64-2 NIST02.l 160978 68 C30H48O 424
D:C-Friedoolean-8-en-3-one 22611-26-3 NIST02.l 160967 64 C30H48O 424
06/03/2010Page 289 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
Retention Time: 16.27
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Unknown-11
3-Methylcholanthrene 56-49-5 NIST02.l 99514 48 C21H16 268
Ethyl .alpha.-oximidostearate 1000126-75-7 NIST02.l 137659 46 C20H39NO3 341
06/03/2010Page 290 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
Retention Time: 16.32
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Unknown-12
4,4,6a,6b,8a,11,12,14b-Octamethyl- 1000194-64-2 NIST02.l 160978 52 C30H48O 424
.beta.-Amyrin 559-70-6 NIST02.l 161263 49 C30H50O 426
06/03/2010Page 291 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
Retention Time: 16.37
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Unknown-13
Ethanone, 1-[5-(5-trifluoromethyl- 1000266-44-5 NIST02.l 102545 43 C11H9F3N2OS 274
10H-Phenoxaphosphine, 2-ethyl-10-h 36360-91-5 NIST02.l 102822 38 C15H15O3P 274
06/03/2010Page 292 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
Retention Time: 16.44
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Unknown-14
Androstan-6-one, (5.alpha.)- 3676-06-0 NIST02.l 103060 43 C19H30O 274
2(1H)-Phenanthrenone, 3,4,4a,4b,5, 7715-44-8 NIST02.l 103086 43 C19H30O 274
06/03/2010Page 293 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
Retention Time: 16.55
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Unknown-15
Stigmast-4-en-3-one 1058-61-3 NIST02.l 158845 66 C29H48O 412
Cholest-5-en-3-one, 4,4-dimethyl- 2220-42-0 NIST02.l 158848 35 C29H48O 412
06/03/2010Page 294 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
Retention Time: 16.75
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Unknown-16
Azulene, 1,4-dimethyl-7-(1-methyle 489-84-9 NIST02.l 55042 51 C15H18 198
Naphthalene, 1,6-dimethyl-4-(1-met 483-78-3 NIST02.l 55043 38 C15H18 198
06/03/2010Page 295 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
Retention Time: 16.86
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Unknown-17
1,3-Diethyl-2-hydroxybenzothiazolo 1000227-15-3 NIST02.l 102705 43 C14H14N2O2S 274
10H-Phenoxaphosphine, 2-ethyl-10-h 36360-91-5 NIST02.l 102822 43 C15H15O3P 274
06/03/2010Page 296 of 623
Data File: p2899.d
Date: 18-MAY-2010 19:58
Client ID: TB-5 3-4 Instrument: BNAMS10.i
Sample Info: 460-13139-E-7-E Operator: BNAMS 4
Retention Time: 17.40
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Unknown-18
.alpha.-Cedrene oxide 1000159-39-1 NIST02.l 69499 55 C15H24O 220
Friedelan-3-one 559-74-0 NIST02.l 161267 43 C30H50O 426
06/03/2010Page 297 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC/MS SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
BNAMS10
Analy Batch No.: 37184
6144Calibration Start Date: Calibration End Date:05/11/2010 14:17
N
05/11/2010 16:30
0.25(mm)Rtx-5MS ID:
INTERNAL STANDARD CURVE EVALUTION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-37184/4 p2723.d2Level IC 460-37184/7 p2726.d3Level IC 460-37184/6 p2725.d4Level ICIS 460-37184/2 p2721.d5Level IC 460-37184/5 p2724.d6Level IC 460-37184/3 p2722.d
ANALYTE RRF
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CURVETYPE
COEFFICIENT
B M1 M2
# %RSD # MAX%RSD
R^2OR COD
# MIN R^2OR COD
MIN RRF
LVL 6
1,4-Dioxane 0.3344 0.2903 0.3185 0.2742 0.3041 Ave 7.00.3140
15.00.3059
2,3,7,8-TCDD (Screen) +++++ +++++ +++++ 0.1162 +++++ Ave+++++
15.00.1162
N-Nitrosodimethylamine 0.7958 0.7918 0.7605 0.7352 0.7200 Ave 4.00.7668
15.00.7617
Pyridine 1.5172 1.4777 1.4043 1.3267 1.3012 Ave 5.91.3964
15.01.4039
Benzaldehyde 0.8555 0.8922 0.6746 0.3984 0.2195 Ave 48.0+++++
* 15.00.6080
Phenol 1.8646 1.7991 1.6198 1.5352 1.4505 Ave 10.01.5320
30.01.6335
Aniline 2.1491 2.1648 1.9550 1.9105 1.7726 Ave 14.11.4427
15.01.8991
Bis(2-chloroethyl)ether 1.5055 1.4088 1.3203 1.2604 1.2286 QuaF 0.99661.8387
0.99000.9479 -0.073
2-Chlorophenol 1.6385 1.5763 1.4663 1.3419 1.2380 Ave 11.61.2722
15.01.4222
Decane 1.2704 1.2423 1.1654 1.1137 1.0305 Ave 10.80.9546
15.01.1295
1,3-Dichlorobenzene 1.8584 1.8317 1.7202 1.6338 1.4936 Ave 9.51.4956
15.01.6722
1,4-Dichlorobenzene 1.8570 1.8114 1.7367 1.5949 1.4701 Ave 10.71.4381
30.01.6514
Benzyl alcohol 0.8469 0.8728 0.8204 0.8191 0.7730 Ave 6.80.7184
15.00.8084
1,2-Dichlorobenzene 1.7686 1.7197 1.6166 1.5197 1.3931 Ave 11.61.3131
15.01.5551
2-Methylphenol 1.3383 1.2827 1.1732 1.0830 0.9986 Ave 12.01.0302
15.01.1510
FORM VI 8270C
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 298 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC/MS SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
BNAMS10
Analy Batch No.: 37184
6144Calibration Start Date: Calibration End Date:05/11/2010 14:17
N
05/11/2010 16:30
0.25(mm)Rtx-5MS ID:
INTERNAL STANDARD CURVE EVALUTION
ANALYTE RRF
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CURVETYPE
COEFFICIENT
B M1 M2
# %RSD # MAX%RSD
R^2OR COD
# MIN R^2OR COD
MIN RRF
LVL 6
bis (2-chloroisopropyl) ether 1.4549 1.3999 1.3266 1.2394 1.1317 Ave 10.91.1177
15.01.2783
o-Toluidine 2.8826 2.7880 2.5140 2.3417 2.2140 Ave 11.2+++++
15.02.5481
Acetophenone 1.8303 1.8975 1.6444 1.5196 1.4083 Ave 12.81.4223
15.01.6204
3 & 4 Methylphenol 1.4050 1.3202 1.1862 1.0648 0.9922 Ave 13.71.0749
15.01.1739
4-Methylphenol 1.4050 1.3168 1.1790 1.0648 0.9922 Ave 13.71.0749
15.01.1721
N-Nitrosodi-n-propylamine 0.8446 0.8860 0.7934 0.7404 0.6671 Ave 11.90.6657
0.0500 15.00.7662
Hexachloroethane 0.6620 0.6496 0.6226 0.6050 0.5553 Ave 7.80.5476
15.00.6070
Nitrobenzene 0.6306 0.5806 0.5472 0.4898 0.4545 QuaF 0.99980.4070
0.99001.5964 0.6970
n,n'-Dimethylaniline 2.4040 2.2483 2.0634 1.8870 1.7586 Ave 13.51.7338
15.02.0159
Isophorone 0.6875 0.6968 0.6583 0.6277 0.6099 Ave 5.30.6352
15.00.6526
2-Nitrophenol 0.2097 0.2172 0.2118 0.2035 0.1993 Ave 3.20.2032
30.00.2074
2,4-Dimethylphenol 0.3756 0.3687 0.3420 0.3123 0.2929 Ave 11.30.2900
15.00.3302
Bis(2-chloroethoxy)methane 0.4292 0.4335 0.4079 0.3908 0.3729 Ave 6.20.3815
15.00.4026
Benzoic acid 0.1117 0.1532 0.1477 0.1430 0.1539 Ave 11.40.1545
15.00.1440
2,4-Dichlorophenol 0.3240 0.3223 0.2995 0.2779 0.2604 Ave 10.80.2500
30.00.2890
1,2,4-Trichlorobenzene 0.3441 0.3599 0.3523 0.3208 0.3050 Ave 7.30.3044
15.00.3311
Naphthalene 1.2625 1.2417 1.1826 1.0725 1.0183 Ave 11.00.9614
15.01.1232
4-Chloroaniline 0.4669 0.4747 0.4460 0.4155 0.3859 Ave 9.00.3882
15.00.4295
Hexachlorobutadiene 0.2068 0.1968 0.1888 0.1724 0.1643 Ave 10.00.1624
30.00.1819
Caprolactam 0.0720 0.0918 0.0794 0.0911 0.0792 Ave 9.20.0820
15.00.0826
FORM VI 8270C
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 299 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC/MS SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
BNAMS10
Analy Batch No.: 37184
6144Calibration Start Date: Calibration End Date:05/11/2010 14:17
N
05/11/2010 16:30
0.25(mm)Rtx-5MS ID:
INTERNAL STANDARD CURVE EVALUTION
ANALYTE RRF
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CURVETYPE
COEFFICIENT
B M1 M2
# %RSD # MAX%RSD
R^2OR COD
# MIN R^2OR COD
MIN RRF
LVL 6
4-Chloro-3-methylphenol 0.3008 0.3171 0.2829 0.2731 0.2561 Ave 8.80.2554
30.00.2809
2-Methylnaphthalene 0.7637 0.7341 0.6805 0.6319 0.5906 Ave 10.80.5981
15.00.6665
1-Methylnaphthalene 0.7273 0.7477 0.6762 0.6289 0.5898 Ave 11.10.5685
15.00.6564
Hexachlorocyclopentadiene 0.2850 0.2637 0.2977 0.3481 0.3599 Ave 14.70.3835
0.0500 15.00.3230
2-tertbutyl-4-methylphenol 0.4897 0.5036 0.4567 0.4288 0.3989 QuaF 0.99090.3185
0.99001.4154 1.6687
2,4,6-Trichlorophenol 0.3931 0.3817 0.3704 0.3515 0.3577 Ave 6.30.4155
30.00.3783
2,4,5-Trichlorophenol 0.3852 0.3989 0.3911 0.3614 0.3545 Ave 7.30.3279
15.00.3698
Diphenyl 1.7136 1.7409 1.6333 1.4791 1.3908 Ave 14.61.1614
15.01.5199
2-Chloronaphthalene 1.3439 1.3326 1.2805 1.1639 1.1049 Ave 9.51.0802
15.01.2177
Diphenyl ether 0.9676 0.9598 0.9136 0.8331 0.8131 Ave 8.20.8140
15.00.8835
2-Nitroaniline 0.3559 0.4077 0.3840 0.3749 0.3538 Ave 11.40.2868
15.00.3605
Dimethylnaphthalene, total 1.0787 1.0835 1.0293 0.9443 0.9243 Ave 7.10.9485
15.01.0014
Dimethyl phthalate 1.2279 1.2744 1.2011 1.1561 1.0957 Ave 5.71.1248
15.01.1800
Coumarin 0.1909 0.2103 0.1868 0.1944 0.1713 Ave 8.10.1700
15.00.1873
2,6-Dinitrotoluene 0.2557 0.2876 0.2762 0.2816 0.2627 Ave 4.40.2749
15.00.2731
Acenaphthylene 2.1544 2.0838 1.9949 1.8523 1.7729 Ave 8.21.7892
15.01.9412
3-Nitroaniline 0.2780 0.3041 0.2860 0.2987 0.2729 Ave 4.10.2877
15.00.2879
3,5-di-tert-butyl-4-hydroxytol 1.0743 1.0917 1.0563 0.9555 0.9045 Ave 9.80.8616
15.00.9906
Acenaphthene 1.3092 1.1826 1.1267 1.0065 0.9419 Ave 13.90.9273
30.01.0824
2,4-Dinitrophenol 0.0693 0.0870 0.0932 0.1206 0.1216 QuaF 0.99470.1255
0.0500 0.99009.5223 -4.359
FORM VI 8270C
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 300 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC/MS SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
BNAMS10
Analy Batch No.: 37184
6144Calibration Start Date: Calibration End Date:05/11/2010 14:17
N
05/11/2010 16:30
0.25(mm)Rtx-5MS ID:
INTERNAL STANDARD CURVE EVALUTION
ANALYTE RRF
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CURVETYPE
COEFFICIENT
B M1 M2
# %RSD # MAX%RSD
R^2OR COD
# MIN R^2OR COD
MIN RRF
LVL 6
4-Nitrophenol 0.1471 0.1550 0.1538 0.1708 0.1577 Ave 6.20.1720
0.0500 15.00.1594
2,4-Dinitrotoluene 0.3001 0.3403 0.3232 0.3272 0.2964 Ave 6.20.2932
15.00.3134
Dibenzofuran 1.7460 1.7462 1.6300 1.4998 1.3910 Ave 10.61.3813
15.01.5657
1-Naphthylamine 0.6314 0.7429 0.7934 0.8769 0.7729 Ave 10.70.8146
30.00.7720
2-Naphthylamine 0.8391 0.9325 0.8713 0.8843 0.8072 Ave 5.00.8501
15.00.8641
Diethyl phthalate 1.1532 1.2021 1.1333 1.0991 1.0349 Ave 7.60.9721
15.01.0991
4-Chlorophenyl phenyl ether 0.5800 0.5749 0.5370 0.4879 0.4542 Ave 10.90.4589
15.00.5155
Fluorene 1.2972 1.2905 1.2256 1.0989 1.0078 Ave 11.71.0032
15.01.1539
4-Nitroaniline 0.2304 0.2587 0.2449 0.2570 0.2343 Ave 5.70.2267
15.00.2420
4,6-Dinitro-2-methylphenol 0.0918 0.1030 0.1092 0.1184 0.1233 Ave 10.40.1151
15.00.1102
N-Nitrosodiphenylamine 0.6518 0.6783 0.6537 0.6015 0.6078 Ave 4.80.6185
30.00.6353
1,2-Diphenylhydrazine 1.1710 1.1698 1.0985 0.9985 0.9776 Ave 7.91.0275
15.01.0738
4-Bromophenyl phenyl ether 0.2512 0.2510 0.2393 0.2245 0.2239 Ave 5.20.2326
15.00.2371
Hexachlorobenzene 0.2621 0.2664 0.2460 0.2307 0.2309 Ave 6.20.2397
15.00.2460
Atrazine 0.1900 0.2050 0.1883 0.1864 0.1802 Ave 8.30.1580
15.00.1847
Pentachlorophenol 0.0991 0.1070 0.1093 0.1207 0.1219 Ave 10.10.1305
30.00.1147
n-Octadecane 0.5101 0.5404 0.5039 0.4540 0.4645 Ave 8.90.4239
15.00.4828
Phenanthrene 1.2423 1.2307 1.1658 1.0952 1.0414 Ave 7.91.0453
15.01.1368
Anthracene 1.2077 1.2242 1.1769 1.1108 1.0470 Ave 6.81.0539
15.01.1367
Carbazole 1.0121 1.0142 0.9757 0.9493 0.8875 Ave 6.00.8869
15.00.9543
FORM VI 8270C
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 301 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC/MS SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
BNAMS10
Analy Batch No.: 37184
6144Calibration Start Date: Calibration End Date:05/11/2010 14:17
N
05/11/2010 16:30
0.25(mm)Rtx-5MS ID:
INTERNAL STANDARD CURVE EVALUTION
ANALYTE RRF
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CURVETYPE
COEFFICIENT
B M1 M2
# %RSD # MAX%RSD
R^2OR COD
# MIN R^2OR COD
MIN RRF
LVL 6
Di-n-butyl phthalate 1.1027 1.1829 1.1721 1.1526 1.0958 Ave 3.51.0964
15.01.1337
Fluoranthene 0.9159 0.9414 0.9319 0.9242 0.8490 Ave 4.70.8462
30.00.9014
Benzidine 0.0851 0.2413 0.1918 0.0988 0.0659 Ave 55.6+++++
* 15.00.1366
Pyrene 1.7105 1.8847 1.6665 1.6234 1.5613 Ave 6.51.6635
15.01.6850
Butyl benzyl phthalate 0.6096 0.6456 0.6396 0.6790 0.6734 Ave 5.70.7176
15.00.6608
Carbamazepine 0.2818 0.3992 0.4412 0.4980 0.5410 QuaF 0.99910.5480
0.99002.0817 -0.164
3,3'-Dichlorobenzidine 0.3069 0.3441 0.3277 0.3052 0.2954 Ave 6.80.2870
15.00.3111
Benzo[a]anthracene 1.2527 1.1088 1.0816 1.0904 1.0678 Ave 6.01.1369
15.01.1230
Bis(2-ethylhexyl) phthalate 0.8133 0.8447 0.8074 0.8253 0.8232 Ave 2.70.8681
15.00.8303
Chrysene 1.0900 1.0443 1.0478 1.0063 0.9683 Ave 5.20.9489
15.01.0176
Di-n-octyl phthalate 1.1765 1.4012 1.4005 1.6095 1.6475 QuaF 0.99971.8204
0.99000.6874 -0.025
Benzo[b]fluoranthene 0.8828 1.0698 1.1304 1.1936 1.2085 Ave 11.81.2468
15.01.1220
Benzo[k]fluoranthene 0.9836 1.3256 1.2367 1.2744 1.2573 Ave 10.01.2804
15.01.2263
Benzo[a]pyrene 0.9730 0.9980 1.0532 1.0313 1.0493 Ave 3.31.0526
30.01.0262
Indeno[1,2,3-cd]pyrene 0.5157 0.7363 0.7771 0.8835 0.9027 QuaF 0.99970.9446
0.99001.2085 -0.054
Dibenz(a,h)anthracene 0.4732 0.6915 0.8277 0.8965 0.9027 QuaF 0.99970.9390
0.99001.1825 -0.042
Benzo[g,h,i]perylene 0.7385 0.7848 0.8445 0.8735 0.8983 Ave 8.30.9231
15.00.8438
2-Fluorophenol 1.4987 1.4708 1.3674 1.2624 1.1903 Ave 9.01.2929
15.01.3471
Phenol-d5 1.7447 1.7117 1.5431 1.4345 1.3243 Ave 11.81.3577
15.01.5193
Nitrobenzene-d5 0.4151 0.4270 0.4021 0.3893 0.3689 Ave 8.60.3356
15.00.3897
FORM VI 8270C
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 302 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC/MS SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
BNAMS10
Analy Batch No.: 37184
6144Calibration Start Date: Calibration End Date:05/11/2010 14:17
N
05/11/2010 16:30
0.25(mm)Rtx-5MS ID:
INTERNAL STANDARD CURVE EVALUTION
ANALYTE RRF
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CURVETYPE
COEFFICIENT
B M1 M2
# %RSD # MAX%RSD
R^2OR COD
# MIN R^2OR COD
MIN RRF
LVL 6
2-Fluorobiphenyl 1.5827 1.6097 1.5251 1.3955 1.3242 Ave 9.01.3144
15.01.4586
2,4,6-Tribromophenol 0.1217 0.1347 0.1322 0.1371 0.1295 Ave 4.80.1397
15.00.1325
Terphenyl-d14 1.0769 1.1483 1.0172 1.0334 0.9919 Ave 5.21.0516
15.01.0532
FORM VI 8270C
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 303 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC/MS SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
BNAMS10
Analy Batch No.: 37184
6144Calibration Start Date: Calibration End Date:05/11/2010 14:17
N
05/11/2010 16:30
GC Column: Rtx-5MS ID: 0.25(mm)
INTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-37184/4 p2723.dLevel 2 IC 460-37184/7 p2726.dLevel 3 IC 460-37184/6 p2725.dLevel 4 ICIS 460-37184/2 p2721.dLevel 5 IC 460-37184/5 p2724.dLevel 6 IC 460-37184/3 p2722.d
ANALYTE CURVETYPE
ISREF
RESPONSE
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CONCENTRATION (UG/ML)
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5LVL 6 LVL 6
1,4-Dioxane AvePHN 11240 22497 33921 83612 135128270394
5.00 10.0 20.0 50.0 80.0120
2,3,7,8-TCDD (Screen) AveCRY +++++ +++++ +++++ 201 ++++++++++
+++++ +++++ +++++ 0.500 ++++++++++
N-Nitrosodimethylamine AveDCB 14340 30434 43821 110186 177396348575
5.00 10.0 20.0 50.0 80.0120
Pyridine AveDCB 27341 56800 80914 198833 320592634756
5.00 10.0 20.0 50.0 80.0120
Benzaldehyde AveDCB 15416 34294 38868 59710 54093+++++
5.00 10.0 20.0 50.0 80.0+++++
Phenol AveDCB 33600 69154 93332 230071 357392696410
5.00 10.0 20.0 50.0 80.0120
Aniline AveDCB 38727 83212 112648 286314 436758655809
5.00 10.0 20.0 50.0 80.0120
Bis(2-chloroethyl)ether QuaFDCB 2713 54151 76076 188896 302701835822
0.500 10.0 20.0 50.0 80.0120
2-Chlorophenol AveDCB 29526 60590 84489 201113 305031578327
5.00 10.0 20.0 50.0 80.0120
Decane AveDCB 22892 47754 67151 166905 253896433933
5.00 10.0 20.0 50.0 80.0120
1,3-Dichlorobenzene AveDCB 33489 70407 99117 244847 368001679871
5.00 10.0 20.0 50.0 80.0120
1,4-Dichlorobenzene AveDCB 33463 69629 100067 239021 362220653703
5.00 10.0 20.0 50.0 80.0120
Benzyl alcohol AveDCB 15262 33551 47273 122755 190447326576
5.00 10.0 20.0 50.0 80.0120
1,2-Dichlorobenzene AveDCB 31870 66103 93147 227747 343239596899
5.00 10.0 20.0 50.0 80.0120
2-Methylphenol AveDCB 24116 49304 67598 162311 246046468324
5.00 10.0 20.0 50.0 80.0120
bis (2-chloroisopropyl) ether AveDCB 26218 53809 76439 185741 278829508059
5.00 10.0 20.0 50.0 80.0120
FORM VI 8270C 06/03/2010Page 304 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC/MS SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
BNAMS10
Analy Batch No.: 37184
6144Calibration Start Date: Calibration End Date:05/11/2010 14:17
N
05/11/2010 16:30
GC Column: Rtx-5MS ID: 0.25(mm)
INTERNAL STANDARD RESPONSE AND CONCENTRATION
ANALYTE CURVETYPE
ISREF
RESPONSE
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CONCENTRATION (UG/ML)
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5LVL 6 LVL 6
o-Toluidine AveDCB 51945 107169 144857 350940 545513+++++
5.00 10.0 20.0 50.0 80.0+++++
Acetophenone AveDCB 32983 72938 94753 227740 346994646534
5.00 10.0 20.0 50.0 80.0120
3 & 4 Methylphenol AveDCB 25319 50748 68352 159577 244458488609
5.00 10.0 20.0 50.0 80.0120
4-Methylphenol AveDCB 25319 50616 67932 159577 244458488609
5.00 10.0 20.0 50.0 80.0120
N-Nitrosodi-n-propylamine AveDCB 1522 34058 45716 110956 164360302592
0.500 10.0 20.0 50.0 80.0120
Hexachloroethane AveDCB 1193 24968 35876 90664 136813248912
0.500 10.0 20.0 50.0 80.0120
Nitrobenzene QuaFNPT 3859 77196 104246 247570 368229641389
0.500 10.0 20.0 50.0 80.0120
n,n'-Dimethylaniline AveDCB 4332 86423 118894 282801 433293788142
0.500 10.0 20.0 50.0 80.0120
Isophorone AveNPT 42075 92650 125399 317241 4941581000971
5.00 10.0 20.0 50.0 80.0120
2-Nitrophenol AveNPT 12831 28884 40349 102839 161449320228
5.00 10.0 20.0 50.0 80.0120
2,4-Dimethylphenol AveNPT 22983 49018 65148 157847 237353457019
5.00 10.0 20.0 50.0 80.0120
Bis(2-chloroethoxy)methane AveNPT 26264 57636 77698 197548 302150601104
5.00 10.0 20.0 50.0 80.0120
Benzoic acid AveNPT 6835 20370 28133 72294 124678243452
5.00 10.0 20.0 50.0 80.0120
2,4-Dichlorophenol AveNPT 19829 42859 57061 140455 210987393900
5.00 10.0 20.0 50.0 80.0120
1,2,4-Trichlorobenzene AveNPT 2106 47858 67115 162132 247105479659
0.500 10.0 20.0 50.0 80.0120
Naphthalene AveNPT 77263 165102 225280 542084 8250611514957
5.00 10.0 20.0 50.0 80.0120
4-Chloroaniline AveNPT 28570 63114 84965 210020 312652611799
5.00 10.0 20.0 50.0 80.0120
Hexachlorobutadiene AveNPT 2531 26169 35968 87146 133125255975
1.00 10.0 20.0 50.0 80.0120
Caprolactam AveNPT 4406 12205 15134 46028 64155129217
5.00 10.0 20.0 50.0 80.0120
4-Chloro-3-methylphenol AveNPT 18405 42159 53886 138012 207519402425
5.00 10.0 20.0 50.0 80.0120
2-Methylnaphthalene AveNPT 46734 97611 129639 319373 478513942529
5.00 10.0 20.0 50.0 80.0120
FORM VI 8270C 06/03/2010Page 305 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC/MS SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
BNAMS10
Analy Batch No.: 37184
6144Calibration Start Date: Calibration End Date:05/11/2010 14:17
N
05/11/2010 16:30
GC Column: Rtx-5MS ID: 0.25(mm)
INTERNAL STANDARD RESPONSE AND CONCENTRATION
ANALYTE CURVETYPE
ISREF
RESPONSE
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CONCENTRATION (UG/ML)
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5LVL 6 LVL 6
1-Methylnaphthalene AveNPT 44511 99420 128821 317846 477852895898
5.00 10.0 20.0 50.0 80.0120
Hexachlorocyclopentadiene AveANT 8342 17302 26785 85502 135650277158
5.00 10.0 20.0 50.0 80.0120
2-tertbutyl-4-methylphenol QuaFNPT 29965 66956 86994 216729 323222501936
5.00 10.0 20.0 50.0 80.0120
2,4,6-Trichlorophenol AveANT 11507 25041 33330 86360 134821300269
5.00 10.0 20.0 50.0 80.0120
2,4,5-Trichlorophenol AveANT 11276 26170 35186 88777 133618236989
5.00 10.0 20.0 50.0 80.0120
Diphenyl AveANT 50166 114214 146952 363363 524191839368
5.00 10.0 20.0 50.0 80.0120
2-Chloronaphthalene AveANT 39343 87432 115207 285932 416432780728
5.00 10.0 20.0 50.0 80.0120
Diphenyl ether AveANT 28326 62972 82198 204654 306430588313
5.00 10.0 20.0 50.0 80.0120
2-Nitroaniline AveANT 20836 26746 34553 92096 133331207268
10.0 10.0 20.0 50.0 80.0120
Dimethylnaphthalene, total AveANT 31577 71084 92612 231987 348362685494
5.00 10.0 20.0 50.0 80.0120
Dimethyl phthalate AveANT 35947 83612 108065 284018 412960812920
5.00 10.0 20.0 50.0 80.0120
Coumarin AveNPT 11680 27957 35579 98245 138768267878
5.00 10.0 20.0 50.0 80.0120
2,6-Dinitrotoluene AveANT 1497 18866 24848 69187 98991198679
1.00 10.0 20.0 50.0 80.0120
Acenaphthylene AveANT 63070 136711 179491 455030 6681661293148
5.00 10.0 20.0 50.0 80.0120
3-Nitroaniline AveANT 16277 19953 25735 73385 102871207920
10.0 10.0 20.0 50.0 80.0120
3,5-di-tert-butyl-4-hydroxytol AveANT 31450 71625 95036 234715 340885622746
5.00 10.0 20.0 50.0 80.0120
Acenaphthene AveANT 38326 77589 101369 247252 354979670223
5.00 10.0 20.0 50.0 80.0120
2,4-Dinitrophenol QuaFANT 6088 11411 12577 29626 4582790715
15.0 20.0 30.0 50.0 80.0120
4-Nitrophenol AveANT 12920 20332 20762 41966 59451124349
15.0 20.0 30.0 50.0 80.0120
2,4-Dinitrotoluene AveANT 1757 22325 29081 80387 111692211919
1.00 10.0 20.0 50.0 80.0120
Dibenzofuran AveANT 51114 114567 146660 368428 524234998346
5.00 10.0 20.0 50.0 80.0120
FORM VI 8270C 06/03/2010Page 306 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC/MS SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
BNAMS10
Analy Batch No.: 37184
6144Calibration Start Date: Calibration End Date:05/11/2010 14:17
N
05/11/2010 16:30
GC Column: Rtx-5MS ID: 0.25(mm)
INTERNAL STANDARD RESPONSE AND CONCENTRATION
ANALYTE CURVETYPE
ISREF
RESPONSE
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CONCENTRATION (UG/ML)
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5LVL 6 LVL 6
1-Naphthylamine AveANT 18483 48739 71386 215410 291293588740
5.00 10.0 20.0 50.0 80.0120
2-Naphthylamine AveANT 24565 61178 78391 217236 304226614439
5.00 10.0 20.0 50.0 80.0120
Diethyl phthalate AveANT 33760 78864 101966 270013 390057702551
5.00 10.0 20.0 50.0 80.0120
4-Chlorophenyl phenyl ether AveANT 16978 37718 48319 119847 171192331646
5.00 10.0 20.0 50.0 80.0120
Fluorene AveANT 37974 84665 110268 269955 379831725070
5.00 10.0 20.0 50.0 80.0120
4-Nitroaniline AveANT 13488 16975 22036 63127 88312163859
10.0 10.0 20.0 50.0 80.0120
4,6-Dinitro-2-methylphenol AvePHN 9258 15967 17449 36105 5481399111
15.0 20.0 30.0 50.0 80.0120
N-Nitrosodiphenylamine AvePHN 21910 52568 69616 183415 270082532569
5.00 10.0 20.0 50.0 80.0120
1,2-Diphenylhydrazine AvePHN 39363 90660 116988 304461 434441884689
5.00 10.0 20.0 50.0 80.0120
4-Bromophenyl phenyl ether AvePHN 8443 19455 25490 68465 99495200243
5.00 10.0 20.0 50.0 80.0120
Hexachlorobenzene AvePHN 881 20649 26198 70336 102624206404
0.500 10.0 20.0 50.0 80.0120
Atrazine AvePHN 6386 15890 20050 56849 80095136072
5.00 10.0 20.0 50.0 80.0120
Pentachlorophenol AvePHN 9996 16586 17454 36809 54159112373
15.0 20.0 30.0 50.0 80.0120
n-Octadecane AvePHN 17149 41882 53666 138422 206400365007
5.00 10.0 20.0 50.0 80.0120
Phenanthrene AvePHN 41761 95378 124157 333937 462778899985
5.00 10.0 20.0 50.0 80.0120
Anthracene AvePHN 40597 94876 125337 338699 465272907378
5.00 10.0 20.0 50.0 80.0120
Carbazole AvePHN 34022 78603 103916 289468 394382763600
5.00 10.0 20.0 50.0 80.0120
Di-n-butyl phthalate AvePHN 37067 91673 124828 351434 486959943979
5.00 10.0 20.0 50.0 80.0120
Fluoranthene AvePHN 30789 72957 99252 281801 377275728544
5.00 10.0 20.0 50.0 80.0120
Benzidine AvePHN 2860 37395 30641 30115 29293+++++
5.00 20.0 30.0 50.0 80.0+++++
Pyrene AveCRY 30421 74386 99692 280847 379631714441
5.00 10.0 20.0 50.0 80.0120
FORM VI 8270C 06/03/2010Page 307 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC/MS SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
BNAMS10
Analy Batch No.: 37184
6144Calibration Start Date: Calibration End Date:05/11/2010 14:17
N
05/11/2010 16:30
GC Column: Rtx-5MS ID: 0.25(mm)
INTERNAL STANDARD RESPONSE AND CONCENTRATION
ANALYTE CURVETYPE
ISREF
RESPONSE
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CONCENTRATION (UG/ML)
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5LVL 6 LVL 6
Butyl benzyl phthalate AveCRY 10842 25479 38263 117469 163744308193
5.00 10.0 20.0 50.0 80.0120
Carbamazepine QuaFCRY 5011 15755 26391 86153 131540235332
5.00 10.0 20.0 50.0 80.0120
3,3'-Dichlorobenzidine AveCRY 10917 27163 29401 52807 71832123262
10.0 20.0 30.0 50.0 80.0120
Benzo[a]anthracene AveCRY 2228 43760 64700 188632 259636488256
0.500 10.0 20.0 50.0 80.0120
Bis(2-ethylhexyl) phthalate AveCRY 14465 33338 48297 142778 200167372822
5.00 10.0 20.0 50.0 80.0120
Chrysene AveCRY 19385 41216 62680 174091 235430407544
5.00 10.0 20.0 50.0 80.0120
Di-n-octyl phthalate QuaFPRY 15513 39057 63179 208803 296100560482
5.00 10.0 20.0 50.0 80.0120
Benzo[b]fluoranthene AvePRY 1164 29819 50994 154848 217207383883
0.500 10.0 20.0 50.0 80.0120
Benzo[k]fluoranthene AvePRY 1297 36950 55791 165327 225977394222
0.500 10.0 20.0 50.0 80.0120
Benzo[a]pyrene AvePRY 1283 27819 47514 133788 188595324081
0.500 10.0 20.0 50.0 80.0120
Indeno[1,2,3-cd]pyrene QuaFPRY 680 20524 35055 114626 162242290818
0.500 10.0 20.0 50.0 80.0120
Dibenz(a,h)anthracene QuaFPRY 624 19276 37340 116311 162253289112
0.500 10.0 20.0 50.0 80.0120
Benzo[g,h,i]perylene AvePRY 9737 21876 38095 113316 161451284212
5.00 10.0 20.0 50.0 80.0120
2-Fluorophenol AveDCB 27007 56536 78793 189188 293278587708
5.00 10.0 20.0 50.0 80.0120
Phenol-d5 AveDCB 31440 65796 88914 214979 326300617160
5.00 10.0 20.0 50.0 80.0120
Nitrobenzene-d5 AveNPT 25404 56772 76600 196791 298910528774
5.00 10.0 20.0 50.0 80.0120
2-Fluorobiphenyl AveANT 46332 105607 137214 342823 499061950013
5.00 10.0 20.0 50.0 80.0120
2,4,6-Tribromophenol AveANT 3562 8837 11894 33691 48819100994
5.00 10.0 20.0 50.0 80.0120
Terphenyl-d14 AveCRY 19152 45322 60848 178781 241181451642
5.00 10.0 20.0 50.0 80.0120
Curve Type Legend:Ave = Average ISTDQuaF = Quadratic ISTD forced zero
FORM VI 8270C 06/03/2010Page 308 of 623
FORM VII
Lab Name: Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC/MS SEMI VOA CONTINUING CALIBRATION DATA
0.25(mm)
460-13139-1
BNAMS10
05/18/2010 10:30
05/11/2010 14:17
05/11/2010 16:30
CCVIS 460-37818/2
Rtx-5MS
TestAmerica Edison
Lab File ID: p2878.d Conc. Units: ug/L
ANALYTE CURVE AVE RRF RRF MIN RRF CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
1,4-Dioxane Ave 0.26100.3059 42700 50000 -14.7 20.0
N-Nitrosodimethylamine Ave 0.72500.7617 47600 50000 -4.8 20.0
Pyridine Ave 1.3171.404 46900 50000 -6.2 20.0
Benzaldehyde Ave 0.46970.6080 38600 50000 -22.7* 20.0
Phenol Ave 1.5291.634 46800 50000 -6.4 20.0
Aniline Ave 1.8231.899 48000 50000 -4.0 20.0
Bis(2-chloroethyl)ether QuaF 1.2431.427 51900 50000 3.7 20.0
2-Chlorophenol Ave 1.3321.422 46800 50000 -6.4 20.0
Decane Ave 1.0821.129 47900 50000 -4.2 20.0
1,3-Dichlorobenzene Ave 1.6011.672 47900 50000 -4.3 20.0
1,4-Dichlorobenzene Ave 1.5751.651 47700 50000 -4.6 20.0
Benzyl alcohol Ave 0.76390.8084 47200 50000 -5.5 20.0
1,2-Dichlorobenzene Ave 1.4941.555 48000 50000 -3.9 20.0
2-Methylphenol Ave 1.0531.151 45700 50000 -8.5 20.0
bis (2-chloroisopropyl) ether
Ave 1.1921.278 46600 50000 -6.8 20.0
Acetophenone Ave 1.4871.620 45900 50000 -8.3 20.0
N-Nitrosodi-n-propylamine Ave 0.66030.7662 0.0500 43100 50000 -13.8 20.0
3 & 4 Methylphenol Ave 1.0021.174 42700 50000 -14.6 20.0
4-Methylphenol Ave 1.0061.172 42900 50000 -14.2 20.0
o-Toluidine Ave 2.3582.548 46300 50000 -7.5 20.0
Hexachloroethane Ave 0.58220.6070 48000 50000 -4.1 20.0
Nitrobenzene QuaF 0.48210.5183 48600 50000 -2.8 20.0
n,n'-Dimethylaniline Ave 1.8542.016 46000 50000 -8.0 20.0
Isophorone Ave 0.61920.6526 47400 50000 -5.1 20.0
2-Nitrophenol Ave 0.21390.2074 51500 50000 3.1 20.0
2,4-Dimethylphenol Ave 0.31630.3302 47900 50000 -4.2 20.0
Bis(2-chloroethoxy)methane Ave 0.38840.4026 48200 50000 -3.5 20.0
Benzoic acid Ave 0.16100.1440 55900 50000 11.8 20.0
2,4-Dichlorophenol Ave 0.28110.2890 48600 50000 -2.7 20.0
1,2,4-Trichlorobenzene Ave 0.32830.3311 49600 50000 -0.9 20.0
Naphthalene Ave 1.0671.123 47500 50000 -5.0 20.0
4-Chloroaniline Ave 0.41000.4295 47700 50000 -4.5 20.0
Hexachlorobutadiene Ave 0.17680.1819 48600 50000 -2.8 20.0
Caprolactam Ave 0.08990.0826 54400 50000 8.9 20.0
4-Chloro-3-methylphenol Ave 0.27400.2809 48800 50000 -2.5 20.0
2-Methylnaphthalene Ave 0.63840.6665 47900 50000 -4.2 20.0
1-Methylnaphthalene Ave 0.63370.6564 48300 50000 -3.5 20.0
Hexachlorocyclopentadiene Ave 0.36530.3230 0.0500 56600 50000 13.1 20.0
2-tertbutyl-4-methylphenol QuaF 0.42730.4327 49300 50000 -1.4 20.0
2,4,6-Trichlorophenol Ave 0.36680.3783 48500 50000 -3.0 20.0
FORM VII 8270C
06/03/2010Page 309 of 623
FORM VII
Lab Name: Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC/MS SEMI VOA CONTINUING CALIBRATION DATA
0.25(mm)
460-13139-1
BNAMS10
05/18/2010 10:30
05/11/2010 14:17
05/11/2010 16:30
CCVIS 460-37818/2
Rtx-5MS
TestAmerica Edison
Lab File ID: p2878.d Conc. Units: ug/L
ANALYTE CURVE AVE RRF RRF MIN RRF CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
2,4,5-Trichlorophenol Ave 0.36610.3698 49500 50000 -1.0 20.0
Diphenyl Ave 1.4611.520 48100 50000 -3.9 20.0
2-Chloronaphthalene Ave 1.1481.218 47200 50000 -5.7 20.0
Diphenyl ether Ave 0.84750.8835 48000 50000 -4.1 20.0
2-Nitroaniline Ave 0.36920.3605 51200 50000 2.4 20.0
Dimethylnaphthalene, total Ave 0.94261.001 47100 50000 -5.9 20.0
Dimethyl phthalate Ave 1.1881.180 50300 50000 0.7 20.0
Coumarin Ave 0.19840.1873 53000 50000 5.9 20.0
2,6-Dinitrotoluene Ave 0.28810.2731 52800 50000 5.5 20.0
Acenaphthylene Ave 1.8411.941 47400 50000 -5.2 20.0
3-Nitroaniline Ave 0.30480.2879 52900 50000 5.8 20.0
3,5-di-tert-butyl-4-hydroxytol
Ave 0.91860.9906 46400 50000 -7.3 20.0
Acenaphthene Ave 0.96521.082 44600 50000 -10.8 20.0
2,4-Dinitrophenol QuaF 0.14330.1029 0.0500 62600 50000 25.2* 20.0
4-Nitrophenol Ave 0.17830.1594 0.0500 55900 50000 11.9 20.0
2,4-Dinitrotoluene Ave 0.34030.3134 54300 50000 8.6 20.0
Dibenzofuran Ave 1.4841.566 47400 50000 -5.2 20.0
2-Naphthylamine Ave 0.90560.8641 52400 50000 4.8 20.0
Diethyl phthalate Ave 1.1361.099 51700 50000 3.3 20.0
4-Chlorophenyl phenyl ether Ave 0.49890.5155 48400 50000 -3.2 20.0
Fluorene Ave 1.1111.154 48100 50000 -3.7 20.0
4-Nitroaniline Ave 0.26650.2420 55100 50000 10.1 20.0
4,6-Dinitro-2-methylphenol Ave 0.13600.1102 61700 50000 23.4* 20.0
N-Nitrosodiphenylamine Ave 0.60440.6353 47600 50000 -4.9 20.0
1,2-Diphenylhydrazine Ave 0.95561.074 44500 50000 -11.0 20.0
4-Bromophenyl phenyl ether Ave 0.23270.2371 49100 50000 -1.9 20.0
Hexachlorobenzene Ave 0.23840.2460 48500 50000 -3.1 20.0
Atrazine Ave 0.18780.1847 50900 50000 1.7 20.0
Pentachlorophenol Ave 0.12450.1147 54300 50000 8.5 20.0
n-Octadecane Ave 0.44850.4828 46400 50000 -7.1 20.0
Phenanthrene Ave 1.0831.137 47600 50000 -4.7 20.0
Anthracene Ave 1.1101.137 48800 50000 -2.3 20.0
Carbazole Ave 0.96730.9543 50700 50000 1.4 20.0
Di-n-butyl phthalate Ave 1.1891.134 52400 50000 4.9 20.0
Fluoranthene Ave 0.95860.9014 53200 50000 6.3 20.0
Benzidine Ave 0.09500.1366 34800 50000 -30.5* 20.0
Pyrene Ave 1.6661.685 49400 50000 -1.1 20.0
Butyl benzyl phthalate Ave 0.71400.6608 54000 50000 8.1 20.0
2,3,7,8-TCDD (Screen) Ave 0.16140.1162 694 500 38.9* 20.0
Carbamazepine QuaF 0.51210.4515 50600 50000 1.2 20.0
FORM VII 8270C
06/03/2010Page 310 of 623
FORM VII
Lab Name: Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC/MS SEMI VOA CONTINUING CALIBRATION DATA
0.25(mm)
460-13139-1
BNAMS10
05/18/2010 10:30
05/11/2010 14:17
05/11/2010 16:30
CCVIS 460-37818/2
Rtx-5MS
TestAmerica Edison
Lab File ID: p2878.d Conc. Units: ug/L
ANALYTE CURVE AVE RRF RRF MIN RRF CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
3,3'-Dichlorobenzidine Ave 0.32680.3111 52500 50000 5.1 20.0
Benzo[a]anthracene Ave 1.1041.123 49100 50000 -1.7 20.0
Bis(2-ethylhexyl) phthalate Ave 0.88510.8303 53300 50000 6.6 20.0
Chrysene Ave 0.99291.018 48800 50000 -2.4 20.0
Di-n-octyl phthalate QuaF 1.8711.509 58800 50000 17.6 20.0
Benzo[b]fluoranthene Ave 1.2181.122 54300 50000 8.6 20.0
Benzo[k]fluoranthene Ave 1.3061.226 53200 50000 6.5 20.0
Benzo[a]pyrene Ave 1.0401.026 50700 50000 1.4 20.0
Indeno[1,2,3-cd]pyrene QuaF 0.83640.7933 48200 50000 -3.6 20.0
Dibenz(a,h)anthracene QuaF 0.85780.7885 48800 50000 -2.4 20.0
Benzo[g,h,i]perylene Ave 0.83710.8438 49600 50000 -0.8 20.0
2-Fluorophenol Ave 1.2601.347 46800 50000 -6.5 20.0
Phenol-d5 Ave 1.4161.519 46600 50000 -6.8 20.0
Nitrobenzene-d5 Ave 0.39200.3897 50300 50000 0.6 20.0
2-Fluorobiphenyl Ave 1.3981.459 47900 50000 -4.2 20.0
2,4,6-Tribromophenol Ave 0.15310.1325 57800 50000 15.5 20.0
Terphenyl-d14 Ave 1.1111.053 52800 50000 5.5 20.0
FORM VII 8270C
06/03/2010Page 311 of 623
Data File: /chem/BNAMS10.i/8270/05-11-10a/11may10.b/p2720.d Report Date: 11-May-2010 15:13
TestAmerica
Data file : /chem/BNAMS10.i/8270/05-11-10a/11may10.b/p2720.dLab Smp Id: DFTPP-459998 Inj Date : 11-MAY-2010 13:45 Operator : BNA2 Inst ID: BNAMS10.iSmp Info : DFTPP-459998Misc Info : Comment : Method : /chem/BNAMS10.i/8270/05-11-10a/11may10.b/BNADFTPP.mMeth Date : 11-May-2010 15:12 monica Quant Type: ESTDCal Date : Cal File: Als bottle: 1 QC Sample: DFTPPDil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Sample Matrix: None
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT MASS RESPONSE ( ug/L) ( ug/L) TARGET RANGE RATIO
== ====== ======== ==== ======== ======= ======= ============ =====
1 dftpp CAS #:
4.598 4.700 -0.102 198 19020 0.00- 100.00 100.00
4.598 4.700 -0.102 51 6950 30.00- 60.00 36.54
4.598 4.700 -0.102 68 0 0.00- 2.00 0.00
4.598 4.700 -0.102 69 7985 0.00- 0.00 41.98
4.598 4.700 -0.102 70 0 0.00- 2.00 0.00
4.598 4.700 -0.102 127 11097 40.00- 60.00 58.34
4.598 4.700 -0.102 197 0 0.00- 1.00 0.00
4.598 4.700 -0.102 199 1335 5.00- 9.00 7.02
4.598 4.700 -0.102 275 4924 10.00- 30.00 25.89
4.598 4.700 -0.102 365 607 1.00- 0.00 3.19
4.598 4.700 -0.102 441 2378 0.01- 100.00 74.17
4.598 4.700 -0.102 442 16043 40.00- 110.00 84.35
4.598 4.700 -0.102 443 3206 17.00- 23.00 19.98
-------------------------------------------------------------------------------
06/03/2010Page 312 of 623
Data File: p2720.d
Date: 11-MAY-2010 13:45
Client ID: Instrument: BNAMS10.i
Sample Info: DFTPP-459998 Operator: BNA2
06/03/2010Page 313 of 623
Data File: p2720.d
Date: 11-MAY-2010 13:45
Client ID: Instrument: BNAMS10.i
Sample Info: DFTPP-459998 Operator: BNA2
1 dftpp
% RELATIVE m/e ION ABUNDANCE CRITERIA ABUNDANCE
+-----+------------------------------------------+---------------------+| | | || 198 | Base Peak, 100% relative abundance | 100.00 || 51 | 30.00 - 60.00% of mass 198 | 36.54 || 68 | Less than 2.00% of mass 69 | 0.00 ( 0.00) || 69 | Mass 69 relative abundance | 41.98 || 70 | Less than 2.00% of mass 69 | 0.00 ( 0.00) || 127 | 40.00 - 60.00% of mass 198 | 58.34 || 197 | Less than 1.00% of mass 198 | 0.00 || 199 | 5.00 - 9.00% of mass 198 | 7.02 || 275 | 10.00 - 30.00% of mass 198 | 25.89 || 365 | Greater than 1.00% of mass 198 | 3.19 || 441 | 0.01 - 100.00% of mass 443 | 12.50 ( 74.17) || 442 | 40.00 - 110.00% of mass 198 | 84.35 || 443 | 17.00 - 23.00% of mass 442 | 16.86 ( 19.98) |+-----+------------------------------------------+---------------------+
06/03/2010Page 314 of 623
Data File: p2720.d
Date: 11-MAY-2010 13:45
Client ID: Instrument: BNAMS10.i
Sample Info: DFTPP-459998 Operator: BNA2
Data File: /chem/BNAMS10.i/8270/05-11-10a/11may10.b/p2720.dSpectrum: Average Spectrum: 4.592 to 4.604 min.
Location of Maximum: 198.00Number of points: 66
m/z Y m/z Y m/z Y m/z Y+------------------+------------------+------------------+------------------+| 39.00 444 | 101.00 174 | 186.00 2833 | 255.00 10406 || 50.00 1808 | 107.00 2857 | 187.00 685 | 256.00 1531 || 51.00 6950 | 108.00 220 | 196.00 467 | 258.00 470 || 52.00 225 | 110.00 5297 | 198.00 19016 | 273.00 168 || 57.00 234 | 111.00 805 | 199.00 1335 | 274.00 760 |+------------------+------------------+------------------+------------------+| 69.00 7985 | 117.00 2136 | 204.00 509 | 275.00 4924 || 74.00 884 | 127.00 11097 | 205.00 1205 | 276.00 598 || 75.00 1287 | 128.00 799 | 206.00 5093 | 277.00 195 || 76.00 239 | 129.00 4311 | 207.00 562 | 296.00 1307 || 77.00 9450 | 130.00 186 | 217.00 1211 | 323.00 406 |+------------------+------------------+------------------+------------------+| 78.00 526 | 141.00 221 | 221.00 959 | 365.00 607 || 79.00 557 | 148.00 454 | 223.00 168 | 423.00 816 || 80.00 236 | 156.00 191 | 224.00 2581 | 441.00 2378 || 81.00 339 | 167.00 1072 | 225.00 536 | 442.00 16043 || 93.00 1057 | 168.00 466 | 227.00 1040 | 443.00 3206 |+------------------+------------------+------------------+------------------+| 98.00 858 | 179.00 579 | 244.00 2009 | || 99.00 701 | 180.00 209 | 246.00 183 | |+------------------+------------------+------------------+------------------+
06/03/2010Page 315 of 623
Data File: /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2877.d Report Date: 18-May-2010 11:27
TestAmerica
Data file : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2877.dLab Smp Id: DFTPP-459998 Inj Date : 18-MAY-2010 10:12 Operator : BNA2 Inst ID: BNAMS10.iSmp Info : DFTPP-459998Misc Info : Comment : Method : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/BNADFTPP.mMeth Date : 11-May-2010 15:12 monica Quant Type: ESTDCal Date : Cal File: Als bottle: 1 QC Sample: DFTPPDil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Sample Matrix: NoneProcessing Host: hpd1
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT MASS RESPONSE ( ug/L) ( ug/L) TARGET RANGE RATIO
== ====== ======== ==== ======== ======= ======= ============ =====
1 dftpp CAS #:
4.492 4.700 -0.208 198 33776 0.00- 100.00 98.20
4.492 4.700 -0.208 51 11271 30.00- 60.00 33.37
4.492 4.700 -0.208 68 0 0.00- 2.00 0.00
4.492 4.700 -0.208 69 12632 0.00- 0.00 37.40
4.492 4.700 -0.208 70 0 0.00- 2.00 0.00
4.492 4.700 -0.208 127 18545 40.00- 60.00 54.91
4.492 4.700 -0.208 197 0 0.00- 1.00 0.00
4.492 4.700 -0.208 199 2362 5.00- 9.00 6.99
4.492 4.700 -0.208 275 9158 10.00- 30.00 27.11
4.492 4.700 -0.208 365 1228 1.00- 0.00 3.64
4.492 4.700 -0.208 441 4875 0.01- 100.00 73.43
4.492 4.700 -0.208 442 34394 40.00- 110.00 101.83
4.492 4.700 -0.208 443 6639 17.00- 23.00 19.30
-------------------------------------------------------------------------------
06/03/2010Page 316 of 623
Data File: p2877.d
Date: 18-MAY-2010 10:12
Client ID: Instrument: BNAMS10.i
Sample Info: DFTPP-459998 Operator: BNA2
06/03/2010Page 317 of 623
Data File: p2877.d
Date: 18-MAY-2010 10:12
Client ID: Instrument: BNAMS10.i
Sample Info: DFTPP-459998 Operator: BNA2
1 dftpp
% RELATIVE m/e ION ABUNDANCE CRITERIA ABUNDANCE
+-----+------------------------------------------+---------------------+| | | || 198 | Base Peak, 100% relative abundance | 100.00 || 51 | 30.00 - 60.00% of mass 198 | 33.37 || 68 | Less than 2.00% of mass 69 | 0.00 ( 0.00) || 69 | Mass 69 relative abundance | 37.40 || 70 | Less than 2.00% of mass 69 | 0.00 ( 0.00) || 127 | 40.00 - 60.00% of mass 198 | 54.91 || 197 | Less than 1.00% of mass 198 | 0.00 || 199 | 5.00 - 9.00% of mass 198 | 6.99 || 275 | 10.00 - 30.00% of mass 198 | 27.11 || 365 | Greater than 1.00% of mass 198 | 3.64 || 441 | 0.01 - 100.00% of mass 443 | 14.43 ( 73.43) || 442 | 40.00 - 110.00% of mass 198 | 101.83 || 443 | 17.00 - 23.00% of mass 442 | 19.66 ( 19.30) |+-----+------------------------------------------+---------------------+
06/03/2010Page 318 of 623
Data File: p2877.d
Date: 18-MAY-2010 10:12
Client ID: Instrument: BNAMS10.i
Sample Info: DFTPP-459998 Operator: BNA2
Data File: /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2877.dSpectrum: Average Spectrum: 4.486 to 4.498 min.
Location of Maximum: 442.00Number of points: 95
m/z Y m/z Y m/z Y m/z Y+------------------+------------------+------------------+------------------+| 39.00 830 | 108.00 721 | 180.00 884 | 245.00 231 || 50.00 3241 | 110.00 8893 | 181.00 223 | 246.00 534 || 51.00 11271 | 111.00 1318 | 185.00 521 | 255.00 18960 || 52.00 568 | 117.00 3401 | 186.00 4726 | 256.00 2865 || 56.00 357 | 122.00 190 | 187.00 1373 | 258.00 998 |+------------------+------------------+------------------+------------------+| 57.00 682 | 123.00 451 | 192.00 396 | 265.00 201 || 63.00 480 | 127.00 18544 | 193.00 205 | 273.00 517 || 69.00 12632 | 128.00 1517 | 196.00 894 | 274.00 1789 || 74.00 1100 | 129.00 7249 | 198.00 33776 | 275.00 9158 || 75.00 2261 | 130.00 466 | 199.00 2362 | 276.00 1221 |+------------------+------------------+------------------+------------------+| 76.00 638 | 135.00 502 | 204.00 1271 | 277.00 803 || 77.00 15462 | 141.00 844 | 205.00 2193 | 296.00 2403 || 78.00 948 | 147.00 462 | 206.00 8503 | 297.00 171 || 79.00 883 | 148.00 825 | 207.00 1251 | 323.00 862 || 80.00 626 | 155.00 446 | 208.00 200 | 334.00 262 |+------------------+------------------+------------------+------------------+| 81.00 1026 | 156.00 671 | 211.00 171 | 365.00 1228 || 86.00 167 | 161.00 172 | 217.00 2081 | 372.00 232 || 93.00 1728 | 165.00 356 | 221.00 1660 | 423.00 1908 || 98.00 1197 | 167.00 1898 | 223.00 492 | 424.00 203 || 99.00 982 | 168.00 634 | 224.00 4614 | 441.00 4875 |+------------------+------------------+------------------+------------------+| 101.00 511 | 174.00 174 | 225.00 1208 | 442.00 34392 || 104.00 169 | 175.00 518 | 227.00 1851 | 443.00 6639 || 105.00 350 | 177.00 180 | 229.00 176 | 444.00 311 || 107.00 4880 | 179.00 1212 | 244.00 3469 | |+------------------+------------------+------------------+------------------+
06/03/2010Page 319 of 623
FORM IForm 1GC/MS SEMI VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: MB 460-37564/1-A
Matrix: p2879.dLab File ID:
Date Collected:8270CAnalysis Method:
Solid
TestAmerica Edison
Level: (low/med)
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Analyzed:
Date Extracted:
Dilution Factor:
Extract. Method: 05/17/2010 09:00
1
3541
05/18/2010 10:57
Low
N
1(mL)
% Moisture:
Sample wt/vol: 15.02(g)
Analysis Batch No.: 37818 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Phenol108-95-2 330 330 40U
2-Chlorophenol95-57-8 330 330 44U
2-Nitrophenol88-75-5 330 330 54U
2,4-Dimethylphenol105-67-9 330 330 53U
2,4-Dichlorophenol120-83-2 330 330 53U
4-Chloro-3-methylphenol59-50-7 330 330 55U
2,4,6-Trichlorophenol88-06-2 330 330 59U
2,4-Dinitrophenol51-28-5 1000 1000 70U
4-Nitrophenol100-02-7 1000 1000 85U
4,6-Dinitro-2-methylphenol534-52-1 1000 1000 160U
Pentachlorophenol87-86-5 1000 1000 160U
N-Nitrosodimethylamine62-75-9 330 330 34U
Bis(2-chloroethyl)ether111-44-4 33 33 6.9U
1,3-Dichlorobenzene541-73-1 330 330 45U
1,4-Dichlorobenzene106-46-7 330 330 49U
1,2-Dichlorobenzene95-50-1 330 330 53U
N-Nitrosodi-n-propylamine621-64-7 33 33 4.4U
Hexachloroethane67-72-1 33 33 5.6U
Nitrobenzene98-95-3 33 33 7.4U
Isophorone78-59-1 330 330 38U
Bis(2-chloroethoxy)methane111-91-1 330 330 47U
1,2,4-Trichlorobenzene120-82-1 33 33 5.4U
Naphthalene91-20-3 330 330 48U
Hexachlorobutadiene87-68-3 67 67 13U
Hexachlorocyclopentadiene77-47-4 330 330 97U
2-Chloronaphthalene91-58-7 330 330 47U
Dimethyl phthalate131-11-3 330 330 45U
Acenaphthylene208-96-8 330 330 47U
2,6-Dinitrotoluene606-20-2 67 67 8.4U
Acenaphthene83-32-9 330 330 47U
2,4-Dinitrotoluene121-14-2 67 67 9.6U
Diethyl phthalate84-66-2 330 330 44U
4-Chlorophenyl phenyl ether7005-72-3 330 330 57U
Fluorene86-73-7 330 330 56U
FORM I 8270C
06/03/2010Page 320 of 623
FORM IForm 1GC/MS SEMI VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: MB 460-37564/1-A
Matrix: p2879.dLab File ID:
Date Collected:8270CAnalysis Method:
Solid
TestAmerica Edison
Level: (low/med)
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Analyzed:
Date Extracted:
Dilution Factor:
Extract. Method: 05/17/2010 09:00
1
3541
05/18/2010 10:57
Low
N
1(mL)
% Moisture:
Sample wt/vol: 15.02(g)
Analysis Batch No.: 37818 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
N-Nitrosodiphenylamine86-30-6 330 330 54U
4-Bromophenyl phenyl ether101-55-3 330 330 59U
Hexachlorobenzene118-74-1 33 33 4.6U
Phenanthrene85-01-8 330 330 58U
Anthracene120-12-7 330 330 58U
Di-n-butyl phthalate84-74-2 330 330 51U
Fluoranthene206-44-0 330 330 55U
Pyrene129-00-0 330 330 57U
Benzidine92-87-5 330 330 70U
Butyl benzyl phthalate85-68-7 330 330 39U
3,3'-Dichlorobenzidine91-94-1 670 670 73U
Benzo[a]anthracene56-55-3 33 33 6.1U
Chrysene218-01-9 330 330 48U
Bis(2-ethylhexyl) phthalate117-81-7 330 330 44U
Di-n-octyl phthalate117-84-0 330 330 39U
Benzo[b]fluoranthene205-99-2 33 33 4.9U
Benzo[k]fluoranthene207-08-9 33 33 4.6U
Benzo[a]pyrene50-32-8 33 33 4.1U
Indeno[1,2,3-cd]pyrene193-39-5 33 33 5.3U
Dibenz(a,h)anthracene53-70-3 33 33 4.0U
Benzo[g,h,i]perylene191-24-2 330 330 35U
bis (2-chloroisopropyl) ether108-60-1 330 330 43U
SURROGATE %RECCAS NO. LIMITS Q
4165-60-0 Nitrobenzene-d5 80 38-105
4165-62-2 Phenol-d5 82 41-118
1718-51-0 Terphenyl-d14 93 16-151
118-79-6 2,4,6-Tribromophenol 82 10-120
367-12-4 2-Fluorophenol 76 37-125
321-60-8 2-Fluorobiphenyl 78 40-109
FORM I 8270C
06/03/2010Page 321 of 623
FORM IForm 1GC/MS SEMI VOA ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: MB 460-37564/1-A
Matrix: p2879.dLab File ID:
Date Collected:8270CAnalysis Method:
Solid
TestAmerica Edison
Level: (low/med)
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Analyzed:
Date Extracted:
Dilution Factor:
Extract. Method: 05/17/2010 09:00
1
3541
05/18/2010 10:57
Low
N
1(mL)
% Moisture:
Sample wt/vol: 15.02(g)
Analysis Batch No.: 37818 ug/KgUnits:
Number TICs Found: TIC Result Total: 170972
QRTCOMPOUND NAME RESULTCAS NO.
Unknown Aldol Condensate-1 497 2.30 T A J
Unknown Aldol Condensate-2 16600 2.72 T A J
FORM I-TIC 8270C
06/03/2010Page 322 of 623
Data File: /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2879.d Report Date: 19-May-2010 14:51
TestAmerica
SEMI-VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2879.dLab Smp Id: MB 460-37564/1-A Inj Date : 18-MAY-2010 10:57 Operator : BNAMS 4 Inst ID: BNAMS10.iSmp Info : MB 460-37564/1-AMisc Info : Comment : Method : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/8270C_08SP.mMeth Date : 18-May-2010 11:53 czhao Quant Type: ISTDCal Date : 11-MAY-2010 16:30 Cal File: p2726.dAls bottle: 3 QC Sample: BLANKDil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd1
Concentration Formula: Amt * DF * Uf*1000*Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorUf 1.00000 ng unit correction factorVt 1.00000 Volume of final extract (ml)Ws 15.00000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE (ug/ml) (ug/Kg)
========================== ==== == ====== ====== ======== ======= =======
$ 16 2-Fluorophenol (SUR) 112 2.963 2.928 (0.704) 494962 75.6545 5000
$ 17 Phenol-d5 (SUR) 99 3.850 3.862 (0.915) 606994 82.2603 5500
* 79 1,4-Dichlorobenzene-d4 152 4.208 4.214 (1.000) 194268 40.0000
23 1,2-Dichlorobenzene 146 4.379 4.385 (1.040) 2312 0.30611 20(aH)
$ 76 Nitrobenzene-d5 (SUR) 82 4.767 4.778 (0.867) 269227 39.9815 2700
* 80 Naphthalene-d8 136 5.495 5.507 (1.000) 691224 40.0000
$ 77 2-Fluorobiphenyl (SUR) 172 6.588 6.594 (0.908) 524401 38.9435 2600
* 82 Acenaphthene-d10 164 7.258 7.264 (1.000) 369280 40.0000
$ 18 2,4,6-Tribromophenol (SUR) 330 8.039 8.045 (1.108) 100304 82.0008 5500
* 83 Phenanthrene-d10 188 8.727 8.733 (1.000) 486284 40.0000
$ 78 Terphenyl-d14 244 10.307 10.307 (0.898) 326248 46.3329 3100
* 81 Chrysene-d12 240 11.482 11.494 (1.000) 267422 40.0000
* 84 Perylene-d12 264 13.398 13.404 (1.000) 185780 40.0000
06/03/2010Page 323 of 623
Data File: /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2879.d Report Date: 19-May-2010 14:51
QC Flag Legend
a - Target compound detected but, quantitated amountBelow Limit Of Quantitation(BLOQ).
H - Operator selected an alternate compound hit.
06/03/2010Page 324 of 623
Data File: /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2879.d Report Date: 19-May-2010 14:51
TestAmerica
SEMI-VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2879.dLab Smp Id: MB 460-37564/1-A Inj Date : 18-MAY-2010 10:57 Operator : BNAMS 4 Inst ID: BNAMS10.iSmp Info : MB 460-37564/1-AMisc Info : Comment : Method : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/8270C_08SP.mMeth Date : 18-May-2010 11:53 czhao Quant Type: ISTDCal Date : 11-MAY-2010 16:30 Cal File: p2726.dAls bottle: 3 QC Sample: BLANKDil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd1
Concentration Formula: Amt * DF * Uf*1000*Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorUf 1.00000 ng unit correction factorVt 1.00000 Volume of final extract (ml)Ws 15.00000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
ISTD RT AREA AMOUNT======== ==== ====== ======
* 79 1,4-Dichlorobenzene-d4 4.208 1159126 40.000
CONCENTRATIONS QUANT
RT AREA ON-COL(ug/ml) FINAL(ug/Kg) QUAL LIBRARY LIB ENTRY CPND #
==== ==== ============= ============ ==== ======= ========= ======
Unknown Aldol Condensate-1 CAS #:
2.305 216311 7.46463068 500 0 0 79
Unknown Aldol Condensate-2 CAS #:
2.716 7203501 248.583797 16000 0 0 79
06/03/2010Page 325 of 623
Data File: p2879.d
Date: 18-MAY-2010 10:57
Client ID: Instrument: BNAMS10.i
Sample Info: MB 460-37564/1-A Operator: BNAMS 4
06/03/2010Page 326 of 623
Data File: p2879.d
Date: 18-MAY-2010 10:57
Client ID: Instrument: BNAMS10.i
Sample Info: MB 460-37564/1-A Operator: BNAMS 4
Retention Time: 2.30
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Unknown Aldol Condensate-1
3-Hexen-2-one 763-93-9 NIST02.l 3109 91 C6H10O 98
3-Penten-2-one, 4-methyl- 141-79-7 NIST02.l 3185 91 C6H10O 98
06/03/2010Page 327 of 623
Data File: p2879.d
Date: 18-MAY-2010 10:57
Client ID: Instrument: BNAMS10.i
Sample Info: MB 460-37564/1-A Operator: BNAMS 4
Retention Time: 2.72
Library Search Compound Match CAS Number Library Entry Quality Formula Weight
Unknown Aldol Condensate-2
2-Pentanone, 4-hydroxy-4-methyl- 123-42-2 NIST02.l 7951 50 C6H12O2 116
(+-)-4-Amino-4,5-dihydro-2(3H)-fur 16504-58-8 NIST02.l 3966 47 C4H7NO2 101
06/03/2010Page 328 of 623
FORM IForm 1GC/MS SEMI VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: LCS 460-37564/2-A
Matrix: p2880.dLab File ID:
Date Collected:8270CAnalysis Method:
Solid
TestAmerica Edison
Level: (low/med)
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Analyzed:
Date Extracted:
Dilution Factor:
Extract. Method: 05/17/2010 09:00
1
3541
05/18/2010 11:25
Low
N
1(mL)
% Moisture:
Sample wt/vol: 15.00(g)
Analysis Batch No.: 37818 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Phenol108-95-2 4950 330 41
2-Chlorophenol95-57-8 5140 330 44
2-Nitrophenol88-75-5 5640 330 54
2,4-Dimethylphenol105-67-9 5280 330 53
2,4-Dichlorophenol120-83-2 5340 330 53
4-Chloro-3-methylphenol59-50-7 5690 330 56
2,4,6-Trichlorophenol88-06-2 5360 330 59
2,4-Dinitrophenol51-28-5 1100 1000 70
4-Nitrophenol100-02-7 6490 1000 85
4,6-Dinitro-2-methylphenol534-52-1 2180 1000 160
Pentachlorophenol87-86-5 4830 1000 160
N-Nitrosodimethylamine62-75-9 2550 330 34
Bis(2-chloroethyl)ether111-44-4 3020 33 6.9
1,3-Dichlorobenzene541-73-1 2490 330 45
1,4-Dichlorobenzene106-46-7 2500 330 49
1,2-Dichlorobenzene95-50-1 2570 330 53
N-Nitrosodi-n-propylamine621-64-7 3040 33 4.4
Hexachloroethane67-72-1 2480 33 5.6
Nitrobenzene98-95-3 2640 33 7.4
Isophorone78-59-1 2850 330 38
Bis(2-chloroethoxy)methane111-91-1 2860 330 47
1,2,4-Trichlorobenzene120-82-1 2740 33 5.4
Naphthalene91-20-3 2710 330 48
Hexachlorobutadiene87-68-3 2710 67 13
Hexachlorocyclopentadiene77-47-4 3110 330 97
2-Chloronaphthalene91-58-7 2700 330 47
Dimethyl phthalate131-11-3 2960 330 45
Acenaphthylene208-96-8 2780 330 47
2,6-Dinitrotoluene606-20-2 3130 67 8.4
Acenaphthene83-32-9 2840 330 47
2,4-Dinitrotoluene121-14-2 3200 67 9.7
Diethyl phthalate84-66-2 3000 330 44
4-Chlorophenyl phenyl ether7005-72-3 2910 330 57
Fluorene86-73-7 2890 330 56
FORM I 8270C
06/03/2010Page 329 of 623
FORM IForm 1GC/MS SEMI VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: LCS 460-37564/2-A
Matrix: p2880.dLab File ID:
Date Collected:8270CAnalysis Method:
Solid
TestAmerica Edison
Level: (low/med)
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Analyzed:
Date Extracted:
Dilution Factor:
Extract. Method: 05/17/2010 09:00
1
3541
05/18/2010 11:25
Low
N
1(mL)
% Moisture:
Sample wt/vol: 15.00(g)
Analysis Batch No.: 37818 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
N-Nitrosodiphenylamine86-30-6 3110 330 54
4-Bromophenyl phenyl ether101-55-3 2910 330 59
Hexachlorobenzene118-74-1 2940 33 4.6
Phenanthrene85-01-8 2850 330 58
Anthracene120-12-7 2870 330 58
Di-n-butyl phthalate84-74-2 2980 330 51
Fluoranthene206-44-0 3040 330 55
Pyrene129-00-0 2850 330 57
Benzidine92-87-5 169 330 70J
Butyl benzyl phthalate85-68-7 3010 330 39
3,3'-Dichlorobenzidine91-94-1 2870 670 73
Benzo[a]anthracene56-55-3 2880 33 6.1
Chrysene218-01-9 2900 330 48
Bis(2-ethylhexyl) phthalate117-81-7 3010 330 44
Di-n-octyl phthalate117-84-0 3130 330 39
Benzo[b]fluoranthene205-99-2 3060 33 4.9
Benzo[k]fluoranthene207-08-9 2990 33 4.6
Benzo[a]pyrene50-32-8 2590 33 4.1
Indeno[1,2,3-cd]pyrene193-39-5 2870 33 5.3
Dibenz(a,h)anthracene53-70-3 2900 33 4.0
Benzo[g,h,i]perylene191-24-2 2980 330 35
bis (2-chloroisopropyl) ether108-60-1 2700 330 43
SURROGATE %RECCAS NO. LIMITS Q
4165-60-0 Nitrobenzene-d5 82 38-105
4165-62-2 Phenol-d5 78 41-118
1718-51-0 Terphenyl-d14 89 16-151
118-79-6 2,4,6-Tribromophenol 99 10-120
367-12-4 2-Fluorophenol 74 37-125
321-60-8 2-Fluorobiphenyl 80 40-109
FORM I 8270C
06/03/2010Page 330 of 623
Data File: /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2880.d Report Date: 19-May-2010 10:38
TestAmerica
SEMI-VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2880.dLab Smp Id: LCS 460-37564/2-A Inj Date : 18-MAY-2010 11:25 Operator : BNAMS 4 Inst ID: BNAMS10.iSmp Info : LCS 460-37564/2-AMisc Info : Comment : Method : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/8270C_08SP.mMeth Date : 18-May-2010 11:53 czhao Quant Type: ISTDCal Date : 11-MAY-2010 16:30 Cal File: p2726.dAls bottle: 4 QC Sample: BSDil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd1
Concentration Formula: Amt * DF * Uf*1000*Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorUf 1.00000 ng unit correction factorVt 1.00000 Volume of final extract (ml)Ws 15.00000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE (ug/ml) (ug/Kg)
========================== ==== == ====== ====== ======== ======= =======
106 1,4-Dioxane 88 1.658 1.576 (0.190) 43993 14.6436 980
19 N-Nitrosodimethylamine 74 1.864 1.799 (0.442) 128281 38.2990 2600
71 Pyridine 79 1.893 1.829 (0.449) 167336 27.1048 1800
$ 16 2-Fluorophenol (SUR) 112 2.963 2.928 (0.703) 441232 74.4848 5000
110 Benzaldehyde 77 3.773 3.768 (0.895) 49396 18.4739 1200
73 Aniline 93 3.885 3.885 (0.922) 252934 30.2868 2000
$ 17 Phenol-d5 (SUR) 99 3.862 3.862 (0.916) 520486 77.9028 5200
1 Phenol 94 3.879 3.874 (0.921) 533237 74.2322 4900
20 bis(2-Chloroethyl)ether 93 3.950 3.950 (0.937) 233807 45.2557 3000
2 2-Chlorophenol 128 4.009 4.009 (0.951) 481959 77.0624 5100
21 1,3-Dichlorobenzene 146 4.155 4.161 (0.986) 274147 37.2813 2500
* 79 1,4-Dichlorobenzene-d4 152 4.214 4.214 (1.000) 175899 40.0000
22 1,4-Dichlorobenzene 146 4.232 4.232 (1.004) 272442 37.5172 2500
06/03/2010Page 331 of 623
Data File: /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2880.d Report Date: 19-May-2010 10:38
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE (ug/ml) (ug/Kg)
========================== ==== == ====== ====== ======== ======= =======
74 Benzyl Alcohol 108 4.355 4.361 (1.033) 157889 44.4117 3000
23 1,2-Dichlorobenzene 146 4.385 4.385 (1.040) 263831 38.5798 2600
24 bis (2-chloroisopropyl) ether 45 4.490 4.496 (1.066) 227997 40.5580 2700
3 2-Methylphenol 108 4.473 4.479 (1.061) 390670 77.1847 5100
126 O-Toluidine 107 4.637 4.643 (1.100) 494679 44.1477 2900
104 Acetophenone 105 4.625 4.631 (1.098) 278784 39.1234 2600
25 N-Nitroso-di-n-propylamine 70 4.655 4.637 (1.105) 153582 45.5830 3000(M)
4 4-Methylphenol 108 4.637 4.643 (1.100) 398603 77.3341 5200
123 3 & 4 Methylphenol 108 4.637 4.643 (1.100) 398603 77.2164 5100
26 Hexachloroethane 117 4.725 4.731 (1.121) 99166 37.1507 2500
$ 76 Nitrobenzene-d5 (SUR) 82 4.772 4.778 (0.868) 239314 41.1500 2700
27 Nitrobenzene 77 4.796 4.802 (0.872) 303507 39.6708 2600
107 N,N-Dimethylaniline 120 4.802 4.808 (1.139) 339983 38.3526 2600
28 Isophorone 82 5.048 5.043 (0.918) 416526 42.7680 2800
5 2-Nitrophenol 139 5.119 5.119 (0.931) 261772 84.5523 5600
6 2,4-Dimethylphenol 122 5.172 5.172 (0.940) 390619 79.2531 5300
29 bis(2-Chloroethoxy)methane 93 5.260 5.266 (0.956) 257509 42.8542 2800
15 Benzoic Acid 122 5.284 5.313 (0.960) 47906 22.2915 1500
7 2,4-Dichlorophenol 162 5.366 5.366 (0.975) 345292 80.0479 5300
30 1,2,4-Trichlorobenzene 180 5.448 5.448 (0.990) 202736 41.0286 2700
* 80 Naphthalene-d8 136 5.501 5.507 (1.000) 596977 40.0000
31 Naphthalene 128 5.524 5.525 (1.004) 680965 40.6236 2700
32 4-Chloroaniline 127 5.577 5.583 (1.014) 191385 29.8547 2000
33 Hexachlorobutadiene 225 5.660 5.660 (1.029) 110356 40.6435 2700
111 Caprolactam 113 5.965 5.965 (1.084) 44462 36.0755 2400
8 4-Chloro-3-methylphenol 107 6.088 6.089 (1.107) 358022 85.4076 5700
34 2-Methylnaphthalene 142 6.218 6.224 (1.130) 431229 43.3529 2900
35 Hexachlorocyclopentadiene 237 6.388 6.388 (0.879) 115168 46.6046 3100
9 2,4,6-Trichlorophenol 196 6.512 6.512 (0.896) 232769 80.4132 5400
10 2,4,5-Trichlorophenol 196 6.553 6.553 (0.902) 229952 81.2645 5400
$ 77 2-Fluorobiphenyl (SUR) 172 6.594 6.594 (0.908) 448441 40.1821 2700
36 2-Chloronaphthalene 162 6.711 6.711 (0.924) 377950 40.5657 2700
102 Diphenyl 154 6.694 6.694 (0.922) 493491 42.4363 2800
103 Diphenyl Ether 170 6.794 6.800 (0.935) 276484 40.8990 2700
37 2-Nitroaniline 65 6.811 6.817 (0.938) 120656 43.7422 2900
38 Dimethylphthalate 163 6.999 7.005 (0.964) 401548 44.4747 3000
40 2,6-Dinitrotoluene 165 7.052 7.058 (0.971) 98206 46.9978 3100
39 Acenaphthylene 152 7.117 7.123 (0.980) 619163 41.6855 2800
41 3-Nitroaniline 138 7.222 7.223 (0.994) 78823 35.7801 2400
* 82 Acenaphthene-d10 164 7.264 7.264 (1.000) 306055 40.0000
42 Acenaphthene 154 7.293 7.299 (1.004) 352666 42.5846 2800
11 2,4-Dinitrophenol 184 7.322 7.328 (1.008) 13497 16.4582 1100
12 4-Nitrophenol 65 7.399 7.399 (1.019) 118788 97.3840 6500
43 Dibenzofuran 168 7.463 7.469 (1.028) 507113 42.3302 2800
44 2,4-Dinitrotoluene 165 7.452 7.458 (1.026) 115161 48.0253 3200
45 Diethylphthalate 149 7.698 7.704 (1.060) 378635 45.0233 3000
47 Fluorene 166 7.804 7.810 (1.074) 382181 43.2890 2900
06/03/2010Page 332 of 623
Data File: /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2880.d Report Date: 19-May-2010 10:38
CONCENTRATIONS
QUANT SIG ON-COLUMN FINAL
Compounds MASS RT EXP RT REL RT RESPONSE (ug/ml) (ug/Kg)
========================== ==== == ====== ====== ======== ======= =======
46 4-Chlorophenyl-phenylether 204 7.804 7.810 (1.074) 172113 43.6381 2900
48 4-Nitroaniline 138 7.828 7.834 (1.078) 76473 41.2995 2800
13 4,6-Dinitro-2-methylphenol 198 7.857 7.863 (0.900) 35370 32.6973 2200
49 N-Nitrosodiphenylamine 169 7.922 7.928 (0.908) 290812 46.6150 3100
75 1,2-Diphenylhydrazine 77 7.963 7.963 (0.912) 413314 39.1939 2600
$ 18 2,4,6-Tribromophenol (SUR) 330 8.045 8.045 (1.108) 100086 98.7255 6600
50 4-Bromophenyl-phenylether 248 8.286 8.292 (0.950) 101793 43.7193 2900
51 Hexachlorobenzene 284 8.356 8.357 (0.958) 106397 44.0462 2900
112 Atrazine 200 8.456 8.456 (0.969) 73116 40.3179 2700
14 Pentachlorophenol 266 8.550 8.550 (0.980) 81672 72.4759 4800
* 83 Phenanthrene-d10 188 8.727 8.733 (1.000) 392818 40.0000
52 Phenanthrene 178 8.750 8.756 (1.003) 477490 42.7720 2800
53 Anthracene 178 8.803 8.803 (1.009) 481158 43.1018 2900
54 Carbazole 167 8.962 8.962 (1.027) 405210 43.2382 2900
55 Di-n-butylphthalate 149 9.308 9.308 (1.067) 496960 44.6354 3000
56 Fluoranthene 202 9.925 9.925 (1.137) 403388 45.5680 3000
58 Benzidine 184 10.054 10.055 (1.152) 3394 2.53069 170(aR)
57 Pyrene 202 10.149 10.149 (0.883) 396245 42.6752 2800
$ 78 Terphenyl-d14 244 10.307 10.307 (0.897) 258602 44.5578 3000
59 Butylbenzylphthalate 149 10.830 10.830 (0.943) 164505 45.1765 3000
61 Benzo(a)anthracene 228 11.476 11.476 (0.999) 267543 43.2332 2900
60 3,3'-Dichlorobenzidine 252 11.447 11.447 (0.996) 73696 42.9941 2900
* 81 Chrysene-d12 240 11.488 11.494 (1.000) 220418 40.0000
62 Chrysene 228 11.523 11.524 (1.003) 243635 43.4486 2900
63 bis(2-Ethylhexyl)phthalate 149 11.523 11.524 (1.003) 206823 45.2018 3000
64 Di-n-octylphthalate 149 12.381 12.381 (0.924) 301629 46.9031 3100
65 Benzo(b)fluoranthene 252 12.881 12.881 (0.961) 212421 45.9154 3100
66 Benzo(k)fluoranthene 252 12.916 12.922 (0.964) 226488 44.7897 3000
67 Benzo(a)pyrene 252 13.321 13.327 (0.994) 164335 38.8351 2600
* 84 Perylene-d12 264 13.404 13.404 (1.000) 164936 40.0000
68 Indeno(1,2,3-cd)pyrene 276 14.908 14.908 (1.112) 153171 43.0472 2900
69 Dibenz(a,h)anthracene 278 14.943 14.943 (1.115) 157066 43.5201 2900
70 Benzo(g,h,i)perylene 276 15.319 15.319 (1.143) 155445 44.6788 3000
QC Flag Legend
a - Target compound detected but, quantitated amountBelow Limit Of Quantitation(BLOQ).
R - Spike/Surrogate failed recovery limits.M - Compound response manually integrated.
06/03/2010Page 333 of 623
Data File: p2880.d
Date: 18-MAY-2010 11:25
Client ID: Instrument: BNAMS10.i
Sample Info: LCS 460-37564/2-A Operator: BNAMS 4
06/03/2010Page 334 of 623
Manual Integration Report
Data File: p2880.dInj. Date and Time: 18-MAY-2010 11:25Instrument ID: BNAMS10.iClient ID: Compound: 25 N-Nitroso-di-n-propylamineCAS #: 621-64-7Report Date: 05/19/2010
Processing Integration Results
RT: 4.63
Response: 92099
Amount: 27
Conc: 1822
Manual Integration Results
RT: 4.65
Response: 153582
Amount: 46
Conc: 3039
Manually Integrated By: wahiedManual Integration Reason: Target Peak Misintegrated (extraneous area removed)
06/03/2010Page 335 of 623
FORM IForm 1GC/MS SEMI VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-1 2-3 MS
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-5 MS
Matrix: p2882.dLab File ID:
Date Collected:8270CAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 11:25
Level: (low/med)
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Analyzed:
Date Extracted:
Dilution Factor:
Extract. Method: 05/17/2010 09:00
1
3541
05/18/2010 12:18
Low
N
1(mL)
% Moisture: 6.5
Sample wt/vol: 15.04(g)
Analysis Batch No.: 37818 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Phenol108-95-2 5410 350 43
2-Chlorophenol95-57-8 5430 350 47
2-Nitrophenol88-75-5 5770 350 58
2,4-Dimethylphenol105-67-9 5560 350 57
2,4-Dichlorophenol120-83-2 5660 350 57
4-Chloro-3-methylphenol59-50-7 6080 350 59
2,4,6-Trichlorophenol88-06-2 4770 350 63
2,4-Dinitrophenol51-28-5 1100 1100 75U
4-Nitrophenol100-02-7 4630 1100 91
4,6-Dinitro-2-methylphenol534-52-1 191 1100 170J
Pentachlorophenol87-86-5 1600 1100 170
N-Nitrosodimethylamine62-75-9 2620 350 36
Bis(2-chloroethyl)ether111-44-4 3190 35 7.4
1,3-Dichlorobenzene541-73-1 2340 350 48
1,4-Dichlorobenzene106-46-7 2440 350 53
1,2-Dichlorobenzene95-50-1 2530 350 56
N-Nitrosodi-n-propylamine621-64-7 3240 35 4.7
Hexachloroethane67-72-1 2360 35 6.0
Nitrobenzene98-95-3 2690 35 7.9
Isophorone78-59-1 2980 350 41
Bis(2-chloroethoxy)methane111-91-1 3020 350 50
1,2,4-Trichlorobenzene120-82-1 2760 35 5.8
Naphthalene91-20-3 2740 350 52
Hexachlorobutadiene87-68-3 2630 71 14
Hexachlorocyclopentadiene77-47-4 3040 350 100
2-Chloronaphthalene91-58-7 2820 350 50
Dimethyl phthalate131-11-3 3030 350 48
Acenaphthylene208-96-8 2920 350 50
2,6-Dinitrotoluene606-20-2 3210 71 9.0
Acenaphthene83-32-9 2980 350 50
2,4-Dinitrotoluene121-14-2 3110 71 10
Diethyl phthalate84-66-2 3010 350 47
4-Chlorophenyl phenyl ether7005-72-3 3010 350 61
Fluorene86-73-7 2970 350 60
FORM I 8270C
06/03/2010Page 336 of 623
FORM IForm 1GC/MS SEMI VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-1 2-3 MS
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-5 MS
Matrix: p2882.dLab File ID:
Date Collected:8270CAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 11:25
Level: (low/med)
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Analyzed:
Date Extracted:
Dilution Factor:
Extract. Method: 05/17/2010 09:00
1
3541
05/18/2010 12:18
Low
N
1(mL)
% Moisture: 6.5
Sample wt/vol: 15.04(g)
Analysis Batch No.: 37818 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
N-Nitrosodiphenylamine86-30-6 3310 350 57
4-Bromophenyl phenyl ether101-55-3 3110 350 63
Hexachlorobenzene118-74-1 3080 35 4.9
Phenanthrene85-01-8 2930 350 62
Anthracene120-12-7 2970 350 62
Di-n-butyl phthalate84-74-2 2980 350 54
Fluoranthene206-44-0 3030 350 59
Pyrene129-00-0 3110 350 61
Benzidine92-87-5 89.3 350 75J
Butyl benzyl phthalate85-68-7 3090 350 41
3,3'-Dichlorobenzidine91-94-1 3100 710 78
Benzo[a]anthracene56-55-3 3010 35 6.5
Chrysene218-01-9 3100 350 51
Bis(2-ethylhexyl) phthalate117-81-7 3100 350 47
Di-n-octyl phthalate117-84-0 3080 350 42
Benzo[b]fluoranthene205-99-2 3160 35 5.2
Benzo[k]fluoranthene207-08-9 3090 35 4.9
Benzo[a]pyrene50-32-8 2660 35 4.3
Indeno[1,2,3-cd]pyrene193-39-5 3110 35 5.6
Dibenz(a,h)anthracene53-70-3 3000 35 4.2
Benzo[g,h,i]perylene191-24-2 3110 350 37
bis (2-chloroisopropyl) ether108-60-1 2780 350 46
SURROGATE %RECCAS NO. LIMITS Q
4165-60-0 Nitrobenzene-d5 80 38-105
4165-62-2 Phenol-d5 79 41-118
1718-51-0 Terphenyl-d14 91 16-151
118-79-6 2,4,6-Tribromophenol 67 10-120
367-12-4 2-Fluorophenol 74 37-125
321-60-8 2-Fluorobiphenyl 80 40-109
FORM I 8270C
06/03/2010Page 337 of 623
FORM IForm 1GC/MS SEMI VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-1 2-3 MSD
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-5 MSD
Matrix: p2883.dLab File ID:
Date Collected:8270CAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 11:25
Level: (low/med)
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Analyzed:
Date Extracted:
Dilution Factor:
Extract. Method: 05/17/2010 09:00
1
3541
05/18/2010 12:46
Low
N
1(mL)
% Moisture: 6.5
Sample wt/vol: 15.03(g)
Analysis Batch No.: 37818 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Phenol108-95-2 5170 350 43
2-Chlorophenol95-57-8 5350 350 47
2-Nitrophenol88-75-5 5620 350 58
2,4-Dimethylphenol105-67-9 5370 350 57
2,4-Dichlorophenol120-83-2 5440 350 57
4-Chloro-3-methylphenol59-50-7 5690 350 59
2,4,6-Trichlorophenol88-06-2 4670 350 63
2,4-Dinitrophenol51-28-5 1100 1100 75U
4-Nitrophenol100-02-7 4630 1100 91
4,6-Dinitro-2-methylphenol534-52-1 1100 1100 170U
Pentachlorophenol87-86-5 1530 1100 170
N-Nitrosodimethylamine62-75-9 2660 350 36
Bis(2-chloroethyl)ether111-44-4 3150 35 7.4
1,3-Dichlorobenzene541-73-1 2390 350 48
1,4-Dichlorobenzene106-46-7 2440 350 53
1,2-Dichlorobenzene95-50-1 2560 350 56
N-Nitrosodi-n-propylamine621-64-7 3100 35 4.7
Hexachloroethane67-72-1 2420 35 6.0
Nitrobenzene98-95-3 2700 35 7.9
Isophorone78-59-1 2900 350 41
Bis(2-chloroethoxy)methane111-91-1 2950 350 50
1,2,4-Trichlorobenzene120-82-1 2770 35 5.8
Naphthalene91-20-3 2780 350 52
Hexachlorobutadiene87-68-3 2720 72 14
Hexachlorocyclopentadiene77-47-4 3150 350 100
2-Chloronaphthalene91-58-7 2860 350 50
Dimethyl phthalate131-11-3 3060 350 48
Acenaphthylene208-96-8 2940 350 50
2,6-Dinitrotoluene606-20-2 3200 72 9.0
Acenaphthene83-32-9 2970 350 50
2,4-Dinitrotoluene121-14-2 3150 72 10
Diethyl phthalate84-66-2 3030 350 47
4-Chlorophenyl phenyl ether7005-72-3 3050 350 61
Fluorene86-73-7 3020 350 60
FORM I 8270C
06/03/2010Page 338 of 623
FORM IForm 1GC/MS SEMI VOA ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-1 2-3 MSD
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-5 MSD
Matrix: p2883.dLab File ID:
Date Collected:8270CAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 11:25
Level: (low/med)
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Analyzed:
Date Extracted:
Dilution Factor:
Extract. Method: 05/17/2010 09:00
1
3541
05/18/2010 12:46
Low
N
1(mL)
% Moisture: 6.5
Sample wt/vol: 15.03(g)
Analysis Batch No.: 37818 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
N-Nitrosodiphenylamine86-30-6 3320 350 58
4-Bromophenyl phenyl ether101-55-3 3130 350 63
Hexachlorobenzene118-74-1 3110 35 4.9
Phenanthrene85-01-8 3030 350 62
Anthracene120-12-7 3040 350 62
Di-n-butyl phthalate84-74-2 3160 350 54
Fluoranthene206-44-0 3230 350 59
Pyrene129-00-0 2980 350 61
Benzidine92-87-5 131 350 75J
Butyl benzyl phthalate85-68-7 3120 350 41
3,3'-Dichlorobenzidine91-94-1 3180 720 78
Benzo[a]anthracene56-55-3 3030 35 6.5
Chrysene218-01-9 3080 350 51
Bis(2-ethylhexyl) phthalate117-81-7 3130 350 47
Di-n-octyl phthalate117-84-0 3150 350 42
Benzo[b]fluoranthene205-99-2 3220 35 5.3
Benzo[k]fluoranthene207-08-9 3180 35 4.9
Benzo[a]pyrene50-32-8 2720 35 4.3
Indeno[1,2,3-cd]pyrene193-39-5 3150 35 5.6
Dibenz(a,h)anthracene53-70-3 3030 35 4.2
Benzo[g,h,i]perylene191-24-2 3170 350 37
bis (2-chloroisopropyl) ether108-60-1 2800 350 46
SURROGATE %RECCAS NO. LIMITS Q
4165-60-0 Nitrobenzene-d5 81 38-105
4165-62-2 Phenol-d5 75 41-118
1718-51-0 Terphenyl-d14 89 16-151
118-79-6 2,4,6-Tribromophenol 66 10-120
367-12-4 2-Fluorophenol 72 37-125
321-60-8 2-Fluorobiphenyl 82 40-109
FORM I 8270C
06/03/2010Page 339 of 623
Lab Name: Job No.:
SDG No.:
Instrument ID:
Analysis Batch Number:
GC/MS SEMI VOA ANALYSIS RUN LOG
DILUTION
FACTOR
COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID
TestAmerica Edison 460-13139-1
BNAMS10
37184
Start Date:
End Date: 05/11/2010 16:30
05/11/2010 13:45
DFTPP 460-37184/1 Rtx-5MS 0.25(mm)105/11/2010 13:45 p2720.d
ICIS 460-37184/2 Rtx-5MS 0.25(mm)105/11/2010 14:17 p2721.d
IC 460-37184/3 Rtx-5MS 0.25(mm)105/11/2010 14:43 p2722.d
IC 460-37184/4 Rtx-5MS 0.25(mm)105/11/2010 15:10 p2723.d
IC 460-37184/5 Rtx-5MS 0.25(mm)105/11/2010 15:36 p2724.d
IC 460-37184/6 Rtx-5MS 0.25(mm)105/11/2010 16:03 p2725.d
IC 460-37184/7 Rtx-5MS 0.25(mm)105/11/2010 16:30 p2726.d
8270C
06/03/2010Page 340 of 623
Lab Name: Job No.:
SDG No.:
Instrument ID:
Analysis Batch Number:
GC/MS SEMI VOA ANALYSIS RUN LOG
DILUTION
FACTOR
COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID
TestAmerica Edison 460-13139-1
BNAMS10
37818
Start Date:
End Date: 05/18/2010 20:25
05/18/2010 10:12
DFTPP 460-37818/1 Rtx-5MS 0.25(mm)105/18/2010 10:12 p2877.d
CCVIS 460-37818/2 Rtx-5MS 0.25(mm)105/18/2010 10:30 p2878.d
MB 460-37564/1-A Rtx-5MS 0.25(mm)105/18/2010 10:57 p2879.d
LCS 460-37564/2-A Rtx-5MS 0.25(mm)105/18/2010 11:25 p2880.d
460-13139-5 TB-1 2-3 Rtx-5MS 0.25(mm)105/18/2010 11:52 p2881.d
460-13139-5 MS TB-1 2-3 MS Rtx-5MS 0.25(mm)105/18/2010 12:18 p2882.d
460-13139-5 MSD TB-1 2-3 MSD Rtx-5MS 0.25(mm)105/18/2010 12:46 p2883.d
ZZZZZ Rtx-5MS 0.25(mm)105/18/2010 13:12
ZZZZZ Rtx-5MS 0.25(mm)105/18/2010 13:39
ZZZZZ Rtx-5MS 0.25(mm)105/18/2010 14:06
ZZZZZ Rtx-5MS 0.25(mm)105/18/2010 14:33
460-13139-2 TB-3 6-7 Rtx-5MS 0.25(mm)105/18/2010 15:00 p2888.d
ZZZZZ Rtx-5MS 0.25(mm)105/18/2010 15:27
ZZZZZ Rtx-5MS 0.25(mm)10005/18/2010 15:54
ZZZZZ Rtx-5MS 0.25(mm)505/18/2010 16:21
ZZZZZ Rtx-5MS 0.25(mm)505/18/2010 16:48
ZZZZZ Rtx-5MS 0.25(mm)505/18/2010 17:16
ZZZZZ Rtx-5MS 0.25(mm)205/18/2010 17:42
ZZZZZ Rtx-5MS 0.25(mm)105/18/2010 18:10
ZZZZZ Rtx-5MS 0.25(mm)505/18/2010 18:36
ZZZZZ Rtx-5MS 0.25(mm)105/18/2010 19:03
ZZZZZ Rtx-5MS 0.25(mm)105/18/2010 19:30
460-13139-7 TB-5 3-4 Rtx-5MS 0.25(mm)105/18/2010 19:58 p2899.d
460-13139-4 TB-2 5-6 Rtx-5MS 0.25(mm)105/18/2010 20:25 p2900.d
8270C
06/03/2010Page 341 of 623
Organic Prep Worksheet
Method: 3541
Analyst: Masongo, Charles
Batch Number: 460-37564 Date Open:
Batch End:
May 17 2010 9:00AM
May 17 2010 3:00PM
Lab ID Client ID Basis Final weight/volume of
sample
Position on the
SoxTherm
OP_Acid_SU_00010 OP_BN_SU_00010 OP8270SP_00012Initial weight/volume of
sample
Method Chain
MB~460-37564/1 15.02 g 1 mL 500 uL500 uL1033541, 8270C
LCS~460-37564/2 15.00 g 1 mL 500 uL500 uL500 uL1043541, 8270C
460-13139-E-5~MS TB-1 2-3 T 15.04 g 1 mL 500 uL500 uL500 uL1053541, 8270C
460-13139-E-5~MS
D
TB-1 2-3 T 15.03 g 1 mL 500 uL500 uL500 uL1063541, 8270C
460-13139-E-1 TB-3 2-3 15.00 g 1 mL 500 uL500 uL107
460-13139-E-2 TB-3 6-7 T 15.00 g 1 mL 500 uL500 uL1083541, 8270C
460-13139-E-3 TB-2 2-3 14.99 g 1 mL 500 uL500 uL109
460-13139-E-4 TB-2 5-6 T 15.05 g 1 mL 500 uL500 uL1103541, 8270C
460-13139-E-5 TB-1 2-3 T 15.02 g 1 mL 500 uL500 uL1113541, 8270C
460-13139-E-6 TB-1 5-6 15.02 g 1 mL 500 uL500 uL112
460-13139-E-7 TB-5 3-4 T 15.01 g 1 mL 500 uL500 uL1133541, 8270C
460-13139-E-8 TB-4 6-7 15.04 g 1 mL 500 uL500 uL114
460-13211-F-1 T 15.00 g 1 mL 500 uL500 uL1
460-13211-E-2 T 15.00 g 1 mL 500 uL500 uL2
First Start time: 9am
Person's name who did the prep: CM
Person's name who witnessed reagent drop: JR
First End time: 3pm
SOP Number: 3541
Balance ID: 28
Person's name who did the concentration: CM
Na2SO4 Lot Number: H52600
Solvent: MeCl2/Acetone mixture
Vendor lot number: G49E31
Blank Soil Lot Number: H52600
06/03/2010Page 342 of 623
Organic Prep Worksheet
Method: 3541
Analyst: Masongo, Charles
Batch Number: 460-37564 Date Open:
Batch End:
May 17 2010 9:00AM
May 17 2010 3:00PM
Lab ID Client ID Basis
Comments
Analysis commentMethod Chain
MB~460-37564/1 3541, 8270C
LCS~460-37564/2 3541, 8270C
460-13139-E-5~MS TB-1 2-3 T3541, 8270C
460-13139-E-5~MS
D
TB-1 2-3 T3541, 8270C
460-13139-E-1 TB-3 2-3
460-13139-E-2 TB-3 6-7 T3541, 8270C
460-13139-E-3 TB-2 2-3
460-13139-E-4 TB-2 5-6 T3541, 8270C
460-13139-E-5 TB-1 2-3 T3541, 8270C
460-13139-E-6 TB-1 5-6
460-13139-E-7 TB-5 3-4 T3541, 8270C
460-13139-E-8 TB-4 6-7
460-13211-F-1 T
460-13211-E-2 T
Batch Comment: BNA 8270C SOIL
06/03/2010Page 343 of 623
Method 8081AOrganochlorine Pesticides (GC) by
Method 8081A
06/03/2010Page 344 of 623
FORM II
GC SEMI VOA SURROGATE RECOVERY
Lab Name: Job No.: 460-13139-1
SDG No.:
Matrix: Solid Level: Low
TestAmerica Edison
GC Column (1): ID: (mm) GC Column (2): ID: (mm)CLP-2 0.53 CLP-1 0.53
#Lab Sample IDClient Sample ID # # #TCX1 TCX2 DCB1 DCB2
460-13139-2TB-3 6-7 115 112 125 105
460-13139-4TB-2 5-6 121 106 155 168 X
460-13139-5TB-1 2-3 117 113 138 118
460-13139-7TB-5 3-4 84 76 78 75
MB 460-37420/1-A 76 75 145 118
LCS 460-37420/2-A
75 71 93 92
460-13147-A-2-B MS
107 94 132 123
460-13147-A-2-C MSD
101 91 147 56 p
QC LIMITSQC LIMITSTCX = Tetrachloro-m-xylene 22-141
DCB = DCB Decachlorobiphenyl 10-165
FORM II 8081A
# Column to be used to flag recovery values
06/03/2010Page 345 of 623
GC SEMI VOA LAB CONTROL SAMPLE RECOVERY
FORM III
Job No.:Lab Name:
SDG No.:
Level:Matrix:Matrix:
Low
460-13139-1
Lab File ID: xf108820.dSolid
Lab ID: LCS 460-37420/2-A Client ID:
TestAmerica Edison
REC
%
REC
QC
LIMITSCONCENTRATION
(ug/Kg)
SPIKE
ADDED
(ug/Kg)
#
LCS LCS
COMPOUND
Aldrin 133 88.9 32-15267
alpha-BHC 133 96.3 41-14572
beta-BHC 133 104 28-15578
delta-BHC 133 121 31-15491
gamma-BHC (Lindane) 133 98.6 33-15274
4,4'-DDD 133 94.7 50-15471
4,4'-DDE 133 98.1 47-15074
4,4'-DDT 133 99.1 39-15474
Dieldrin 133 88.6 40-14766
Endosulfan I 133 93.6 42-14770
Endosulfan II 133 101 32-15076
Endosulfan sulfate 133 103 37-14377
Endrin 133 101 44-14976
Endrin aldehyde 133 103 34-14278
Heptachlor 133 93.0 32-15270
Heptachlor epoxide 133 97.0 33-14973
FORM III 8081A
# Column to be used to flag recovery and RPD values
06/03/2010Page 346 of 623
GC SEMI VOA LAB CONTROL SAMPLE RECOVERY
FORM III
Job No.:Lab Name:
SDG No.:
Level:Matrix:Matrix:
Low
460-13139-1
Lab File ID: xr108820.dSolid
Lab ID: LCS 460-37420/2-A Client ID:
TestAmerica Edison
REC
%
REC
QC
LIMITSCONCENTRATION
(ug/Kg)
SPIKE
ADDED
(ug/Kg)
#
LCS LCS
COMPOUND
Aldrin 133 82.2 32-15262
alpha-BHC 133 89.0 41-14567
beta-BHC 133 102 28-15576
delta-BHC 133 109 31-15482
gamma-BHC (Lindane) 133 90.2 33-15268
4,4'-DDD 133 93.4 50-15470
4,4'-DDE 133 94.8 47-15071
4,4'-DDT 133 97.2 39-15473
Dieldrin 133 89.6 40-14767
Endosulfan I 133 93.3 42-14770
Endosulfan II 133 101 32-15075
Endosulfan sulfate 133 101 37-14376
Endrin 133 104 44-14978
Endrin aldehyde 133 104 34-14278
Heptachlor 133 87.2 32-15265
Heptachlor epoxide 133 93.5 33-14970
FORM III 8081A
# Column to be used to flag recovery and RPD values
06/03/2010Page 347 of 623
GC SEMI VOA MATRIX SPIKE RECOVERY
FORM III
Job No.:Lab Name:
SDG No.:
Level:Matrix:Matrix:
Low
460-13139-1
Lab File ID: xf108822.dSolid
Lab ID: 460-13147-A-2-B MS Client ID:
TestAmerica Edison
LIMITS
COMPOUND
CONCENTRATION %
REC
QC
REC
SAMPLE
CONCENTRATION
SPIKE
ADDED
(ug/Kg) (ug/Kg) (ug/Kg)
#
MS MS
153 151 32-152Aldrin 997.7 U
153 154 41-145alpha-BHC 1007.7 U
153 153 28-155beta-BHC 1007.7 U
153 167 31-154delta-BHC 1097.7 U
153 155 33-152gamma-BHC (Lindane) 1017.7 U
153 159 50-1544,4'-DDD 1047.7 U
153 169 47-1504,4'-DDE 1107.7 U
153 162 39-1544,4'-DDT 1026.4 J
153 150 40-147Dieldrin 987.7 U
153 144 42-147Endosulfan I 947.7 U
153 152 32-150Endosulfan II 997.7 U
153 147 37-143Endosulfan sulfate 967.7 U
153 168 44-149Endrin 1097.7 U
153 145 34-142Endrin aldehyde 957.7 U
153 139 32-152Heptachlor 917.7 U
153 149 33-149Heptachlor epoxide 977.7 U
FORM III 8081A
# Column to be used to flag recovery and RPD values
06/03/2010Page 348 of 623
GC SEMI VOA MATRIX SPIKE RECOVERY
FORM III
Job No.:Lab Name:
SDG No.:
Level:Matrix:Matrix:
Low
460-13139-1
Lab File ID: xr108822.dSolid
Lab ID: 460-13147-A-2-B MS Client ID:
TestAmerica Edison
LIMITS
COMPOUND
CONCENTRATION %
REC
QC
REC
SAMPLE
CONCENTRATION
SPIKE
ADDED
(ug/Kg) (ug/Kg) (ug/Kg)
#
MS MS
153 127 32-152Aldrin 837.7 U
153 129 41-145alpha-BHC 857.7 U
153 128 28-155beta-BHC 847.7 U
153 142 31-154delta-BHC 937.7 U
153 130 33-152gamma-BHC (Lindane) 857.7 U
153 134 50-1544,4'-DDD 877.7 U
153 135 47-1504,4'-DDE 887.7 U
153 131 39-1544,4'-DDT 824.8 J
153 128 40-147Dieldrin 837.7 U
153 135 42-147Endosulfan I 887.7 U
153 123 32-150Endosulfan II 807.7 U
153 118 37-143Endosulfan sulfate 777.7 U
153 148 44-149Endrin 967.7 U
153 116 34-142Endrin aldehyde 767.7 U
153 137 32-152Heptachlor 907.7 U
153 132 33-149Heptachlor epoxide 867.7 U
FORM III 8081A
# Column to be used to flag recovery and RPD values
06/03/2010Page 349 of 623
GC SEMI VOA MATRIX SPIKE DUPLICATE RECOVERY
FORM III
Job No.:Lab Name:
SDG No.:
Level:Matrix:Matrix:
Low
460-13139-1
Lab File ID: xf108823.dSolid
Lab ID: 460-13147-A-2-C MSD Client ID:
TestAmerica Edison
COMPOUND
SPIKE
ADDED CONCENTRATION %
REC
%
RPD
QC LIMITS
RPD REC (ug/Kg) (ug/Kg)
#
MSD MSD
153 145 30 32-152Aldrin 495
153 145 30 41-145alpha-BHC 694
153 144 30 28-155beta-BHC 694
153 159 30 31-154delta-BHC 5103
153 147 30 33-152gamma-BHC (Lindane) 596
153 156 30 50-1544,4'-DDD 2102
153 161 30 47-1504,4'-DDE 5105
153 150 30 39-1544,4'-DDT 894
153 140 30 40-147Dieldrin 791
153 137 30 42-147Endosulfan I 589
153 145 30 32-150Endosulfan II 595
153 147 30 37-143Endosulfan sulfate 096
153 163 30 44-149Endrin 3106
153 137 30 34-142Endrin aldehyde 689
153 125 30 32-152Heptachlor 1082
153 140 30 33-149Heptachlor epoxide 692
FORM III 8081A
# Column to be used to flag recovery and RPD values
06/03/2010Page 350 of 623
GC SEMI VOA MATRIX SPIKE DUPLICATE RECOVERY
FORM III
Job No.:Lab Name:
SDG No.:
Level:Matrix:Matrix:
Low
460-13139-1
Lab File ID: xr108823.dSolid
Lab ID: 460-13147-A-2-C MSD Client ID:
TestAmerica Edison
COMPOUND
SPIKE
ADDED CONCENTRATION %
REC
%
RPD
QC LIMITS
RPD REC (ug/Kg) (ug/Kg)
#
MSD MSD
153 122 30 32-152Aldrin 480
153 122 30 41-145alpha-BHC 680
153 125 30 28-155beta-BHC 282
153 134 30 31-154delta-BHC 687
153 121 30 33-152gamma-BHC (Lindane) 779
153 118 30 50-1544,4'-DDD 1377
153 122 30 47-1504,4'-DDE 1179
153 118 30 39-1544,4'-DDT 1074
153 120 30 40-147Dieldrin 778
153 126 30 42-147Endosulfan I 782
153 113 30 32-150Endosulfan II 874
153 109 30 37-143Endosulfan sulfate 871
153 133 30 44-149Endrin 1087
153 95.9 30 34-142Endrin aldehyde 1963
153 122 30 32-152Heptachlor 1279
153 122 30 33-149Heptachlor epoxide 879
FORM III 8081A
# Column to be used to flag recovery and RPD values
06/03/2010Page 351 of 623
FORM IV
GC SEMI VOA METHOD BLANK SUMMARY
Lab Name:
SDG No.:
Job No.: 460-13139-1TestAmerica Edison
Date Analyzed:(1)
Instrument ID:(1)
GC Column:(1) ID:
Instrument ID:(2)
Date Extracted: 05/14/2010 09:15
Date Analyzed:(2)
GC Column:(2) ID:CLP-10.53(mm) 0.53(mm)
PESTGC1
05/17/2010 09:37
Lab File ID:(1) Lab File ID:(2)
Matrix: Solid
xr108835.d
Lab Sample ID: MB 460-37420/1-A
xf108835.d
05/17/2010 09:37
PESTGC1
CLP-2
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:
ANALYZED 2
DATEDATE
ANALYZED 1LAB SAMPLE IDCLIENT SAMPLE ID
LCS 460-37420/2-A 05/17/2010 05:43 05/17/2010 05:43
460-13147-A-2-B MS 05/17/2010 06:36 05/17/2010 06:36
460-13147-A-2-C MSD 05/17/2010 06:50 05/17/2010 06:50
460-13139-2TB-3 6-7 05/17/2010 08:00 05/17/2010 08:00
460-13139-4TB-2 5-6 05/17/2010 08:27 05/17/2010 08:27
460-13139-5TB-1 2-3 05/17/2010 08:41 05/17/2010 08:41
460-13139-7TB-5 3-4 05/17/2010 09:09 05/17/2010 09:09
FORM IV 8081A
06/03/2010Page 352 of 623
PESTICIDES ANALYTICAL SEQUENCE
Lab Name: Job No.:
SDG No.:
FORM VIII
TestAmerica Edison 460-13139-1
Calibration ID:
Calibration Start Date:Instrument ID: PESTGC1
GC Column:
6135
Calibration End Date:
05/11/2010 12:47
05/11/2010 13:42CLP-2 ID: 0.53(mm)
THE ANALYTICAL SEQUENCE OF BLANKS, SAMPLES, STANDARDS, MS/MSDs AND LCSs IS GIVEN BELOW:
# #RT RT
TCX DCB
UPPER LIMIT
LOWER LIMIT
2.34
2.24
10.43
10.23
SURROGATE RT FROM CONTINUING CALIBRATION 2.29 10.33
LAB SAMPLE ID DATE ANALYZEDCLIENT SAMPLE ID LAB FILE ID
CCVRT 460-37575/5 05/17/2010 05:29 2.29 10.33xf108819.d
LCS 460-37420/2-A 05/17/2010 05:43 2.30 10.34xf108820.d
460-13147-A-2-B MS 05/17/2010 06:36 2.29 10.33xf108822.d
460-13147-A-2-C MSD 05/17/2010 06:50 2.29 10.33xf108823.d
460-13139-2 05/17/2010 08:00 2.29 10.33TB-3 6-7 xf108828.d
460-13139-4 05/17/2010 08:27 2.29 10.33TB-2 5-6 xf108830.d
460-13139-5 05/17/2010 08:41 2.28 10.33TB-1 2-3 xf108831.d
460-13139-7 05/17/2010 09:09 2.29 10.33TB-5 3-4 xf108833.d
MB 460-37420/1-A 05/17/2010 09:37 2.28 10.33xf108835.d
CCV 460-37575/23 05/17/2010 10:04 2.29 10.33xf108837.d
TCX = Tetrachloro-m-xylene
DCB = DCB Decachlorobiphenyl
TCX RT Limit = ± 0.05 minutes of surrogate RTDCB RT Limit = ± 0.10 minutes of surrogate RT
# Column used to flag values outside QC limits
FORM VIII 8081A
06/03/2010Page 353 of 623
PESTICIDES ANALYTICAL SEQUENCE
Lab Name: Job No.:
SDG No.:
FORM VIII
TestAmerica Edison 460-13139-1
Calibration ID:
Calibration Start Date:Instrument ID: PESTGC1
GC Column:
6134
Calibration End Date:
05/11/2010 12:47
05/11/2010 13:42CLP-1 ID: 0.53(mm)
THE ANALYTICAL SEQUENCE OF BLANKS, SAMPLES, STANDARDS, MS/MSDs AND LCSs IS GIVEN BELOW:
# #RT RT
TCX DCB
UPPER LIMIT
LOWER LIMIT
2.04
1.94
9.61
9.41
SURROGATE RT FROM CONTINUING CALIBRATION 1.99 9.51
LAB SAMPLE ID DATE ANALYZEDCLIENT SAMPLE ID LAB FILE ID
CCVRT 460-37575/5 05/17/2010 05:29 1.99 9.51xr108819.d
LCS 460-37420/2-A 05/17/2010 05:43 1.98 9.52xr108820.d
460-13147-A-2-B MS 05/17/2010 06:36 1.99 9.51xr108822.d
460-13147-A-2-C MSD 05/17/2010 06:50 1.99 9.51xr108823.d
460-13139-2 05/17/2010 08:00 1.99 9.51TB-3 6-7 xr108828.d
460-13139-4 05/17/2010 08:27 1.99 9.51TB-2 5-6 xr108830.d
460-13139-5 05/17/2010 08:41 1.98 9.51TB-1 2-3 xr108831.d
460-13139-7 05/17/2010 09:09 1.99 9.51TB-5 3-4 xr108833.d
MB 460-37420/1-A 05/17/2010 09:37 1.98 9.51xr108835.d
CCV 460-37575/23 05/17/2010 10:04 1.98 9.51xr108837.d
TCX = Tetrachloro-m-xylene
DCB = DCB Decachlorobiphenyl
TCX RT Limit = ± 0.05 minutes of surrogate RTDCB RT Limit = ± 0.10 minutes of surrogate RT
# Column used to flag values outside QC limits
FORM VIII 8081A
06/03/2010Page 354 of 623
FORM XForm 1
Client Sample ID:
Lab Name: Job No.:
SDG No.:
Lab Sample ID: 460-13139-4
Instrument ID (1): Instrument ID (2):
Date Analyzed (1): Date Analyzed (2):
GC Column (1): ID: GC Column (2): ID:
TB-2 5-6
TestAmerica Edison 460-13139-1
IDENTIFICATION SUMMARYForm 1
0.53(mm) 0.53(mm)
05/17/2010 08:27 05/17/2010 08:27
PESTGC1 PESTGC1
CLP-2 CLP-1
ANALYTE COL PEAK RTRT WINDOW
FROM TO PEAK MEANRPD
CONCENTRATION
7.297.157.2214,4'-DDE 13 43.2
5.275.135.192 8.6
7.567.427.521Dieldrin 10 60.0
6.045.905.982 5.5
8.037.897.9614,4'-DDD 55 32.5
6.806.666.732 40
8.408.268.3314,4'-DDT 29 7.8
7.357.217.282 27
Chlordane 1 1 3.50 3.40 3.54 388 290 49.9
3 4.86 4.80 4.94 116
4 6.53 6.48 6.62 337
5 6.77 6.72 6.86 287
6 6.90 6.84 6.98 434
8 8.09 8.09 8.23 171
2 3 3.44 3.36 3.50 90.5 170
4 4.19 4.12 4.26 79.6
5 4.65 4.58 4.72 274
6 4.97 4.89 5.03 250
FORM X 8081A
06/03/2010Page 355 of 623
FORM XForm 1
Client Sample ID:
Lab Name: Job No.:
SDG No.:
Lab Sample ID: 460-13139-7
Instrument ID (1): Instrument ID (2):
Date Analyzed (1): Date Analyzed (2):
GC Column (1): ID: GC Column (2): ID:
TB-5 3-4
TestAmerica Edison 460-13139-1
IDENTIFICATION SUMMARYForm 1
0.53(mm) 0.53(mm)
05/17/2010 09:09 05/17/2010 09:09
PESTGC1 PESTGC1
CLP-2 CLP-1
ANALYTE COL PEAK RTRT WINDOW
FROM TO PEAK MEANRPD
CONCENTRATION
3.163.063.111gamma-BHC (Lindane) 16 55.8
2.662.562.582 28
7.297.157.2314,4'-DDE 35 65.2
5.275.135.202 18
7.567.427.491Dieldrin 22 23.2
6.045.905.982 28
Chlordane 1 1 3.47 3.40 3.54 926 1700 25.7
3 4.86 4.80 4.94 1120
4 6.53 6.48 6.62 1770
5 6.77 6.72 6.86 1860
6 6.90 6.84 6.98 1900
7 7.95 7.88 8.02 3800
8 8.12 8.09 8.23 368
2 1 2.92 2.84 2.98 608 1300
2 3.02 2.91 3.05 264
3 3.44 3.36 3.50 1410
4 4.19 4.12 4.26 1800
5 4.65 4.58 4.72 1180
6 4.95 4.89 5.03 1490
7 6.63 6.57 6.71 2310
FORM X 8081A
06/03/2010Page 356 of 623
FORM XForm 1
Client Sample ID:
Lab Name: Job No.:
SDG No.:
Lab Sample ID: LCS 460-37420/2-A
Instrument ID (1): Instrument ID (2):
Date Analyzed (1): Date Analyzed (2):
GC Column (1): ID: GC Column (2): ID:
TestAmerica Edison 460-13139-1
IDENTIFICATION SUMMARYForm 1
0.53(mm) 0.53(mm)
05/17/2010 05:43 05/17/2010 05:43
PESTGC1 PESTGC1
CLP-2 CLP-1
ANALYTE COL PEAK RTRT WINDOW
FROM TO PEAK MEANRPD
CONCENTRATION
2.822.722.791alpha-BHC 96.3 7.9
2.432.332.382 89.0
3.163.063.131gamma-BHC (Lindane) 98.6 8.9
2.662.562.612 90.2
3.243.143.221beta-BHC 104 2.8
2.722.622.672 102
3.623.523.601delta-BHC 121 10.3
2.862.762.812 109
3.743.643.731Heptachlor 93.0 6.4
3.032.932.992 87.2
4.534.434.541Aldrin 88.9 7.9
3.323.223.282 82.2
6.105.966.101Heptachlor epoxide 97.0 3.7
4.414.274.362 93.5
7.106.967.081Endosulfan I 93.6 0.3
5.405.265.362 93.3
7.297.157.2614,4'-DDE 98.1 3.5
5.275.135.222 94.8
7.567.427.521Dieldrin 88.6 1.1
6.045.906.002 89.6
7.927.787.881Endrin 101 3.2
6.626.486.572 104
8.037.897.9914,4'-DDD 94.7 1.4
6.806.666.752 93.4
8.168.028.121Endosulfan II 101 0.9
7.136.997.082 101
8.408.268.3514,4'-DDT 99.1 2.0
7.357.217.302 97.2
8.558.418.501Endrin aldehyde 103 0.5
7.747.607.682 104
8.888.748.831Endosulfan sulfate 103 1.9
8.228.088.162 101
FORM X 8081A
06/03/2010Page 357 of 623
FORM XForm 1
Client Sample ID:
Lab Name: Job No.:
SDG No.:
Lab Sample ID: 460-13147-A-2-B MS
Instrument ID (1): Instrument ID (2):
Date Analyzed (1): Date Analyzed (2):
GC Column (1): ID: GC Column (2): ID:
TestAmerica Edison 460-13139-1
IDENTIFICATION SUMMARYForm 1
0.53(mm) 0.53(mm)
05/17/2010 06:36 05/17/2010 06:36
PESTGC1 PESTGC1
CLP-2 CLP-1
ANALYTE COL PEAK RTRT WINDOW
FROM TO PEAK MEANRPD
CONCENTRATION
2.822.722.771alpha-BHC 154 17.1
2.432.332.382 129
3.163.063.111gamma-BHC (Lindane) 155 17.7
2.662.562.612 130
3.243.143.191beta-BHC 153 17.3
2.722.622.672 128
3.623.523.571delta-BHC 167 16.1
2.862.762.812 142
3.743.643.691Heptachlor 139 1.0
3.032.932.992 137
4.534.434.481Aldrin 151 17.6
3.323.223.282 127
6.105.966.041Heptachlor epoxide 149 12.4
4.414.274.352 132
7.106.967.041Endosulfan I 144 6.6
5.405.265.332 135
7.297.157.2314,4'-DDE 169 22.2
5.275.135.202 135
7.567.427.491Dieldrin 150 15.8
6.045.905.972 128
7.927.787.861Endrin 168 12.8
6.626.486.552 148
8.037.897.9614,4'-DDD 159 17.2
6.806.666.732 134
8.168.028.091Endosulfan II 152 21.4
7.136.997.072 123
8.408.268.3314,4'-DDT 162 21.7
7.357.217.292 131
8.558.418.481Endrin aldehyde 145 22.7
7.747.607.672 116
8.888.748.811Endosulfan sulfate 147 21.4
8.228.088.152 118
FORM X 8081A
06/03/2010Page 358 of 623
FORM XForm 1
Client Sample ID:
Lab Name: Job No.:
SDG No.:
Lab Sample ID: 460-13147-A-2-C MSD
Instrument ID (1): Instrument ID (2):
Date Analyzed (1): Date Analyzed (2):
GC Column (1): ID: GC Column (2): ID:
TestAmerica Edison 460-13139-1
IDENTIFICATION SUMMARYForm 1
0.53(mm) 0.53(mm)
05/17/2010 06:50 05/17/2010 06:50
PESTGC1 PESTGC1
CLP-2 CLP-1
ANALYTE COL PEAK RTRT WINDOW
FROM TO PEAK MEANRPD
CONCENTRATION
2.822.722.771alpha-BHC 145 17.0
2.432.332.382 122
3.163.063.111gamma-BHC (Lindane) 147 19.4
2.662.562.612 121
3.243.143.191beta-BHC 144 13.8
2.722.622.672 125
3.623.523.571delta-BHC 159 16.8
2.862.762.812 134
3.743.643.691Heptachlor 125 3.0
3.032.932.982 122
4.534.434.481Aldrin 145 17.3
3.323.223.272 122
6.105.966.041Heptachlor epoxide 140 14.3
4.414.274.352 122
7.106.967.041Endosulfan I 137 8.0
5.405.265.332 126
7.297.157.2314,4'-DDE 161 27.6
5.275.135.202 122
7.567.427.491Dieldrin 140 15.4
6.045.905.972 120
7.927.787.861Endrin 163 20.0
6.626.486.552 133
8.037.897.9614,4'-DDD 156 27.8
6.806.666.732 118
8.168.028.091Endosulfan II 145 24.6
7.136.997.062 113
8.408.268.3314,4'-DDT 150 24.1
7.357.217.282 118
8.558.418.481Endrin aldehyde 137 35.3
7.747.607.672 95.9
8.888.748.811Endosulfan sulfate 147 30.0
8.228.088.152 109
FORM X 8081A
06/03/2010Page 359 of 623
FORM IForm 1PESTICIDES ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-3 6-7
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-2
Matrix: xf108828.dLab File ID:
Date Collected:8081AAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 09:45
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 09:15
05/17/2010 08:00
N
10(mL)
1(uL)
Sample wt/vol: 15.00(g)
% Moisture: 18.8
GC Column: ID: 0.53(mm)CLP-2
Analysis Batch No.: 37575 ug/KgUnits:
SURROGATE %RECCAS NO. LIMITS Q
877-09-8 Tetrachloro-m-xylene 115 22-141
2051-24-3 DCB Decachlorobiphenyl 125 10-165
FORM I 8081A
06/03/2010Page 360 of 623
Data File: xf108828.d Report Date: 17-May-2010 11:17
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC1.i/8081T/front/May10/05-17-10/17may10a.b/xf108828.dLab Smp Id: 460-13139-e-2-b Inj Date : 17-MAY-2010 08:00 Operator : 462 Inst ID: PESTGC1.iSmp Info : 460-13139-e-2-bMisc Info : Comment : Method : /chem1/PESTGC1.i/8081T/front/May10/05-17-10/17may10a.b/09Xf8081.mMeth Date : 17-May-2010 11:16 ferdie Quant Type: ESTDCal Date : 11-MAY-2010 14:10 Cal File: xf108641.dAls bottle: 1 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: Allpest.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (uL)(1000 low, 2Ws 15.00000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 28 Tetrachloro-m-xylene CAS #: 877-09-8
2.287 2.287 0.000 129307 57.5645 38 80.00- 120.00 100.00
-------------------------------------------------------------------------------
$ 30 Decachlorobiphenyl CAS #: 2051-24-3
10.333 10.333 0.000 81991 62.6568 42 80.00- 120.00 100.00
-------------------------------------------------------------------------------
06/03/2010Page 361 of 623
Data File: xf108828.d
Date: 17-MAY-2010 08:00
Client ID: Instrument: PESTGC1.i
Sample Info: 460-13139-e-2-b Operator: 462
06/03/2010Page 362 of 623
FORM IForm 1PESTICIDES ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-3 6-7
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-2
Matrix: xr108828.dLab File ID:
Date Collected:8081AAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 09:45
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 09:15
05/17/2010 08:00
N
10(mL)
1(uL)
Sample wt/vol: 15.00(g)
% Moisture: 18.8
GC Column: ID: 0.53(mm)CLP-1
Analysis Batch No.: 37575 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Aldrin309-00-2 8.3 8.3 1.8U
alpha-BHC319-84-6 8.3 8.3 1.5U
beta-BHC319-85-7 8.3 8.3 1.1U
delta-BHC319-86-8 8.3 8.3 1.3U
gamma-BHC (Lindane)58-89-9 8.3 8.3 0.96U
Chlordane57-74-9 83 83 18U
4,4'-DDD72-54-8 8.3 8.3 0.99U
4,4'-DDE72-55-9 8.3 8.3 1.6U
4,4'-DDT50-29-3 8.3 8.3 1.0U
Dieldrin60-57-1 8.3 8.3 1.6U
Endosulfan I959-98-8 8.3 8.3 1.7U
Endosulfan II33213-65-9 8.3 8.3 1.2U
Endosulfan sulfate1031-07-8 8.3 8.3 1.1U
Endrin72-20-8 8.3 8.3 1.2U
Endrin aldehyde7421-93-4 8.3 8.3 2.1U
Heptachlor76-44-8 8.3 8.3 1.2U
Heptachlor epoxide1024-57-3 8.3 8.3 1.7U
Toxaphene8001-35-2 83 83 17U
SURROGATE %RECCAS NO. LIMITS Q
877-09-8 Tetrachloro-m-xylene 112 22-141
2051-24-3 DCB Decachlorobiphenyl 105 10-165
FORM I 8081A
06/03/2010Page 363 of 623
Data File: xr108828.d Page 1 Report Date: 17-May-2010 11:17
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC1.i/8081T/rear/May10/05-17-10/17may10a.b/xr108828.dLab Smp Id: 460-13139-e-2-b Inj Date : 17-MAY-2010 08:00 Operator : 462 Inst ID: PESTGC1.iSmp Info : 460-13139-e-2-bMisc Info : Comment : Method : /chem1/PESTGC1.i/8081T/rear/May10/05-17-10/17may10a.b/09Xr8081.mMeth Date : 17-May-2010 08:58 ferdie Quant Type: ESTDCal Date : 11-MAY-2010 14:10 Cal File: xr108641.dAls bottle: 1 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: Allpest.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (uL)(1000 low, 2Ws 15.00000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 28 Tetrachloro-m-xylene CAS #: 877-09-8
1.987 1.987 0.000 227401 55.8844 37 80.00- 120.00 100.00
-------------------------------------------------------------------------------
$ 30 Decachlorobiphenyl CAS #: 2051-24-3
9.513 9.513 0.000 132431 52.4024 35 80.00- 120.00 100.00
-------------------------------------------------------------------------------
06/03/2010Page 364 of 623
Data File: xr108828.d
Date: 17-MAY-2010 08:00
Client ID: Instrument: PESTGC1.i
Sample Info: 460-13139-e-2-b Operator: 462
06/03/2010Page 365 of 623
FORM IForm 1PESTICIDES ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-2 5-6
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-4
Matrix: xf108830.dLab File ID:
Date Collected:8081AAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 10:45
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 09:15
05/17/2010 08:27
N
10(mL)
1(uL)
Sample wt/vol: 15.01(g)
% Moisture: 12.8
GC Column: ID: 0.53(mm)CLP-2
Analysis Batch No.: 37575 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
4,4'-DDD72-54-8 55 7.7 0.92
4,4'-DDT50-29-3 29 7.7 0.96
SURROGATE %RECCAS NO. LIMITS Q
877-09-8 Tetrachloro-m-xylene 121 22-141
2051-24-3 DCB Decachlorobiphenyl 155 10-165
FORM I 8081A
06/03/2010Page 366 of 623
Data File: xf108830.d Report Date: 17-May-2010 11:17
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC1.i/8081T/front/May10/05-17-10/17may10a.b/xf108830.dLab Smp Id: 460-13139-e-4-b Inj Date : 17-MAY-2010 08:27 Operator : 462 Inst ID: PESTGC1.iSmp Info : 460-13139-e-4-bMisc Info : Comment : Method : /chem1/PESTGC1.i/8081T/front/May10/05-17-10/17may10a.b/09Xf8081.mMeth Date : 17-May-2010 11:16 ferdie Quant Type: ESTDCal Date : 11-MAY-2010 14:10 Cal File: xf108641.dAls bottle: 1 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: Allpest.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (uL)(1000 low, 2Ws 15.00000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 28 Tetrachloro-m-xylene CAS #: 877-09-8
2.287 2.287 0.000 135629 60.3789 40 80.00- 120.00 100.00
-------------------------------------------------------------------------------
6 Chlordane CAS #: 57-74-9
3.503 3.470 0.033 56067 507.927 340 80.00- 120.00 100.00
3.697 3.700 -0.003 0 106.80- 160.20 0.00
4.860 4.870 -0.010 20965 151.507 100 100.29- 150.43 37.39
6.533 6.547 -0.014 154574 441.350 290 253.83- 380.74 275.70
6.770 6.787 -0.017 116242 376.157 250 223.96- 335.95 207.33
6.900 6.913 -0.013 162517 568.653 380 207.13- 310.69 289.86
7.960 7.953 0.007 0 38.42- 57.62 0.00
8.093 8.160 -0.067 22471 223.759 150 72.78- 109.17 40.08
Average of Peak Concentrations = 250
-------------------------------------------------------------------------------
06/03/2010Page 367 of 623
Data File: xf108830.d Report Date: 17-May-2010 11:17
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
65 gamma-Chlordane CAS #: 5103-74-2
6.533 6.540 -0.007 154574 49.2684 33 80.00- 120.00 100.00
-------------------------------------------------------------------------------
66 alpha-Chlordane CAS #: 5103-71-9
6.900 6.903 -0.003 162517 56.3061 38 80.00- 120.00 100.00
-------------------------------------------------------------------------------
8 4,4'-DDE CAS #: 72-55-9
7.223 7.230 -0.007 41866 17.5219 12 80.00- 120.00 100.00
-------------------------------------------------------------------------------
10 Dieldrin CAS #: 60-57-1
7.520 7.490 0.030 33630 13.3142 8.9 80.00- 120.00 100.00
-------------------------------------------------------------------------------
7 4,4'-DDD CAS #: 72-54-8
7.960 7.967 -0.007 139431 72.5796 48 80.00- 120.00 100.00(M)
-------------------------------------------------------------------------------
9 4,4'-DDT CAS #: 50-29-3
8.327 8.330 -0.003 67783 38.0943 25 80.00- 120.00 100.00
-------------------------------------------------------------------------------
$ 30 Decachlorobiphenyl CAS #: 2051-24-3
10.330 10.333 -0.003 101186 77.3255 52 80.00- 120.00 100.00
-------------------------------------------------------------------------------
QC Flag Legend
M - Compound response manually integrated.
06/03/2010Page 368 of 623
Data File: xf108830.d
Date: 17-MAY-2010 08:27
Client ID: Instrument: PESTGC1.i
Sample Info: 460-13139-e-4-b Operator: 462
06/03/2010Page 369 of 623
Manual Integration Report
Data File: xf108830.dInj. Date and Time: 17-MAY-2010 08:27Instrument ID: PESTGC1.iClient ID: Compound: 7 4,4'-DDDCAS #: 72-54-8Report Date: 05/17/2010
Processing Integration Results
Not Detected
Expected RT: 7.96
Manual Integration Results
RT: 7.96
Response: 139431
Amount: 72.58
Conc: 48.39
Manually Integrated By: ferdieManual Integration Reason:
06/03/2010Page 370 of 623
FORM IForm 1PESTICIDES ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-2 5-6
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-4
Matrix: xr108830.dLab File ID:
Date Collected:8081AAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 10:45
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 09:15
05/17/2010 08:27
N
10(mL)
1(uL)
Sample wt/vol: 15.01(g)
% Moisture: 12.8
GC Column: ID: 0.53(mm)CLP-1
Analysis Batch No.: 37575 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Aldrin309-00-2 7.7 7.7 1.7U
alpha-BHC319-84-6 7.7 7.7 1.4U
beta-BHC319-85-7 7.7 7.7 1.0U
delta-BHC319-86-8 7.7 7.7 1.2U
gamma-BHC (Lindane)58-89-9 7.7 7.7 0.89U
Chlordane57-74-9 170 77 17p
4,4'-DDE72-55-9 8.6 7.7 1.5p
Dieldrin60-57-1 5.5 7.7 1.5J p
Endosulfan I959-98-8 7.7 7.7 1.6U
Endosulfan II33213-65-9 7.7 7.7 1.2U
Endosulfan sulfate1031-07-8 7.7 7.7 0.99U
Endrin72-20-8 7.7 7.7 1.1U
Endrin aldehyde7421-93-4 7.7 7.7 1.9U
Heptachlor76-44-8 7.7 7.7 1.1U
Heptachlor epoxide1024-57-3 7.7 7.7 1.5U
Toxaphene8001-35-2 77 77 16U
SURROGATE %RECCAS NO. LIMITS Q
877-09-8 Tetrachloro-m-xylene 106 22-141
2051-24-3 DCB Decachlorobiphenyl X168 10-165
FORM I 8081A
06/03/2010Page 371 of 623
Data File: xr108830.d Page 1 Report Date: 17-May-2010 11:17
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC1.i/8081T/rear/May10/05-17-10/17may10a.b/xr108830.dLab Smp Id: 460-13139-e-4-b Inj Date : 17-MAY-2010 08:27 Operator : 462 Inst ID: PESTGC1.iSmp Info : 460-13139-e-4-bMisc Info : Comment : Method : /chem1/PESTGC1.i/8081T/rear/May10/05-17-10/17may10a.b/09Xr8081.mMeth Date : 17-May-2010 08:58 ferdie Quant Type: ESTDCal Date : 11-MAY-2010 14:10 Cal File: xr108641.dAls bottle: 1 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: Allpest.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (uL)(1000 low, 2Ws 15.00000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 28 Tetrachloro-m-xylene CAS #: 877-09-8
1.987 1.987 0.000 216061 53.0976 35 80.00- 120.00 100.00
-------------------------------------------------------------------------------
6 Chlordane CAS #: 57-74-9
2.917 2.913 0.004 0 80.00- 120.00 0.00(T)
0.000 2.983 -2.983 0 121.97- 182.95 0.00
3.440 3.433 0.007 30596 118.481 79 115.53- 173.30 347.95
4.190 4.193 -0.003 12263 104.189 69 52.66- 78.99 139.47
4.653 4.653 0.000 239639 358.874 240 298.74- 448.12 2725.28
4.967 4.963 0.004 343276 326.948 220 469.73- 704.59 3903.88
0.000 6.637 -6.637 0 64.26- 96.39 0.00
0.000 6.920 -6.920 0 102.24- 153.36 0.00
Average of Peak Concentrations = 150
-------------------------------------------------------------------------------
06/03/2010Page 372 of 623
Data File: xr108830.d Page 2 Report Date: 17-May-2010 11:17
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
65 gamma-Chlordane CAS #: 5103-74-2
4.653 4.653 0.000 239639 44.8290 30 80.00- 120.00 100.00
-------------------------------------------------------------------------------
66 alpha-Chlordane CAS #: 5103-71-9
4.967 4.987 -0.020 343276 66.0699 44 80.00- 120.00 100.00
-------------------------------------------------------------------------------
8 4,4'-DDE CAS #: 72-55-9
5.193 5.203 -0.010 51169 11.2943 7.5 80.00- 120.00 100.00
-------------------------------------------------------------------------------
10 Dieldrin CAS #: 60-57-1
5.980 5.977 0.003 36344 7.16706 4.8 80.00- 120.00 100.00
-------------------------------------------------------------------------------
7 4,4'-DDD CAS #: 72-54-8
6.730 6.737 -0.007 206293 52.2907 35 80.00- 120.00 100.00
-------------------------------------------------------------------------------
9 4,4'-DDT CAS #: 50-29-3
7.283 7.287 -0.004 133598 35.2224 23 80.00- 120.00 100.00
-------------------------------------------------------------------------------
$ 30 Decachlorobiphenyl CAS #: 2051-24-3
9.513 9.513 0.000 212206 83.9690 56 80.00- 120.00 100.00(R)
-------------------------------------------------------------------------------
QC Flag Legend
T - Target compound detected outside RT window.R - Spike/Surrogate failed recovery limits.
06/03/2010Page 373 of 623
Data File: xr108830.d
Date: 17-MAY-2010 08:27
Client ID: Instrument: PESTGC1.i
Sample Info: 460-13139-e-4-b Operator: 462
06/03/2010Page 374 of 623
FORM IForm 1PESTICIDES ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-1 2-3
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-5
Matrix: xf108831.dLab File ID:
Date Collected:8081AAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 11:25
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 09:15
05/17/2010 08:41
N
10(mL)
1(uL)
Sample wt/vol: 15.00(g)
% Moisture: 6.5
GC Column: ID: 0.53(mm)CLP-2
Analysis Batch No.: 37575 ug/KgUnits:
SURROGATE %RECCAS NO. LIMITS Q
877-09-8 Tetrachloro-m-xylene 117 22-141
2051-24-3 DCB Decachlorobiphenyl 138 10-165
FORM I 8081A
06/03/2010Page 375 of 623
Data File: xf108831.d Report Date: 17-May-2010 11:17
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC1.i/8081T/front/May10/05-17-10/17may10a.b/xf108831.dLab Smp Id: 460-13139-e-5-b Inj Date : 17-MAY-2010 08:41 Operator : 462 Inst ID: PESTGC1.iSmp Info : 460-13139-e-5-bMisc Info : Comment : Method : /chem1/PESTGC1.i/8081T/front/May10/05-17-10/17may10a.b/09Xf8081.mMeth Date : 17-May-2010 11:16 ferdie Quant Type: ESTDCal Date : 11-MAY-2010 14:10 Cal File: xf108641.dAls bottle: 1 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: Allpest.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (uL)(1000 low, 2Ws 15.00000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 28 Tetrachloro-m-xylene CAS #: 877-09-8
2.283 2.287 -0.004 131445 58.5163 39 80.00- 120.00 100.00
-------------------------------------------------------------------------------
$ 30 Decachlorobiphenyl CAS #: 2051-24-3
10.333 10.333 0.000 90555 69.2013 46 80.00- 120.00 100.00
-------------------------------------------------------------------------------
06/03/2010Page 376 of 623
Data File: xf108831.d
Date: 17-MAY-2010 08:41
Client ID: Instrument: PESTGC1.i
Sample Info: 460-13139-e-5-b Operator: 462
06/03/2010Page 377 of 623
FORM IForm 1PESTICIDES ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-1 2-3
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-5
Matrix: xr108831.dLab File ID:
Date Collected:8081AAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 11:25
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 09:15
05/17/2010 08:41
N
10(mL)
1(uL)
Sample wt/vol: 15.00(g)
% Moisture: 6.5
GC Column: ID: 0.53(mm)CLP-1
Analysis Batch No.: 37575 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Aldrin309-00-2 7.2 7.2 1.6U
alpha-BHC319-84-6 7.2 7.2 1.3U
beta-BHC319-85-7 7.2 7.2 0.97U
delta-BHC319-86-8 7.2 7.2 1.1U
gamma-BHC (Lindane)58-89-9 7.2 7.2 0.83U
Chlordane57-74-9 72 72 16U
4,4'-DDD72-54-8 7.2 7.2 0.86U
4,4'-DDE72-55-9 7.2 7.2 1.4U
4,4'-DDT50-29-3 7.2 7.2 0.90U
Dieldrin60-57-1 7.2 7.2 1.4U
Endosulfan I959-98-8 7.2 7.2 1.5U
Endosulfan II33213-65-9 7.2 7.2 1.1U
Endosulfan sulfate1031-07-8 7.2 7.2 0.92U
Endrin72-20-8 7.2 7.2 1.0U
Endrin aldehyde7421-93-4 7.2 7.2 1.8U
Heptachlor76-44-8 7.2 7.2 1.0U
Heptachlor epoxide1024-57-3 7.2 7.2 1.4U
Toxaphene8001-35-2 72 72 15U
SURROGATE %RECCAS NO. LIMITS Q
877-09-8 Tetrachloro-m-xylene 113 22-141
2051-24-3 DCB Decachlorobiphenyl 118 10-165
FORM I 8081A
06/03/2010Page 378 of 623
Data File: xr108831.d Page 1 Report Date: 17-May-2010 11:17
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC1.i/8081T/rear/May10/05-17-10/17may10a.b/xr108831.dLab Smp Id: 460-13139-e-5-b Inj Date : 17-MAY-2010 08:41 Operator : 462 Inst ID: PESTGC1.iSmp Info : 460-13139-e-5-bMisc Info : Comment : Method : /chem1/PESTGC1.i/8081T/rear/May10/05-17-10/17may10a.b/09Xr8081.mMeth Date : 17-May-2010 08:58 ferdie Quant Type: ESTDCal Date : 11-MAY-2010 14:10 Cal File: xr108641.dAls bottle: 1 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: Allpest.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (uL)(1000 low, 2Ws 15.00000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 28 Tetrachloro-m-xylene CAS #: 877-09-8
1.983 1.987 -0.004 230813 56.7229 38 80.00- 120.00 100.00
-------------------------------------------------------------------------------
$ 30 Decachlorobiphenyl CAS #: 2051-24-3
9.513 9.513 0.000 148700 58.8399 39 80.00- 120.00 100.00
-------------------------------------------------------------------------------
06/03/2010Page 379 of 623
Data File: xr108831.d
Date: 17-MAY-2010 08:41
Client ID: Instrument: PESTGC1.i
Sample Info: 460-13139-e-5-b Operator: 462
06/03/2010Page 380 of 623
FORM IForm 1PESTICIDES ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-5 3-4
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-7
Matrix: xf108833.dLab File ID:
Date Collected:8081AAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 12:30
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 09:15
05/17/2010 09:09
N
10(mL)
1(uL)
Sample wt/vol: 15.00(g)
% Moisture: 61.5
GC Column: ID: 0.53(mm)CLP-2
Analysis Batch No.: 37575 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
gamma-BHC (Lindane)58-89-9 16 17 2.0J p
Chlordane57-74-9 1700 170 38
SURROGATE %RECCAS NO. LIMITS Q
877-09-8 Tetrachloro-m-xylene 84 22-141
2051-24-3 DCB Decachlorobiphenyl 78 10-165
FORM I 8081A
06/03/2010Page 381 of 623
Data File: xf108833.d Report Date: 17-May-2010 11:17
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC1.i/8081T/front/May10/05-17-10/17may10a.b/xf108833.dLab Smp Id: 460-13139-e-7-b Inj Date : 17-MAY-2010 09:09 Operator : 462 Inst ID: PESTGC1.iSmp Info : 460-13139-e-7-bMisc Info : Comment : Method : /chem1/PESTGC1.i/8081T/front/May10/05-17-10/17may10a.b/09Xf8081.mMeth Date : 17-May-2010 11:16 ferdie Quant Type: ESTDCal Date : 11-MAY-2010 14:10 Cal File: xf108641.dAls bottle: 1 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: Allpest.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (uL)(1000 low, 2Ws 15.00000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 28 Tetrachloro-m-xylene CAS #: 877-09-8
2.287 2.287 0.000 94721 42.1676 28 80.00- 120.00 100.00
-------------------------------------------------------------------------------
5 gamma-BHC (Lindane) CAS #: 58-89-9
3.110 3.110 0.000 26539 9.23526 6.2 80.00- 120.00 100.00
-------------------------------------------------------------------------------
6 Chlordane CAS #: 57-74-9
3.470 3.470 0.000 58993 534.434 360 80.00- 120.00 100.00
3.740 3.700 0.040 0 106.80- 160.20 0.00
4.863 4.870 -0.007 89230 644.837 430 100.29- 150.43 151.26
6.533 6.547 -0.014 357199 1019.90 680 253.83- 380.74 605.49
6.773 6.787 -0.014 332123 1074.74 720 223.96- 335.95 562.99
6.900 6.913 -0.013 312475 1093.36 730 207.13- 310.69 529.68
06/03/2010Page 382 of 623
Data File: xf108833.d Report Date: 17-May-2010 11:17
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
6 Chlordane (continued)
7.947 7.953 -0.006 116142 2191.11 1500 38.42- 57.62 196.87
8.117 8.160 -0.043 21339 212.487 140 72.78- 109.17 36.17
Average of Peak Concentrations = 640
-------------------------------------------------------------------------------
65 gamma-Chlordane CAS #: 5103-74-2
6.533 6.540 -0.007 357199 113.852 76 80.00- 120.00 100.00
-------------------------------------------------------------------------------
66 alpha-Chlordane CAS #: 5103-71-9
6.900 6.903 -0.003 312475 108.261 72 80.00- 120.00 100.00
-------------------------------------------------------------------------------
8 4,4'-DDE CAS #: 72-55-9
7.227 7.230 -0.003 48425 20.2670 14 80.00- 120.00 100.00
-------------------------------------------------------------------------------
10 Dieldrin CAS #: 60-57-1
7.487 7.490 -0.003 31962 12.6539 8.4 80.00- 120.00 100.00
-------------------------------------------------------------------------------
$ 30 Decachlorobiphenyl CAS #: 2051-24-3
10.333 10.333 0.000 51005 38.9776 26 80.00- 120.00 100.00
-------------------------------------------------------------------------------
06/03/2010Page 383 of 623
Data File: xf108833.d
Date: 17-MAY-2010 09:09
Client ID: Instrument: PESTGC1.i
Sample Info: 460-13139-e-7-b Operator: 462
06/03/2010Page 384 of 623
FORM IForm 1PESTICIDES ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-5 3-4
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-7
Matrix: xr108833.dLab File ID:
Date Collected:8081AAnalysis Method:
Soil
TestAmerica Edison
05/12/2010 12:30
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 09:15
05/17/2010 09:09
N
10(mL)
1(uL)
Sample wt/vol: 15.00(g)
% Moisture: 61.5
GC Column: ID: 0.53(mm)CLP-1
Analysis Batch No.: 37575 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Aldrin309-00-2 17 17 3.8U
alpha-BHC319-84-6 17 17 3.2U
beta-BHC319-85-7 17 17 2.4U
delta-BHC319-86-8 17 17 2.7U
4,4'-DDD72-54-8 17 17 2.1U
4,4'-DDE72-55-9 18 17 3.4p
4,4'-DDT50-29-3 17 17 2.2U
Dieldrin60-57-1 28 17 3.4
Endosulfan I959-98-8 17 17 3.7U
Endosulfan II33213-65-9 17 17 2.6U
Endosulfan sulfate1031-07-8 17 17 2.2U
Endrin72-20-8 17 17 2.4U
Endrin aldehyde7421-93-4 17 17 4.3U
Heptachlor76-44-8 17 17 2.5U
Heptachlor epoxide1024-57-3 17 17 3.5U
Toxaphene8001-35-2 170 170 36U
SURROGATE %RECCAS NO. LIMITS Q
877-09-8 Tetrachloro-m-xylene 76 22-141
2051-24-3 DCB Decachlorobiphenyl 75 10-165
FORM I 8081A
06/03/2010Page 385 of 623
Data File: xr108833.d Page 1 Report Date: 17-May-2010 11:17
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC1.i/8081T/rear/May10/05-17-10/17may10a.b/xr108833.dLab Smp Id: 460-13139-e-7-b Inj Date : 17-MAY-2010 09:09 Operator : 462 Inst ID: PESTGC1.iSmp Info : 460-13139-e-7-bMisc Info : Comment : Method : /chem1/PESTGC1.i/8081T/rear/May10/05-17-10/17may10a.b/09Xr8081.mMeth Date : 17-May-2010 08:58 ferdie Quant Type: ESTDCal Date : 11-MAY-2010 14:10 Cal File: xr108641.dAls bottle: 1 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: Allpest.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (uL)(1000 low, 2Ws 15.00000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 28 Tetrachloro-m-xylene CAS #: 877-09-8
1.987 1.987 0.000 153679 37.7670 25 80.00- 120.00 100.00
-------------------------------------------------------------------------------
5 gamma-BHC (Lindane) CAS #: 58-89-9
2.577 2.607 -0.030 85063 16.3746 11 80.00- 120.00 100.00
-------------------------------------------------------------------------------
6 Chlordane CAS #: 57-74-9
2.917 2.913 0.004 62693 350.601 230 80.00- 120.00 100.00(T)
3.017 2.983 0.034 41598 152.587 100 121.97- 182.95 66.35
3.437 3.433 0.004 209490 811.235 540 115.53- 173.30 334.15
4.193 4.193 0.000 122302 1039.10 690 52.66- 78.99 195.08
4.650 4.653 -0.003 456141 683.099 460 298.74- 448.12 727.58
4.953 4.963 -0.010 904701 861.669 570 469.73- 704.59 1443.07
06/03/2010Page 386 of 623
Data File: xr108833.d Page 2 Report Date: 17-May-2010 11:17
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
6 Chlordane (continued)
6.633 6.637 -0.004 191468 1333.05 890 64.26- 96.39 305.41
0.000 6.920 -6.920 0 102.24- 153.36 0.00
Average of Peak Concentrations = 500
-------------------------------------------------------------------------------
65 gamma-Chlordane CAS #: 5103-74-2
4.650 4.653 -0.003 456141 85.3297 57 80.00- 120.00 100.00
-------------------------------------------------------------------------------
66 alpha-Chlordane CAS #: 5103-71-9
4.953 4.987 -0.034 904701 174.127 120 80.00- 120.00 100.00
-------------------------------------------------------------------------------
8 4,4'-DDE CAS #: 72-55-9
5.197 5.203 -0.006 46677 10.3028 6.9 80.00- 120.00 100.00
-------------------------------------------------------------------------------
10 Dieldrin CAS #: 60-57-1
5.983 5.977 0.006 80996 15.9725 11 80.00- 120.00 100.00
-------------------------------------------------------------------------------
$ 30 Decachlorobiphenyl CAS #: 2051-24-3
9.510 9.513 -0.003 94677 37.4633 25 80.00- 120.00 100.00
-------------------------------------------------------------------------------
QC Flag Legend
T - Target compound detected outside RT window.
06/03/2010Page 387 of 623
Data File: xr108833.d
Date: 17-MAY-2010 09:09
Client ID: Instrument: PESTGC1.i
Sample Info: 460-13139-e-7-b Operator: 462
06/03/2010Page 388 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC1
Analy Batch No.: 37146
6135Calibration Start Date: Calibration End Date:05/11/2010 12:47
N
05/11/2010 13:42
0.53(mm)GC Column: CLP-2 ID:
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-37146/5 xf108635.dLevel 2 IC 460-37146/6 xf108636.dLevel 3 IC 460-37146/7 xf108637.dLevel 4 IC 460-37146/8 xf108638.dLevel 5 IC 460-37146/9 xf108639.d
ANALYTE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 AVG RTRT WINDOW
alpha-BHC 2.7782.727 - 2.8272.787 2.777 2.777 2.773 2.777gamma-BHC (Lindane) 3.1173.067 - 3.1673.127 3.113 3.117 3.113 3.113beta-BHC 3.2013.150 - 3.2503.210 3.200 3.200 3.197 3.197delta-BHC 3.5763.523 - 3.6233.590 3.573 3.573 3.570 3.573Heptachlor 3.7073.653 - 3.7533.723 3.703 3.703 3.700 3.703Aldrin 4.5014.447 - 4.5474.523 4.497 4.497 4.493 4.493Heptachlor epoxide 6.0555.980 - 6.1206.077 6.050 6.050 6.050 6.047gamma-Chlordane 6.5536.480 - 6.6206.573 6.550 6.550 6.547 6.547alpha-Chlordane 6.9176.843 - 6.9836.933 6.913 6.913 6.913 6.910Endosulfan I 7.0496.977 - 7.1177.063 7.047 7.047 7.047 7.0434,4'-DDE 7.2387.167 - 7.3077.250 7.237 7.237 7.233 7.233Dieldrin 7.4987.427 - 7.5677.507 7.497 7.497 7.497 7.493Endrin 7.8637.793 - 7.9337.870 7.863 7.863 7.860 7.8604,4'-DDD 7.9727.900 - 8.0407.980 7.970 7.970 7.970 7.970Endosulfan II 8.1038.030 - 8.1708.110 8.103 8.100 8.100 8.1004,4'-DDT 8.3368.263 - 8.4038.343 8.337 8.333 8.333 8.333Endrin aldehyde 8.4908.420 - 8.5608.497 8.490 8.490 8.487 8.487Endosulfan sulfate 8.8178.747 - 8.8878.823 8.817 8.817 8.817 8.813Methoxychlor 9.1319.060 - 9.2009.137 9.130 9.130 9.130 9.130Endrin ketone 9.4099.337 - 9.4779.413 9.410 9.407 9.407 9.407Tetrachloro-m-xylene 2.2882.237 - 2.3372.293 2.287 2.287 2.287 2.287DCB Decachlorobiphenyl 10.34110.240 - 10.44010.343 10.340 10.340 10.340 10.340
FORM VI 8081A 06/03/2010Page 389 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC1
Analy Batch No.: 37146
6135Calibration Start Date: Calibration End Date:05/11/2010 12:47
N
05/11/2010 13:42
0.53(mm)CLP-2 ID:
EXTERNAL STANDARD CURVE EVALUTION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-37146/5 xf108635.d2Level IC 460-37146/6 xf108636.d3Level IC 460-37146/7 xf108637.d4Level IC 460-37146/8 xf108638.d5Level IC 460-37146/9 xf108639.d
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 4LVL 3LVL 2LVL 1
RRFANALYTE MIN RRF
LVL 5
alpha-BHC Ave 9.5 20.031563642.8 3225.2 3035.5 2986.52889.3
gamma-BHC (Lindane) Ave 10.6 20.028743381.3 2925.0 2738.7 2712.52610.8
beta-BHC Ave 19.3 20.014541925.8 1488.7 1334.9 1292.41226.9
delta-BHC Ave 3.3 20.029643080.4 3041.6 2922.3 2939.12834.6
Heptachlor Ave 8.0 20.031493551.3 3222.3 3044.2 3019.92909.2
Aldrin Ave 3.3 20.031233286.2 3136.6 3068.7 3111.13013.3
Heptachlor epoxide Ave 10.6 20.030883637.2 3124.9 2960.7 2919.32798.4
gamma-Chlordane Ave 10.7 20.031373691.7 3164.0 2957.0 3062.22812.1
alpha-Chlordane Ave 12.8 20.028863503.7 2935.3 2736.8 2687.32568.5
Endosulfan I Ave 10.0 20.026453090.9 2661.6 2536.1 2516.02418.9
4,4'-DDE Ave 1.9 20.023892456.2 2378.2 2354.2 2414.32343.9
Dieldrin Ave 6.5 20.025262797.8 2549.6 2450.8 2458.92372.3
Endrin Ave 7.0 20.019792217.5 1979.7 1890.0 1924.01884.2
4,4'-DDD Ave 6.0 20.019212111.6 1935.2 1867.6 1876.71814.3
Endosulfan II Ave 10.8 20.021782576.2 2190.5 2086.6 2065.91970.5
FORM VI 8081A
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 390 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC1
Analy Batch No.: 37146
6135Calibration Start Date: Calibration End Date:05/11/2010 12:47
N
05/11/2010 13:42
0.53(mm)CLP-2 ID:
EXTERNAL STANDARD CURVE EVALUTION
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 4LVL 3LVL 2LVL 1
RRFANALYTE MIN RRF
LVL 5
4,4'-DDT Ave 4.3 20.017791907.7 1746.1 1705.4 1774.61762.9
Endrin aldehyde Ave 13.5 20.017552163.5 1733.0 1670.2 1640.71566.6
Endosulfan sulfate Ave 10.9 20.019482306.6 1970.3 1860.8 1831.81769.8
Methoxychlor Ave 11.9 20.09991204.6 1003.1 935.69 927.02925.17
Endrin ketone Ave 12.2 20.022072653.4 2247.7 2106.0 2056.01973.1
Tetrachloro-m-xylene Ave 5.7 20.022462369.4 2378.1 2211.0 2196.92076.0
DCB Decachlorobiphenyl Ave 5.0 20.013091347.5 1377.5 1313.4 1298.31206.2
FORM VI 8081A
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 391 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC1
Analy Batch No.: 37146
6135Calibration Start Date: Calibration End Date:05/11/2010 12:47
N
05/11/2010 13:42
GC Column: CLP-2 ID: 0.53(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-37146/5 xf108635.dLevel 2 IC 460-37146/6 xf108636.dLevel 3 IC 460-37146/7 xf108637.dLevel 4 IC 460-37146/8 xf108638.dLevel 5 IC 460-37146/9 xf108639.d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UG/L)
LVL 1 LVL 1LVL 2 LVL 2LVL 3 LVL 3LVL 4 LVL 4LVL 5 LVL 5
alpha-BHC Ave 36428 161260 303553 746634 1444652 10.0 50.0 100 250 500gamma-BHC (Lindane) Ave 33813 146248 273872 678129 1305403 10.0 50.0 100 250 500beta-BHC Ave 19258 74437 133487 323092 613439 10.0 50.0 100 250 500delta-BHC Ave 30804 152081 292227 734786 1417324 10.0 50.0 100 250 500Heptachlor Ave 35513 161115 304423 754965 1454592 10.0 50.0 100 250 500Aldrin Ave 32862 156829 306871 777774 1506651 10.0 50.0 100 250 500Heptachlor epoxide Ave 36372 156243 296068 729816 1399176 10.0 50.0 100 250 500gamma-Chlordane Ave 36917 158200 295695 765545 1406046 10.0 50.0 100 250 500alpha-Chlordane Ave 35037 146766 273678 671826 1284233 10.0 50.0 100 250 500Endosulfan I Ave 30909 133078 253605 628993 1209466 10.0 50.0 100 250 5004,4'-DDE Ave 24562 118910 235417 603576 1171958 10.0 50.0 100 250 500Dieldrin Ave 27978 127479 245078 614720 1186157 10.0 50.0 100 250 500Endrin Ave 22175 98986 188999 480995 942121 10.0 50.0 100 250 5004,4'-DDD Ave 21116 96759 186757 469180 907157 10.0 50.0 100 250 500Endosulfan II Ave 25762 109525 208663 516465 985225 10.0 50.0 100 250 5004,4'-DDT Ave 19077 87305 170540 443648 881471 10.0 50.0 100 250 500Endrin aldehyde Ave 21635 86649 167018 410169 783293 10.0 50.0 100 250 500Endosulfan sulfate Ave 23066 98516 186083 457948 884919 10.0 50.0 100 250 500Methoxychlor Ave 12046 50153 93569 231756 462587 10.0 50.0 100 250 500Endrin ketone Ave 26534 112387 210601 514011 986528 10.0 50.0 100 250 500Tetrachloro-m-xylene Ave 59236 118907 221104 329529 415202 25.0 50.0 100 150 200DCB Decachlorobiphenyl Ave 33688 68873 131344 194739 241237 25.0 50.0 100 150 200
Curve Type Legend:Ave = Average
FORM VI 8081A 06/03/2010Page 392 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC1
Analy Batch No.: 37146
6134Calibration Start Date: Calibration End Date:05/11/2010 12:47
N
05/11/2010 13:42
0.53(mm)GC Column: CLP-1 ID:
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-37146/5 xr108635.dLevel 2 IC 460-37146/6 xr108636.dLevel 3 IC 460-37146/7 xr108637.dLevel 4 IC 460-37146/8 xr108638.dLevel 5 IC 460-37146/9 xr108639.d
ANALYTE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 AVG RTRT WINDOW
alpha-BHC 2.3812.330 - 2.4302.383 2.380 2.380 2.380 2.380gamma-BHC (Lindane) 2.6082.560 - 2.6602.610 2.607 2.610 2.607 2.607beta-BHC 2.6732.623 - 2.7232.677 2.673 2.673 2.670 2.673delta-BHC 2.8102.760 - 2.8602.813 2.810 2.810 2.807 2.810Heptachlor 2.9852.937 - 3.0372.987 2.983 2.987 2.983 2.983Aldrin 3.2753.227 - 3.3273.280 3.273 3.277 3.273 3.273Heptachlor epoxide 4.3514.280 - 4.4204.360 4.350 4.350 4.347 4.350gamma-Chlordane 4.6554.583 - 4.7234.663 4.653 4.653 4.650 4.653alpha-Chlordane 4.9904.917 - 5.0575.000 4.990 4.987 4.987 4.9874,4'-DDE 5.2055.133 - 5.2735.213 5.207 5.203 5.203 5.200Endosulfan I 5.3415.270 - 5.4105.350 5.340 5.340 5.337 5.337Dieldrin 5.9805.910 - 6.0505.987 5.980 5.980 5.977 5.977Endrin 6.5576.487 - 6.6276.563 6.557 6.557 6.557 6.5534,4'-DDD 6.7386.667 - 6.8076.743 6.740 6.737 6.737 6.733Endosulfan II 7.0707.000 - 7.1407.073 7.070 7.070 7.070 7.0674,4'-DDT 7.2897.220 - 7.3607.290 7.290 7.290 7.287 7.287Endrin aldehyde 7.6727.603 - 7.7437.673 7.673 7.673 7.670 7.670Methoxychlor 7.8857.813 - 7.9537.887 7.887 7.883 7.883 7.883Endosulfan sulfate 8.1558.087 - 8.2278.157 8.157 8.157 8.153 8.153Endrin ketone 8.4678.397 - 8.5378.470 8.467 8.467 8.467 8.463Tetrachloro-m-xylene 1.9841.937 - 2.0371.983 1.983 1.987 1.983 1.983DCB Decachlorobiphenyl 9.5179.417 - 9.6179.517 9.517 9.517 9.517 9.517
FORM VI 8081A 06/03/2010Page 393 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC1
Analy Batch No.: 37146
6134Calibration Start Date: Calibration End Date:05/11/2010 12:47
N
05/11/2010 13:42
0.53(mm)CLP-1 ID:
EXTERNAL STANDARD CURVE EVALUTION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-37146/5 xr108635.d2Level IC 460-37146/6 xr108636.d3Level IC 460-37146/7 xr108637.d4Level IC 460-37146/8 xr108638.d5Level IC 460-37146/9 xr108639.d
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 4LVL 3LVL 2LVL 1
RRFANALYTE MIN RRF
LVL 5
alpha-BHC Ave 13.6 20.059487207.4 6222.7 5718.8 5478.45114.7
gamma-BHC (Lindane) Ave 16.9 20.051956583.1 5459.6 4915.8 4689.44326.2
beta-BHC Ave 16.1 20.028383566.1 2951.4 2732.6 2550.92391.2
delta-BHC Ave 12.4 20.054726551.7 5640.6 5270.9 5119.94774.6
Heptachlor Ave 14.4 20.054136626.2 5650.1 5218.3 4965.14606.1
Aldrin Ave 10.3 20.051505951.2 5340.0 5023.9 4887.34548.9
Heptachlor epoxide Ave 12.0 20.052956311.3 5436.5 5111.5 4971.94642.6
gamma-Chlordane Ave 12.1 20.053466403.7 5446.6 5122.6 5025.94729.4
alpha-Chlordane Ave 11.8 20.051966170.5 5344.5 5020.5 4875.94566.9
4,4'-DDE Ave 3.6 20.045314725.9 4622.6 4504.6 4508.64290.8
Endosulfan I Ave 9.5 20.049545689.8 5057.7 4805.7 4785.34430.4
Dieldrin Ave 6.5 20.050715579.0 5137.4 4974.7 4977.44686.3
Endrin Ave 5.3 20.043004623.8 4407.6 4228.5 4220.74017.4
4,4'-DDD Ave 2.0 20.039454023.2 4007.4 3915.4 3954.83824.7
Endosulfan II Ave 11.1 20.043685152.0 4464.0 4225.2 4112.33884.9
FORM VI 8081A
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 394 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC1
Analy Batch No.: 37146
6134Calibration Start Date: Calibration End Date:05/11/2010 12:47
N
05/11/2010 13:42
0.53(mm)CLP-1 ID:
EXTERNAL STANDARD CURVE EVALUTION
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 4LVL 3LVL 2LVL 1
RRFANALYTE MIN RRF
LVL 5
4,4'-DDT Ave 4.3 20.037934064.1 3807.1 3682.4 3756.43655.0
Endrin aldehyde Ave 14.1 20.033934191.1 3441.5 3227.9 3135.32970.7
Methoxychlor Ave 11.7 20.020062390.4 2063.2 1907.4 1863.51807.6
Endosulfan sulfate Ave 12.4 20.036964441.0 3786.4 3553.9 3443.33253.9
Endrin ketone Ave 12.4 20.043675212.8 4518.0 4241.2 4076.63786.0
Tetrachloro-m-xylene Ave 5.8 20.040694301.3 4326.5 4003.1 3934.73780.1
DCB Decachlorobiphenyl Ave 3.0 20.025272548.3 2547.6 2570.1 2574.42395.6
FORM VI 8081A
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 395 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC1
Analy Batch No.: 37146
6134Calibration Start Date: Calibration End Date:05/11/2010 12:47
N
05/11/2010 13:42
GC Column: CLP-1 ID: 0.53(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-37146/5 xr108635.dLevel 2 IC 460-37146/6 xr108636.dLevel 3 IC 460-37146/7 xr108637.dLevel 4 IC 460-37146/8 xr108638.dLevel 5 IC 460-37146/9 xr108639.d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UG/L)
LVL 1 LVL 1LVL 2 LVL 2LVL 3 LVL 3LVL 4 LVL 4LVL 5 LVL 5
alpha-BHC Ave 72074 311135 571876 1369592 2557369 10.0 50.0 100 250 500gamma-BHC (Lindane) Ave 65831 272981 491580 1172351 2163100 10.0 50.0 100 250 500beta-BHC Ave 35661 147570 273259 637728 1195601 10.0 50.0 100 250 500delta-BHC Ave 65517 282029 527092 1279970 2387292 10.0 50.0 100 250 500Heptachlor Ave 66262 282507 521826 1241271 2303062 10.0 50.0 100 250 500Aldrin Ave 59512 266999 502394 1221823 2274452 10.0 50.0 100 250 500Heptachlor epoxide Ave 63113 271825 511152 1242984 2321322 10.0 50.0 100 250 500gamma-Chlordane Ave 64037 272329 512255 1256480 2364701 10.0 50.0 100 250 500alpha-Chlordane Ave 61705 267224 502049 1218970 2283442 10.0 50.0 100 250 5004,4'-DDE Ave 47259 231132 450457 1127145 2145422 10.0 50.0 100 250 500Endosulfan I Ave 56898 252887 480568 1196330 2215214 10.0 50.0 100 250 500Dieldrin Ave 55790 256872 497473 1244342 2343168 10.0 50.0 100 250 500Endrin Ave 46238 220380 422846 1055167 2008700 10.0 50.0 100 250 5004,4'-DDD Ave 40232 200372 391542 988702 1912370 10.0 50.0 100 250 500Endosulfan II Ave 51520 223198 422515 1028068 1942470 10.0 50.0 100 250 5004,4'-DDT Ave 40641 190354 368241 939092 1827480 10.0 50.0 100 250 500Endrin aldehyde Ave 41911 172075 322789 783823 1485364 10.0 50.0 100 250 500Methoxychlor Ave 23904 103158 190743 465865 903822 10.0 50.0 100 250 500Endosulfan sulfate Ave 44410 189322 355394 860822 1626926 10.0 50.0 100 250 500Endrin ketone Ave 52128 225899 424117 1019160 1892989 10.0 50.0 100 250 500Tetrachloro-m-xylene Ave 107532 216323 400310 590211 756017 25.0 50.0 100 150 200DCB Decachlorobiphenyl Ave 63708 127382 257005 386160 479113 25.0 50.0 100 150 200
Curve Type Legend:Ave = Average
FORM VI 8081A 06/03/2010Page 396 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC1
Analy Batch No.: 37146
6137Calibration Start Date: Calibration End Date:05/11/2010 13:56
N
05/11/2010 13:56
0.53(mm)GC Column: CLP-2 ID:
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-37146/10 xf108640.d
ANALYTE LVL 1 AVG RTRT WINDOW
Chlordane (technical) Peak 1 3.4703.400 - 3.5403.470Chlordane (technical) Peak 2 3.7003.630 - 3.7703.700Chlordane (technical) Peak 3 4.8704.800 - 4.9404.870Chlordane (technical) Peak 4 6.5476.477 - 6.6176.547Chlordane (technical) Peak 5 6.7876.717 - 6.8576.787Chlordane (technical) Peak 6 6.9136.843 - 6.9836.913Chlordane (technical) Peak 7 7.9537.883 - 8.0237.953Chlordane (technical) Peak 8 8.1608.090 - 8.2308.160
FORM VI 8081A 06/03/2010Page 397 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC1
Analy Batch No.: 37146
6137Calibration Start Date: Calibration End Date:05/11/2010 13:56
N
05/11/2010 13:56
0.53(mm)CLP-2 ID:
EXTERNAL STANDARD CURVE EVALUTION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-37146/10 xf108640.d
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 1
RRFANALYTE MIN RRF
110.38Chlordane (technical) Peak Ave 110 20.0147.36Chlordane (technical) Peak Ave 147 20.0138.38Chlordane (technical) Peak Ave 138 20.0350.23Chlordane (technical) Peak Ave 350 20.0309.03Chlordane (technical) Peak Ave 309 20.0285.79Chlordane (technical) Peak Ave 286 20.053.006Chlordane (technical) Peak Ave 53 20.0100.43Chlordane (technical) Peak Ave 100 20.0
FORM VI 8081A
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 398 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC1
Analy Batch No.: 37146
6137Calibration Start Date: Calibration End Date:05/11/2010 13:56
N
05/11/2010 13:56
GC Column: CLP-2 ID: 0.53(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-37146/10 xf108640.d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UG/L)
LVL 1 LVL 1
Chlordane (technical) Peak 1 Ave 110384 1000Chlordane (technical) Peak 2 Ave 147359 1000Chlordane (technical) Peak 3 Ave 138376 1000Chlordane (technical) Peak 4 Ave 350230 1000Chlordane (technical) Peak 5 Ave 309025 1000Chlordane (technical) Peak 6 Ave 285793 1000Chlordane (technical) Peak 7 Ave 53006 1000Chlordane (technical) Peak 8 Ave 100425 1000
Curve Type Legend:Ave = Average
FORM VI 8081A 06/03/2010Page 399 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC1
Analy Batch No.: 37146
6136Calibration Start Date: Calibration End Date:05/11/2010 13:56
N
05/11/2010 13:56
0.53(mm)GC Column: CLP-1 ID:
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-37146/10 xr108640.d
ANALYTE LVL 1 AVG RTRT WINDOW
Chlordane (technical) Peak 1 2.9132.843 - 2.9832.913Chlordane (technical) Peak 2 2.9832.913 - 3.0532.983Chlordane (technical) Peak 3 3.4333.363 - 3.5033.433Chlordane (technical) Peak 4 4.1934.123 - 4.2634.193Chlordane (technical) Peak 5 4.6534.583 - 4.7234.653Chlordane (technical) Peak 6 4.9634.893 - 5.0334.963Chlordane (technical) Peak 7 6.6376.567 - 6.7076.637Chlordane (technical) Peak 8 6.9206.850 - 6.9906.920
FORM VI 8081A 06/03/2010Page 400 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC1
Analy Batch No.: 37146
6136Calibration Start Date: Calibration End Date:05/11/2010 13:56
N
05/11/2010 13:56
0.53(mm)CLP-1 ID:
EXTERNAL STANDARD CURVE EVALUTION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-37146/10 xr108640.d
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 1
RRFANALYTE MIN RRF
178.82Chlordane (technical) Peak Ave 179 20.0272.62Chlordane (technical) Peak Ave 273 20.0258.24Chlordane (technical) Peak Ave 258 20.0117.70Chlordane (technical) Peak Ave 118 20.0667.75Chlordane (technical) Peak Ave 668 20.01049.9Chlordane (technical) Peak Ave 1050 20.0143.63Chlordane (technical) Peak Ave 144 20.0228.52Chlordane (technical) Peak Ave 229 20.0
FORM VI 8081A
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 401 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC1
Analy Batch No.: 37146
6136Calibration Start Date: Calibration End Date:05/11/2010 13:56
N
05/11/2010 13:56
GC Column: CLP-1 ID: 0.53(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-37146/10 xr108640.d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UG/L)
LVL 1 LVL 1
Chlordane (technical) Peak 1 Ave 178816 1000Chlordane (technical) Peak 2 Ave 272618 1000Chlordane (technical) Peak 3 Ave 258236 1000Chlordane (technical) Peak 4 Ave 117700 1000Chlordane (technical) Peak 5 Ave 667752 1000Chlordane (technical) Peak 6 Ave 1049940 1000Chlordane (technical) Peak 7 Ave 143631 1000Chlordane (technical) Peak 8 Ave 228523 1000
Curve Type Legend:Ave = Average
FORM VI 8081A 06/03/2010Page 402 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC1
Analy Batch No.: 37146
6139Calibration Start Date: Calibration End Date:05/11/2010 14:10
N
05/11/2010 14:10
0.53(mm)GC Column: CLP-2 ID:
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-37146/11 xf108641.d
ANALYTE LVL 1 AVG RTRT WINDOW
Toxaphene Peak 1 8.1978.127 - 8.2678.197Toxaphene Peak 2 8.5008.430 - 8.5708.500Toxaphene Peak 3 8.6038.533 - 8.6738.603Toxaphene Peak 4 8.8108.740 - 8.8808.810Toxaphene Peak 5 9.1139.043 - 9.1839.113Toxaphene Peak 6 9.1779.107 - 9.2479.177Toxaphene Peak 7 9.5009.430 - 9.5709.500Toxaphene Peak 8 9.6409.570 - 9.7109.640
FORM VI 8081A 06/03/2010Page 403 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC1
Analy Batch No.: 37146
6139Calibration Start Date: Calibration End Date:05/11/2010 14:10
N
05/11/2010 14:10
0.53(mm)CLP-2 ID:
EXTERNAL STANDARD CURVE EVALUTION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-37146/11 xf108641.d
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 1
RRFANALYTE MIN RRF
122.49Toxaphene Peak 1 Ave 122 20.0112.92Toxaphene Peak 2 Ave 113 20.098.212Toxaphene Peak 3 Ave 98 20.064.477Toxaphene Peak 4 Ave 64 20.0101.14Toxaphene Peak 5 Ave 101 20.0121.79Toxaphene Peak 6 Ave 122 20.050.603Toxaphene Peak 7 Ave 51 20.056.145Toxaphene Peak 8 Ave 56 20.0
FORM VI 8081A
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 404 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC1
Analy Batch No.: 37146
6139Calibration Start Date: Calibration End Date:05/11/2010 14:10
N
05/11/2010 14:10
GC Column: CLP-2 ID: 0.53(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-37146/11 xf108641.d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UG/L)
LVL 1 LVL 1
Toxaphene Peak 1 Ave 122493 1000Toxaphene Peak 2 Ave 112915 1000Toxaphene Peak 3 Ave 98212 1000Toxaphene Peak 4 Ave 64477 1000Toxaphene Peak 5 Ave 101138 1000Toxaphene Peak 6 Ave 121791 1000Toxaphene Peak 7 Ave 50603 1000Toxaphene Peak 8 Ave 56145 1000
Curve Type Legend:Ave = Average
FORM VI 8081A 06/03/2010Page 405 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC1
Analy Batch No.: 37146
6138Calibration Start Date: Calibration End Date:05/11/2010 14:10
N
05/11/2010 14:10
0.53(mm)GC Column: CLP-1 ID:
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-37146/11 xr108641.d
ANALYTE LVL 1 AVG RTRT WINDOW
Toxaphene Peak 1 7.5637.493 - 7.6337.563Toxaphene Peak 2 7.6407.570 - 7.7107.640Toxaphene Peak 3 7.8177.747 - 7.8877.817Toxaphene Peak 4 7.9437.873 - 8.0137.943Toxaphene Peak 5 8.0377.967 - 8.1078.037Toxaphene Peak 6 8.1178.047 - 8.1878.117Toxaphene Peak 7 8.4408.370 - 8.5108.440Toxaphene Peak 8 8.6108.540 - 8.6808.610
FORM VI 8081A 06/03/2010Page 406 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC1
Analy Batch No.: 37146
6138Calibration Start Date: Calibration End Date:05/11/2010 14:10
N
05/11/2010 14:10
0.53(mm)CLP-1 ID:
EXTERNAL STANDARD CURVE EVALUTION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-37146/11 xr108641.d
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 1
RRFANALYTE MIN RRF
318.65Toxaphene Peak 1 Ave 319 20.0228.60Toxaphene Peak 2 Ave 229 20.0249.56Toxaphene Peak 3 Ave 250 20.0189.17Toxaphene Peak 4 Ave 189 20.0203.69Toxaphene Peak 5 Ave 204 20.0346.52Toxaphene Peak 6 Ave 347 20.0142.50Toxaphene Peak 7 Ave 143 20.088.612Toxaphene Peak 8 Ave 89 20.0
FORM VI 8081A
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 407 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC1
Analy Batch No.: 37146
6138Calibration Start Date: Calibration End Date:05/11/2010 14:10
N
05/11/2010 14:10
GC Column: CLP-1 ID: 0.53(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-37146/11 xr108641.d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UG/L)
LVL 1 LVL 1
Toxaphene Peak 1 Ave 318647 1000Toxaphene Peak 2 Ave 228602 1000Toxaphene Peak 3 Ave 249559 1000Toxaphene Peak 4 Ave 189171 1000Toxaphene Peak 5 Ave 203690 1000Toxaphene Peak 6 Ave 346524 1000Toxaphene Peak 7 Ave 142501 1000Toxaphene Peak 8 Ave 88612 1000
Curve Type Legend:Ave = Average
FORM VI 8081A 06/03/2010Page 408 of 623
FORM VII
Lab Name: Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
PESTICIDES PERFORMANCE EVALUATION MIXTURE (PEM)
0.53(mm)
460-13139-1
PESTGC1
05/17/2010 05:13
05/11/2010 12:47
05/11/2010 13:42
PEM 460-37575/4
CLP-2
TestAmerica Edison
Lab File ID: xf108818.d Conc. Units: ug/L
#LIMITBREAKDOWN (%)PEAK AREARTANALYTE
7.87Endrin 609276 6.41 15
8.50Endrin aldehyde 12596
9.41Endrin ketone 29168
#LIMITBREAKDOWN (%)PEAK AREARTANALYTE
8.344,4'-DDT 552424 4.78 15
7.984,4'-DDD 18240
7.264,4'-DDE 9472
FORM VII 8081A
06/03/2010Page 409 of 623
Data File: xf108818.d Report Date: 17-May-2010 11:16
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC1.i/8081T/front/May10/05-17-10/17may10a.b/xf108818.dLab Smp Id: SGDDT/Ei_00009 Inj Date : 17-MAY-2010 05:13 Operator : 462 Inst ID: PESTGC1.iSmp Info : SGDDT/Ei_00009Misc Info : Comment : Method : /chem1/PESTGC1.i/8081T/front/May10/05-17-10/17may10a.b/09Xf8081.mMeth Date : 17-May-2010 11:16 ferdie Quant Type: ESTDCal Date : 11-MAY-2010 14:10 Cal File: xf108641.dAls bottle: 1 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: END_DDT.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (uL)(1000 low, 2Ws 15.00000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
7 4,4'-DDD CAS #: 72-54-8
7.983 7.967 0.016 18240 9.49468 6.3 80.00- 120.00 100.00(a)
-------------------------------------------------------------------------------
8 4,4'-DDE CAS #: 72-55-9
7.260 7.230 0.030 9472 3.96424 2.6 80.00- 120.00 100.00(a)
-------------------------------------------------------------------------------
9 4,4'-DDT CAS #: 50-29-3
8.343 8.330 0.013 552424 310.464 210 80.00- 120.00 100.00
-------------------------------------------------------------------------------
14 Endrin CAS #: 72-20-8
7.873 7.857 0.016 609276 307.857 200 80.00- 120.00 100.00
-------------------------------------------------------------------------------
15 Endrin aldehyde CAS #: 7421-93-4
8.500 8.483 0.017 12596 7.17809 4.8 80.00- 120.00 100.00(a)
-------------------------------------------------------------------------------
06/03/2010Page 410 of 623
Data File: xf108818.d Report Date: 17-May-2010 11:16
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
16 Endrin ketone CAS #: 53494-70-5
9.413 9.403 0.010 29168 13.2146 8.8 80.00- 120.00 100.00
-------------------------------------------------------------------------------
QC Flag Legend
a - Target compound detected but, quantitated amountBelow Limit Of Quantitation(BLOQ).
06/03/2010Page 411 of 623
Data File: xf108818.d
Date: 17-MAY-2010 05:13
Client ID: Instrument: PESTGC1.i
Sample Info: SGDDT/Ei_00009 Operator: 462
06/03/2010Page 412 of 623
FORM VII
Lab Name: Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
PESTICIDES PERFORMANCE EVALUATION MIXTURE (PEM)
0.53(mm)
460-13139-1
PESTGC1
05/17/2010 05:13
05/11/2010 12:47
05/11/2010 13:42
PEM 460-37575/4
CLP-1
TestAmerica Edison
Lab File ID: xr108818.d Conc. Units: ug/L
#LIMITBREAKDOWN (%)PEAK AREARTANALYTE
6.57Endrin 1349360 4.96 15
7.68Endrin aldehyde 19144
8.47Endrin ketone 51211
#LIMITBREAKDOWN (%)PEAK AREARTANALYTE
7.294,4'-DDT 1136924 4.07 15
6.754,4'-DDD 30034
5.224,4'-DDE 18162
FORM VII 8081A
06/03/2010Page 413 of 623
Data File: xr108818.d Page 1 Report Date: 17-May-2010 11:16
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC1.i/8081T/rear/May10/05-17-10/17may10a.b/xr108818.dLab Smp Id: SGDDT/Ei_00009 Inj Date : 17-MAY-2010 05:13 Operator : 462 Inst ID: PESTGC1.iSmp Info : SGDDT/Ei_00009Misc Info : Comment : Method : /chem1/PESTGC1.i/8081T/rear/May10/05-17-10/17may10a.b/09Xr8081.mMeth Date : 17-May-2010 08:58 ferdie Quant Type: ESTDCal Date : 11-MAY-2010 14:10 Cal File: xr108641.dAls bottle: 1 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: END_DDT.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (uL)(1000 low, 2Ws 15.00000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
7 4,4'-DDD CAS #: 72-54-8
6.753 6.737 0.016 30034 7.61295 5.1 80.00- 120.00 100.00(a)
-------------------------------------------------------------------------------
8 4,4'-DDE CAS #: 72-55-9
5.220 5.203 0.017 18162 4.00882 2.7 80.00- 120.00 100.00(a)
-------------------------------------------------------------------------------
9 4,4'-DDT CAS #: 50-29-3
7.293 7.287 0.006 1136924 299.744 200 80.00- 120.00 100.00
-------------------------------------------------------------------------------
14 Endrin CAS #: 72-20-8
6.570 6.557 0.013 1349360 313.835 210 80.00- 120.00 100.00
-------------------------------------------------------------------------------
15 Endrin aldehyde CAS #: 7421-93-4
7.680 7.673 0.007 19144 5.64170 3.8 80.00- 120.00 100.00(a)
-------------------------------------------------------------------------------
06/03/2010Page 414 of 623
Data File: xr108818.d Page 2 Report Date: 17-May-2010 11:16
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
16 Endrin ketone CAS #: 53494-70-5
8.470 8.463 0.007 51211 11.7270 7.8 80.00- 120.00 100.00
-------------------------------------------------------------------------------
QC Flag Legend
a - Target compound detected but, quantitated amountBelow Limit Of Quantitation(BLOQ).
06/03/2010Page 415 of 623
Data File: xr108818.d
Date: 17-MAY-2010 05:13
Client ID: Instrument: PESTGC1.i
Sample Info: SGDDT/Ei_00009 Operator: 462
06/03/2010Page 416 of 623
FORM VII
Lab Name: Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
PESTICIDES CONTINUING CALIBRATION DATA
0.53(mm)
460-13139-1
PESTGC1
05/17/2010 05:29
05/11/2010 12:47
05/11/2010 13:42
CCVRT 460-37575/5
CLP-2
TestAmerica Edison
Lab File ID: xf108819.d Conc. Units: ug/L
ANALYTE CURVE AVE RRF RRF MIN RRF CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
alpha-BHC Ave 32973156 104 100 4.5 15.0
gamma-BHC (Lindane) Ave 29512874 103 100 2.7 15.0
beta-BHC Ave 14351454 98.7 100 -1.3 15.0
delta-BHC Ave 31502964 106 100 6.3 15.0
Heptachlor Ave 32423149 103 100 3.0 15.0
Aldrin Ave 33743123 108 100 8.0 15.0
Heptachlor epoxide Ave 32123088 104 100 4.0 15.0
gamma-Chlordane Ave 34333137 109 100 9.4 15.0
alpha-Chlordane Ave 29642886 103 100 2.7 15.0
Endosulfan I Ave 27342645 103 100 3.4 15.0
4,4'-DDE Ave 25452389 107 100 6.5 15.0
Dieldrin Ave 26302526 104 100 4.1 15.0
Endrin Ave 20521979 104 100 3.7 15.0
4,4'-DDD Ave 19451921 101 100 1.2 15.0
Endosulfan II Ave 21942178 101 100 0.7 15.0
4,4'-DDT Ave 18601779 105 100 4.5 15.0
Endrin aldehyde Ave 17841755 102 100 1.6 15.0
Endosulfan sulfate Ave 19801948 102 100 1.7 15.0
Methoxychlor Ave 918.8999 92.0 100 -8.0 15.0
Endrin ketone Ave 22342207 101 100 1.2 15.0
Tetrachloro-m-xylene Ave 24642246 110 100 9.7 15.0
DCB Decachlorobiphenyl Ave 14171309 108 100 8.3 15.0
FORM VII 8081A
06/03/2010Page 417 of 623
FORM VII
Lab Name: Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
PESTICIDES CONTINUING CALIBRATION RETENTION TIME SUMMARY
0.53(mm)
460-13139-1
PESTGC1
05/17/2010 05:29
05/11/2010 12:47
05/11/2010 13:42
CCVRT 460-37575/5
CLP-2
TestAmerica Edison
Lab File ID: xf108819.d
Analyte RTTO FROM
RT WINDOW
alpha-BHC 2.77 2.72 2.82
gamma-BHC (Lindane) 3.11 3.06 3.16
beta-BHC 3.20 3.14 3.24
delta-BHC 3.57 3.52 3.62
Heptachlor 3.70 3.64 3.74
Aldrin 4.49 4.43 4.53
Heptachlor epoxide 6.04 5.96 6.10
gamma-Chlordane 6.54 6.46 6.60
alpha-Chlordane 6.90 6.83 6.97
Endosulfan I 7.04 6.96 7.10
4,4'-DDE 7.23 7.15 7.29
Dieldrin 7.49 7.42 7.56
Endrin 7.86 7.78 7.92
4,4'-DDD 7.97 7.89 8.03
Endosulfan II 8.10 8.02 8.16
4,4'-DDT 8.33 8.26 8.40
Endrin aldehyde 8.48 8.41 8.55
Endosulfan sulfate 8.81 8.74 8.88
Methoxychlor 9.12 9.05 9.19
Endrin ketone 9.40 9.33 9.47
Tetrachloro-m-xylene 2.29 2.24 2.34
DCB Decachlorobiphenyl 10.33 10.23 10.43
Form VII 8081A
06/03/2010Page 418 of 623
FORM VII
Lab Name: Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
PESTICIDES CONTINUING CALIBRATION DATA
0.53(mm)
460-13139-1
PESTGC1
05/17/2010 05:29
05/11/2010 12:47
05/11/2010 13:42
CCVRT 460-37575/5
CLP-1
TestAmerica Edison
Lab File ID: xr108819.d Conc. Units: ug/L
ANALYTE CURVE AVE RRF RRF MIN RRF CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
alpha-BHC Ave 61405948 103 100 3.2 15.0
gamma-BHC (Lindane) Ave 52675195 101 100 1.4 15.0
beta-BHC Ave 29512838 104 100 4.0 15.0
delta-BHC Ave 57055472 104 100 4.3 15.0
Heptachlor Ave 56315413 104 100 4.0 15.0
Aldrin Ave 54675150 106 100 6.1 15.0
Heptachlor epoxide Ave 54765295 103 100 3.4 15.0
gamma-Chlordane Ave 54605346 102 100 2.1 15.0
alpha-Chlordane Ave 49395196 95.1 100 -4.9 15.0
4,4'-DDE Ave 47704531 105 100 5.3 15.0
Endosulfan I Ave 52234954 105 100 5.4 15.0
Dieldrin Ave 53695071 106 100 5.9 15.0
Endrin Ave 46994300 109 100 9.3 15.0
4,4'-DDD Ave 40633945 103 100 3.0 15.0
Endosulfan II Ave 45624368 104 100 4.4 15.0
4,4'-DDT Ave 41663793 110 100 9.8 15.0
Endrin aldehyde Ave 36283393 107 100 6.9 15.0
Methoxychlor Ave 21142006 105 100 5.3 15.0
Endosulfan sulfate Ave 38753696 105 100 4.9 15.0
Endrin ketone Ave 45364367 104 100 3.9 15.0
Tetrachloro-m-xylene Ave 42714069 105 100 5.0 15.0
DCB Decachlorobiphenyl Ave 25832527 102 100 2.2 15.0
FORM VII 8081A
06/03/2010Page 419 of 623
FORM VII
Lab Name: Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
PESTICIDES CONTINUING CALIBRATION RETENTION TIME SUMMARY
0.53(mm)
460-13139-1
PESTGC1
05/17/2010 05:29
05/11/2010 12:47
05/11/2010 13:42
CCVRT 460-37575/5
CLP-1
TestAmerica Edison
Lab File ID: xr108819.d
Analyte RTTO FROM
RT WINDOW
alpha-BHC 2.38 2.33 2.43
gamma-BHC (Lindane) 2.61 2.56 2.66
beta-BHC 2.67 2.62 2.72
delta-BHC 2.81 2.76 2.86
Heptachlor 2.99 2.93 3.03
Aldrin 3.28 3.22 3.32
Heptachlor epoxide 4.35 4.27 4.41
gamma-Chlordane 4.65 4.58 4.72
alpha-Chlordane 4.99 4.91 5.05
4,4'-DDE 5.20 5.13 5.27
Endosulfan I 5.34 5.26 5.40
Dieldrin 5.98 5.90 6.04
Endrin 6.56 6.48 6.62
4,4'-DDD 6.74 6.66 6.80
Endosulfan II 7.07 6.99 7.13
4,4'-DDT 7.29 7.21 7.35
Endrin aldehyde 7.67 7.60 7.74
Methoxychlor 7.88 7.81 7.95
Endosulfan sulfate 8.15 8.08 8.22
Endrin ketone 8.46 8.39 8.53
Tetrachloro-m-xylene 1.99 1.93 2.03
DCB Decachlorobiphenyl 9.51 9.41 9.61
Form VII 8081A
06/03/2010Page 420 of 623
FORM VII
Lab Name: Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
PESTICIDES CONTINUING CALIBRATION DATA
0.53(mm)
460-13139-1
PESTGC1
05/17/2010 10:04
05/11/2010 12:47
05/11/2010 13:42
CCV 460-37575/23
CLP-2
TestAmerica Edison
Lab File ID: xf108837.d Conc. Units: ug/L
ANALYTE CURVE AVE RRF RRF MIN RRF CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
alpha-BHC Ave 31283156 99.1 100 -0.9 15.0
gamma-BHC (Lindane) Ave 28242874 98.3 100 -1.7 15.0
beta-BHC Ave 13851454 95.3 100 -4.7 15.0
delta-BHC Ave 29842964 101 100 0.7 15.0
Heptachlor Ave 30203149 95.9 100 -4.1 15.0
Aldrin Ave 31583123 101 100 1.1 15.0
Heptachlor epoxide Ave 29963088 97.0 100 -3.0 15.0
gamma-Chlordane Ave 30003137 95.6 100 -4.4 15.0
alpha-Chlordane Ave 27702886 96.0 100 -4.0 15.0
Endosulfan I Ave 25562645 96.7 100 -3.3 15.0
4,4'-DDE Ave 23772389 99.5 100 -0.5 15.0
Dieldrin Ave 24712526 97.8 100 -2.2 15.0
Endrin Ave 19251979 97.3 100 -2.7 15.0
4,4'-DDD Ave 19401921 101 100 1.0 15.0
Endosulfan II Ave 20592178 94.6 100 -5.4 15.0
4,4'-DDT Ave 15681779 88.1 100 -11.9 15.0
Endrin aldehyde Ave 16121755 91.9 100 -8.1 15.0
Endosulfan sulfate Ave 18371948 94.3 100 -5.7 15.0
Methoxychlor Ave 888.7999 88.9 100 -11.1 15.0
Endrin ketone Ave 20562207 93.2 100 -6.8 15.0
Tetrachloro-m-xylene Ave 22612246 101 100 0.7 15.0
DCB Decachlorobiphenyl Ave 13071309 99.9 100 -0.1 15.0
FORM VII 8081A
06/03/2010Page 421 of 623
FORM VII
Lab Name: Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
PESTICIDES CONTINUING CALIBRATION RETENTION TIME SUMMARY
0.53(mm)
460-13139-1
PESTGC1
05/17/2010 10:04
05/11/2010 12:47
05/11/2010 13:42
CCV 460-37575/23
CLP-2
TestAmerica Edison
Lab File ID: xf108837.d
Analyte RTTO FROM
RT WINDOW
alpha-BHC 2.77 2.72 2.82
gamma-BHC (Lindane) 3.11 3.06 3.16
beta-BHC 3.19 3.14 3.24
delta-BHC 3.57 3.52 3.62
Heptachlor 3.69 3.64 3.74
Aldrin 4.48 4.43 4.53
Heptachlor epoxide 6.03 5.96 6.10
gamma-Chlordane 6.53 6.46 6.60
alpha-Chlordane 6.90 6.83 6.97
Endosulfan I 7.03 6.96 7.10
4,4'-DDE 7.22 7.15 7.29
Dieldrin 7.49 7.42 7.56
Endrin 7.85 7.78 7.92
4,4'-DDD 7.96 7.89 8.03
Endosulfan II 8.09 8.02 8.16
4,4'-DDT 8.33 8.26 8.40
Endrin aldehyde 8.48 8.41 8.55
Endosulfan sulfate 8.81 8.74 8.88
Methoxychlor 9.12 9.05 9.19
Endrin ketone 9.40 9.33 9.47
Tetrachloro-m-xylene 2.29 2.24 2.34
DCB Decachlorobiphenyl 10.33 10.23 10.43
Form VII 8081A
06/03/2010Page 422 of 623
FORM VII
Lab Name: Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
PESTICIDES CONTINUING CALIBRATION DATA
0.53(mm)
460-13139-1
PESTGC1
05/17/2010 10:04
05/11/2010 12:47
05/11/2010 13:42
CCV 460-37575/23
CLP-1
TestAmerica Edison
Lab File ID: xr108837.d Conc. Units: ug/L
ANALYTE CURVE AVE RRF RRF MIN RRF CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
alpha-BHC Ave 61885948 104 100 4.0 15.0
gamma-BHC (Lindane) Ave 52625195 101 100 1.3 15.0
beta-BHC Ave 29502838 104 100 3.9 15.0
delta-BHC Ave 57205472 105 100 4.5 15.0
Heptachlor Ave 54575413 101 100 0.8 15.0
Aldrin Ave 53275150 103 100 3.4 15.0
Heptachlor epoxide Ave 53045295 100 100 0.2 15.0
gamma-Chlordane Ave 53045346 99.2 100 -0.8 15.0
alpha-Chlordane Ave 51965196 100 100 0.0 15.0
4,4'-DDE Ave 46334531 102 100 2.3 15.0
Endosulfan I Ave 50604954 102 100 2.1 15.0
Dieldrin Ave 51915071 102 100 2.4 15.0
Endrin Ave 44854300 104 100 4.3 15.0
4,4'-DDD Ave 42603945 108 100 8.0 15.0
Endosulfan II Ave 43734368 100 100 0.1 15.0
4,4'-DDT Ave 35593793 93.8 100 -6.2 15.0
Endrin aldehyde Ave 32893393 96.9 100 -3.1 15.0
Methoxychlor Ave 19012006 94.7 100 -5.3 15.0
Endosulfan sulfate Ave 36073696 97.6 100 -2.4 15.0
Endrin ketone Ave 41254367 94.5 100 -5.5 15.0
Tetrachloro-m-xylene Ave 43824069 108 100 7.7 15.0
DCB Decachlorobiphenyl Ave 24042527 95.1 100 -4.9 15.0
FORM VII 8081A
06/03/2010Page 423 of 623
FORM VII
Lab Name: Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
PESTICIDES CONTINUING CALIBRATION RETENTION TIME SUMMARY
0.53(mm)
460-13139-1
PESTGC1
05/17/2010 10:04
05/11/2010 12:47
05/11/2010 13:42
CCV 460-37575/23
CLP-1
TestAmerica Edison
Lab File ID: xr108837.d
Analyte RTTO FROM
RT WINDOW
alpha-BHC 2.38 2.33 2.43
gamma-BHC (Lindane) 2.61 2.56 2.66
beta-BHC 2.67 2.62 2.72
delta-BHC 2.81 2.76 2.86
Heptachlor 2.98 2.93 3.03
Aldrin 3.27 3.22 3.32
Heptachlor epoxide 4.34 4.27 4.41
gamma-Chlordane 4.65 4.58 4.72
alpha-Chlordane 4.98 4.91 5.05
4,4'-DDE 5.20 5.13 5.27
Endosulfan I 5.33 5.26 5.40
Dieldrin 5.97 5.90 6.04
Endrin 6.55 6.48 6.62
4,4'-DDD 6.73 6.66 6.80
Endosulfan II 7.06 6.99 7.13
4,4'-DDT 7.28 7.21 7.35
Endrin aldehyde 7.67 7.60 7.74
Methoxychlor 7.88 7.81 7.95
Endosulfan sulfate 8.15 8.08 8.22
Endrin ketone 8.46 8.39 8.53
Tetrachloro-m-xylene 1.98 1.93 2.03
DCB Decachlorobiphenyl 9.51 9.41 9.61
Form VII 8081A
06/03/2010Page 424 of 623
FORM IForm 1PESTICIDES ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: MB 460-37420/1-A
Matrix: xf108835.dLab File ID:
Date Collected:8081AAnalysis Method:
Solid
TestAmerica Edison
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 09:15
05/17/2010 09:37
N
10(mL)
1(uL)
Sample wt/vol: 15.00(g)
% Moisture:
GC Column: ID: 0.53(mm)CLP-2
Analysis Batch No.: 37575 ug/KgUnits:
SURROGATE %RECCAS NO. LIMITS Q
877-09-8 Tetrachloro-m-xylene 76 22-141
2051-24-3 DCB Decachlorobiphenyl 145 10-165
FORM I 8081A
06/03/2010Page 425 of 623
Data File: xf108835.d Report Date: 17-May-2010 11:17
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC1.i/8081T/front/May10/05-17-10/17may10a.b/xf108835.dLab Smp Id: mb 460-37420/1-a Inj Date : 17-MAY-2010 09:37 Operator : 462 Inst ID: PESTGC1.iSmp Info : mb 460-37420/1-aMisc Info : Comment : Method : /chem1/PESTGC1.i/8081T/front/May10/05-17-10/17may10a.b/09Xf8081.mMeth Date : 17-May-2010 11:16 ferdie Quant Type: ESTDCal Date : 11-MAY-2010 14:10 Cal File: xf108641.dAls bottle: 1 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: Allpest.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (uL)(1000 low, 2Ws 15.00000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 28 Tetrachloro-m-xylene CAS #: 877-09-8
2.283 2.287 -0.004 85900 38.2407 25 80.00- 120.00 100.00
-------------------------------------------------------------------------------
$ 30 Decachlorobiphenyl CAS #: 2051-24-3
10.333 10.333 0.000 95179 72.7350 48 80.00- 120.00 100.00
-------------------------------------------------------------------------------
06/03/2010Page 426 of 623
Data File: xf108835.d
Date: 17-MAY-2010 09:37
Client ID: Instrument: PESTGC1.i
Sample Info: mb 460-37420/1-a Operator: 462
06/03/2010Page 427 of 623
FORM IForm 1PESTICIDES ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: MB 460-37420/1-A
Matrix: xr108835.dLab File ID:
Date Collected:8081AAnalysis Method:
Solid
TestAmerica Edison
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 09:15
05/17/2010 09:37
N
10(mL)
1(uL)
Sample wt/vol: 15.00(g)
% Moisture:
GC Column: ID: 0.53(mm)CLP-1
Analysis Batch No.: 37575 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Aldrin309-00-2 6.7 6.7 1.5U
alpha-BHC319-84-6 6.7 6.7 1.2U
beta-BHC319-85-7 6.7 6.7 0.91U
delta-BHC319-86-8 6.7 6.7 1.0U
gamma-BHC (Lindane)58-89-9 6.7 6.7 0.78U
Chlordane57-74-9 67 67 15U
4,4'-DDD72-54-8 6.7 6.7 0.80U
4,4'-DDE72-55-9 6.7 6.7 1.3U
4,4'-DDT50-29-3 6.7 6.7 0.84U
Dieldrin60-57-1 6.7 6.7 1.3U
Endosulfan I959-98-8 6.7 6.7 1.4U
Endosulfan II33213-65-9 6.7 6.7 1.0U
Endosulfan sulfate1031-07-8 6.7 6.7 0.86U
Endrin72-20-8 6.7 6.7 0.94U
Endrin aldehyde7421-93-4 6.7 6.7 1.7U
Heptachlor76-44-8 6.7 6.7 0.96U
Heptachlor epoxide1024-57-3 6.7 6.7 1.4U
Toxaphene8001-35-2 67 67 14U
SURROGATE %RECCAS NO. LIMITS Q
877-09-8 Tetrachloro-m-xylene 75 22-141
2051-24-3 DCB Decachlorobiphenyl 118 10-165
FORM I 8081A
06/03/2010Page 428 of 623
Data File: xr108835.d Page 1 Report Date: 17-May-2010 11:17
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC1.i/8081T/rear/May10/05-17-10/17may10a.b/xr108835.dLab Smp Id: mb 460-37420/1-a Inj Date : 17-MAY-2010 09:37 Operator : 462 Inst ID: PESTGC1.iSmp Info : mb 460-37420/1-aMisc Info : Comment : Method : /chem1/PESTGC1.i/8081T/rear/May10/05-17-10/17may10a.b/09Xr8081.mMeth Date : 17-May-2010 08:58 ferdie Quant Type: ESTDCal Date : 11-MAY-2010 14:10 Cal File: xr108641.dAls bottle: 1 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: Allpest.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (uL)(1000 low, 2Ws 15.00000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 28 Tetrachloro-m-xylene CAS #: 877-09-8
1.983 1.987 -0.004 152446 37.4640 25 80.00- 120.00 100.00
-------------------------------------------------------------------------------
$ 30 Decachlorobiphenyl CAS #: 2051-24-3
9.513 9.513 0.000 148995 58.9567 39 80.00- 120.00 100.00
-------------------------------------------------------------------------------
06/03/2010Page 429 of 623
Data File: xr108835.d
Date: 17-MAY-2010 09:37
Client ID: Instrument: PESTGC1.i
Sample Info: mb 460-37420/1-a Operator: 462
06/03/2010Page 430 of 623
FORM IForm 1PESTICIDES ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: LCS 460-37420/2-A
Matrix: xf108820.dLab File ID:
Date Collected:8081AAnalysis Method:
Solid
TestAmerica Edison
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 09:15
05/17/2010 05:43
N
10(mL)
1(uL)
Sample wt/vol: 15.00(g)
% Moisture:
GC Column: ID: 0.53(mm)CLP-2
Analysis Batch No.: 37575 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Aldrin309-00-2 88.9 6.7 1.5
alpha-BHC319-84-6 96.3 6.7 1.2
beta-BHC319-85-7 104 6.7 0.91
delta-BHC319-86-8 121 6.7 1.0
gamma-BHC (Lindane)58-89-9 98.6 6.7 0.78
Chlordane57-74-9 67 67 15U
4,4'-DDD72-54-8 94.7 6.7 0.80
4,4'-DDE72-55-9 98.1 6.7 1.3
4,4'-DDT50-29-3 99.1 6.7 0.84
Dieldrin60-57-1 88.6 6.7 1.3
Endosulfan I959-98-8 93.6 6.7 1.4
Endosulfan II33213-65-9 101 6.7 1.0
Endosulfan sulfate1031-07-8 103 6.7 0.86
Endrin72-20-8 101 6.7 0.94
Endrin aldehyde7421-93-4 103 6.7 1.7
Heptachlor76-44-8 93.0 6.7 0.96
Heptachlor epoxide1024-57-3 97.0 6.7 1.4
Toxaphene8001-35-2 67 67 14U
SURROGATE %RECCAS NO. LIMITS Q
877-09-8 Tetrachloro-m-xylene 75 22-141
2051-24-3 DCB Decachlorobiphenyl 93 10-165
FORM I 8081A
06/03/2010Page 431 of 623
Data File: xf108820.d Report Date: 17-May-2010 11:42
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC1.i/8081T/front/May10/05-17-10/17may10a.b/xf108820.dLab Smp Id: lcs 460-37420/2-a Inj Date : 17-MAY-2010 05:43 Operator : 462 Inst ID: PESTGC1.iSmp Info : lcs 460-37420/2-aMisc Info : Comment : Method : /chem1/PESTGC1.i/8081T/front/May10/05-17-10/17may10a.b/09Xf8081.mMeth Date : 17-May-2010 11:24 ferdie Quant Type: ESTDCal Date : 11-MAY-2010 14:10 Cal File: xf108641.dAls bottle: 1 QC Sample: BSDil Factor: 1.00000 Integrator: Falcon Compound Sublist: Allpest.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (uL)(1000 low, 2Ws 15.00000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 28 Tetrachloro-m-xylene CAS #: 877-09-8
2.297 2.287 0.010 84665 37.6912 25 80.00- 120.00 100.00
-------------------------------------------------------------------------------
2 alpha-BHC CAS #: 319-84-6
2.787 2.773 0.014 455846 144.444 96 80.00- 120.00 100.00
-------------------------------------------------------------------------------
5 gamma-BHC (Lindane) CAS #: 58-89-9
3.130 3.110 0.020 424962 147.882 98 80.00- 120.00 100.00
-------------------------------------------------------------------------------
3 beta-BHC CAS #: 319-85-7
3.217 3.193 0.024 227814 156.710 100 80.00- 120.00 100.00
-------------------------------------------------------------------------------
4 delta-BHC CAS #: 319-86-8
3.600 3.567 0.033 539355 181.992 120 80.00- 120.00 100.00
-------------------------------------------------------------------------------
06/03/2010Page 432 of 623
Data File: xf108820.d Report Date: 17-May-2010 11:42
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
17 Heptachlor CAS #: 76-44-8
3.733 3.693 0.040 439419 139.526 93 80.00- 120.00 100.00
-------------------------------------------------------------------------------
1 Aldrin CAS #: 309-00-2
4.540 4.480 0.060 416438 133.338 89 80.00- 120.00 100.00
-------------------------------------------------------------------------------
18 Heptachlor epoxide CAS #: 1024-57-3
6.100 6.033 0.067 449342 145.509 97 80.00- 120.00 100.00
-------------------------------------------------------------------------------
65 gamma-Chlordane CAS #: 5103-74-2
6.593 6.533 0.060 447261 142.559 95 80.00- 120.00 100.00
-------------------------------------------------------------------------------
66 alpha-Chlordane CAS #: 5103-71-9
6.953 6.897 0.056 399977 138.577 92 80.00- 120.00 100.00
-------------------------------------------------------------------------------
11 Endosulfan I CAS #: 959-98-8
7.080 7.033 0.047 371309 140.399 94 80.00- 120.00 100.00
-------------------------------------------------------------------------------
8 4,4'-DDE CAS #: 72-55-9
7.263 7.223 0.040 351669 147.181 98 80.00- 120.00 100.00
-------------------------------------------------------------------------------
10 Dieldrin CAS #: 60-57-1
7.517 7.487 0.030 335800 132.944 89 80.00- 120.00 100.00
-------------------------------------------------------------------------------
14 Endrin CAS #: 72-20-8
7.880 7.853 0.027 299228 151.195 100 80.00- 120.00 100.00
-------------------------------------------------------------------------------
7 4,4'-DDD CAS #: 72-54-8
7.987 7.963 0.024 272949 142.081 95 80.00- 120.00 100.00
-------------------------------------------------------------------------------
12 Endosulfan II CAS #: 33213-65-9
8.117 8.093 0.024 331407 152.166 100 80.00- 120.00 100.00
-------------------------------------------------------------------------------
9 4,4'-DDT CAS #: 50-29-3
8.350 8.327 0.023 264580 148.695 99 80.00- 120.00 100.00
-------------------------------------------------------------------------------
15 Endrin aldehyde CAS #: 7421-93-4
8.503 8.480 0.023 272239 155.141 100 80.00- 120.00 100.00
-------------------------------------------------------------------------------
13 Endosulfan sulfate CAS #: 1031-07-8
8.830 8.807 0.023 301417 154.742 100 80.00- 120.00 100.00
-------------------------------------------------------------------------------
19 Methoxychlor CAS #: 72-43-5
9.140 9.120 0.020 127407 127.521 85 80.00- 120.00 100.00
-------------------------------------------------------------------------------
16 Endrin ketone CAS #: 53494-70-5
9.417 9.400 0.017 310105 140.494 94 80.00- 120.00 100.00
-------------------------------------------------------------------------------
06/03/2010Page 433 of 623
Data File: xf108820.d Report Date: 17-May-2010 11:42
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 30 Decachlorobiphenyl CAS #: 2051-24-3
10.343 10.333 0.010 60842 46.4952 31 80.00- 120.00 100.00
-------------------------------------------------------------------------------
06/03/2010Page 434 of 623
Data File: xf108820.d
Date: 17-MAY-2010 05:43
Client ID: Instrument: PESTGC1.i
Sample Info: lcs 460-37420/2-a Operator: 462
06/03/2010Page 435 of 623
FORM IForm 1PESTICIDES ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: LCS 460-37420/2-A
Matrix: xr108820.dLab File ID:
Date Collected:8081AAnalysis Method:
Solid
TestAmerica Edison
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 09:15
05/17/2010 05:43
N
10(mL)
1(uL)
Sample wt/vol: 15.00(g)
% Moisture:
GC Column: ID: 0.53(mm)CLP-1
Analysis Batch No.: 37575 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Aldrin309-00-2 82.2 6.7 1.5
alpha-BHC319-84-6 89.0 6.7 1.2
beta-BHC319-85-7 102 6.7 0.91
delta-BHC319-86-8 109 6.7 1.0
gamma-BHC (Lindane)58-89-9 90.2 6.7 0.78
Chlordane57-74-9 67 67 15U
4,4'-DDD72-54-8 93.4 6.7 0.80
4,4'-DDE72-55-9 94.8 6.7 1.3
4,4'-DDT50-29-3 97.2 6.7 0.84
Dieldrin60-57-1 89.6 6.7 1.3
Endosulfan I959-98-8 93.3 6.7 1.4
Endosulfan II33213-65-9 101 6.7 1.0
Endosulfan sulfate1031-07-8 101 6.7 0.86
Endrin72-20-8 104 6.7 0.94
Endrin aldehyde7421-93-4 104 6.7 1.7
Heptachlor76-44-8 87.2 6.7 0.96
Heptachlor epoxide1024-57-3 93.5 6.7 1.4
Toxaphene8001-35-2 67 67 14U
SURROGATE %RECCAS NO. LIMITS Q
877-09-8 Tetrachloro-m-xylene 71 22-141
2051-24-3 DCB Decachlorobiphenyl 92 10-165
FORM I 8081A
06/03/2010Page 436 of 623
Data File: xr108820.d Page 1 Report Date: 17-May-2010 11:16
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC1.i/8081T/rear/May10/05-17-10/17may10a.b/xr108820.dLab Smp Id: lcs 460-37420/2-a Inj Date : 17-MAY-2010 05:43 Operator : 462 Inst ID: PESTGC1.iSmp Info : lcs 460-37420/2-aMisc Info : Comment : Method : /chem1/PESTGC1.i/8081T/rear/May10/05-17-10/17may10a.b/09Xr8081.mMeth Date : 17-May-2010 08:58 ferdie Quant Type: ESTDCal Date : 11-MAY-2010 14:10 Cal File: xr108641.dAls bottle: 1 QC Sample: BSDil Factor: 1.00000 Integrator: Falcon Compound Sublist: Allpest.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (uL)(1000 low, 2Ws 15.00000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 28 Tetrachloro-m-xylene CAS #: 877-09-8
1.980 1.987 -0.007 144623 35.5415 24 80.00- 120.00 100.00
-------------------------------------------------------------------------------
2 alpha-BHC CAS #: 319-84-6
2.380 2.380 0.000 794220 133.518 89 80.00- 120.00 100.00
-------------------------------------------------------------------------------
5 gamma-BHC (Lindane) CAS #: 58-89-9
2.607 2.607 0.000 702767 135.282 90 80.00- 120.00 100.00
-------------------------------------------------------------------------------
3 beta-BHC CAS #: 319-85-7
2.673 2.673 0.000 432408 152.340 100 80.00- 120.00 100.00
-------------------------------------------------------------------------------
4 delta-BHC CAS #: 319-86-8
2.810 2.810 0.000 897926 164.109 110 80.00- 120.00 100.00
-------------------------------------------------------------------------------
06/03/2010Page 437 of 623
Data File: xr108820.d Page 2 Report Date: 17-May-2010 11:16
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
17 Heptachlor CAS #: 76-44-8
2.987 2.987 0.000 708298 130.847 87 80.00- 120.00 100.00
-------------------------------------------------------------------------------
1 Aldrin CAS #: 309-00-2
3.277 3.277 0.000 634789 123.254 82 80.00- 120.00 100.00
-------------------------------------------------------------------------------
18 Heptachlor epoxide CAS #: 1024-57-3
4.363 4.350 0.013 742239 140.183 93 80.00- 120.00 100.00
-------------------------------------------------------------------------------
65 gamma-Chlordane CAS #: 5103-74-2
4.670 4.653 0.017 731852 136.907 91 80.00- 120.00 100.00
-------------------------------------------------------------------------------
66 alpha-Chlordane CAS #: 5103-71-9
5.003 4.987 0.016 713323 137.292 92 80.00- 120.00 100.00
-------------------------------------------------------------------------------
8 4,4'-DDE CAS #: 72-55-9
5.223 5.203 0.020 643942 142.135 95 80.00- 120.00 100.00
-------------------------------------------------------------------------------
11 Endosulfan I CAS #: 959-98-8
5.357 5.337 0.020 693640 140.022 93 80.00- 120.00 100.00
-------------------------------------------------------------------------------
10 Dieldrin CAS #: 60-57-1
5.997 5.977 0.020 681463 134.385 90 80.00- 120.00 100.00
-------------------------------------------------------------------------------
14 Endrin CAS #: 72-20-8
6.573 6.557 0.016 671332 156.139 100 80.00- 120.00 100.00
-------------------------------------------------------------------------------
7 4,4'-DDD CAS #: 72-54-8
6.753 6.737 0.016 552980 140.168 93 80.00- 120.00 100.00
-------------------------------------------------------------------------------
12 Endosulfan II CAS #: 33213-65-9
7.083 7.067 0.016 658465 150.759 100 80.00- 120.00 100.00
-------------------------------------------------------------------------------
9 4,4'-DDT CAS #: 50-29-3
7.300 7.287 0.013 552775 145.736 97 80.00- 120.00 100.00
-------------------------------------------------------------------------------
15 Endrin aldehyde CAS #: 7421-93-4
7.680 7.673 0.007 528827 155.844 100 80.00- 120.00 100.00
-------------------------------------------------------------------------------
19 Methoxychlor CAS #: 72-43-5
7.890 7.883 0.007 265576 132.363 88 80.00- 120.00 100.00
-------------------------------------------------------------------------------
13 Endosulfan sulfate CAS #: 1031-07-8
8.160 8.153 0.007 561203 151.853 100 80.00- 120.00 100.00
-------------------------------------------------------------------------------
16 Endrin ketone CAS #: 53494-70-5
8.473 8.463 0.010 616529 141.182 94 80.00- 120.00 100.00
-------------------------------------------------------------------------------
06/03/2010Page 438 of 623
Data File: xr108820.d Page 3 Report Date: 17-May-2010 11:16
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 30 Decachlorobiphenyl CAS #: 2051-24-3
9.520 9.513 0.007 116320 46.0273 31 80.00- 120.00 100.00
-------------------------------------------------------------------------------
06/03/2010Page 439 of 623
Data File: xr108820.d
Date: 17-MAY-2010 05:43
Client ID: Instrument: PESTGC1.i
Sample Info: lcs 460-37420/2-a Operator: 462
06/03/2010Page 440 of 623
FORM IForm 1PESTICIDES ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: 460-13147-A-2-B MS
Matrix: xf108822.dLab File ID:
Date Collected:8081AAnalysis Method:
Solid
TestAmerica Edison
05/12/2010 15:30
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 09:15
05/17/2010 06:36
N
10(mL)
1(uL)
Sample wt/vol: 15.01(g)
% Moisture: 13.0
GC Column: ID: 0.53(mm)CLP-2
Analysis Batch No.: 37575 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Aldrin309-00-2 151 7.7 1.7
alpha-BHC319-84-6 154 7.7 1.4
beta-BHC319-85-7 153 7.7 1.0
delta-BHC319-86-8 167 7.7 1.2
gamma-BHC (Lindane)58-89-9 155 7.7 0.90
Chlordane57-74-9 77 77 17U
4,4'-DDD72-54-8 159 7.7 0.92
4,4'-DDE72-55-9 169 7.7 1.5
4,4'-DDT50-29-3 162 7.7 0.96
Dieldrin60-57-1 150 7.7 1.5
Endosulfan I959-98-8 144 7.7 1.6
Endosulfan II33213-65-9 152 7.7 1.2
Endosulfan sulfate1031-07-8 147 7.7 0.99
Endrin72-20-8 168 7.7 1.1
Endrin aldehyde7421-93-4 145 7.7 1.9
Heptachlor76-44-8 139 7.7 1.1
Heptachlor epoxide1024-57-3 149 7.7 1.6
Toxaphene8001-35-2 77 77 16U
SURROGATE %RECCAS NO. LIMITS Q
877-09-8 Tetrachloro-m-xylene 107 22-141
2051-24-3 DCB Decachlorobiphenyl 132 10-165
FORM I 8081A
06/03/2010Page 441 of 623
FORM IForm 1PESTICIDES ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: 460-13147-A-2-B MS
Matrix: xr108822.dLab File ID:
Date Collected:8081AAnalysis Method:
Solid
TestAmerica Edison
05/12/2010 15:30
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 09:15
05/17/2010 06:36
N
10(mL)
1(uL)
Sample wt/vol: 15.01(g)
% Moisture: 13.0
GC Column: ID: 0.53(mm)CLP-1
Analysis Batch No.: 37575 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Aldrin309-00-2 127 7.7 1.7
alpha-BHC319-84-6 129 7.7 1.4
beta-BHC319-85-7 128 7.7 1.0
delta-BHC319-86-8 142 7.7 1.2
gamma-BHC (Lindane)58-89-9 130 7.7 0.90
Chlordane57-74-9 77 77 17U
4,4'-DDD72-54-8 134 7.7 0.92
4,4'-DDE72-55-9 135 7.7 1.5
4,4'-DDT50-29-3 131 7.7 0.96
Dieldrin60-57-1 128 7.7 1.5
Endosulfan I959-98-8 135 7.7 1.6
Endosulfan II33213-65-9 123 7.7 1.2
Endosulfan sulfate1031-07-8 118 7.7 0.99
Endrin72-20-8 148 7.7 1.1
Endrin aldehyde7421-93-4 116 7.7 1.9
Heptachlor76-44-8 137 7.7 1.1
Heptachlor epoxide1024-57-3 132 7.7 1.6
Toxaphene8001-35-2 77 77 16U
SURROGATE %RECCAS NO. LIMITS Q
877-09-8 Tetrachloro-m-xylene 94 22-141
2051-24-3 DCB Decachlorobiphenyl 123 10-165
FORM I 8081A
06/03/2010Page 442 of 623
FORM IForm 1PESTICIDES ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: 460-13147-A-2-C MSD
Matrix: xf108823.dLab File ID:
Date Collected:8081AAnalysis Method:
Solid
TestAmerica Edison
05/12/2010 15:30
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 09:15
05/17/2010 06:50
N
10(mL)
1(uL)
Sample wt/vol: 15.00(g)
% Moisture: 13.0
GC Column: ID: 0.53(mm)CLP-2
Analysis Batch No.: 37575 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Aldrin309-00-2 145 7.7 1.7
alpha-BHC319-84-6 145 7.7 1.4
beta-BHC319-85-7 144 7.7 1.0
delta-BHC319-86-8 159 7.7 1.2
gamma-BHC (Lindane)58-89-9 147 7.7 0.90
Chlordane57-74-9 77 77 17U
4,4'-DDD72-54-8 156 7.7 0.92
4,4'-DDE72-55-9 161 7.7 1.5
4,4'-DDT50-29-3 150 7.7 0.97
Dieldrin60-57-1 140 7.7 1.5
Endosulfan I959-98-8 137 7.7 1.6
Endosulfan II33213-65-9 145 7.7 1.2
Endosulfan sulfate1031-07-8 147 7.7 0.99
Endrin72-20-8 163 7.7 1.1
Endrin aldehyde7421-93-4 137 7.7 1.9
Heptachlor76-44-8 125 7.7 1.1
Heptachlor epoxide1024-57-3 140 7.7 1.6
Toxaphene8001-35-2 77 77 16U
SURROGATE %RECCAS NO. LIMITS Q
877-09-8 Tetrachloro-m-xylene 101 22-141
2051-24-3 DCB Decachlorobiphenyl 147 10-165
FORM I 8081A
06/03/2010Page 443 of 623
FORM IForm 1PESTICIDES ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: 460-13147-A-2-C MSD
Matrix: xr108823.dLab File ID:
Date Collected:8081AAnalysis Method:
Solid
TestAmerica Edison
05/12/2010 15:30
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 09:15
05/17/2010 06:50
N
10(mL)
1(uL)
Sample wt/vol: 15.00(g)
% Moisture: 13.0
GC Column: ID: 0.53(mm)CLP-1
Analysis Batch No.: 37575 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Aldrin309-00-2 122 7.7 1.7
alpha-BHC319-84-6 122 7.7 1.4
beta-BHC319-85-7 125 7.7 1.0
delta-BHC319-86-8 134 7.7 1.2
gamma-BHC (Lindane)58-89-9 121 7.7 0.90
Chlordane57-74-9 77 77 17U
4,4'-DDD72-54-8 118 7.7 0.92
4,4'-DDE72-55-9 122 7.7 1.5
4,4'-DDT50-29-3 118 7.7 0.97
Dieldrin60-57-1 120 7.7 1.5
Endosulfan I959-98-8 126 7.7 1.6
Endosulfan II33213-65-9 113 7.7 1.2
Endosulfan sulfate1031-07-8 109 7.7 0.99
Endrin72-20-8 133 7.7 1.1
Endrin aldehyde7421-93-4 95.9 7.7 1.9
Heptachlor76-44-8 122 7.7 1.1
Heptachlor epoxide1024-57-3 122 7.7 1.6
Toxaphene8001-35-2 77 77 16U
SURROGATE %RECCAS NO. LIMITS Q
877-09-8 Tetrachloro-m-xylene 91 22-141
2051-24-3 DCB Decachlorobiphenyl p56 10-165
FORM I 8081A
06/03/2010Page 444 of 623
Lab Name: Job No.:
SDG No.:
Instrument ID:
Analysis Batch Number:
PESTICIDES ANALYSIS RUN LOG
DILUTION
FACTOR
COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID
TestAmerica Edison 460-13139-1
PESTGC1
37146
Start Date:
End Date: 05/11/2010 14:23
05/11/2010 11:47
RINSE 460-37146/1 CLP-2 0.53(mm)105/11/2010 11:47
RINSE 460-37146/1 CLP-1 0.53(mm)105/11/2010 11:47
PIBLK 460-37146/2 CLP-2 0.53(mm)105/11/2010 12:04
PIBLK 460-37146/2 CLP-1 0.53(mm)105/11/2010 12:04
RESC 460-37146/3 CLP-2 0.53(mm)105/11/2010 12:18
RESC 460-37146/3 CLP-1 0.53(mm)105/11/2010 12:18
PEM 460-37146/4 CLP-2 0.53(mm)105/11/2010 12:32
PEM 460-37146/4 CLP-1 0.53(mm)105/11/2010 12:32
IC 460-37146/5 CLP-2 0.53(mm)105/11/2010 12:47 xf108635.d
IC 460-37146/5 CLP-1 0.53(mm)105/11/2010 12:47 xr108635.d
IC 460-37146/6 CLP-2 0.53(mm)105/11/2010 13:00 xf108636.d
IC 460-37146/6 CLP-1 0.53(mm)105/11/2010 13:00 xr108636.d
IC 460-37146/7 CLP-2 0.53(mm)105/11/2010 13:14 xf108637.d
IC 460-37146/7 CLP-1 0.53(mm)105/11/2010 13:14 xr108637.d
IC 460-37146/8 CLP-2 0.53(mm)105/11/2010 13:28 xf108638.d
IC 460-37146/8 CLP-1 0.53(mm)105/11/2010 13:28 xr108638.d
IC 460-37146/9 CLP-2 0.53(mm)105/11/2010 13:42 xf108639.d
IC 460-37146/9 CLP-1 0.53(mm)105/11/2010 13:42 xr108639.d
IC 460-37146/10 CLP-2 0.53(mm)105/11/2010 13:56 xf108640.d
IC 460-37146/10 CLP-1 0.53(mm)105/11/2010 13:56 xr108640.d
IC 460-37146/11 CLP-2 0.53(mm)105/11/2010 14:10 xf108641.d
IC 460-37146/11 CLP-1 0.53(mm)105/11/2010 14:10 xr108641.d
ICV 460-37146/12 CLP-2 0.53(mm)105/11/2010 14:23
ICV 460-37146/12 CLP-1 0.53(mm)105/11/2010 14:23
8081A
06/03/2010Page 445 of 623
Lab Name: Job No.:
SDG No.:
Instrument ID:
Analysis Batch Number:
PESTICIDES ANALYSIS RUN LOG
DILUTION
FACTOR
COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID
TestAmerica Edison 460-13139-1
PESTGC1
37575
Start Date:
End Date: 05/17/2010 10:04
05/17/2010 04:31
RINSE 460-37575/1 CLP-2 0.53(mm)105/17/2010 04:31
RINSE 460-37575/1 CLP-1 0.53(mm)105/17/2010 04:31
PIBLK 460-37575/2 CLP-2 0.53(mm)105/17/2010 04:45
PIBLK 460-37575/2 CLP-1 0.53(mm)105/17/2010 04:45
ZZZZZ CLP-2 0.53(mm)105/17/2010 04:59
ZZZZZ CLP-1 0.53(mm)105/17/2010 04:59
PEM 460-37575/4 CLP-2 0.53(mm)105/17/2010 05:13 xf108818.d
PEM 460-37575/4 CLP-1 0.53(mm)105/17/2010 05:13 xr108818.d
CCVRT 460-37575/5 CLP-2 0.53(mm)105/17/2010 05:29 xf108819.d
CCVRT 460-37575/5 CLP-1 0.53(mm)105/17/2010 05:29 xr108819.d
LCS 460-37420/2-A CLP-2 0.53(mm)105/17/2010 05:43 xf108820.d
LCS 460-37420/2-A CLP-1 0.53(mm)105/17/2010 05:43 xr108820.d
ZZZZZ CLP-2 0.53(mm)105/17/2010 06:23
ZZZZZ CLP-1 0.53(mm)105/17/2010 06:23
460-13147-A-2-B MS CLP-2 0.53(mm)105/17/2010 06:36 xf108822.d
460-13147-A-2-B MS CLP-1 0.53(mm)105/17/2010 06:36 xr108822.d
460-13147-A-2-C MSD CLP-2 0.53(mm)105/17/2010 06:50 xf108823.d
460-13147-A-2-C MSD CLP-1 0.53(mm)105/17/2010 06:50 xr108823.d
ZZZZZ CLP-2 0.53(mm)105/17/2010 07:04
ZZZZZ CLP-1 0.53(mm)105/17/2010 07:04
ZZZZZ CLP-2 0.53(mm)105/17/2010 07:18
ZZZZZ CLP-1 0.53(mm)105/17/2010 07:18
ZZZZZ CLP-2 0.53(mm)105/17/2010 07:32
ZZZZZ CLP-1 0.53(mm)105/17/2010 07:32
ZZZZZ CLP-2 0.53(mm)105/17/2010 07:46
ZZZZZ CLP-1 0.53(mm)105/17/2010 07:46
460-13139-2 TB-3 6-7 CLP-2 0.53(mm)105/17/2010 08:00 xf108828.d
460-13139-2 TB-3 6-7 CLP-1 0.53(mm)105/17/2010 08:00 xr108828.d
ZZZZZ CLP-2 0.53(mm)105/17/2010 08:13
ZZZZZ CLP-1 0.53(mm)105/17/2010 08:13
460-13139-4 TB-2 5-6 CLP-2 0.53(mm)105/17/2010 08:27 xf108830.d
460-13139-4 TB-2 5-6 CLP-1 0.53(mm)105/17/2010 08:27 xr108830.d
460-13139-5 TB-1 2-3 CLP-2 0.53(mm)105/17/2010 08:41 xf108831.d
460-13139-5 TB-1 2-3 CLP-1 0.53(mm)105/17/2010 08:41 xr108831.d
ZZZZZ CLP-2 0.53(mm)105/17/2010 08:55
ZZZZZ CLP-1 0.53(mm)105/17/2010 08:55
460-13139-7 TB-5 3-4 CLP-2 0.53(mm)105/17/2010 09:09 xf108833.d
460-13139-7 TB-5 3-4 CLP-1 0.53(mm)105/17/2010 09:09 xr108833.d
ZZZZZ CLP-2 0.53(mm)105/17/2010 09:23
ZZZZZ CLP-1 0.53(mm)105/17/2010 09:23
MB 460-37420/1-A CLP-2 0.53(mm)105/17/2010 09:37 xf108835.d
MB 460-37420/1-A CLP-1 0.53(mm)105/17/2010 09:37 xr108835.d
PIBLK 460-37575/22 CLP-2 0.53(mm)105/17/2010 09:51
PIBLK 460-37575/22 CLP-1 0.53(mm)105/17/2010 09:51
CCV 460-37575/23 CLP-2 0.53(mm)105/17/2010 10:04 xf108837.d
8081A
06/03/2010Page 446 of 623
Lab Name: Job No.:
SDG No.:
Instrument ID:
Analysis Batch Number:
PESTICIDES ANALYSIS RUN LOG
DILUTION
FACTOR
COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID
TestAmerica Edison 460-13139-1
PESTGC1
37575
Start Date:
End Date: 05/17/2010 10:04
05/17/2010 04:31
CCV 460-37575/23 CLP-1 0.53(mm)105/17/2010 10:04 xr108837.d
8081A
06/03/2010Page 447 of 623
Organic Prep Worksheet
Method: 3541
Analyst: Patel, Harsh
Batch Number: 460-37420 Date Open:
Batch End:
May 14 2010 9:15AM
May 14 2010 3:00PM
Lab ID Client ID Basis Final weight/volume of
sample
Position on the
SoxTherm
OP_PESTSP_00004 OPPSTPCBSU_00014Initial weight/volume of
sample
Method Chain
MB~460-37420/1 15.00 g 10 mL 50 uL1213541, 8081A
LCS~460-37420/2 15.00 g 10 mL 50 uL100 uL1223541, 8081A
460-13147-A-2~MS T 15.01 g 10 mL 50 uL100 uL1233541, 8081A
460-13147-A-2~MS
D
T 15.00 g 10 mL 50 uL100 uL1243541, 8081A
460-13139-E-1 TB-3 2-3 T 15.02 g 10 mL 50 uL125
460-13139-E-2 TB-3 6-7 T 15.00 g 10 mL 50 uL1263541, 8081A
460-13139-E-3 TB-2 2-3 T 15.00 g 10 mL 50 uL67
460-13139-E-4 TB-2 5-6 T 15.01 g 10 mL 50 uL683541, 8081A
460-13139-E-5 TB-1 2-3 T 15.00 g 10 mL 50 uL693541, 8081A
460-13139-E-6 TB-1 5-6 T 15.00 g 10 mL 50 uL70
460-13139-E-7 TB-5 3-4 T 15.00 g 10 mL 50 uL713541, 8081A
460-13139-E-8 TB-4 6-7 T 15.01 g 10 mL 50 uL72
460-13146-G-1 T 15.00 g 10 mL 50 uL1
460-13147-B-1 T 15.00 g 10 mL 50 uL2
460-13147-A-2 T 15.02 g 10 mL 50 uL3
460-13148-B-1 T 15.00 g 10 mL 50 uL4
First Start time: 8.30am
Person's name who did the prep: hp
Person's name who witnessed reagent drop: JR
First End time: 3.00pm
Balance ID: 28
Person's name who did the concentration: hp
Na2SO4 Lot Number: H52600
Solvent: Acetone/Hexane mix
Vendor lot number: H35E05
Florisil Lot #: H38553
06/03/2010Page 448 of 623
Organic Prep Worksheet
Method: 3541
Analyst: Patel, Harsh
Batch Number: 460-37420 Date Open:
Batch End:
May 14 2010 9:15AM
May 14 2010 3:00PM
Lab ID Client ID Basis
Comments
Analysis commentMethod Chain
MB~460-37420/1 3541, 8081A
LCS~460-37420/2 3541, 8081A
460-13147-A-2~MS T3541, 8081A
460-13147-A-2~MS
D
T3541, 8081A
460-13139-E-1 TB-3 2-3 T
460-13139-E-2 TB-3 6-7 T3541, 8081A
460-13139-E-3 TB-2 2-3 T
460-13139-E-4 TB-2 5-6 T3541, 8081A
460-13139-E-5 TB-1 2-3 T3541, 8081A
460-13139-E-6 TB-1 5-6 T
460-13139-E-7 TB-5 3-4 T3541, 8081A
460-13139-E-8 TB-4 6-7 T
460-13146-G-1 T
460-13147-B-1 T
460-13147-A-2 T
460-13148-B-1 T
Batch Comment: PEST soil
06/03/2010Page 449 of 623
Method 8082Polychlorinated Biphenyls (PCBs) by
Gas Chromatography by Method 8082
06/03/2010Page 450 of 623
FORM II
GC SEMI VOA SURROGATE RECOVERY
Lab Name: Job No.: 460-13139-1
SDG No.:
Matrix: Solid Level: Low
TestAmerica Edison
GC Column (1): ID: (mm) GC Column (2): ID: (mm)CLP-2 0.53 CLP-1 0.53
#Lab Sample IDClient Sample ID #DCB1 DCB2
460-13139-2TB-3 6-7 106 108
460-13139-4TB-2 5-6 110 97
460-13139-5TB-1 2-3 109 113
460-13139-7TB-5 3-4 65 55
MB 460-37391/1-A 98 94
LCS 460-37391/2-A
104 110
460-13137-A-1-B MS
108 106
460-13137-A-1-C MSD
91 91
QC LIMITSQC LIMITSDCB = DCB Decachlorobiphenyl 27-165
FORM II 8082
# Column to be used to flag recovery values
06/03/2010Page 451 of 623
GC SEMI VOA LAB CONTROL SAMPLE RECOVERY
FORM III
Job No.:Lab Name:
SDG No.:
Level:Matrix:Matrix:
Low
460-13139-1
Lab File ID: of077396.dSolid
Lab ID: LCS 460-37391/2-A Client ID:
TestAmerica Edison
REC
%
REC
QC
LIMITSCONCENTRATION
(ug/Kg)
SPIKE
ADDED
(ug/Kg)
#
LCS LCS
COMPOUND
Aroclor 1016 333 316 62-14895
Aroclor 1260 333 328 58-14598
FORM III 8082
# Column to be used to flag recovery and RPD values
06/03/2010Page 452 of 623
GC SEMI VOA LAB CONTROL SAMPLE RECOVERY
FORM III
Job No.:Lab Name:
SDG No.:
Level:Matrix:Matrix:
Low
460-13139-1
Lab File ID: or077396.dSolid
Lab ID: LCS 460-37391/2-A Client ID:
TestAmerica Edison
REC
%
REC
QC
LIMITSCONCENTRATION
(ug/Kg)
SPIKE
ADDED
(ug/Kg)
#
LCS LCS
COMPOUND
Aroclor 1016 333 278 62-14883
Aroclor 1260 333 314 58-14594
FORM III 8082
# Column to be used to flag recovery and RPD values
06/03/2010Page 453 of 623
GC SEMI VOA MATRIX SPIKE RECOVERY
FORM III
Job No.:Lab Name:
SDG No.:
Level:Matrix:Matrix:
Low
460-13139-1
Lab File ID: of077398.dSolid
Lab ID: 460-13137-A-1-B MS Client ID:
TestAmerica Edison
LIMITS
COMPOUND
CONCENTRATION %
REC
QC
REC
SAMPLE
CONCENTRATION
SPIKE
ADDED
(ug/Kg) (ug/Kg) (ug/Kg)
#
MS MS
343 357 62-148Aroclor 1016 10469 U
343 362 58-145Aroclor 1260 10669 U
FORM III 8082
# Column to be used to flag recovery and RPD values
06/03/2010Page 454 of 623
GC SEMI VOA MATRIX SPIKE RECOVERY
FORM III
Job No.:Lab Name:
SDG No.:
Level:Matrix:Matrix:
Low
460-13139-1
Lab File ID: or077398.dSolid
Lab ID: 460-13137-A-1-B MS Client ID:
TestAmerica Edison
LIMITS
COMPOUND
CONCENTRATION %
REC
QC
REC
SAMPLE
CONCENTRATION
SPIKE
ADDED
(ug/Kg) (ug/Kg) (ug/Kg)
#
MS MS
343 321 62-148Aroclor 1016 9469 U
343 331 58-145Aroclor 1260 9669 U
FORM III 8082
# Column to be used to flag recovery and RPD values
06/03/2010Page 455 of 623
GC SEMI VOA MATRIX SPIKE DUPLICATE RECOVERY
FORM III
Job No.:Lab Name:
SDG No.:
Level:Matrix:Matrix:
Low
460-13139-1
Lab File ID: of077399.dSolid
Lab ID: 460-13137-A-1-C MSD Client ID:
TestAmerica Edison
COMPOUND
SPIKE
ADDED CONCENTRATION %
REC
%
RPD
QC LIMITS
RPD REC (ug/Kg) (ug/Kg)
#
MSD MSD
343 364 30 62-148Aroclor 1016 2106
343 376 30 58-145Aroclor 1260 4110
FORM III 8082
# Column to be used to flag recovery and RPD values
06/03/2010Page 456 of 623
GC SEMI VOA MATRIX SPIKE DUPLICATE RECOVERY
FORM III
Job No.:Lab Name:
SDG No.:
Level:Matrix:Matrix:
Low
460-13139-1
Lab File ID: or077399.dSolid
Lab ID: 460-13137-A-1-C MSD Client ID:
TestAmerica Edison
COMPOUND
SPIKE
ADDED CONCENTRATION %
REC
%
RPD
QC LIMITS
RPD REC (ug/Kg) (ug/Kg)
#
MSD MSD
343 335 30 62-148Aroclor 1016 498
343 343 30 58-145Aroclor 1260 4100
FORM III 8082
# Column to be used to flag recovery and RPD values
06/03/2010Page 457 of 623
FORM IV
GC SEMI VOA METHOD BLANK SUMMARY
Lab Name:
SDG No.:
Job No.: 460-13139-1TestAmerica Edison
Date Analyzed:(1)
Instrument ID:(1)
GC Column:(1) ID:
Instrument ID:(2)
Date Extracted: 05/14/2010 07:19
Date Analyzed:(2)
GC Column:(2) ID:CLP-10.53(mm) 0.53(mm)
PESTGC7
05/14/2010 18:20
Lab File ID:(1) Lab File ID:(2)
Matrix: Solid
or077395.d
Lab Sample ID: MB 460-37391/1-A
of077395.d
05/14/2010 18:20
PESTGC7
CLP-2
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:
ANALYZED 2
DATEDATE
ANALYZED 1LAB SAMPLE IDCLIENT SAMPLE ID
LCS 460-37391/2-A 05/14/2010 18:37 05/14/2010 18:37
460-13137-A-1-B MS 05/14/2010 19:09 05/14/2010 19:09
460-13137-A-1-C MSD 05/14/2010 19:26 05/14/2010 19:26
460-13139-2TB-3 6-7 05/14/2010 19:59 05/14/2010 19:59
460-13139-4TB-2 5-6 05/14/2010 20:32 05/14/2010 20:32
460-13139-5TB-1 2-3 05/14/2010 20:48 05/14/2010 20:48
460-13139-7TB-5 3-4 05/14/2010 21:21 05/14/2010 21:21
FORM IV 8082
06/03/2010Page 458 of 623
PCBS ANALYTICAL SEQUENCE
Lab Name: Job No.:
SDG No.:
FORM VIII
TestAmerica Edison 460-13139-1
Calibration ID:
Calibration Start Date:Instrument ID: PESTGC7
GC Column:
6034
Calibration End Date:
05/04/2010 16:54
05/04/2010 17:58CLP-2 ID: 0.53(mm)
THE ANALYTICAL SEQUENCE OF BLANKS, SAMPLES, STANDARDS, MS/MSDs AND LCSs IS GIVEN BELOW:
# #RT RT
TCX DCB
UPPER LIMIT
LOWER LIMIT
2.14
2.04
10.31
10.11
SURROGATE RT FROM CONTINUING CALIBRATION 2.09 10.21
LAB SAMPLE ID DATE ANALYZEDCLIENT SAMPLE ID LAB FILE ID
CCVRT 460-37531/3 05/14/2010 17:55 2.09 10.21of077394.d
MB 460-37391/1-A 05/14/2010 18:20 10.21of077395.d
LCS 460-37391/2-A 05/14/2010 18:37 10.21of077396.d
460-13137-A-1-B MS 05/14/2010 19:09 10.21of077398.d
460-13137-A-1-C MSD 05/14/2010 19:26 10.21of077399.d
460-13139-2 05/14/2010 19:59 10.21TB-3 6-7 of077401.d
460-13139-4 05/14/2010 20:32 10.21TB-2 5-6 of077403.d
460-13139-5 05/14/2010 20:48 10.21TB-1 2-3 of077404.d
460-13139-7 05/14/2010 21:21 10.21TB-5 3-4 of077406.d
CCV 460-37531/25 05/15/2010 00:03 2.08 10.20of077416.d
TCX = Tetrachloro-m-xylene
DCB = DCB Decachlorobiphenyl
TCX RT Limit = ± 0.05 minutes of surrogate RTDCB RT Limit = ± 0.10 minutes of surrogate RT
# Column used to flag values outside QC limits
FORM VIII 8082
06/03/2010Page 459 of 623
PCBS ANALYTICAL SEQUENCE
Lab Name: Job No.:
SDG No.:
FORM VIII
TestAmerica Edison 460-13139-1
Calibration ID:
Calibration Start Date:Instrument ID: PESTGC7
GC Column:
6042
Calibration End Date:
05/04/2010 16:54
05/04/2010 17:58CLP-1 ID: 0.53(mm)
THE ANALYTICAL SEQUENCE OF BLANKS, SAMPLES, STANDARDS, MS/MSDs AND LCSs IS GIVEN BELOW:
# #RT RT
TCX DCB
UPPER LIMIT
LOWER LIMIT
2.03
1.93
9.38
9.18
SURROGATE RT FROM CONTINUING CALIBRATION 1.98 9.28
LAB SAMPLE ID DATE ANALYZEDCLIENT SAMPLE ID LAB FILE ID
CCVRT 460-37531/3 05/14/2010 17:55 1.98 9.28or077394.d
MB 460-37391/1-A 05/14/2010 18:20 9.28or077395.d
LCS 460-37391/2-A 05/14/2010 18:37 9.28or077396.d
460-13137-A-1-B MS 05/14/2010 19:09 9.28or077398.d
460-13137-A-1-C MSD 05/14/2010 19:26 9.28or077399.d
460-13139-2 05/14/2010 19:59 9.28TB-3 6-7 or077401.d
460-13139-4 05/14/2010 20:32 9.28TB-2 5-6 or077403.d
460-13139-5 05/14/2010 20:48 9.28TB-1 2-3 or077404.d
460-13139-7 05/14/2010 21:21 9.28TB-5 3-4 or077406.d
CCV 460-37531/25 05/15/2010 00:03 1.98 9.28or077416.d
TCX = Tetrachloro-m-xylene
DCB = DCB Decachlorobiphenyl
TCX RT Limit = ± 0.05 minutes of surrogate RTDCB RT Limit = ± 0.10 minutes of surrogate RT
# Column used to flag values outside QC limits
FORM VIII 8082
06/03/2010Page 460 of 623
FORM XForm 1
Client Sample ID:
Lab Name: Job No.:
SDG No.:
Lab Sample ID: LCS 460-37391/2-A
Instrument ID (1): Instrument ID (2):
Date Analyzed (1): Date Analyzed (2):
GC Column (1): ID: GC Column (2): ID:
TestAmerica Edison 460-13139-1
IDENTIFICATION SUMMARYForm 1
0.53(mm) 0.53(mm)
05/14/2010 18:37 05/14/2010 18:37
PESTGC7 PESTGC7
CLP-2 CLP-1
ANALYTE COL PEAK RTRT WINDOW
FROM TO PEAK MEANRPD
CONCENTRATION
Aroclor 1016 1 1 2.57 2.49 2.63 285 316 12.7
2 3.01 2.92 3.06 309
3 3.27 3.19 3.33 331
4 3.52 3.44 3.58 306
5 3.68 3.60 3.74 316
6 3.97 3.89 4.03 329
7 4.24 4.16 4.30 308
8 4.39 4.31 4.45 344
2 1 2.28 2.19 2.33 258 278
2 2.59 2.51 2.65 279
3 2.78 2.70 2.84 278
4 3.04 2.97 3.11 287
5 3.19 3.11 3.25 285
6 3.25 3.17 3.31 272
7 3.62 3.54 3.68 291
8 3.71 3.64 3.78 274
Aroclor 1260 1 1 5.84 5.76 5.90 330 328 4.4
2 6.13 6.05 6.19 331
3 6.65 6.58 6.72 319
4 6.82 6.74 6.88 329
5 6.91 6.83 6.97 343
6 7.35 7.28 7.42 330
7 8.77 8.69 8.83 317
8 9.63 9.56 9.70 328
2 1 5.02 4.95 5.09 310 314
2 5.37 5.29 5.43 307
3 5.71 5.64 5.78 303
4 5.85 5.78 5.92 313
5 6.17 6.09 6.23 302
6 7.09 7.02 7.16 290
7 7.24 7.17 7.31 352
8 8.43 8.35 8.49 334
FORM X 8082
06/03/2010Page 461 of 623
FORM XForm 1
Client Sample ID:
Lab Name: Job No.:
SDG No.:
Lab Sample ID: 460-13137-A-1-B MS
Instrument ID (1): Instrument ID (2):
Date Analyzed (1): Date Analyzed (2):
GC Column (1): ID: GC Column (2): ID:
TestAmerica Edison 460-13139-1
IDENTIFICATION SUMMARYForm 1
0.53(mm) 0.53(mm)
05/14/2010 19:09 05/14/2010 19:09
PESTGC7 PESTGC7
CLP-2 CLP-1
ANALYTE COL PEAK RTRT WINDOW
FROM TO PEAK MEANRPD
CONCENTRATION
Aroclor 1016 1 1 2.57 2.49 2.63 352 357 10.7
2 3.00 2.92 3.06 350
3 3.26 3.19 3.33 354
4 3.51 3.44 3.58 347
5 3.67 3.60 3.74 355
6 3.96 3.89 4.03 389
7 4.23 4.16 4.30 330
8 4.39 4.31 4.45 380
2 1 2.27 2.19 2.33 300 321
2 2.59 2.51 2.65 323
3 2.78 2.70 2.84 318
4 3.04 2.97 3.11 329
5 3.19 3.11 3.25 326
6 3.25 3.17 3.31 309
7 3.62 3.54 3.68 324
8 3.71 3.64 3.78 339
Aroclor 1260 1 1 5.83 5.76 5.90 361 362 9.1
2 6.12 6.05 6.19 363
3 6.65 6.58 6.72 354
4 6.81 6.74 6.88 361
5 6.90 6.83 6.97 365
6 7.35 7.28 7.42 362
7 8.76 8.69 8.83 364
8 9.63 9.56 9.70 365
2 1 5.02 4.95 5.09 336 331
2 5.37 5.29 5.43 336
3 5.71 5.64 5.78 333
4 5.85 5.78 5.92 336
5 6.17 6.09 6.23 325
6 7.09 7.02 7.16 306
7 7.24 7.17 7.31 331
8 8.42 8.35 8.49 340
FORM X 8082
06/03/2010Page 462 of 623
FORM XForm 1
Client Sample ID:
Lab Name: Job No.:
SDG No.:
Lab Sample ID: 460-13137-A-1-C MSD
Instrument ID (1): Instrument ID (2):
Date Analyzed (1): Date Analyzed (2):
GC Column (1): ID: GC Column (2): ID:
TestAmerica Edison 460-13139-1
IDENTIFICATION SUMMARYForm 1
0.53(mm) 0.53(mm)
05/14/2010 19:26 05/14/2010 19:26
PESTGC7 PESTGC7
CLP-2 CLP-1
ANALYTE COL PEAK RTRT WINDOW
FROM TO PEAK MEANRPD
CONCENTRATION
Aroclor 1016 1 1 2.57 2.49 2.63 349 364 8.1
2 3.00 2.92 3.06 352
3 3.27 3.19 3.33 369
4 3.52 3.44 3.58 361
5 3.68 3.60 3.74 370
6 3.96 3.89 4.03 365
7 4.24 4.16 4.30 349
8 4.39 4.31 4.45 394
2 1 2.28 2.19 2.33 297 335
2 2.59 2.51 2.65 326
3 2.78 2.70 2.84 327
4 3.04 2.97 3.11 345
5 3.19 3.11 3.25 342
6 3.25 3.17 3.31 332
7 3.62 3.54 3.68 343
8 3.71 3.64 3.78 371
Aroclor 1260 1 1 5.84 5.76 5.90 375 376 9.2
2 6.12 6.05 6.19 377
3 6.65 6.58 6.72 373
4 6.81 6.74 6.88 379
5 6.91 6.83 6.97 388
6 7.35 7.28 7.42 383
7 8.76 8.69 8.83 378
8 9.63 9.56 9.70 360
2 1 5.02 4.95 5.09 353 343
2 5.37 5.29 5.43 353
3 5.71 5.64 5.78 351
4 5.85 5.78 5.92 357
5 6.17 6.09 6.23 347
6 7.09 7.02 7.16 324
7 7.24 7.17 7.31 326
8 8.42 8.35 8.49 335
FORM X 8082
06/03/2010Page 463 of 623
FORM IForm 1PCBS ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-3 6-7
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-2
Matrix: of077401.dLab File ID:
Date Collected:8082Analysis Method:
Soil
TestAmerica Edison
05/12/2010 09:45
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 07:19
05/14/2010 19:59
N
10(mL)
Sample wt/vol: 15.00(g)
% Moisture: 18.8
GC Column: ID: 0.53(mm)CLP-2
Analysis Batch No.: 37531 ug/KgUnits:
SURROGATE %RECCAS NO. LIMITS Q
2051-24-3 DCB Decachlorobiphenyl 106 27-165
FORM I 8082
06/03/2010Page 464 of 623
Data File: of077401.d Report Date: 16-May-2010 18:33
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC7.i/8082/front/May10/05-14-10/14may10a.b/of077401.dLab Smp Id: 460-13139-E-2-A Client Smp ID: TB-3 6-7Inj Date : 14-MAY-2010 19:59 Operator : 615 Inst ID: PESTGC7.iSmp Info : 460-13139-E-2-AMisc Info : 460-13139-E-2-AComment : Method : /chem1/PESTGC7.i/8082/front/May10/05-14-10/14may10a.b/08Of8082.mMeth Date : 05-May-2010 00:12 diazc Quant Type: ESTDCal Date : 04-MAY-2010 19:52 Cal File: of077121.dAls bottle: 10 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: AllPCB.subTarget Version: 3.50 Sample Matrix: SOLIDProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (mL)Ws 15.00000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 30 Decachlorobiphenyl(surr) CAS #: 2051-24-3
10.205 10.205 0.000 184874 53.1503 35 80.00- 120.00 100.00
-------------------------------------------------------------------------------
06/03/2010Page 465 of 623
Data File: of077401.d
Date: 14-MAY-2010 19:59
Client ID: TB-3 6-7 Instrument: PESTGC7.i
Sample Info: 460-13139-E-2-A Operator: 615
06/03/2010Page 466 of 623
FORM IForm 1PCBS ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-3 6-7
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-2
Matrix: or077401.dLab File ID:
Date Collected:8082Analysis Method:
Soil
TestAmerica Edison
05/12/2010 09:45
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 07:19
05/14/2010 19:59
N
10(mL)
Sample wt/vol: 15.00(g)
% Moisture: 18.8
GC Column: ID: 0.53(mm)CLP-1
Analysis Batch No.: 37531 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Aroclor 101612674-11-2 83 83 16U
Aroclor 122111104-28-2 83 83 25U
Aroclor 123211141-16-5 83 83 47U
Aroclor 124253469-21-9 83 83 16U
Aroclor 124812672-29-6 83 83 22U
Aroclor 125411097-69-1 83 83 28U
Aroclor 126011096-82-5 83 83 9.2U
Aroclor 126237324-23-5 83 83 14U
Aroclor 126811100-14-4 83 83 14U
SURROGATE %RECCAS NO. LIMITS Q
2051-24-3 DCB Decachlorobiphenyl 108 27-165
FORM I 8082
06/03/2010Page 467 of 623
Data File: or077401.d Page 1 Report Date: 16-May-2010 18:33
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC7.i/8082/rear/May10/05-14-10/14may10a.b/or077401.dLab Smp Id: 460-13139-E-2-A Client Smp ID: TB-3 6-7Inj Date : 14-MAY-2010 19:59 Operator : 615 Inst ID: PESTGC7.iSmp Info : 460-13139-E-2-AMisc Info : 460-13139-E-2-AComment : Method : /chem1/PESTGC7.i/8082/rear/May10/05-14-10/14may10a.b/08Or8082.mMeth Date : 05-May-2010 00:19 diazc Quant Type: ESTDCal Date : 04-MAY-2010 19:52 Cal File: or077121.dAls bottle: 10 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: AllPCB.subTarget Version: 3.50 Sample Matrix: SOLIDProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (mL)Ws 15.00000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 30 Decachlorobiphenyl(surr) CAS #: 2051-24-3
9.277 9.278 -0.001 130822 54.1694 80.00- 120.00 100.00(aR)
-------------------------------------------------------------------------------
QC Flag Legend
a - Target compound detected but, quantitated amountBelow Limit Of Quantitation(BLOQ).
R - Spike/Surrogate failed recovery limits.
06/03/2010Page 468 of 623
Data File: or077401.d
Date: 14-MAY-2010 19:59
Client ID: TB-3 6-7 Instrument: PESTGC7.i
Sample Info: 460-13139-E-2-A Operator: 615
06/03/2010Page 469 of 623
FORM IForm 1PCBS ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-2 5-6
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-4
Matrix: of077403.dLab File ID:
Date Collected:8082Analysis Method:
Soil
TestAmerica Edison
05/12/2010 10:45
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 07:19
05/14/2010 20:32
N
10(mL)
Sample wt/vol: 15.03(g)
% Moisture: 12.8
GC Column: ID: 0.53(mm)CLP-2
Analysis Batch No.: 37531 ug/KgUnits:
SURROGATE %RECCAS NO. LIMITS Q
2051-24-3 DCB Decachlorobiphenyl 110 27-165
FORM I 8082
06/03/2010Page 470 of 623
Data File: of077403.d Report Date: 16-May-2010 18:33
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC7.i/8082/front/May10/05-14-10/14may10a.b/of077403.dLab Smp Id: 460-13139-E-4-A Client Smp ID: TB-2 5-6Inj Date : 14-MAY-2010 20:32 Operator : 615 Inst ID: PESTGC7.iSmp Info : 460-13139-E-4-AMisc Info : 460-13139-E-4-AComment : Method : /chem1/PESTGC7.i/8082/front/May10/05-14-10/14may10a.b/08Of8082.mMeth Date : 05-May-2010 00:12 diazc Quant Type: ESTDCal Date : 04-MAY-2010 19:52 Cal File: of077121.dAls bottle: 12 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: AllPCB.subTarget Version: 3.50 Sample Matrix: SOLIDProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (mL)Ws 15.03000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 30 Decachlorobiphenyl(surr) CAS #: 2051-24-3
10.205 10.205 0.000 190649 54.8106 36 80.00- 120.00 100.00
-------------------------------------------------------------------------------
06/03/2010Page 471 of 623
Data File: of077403.d
Date: 14-MAY-2010 20:32
Client ID: TB-2 5-6 Instrument: PESTGC7.i
Sample Info: 460-13139-E-4-A Operator: 615
06/03/2010Page 472 of 623
FORM IForm 1PCBS ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-2 5-6
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-4
Matrix: or077403.dLab File ID:
Date Collected:8082Analysis Method:
Soil
TestAmerica Edison
05/12/2010 10:45
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 07:19
05/14/2010 20:32
N
10(mL)
Sample wt/vol: 15.03(g)
% Moisture: 12.8
GC Column: ID: 0.53(mm)CLP-1
Analysis Batch No.: 37531 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Aroclor 101612674-11-2 77 77 15U
Aroclor 122111104-28-2 77 77 23U
Aroclor 123211141-16-5 77 77 43U
Aroclor 124253469-21-9 77 77 15U
Aroclor 124812672-29-6 77 77 20U
Aroclor 125411097-69-1 77 77 26U
Aroclor 126011096-82-5 77 77 8.6U
Aroclor 126237324-23-5 77 77 13U
Aroclor 126811100-14-4 77 77 13U
SURROGATE %RECCAS NO. LIMITS Q
2051-24-3 DCB Decachlorobiphenyl 97 27-165
FORM I 8082
06/03/2010Page 473 of 623
Data File: or077403.d Page 1 Report Date: 16-May-2010 18:33
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC7.i/8082/rear/May10/05-14-10/14may10a.b/or077403.dLab Smp Id: 460-13139-E-4-A Client Smp ID: TB-2 5-6Inj Date : 14-MAY-2010 20:32 Operator : 615 Inst ID: PESTGC7.iSmp Info : 460-13139-E-4-AMisc Info : 460-13139-E-4-AComment : Method : /chem1/PESTGC7.i/8082/rear/May10/05-14-10/14may10a.b/08Or8082.mMeth Date : 05-May-2010 00:19 diazc Quant Type: ESTDCal Date : 04-MAY-2010 19:52 Cal File: or077121.dAls bottle: 12 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: AllPCB.subTarget Version: 3.50 Sample Matrix: SOLIDProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (mL)Ws 15.03000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 30 Decachlorobiphenyl(surr) CAS #: 2051-24-3
9.277 9.278 -0.001 117209 48.5327 80.00- 120.00 100.00(aR)
-------------------------------------------------------------------------------
QC Flag Legend
a - Target compound detected but, quantitated amountBelow Limit Of Quantitation(BLOQ).
R - Spike/Surrogate failed recovery limits.
06/03/2010Page 474 of 623
Data File: or077403.d
Date: 14-MAY-2010 20:32
Client ID: TB-2 5-6 Instrument: PESTGC7.i
Sample Info: 460-13139-E-4-A Operator: 615
06/03/2010Page 475 of 623
FORM IForm 1PCBS ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-1 2-3
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-5
Matrix: of077404.dLab File ID:
Date Collected:8082Analysis Method:
Soil
TestAmerica Edison
05/12/2010 11:25
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 07:19
05/14/2010 20:48
N
10(mL)
Sample wt/vol: 15.02(g)
% Moisture: 6.5
GC Column: ID: 0.53(mm)CLP-2
Analysis Batch No.: 37531 ug/KgUnits:
SURROGATE %RECCAS NO. LIMITS Q
2051-24-3 DCB Decachlorobiphenyl 109 27-165
FORM I 8082
06/03/2010Page 476 of 623
Data File: of077404.d Report Date: 16-May-2010 18:33
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC7.i/8082/front/May10/05-14-10/14may10a.b/of077404.dLab Smp Id: 460-13139-E-5-A Client Smp ID: TB-1 2-3Inj Date : 14-MAY-2010 20:48 Operator : 615 Inst ID: PESTGC7.iSmp Info : 460-13139-E-5-AMisc Info : 460-13139-E-5-AComment : Method : /chem1/PESTGC7.i/8082/front/May10/05-14-10/14may10a.b/08Of8082.mMeth Date : 05-May-2010 00:12 diazc Quant Type: ESTDCal Date : 04-MAY-2010 19:52 Cal File: of077121.dAls bottle: 13 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: AllPCB.subTarget Version: 3.50 Sample Matrix: SOLIDProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (mL)Ws 15.02000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 30 Decachlorobiphenyl(surr) CAS #: 2051-24-3
10.207 10.205 0.002 190389 54.7359 36 80.00- 120.00 100.00
-------------------------------------------------------------------------------
06/03/2010Page 477 of 623
Data File: of077404.d
Date: 14-MAY-2010 20:48
Client ID: TB-1 2-3 Instrument: PESTGC7.i
Sample Info: 460-13139-E-5-A Operator: 615
06/03/2010Page 478 of 623
FORM IForm 1PCBS ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-1 2-3
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-5
Matrix: or077404.dLab File ID:
Date Collected:8082Analysis Method:
Soil
TestAmerica Edison
05/12/2010 11:25
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 07:19
05/14/2010 20:48
N
10(mL)
Sample wt/vol: 15.02(g)
% Moisture: 6.5
GC Column: ID: 0.53(mm)CLP-1
Analysis Batch No.: 37531 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Aroclor 101612674-11-2 72 72 14U
Aroclor 122111104-28-2 72 72 22U
Aroclor 123211141-16-5 72 72 41U
Aroclor 124253469-21-9 72 72 14U
Aroclor 124812672-29-6 72 72 19U
Aroclor 125411097-69-1 72 72 24U
Aroclor 126011096-82-5 72 72 8.0U
Aroclor 126237324-23-5 72 72 12U
Aroclor 126811100-14-4 72 72 12U
SURROGATE %RECCAS NO. LIMITS Q
2051-24-3 DCB Decachlorobiphenyl 113 27-165
FORM I 8082
06/03/2010Page 479 of 623
Data File: or077404.d Page 1 Report Date: 16-May-2010 18:33
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC7.i/8082/rear/May10/05-14-10/14may10a.b/or077404.dLab Smp Id: 460-13139-E-5-A Client Smp ID: TB-1 2-3Inj Date : 14-MAY-2010 20:48 Operator : 615 Inst ID: PESTGC7.iSmp Info : 460-13139-E-5-AMisc Info : 460-13139-E-5-AComment : Method : /chem1/PESTGC7.i/8082/rear/May10/05-14-10/14may10a.b/08Or8082.mMeth Date : 05-May-2010 00:19 diazc Quant Type: ESTDCal Date : 04-MAY-2010 19:52 Cal File: or077121.dAls bottle: 13 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: AllPCB.subTarget Version: 3.50 Sample Matrix: SOLIDProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (mL)Ws 15.02000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 30 Decachlorobiphenyl(surr) CAS #: 2051-24-3
9.277 9.278 -0.001 136579 56.5532 80.00- 120.00 100.00(aR)
-------------------------------------------------------------------------------
QC Flag Legend
a - Target compound detected but, quantitated amountBelow Limit Of Quantitation(BLOQ).
R - Spike/Surrogate failed recovery limits.
06/03/2010Page 480 of 623
Data File: or077404.d
Date: 14-MAY-2010 20:48
Client ID: TB-1 2-3 Instrument: PESTGC7.i
Sample Info: 460-13139-E-5-A Operator: 615
06/03/2010Page 481 of 623
FORM IForm 1PCBS ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-5 3-4
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-7
Matrix: of077406.dLab File ID:
Date Collected:8082Analysis Method:
Soil
TestAmerica Edison
05/12/2010 12:30
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 07:19
05/14/2010 21:21
N
10(mL)
Sample wt/vol: 15.02(g)
% Moisture: 61.5
GC Column: ID: 0.53(mm)CLP-2
Analysis Batch No.: 37531 ug/KgUnits:
SURROGATE %RECCAS NO. LIMITS Q
2051-24-3 DCB Decachlorobiphenyl 65 27-165
FORM I 8082
06/03/2010Page 482 of 623
Data File: of077406.d Report Date: 16-May-2010 18:33
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC7.i/8082/front/May10/05-14-10/14may10a.b/of077406.dLab Smp Id: 460-13139-E-7-A Client Smp ID: TB-5 3-4Inj Date : 14-MAY-2010 21:21 Operator : 615 Inst ID: PESTGC7.iSmp Info : 460-13139-E-7-AMisc Info : 460-13139-E-7-AComment : Method : /chem1/PESTGC7.i/8082/front/May10/05-14-10/14may10a.b/08Of8082.mMeth Date : 05-May-2010 00:12 diazc Quant Type: ESTDCal Date : 04-MAY-2010 19:52 Cal File: of077121.dAls bottle: 15 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: AllPCB.subTarget Version: 3.50 Sample Matrix: SOLIDProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (mL)Ws 15.02000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 30 Decachlorobiphenyl(surr) CAS #: 2051-24-3
10.205 10.205 0.000 112937 32.4688 22 80.00- 120.00 100.00
-------------------------------------------------------------------------------
06/03/2010Page 483 of 623
Data File: of077406.d
Date: 14-MAY-2010 21:21
Client ID: TB-5 3-4 Instrument: PESTGC7.i
Sample Info: 460-13139-E-7-A Operator: 615
06/03/2010Page 484 of 623
FORM IForm 1PCBS ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
TB-5 3-4
SDG No.:
460-13139-1
Lab Sample ID: 460-13139-7
Matrix: or077406.dLab File ID:
Date Collected:8082Analysis Method:
Soil
TestAmerica Edison
05/12/2010 12:30
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 07:19
05/14/2010 21:21
N
10(mL)
Sample wt/vol: 15.02(g)
% Moisture: 61.5
GC Column: ID: 0.53(mm)CLP-1
Analysis Batch No.: 37531 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Aroclor 101612674-11-2 170 170 33U
Aroclor 122111104-28-2 170 170 52U
Aroclor 123211141-16-5 170 170 99U
Aroclor 124253469-21-9 170 170 33U
Aroclor 124812672-29-6 170 170 46U
Aroclor 125411097-69-1 170 170 59U
Aroclor 126011096-82-5 170 170 19U
Aroclor 126237324-23-5 170 170 30U
Aroclor 126811100-14-4 170 170 30U
SURROGATE %RECCAS NO. LIMITS Q
2051-24-3 DCB Decachlorobiphenyl 55 27-165
FORM I 8082
06/03/2010Page 485 of 623
Data File: or077406.d Page 1 Report Date: 16-May-2010 18:34
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC7.i/8082/rear/May10/05-14-10/14may10a.b/or077406.dLab Smp Id: 460-13139-E-7-A Client Smp ID: TB-5 3-4Inj Date : 14-MAY-2010 21:21 Operator : 615 Inst ID: PESTGC7.iSmp Info : 460-13139-E-7-AMisc Info : 460-13139-E-7-AComment : Method : /chem1/PESTGC7.i/8082/rear/May10/05-14-10/14may10a.b/08Or8082.mMeth Date : 05-May-2010 00:19 diazc Quant Type: ESTDCal Date : 04-MAY-2010 19:52 Cal File: or077121.dAls bottle: 15 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: AllPCB.subTarget Version: 3.50 Sample Matrix: SOLIDProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (mL)Ws 15.02000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 30 Decachlorobiphenyl(surr) CAS #: 2051-24-3
9.277 9.278 -0.001 66819 27.6677 80.00- 120.00 100.00(aR)
-------------------------------------------------------------------------------
QC Flag Legend
a - Target compound detected but, quantitated amountBelow Limit Of Quantitation(BLOQ).
R - Spike/Surrogate failed recovery limits.
06/03/2010Page 486 of 623
Data File: or077406.d
Date: 14-MAY-2010 21:21
Client ID: TB-5 3-4 Instrument: PESTGC7.i
Sample Info: 460-13139-E-7-A Operator: 615
06/03/2010Page 487 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6034Calibration Start Date: Calibration End Date:05/04/2010 16:54
N
05/04/2010 17:58
0.53(mm)GC Column: CLP-2 ID:
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/4 of077110.dLevel 2 IC 460-36537/5 of077111.dLevel 3 IC 460-36537/6 of077112.dLevel 4 IC 460-36537/7 of077113.dLevel 5 IC 460-36537/8 of077114.d
ANALYTE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 AVG RTRT WINDOW
PCB-1016 Peak 1 2.5572.485 - 2.6252.562 2.555 2.555 2.555 2.558PCB-1016 Peak 2 2.9922.920 - 3.0602.997 2.990 2.990 2.990 2.993PCB-1016 Peak 3 3.2583.185 - 3.3253.263 3.257 3.255 3.255 3.258PCB-1016 Peak 4 3.5073.435 - 3.5753.512 3.505 3.505 3.505 3.508PCB-1016 Peak 5 3.6673.595 - 3.7353.672 3.665 3.665 3.665 3.668PCB-1016 Peak 6 3.9573.885 - 4.0253.962 3.955 3.955 3.955 3.958PCB-1016 Peak 7 4.2294.157 - 4.2974.233 4.228 4.227 4.227 4.230PCB-1016 Peak 8 4.3824.310 - 4.4504.387 4.382 4.380 4.380 4.383PCB-1260 Peak 1 5.8325.762 - 5.9025.837 5.832 5.832 5.830 5.832PCB-1260 Peak 2 6.1196.048 - 6.1886.123 6.118 6.118 6.117 6.120PCB-1260 Peak 3 6.6476.575 - 6.7156.652 6.647 6.645 6.645 6.647PCB-1260 Peak 4 6.8086.737 - 6.8776.812 6.808 6.807 6.805 6.808PCB-1260 Peak 5 6.9016.830 - 6.9706.905 6.900 6.900 6.898 6.902PCB-1260 Peak 6 7.3467.275 - 7.4157.350 7.345 7.345 7.343 7.347PCB-1260 Peak 7 8.7598.688 - 8.8288.763 8.758 8.758 8.757 8.758PCB-1260 Peak 8 9.6289.557 - 9.6979.630 9.628 9.627 9.627 9.627Tetrachloro-m-xylene 2.0792.027 - 2.1272.083 2.077 2.077 2.078 2.080DCB Decachlorobiphenyl 10.20610.105 - 10.30510.208 10.207 10.205 10.205 10.205
FORM VI 8082 06/03/2010Page 488 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6034Calibration Start Date: Calibration End Date:05/04/2010 16:54
N
05/04/2010 17:58
0.53(mm)CLP-2 ID:
EXTERNAL STANDARD CURVE EVALUTION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-36537/4 of077110.d2Level IC 460-36537/5 of077111.d3Level IC 460-36537/6 of077112.d4Level IC 460-36537/7 of077113.d5Level IC 460-36537/8 of077114.d
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 4LVL 3LVL 2LVL 1
RRFANALYTE MIN RRF
LVL 5
PCB-1016 Peak 1 Ave 10.7 20.0113127.61 122.80 112.44 105.0698.465
PCB-1016 Peak 2 Ave 18.2 20.0236302.64 243.74 238.15 208.12189.69
PCB-1016 Peak 3 Ave 11.3 20.0110120.89 117.41 119.93 94.67299.372
PCB-1016 Peak 4 Ave 11.7 20.0428492.83 448.10 442.92 390.85365.56
PCB-1016 Peak 5 Ave 11.1 20.0201228.07 210.75 207.52 185.34171.51
PCB-1016 Peak 6 Ave 18.4 20.0133168.38 144.54 123.03 126.89103.18
PCB-1016 Peak 7 Ave 14.1 20.0154170.71 169.33 162.72 150.00118.28
PCB-1016 Peak 8 Ave 8.1 20.0156153.95 158.62 175.59 143.67146.53
PCB-1260 Peak 1 Ave 14.2 20.0304366.22 317.29 309.03 272.59254.89
PCB-1260 Peak 2 Ave 15.2 20.0340415.24 356.59 345.81 296.98286.16
PCB-1260 Peak 3 Ave 10.9 20.0484552.60 506.64 495.66 442.06420.61
PCB-1260 Peak 4 Ave 13.3 20.0243287.87 254.67 245.99 218.49205.73
PCB-1260 Peak 5 Ave 10.3 20.0146161.95 154.69 154.78 130.44130.01
PCB-1260 Peak 6 Ave 10.3 20.0266300.20 277.11 276.36 241.12234.86
PCB-1260 Peak 7 Ave 8.0 20.0371392.33 384.93 395.37 353.36327.05
FORM VI 8082
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 489 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6034Calibration Start Date: Calibration End Date:05/04/2010 16:54
N
05/04/2010 17:58
0.53(mm)CLP-2 ID:
EXTERNAL STANDARD CURVE EVALUTION
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 4LVL 3LVL 2LVL 1
RRFANALYTE MIN RRF
LVL 5
PCB-1260 Peak 8 Ave 6.9 20.0125128.52 133.20 132.09 119.99112.83
Tetrachloro-m-xylene Ave 4.1 20.049844917.9 5121.6 5256.6 4888.74733.7
DCB Decachlorobiphenyl Ave 7.2 20.034783677.5 3685.1 3603.0 3281.63144.4
FORM VI 8082
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 490 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6034Calibration Start Date: Calibration End Date:05/04/2010 16:54
N
05/04/2010 17:58
GC Column: CLP-2 ID: 0.53(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/4 of077110.dLevel 2 IC 460-36537/5 of077111.dLevel 3 IC 460-36537/6 of077112.dLevel 4 IC 460-36537/7 of077113.dLevel 5 IC 460-36537/8 of077114.d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UG/L)
LVL 1 LVL 1LVL 2 LVL 2LVL 3 LVL 3LVL 4 LVL 4LVL 5 LVL 5
PCB-1016 Peak 1 Ave 12761 61402 112436 157593 246162 100 500 1000 1500 2500PCB-1016 Peak 2 Ave 30264 121868 238150 312174 474233 100 500 1000 1500 2500PCB-1016 Peak 3 Ave 12089 58707 119927 142008 248429 100 500 1000 1500 2500PCB-1016 Peak 4 Ave 49283 224051 442921 586273 913898 100 500 1000 1500 2500PCB-1016 Peak 5 Ave 22807 105377 207521 278004 428764 100 500 1000 1500 2500PCB-1016 Peak 6 Ave 16838 72269 123032 190341 257947 100 500 1000 1500 2500PCB-1016 Peak 7 Ave 17071 84666 162717 224998 295709 100 500 1000 1500 2500PCB-1016 Peak 8 Ave 15395 79310 175591 215509 366327 100 500 1000 1500 2500PCB-1260 Peak 1 Ave 36622 158643 309028 408879 637225 100 500 1000 1500 2500PCB-1260 Peak 2 Ave 41524 178297 345807 445464 715394 100 500 1000 1500 2500PCB-1260 Peak 3 Ave 55260 253320 495657 663088 1051514 100 500 1000 1500 2500PCB-1260 Peak 4 Ave 28787 127333 245987 327740 514318 100 500 1000 1500 2500PCB-1260 Peak 5 Ave 16195 77346 154781 195657 325031 100 500 1000 1500 2500PCB-1260 Peak 6 Ave 30020 138556 276362 361675 587157 100 500 1000 1500 2500PCB-1260 Peak 7 Ave 39233 192463 395372 530042 817635 100 500 1000 1500 2500PCB-1260 Peak 8 Ave 12852 66601 132085 179981 282076 100 500 1000 1500 2500Tetrachloro-m-xylene Ave 122947 256079 525659 733307 946740 25.0 50.0 100 150 200DCB Decachlorobiphenyl Ave 91938 184256 360298 492235 628886 25.0 50.0 100 150 200
Curve Type Legend:Ave = Average
FORM VI 8082 06/03/2010Page 491 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6042Calibration Start Date: Calibration End Date:05/04/2010 16:54
N
05/04/2010 17:58
0.53(mm)GC Column: CLP-1 ID:
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/4 or077110.dLevel 2 IC 460-36537/5 or077111.dLevel 3 IC 460-36537/6 or077112.dLevel 4 IC 460-36537/7 or077113.dLevel 5 IC 460-36537/8 or077114.d
ANALYTE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 AVG RTRT WINDOW
PCB-1016 Peak 1 2.2642.193 - 2.3332.268 2.263 2.263 2.263 2.263PCB-1016 Peak 2 2.5832.512 - 2.6522.585 2.583 2.582 2.583 2.582PCB-1016 Peak 3 2.7722.702 - 2.8422.775 2.772 2.772 2.772 2.772PCB-1016 Peak 4 3.0362.965 - 3.1053.038 3.035 3.035 3.035 3.035PCB-1016 Peak 5 3.1783.107 - 3.2473.182 3.178 3.177 3.177 3.177PCB-1016 Peak 6 3.2393.168 - 3.3083.240 3.238 3.238 3.238 3.238PCB-1016 Peak 7 3.6113.540 - 3.6803.613 3.612 3.610 3.610 3.610PCB-1016 Peak 8 3.7083.637 - 3.7773.712 3.708 3.707 3.707 3.707PCB-1260 Peak 1 5.0194.948 - 5.0885.022 5.020 5.018 5.018 5.018PCB-1260 Peak 2 5.3635.292 - 5.4325.365 5.363 5.362 5.362 5.362PCB-1260 Peak 3 5.7085.637 - 5.7775.710 5.708 5.707 5.707 5.707PCB-1260 Peak 4 5.8505.778 - 5.9185.853 5.850 5.848 5.848 5.848PCB-1260 Peak 5 6.1636.093 - 6.2336.165 6.163 6.163 6.162 6.162PCB-1260 Peak 6 7.0857.015 - 7.1557.088 7.087 7.085 7.083 7.083PCB-1260 Peak 7 7.2367.167 - 7.3077.238 7.237 7.237 7.235 7.235PCB-1260 Peak 8 8.4228.352 - 8.4928.425 8.423 8.422 8.420 8.420Tetrachloro-m-xylene 1.9701.918 - 2.0181.972 1.970 1.968 1.970 1.970DCB Decachlorobiphenyl 9.2799.178 - 9.3789.280 9.278 9.278 9.278 9.278
FORM VI 8082 06/03/2010Page 492 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6042Calibration Start Date: Calibration End Date:05/04/2010 16:54
N
05/04/2010 17:58
0.53(mm)CLP-1 ID:
EXTERNAL STANDARD CURVE EVALUTION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-36537/4 or077110.d2Level IC 460-36537/5 or077111.d3Level IC 460-36537/6 or077112.d4Level IC 460-36537/7 or077113.d5Level IC 460-36537/8 or077114.d
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 4LVL 3LVL 2LVL 1
RRFANALYTE MIN RRF
LVL 5
PCB-1016 Peak 1 Ave 17.8 20.07697.650 78.324 72.815 67.43562.786
PCB-1016 Peak 2 Ave 17.4 20.0131165.15 139.63 128.56 115.05106.79
PCB-1016 Peak 3 Ave 7.8 20.09298.330 96.916 94.289 86.39381.814
PCB-1016 Peak 4 Ave 6.7 20.0248259.63 259.90 261.00 235.62225.47
PCB-1016 Peak 5 Ave 11.8 20.0102117.49 107.59 104.68 92.29787.665
PCB-1016 Peak 6 Ave 3.3 20.07068.620 70.728 73.485 69.91767.436
PCB-1016 Peak 7 Ave 10.4 20.0107120.06 113.04 108.52 98.49492.460
PCB-1016 Peak 8 Ave 8.3 20.04542.210 46.350 50.679 46.16941.281
PCB-1260 Peak 1 Ave 15.9 20.0159196.35 167.43 155.77 142.08131.21
PCB-1260 Peak 2 Ave 16.0 20.0279346.02 293.32 274.62 248.75231.21
PCB-1260 Peak 3 Ave 10.0 20.0255288.49 268.85 258.77 237.06224.03
PCB-1260 Peak 4 Ave 14.4 20.0125153.18 130.39 122.95 113.59106.36
PCB-1260 Peak 5 Ave 12.4 20.0130152.44 137.14 128.84 117.31112.21
PCB-1260 Peak 6 Ave 5.1 20.0147150.48 145.81 158.32 144.34138.14
PCB-1260 Peak 7 Ave 4.7 20.09086.650 90.200 97.509 89.03687.752
FORM VI 8082
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 493 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6042Calibration Start Date: Calibration End Date:05/04/2010 16:54
N
05/04/2010 17:58
0.53(mm)CLP-1 ID:
EXTERNAL STANDARD CURVE EVALUTION
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 4LVL 3LVL 2LVL 1
RRFANALYTE MIN RRF
LVL 5
PCB-1260 Peak 8 Ave 9.7 20.07362.650 70.488 81.271 77.33274.842
Tetrachloro-m-xylene Ave 6.1 20.026452408.4 2781.1 2803.9 2648.72584.3
DCB Decachlorobiphenyl Ave 7.7 20.024152521.6 2622.5 2482.6 2280.62168.0
FORM VI 8082
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 494 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6042Calibration Start Date: Calibration End Date:05/04/2010 16:54
N
05/04/2010 17:58
GC Column: CLP-1 ID: 0.53(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/4 or077110.dLevel 2 IC 460-36537/5 or077111.dLevel 3 IC 460-36537/6 or077112.dLevel 4 IC 460-36537/7 or077113.dLevel 5 IC 460-36537/8 or077114.d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UG/L)
LVL 1 LVL 1LVL 2 LVL 2LVL 3 LVL 3LVL 4 LVL 4LVL 5 LVL 5
PCB-1016 Peak 1 Ave 9765 39162 72815 101152 156966 100 500 1000 1500 2500PCB-1016 Peak 2 Ave 16515 69813 128558 172571 266964 100 500 1000 1500 2500PCB-1016 Peak 3 Ave 9833 48458 94289 129589 204534 100 500 1000 1500 2500PCB-1016 Peak 4 Ave 25963 129952 261001 353428 563686 100 500 1000 1500 2500PCB-1016 Peak 5 Ave 11749 53797 104682 138446 219162 100 500 1000 1500 2500PCB-1016 Peak 6 Ave 6862 35364 73485 104875 168591 100 500 1000 1500 2500PCB-1016 Peak 7 Ave 12006 56520 108515 147741 231150 100 500 1000 1500 2500PCB-1016 Peak 8 Ave 4221 23175 50679 69254 103203 100 500 1000 1500 2500PCB-1260 Peak 1 Ave 19635 83715 155769 213120 328021 100 500 1000 1500 2500PCB-1260 Peak 2 Ave 34602 146660 274615 373132 578023 100 500 1000 1500 2500PCB-1260 Peak 3 Ave 28849 134423 258774 355594 560083 100 500 1000 1500 2500PCB-1260 Peak 4 Ave 15318 65197 122945 170391 265894 100 500 1000 1500 2500PCB-1260 Peak 5 Ave 15244 68570 128841 175968 280519 100 500 1000 1500 2500PCB-1260 Peak 6 Ave 15048 72904 158321 216511 345343 100 500 1000 1500 2500PCB-1260 Peak 7 Ave 8665 45100 97509 133554 219380 100 500 1000 1500 2500PCB-1260 Peak 8 Ave 6265 35244 81271 115998 187104 100 500 1000 1500 2500Tetrachloro-m-xylene Ave 60210 139056 280394 397305 516858 25.0 50.0 100 150 200DCB Decachlorobiphenyl Ave 63041 131126 248257 342086 433591 25.0 50.0 100 150 200
Curve Type Legend:Ave = Average
FORM VI 8082 06/03/2010Page 495 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6035Calibration Start Date: Calibration End Date:05/04/2010 18:15
N
05/04/2010 18:15
0.53(mm)GC Column: CLP-2 ID:
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/9 of077115.d
ANALYTE LVL 1 AVG RTRT WINDOW
PCB-1221 Peak 1 1.6731.603 - 1.7431.673PCB-1221 Peak 2 1.9881.918 - 2.0581.988PCB-1221 Peak 3 2.3532.283 - 2.4232.353PCB-1221 Peak 4 2.4952.425 - 2.5652.495PCB-1221 Peak 5 2.5582.488 - 2.6282.558PCB-1221 Peak 6 3.0602.990 - 3.1303.060PCB-1221 Peak 7 3.2623.192 - 3.3323.262PCB-1221 Peak 8 3.5103.440 - 3.5803.510
FORM VI 8082 06/03/2010Page 496 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6035Calibration Start Date: Calibration End Date:05/04/2010 18:15
N
05/04/2010 18:15
0.53(mm)CLP-2 ID:
EXTERNAL STANDARD CURVE EVALUTION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-36537/9 of077115.d
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 1
RRFANALYTE MIN RRF
64.656PCB-1221 Peak 1 Ave 65 20.012.481PCB-1221 Peak 2 Ave 12 20.060.208PCB-1221 Peak 3 Ave 60 20.039.669PCB-1221 Peak 4 Ave 40 20.0158.59PCB-1221 Peak 5 Ave 159 20.027.866PCB-1221 Peak 6 Ave 28 20.011.526PCB-1221 Peak 7 Ave 12 20.024.711PCB-1221 Peak 8 Ave 25 20.0
FORM VI 8082
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 497 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6035Calibration Start Date: Calibration End Date:05/04/2010 18:15
N
05/04/2010 18:15
GC Column: CLP-2 ID: 0.53(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/9 of077115.d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UG/L)
LVL 1 LVL 1
PCB-1221 Peak 1 Ave 64656 1000PCB-1221 Peak 2 Ave 12481 1000PCB-1221 Peak 3 Ave 60208 1000PCB-1221 Peak 4 Ave 39669 1000PCB-1221 Peak 5 Ave 158588 1000PCB-1221 Peak 6 Ave 27866 1000PCB-1221 Peak 7 Ave 11526 1000PCB-1221 Peak 8 Ave 24711 1000
Curve Type Legend:Ave = Average
FORM VI 8082 06/03/2010Page 498 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6043Calibration Start Date: Calibration End Date:05/04/2010 18:15
N
05/04/2010 18:15
0.53(mm)GC Column: CLP-1 ID:
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/9 or077115.d
ANALYTE LVL 1 AVG RTRT WINDOW
PCB-1221 Peak 1 1.5851.515 - 1.6551.585PCB-1221 Peak 2 1.8651.795 - 1.9351.865PCB-1221 Peak 3 2.1032.033 - 2.1732.103PCB-1221 Peak 4 2.2632.193 - 2.3332.263PCB-1221 Peak 5 2.6522.582 - 2.7222.652PCB-1221 Peak 6 2.7132.643 - 2.7832.713PCB-1221 Peak 7 2.7532.683 - 2.8232.753PCB-1221 Peak 8 3.0382.968 - 3.1083.038
FORM VI 8082 06/03/2010Page 499 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6043Calibration Start Date: Calibration End Date:05/04/2010 18:15
N
05/04/2010 18:15
0.53(mm)CLP-1 ID:
EXTERNAL STANDARD CURVE EVALUTION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-36537/9 or077115.d
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 1
RRFANALYTE MIN RRF
32.298PCB-1221 Peak 1 Ave 32 20.08.3490PCB-1221 Peak 2 Ave 8 20.031.460PCB-1221 Peak 3 Ave 31 20.0102.55PCB-1221 Peak 4 Ave 103 20.05.6420PCB-1221 Peak 5 Ave 6 20.012.402PCB-1221 Peak 6 Ave 12 20.07.3820PCB-1221 Peak 7 Ave 7 20.011.910PCB-1221 Peak 8 Ave 12 20.0
FORM VI 8082
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 500 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6043Calibration Start Date: Calibration End Date:05/04/2010 18:15
N
05/04/2010 18:15
GC Column: CLP-1 ID: 0.53(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/9 or077115.d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UG/L)
LVL 1 LVL 1
PCB-1221 Peak 1 Ave 32298 1000PCB-1221 Peak 2 Ave 8349 1000PCB-1221 Peak 3 Ave 31460 1000PCB-1221 Peak 4 Ave 102550 1000PCB-1221 Peak 5 Ave 5642 1000PCB-1221 Peak 6 Ave 12402 1000PCB-1221 Peak 7 Ave 7382 1000PCB-1221 Peak 8 Ave 11910 1000
Curve Type Legend:Ave = Average
FORM VI 8082 06/03/2010Page 501 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6036Calibration Start Date: Calibration End Date:05/04/2010 18:31
N
05/04/2010 18:31
0.53(mm)GC Column: CLP-2 ID:
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/10 of077116.d
ANALYTE LVL 1 AVG RTRT WINDOW
PCB-1232 Peak 1 2.5602.490 - 2.6302.560PCB-1232 Peak 2 2.9952.925 - 3.0652.995PCB-1232 Peak 3 3.2603.190 - 3.3303.260PCB-1232 Peak 4 3.6703.600 - 3.7403.670PCB-1232 Peak 5 3.7933.723 - 3.8633.793PCB-1232 Peak 6 3.9103.840 - 3.9803.910PCB-1232 Peak 7 4.2324.162 - 4.3024.232PCB-1232 Peak 8 4.3854.315 - 4.4554.385
FORM VI 8082 06/03/2010Page 502 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6036Calibration Start Date: Calibration End Date:05/04/2010 18:31
N
05/04/2010 18:31
0.53(mm)CLP-2 ID:
EXTERNAL STANDARD CURVE EVALUTION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-36537/10 of077116.d
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 1
RRFANALYTE MIN RRF
108.16PCB-1232 Peak 1 Ave 108 20.0118.09PCB-1232 Peak 2 Ave 118 20.053.332PCB-1232 Peak 3 Ave 53 20.087.901PCB-1232 Peak 4 Ave 88 20.049.526PCB-1232 Peak 5 Ave 50 20.049.369PCB-1232 Peak 6 Ave 49 20.066.746PCB-1232 Peak 7 Ave 67 20.078.406PCB-1232 Peak 8 Ave 78 20.0
FORM VI 8082
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 503 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6036Calibration Start Date: Calibration End Date:05/04/2010 18:31
N
05/04/2010 18:31
GC Column: CLP-2 ID: 0.53(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/10 of077116.d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UG/L)
LVL 1 LVL 1
PCB-1232 Peak 1 Ave 108156 1000PCB-1232 Peak 2 Ave 118089 1000PCB-1232 Peak 3 Ave 53332 1000PCB-1232 Peak 4 Ave 87901 1000PCB-1232 Peak 5 Ave 49526 1000PCB-1232 Peak 6 Ave 49369 1000PCB-1232 Peak 7 Ave 66746 1000PCB-1232 Peak 8 Ave 78406 1000
Curve Type Legend:Ave = Average
FORM VI 8082 06/03/2010Page 504 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6044Calibration Start Date: Calibration End Date:05/04/2010 18:31
N
05/04/2010 18:31
0.53(mm)GC Column: CLP-1 ID:
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/10 or077116.d
ANALYTE LVL 1 AVG RTRT WINDOW
PCB-1232 Peak 1 2.2632.193 - 2.3332.263PCB-1232 Peak 2 2.5832.513 - 2.6532.583PCB-1232 Peak 3 2.7722.702 - 2.8422.772PCB-1232 Peak 4 3.0352.965 - 3.1053.035PCB-1232 Peak 5 3.1783.108 - 3.2483.178PCB-1232 Peak 6 3.2383.168 - 3.3083.238PCB-1232 Peak 7 3.6103.540 - 3.6803.610PCB-1232 Peak 8 3.9903.920 - 4.0603.990
FORM VI 8082 06/03/2010Page 505 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6044Calibration Start Date: Calibration End Date:05/04/2010 18:31
N
05/04/2010 18:31
0.53(mm)CLP-1 ID:
EXTERNAL STANDARD CURVE EVALUTION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-36537/10 or077116.d
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 1
RRFANALYTE MIN RRF
73.523PCB-1232 Peak 1 Ave 74 20.058.193PCB-1232 Peak 2 Ave 58 20.040.586PCB-1232 Peak 3 Ave 41 20.0105.81PCB-1232 Peak 4 Ave 106 20.043.298PCB-1232 Peak 5 Ave 43 20.027.907PCB-1232 Peak 6 Ave 28 20.049.124PCB-1232 Peak 7 Ave 49 20.015.863PCB-1232 Peak 8 Ave 16 20.0
FORM VI 8082
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 506 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6044Calibration Start Date: Calibration End Date:05/04/2010 18:31
N
05/04/2010 18:31
GC Column: CLP-1 ID: 0.53(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/10 or077116.d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UG/L)
LVL 1 LVL 1
PCB-1232 Peak 1 Ave 73523 1000PCB-1232 Peak 2 Ave 58193 1000PCB-1232 Peak 3 Ave 40586 1000PCB-1232 Peak 4 Ave 105811 1000PCB-1232 Peak 5 Ave 43298 1000PCB-1232 Peak 6 Ave 27907 1000PCB-1232 Peak 7 Ave 49124 1000PCB-1232 Peak 8 Ave 15863 1000
Curve Type Legend:Ave = Average
FORM VI 8082 06/03/2010Page 507 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6037Calibration Start Date: Calibration End Date:05/04/2010 18:47
N
05/04/2010 18:47
0.53(mm)GC Column: CLP-2 ID:
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/11 of077117.d
ANALYTE LVL 1 AVG RTRT WINDOW
PCB-1242 Peak 1 2.5552.485 - 2.6252.555PCB-1242 Peak 2 2.9922.922 - 3.0622.992PCB-1242 Peak 3 3.2573.187 - 3.3273.257PCB-1242 Peak 4 3.5053.435 - 3.5753.505PCB-1242 Peak 5 3.6653.595 - 3.7353.665PCB-1242 Peak 6 3.9053.835 - 3.9753.905PCB-1242 Peak 7 4.3804.310 - 4.4504.380PCB-1242 Peak 8 4.7574.687 - 4.8274.757
FORM VI 8082 06/03/2010Page 508 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6037Calibration Start Date: Calibration End Date:05/04/2010 18:47
N
05/04/2010 18:47
0.53(mm)CLP-2 ID:
EXTERNAL STANDARD CURVE EVALUTION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-36537/11 of077117.d
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 1
RRFANALYTE MIN RRF
94.763PCB-1242 Peak 1 Ave 95 20.0185.32PCB-1242 Peak 2 Ave 185 20.087.709PCB-1242 Peak 3 Ave 88 20.0339.13PCB-1242 Peak 4 Ave 339 20.0161.07PCB-1242 Peak 5 Ave 161 20.083.566PCB-1242 Peak 6 Ave 84 20.0148.19PCB-1242 Peak 7 Ave 148 20.0158.51PCB-1242 Peak 8 Ave 159 20.0
FORM VI 8082
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 509 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6037Calibration Start Date: Calibration End Date:05/04/2010 18:47
N
05/04/2010 18:47
GC Column: CLP-2 ID: 0.53(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/11 of077117.d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UG/L)
LVL 1 LVL 1
PCB-1242 Peak 1 Ave 94763 1000PCB-1242 Peak 2 Ave 185324 1000PCB-1242 Peak 3 Ave 87709 1000PCB-1242 Peak 4 Ave 339132 1000PCB-1242 Peak 5 Ave 161074 1000PCB-1242 Peak 6 Ave 83566 1000PCB-1242 Peak 7 Ave 148191 1000PCB-1242 Peak 8 Ave 158514 1000
Curve Type Legend:Ave = Average
FORM VI 8082 06/03/2010Page 510 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6045Calibration Start Date: Calibration End Date:05/04/2010 18:47
N
05/04/2010 18:47
0.53(mm)GC Column: CLP-1 ID:
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/11 or077117.d
ANALYTE LVL 1 AVG RTRT WINDOW
PCB-1242 Peak 1 2.2652.195 - 2.3352.265PCB-1242 Peak 2 2.5832.513 - 2.6532.583PCB-1242 Peak 3 2.7732.703 - 2.8432.773PCB-1242 Peak 4 3.0372.967 - 3.1073.037PCB-1242 Peak 5 3.1783.108 - 3.2483.178PCB-1242 Peak 6 3.3833.313 - 3.4533.383PCB-1242 Peak 7 3.6123.542 - 3.6823.612PCB-1242 Peak 8 4.3374.267 - 4.4074.337
FORM VI 8082 06/03/2010Page 511 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6045Calibration Start Date: Calibration End Date:05/04/2010 18:47
N
05/04/2010 18:47
0.53(mm)CLP-1 ID:
EXTERNAL STANDARD CURVE EVALUTION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-36537/11 or077117.d
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 1
RRFANALYTE MIN RRF
60.615PCB-1242 Peak 1 Ave 61 20.097.066PCB-1242 Peak 2 Ave 97 20.070.047PCB-1242 Peak 3 Ave 70 20.0196.64PCB-1242 Peak 4 Ave 197 20.079.039PCB-1242 Peak 5 Ave 79 20.096.474PCB-1242 Peak 6 Ave 96 20.085.652PCB-1242 Peak 7 Ave 86 20.060.313PCB-1242 Peak 8 Ave 60 20.0
FORM VI 8082
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 512 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6045Calibration Start Date: Calibration End Date:05/04/2010 18:47
N
05/04/2010 18:47
GC Column: CLP-1 ID: 0.53(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/11 or077117.d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UG/L)
LVL 1 LVL 1
PCB-1242 Peak 1 Ave 60615 1000PCB-1242 Peak 2 Ave 97066 1000PCB-1242 Peak 3 Ave 70047 1000PCB-1242 Peak 4 Ave 196639 1000PCB-1242 Peak 5 Ave 79039 1000PCB-1242 Peak 6 Ave 96474 1000PCB-1242 Peak 7 Ave 85652 1000PCB-1242 Peak 8 Ave 60313 1000
Curve Type Legend:Ave = Average
FORM VI 8082 06/03/2010Page 513 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6038Calibration Start Date: Calibration End Date:05/04/2010 19:03
N
05/04/2010 19:03
0.53(mm)GC Column: CLP-2 ID:
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/12 of077118.d
ANALYTE LVL 1 AVG RTRT WINDOW
PCB-1248 Peak 1 2.9902.920 - 3.0602.990PCB-1248 Peak 2 3.5033.433 - 3.5733.503PCB-1248 Peak 3 3.8033.733 - 3.8733.803PCB-1248 Peak 4 3.9053.835 - 3.9753.905PCB-1248 Peak 5 4.2274.157 - 4.2974.227PCB-1248 Peak 6 4.3804.310 - 4.4504.380PCB-1248 Peak 7 4.7034.633 - 4.7734.703PCB-1248 Peak 8 4.7534.683 - 4.8234.753
FORM VI 8082 06/03/2010Page 514 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6038Calibration Start Date: Calibration End Date:05/04/2010 19:03
N
05/04/2010 19:03
0.53(mm)CLP-2 ID:
EXTERNAL STANDARD CURVE EVALUTION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-36537/12 of077118.d
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 1
RRFANALYTE MIN RRF
96.587PCB-1248 Peak 1 Ave 97 20.0223.39PCB-1248 Peak 2 Ave 223 20.039.427PCB-1248 Peak 3 Ave 39 20.0140.34PCB-1248 Peak 4 Ave 140 20.0187.79PCB-1248 Peak 5 Ave 188 20.0231.65PCB-1248 Peak 6 Ave 232 20.0156.03PCB-1248 Peak 7 Ave 156 20.0297.51PCB-1248 Peak 8 Ave 298 20.0
FORM VI 8082
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 515 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6038Calibration Start Date: Calibration End Date:05/04/2010 19:03
N
05/04/2010 19:03
GC Column: CLP-2 ID: 0.53(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/12 of077118.d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UG/L)
LVL 1 LVL 1
PCB-1248 Peak 1 Ave 96587 1000PCB-1248 Peak 2 Ave 223386 1000PCB-1248 Peak 3 Ave 39427 1000PCB-1248 Peak 4 Ave 140343 1000PCB-1248 Peak 5 Ave 187787 1000PCB-1248 Peak 6 Ave 231645 1000PCB-1248 Peak 7 Ave 156031 1000PCB-1248 Peak 8 Ave 297509 1000
Curve Type Legend:Ave = Average
FORM VI 8082 06/03/2010Page 516 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6046Calibration Start Date: Calibration End Date:05/04/2010 19:03
N
05/04/2010 19:03
0.53(mm)GC Column: CLP-1 ID:
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/12 or077118.d
ANALYTE LVL 1 AVG RTRT WINDOW
PCB-1248 Peak 1 2.5822.512 - 2.6522.582PCB-1248 Peak 2 3.0332.963 - 3.1033.033PCB-1248 Peak 3 3.2373.167 - 3.3073.237PCB-1248 Peak 4 3.3783.308 - 3.4483.378PCB-1248 Peak 5 3.6083.538 - 3.6783.608PCB-1248 Peak 6 3.7033.633 - 3.7733.703PCB-1248 Peak 7 3.9883.918 - 4.0583.988PCB-1248 Peak 8 4.3334.263 - 4.4034.333
FORM VI 8082 06/03/2010Page 517 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6046Calibration Start Date: Calibration End Date:05/04/2010 19:03
N
05/04/2010 19:03
0.53(mm)CLP-1 ID:
EXTERNAL STANDARD CURVE EVALUTION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-36537/12 or077118.d
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 1
RRFANALYTE MIN RRF
51.708PCB-1248 Peak 1 Ave 52 20.0140.47PCB-1248 Peak 2 Ave 140 20.027.055PCB-1248 Peak 3 Ave 27 20.0230.64PCB-1248 Peak 4 Ave 231 20.0132.03PCB-1248 Peak 5 Ave 132 20.079.703PCB-1248 Peak 6 Ave 80 20.052.018PCB-1248 Peak 7 Ave 52 20.0120.25PCB-1248 Peak 8 Ave 120 20.0
FORM VI 8082
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 518 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6046Calibration Start Date: Calibration End Date:05/04/2010 19:03
N
05/04/2010 19:03
GC Column: CLP-1 ID: 0.53(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/12 or077118.d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UG/L)
LVL 1 LVL 1
PCB-1248 Peak 1 Ave 51708 1000PCB-1248 Peak 2 Ave 140469 1000PCB-1248 Peak 3 Ave 27055 1000PCB-1248 Peak 4 Ave 230642 1000PCB-1248 Peak 5 Ave 132027 1000PCB-1248 Peak 6 Ave 79703 1000PCB-1248 Peak 7 Ave 52018 1000PCB-1248 Peak 8 Ave 120253 1000
Curve Type Legend:Ave = Average
FORM VI 8082 06/03/2010Page 519 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6039Calibration Start Date: Calibration End Date:05/04/2010 19:19
N
05/04/2010 19:19
0.53(mm)GC Column: CLP-2 ID:
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/13 of077119.d
ANALYTE LVL 1 AVG RTRT WINDOW
PCB-1254 Peak 1 3.9033.833 - 3.9733.903PCB-1254 Peak 2 4.7454.675 - 4.8154.745PCB-1254 Peak 3 4.9934.923 - 5.0634.993PCB-1254 Peak 4 5.4285.358 - 5.4985.428PCB-1254 Peak 5 5.5785.508 - 5.6485.578PCB-1254 Peak 6 6.3486.278 - 6.4186.348PCB-1254 Peak 7 6.6486.578 - 6.7186.648PCB-1254 Peak 8 7.2807.210 - 7.3507.280
FORM VI 8082 06/03/2010Page 520 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6039Calibration Start Date: Calibration End Date:05/04/2010 19:19
N
05/04/2010 19:19
0.53(mm)CLP-2 ID:
EXTERNAL STANDARD CURVE EVALUTION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-36537/13 of077119.d
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 1
RRFANALYTE MIN RRF
153.00PCB-1254 Peak 1 Ave 153 20.0224.66PCB-1254 Peak 2 Ave 225 20.0230.71PCB-1254 Peak 3 Ave 231 20.0173.21PCB-1254 Peak 4 Ave 173 20.0363.62PCB-1254 Peak 5 Ave 364 20.0194.55PCB-1254 Peak 6 Ave 195 20.0374.30PCB-1254 Peak 7 Ave 374 20.073.378PCB-1254 Peak 8 Ave 73 20.0
FORM VI 8082
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 521 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6039Calibration Start Date: Calibration End Date:05/04/2010 19:19
N
05/04/2010 19:19
GC Column: CLP-2 ID: 0.53(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/13 of077119.d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UG/L)
LVL 1 LVL 1
PCB-1254 Peak 1 Ave 152999 1000PCB-1254 Peak 2 Ave 224655 1000PCB-1254 Peak 3 Ave 230707 1000PCB-1254 Peak 4 Ave 173208 1000PCB-1254 Peak 5 Ave 363620 1000PCB-1254 Peak 6 Ave 194545 1000PCB-1254 Peak 7 Ave 374295 1000PCB-1254 Peak 8 Ave 73378 1000
Curve Type Legend:Ave = Average
FORM VI 8082 06/03/2010Page 522 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6047Calibration Start Date: Calibration End Date:05/04/2010 19:19
N
05/04/2010 19:19
0.53(mm)GC Column: CLP-1 ID:
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/13 or077119.d
ANALYTE LVL 1 AVG RTRT WINDOW
PCB-1254 Peak 1 4.0283.958 - 4.0984.028PCB-1254 Peak 2 4.0834.013 - 4.1534.083PCB-1254 Peak 3 4.3304.260 - 4.4004.330PCB-1254 Peak 4 4.6524.582 - 4.7224.652PCB-1254 Peak 5 4.7984.728 - 4.8684.798PCB-1254 Peak 6 5.1405.070 - 5.2105.140PCB-1254 Peak 7 5.3625.292 - 5.4325.362PCB-1254 Peak 8 5.7075.637 - 5.7775.707
FORM VI 8082 06/03/2010Page 523 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6047Calibration Start Date: Calibration End Date:05/04/2010 19:19
N
05/04/2010 19:19
0.53(mm)CLP-1 ID:
EXTERNAL STANDARD CURVE EVALUTION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-36537/13 or077119.d
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 1
RRFANALYTE MIN RRF
104.84PCB-1254 Peak 1 Ave 105 20.086.222PCB-1254 Peak 2 Ave 86 20.0161.50PCB-1254 Peak 3 Ave 161 20.0116.34PCB-1254 Peak 4 Ave 116 20.0200.69PCB-1254 Peak 5 Ave 201 20.0144.50PCB-1254 Peak 6 Ave 144 20.0151.46PCB-1254 Peak 7 Ave 151 20.0214.05PCB-1254 Peak 8 Ave 214 20.0
FORM VI 8082
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 524 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6047Calibration Start Date: Calibration End Date:05/04/2010 19:19
N
05/04/2010 19:19
GC Column: CLP-1 ID: 0.53(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/13 or077119.d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UG/L)
LVL 1 LVL 1
PCB-1254 Peak 1 Ave 104835 1000PCB-1254 Peak 2 Ave 86222 1000PCB-1254 Peak 3 Ave 161497 1000PCB-1254 Peak 4 Ave 116344 1000PCB-1254 Peak 5 Ave 200690 1000PCB-1254 Peak 6 Ave 144495 1000PCB-1254 Peak 7 Ave 151457 1000PCB-1254 Peak 8 Ave 214049 1000
Curve Type Legend:Ave = Average
FORM VI 8082 06/03/2010Page 525 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6040Calibration Start Date: Calibration End Date:05/04/2010 19:36
N
05/04/2010 19:36
0.53(mm)GC Column: CLP-2 ID:
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/14 of077120.d
ANALYTE LVL 1 AVG RTRT WINDOW
PCB-1262 Peak 1 5.8355.765 - 5.9055.835PCB-1262 Peak 2 6.1226.052 - 6.1926.122PCB-1262 Peak 3 6.8106.740 - 6.8806.810PCB-1262 Peak 4 7.3487.278 - 7.4187.348PCB-1262 Peak 5 8.7578.687 - 8.8278.757PCB-1262 Peak 6 8.8538.783 - 8.9238.853PCB-1262 Peak 7 9.6279.557 - 9.6979.627PCB-1262 Peak 8 9.9689.898 - 10.0389.968
FORM VI 8082 06/03/2010Page 526 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6040Calibration Start Date: Calibration End Date:05/04/2010 19:36
N
05/04/2010 19:36
0.53(mm)CLP-2 ID:
EXTERNAL STANDARD CURVE EVALUTION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-36537/14 of077120.d
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 1
RRFANALYTE MIN RRF
167.97PCB-1262 Peak 1 Ave 168 20.0192.74PCB-1262 Peak 2 Ave 193 20.0263.16PCB-1262 Peak 3 Ave 263 20.0236.30PCB-1262 Peak 4 Ave 236 20.0309.61PCB-1262 Peak 5 Ave 310 20.0228.47PCB-1262 Peak 6 Ave 228 20.0164.26PCB-1262 Peak 7 Ave 164 20.052.898PCB-1262 Peak 8 Ave 53 20.0
FORM VI 8082
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 527 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6040Calibration Start Date: Calibration End Date:05/04/2010 19:36
N
05/04/2010 19:36
GC Column: CLP-2 ID: 0.53(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/14 of077120.d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UG/L)
LVL 1 LVL 1
PCB-1262 Peak 1 Ave 167965 1000PCB-1262 Peak 2 Ave 192741 1000PCB-1262 Peak 3 Ave 263161 1000PCB-1262 Peak 4 Ave 236303 1000PCB-1262 Peak 5 Ave 309611 1000PCB-1262 Peak 6 Ave 228466 1000PCB-1262 Peak 7 Ave 164264 1000PCB-1262 Peak 8 Ave 52898 1000
Curve Type Legend:Ave = Average
FORM VI 8082 06/03/2010Page 528 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6048Calibration Start Date: Calibration End Date:05/04/2010 19:36
N
05/04/2010 19:36
0.53(mm)GC Column: CLP-1 ID:
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/14 or077120.d
ANALYTE LVL 1 AVG RTRT WINDOW
PCB-1262 Peak 1 4.8524.782 - 4.9224.852PCB-1262 Peak 2 5.0204.950 - 5.0905.020PCB-1262 Peak 3 5.7085.638 - 5.7785.708PCB-1262 Peak 4 5.8505.780 - 5.9205.850PCB-1262 Peak 5 6.1636.093 - 6.2336.163PCB-1262 Peak 6 7.0857.015 - 7.1557.085PCB-1262 Peak 7 7.2357.165 - 7.3057.235PCB-1262 Peak 8 8.4228.352 - 8.4928.422
FORM VI 8082 06/03/2010Page 529 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6048Calibration Start Date: Calibration End Date:05/04/2010 19:36
N
05/04/2010 19:36
0.53(mm)CLP-1 ID:
EXTERNAL STANDARD CURVE EVALUTION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-36537/14 or077120.d
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 1
RRFANALYTE MIN RRF
81.556PCB-1262 Peak 1 Ave 82 20.088.062PCB-1262 Peak 2 Ave 88 20.0102.23PCB-1262 Peak 3 Ave 102 20.0134.50PCB-1262 Peak 4 Ave 134 20.0139.54PCB-1262 Peak 5 Ave 140 20.073.726PCB-1262 Peak 6 Ave 74 20.0130.91PCB-1262 Peak 7 Ave 131 20.0101.17PCB-1262 Peak 8 Ave 101 20.0
FORM VI 8082
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 530 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6048Calibration Start Date: Calibration End Date:05/04/2010 19:36
N
05/04/2010 19:36
GC Column: CLP-1 ID: 0.53(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/14 or077120.d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UG/L)
LVL 1 LVL 1
PCB-1262 Peak 1 Ave 81556 1000PCB-1262 Peak 2 Ave 88062 1000PCB-1262 Peak 3 Ave 102233 1000PCB-1262 Peak 4 Ave 134495 1000PCB-1262 Peak 5 Ave 139542 1000PCB-1262 Peak 6 Ave 73726 1000PCB-1262 Peak 7 Ave 130913 1000PCB-1262 Peak 8 Ave 101169 1000
Curve Type Legend:Ave = Average
FORM VI 8082 06/03/2010Page 531 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6041Calibration Start Date: Calibration End Date:05/04/2010 19:52
N
05/04/2010 19:52
0.53(mm)GC Column: CLP-2 ID:
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/15 of077121.d
ANALYTE LVL 1 AVG RTRT WINDOW
PCB-1268 Peak 1 6.8076.737 - 6.8776.807PCB-1268 Peak 2 7.3507.280 - 7.4207.350PCB-1268 Peak 3 8.7488.678 - 8.8188.748PCB-1268 Peak 4 8.8408.770 - 8.9108.840PCB-1268 Peak 5 9.2429.172 - 9.3129.242PCB-1268 Peak 6 9.3789.308 - 9.4489.378PCB-1268 Peak 7 9.6279.557 - 9.6979.627PCB-1268 Peak 8 9.9679.897 - 10.0379.967
FORM VI 8082 06/03/2010Page 532 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6041Calibration Start Date: Calibration End Date:05/04/2010 19:52
N
05/04/2010 19:52
0.53(mm)CLP-2 ID:
EXTERNAL STANDARD CURVE EVALUTION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-36537/15 of077121.d
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 1
RRFANALYTE MIN RRF
154.40PCB-1268 Peak 1 Ave 154 20.0187.29PCB-1268 Peak 2 Ave 187 20.0635.17PCB-1268 Peak 3 Ave 635 20.0699.68PCB-1268 Peak 4 Ave 700 20.0518.35PCB-1268 Peak 5 Ave 518 20.0165.76PCB-1268 Peak 6 Ave 166 20.0231.27PCB-1268 Peak 7 Ave 231 20.01224.8PCB-1268 Peak 8 Ave 1225 20.0
FORM VI 8082
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 533 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6041Calibration Start Date: Calibration End Date:05/04/2010 19:52
N
05/04/2010 19:52
GC Column: CLP-2 ID: 0.53(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/15 of077121.d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UG/L)
LVL 1 LVL 1
PCB-1268 Peak 1 Ave 154403 1000PCB-1268 Peak 2 Ave 187291 1000PCB-1268 Peak 3 Ave 635171 1000PCB-1268 Peak 4 Ave 699678 1000PCB-1268 Peak 5 Ave 518349 1000PCB-1268 Peak 6 Ave 165755 1000PCB-1268 Peak 7 Ave 231270 1000PCB-1268 Peak 8 Ave 1224753 1000
Curve Type Legend:Ave = Average
FORM VI 8082 06/03/2010Page 534 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6049Calibration Start Date: Calibration End Date:05/04/2010 19:52
N
05/04/2010 19:52
0.53(mm)GC Column: CLP-1 ID:
EXTERNAL STANDARD RETENTION TIME SUMMARY
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/15 or077121.d
ANALYTE LVL 1 AVG RTRT WINDOW
PCB-1268 Peak 1 5.8485.778 - 5.9185.848PCB-1268 Peak 2 6.1556.085 - 6.2256.155PCB-1268 Peak 3 7.1527.082 - 7.2227.152PCB-1268 Peak 4 7.2227.152 - 7.2927.222PCB-1268 Peak 5 7.5977.527 - 7.6677.597PCB-1268 Peak 6 7.7757.705 - 7.8457.775PCB-1268 Peak 7 8.4188.348 - 8.4888.418PCB-1268 Peak 8 8.9938.923 - 9.0638.993
FORM VI 8082 06/03/2010Page 535 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: GC Column: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6049Calibration Start Date: Calibration End Date:05/04/2010 19:52
N
05/04/2010 19:52
0.53(mm)CLP-1 ID:
EXTERNAL STANDARD CURVE EVALUTION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-36537/15 or077121.d
MIN R^2OR COD
#R^2OR COD
MAX%RSD
#%RSD#COEFFICIENT
M2M1B
CURVETYPE
LVL 1
RRFANALYTE MIN RRF
80.080PCB-1268 Peak 1 Ave 80 20.098.820PCB-1268 Peak 2 Ave 99 20.0349.63PCB-1268 Peak 3 Ave 350 20.0411.08PCB-1268 Peak 4 Ave 411 20.0316.72PCB-1268 Peak 5 Ave 317 20.097.295PCB-1268 Peak 6 Ave 97 20.0149.31PCB-1268 Peak 7 Ave 149 20.0892.46PCB-1268 Peak 8 Ave 892 20.0
FORM VI 8082
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
06/03/2010Page 536 of 623
FORM VI
Lab Name: Job No.:
Calibration ID:
SDG No.:
Instrument ID: Heated Purge: (Y/N)
GC SEMI VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-13139-1
PESTGC7
Analy Batch No.: 36537
6049Calibration Start Date: Calibration End Date:05/04/2010 19:52
N
05/04/2010 19:52
GC Column: CLP-1 ID: 0.53(mm)
EXTERNAL STANDARD RESPONSE AND CONCENTRATION
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/15 or077121.d
CURVETYPE
RESPONSEANALYTE CONCENTRATION (UG/L)
LVL 1 LVL 1
PCB-1268 Peak 1 Ave 80080 1000PCB-1268 Peak 2 Ave 98820 1000PCB-1268 Peak 3 Ave 349627 1000PCB-1268 Peak 4 Ave 411079 1000PCB-1268 Peak 5 Ave 316716 1000PCB-1268 Peak 6 Ave 97295 1000PCB-1268 Peak 7 Ave 149313 1000PCB-1268 Peak 8 Ave 892458 1000
Curve Type Legend:Ave = Average
FORM VI 8082 06/03/2010Page 537 of 623
FORM VII
Lab Name: Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
PCBS CONTINUING CALIBRATION DATA
0.53(mm)
460-13139-1
PESTGC7
05/14/2010 17:55
05/04/2010 16:54
05/04/2010 17:58
CCVRT 460-37531/3
CLP-2
TestAmerica Edison
Lab File ID: of077394.d Conc. Units: ug/L
ANALYTE CURVE AVE RRF RRF MIN RRF CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
PCB-1016 Peak 1 Ave 118.1113.3 1040 1000 4.2 15.0
PCB-1016 Peak 2 Ave 251.8236.5 1060 1000 6.5 15.0
PCB-1016 Peak 3 Ave 131.8110.5 1190 1000 19.3* 15.0
PCB-1016 Peak 4 Ave 469.7428.1 1100 1000 9.7 15.0
PCB-1016 Peak 5 Ave 223.7200.6 1110 1000 11.5 15.0
PCB-1016 Peak 6 Ave 152.6133.2 1150 1000 14.6 15.0
PCB-1016 Peak 7 Ave 155.0154.2 1010 1000 0.5 15.0
PCB-1016 Peak 8 Ave 188.5155.7 1210 1000 21.1* 15.0
PCB-1260 Peak 1 Ave 333.3304.0 1100 1000 9.7 15.0
PCB-1260 Peak 2 Ave 374.5340.2 1100 1000 10.1 15.0
PCB-1260 Peak 3 Ave 542.2483.5 1120 1000 12.1 15.0
PCB-1260 Peak 4 Ave 268.1242.5 1110 1000 10.5 15.0
PCB-1260 Peak 5 Ave 168.4146.4 1150 1000 15.1* 15.0
PCB-1260 Peak 6 Ave 307.0265.9 1150 1000 15.4* 15.0
PCB-1260 Peak 7 Ave 417.6370.6 1130 1000 12.7 15.0
PCB-1260 Peak 8 Ave 148.5125.3 1180 1000 18.5* 15.0
Tetrachloro-m-xylene Ave 56494984 113 100 13.4 15.0
DCB Decachlorobiphenyl Ave 38383478 110 100 10.3 15.0
FORM VII 8082
06/03/2010Page 538 of 623
FORM VII
Lab Name: Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
PCBS CONTINUING CALIBRATION RETENTION TIME SUMMARY
0.53(mm)
460-13139-1
PESTGC7
05/14/2010 17:55
05/04/2010 16:54
05/04/2010 17:58
CCVRT 460-37531/3
CLP-2
TestAmerica Edison
Lab File ID: of077394.d
Analyte RTTO FROM
RT WINDOW
PCB-1016 Peak 1 2.57 2.49 2.63
PCB-1016 Peak 2 3.00 2.92 3.06
PCB-1016 Peak 3 3.27 3.19 3.33
PCB-1016 Peak 4 3.52 3.44 3.58
PCB-1016 Peak 5 3.68 3.60 3.74
PCB-1016 Peak 6 3.97 3.89 4.03
PCB-1016 Peak 7 4.24 4.16 4.30
PCB-1016 Peak 8 4.39 4.31 4.45
PCB-1260 Peak 1 5.84 5.76 5.90
PCB-1260 Peak 2 6.13 6.05 6.19
PCB-1260 Peak 3 6.65 6.58 6.72
PCB-1260 Peak 4 6.81 6.74 6.88
PCB-1260 Peak 5 6.91 6.83 6.97
PCB-1260 Peak 6 7.35 7.28 7.42
PCB-1260 Peak 7 8.77 8.69 8.83
PCB-1260 Peak 8 9.63 9.56 9.70
Tetrachloro-m-xylene 2.09 2.03 2.13
DCB Decachlorobiphenyl 10.21 10.11 10.31
Form VII 8082
06/03/2010Page 539 of 623
FORM VII
Lab Name: Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
PCBS CONTINUING CALIBRATION DATA
0.53(mm)
460-13139-1
PESTGC7
05/14/2010 17:55
05/04/2010 16:54
05/04/2010 17:58
CCVRT 460-37531/3
CLP-1
TestAmerica Edison
Lab File ID: or077394.d Conc. Units: ug/L
ANALYTE CURVE AVE RRF RRF MIN RRF CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
PCB-1016 Peak 1 Ave 74.9275.80 988 1000 -1.2 15.0
PCB-1016 Peak 2 Ave 132.2131.0 1010 1000 0.9 15.0
PCB-1016 Peak 3 Ave 97.0191.55 1060 1000 6.0 15.0
PCB-1016 Peak 4 Ave 267.8248.3 1080 1000 7.8 15.0
PCB-1016 Peak 5 Ave 106.5101.9 1040 1000 4.4 15.0
PCB-1016 Peak 6 Ave 76.4170.04 1090 1000 9.1 15.0
PCB-1016 Peak 7 Ave 112.4106.5 1060 1000 5.6 15.0
PCB-1016 Peak 8 Ave 49.1045.34 1080 1000 8.3 15.0
PCB-1260 Peak 1 Ave 163.1158.6 1030 1000 2.9 15.0
PCB-1260 Peak 2 Ave 288.1278.8 1030 1000 3.4 15.0
PCB-1260 Peak 3 Ave 270.6255.4 1060 1000 5.9 15.0
PCB-1260 Peak 4 Ave 128.4125.3 1030 1000 2.5 15.0
PCB-1260 Peak 5 Ave 132.9129.6 1030 1000 2.6 15.0
PCB-1260 Peak 6 Ave 162.4147.4 1100 1000 10.2 15.0
PCB-1260 Peak 7 Ave 95.3490.23 1060 1000 5.7 15.0
PCB-1260 Peak 8 Ave 84.3973.32 1150 1000 15.1* 15.0
Tetrachloro-m-xylene Ave 29002645 110 100 9.6 15.0
DCB Decachlorobiphenyl Ave 25892415 107 100 7.2 15.0
FORM VII 8082
06/03/2010Page 540 of 623
FORM VII
Lab Name: Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
PCBS CONTINUING CALIBRATION RETENTION TIME SUMMARY
0.53(mm)
460-13139-1
PESTGC7
05/14/2010 17:55
05/04/2010 16:54
05/04/2010 17:58
CCVRT 460-37531/3
CLP-1
TestAmerica Edison
Lab File ID: or077394.d
Analyte RTTO FROM
RT WINDOW
PCB-1016 Peak 1 2.27 2.19 2.33
PCB-1016 Peak 2 2.59 2.51 2.65
PCB-1016 Peak 3 2.78 2.70 2.84
PCB-1016 Peak 4 3.04 2.97 3.11
PCB-1016 Peak 5 3.19 3.11 3.25
PCB-1016 Peak 6 3.25 3.17 3.31
PCB-1016 Peak 7 3.62 3.54 3.68
PCB-1016 Peak 8 3.71 3.64 3.78
PCB-1260 Peak 1 5.02 4.95 5.09
PCB-1260 Peak 2 5.37 5.29 5.43
PCB-1260 Peak 3 5.71 5.64 5.78
PCB-1260 Peak 4 5.85 5.78 5.92
PCB-1260 Peak 5 6.17 6.09 6.23
PCB-1260 Peak 6 7.09 7.02 7.16
PCB-1260 Peak 7 7.24 7.17 7.31
PCB-1260 Peak 8 8.42 8.35 8.49
Tetrachloro-m-xylene 1.98 1.92 2.02
DCB Decachlorobiphenyl 9.28 9.18 9.38
Form VII 8082
06/03/2010Page 541 of 623
FORM VII
Lab Name: Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
PCBS CONTINUING CALIBRATION DATA
0.53(mm)
460-13139-1
PESTGC7
05/15/2010 00:03
05/04/2010 16:54
05/04/2010 17:58
CCV 460-37531/25
CLP-2
TestAmerica Edison
Lab File ID: of077416.d Conc. Units: ug/L
ANALYTE CURVE AVE RRF RRF MIN RRF CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
PCB-1016 Peak 1 Ave 112.7113.3 995 1000 -0.5 15.0
PCB-1016 Peak 2 Ave 243.6236.5 1030 1000 3.0 15.0
PCB-1016 Peak 3 Ave 124.8110.5 1130 1000 13.0 15.0
PCB-1016 Peak 4 Ave 450.4428.1 1050 1000 5.2 15.0
PCB-1016 Peak 5 Ave 213.4200.6 1060 1000 6.4 15.0
PCB-1016 Peak 6 Ave 130.5133.2 980 1000 -2.0 15.0
PCB-1016 Peak 7 Ave 160.3154.2 1040 1000 4.0 15.0
PCB-1016 Peak 8 Ave 164.1155.7 1050 1000 5.4 15.0
PCB-1260 Peak 1 Ave 310.4304.0 1020 1000 2.1 15.0
PCB-1260 Peak 2 Ave 349.7340.2 1030 1000 2.8 15.0
PCB-1260 Peak 3 Ave 504.4483.5 1040 1000 4.3 15.0
PCB-1260 Peak 4 Ave 249.7242.5 1030 1000 2.9 15.0
PCB-1260 Peak 5 Ave 155.0146.4 1060 1000 5.9 15.0
PCB-1260 Peak 6 Ave 283.3265.9 1070 1000 6.5 15.0
PCB-1260 Peak 7 Ave 407.6370.6 1100 1000 10.0 15.0
PCB-1260 Peak 8 Ave 136.7125.3 1090 1000 9.0 15.0
Tetrachloro-m-xylene Ave 53624984 108 100 7.6 15.0
DCB Decachlorobiphenyl Ave 34853478 100 100 0.2 15.0
FORM VII 8082
06/03/2010Page 542 of 623
FORM VII
Lab Name: Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
PCBS CONTINUING CALIBRATION RETENTION TIME SUMMARY
0.53(mm)
460-13139-1
PESTGC7
05/15/2010 00:03
05/04/2010 16:54
05/04/2010 17:58
CCV 460-37531/25
CLP-2
TestAmerica Edison
Lab File ID: of077416.d
Analyte RTTO FROM
RT WINDOW
PCB-1016 Peak 1 2.56 2.49 2.63
PCB-1016 Peak 2 2.99 2.92 3.06
PCB-1016 Peak 3 3.26 3.19 3.33
PCB-1016 Peak 4 3.51 3.44 3.58
PCB-1016 Peak 5 3.67 3.60 3.74
PCB-1016 Peak 6 3.96 3.89 4.03
PCB-1016 Peak 7 4.23 4.16 4.30
PCB-1016 Peak 8 4.38 4.31 4.45
PCB-1260 Peak 1 5.83 5.76 5.90
PCB-1260 Peak 2 6.12 6.05 6.19
PCB-1260 Peak 3 6.64 6.58 6.72
PCB-1260 Peak 4 6.81 6.74 6.88
PCB-1260 Peak 5 6.90 6.83 6.97
PCB-1260 Peak 6 7.34 7.28 7.42
PCB-1260 Peak 7 8.76 8.69 8.83
PCB-1260 Peak 8 9.63 9.56 9.70
Tetrachloro-m-xylene 2.08 2.03 2.13
DCB Decachlorobiphenyl 10.20 10.11 10.31
Form VII 8082
06/03/2010Page 543 of 623
FORM VII
Lab Name: Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
PCBS CONTINUING CALIBRATION DATA
0.53(mm)
460-13139-1
PESTGC7
05/15/2010 00:03
05/04/2010 16:54
05/04/2010 17:58
CCV 460-37531/25
CLP-1
TestAmerica Edison
Lab File ID: or077416.d Conc. Units: ug/L
ANALYTE CURVE AVE RRF RRF MIN RRF CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
PCB-1016 Peak 1 Ave 73.8175.80 974 1000 -2.6 15.0
PCB-1016 Peak 2 Ave 130.6131.0 996 1000 -0.4 15.0
PCB-1016 Peak 3 Ave 96.6391.55 1060 1000 5.5 15.0
PCB-1016 Peak 4 Ave 265.8248.3 1070 1000 7.0 15.0
PCB-1016 Peak 5 Ave 105.7101.9 1040 1000 3.6 15.0
PCB-1016 Peak 6 Ave 75.9670.04 1080 1000 8.5 15.0
PCB-1016 Peak 7 Ave 111.5106.5 1050 1000 4.7 15.0
PCB-1016 Peak 8 Ave 50.4445.34 1110 1000 11.2 15.0
PCB-1260 Peak 1 Ave 160.9158.6 1010 1000 1.5 15.0
PCB-1260 Peak 2 Ave 282.9278.8 1010 1000 1.5 15.0
PCB-1260 Peak 3 Ave 267.1255.4 1050 1000 4.5 15.0
PCB-1260 Peak 4 Ave 126.1125.3 1010 1000 0.6 15.0
PCB-1260 Peak 5 Ave 131.2129.6 1010 1000 1.3 15.0
PCB-1260 Peak 6 Ave 149.5147.4 1010 1000 1.4 15.0
PCB-1260 Peak 7 Ave 98.9690.23 1100 1000 9.7 15.0
PCB-1260 Peak 8 Ave 83.3073.32 1140 1000 13.6 15.0
Tetrachloro-m-xylene Ave 28352645 107 100 7.2 15.0
DCB Decachlorobiphenyl Ave 25772415 107 100 6.7 15.0
FORM VII 8082
06/03/2010Page 544 of 623
FORM VII
Lab Name: Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
PCBS CONTINUING CALIBRATION RETENTION TIME SUMMARY
0.53(mm)
460-13139-1
PESTGC7
05/15/2010 00:03
05/04/2010 16:54
05/04/2010 17:58
CCV 460-37531/25
CLP-1
TestAmerica Edison
Lab File ID: or077416.d
Analyte RTTO FROM
RT WINDOW
PCB-1016 Peak 1 2.27 2.19 2.33
PCB-1016 Peak 2 2.59 2.51 2.65
PCB-1016 Peak 3 2.78 2.70 2.84
PCB-1016 Peak 4 3.04 2.97 3.11
PCB-1016 Peak 5 3.18 3.11 3.25
PCB-1016 Peak 6 3.24 3.17 3.31
PCB-1016 Peak 7 3.61 3.54 3.68
PCB-1016 Peak 8 3.71 3.64 3.78
PCB-1260 Peak 1 5.02 4.95 5.09
PCB-1260 Peak 2 5.36 5.29 5.43
PCB-1260 Peak 3 5.71 5.64 5.78
PCB-1260 Peak 4 5.85 5.78 5.92
PCB-1260 Peak 5 6.16 6.09 6.23
PCB-1260 Peak 6 7.08 7.02 7.16
PCB-1260 Peak 7 7.23 7.17 7.31
PCB-1260 Peak 8 8.42 8.35 8.49
Tetrachloro-m-xylene 1.98 1.92 2.02
DCB Decachlorobiphenyl 9.28 9.18 9.38
Form VII 8082
06/03/2010Page 545 of 623
FORM IForm 1PCBS ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: MB 460-37391/1-A
Matrix: of077395.dLab File ID:
Date Collected:8082Analysis Method:
Solid
TestAmerica Edison
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 07:19
05/14/2010 18:20
N
10(mL)
Sample wt/vol: 15.00(g)
% Moisture:
GC Column: ID: 0.53(mm)CLP-2
Analysis Batch No.: 37531 ug/KgUnits:
SURROGATE %RECCAS NO. LIMITS Q
2051-24-3 DCB Decachlorobiphenyl 98 27-165
FORM I 8082
06/03/2010Page 546 of 623
Data File: of077395.d Report Date: 16-May-2010 18:32
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC7.i/8082/front/May10/05-14-10/14may10a.b/of077395.dLab Smp Id: MB 460-37391/1-A Inj Date : 14-MAY-2010 18:20 Operator : 615 Inst ID: PESTGC7.iSmp Info : MB 460-37391/1-AMisc Info : Comment : Method : /chem1/PESTGC7.i/8082/front/May10/05-14-10/14may10a.b/08Of8082.mMeth Date : 05-May-2010 00:12 diazc Quant Type: ESTDCal Date : 04-MAY-2010 19:52 Cal File: of077121.dAls bottle: 4 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: AllPCB.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (mL)Ws 15.00000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 30 Decachlorobiphenyl(surr) CAS #: 2051-24-3
10.212 10.205 0.007 169651 48.7738 32 80.00- 120.00 100.00
-------------------------------------------------------------------------------
06/03/2010Page 547 of 623
Data File: of077395.d
Date: 14-MAY-2010 18:20
Client ID: Instrument: PESTGC7.i
Sample Info: MB 460-37391/1-A Operator: 615
06/03/2010Page 548 of 623
FORM IForm 1PCBS ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: MB 460-37391/1-A
Matrix: or077395.dLab File ID:
Date Collected:8082Analysis Method:
Solid
TestAmerica Edison
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 07:19
05/14/2010 18:20
N
10(mL)
Sample wt/vol: 15.00(g)
% Moisture:
GC Column: ID: 0.53(mm)CLP-1
Analysis Batch No.: 37531 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Aroclor 101612674-11-2 67 67 13U
Aroclor 122111104-28-2 67 67 20U
Aroclor 123211141-16-5 67 67 38U
Aroclor 124253469-21-9 67 67 13U
Aroclor 124812672-29-6 67 67 18U
Aroclor 125411097-69-1 67 67 23U
Aroclor 126011096-82-5 67 67 7.5U
Aroclor 126237324-23-5 67 67 12U
Aroclor 126811100-14-4 67 67 12U
SURROGATE %RECCAS NO. LIMITS Q
2051-24-3 DCB Decachlorobiphenyl 94 27-165
FORM I 8082
06/03/2010Page 549 of 623
Data File: or077395.d Page 1 Report Date: 16-May-2010 18:32
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC7.i/8082/rear/May10/05-14-10/14may10a.b/or077395.dLab Smp Id: MB 460-37391/1-A Inj Date : 14-MAY-2010 18:20 Operator : 615 Inst ID: PESTGC7.iSmp Info : MB 460-37391/1-AMisc Info : Comment : Method : /chem1/PESTGC7.i/8082/rear/May10/05-14-10/14may10a.b/08Or8082.mMeth Date : 05-May-2010 00:19 diazc Quant Type: ESTDCal Date : 04-MAY-2010 19:52 Cal File: or077121.dAls bottle: 4 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: AllPCB.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (mL)Ws 15.00000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
$ 30 Decachlorobiphenyl(surr) CAS #: 2051-24-3
9.280 9.278 0.002 113769 47.1083 80.00- 120.00 100.00(aR)
-------------------------------------------------------------------------------
QC Flag Legend
a - Target compound detected but, quantitated amountBelow Limit Of Quantitation(BLOQ).
R - Spike/Surrogate failed recovery limits.
06/03/2010Page 550 of 623
Data File: or077395.d
Date: 14-MAY-2010 18:20
Client ID: Instrument: PESTGC7.i
Sample Info: MB 460-37391/1-A Operator: 615
06/03/2010Page 551 of 623
FORM IForm 1PCBS ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: LCS 460-37391/2-A
Matrix: of077396.dLab File ID:
Date Collected:8082Analysis Method:
Solid
TestAmerica Edison
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 07:19
05/14/2010 18:37
N
10(mL)
Sample wt/vol: 15.00(g)
% Moisture:
GC Column: ID: 0.53(mm)CLP-2
Analysis Batch No.: 37531 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Aroclor 101612674-11-2 316 67 13
Aroclor 122111104-28-2 67 67 20U
Aroclor 123211141-16-5 67 67 38U
Aroclor 124253469-21-9 67 67 13U
Aroclor 124812672-29-6 67 67 18U
Aroclor 125411097-69-1 67 67 23U
Aroclor 126011096-82-5 328 67 7.5
Aroclor 126237324-23-5 67 67 12U
Aroclor 126811100-14-4 67 67 12U
SURROGATE %RECCAS NO. LIMITS Q
2051-24-3 DCB Decachlorobiphenyl 104 27-165
FORM I 8082
06/03/2010Page 552 of 623
Data File: of077396.d Report Date: 16-May-2010 18:32
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC7.i/8082/front/May10/05-14-10/14may10a.b/of077396.dLab Smp Id: LCS 460-37391/2-A Inj Date : 14-MAY-2010 18:37 Operator : 615 Inst ID: PESTGC7.iSmp Info : LCS 460-37391/2-AMisc Info : Comment : Method : /chem1/PESTGC7.i/8082/front/May10/05-14-10/14may10a.b/08Of8082.mMeth Date : 05-May-2010 00:12 diazc Quant Type: ESTDCal Date : 04-MAY-2010 19:52 Cal File: of077121.dAls bottle: 5 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: AllPCB.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (mL)Ws 15.00000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
21 Aroclor-1016 CAS #: 12674-11-2
2.570 2.555 0.015 48413 427.392 280 80.00- 120.00 100.00(M)
3.005 2.990 0.015 109671 463.790 310 154.12- 231.18 226.53
3.268 3.255 0.013 54836 496.456 330 80.74- 121.11 113.27
3.517 3.505 0.012 196527 459.119 310 297.01- 445.51 405.94
3.677 3.665 0.012 95218 474.578 320 139.34- 209.02 196.68
3.967 3.955 0.012 65663 492.949 330 83.83- 125.74 135.63
4.238 4.227 0.011 71216 461.817 310 96.10- 144.15 147.10
4.390 4.380 0.010 80281 515.703 340 119.05- 178.58 165.83
Average of Peak Concentrations = 320
-------------------------------------------------------------------------------
27 Aroclor-1260 CAS #: 11096-82-5
5.838 5.832 0.006 150452 494.905 330 80.00- 120.00 100.00(M)
06/03/2010Page 553 of 623
Data File: of077396.d Report Date: 16-May-2010 18:32
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
27 Aroclor-1260 (continued)
6.125 6.118 0.007 168663 495.842 330 89.81- 134.72 112.10
6.653 6.645 0.008 231224 478.217 320 132.01- 198.02 153.69
6.815 6.807 0.008 119847 494.115 330 64.57- 96.85 79.66
6.908 6.900 0.008 75364 514.870 340 40.81- 61.21 50.09
7.353 7.345 0.008 131515 494.546 330 73.71- 110.57 87.41
8.765 8.758 0.007 175999 474.892 320 102.65- 153.97 116.98
9.632 9.627 0.005 61568 491.267 330 35.41- 53.12 40.92
Average of Peak Concentrations = 330
-------------------------------------------------------------------------------
$ 30 Decachlorobiphenyl(surr) CAS #: 2051-24-3
10.207 10.205 0.002 180882 52.0026 35 80.00- 120.00 100.00
-------------------------------------------------------------------------------
QC Flag Legend
M - Compound response manually integrated.
06/03/2010Page 554 of 623
Data File: of077396.d
Date: 14-MAY-2010 18:37
Client ID: Instrument: PESTGC7.i
Sample Info: LCS 460-37391/2-A Operator: 615
06/03/2010Page 555 of 623
Manual Integration Report
Data File: of077396.dInj. Date and Time: 14-MAY-2010 18:37Instrument ID: PESTGC7.iClient ID: Compound: 21 Aroclor-1016CAS #: 12674-11-2Report Date: 05/16/2010
Processing Integration Results
Not Detected
Expected RT: 2.56
Manual Integration Results
RT: 2.57
Response: 48413
Amount: 473.98
Conc: 320.00
Manually Integrated By: diazcManual Integration Reason: Baseline Event
06/03/2010Page 556 of 623
Manual Integration Report
Data File: of077396.dInj. Date and Time: 14-MAY-2010 18:37Instrument ID: PESTGC7.iClient ID: Compound: 27 Aroclor-1260CAS #: 11096-82-5Report Date: 05/16/2010
Processing Integration Results
Not Detected
Expected RT: 5.83
Manual Integration Results
RT: 5.84
Response: 150452
Amount: 492.33
Conc: 330.00
Manually Integrated By: diazcManual Integration Reason: Baseline Event
06/03/2010Page 557 of 623
FORM IForm 1PCBS ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: LCS 460-37391/2-A
Matrix: or077396.dLab File ID:
Date Collected:8082Analysis Method:
Solid
TestAmerica Edison
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 07:19
05/14/2010 18:37
N
10(mL)
Sample wt/vol: 15.00(g)
% Moisture:
GC Column: ID: 0.53(mm)CLP-1
Analysis Batch No.: 37531 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Aroclor 101612674-11-2 278 67 13
Aroclor 122111104-28-2 67 67 20U
Aroclor 123211141-16-5 67 67 38U
Aroclor 124253469-21-9 67 67 13U
Aroclor 124812672-29-6 67 67 18U
Aroclor 125411097-69-1 67 67 23U
Aroclor 126011096-82-5 314 67 7.5
Aroclor 126237324-23-5 67 67 12U
Aroclor 126811100-14-4 67 67 12U
SURROGATE %RECCAS NO. LIMITS Q
2051-24-3 DCB Decachlorobiphenyl 110 27-165
FORM I 8082
06/03/2010Page 558 of 623
Data File: or077396.d Page 1 Report Date: 16-May-2010 18:32
TestAmerica
GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC7.i/8082/rear/May10/05-14-10/14may10a.b/or077396.dLab Smp Id: LCS 460-37391/2-A Inj Date : 14-MAY-2010 18:37 Operator : 615 Inst ID: PESTGC7.iSmp Info : LCS 460-37391/2-AMisc Info : Comment : Method : /chem1/PESTGC7.i/8082/rear/May10/05-14-10/14may10a.b/08Or8082.mMeth Date : 05-May-2010 00:19 diazc Quant Type: ESTDCal Date : 04-MAY-2010 19:52 Cal File: or077121.dAls bottle: 5 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: AllPCB.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3
Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable
Name Value Description-------------- -------------- -----------------------
DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (mL)Ws 15.00000 Weight of sample extracted (g)M 0.00000 % Moisture
Cpnd Variable Local Compound Variable
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
21 Aroclor-1016 CAS #: 12674-11-2
2.275 2.263 0.012 29358 387.298 80.00- 120.00 100.00(aM)
2.592 2.582 0.010 54887 418.878 136.06- 204.09 186.96
2.782 2.772 0.010 38222 417.507 104.24- 156.37 130.19
3.043 3.035 0.008 107031 431.011 287.29- 430.94 364.57
3.187 3.177 0.010 43575 427.434 111.70- 167.55 148.43
3.247 3.238 0.009 28586 408.154 85.92- 128.89 97.37
3.617 3.610 0.007 46506 436.619 117.81- 176.71 158.41
3.713 3.707 0.006 18656 411.488 52.60- 78.90 63.55
-------------------------------------------------------------------------------
27 Aroclor-1260 CAS #: 11096-82-5
5.023 5.018 0.005 73720 464.912 80.00- 120.00 100.00(a)
5.365 5.362 0.003 128572 461.189 140.97- 211.46 174.41
06/03/2010Page 559 of 623
Data File: or077396.d Page 2 Report Date: 16-May-2010 18:32
CONCENTRATIONS
ON-COL FINAL
RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO
== ====== ======== ======== ======= ======= ============ =====
27 Aroclor-1260 (continued)
5.712 5.707 0.005 116240 455.056 136.60- 204.90 157.68
5.852 5.848 0.004 58772 469.072 64.85- 97.27 79.72
6.165 6.163 0.002 58784 453.622 68.41- 102.62 79.74
7.088 7.085 0.003 64104 434.847 84.22- 126.34 86.96
7.238 7.237 0.001 47649 528.087 53.50- 80.26 64.64
8.425 8.422 0.003 36769 501.510 45.63- 68.45 49.88
-------------------------------------------------------------------------------
$ 30 Decachlorobiphenyl(surr) CAS #: 2051-24-3
9.278 9.278 0.000 132329 54.7934 80.00- 120.00 100.00(aR)
-------------------------------------------------------------------------------
QC Flag Legend
a - Target compound detected but, quantitated amountBelow Limit Of Quantitation(BLOQ).
R - Spike/Surrogate failed recovery limits.M - Compound response manually integrated.
06/03/2010Page 560 of 623
Data File: or077396.d
Date: 14-MAY-2010 18:37
Client ID: Instrument: PESTGC7.i
Sample Info: LCS 460-37391/2-A Operator: 615
06/03/2010Page 561 of 623
Manual Integration Report
Data File: or077396.dInj. Date and Time: 14-MAY-2010 18:37Instrument ID: PESTGC7.iClient ID: Compound: 21 Aroclor-1016CAS #: 12674-11-2Report Date: 05/16/2010
Processing Integration Results
Not Detected
Expected RT: 2.26
Manual Integration Results
RT: 2.27
Response: 29358
Amount: 417.30
Conc: 0.00
Manually Integrated By: diazcManual Integration Reason: Baseline Event
06/03/2010Page 562 of 623
FORM IForm 1PCBS ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: 460-13137-A-1-B MS
Matrix: of077398.dLab File ID:
Date Collected:8082Analysis Method:
Solid
TestAmerica Edison
05/12/2010 09:50
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 07:19
05/14/2010 19:09
N
10(mL)
Sample wt/vol: 15.03(g)
% Moisture: 3.0
GC Column: ID: 0.53(mm)CLP-2
Analysis Batch No.: 37531 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Aroclor 101612674-11-2 357 69 13
Aroclor 122111104-28-2 69 69 21U
Aroclor 123211141-16-5 69 69 39U
Aroclor 124253469-21-9 69 69 13U
Aroclor 124812672-29-6 69 69 18U
Aroclor 125411097-69-1 69 69 24U
Aroclor 126011096-82-5 362 69 7.7
Aroclor 126237324-23-5 69 69 12U
Aroclor 126811100-14-4 69 69 12U
SURROGATE %RECCAS NO. LIMITS Q
2051-24-3 DCB Decachlorobiphenyl 108 27-165
FORM I 8082
06/03/2010Page 563 of 623
FORM IForm 1PCBS ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: 460-13137-A-1-B MS
Matrix: or077398.dLab File ID:
Date Collected:8082Analysis Method:
Solid
TestAmerica Edison
05/12/2010 09:50
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 07:19
05/14/2010 19:09
N
10(mL)
Sample wt/vol: 15.03(g)
% Moisture: 3.0
GC Column: ID: 0.53(mm)CLP-1
Analysis Batch No.: 37531 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Aroclor 101612674-11-2 321 69 13
Aroclor 122111104-28-2 69 69 21U
Aroclor 123211141-16-5 69 69 39U
Aroclor 124253469-21-9 69 69 13U
Aroclor 124812672-29-6 69 69 18U
Aroclor 125411097-69-1 69 69 24U
Aroclor 126011096-82-5 331 69 7.7
Aroclor 126237324-23-5 69 69 12U
Aroclor 126811100-14-4 69 69 12U
SURROGATE %RECCAS NO. LIMITS Q
2051-24-3 DCB Decachlorobiphenyl 106 27-165
FORM I 8082
06/03/2010Page 564 of 623
FORM IForm 1PCBS ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: 460-13137-A-1-C MSD
Matrix: of077399.dLab File ID:
Date Collected:8082Analysis Method:
Solid
TestAmerica Edison
05/12/2010 09:50
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 07:19
05/14/2010 19:26
N
10(mL)
Sample wt/vol: 15.02(g)
% Moisture: 3.0
GC Column: ID: 0.53(mm)CLP-2
Analysis Batch No.: 37531 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Aroclor 101612674-11-2 364 69 13
Aroclor 122111104-28-2 69 69 21U
Aroclor 123211141-16-5 69 69 39U
Aroclor 124253469-21-9 69 69 13U
Aroclor 124812672-29-6 69 69 18U
Aroclor 125411097-69-1 69 69 24U
Aroclor 126011096-82-5 376 69 7.7
Aroclor 126237324-23-5 69 69 12U
Aroclor 126811100-14-4 69 69 12U
SURROGATE %RECCAS NO. LIMITS Q
2051-24-3 DCB Decachlorobiphenyl 91 27-165
FORM I 8082
06/03/2010Page 565 of 623
FORM IForm 1PCBS ORGANICS ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG No.:
460-13139-1
Lab Sample ID: 460-13137-A-1-C MSD
Matrix: or077399.dLab File ID:
Date Collected:8082Analysis Method:
Solid
TestAmerica Edison
05/12/2010 09:50
Con. Extract Vol.:Volume:Injection Volume:
GPC Cleanup:(Y/N)
Date Extracted:
Date Analyzed:
Dilution Factor: 1
Extraction Method: 3541 05/14/2010 07:19
05/14/2010 19:26
N
10(mL)
Sample wt/vol: 15.02(g)
% Moisture: 3.0
GC Column: ID: 0.53(mm)CLP-1
Analysis Batch No.: 37531 ug/KgUnits:
CAS NO. COMPOUND NAME RESULT Q MDLRL
Aroclor 101612674-11-2 335 69 13
Aroclor 122111104-28-2 69 69 21U
Aroclor 123211141-16-5 69 69 39U
Aroclor 124253469-21-9 69 69 13U
Aroclor 124812672-29-6 69 69 18U
Aroclor 125411097-69-1 69 69 24U
Aroclor 126011096-82-5 343 69 7.7
Aroclor 126237324-23-5 69 69 12U
Aroclor 126811100-14-4 69 69 12U
SURROGATE %RECCAS NO. LIMITS Q
2051-24-3 DCB Decachlorobiphenyl 91 27-165
FORM I 8082
06/03/2010Page 566 of 623
Lab Name: Job No.:
SDG No.:
Instrument ID:
Analysis Batch Number:
PCBS ANALYSIS RUN LOG
DILUTION
FACTOR
COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID
TestAmerica Edison 460-13139-1
PESTGC7
36537
Start Date:
End Date: 05/04/2010 20:08
05/04/2010 16:04
ZZZZZ CLP-2 0.53(mm)105/04/2010 16:04
ZZZZZ CLP-1 0.53(mm)105/04/2010 16:04
PIBLK 460-36537/2 CLP-2 0.53(mm)105/04/2010 16:21
PIBLK 460-36537/2 CLP-1 0.53(mm)105/04/2010 16:21
ZZZZZ CLP-2 0.53(mm)105/04/2010 16:37
ZZZZZ CLP-1 0.53(mm)105/04/2010 16:37
IC 460-36537/4 CLP-2 0.53(mm)105/04/2010 16:54 of077110.d
IC 460-36537/4 CLP-1 0.53(mm)105/04/2010 16:54 or077110.d
IC 460-36537/5 CLP-2 0.53(mm)105/04/2010 17:10 of077111.d
IC 460-36537/5 CLP-1 0.53(mm)105/04/2010 17:10 or077111.d
IC 460-36537/6 CLP-2 0.53(mm)105/04/2010 17:26 of077112.d
IC 460-36537/6 CLP-1 0.53(mm)105/04/2010 17:26 or077112.d
IC 460-36537/7 CLP-2 0.53(mm)105/04/2010 17:42 of077113.d
IC 460-36537/7 CLP-1 0.53(mm)105/04/2010 17:42 or077113.d
IC 460-36537/8 CLP-2 0.53(mm)105/04/2010 17:58 of077114.d
IC 460-36537/8 CLP-1 0.53(mm)105/04/2010 17:58 or077114.d
IC 460-36537/9 CLP-2 0.53(mm)105/04/2010 18:15 of077115.d
IC 460-36537/9 CLP-1 0.53(mm)105/04/2010 18:15 or077115.d
IC 460-36537/10 CLP-2 0.53(mm)105/04/2010 18:31 of077116.d
IC 460-36537/10 CLP-1 0.53(mm)105/04/2010 18:31 or077116.d
IC 460-36537/11 CLP-2 0.53(mm)105/04/2010 18:47 of077117.d
IC 460-36537/11 CLP-1 0.53(mm)105/04/2010 18:47 or077117.d
IC 460-36537/12 CLP-2 0.53(mm)105/04/2010 19:03 of077118.d
IC 460-36537/12 CLP-1 0.53(mm)105/04/2010 19:03 or077118.d
IC 460-36537/13 CLP-2 0.53(mm)105/04/2010 19:19 of077119.d
IC 460-36537/13 CLP-1 0.53(mm)105/04/2010 19:19 or077119.d
IC 460-36537/14 CLP-2 0.53(mm)105/04/2010 19:36 of077120.d
IC 460-36537/14 CLP-1 0.53(mm)105/04/2010 19:36 or077120.d
IC 460-36537/15 CLP-2 0.53(mm)105/04/2010 19:52 of077121.d
IC 460-36537/15 CLP-1 0.53(mm)105/04/2010 19:52 or077121.d
ZZZZZ CLP-2 0.53(mm)105/04/2010 20:08
ZZZZZ CLP-1 0.53(mm)105/04/2010 20:08
8082
06/03/2010Page 567 of 623
Lab Name: Job No.:
SDG No.:
Instrument ID:
Analysis Batch Number:
PCBS ANALYSIS RUN LOG
DILUTION
FACTOR
COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID
TestAmerica Edison 460-13139-1
PESTGC7
37531
Start Date:
End Date: 05/15/2010 00:03
05/14/2010 17:22
RINSE 460-37531/1 CLP-2 0.53(mm)105/14/2010 17:22
RINSE 460-37531/1 CLP-1 0.53(mm)105/14/2010 17:22
PIBLK 460-37531/2 CLP-2 0.53(mm)105/14/2010 17:39
PIBLK 460-37531/2 CLP-1 0.53(mm)105/14/2010 17:39
CCVRT 460-37531/3 CLP-2 0.53(mm)105/14/2010 17:55 of077394.d
CCVRT 460-37531/3 CLP-1 0.53(mm)105/14/2010 17:55 or077394.d
MB 460-37391/1-A CLP-2 0.53(mm)105/14/2010 18:20 of077395.d
MB 460-37391/1-A CLP-1 0.53(mm)105/14/2010 18:20 or077395.d
LCS 460-37391/2-A CLP-2 0.53(mm)105/14/2010 18:37 of077396.d
LCS 460-37391/2-A CLP-1 0.53(mm)105/14/2010 18:37 or077396.d
ZZZZZ CLP-2 0.53(mm)105/14/2010 18:53
ZZZZZ CLP-1 0.53(mm)105/14/2010 18:53
460-13137-A-1-B MS CLP-2 0.53(mm)105/14/2010 19:09 of077398.d
460-13137-A-1-B MS CLP-1 0.53(mm)105/14/2010 19:09 or077398.d
460-13137-A-1-C MSD CLP-2 0.53(mm)105/14/2010 19:26 of077399.d
460-13137-A-1-C MSD CLP-1 0.53(mm)105/14/2010 19:26 or077399.d
ZZZZZ CLP-2 0.53(mm)105/14/2010 19:43
ZZZZZ CLP-1 0.53(mm)105/14/2010 19:43
460-13139-2 TB-3 6-7 CLP-2 0.53(mm)105/14/2010 19:59 of077401.d
460-13139-2 TB-3 6-7 CLP-1 0.53(mm)105/14/2010 19:59 or077401.d
ZZZZZ CLP-2 0.53(mm)105/14/2010 20:15
ZZZZZ CLP-1 0.53(mm)105/14/2010 20:15
460-13139-4 TB-2 5-6 CLP-2 0.53(mm)105/14/2010 20:32 of077403.d
460-13139-4 TB-2 5-6 CLP-1 0.53(mm)105/14/2010 20:32 or077403.d
460-13139-5 TB-1 2-3 CLP-2 0.53(mm)105/14/2010 20:48 of077404.d
460-13139-5 TB-1 2-3 CLP-1 0.53(mm)105/14/2010 20:48 or077404.d
ZZZZZ CLP-2 0.53(mm)105/14/2010 21:05
ZZZZZ CLP-1 0.53(mm)105/14/2010 21:05
460-13139-7 TB-5 3-4 CLP-2 0.53(mm)105/14/2010 21:21 of077406.d
460-13139-7 TB-5 3-4 CLP-1 0.53(mm)105/14/2010 21:21 or077406.d
ZZZZZ CLP-2 0.53(mm)105/14/2010 21:38
ZZZZZ CLP-1 0.53(mm)105/14/2010 21:38
ZZZZZ CLP-2 0.53(mm)105/14/2010 21:54
ZZZZZ CLP-1 0.53(mm)105/14/2010 21:54
ZZZZZ CLP-2 0.53(mm)105/14/2010 22:10
ZZZZZ CLP-1 0.53(mm)105/14/2010 22:10
ZZZZZ CLP-2 0.53(mm)105/14/2010 22:27
ZZZZZ CLP-1 0.53(mm)105/14/2010 22:27
ZZZZZ CLP-2 0.53(mm)105/14/2010 22:43
ZZZZZ CLP-1 0.53(mm)105/14/2010 22:43
ZZZZZ CLP-2 0.53(mm)105/14/2010 22:58
ZZZZZ CLP-1 0.53(mm)105/14/2010 22:58
ZZZZZ CLP-2 0.53(mm)105/14/2010 23:15
ZZZZZ CLP-1 0.53(mm)105/14/2010 23:15
ZZZZZ CLP-2 0.53(mm)105/14/2010 23:31
8082
06/03/2010Page 568 of 623
Lab Name: Job No.:
SDG No.:
Instrument ID:
Analysis Batch Number:
PCBS ANALYSIS RUN LOG
DILUTION
FACTOR
COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID
TestAmerica Edison 460-13139-1
PESTGC7
37531
Start Date:
End Date: 05/15/2010 00:03
05/14/2010 17:22
ZZZZZ CLP-1 0.53(mm)105/14/2010 23:31
PIBLK 460-37531/24 CLP-2 0.53(mm)105/14/2010 23:47
PIBLK 460-37531/24 CLP-1 0.53(mm)105/14/2010 23:47
CCV 460-37531/25 CLP-2 0.53(mm)105/15/2010 00:03 of077416.d
CCV 460-37531/25 CLP-1 0.53(mm)105/15/2010 00:03 or077416.d
8082
06/03/2010Page 569 of 623
Organic Prep Worksheet
Method: 3541
Analyst: Alinea, Archilles R
Batch Number: 460-37391 Date Open:
Batch End:
May 14 2010 7:19AM
May 14 2010 2:30PM
Lab ID Client ID Basis Final weight/volume of
sample
Position on the
SoxTherm
OP_PCBSP_00013 OPPSTPCBSU_00014Initial weight/volume of
sample
Method Chain
MB~460-37391/1 15.00 g 10 mL 50 uL733541, 8082
LCS~460-37391/2 15.00 g 10 mL 50 uL50 uL743541, 8082
460-13137-A-1~MS T 15.03 g 10 mL 50 uL50 uL753541, 8082
460-13137-A-1~MS
D
T 15.02 g 10 mL 50 uL50 uL763541, 8082
460-13139-E-1 TB-3 2-3 T 15.04 g 10 mL 50 uL77
460-13139-E-2 TB-3 6-7 T 15.00 g 10 mL 50 uL783541, 8082
460-13139-E-3 TB-2 2-3 T 15.05 g 10 mL 50 uL79
460-13139-E-4 TB-2 5-6 T 15.03 g 10 mL 50 uL803541, 8082
460-13139-E-5 TB-1 2-3 T 15.02 g 10 mL 50 uL813541, 8082
460-13139-E-6 TB-1 5-6 T 15.04 g 10 mL 50 uL82
460-13139-E-7 TB-5 3-4 T 15.02 g 10 mL 50 uL833541, 8082
460-13139-E-8 TB-4 6-7 T 15.01 g 10 mL 50 uL84
460-13137-A-1 T 15.00 g 10 mL 50 uL85
460-13137-A-2 T 15.02 g 10 mL 50 uL86
460-13137-A-3 T 15.03 g 10 mL 50 uL87
460-13137-A-4 T 15.03 g 10 mL 50 uL88
460-13137-A-5 T 15.02 g 10 mL 50 uL89
460-13137-A-6 T 15.01 g 10 mL 50 uL90
460-13137-A-7 T 15.00 g 10 mL 50 uL97
460-13137-A-8 T 15.04 g 10 mL 50 uL98
460-13146-G-1 T 15.01 g 10 mL 50 uL99
460-13147-A-1 T 15.03 g 10 mL 50 uL100
460-13147-B-2 T 15.02 g 10 mL 50 uL101
460-13148-B-1 T 15.05 g 10 mL 50 uL102
First Start time: 719am
Person's name who did the prep: archie
Person's name who witnessed reagent drop: juan r
First End time: 230pm
SOP Number: 3541
Balance ID: 30
Na2SO4 Lot Number: h39602
Solvent: hex./ace. mixed
Vendor lot number: h35e09
Blank Soil Lot Number: h39602
Florisil Lot #: n/a
TBA Lot #: op083
06/03/2010Page 570 of 623
Organic Prep Worksheet
Method: 3541
Analyst: Alinea, Archilles R
Batch Number: 460-37391 Date Open:
Batch End:
May 14 2010 7:19AM
May 14 2010 2:30PM
Lab ID Client ID Basis
Comments
Analysis commentMethod Chain
MB~460-37391/1 3541, 8082
LCS~460-37391/2 3541, 8082
460-13137-A-1~MS T3541, 8082
460-13137-A-1~MS
D
T3541, 8082
460-13139-E-1 TB-3 2-3 T
460-13139-E-2 TB-3 6-7 T3541, 8082
460-13139-E-3 TB-2 2-3 T
460-13139-E-4 TB-2 5-6 T3541, 8082
460-13139-E-5 TB-1 2-3 T3541, 8082
460-13139-E-6 TB-1 5-6 T
460-13139-E-7 TB-5 3-4 T3541, 8082
460-13139-E-8 TB-4 6-7 T
460-13137-A-1 T
460-13137-A-2 T
460-13137-A-3 T
460-13137-A-4 T
460-13137-A-5 T
460-13137-A-6 T
460-13137-A-7 T
460-13137-A-8 T
460-13146-G-1 T
460-13147-A-1 T
460-13147-B-2 T
460-13148-B-1 T
Batch Comment: pcb-soil
06/03/2010Page 571 of 623
METALS
06/03/2010Page 572 of 623
COVER PAGE
Lab Name: Job Number:
Client Sample ID Lab Sample ID
METALS
Project: Dumont Fields - Twin Boro
SDG No.:
460-13139-1TestAmerica Edison
TB-3 6-7 460-13139-2
TB-2 5-6 460-13139-4
TB-1 2-3 460-13139-5
TB-5 3-4 460-13139-7
Comments:
06/03/2010Page 573 of 623
1A-IN
INORGANIC ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG ID.:
Matrix:
Lab Sample ID: 460-13139-2
Date Received: 05/13/2010 18:30
460-13139-1
TB-3 6-7
Soil 05/12/2010 09:45Date Sampled:
Reporting Basis: DRY
METALS
TestAmerica Edison
% Solids: 81.2
CAS No. Analyte Conc. CUnits Q MethodRL MDL DIL
7440-36-0 Antimony 2.3 Umg/Kg2.3 1.0 4 6010B
7440-38-2 Arsenic 1.9 mg/Kg1.2 0.81 4 6010B
7440-41-7 Beryllium 0.20 Jmg/Kg0.46 0.20 4 6010B
7440-43-9 Cadmium 1.2 Umg/Kg1.2 0.18 4 6010B
7440-47-3 Chromium 9.1 mg/Kg2.3 1.4 4 6010B
7440-50-8 Copper 13.9 mg/Kg5.8 0.95 4 6010B
7439-92-1 Lead 17.5 mg/Kg1.2 0.58 4 6010B
7440-02-0 Nickel 7.0 Jmg/Kg9.3 0.62 4 6010B
7782-49-2 Selenium 2.3 Umg/Kg2.3 1.1 4 6010B
7440-22-4 Silver 2.3 Umg/Kg2.3 0.18 4 6010B
7440-28-0 Thallium 2.3 Umg/Kg2.3 1.1 4 6010B
7440-66-6 Zinc 31.3 mg/Kg7.0 1.1 4 6010B
7439-97-6 Mercury 0.039 Umg/Kg0.039 0.030 1 7471A
FORM IA-IN 06/03/2010Page 574 of 623
1A-IN
INORGANIC ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG ID.:
Matrix:
Lab Sample ID: 460-13139-4
Date Received: 05/13/2010 18:30
460-13139-1
TB-2 5-6
Soil 05/12/2010 10:45Date Sampled:
Reporting Basis: DRY
METALS
TestAmerica Edison
% Solids: 87.2
CAS No. Analyte Conc. CUnits Q MethodRL MDL DIL
7440-36-0 Antimony 2.3 Umg/Kg2.3 1.0 4 6010B
7440-38-2 Arsenic 4.5 mg/Kg1.1 0.80 4 6010B
7440-41-7 Beryllium 0.37 Jmg/Kg0.46 0.20 4 6010B
7440-43-9 Cadmium 0.98 Jmg/Kg1.1 0.18 4 6010B
7440-47-3 Chromium 17.9 mg/Kg2.3 1.4 4 6010B
7440-50-8 Copper 71.8 mg/Kg5.7 0.94 4 6010B
7439-92-1 Lead 251 mg/Kg1.1 0.57 4 6010B
7440-02-0 Nickel 11.9 mg/Kg9.2 0.61 4 6010B
7782-49-2 Selenium 2.3 Umg/Kg2.3 1.1 4 6010B
7440-22-4 Silver 4.9 mg/Kg B2.3 0.17 4 6010B
7440-28-0 Thallium 2.3 Umg/Kg2.3 1.1 4 6010B
7440-66-6 Zinc 137 mg/Kg6.9 1.1 4 6010B
7439-97-6 Mercury 0.22 mg/Kg0.035 0.028 1 7471A
FORM IA-IN 06/03/2010Page 575 of 623
1A-IN
INORGANIC ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG ID.:
Matrix:
Lab Sample ID: 460-13139-5
Date Received: 05/13/2010 18:30
460-13139-1
TB-1 2-3
Soil 05/12/2010 11:25Date Sampled:
Reporting Basis: DRY
METALS
TestAmerica Edison
% Solids: 93.5
CAS No. Analyte Conc. CUnits Q MethodRL MDL DIL
7440-36-0 Antimony 2.0 Umg/Kg2.0 0.89 4 6010B
7440-38-2 Arsenic 1.4 mg/Kg1.0 0.70 4 6010B
7440-41-7 Beryllium 0.40 Umg/Kg0.40 0.18 4 6010B
7440-43-9 Cadmium 1.0 Umg/Kg1.0 0.16 4 6010B
7440-47-3 Chromium 4.6 mg/Kg2.0 1.2 4 6010B
7440-50-8 Copper 7.2 mg/Kg5.0 0.82 4 6010B
7439-92-1 Lead 7.9 mg/Kg1.0 0.50 4 6010B
7440-02-0 Nickel 5.4 Jmg/Kg8.1 0.54 4 6010B
7782-49-2 Selenium 2.0 Umg/Kg2.0 0.94 4 6010B
7440-22-4 Silver 2.0 Umg/Kg2.0 0.15 4 6010B
7440-28-0 Thallium 2.0 Umg/Kg2.0 0.98 4 6010B
7440-66-6 Zinc 19.2 mg/Kg6.1 0.99 4 6010B
7439-97-6 Mercury 0.035 Umg/Kg0.035 0.028 1 7471A
FORM IA-IN 06/03/2010Page 576 of 623
1A-IN
INORGANIC ANALYSIS DATA SHEET
Client Sample ID:
Lab Name: Job No.:
SDG ID.:
Matrix:
Lab Sample ID: 460-13139-7
Date Received: 05/13/2010 18:30
460-13139-1
TB-5 3-4
Soil 05/12/2010 12:30Date Sampled:
Reporting Basis: DRY
METALS
TestAmerica Edison
% Solids: 38.5
CAS No. Analyte Conc. CUnits Q MethodRL MDL DIL
7440-36-0 Antimony 5.1 Umg/Kg5.1 2.2 4 6010B
7440-38-2 Arsenic 3.2 mg/Kg2.5 1.8 4 6010B
7440-41-7 Beryllium 1.0 Umg/Kg1.0 0.45 4 6010B
7440-43-9 Cadmium 1.1 Jmg/Kg2.5 0.40 4 6010B
7440-47-3 Chromium 6.7 mg/Kg5.1 3.0 4 6010B
7440-50-8 Copper 22.0 mg/Kg12.7 2.1 4 6010B
7439-92-1 Lead 222 mg/Kg2.5 1.3 4 6010B
7440-02-0 Nickel 7.0 Jmg/Kg20.4 1.4 4 6010B
7782-49-2 Selenium 5.1 Umg/Kg5.1 2.4 4 6010B
7440-22-4 Silver 5.1 Umg/Kg5.1 0.39 4 6010B
7440-28-0 Thallium 5.1 Umg/Kg5.1 2.5 4 6010B
7440-66-6 Zinc 152 mg/Kg15.3 2.5 4 6010B
7439-97-6 Mercury 0.31 mg/Kg0.082 0.064 1 7471A
FORM IA-IN 06/03/2010Page 577 of 623
2A-IN
Lab Name: Job No.:
SDG No.:
Concentration Units:
CALIBRATION VERIFICATIONS
METALS
ICV Source:
CCV Source:
TestAmerica Edison 460-13139-1
ug/LME_CCV_DUO_00013
ME_CCV_DUO_00013
Analyte
ICV 460-37705/6
05/18/2010 11:04
Found C True %R
CCV 460-37705/18
05/18/2010 11:40
CCV 460-37705/30
05/18/2010 12:16
Found FoundC CTrue %R True %R
Antimony 962 949 9451000 1000 100096 95 94
Arsenic 2370 2340 23302500 2500 250095 94 93
Beryllium 996 1000 9861000 1000 1000100 100 99
Cadmium 1200 1190 11801250 1250 125096 95 94
Chromium 5100 5000 50205000 5000 5000102 100 100
Copper 12480 12430 1241012500 12500 12500100 99 99
Lead 7240 7160 71207500 7500 750097 95 95
Nickel 2420 2390 23802500 2500 250097 96 95
Selenium 2390 2350 23402500 2500 250095 94 94
Silver 1240 1210 12201250 1250 125099 97 97
Thallium 2440 2480 24902500 2500 250098 99 100
Zinc 2410 2390 23802500 2500 250096 96 95
FORM II-IN
Note! Calculations are performed before rounding to avoid round-off errors in calculated results.
Italicized analytes were not requested for this sequence.
06/03/2010Page 578 of 623
2A-IN
Lab Name: Job No.:
SDG No.:
Concentration Units:
CALIBRATION VERIFICATIONS
METALS
ICV Source:
CCV Source:
TestAmerica Edison 460-13139-1
ug/LME_DCAL-IN_00284
ME_DCAL-IN_00284
Analyte
ICV 460-37424/26-A
05/14/2010 12:16
Found C True %R
CCV 460-37424/28-A
05/14/2010 12:42
CCV 460-37424/28-A
05/14/2010 13:06
Found FoundC CTrue %R True %R
Mercury 842 837 855833 833 833101 100 103
FORM II-IN
Note! Calculations are performed before rounding to avoid round-off errors in calculated results.
Italicized analytes were not requested for this sequence.
06/03/2010Page 579 of 623
Lab Name: Job No.:
Concentration Units:
SDG No.:
INSTRUMENT BLANKS
METALS
TestAmerica Edison 460-13139-1
ug/L
CFoundCFoundCFoundCFoundRLAnalyte
ICB 460-37705/7 CCB 460-37705/19 CCB 460-37705/31
05/18/2010 11:08 05/18/2010 11:44 05/18/2010 12:19
3-IN
Antimony 10.0 10.0 10.010.0 U U U
Arsenic 5.0 5.0 5.05.0 U U U
Beryllium 2.0 2.0 2.02.0 U U U
Cadmium 5.0 5.0 5.05.0 U U U
Chromium 10.0 10.0 10.010.0 U U U
Copper 25.0 11.6 25.025.0 U J U
Lead 5.0 5.0 5.05.0 U U U
Nickel 40.0 40.0 40.040.0 U U U
Selenium 10.0 10.0 10.010.0 U U U
Silver 10.0 1.35 10.010.0 U J U
Thallium 10.0 10.0 10.010.0 U U U
Zinc 30.0 30.0 30.030.0 U U U
FORM III-IN
Italicized analytes were not requested for this sequence.
06/03/2010Page 580 of 623
Lab Name: Job No.:
Concentration Units:
SDG No.:
INSTRUMENT BLANKS
METALS
TestAmerica Edison 460-13139-1
ug/L
CFoundCFoundCFoundCFoundRLAnalyte
ICB 460-37472/8 CCB 460-37472/21 CCB 460-37472/33
05/14/2010 12:18 05/14/2010 12:44 05/14/2010 13:08
3-IN
Mercury 0.20 0.20 0.200.20 U U U
FORM III-IN
Italicized analytes were not requested for this sequence.
06/03/2010Page 581 of 623
Lab Name: Job No.:
SDG No.:
Lab Sample ID: MB 460-37477/1-A ^2Concentration Units: mg/Kg
CAS No. Analyte Concentration C Q Method
3-IN
Batch No.:
460-13139-1
Instrument Code: ICP4
METHOD BLANK
METALS
37705
TestAmerica Edison
7440-36-0 Antimony 1.0 U 6010B
7440-38-2 Arsenic 0.50 U 6010B
7440-41-7 Beryllium 0.20 U 6010B
7440-43-9 Cadmium 0.50 U 6010B
7440-47-3 Chromium 1.0 U 6010B
7440-50-8 Copper 2.5 U 6010B
7439-92-1 Lead 0.50 U 6010B
7440-02-0 Nickel 4.0 U 6010B
7782-49-2 Selenium 1.0 U 6010B
7440-22-4 Silver 0.0811 J 6010B
7440-28-0 Thallium 1.0 U 6010B
7440-66-6 Zinc 3.0 U 6010B
FORM III-IN
06/03/2010Page 582 of 623
Lab Name: Job No.:
SDG No.:
Lab Sample ID: MB 460-37424/1-AConcentration Units: mg/Kg
CAS No. Analyte Concentration C Q Method
3-IN
Batch No.:
460-13139-1
Instrument Code: LEEMAN5
METHOD BLANK
METALS
37472
TestAmerica Edison
7439-97-6 Mercury 0.033 U 7471A
FORM III-IN
06/03/2010Page 583 of 623
4A-IN
Lab Name: Job No.:
Instrument ID:
ICS Source:
Concentration Units:
Analyte
True
PercentRecovery
Found
SDG No.:
Lab File ID:
Solution A Solution A
Lab Sample ID:
TestAmerica Edison 460-13139-1
ICSA 460-37705/8
05182010A.txt
ug/L
ME_ICSA_Duo_00013
ICP4
INTERFERENCE CHECK STANDARD
METALS
-0.0551Antimony
1.34Arsenic
-0.165Beryllium
-0.674Cadmium
-1.85Chromium
9.81Copper
1.65Lead
5.93Nickel
-0.864Selenium
2.20Silver
1.72Thallium
-4.84Zinc
482000Aluminum 500000 96
0.0719Barium
475400Calcium 500000 95
1.70Cobalt
171600Iron 200000 86
436700Magnesium 500000 87
0.742Manganese
-1.82Molybdenum
100Potassium
33.3Sodium
5.06Strontium
-0.316Tin
0.619Titanium
1.41Vanadium
FORM IVA-IN
Calculations are performed before rounding to avoid round-off errors in calculated results.
06/03/2010Page 584 of 623
4A-IN
Lab Name: Job No.:
Instrument ID:
ICS Source:
Concentration Units:
Analyte
True
PercentRecovery
Found
SDG No.:
Lab File ID:
Solution AB Solution AB
Lab Sample ID:
TestAmerica Edison 460-13139-1
ICSAB 460-37705/9
05182010A.txt
ug/L
ME_ICSAB_DUO_00011
ICP4
INTERFERENCE CHECK STANDARD
METALS
86.4Antimony 100 86
92.1Arsenic 100 92
96.5Beryllium 100 97
85.6Cadmium 100 86
98.4Chromium 100 98
97.1Copper 100 97
88.3Lead 100 88
91.9Nickel 100 92
88.0Selenium 100 88
102Silver 100 102
87.4Thallium 100 87
83.0Zinc 100 83
493700Aluminum 500000 99
91.5Barium 100 92
488500Calcium 500000 98
87.7Cobalt 100 88
172600Iron 200000 86
435600Magnesium 500000 87
99.7Manganese 100 100
85.2Molybdenum 100 85
10160Potassium 10000 102
10360Sodium 10000 104
104Strontium 100 104
85.0Tin 100 85
91.2Titanium 100 91
100Vanadium 100 100
FORM IVA-IN
Calculations are performed before rounding to avoid round-off errors in calculated results.
06/03/2010Page 585 of 623
4A-IN
Lab Name: Job No.:
Instrument ID:
ICS Source:
Concentration Units:
Analyte
True
PercentRecovery
Found
SDG No.:
Lab File ID:
Solution A Solution A
Lab Sample ID:
TestAmerica Edison 460-13139-1
ICSA 460-37705/33
05182010A.txt
ug/L
ME_ICSA_Duo_00013
ICP4
INTERFERENCE CHECK STANDARD
METALS
-1.32Antimony
4.24Arsenic
-0.103Beryllium
-0.641Cadmium
-1.60Chromium
4.48Copper
1.61Lead
5.87Nickel
-2.41Selenium
0.247Silver
0.567Thallium
-5.18Zinc
485400Aluminum 500000 97
-0.160Barium
474000Calcium 500000 95
1.58Cobalt
168900Iron 200000 84
426200Magnesium 500000 85
0.404Manganese
-1.68Molybdenum
-50.9Potassium
-23.5Sodium
5.10Strontium
0.221Tin
-0.130Titanium
1.47Vanadium
FORM IVA-IN
Calculations are performed before rounding to avoid round-off errors in calculated results.
06/03/2010Page 586 of 623
4A-IN
Lab Name: Job No.:
Instrument ID:
ICS Source:
Concentration Units:
Analyte
True
PercentRecovery
Found
SDG No.:
Lab File ID:
Solution AB Solution AB
Lab Sample ID:
TestAmerica Edison 460-13139-1
ICSAB 460-37705/34
05182010A.txt
ug/L
ME_ICSAB_DUO_00011
ICP4
INTERFERENCE CHECK STANDARD
METALS
88.5Antimony 100 88
94.4Arsenic 100 94
94.2Beryllium 100 94
86.5Cadmium 100 86
98.8Chromium 100 99
96.5Copper 100 96
87.3Lead 100 87
91.8Nickel 100 92
88.3Selenium 100 88
103Silver 100 103
88.8Thallium 100 89
84.7Zinc 100 85
486100Aluminum 500000 97
92.3Barium 100 92
478800Calcium 500000 96
88.4Cobalt 100 88
171800Iron 200000 86
437200Magnesium 500000 87
98.9Manganese 100 99
84.8Molybdenum 100 85
9650Potassium 10000 96
10080Sodium 10000 101
101Strontium 100 101
86.2Tin 100 86
91.0Titanium 100 91
100Vanadium 100 100
FORM IVA-IN
Calculations are performed before rounding to avoid round-off errors in calculated results.
06/03/2010Page 587 of 623
MATRIX SPIKE SAMPLE RECOVERY
METALS
5A-IN
TB-1 2-3 MS
Lab Name: Job No.:
SDG No.:
Client ID: Lab ID: 460-13139-5 MS
460-13139-1
Matrix: Concentration Units: mg/KgSolid
TestAmerica Edison
% Solids: 93.5
ControlLimit%RAnalyte SSR
C
SampleResult (SR)
C
SpikeAdded (SA) %R Q Method
Mercury 75-1250.214 0.035 0.178 120 7471AU
SSR = Spiked Sample Result
FORM VA - IN
Note - Results and Reporting Limits have been adjusted for dry weight.
Calculations are performed before rounding to avoid round-off errors in calculated results.
06/03/2010Page 588 of 623
6-IN
DUPLICATES
TB-1 2-3 DU
Lab Name: Job No.:
SDG No.:
Matrix: Concentration Units: mg/Kg
Analyte
ControlLimit Sample (S)
C
Duplicate (D)
CRPD Q Method
460-13139-1
Solid
METALS
% Solids for Sample: 93.5 % Solids for Duplicate:
Client ID: Lab ID: 460-13139-5 DU
93.5
TestAmerica Edison
Mercury 0.035 U0.0350.035 NC 7471AU
FORM VI-IN
Calculations are performed before rounding to avoid round-off errors in calculated results.
06/03/2010Page 589 of 623
7A-IN
LCS-STANDARD REFERENCE MATERIAL
METALS
Lab ID: LCSSRM 460-37477/2-A ^4
Lab Name: Job No.: 460-13139-1
Sample Matrix: Solid LCS Source: ME_LCSS_62_00002
TestAmerica Edison
Analyte
Solid(mg/Kg)
True Found C %R Limits Q Method
Antimony 66.1 68.57 104 6010B32.0 353
Arsenic 102 93.00 91 6010B69.7 131
Beryllium 76.1 73.49 97 6010B74.0 126
Cadmium 59.5 53.69 90 6010B73.3 127
Chromium 231 228.8 99 6010B70.8 129
Copper 171 171.5 101 6010B75.3 124
Lead 84.3 86.10 102 6010B69.8 130
Nickel 131 123.8 94 6010B73.2 127
Selenium 280 249.4 89 6010B69.6 130
Silver 29.5 29.73 101 6010B65.1 135
Thallium 119 124.3 105 6010B67.8 133
Zinc 582 538.2 92 6010B73.6 127
Calculations are performed before rounding to avoid round-off errors in calculated results.
FORM VIIA - IN
06/03/2010Page 590 of 623
7A-IN
LCS-STANDARD REFERENCE MATERIAL
METALS
Lab ID: LCSSRM 460-37424/2-A ^10
Lab Name: Job No.: 460-13139-1
Sample Matrix: Solid LCS Source: ME_LCSS_62_00002
TestAmerica Edison
Analyte
Solid(mg/Kg)
True Found C %R Limits Q Method
Mercury 8.46 9.15 108 7471A51.3 149
Calculations are performed before rounding to avoid round-off errors in calculated results.
FORM VIIA - IN
06/03/2010Page 591 of 623
8-IN
Lab ID: 460-13139-5
Lab Name: Job No:
Matrix: Concentration Units: mg/Kg
Analyte
Initial SampleResult (I) C
SerialDilutionResult (S) C
%Difference Q Method
SDG No:
Solid
460-13139-1
ICP-AES AND ICP-MS SERIAL DILUTIONS
METALS
TestAmerica Edison
Mercury 0.035 U 0.18 U NC 7471A
FORM VIII-IN
Calculations are performed before rounding to avoid round-off errors in calculated results.
06/03/2010Page 592 of 623
9-IN
12/30/2008 10:24
Instrument ID: ICP4
460-13139-1Job Number:
Solid
3050B
Leach Method:
Prep Method:
Analysis Method:
Matrix:
SDG Number:
Lab Name:
DETECTION LIMITS
Analyte Wavelength/Mass
RL MDL
6010B MDL Date:
(mg/Kg) (mg/Kg)
METALS
TestAmerica Edison
Antimony 206.8 0.220.5
Arsenic 189.0 0.1740.25
Beryllium 313.0 0.0440.1
Cadmium 226.5 0.0390.25
Chromium 267.7 0.2970.5
Copper 324.7 0.2041.25
Lead 220.6 0.1250.25
Nickel 231.6 0.1342
Selenium 196.0 0.2340.5
Silver 328.0 0.0380.5
Thallium 190.8 0.2420.5
Zinc 206.2 0.2451.5
FORM IX - IN
06/03/2010Page 593 of 623
9-IN
12/30/2008 14:33
Instrument ID: LEEMAN5
460-13139-1Job Number:
Solid
7471A
Leach Method:
Prep Method:
Analysis Method:
Matrix:
SDG Number:
Lab Name:
DETECTION LIMITS
Analyte Wavelength/Mass
RL MDL
7471A MDL Date:
(mg/Kg) (mg/Kg)
METALS
TestAmerica Edison
Mercury 0.0260.033
FORM IX - IN
06/03/2010Page 594 of 623
11-IN
Lab Name: TestAmerica Edison Job No: 460-13139-1
Instrument ID: Date:
Analyte
Integ.Time(Sec.)
Concentration
Method
ICP-AES AND ICP-MS LINEAR RANGES
ICP4
SDG No.:
(ug/L)
01/06/2009 11:38
METALS
Antimony 2000 6010B
Arsenic 10000 6010B
Beryllium 2000 6010B
Cadmium 5000 6010B
Chromium 10000 6010B
Copper 25000 6010B
Lead 20000 6010B
Nickel 5000 6010B
Selenium 10000 6010B
Silver 2500 6010B
Thallium 10000 6010B
Zinc 5000 6010B
FORM XI - IN
06/03/2010Page 595 of 623
12-IN
PREPARATION LOG
Lab Name: Job No.:
SDG No.:
Preparation Method:
LabSampleID
PreparationDate
InitialWeight
Final Volume
PrepBatch
460-13139-1
METALS
3050B
InitialVolume
(g) (mL)
TestAmerica Edison
05/14/2010 15:42 37477MB 460-37477/1-A ^2 501.00
05/14/2010 15:42 37477LCSSRM 460-37477/2-A ^4
501.02
05/14/2010 15:42 37477460-13139-2 501.06
05/14/2010 15:42 37477460-13139-4 501.00
05/14/2010 15:42 37477460-13139-5 501.06
05/14/2010 15:42 37477460-13139-7 501.02
FORM XII-IN
06/03/2010Page 596 of 623
12-IN
PREPARATION LOG
Lab Name: Job No.:
SDG No.:
Preparation Method:
LabSampleID
PreparationDate
InitialWeight
Final Volume
PrepBatch
460-13139-1
METALS
7471A
InitialVolume
(g) (mL)
TestAmerica Edison
05/14/2010 09:25 37424MB 460-37424/1-A 1000.60
05/14/2010 09:25 37424LCSSRM 460-37424/2-A ^10
1000.60
05/14/2010 09:25 37424460-13139-5 1000.60
05/14/2010 09:25 37424460-13139-5 DU 1000.60
05/14/2010 09:25 37424460-13139-5 MS 1000.60
05/14/2010 09:25 37424460-13139-2 1000.63
05/14/2010 09:25 37424460-13139-4 1000.64
05/14/2010 09:25 37424460-13139-7 1000.63
FORM XII-IN
06/03/2010Page 597 of 623
13-IN
ANALYSIS RUN LOG
Lab Name: Job No.:
SDG No.:
Instrument ID: Method:
Start Date: End Date:
TestAmerica Edison 460-13139-1
ICP4
05/18/2010 10:49 05/18/2010 12:34
6010B
METALS
LabSampleID
D/F
Time
Analytes
Ag
As
Be
Cd
Cr
Cu
Ni
Pb
Sb
Se
Tl
Zn
Type
10:49ZZZZZZ
10:52ZZZZZZ
10:55ZZZZZZ
10:58ZZZZZZ
11:01ZZZZZZ
1 11:04 X X X X X X X X X X X XICV 460-37705/6
1 11:08 X X X X X X X X X X X XICB 460-37705/7
1 11:11 X X X X X X X X X X X XICSA 460-37705/8
1 11:14 X X X X X X X X X X X XICSAB 460-37705/9
11:17ZZZZZZ
2 11:20 X X X X X X X X X X X XMB 460-37477/1-A ^2 T
4 11:23 X X X X X X X X X X X XLCSSRM 460-37477/2-A ^4
T
11:26ZZZZZZ
11:29ZZZZZZ
11:32ZZZZZZ
11:34ZZZZZZ
11:37ZZZZZZ
1 11:40 X X X X X X X X X X X XCCV 460-37705/18
1 11:44 X X X X X X X X X X X XCCB 460-37705/19
11:46ZZZZZZ
11:49ZZZZZZ
11:53ZZZZZZ
4 11:55 X X X X X X X X X X X X460-13139-2 T
11:58ZZZZZZ
4 12:01 X X X X X X X X X X X X460-13139-4 T
4 12:04 X X X X X X X X X X X X460-13139-5 T
12:07ZZZZZZ
4 12:10 X X X X X X X X X X X X460-13139-7 T
12:13ZZZZZZ
1 12:16 X X X X X X X X X X X XCCV 460-37705/30
1 12:19 X X X X X X X X X X X XCCB 460-37705/31
12:22ZZZZZZ
1 12:25 X X X X X X X X X X X XICSA 460-37705/33
1 12:28 X X X X X X X X X X X XICSAB 460-37705/34
12:31CCV 460-37705/35
12:34CCB 460-37705/36
Prep Types
T = Total/NA
FORM XIII-IN 06/03/2010Page 598 of 623
13-IN
ANALYSIS RUN LOG
Lab Name: Job No.:
SDG No.:
Instrument ID: Method:
Start Date: End Date:
TestAmerica Edison 460-13139-1
LEEMAN5
05/14/2010 12:04 05/14/2010 13:08
7471A
METALS
LabSampleID
D/F
Time
Analytes
Hg
Type
12:04 XIC 460-37424/20-A
12:06 XIC 460-37424/21-A
12:08 XIC 460-37424/22-A
12:10 XIC 460-37424/23-A
12:12 XIC 460-37424/24-A
12:14 XIC 460-37424/25-A
1 12:16 XICV 460-37424/26-A
1 12:18 XICB 460-37472/8
12:20ZZZZZZ
1 12:22 XMB 460-37424/1-A T
10 12:24 XLCSSRM 460-37424/2-A ^10
T
1 12:26 X460-13139-5 T
1 12:28 X460-13139-5 DU T
1 12:31 X460-13139-5 MS T
12:33ZZZZZZ
12:34ZZZZZZ
12:36ZZZZZZ
12:38ZZZZZZ
12:41ZZZZZZ
1 12:42 XCCV 460-37424/28-A
1 12:44 XCCB 460-37472/21
12:46ZZZZZZ
12:48ZZZZZZ
12:50ZZZZZZ
1 12:52 X460-13139-2 T
12:53ZZZZZZ
1 12:55 X460-13139-4 T
12:57ZZZZZZ
1 12:59 X460-13139-7 T
13:01ZZZZZZ
5 13:04 X460-13139-5 SD T
1 13:06 XCCV 460-37424/28-A
1 13:08 XCCB 460-37472/33
Prep Types
T = Total/NA
FORM XIII-IN 06/03/2010Page 599 of 623
Metals Worksheet
Method: 7471A
Analyst: Sheikh, Razia B
Batch Number: 460-37424 Date Open:
Batch End:
May 14 2010 9:25AM
Lab ID Client ID Basis Final weight/volume of
sample
ME_DCAL-IN_00284 ME_DICV-IN_00286 ME_LCSS_62_00002Initial weight/volume of
sample
Method Chain
MB~460-37424/1 0.60 g 100 mL7471A, 7471A
LCSSRM~460-3742
4/2
0.60 g 100 mL 0.60 g7471A, 7471A
460-13139-E-5 TB-1 2-3 T 0.60 g 100 mL7471A, 7471A
460-13139-E-5~DU TB-1 2-3 T 0.60 g 100 mL7471A, 7471A
460-13139-E-5~MS TB-1 2-3 T 0.60 g 100 mL 1.00 mL7471A, 7471A
460-13148-D-1 T 0.68 g 100 mL
460-13118-A-1 T 0.63 g 100 mL
460-13118-A-2 T 0.61 g 100 mL
460-13118-A-3 T 0.61 g 100 mL
460-13146-F-1 T 0.69 g 100 mL
460-13147-B-1 T 0.68 g 100 mL
460-13147-A-2 T 0.61 g 100 mL
460-13139-E-1 TB-3 2-3 T 0.66 g 100 mL
460-13139-E-2 TB-3 6-7 T 0.63 g 100 mL7471A, 7471A
460-13139-E-3 TB-2 2-3 T 0.65 g 100 mL
460-13139-E-4 TB-2 5-6 T 0.64 g 100 mL7471A, 7471A
460-13139-E-6 TB-1 5-6 T 0.65 g 100 mL
460-13139-E-7 TB-5 3-4 T 0.63 g 100 mL7471A, 7471A
460-13139-E-8 TB-4 6-7 T 0.70 g 100 mL
IC~460-37424/20 0.60 g 100 mL
IC~460-37424/21 0.60 g 100 mL 0.1 mL
IC~460-37424/22 0.60 g 100 mL 1.0 mL
IC~460-37424/23 0.60 g 100 mL 2.0 mL
IC~460-37424/24 0.60 g 100 mL 5.0 mL
IC~460-37424/25 0.60 g 100 mL 10.0 mL
06/03/2010Page 600 of 623
Metals Worksheet
Method: 7471A
Analyst: Sheikh, Razia B
Batch Number: 460-37424 Date Open:
Batch End:
May 14 2010 9:25AM
Lab ID Client ID Basis Final weight/volume of
sample
ME_DCAL-IN_00284 ME_DICV-IN_00286 ME_LCSS_62_00002Initial weight/volume of
sample
Method Chain
ICV~460-37424/26 0.60 g 100 mL 5.0 mL7471A, 7471A
qcs 0.60 g 100 mL 5.0 mL
CCV~460-37424/28 0.60 g 100 mL 5.0 mL7471A, 7471A
Hood ID or number: 1
Balance ID: 33
Lot # of Nitric Acid: h51022
Lot # of hydrochloric acid: h42a18
Potassium Permanganate Lot Number: 00605lh
Sulfuric Acid Lot Number: h46f04
Stannous Chloride Lot Number: g37640
Oven, Bath or Block Temperature 1: 121c
NaCL Lot #: g28618
Hydroxylamine Hydrochloride Lot: g50470
06/03/2010Page 601 of 623
Metals Worksheet
Method: 3050B
Analyst: Cheema, Ali R
Batch Number: 460-37477 Date Open:
Batch End:
May 14 2010 3:42PM
Lab ID Client ID Basis Final weight/volume of
sample
ME_LCS-int_00020 ME_LCSS_62_00002Initial weight/volume of
sample
Method Chain
MB~460-37477/1 1.00 g 50 mL3050B, 6010B
LCSSRM~460-3747
7/2
1.02 g 50 mL 1.00 g3050B, 6010B
460-13152-A-3 T 1.09 g 50 mL
460-13152-A-1 T 1.05 g 50 mL
460-13152-A-2 T 1.07 g 50 mL
460-13139-E-1 TB-3 2-3 T 1.02 g 50 mL
460-13139-E-2 TB-3 6-7 T 1.06 g 50 mL3050B, 6010B
460-13139-E-3 TB-2 2-3 T 1.06 g 50 mL
460-13139-E-4 TB-2 5-6 T 1.00 g 50 mL3050B, 6010B
460-13139-E-5 TB-1 2-3 T 1.06 g 50 mL3050B, 6010B
460-13139-E-6 TB-1 5-6 T 1.00 g 50 mL
460-13139-E-7 TB-5 3-4 T 1.02 g 50 mL3050B, 6010B
460-13139-E-8 TB-4 6-7 T 1.02 g 50 mL
460-13139-E-8~DU T 1.02 g 50 mL
460-13139-E-8~MS T 1.02 g 50 mL 2 mL
Balance ID: 35
Lot # of hydrochloric acid: H35A01
Lot # of Nitric Acid: J04031
Hydrogen peroxide lot number: H26J05
Temperature: 95 Degrees C
06/03/2010Page 602 of 623
GENERAL CHEMISTRY
06/03/2010Page 603 of 623
COVER PAGE
Lab Name: Job Number:
Client Sample ID Lab Sample ID
GENERAL CHEMISTRY
Project: Dumont Fields - Twin Boro
SDG No.:
460-13139-1TestAmerica Edison
TB-3 2-3 460-13139-1
TB-3 6-7 460-13139-2
TB-2 2-3 460-13139-3
TB-2 5-6 460-13139-4
TB-1 2-3 460-13139-5
TB-1 5-6 460-13139-6
TB-5 3-4 460-13139-7
TB-4 6-7 460-13139-8
Comments:
06/03/2010Page 604 of 623
9-IN
02/15/2007 17:07
Instrument ID: NOEQUIP
460-13139-1Job Number:
Solid
Leach Method:
Prep Method:
Analysis Method:
Matrix:
SDG Number:
Lab Name:
DETECTION LIMITS
Analyte Wavelength/Mass
RL
Moisture RL Date:
(%)
GENERAL CHEMISTRY
TestAmerica Edison
Percent Moisture 1
Percent Solids 1
FORM IX - IN
06/03/2010Page 605 of 623
13-IN
ANALYSIS RUN LOG
Lab Name: Job No.:
SDG No.:
Instrument ID: Method:
Start Date: End Date:
TestAmerica Edison 460-13139-1
NOEQUIP
05/14/2010 21:47 05/14/2010 21:54
Moisture
GENERAL CHEMISTRY
LabSampleID
D/F
Time
Analytes
%Sol
Moist
Type
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
1 21:47 X X460-13139-1 T
1 21:47 X X460-13139-2 T
1 21:47 X X460-13139-3 T
1 21:47 X X460-13139-4 T
1 21:47 X X460-13139-5 T
1 21:47 X X460-13139-6 T
1 21:47 X X460-13139-8 T
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
1 21:47 X X460-13146-A-1 DU T
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
FORM XIII-IN 06/03/2010Page 606 of 623
13-IN
ANALYSIS RUN LOG
Lab Name: Job No.:
SDG No.:
Instrument ID: Method:
Start Date: End Date:
TestAmerica Edison 460-13139-1
NOEQUIP
05/14/2010 21:47 05/14/2010 21:54
Moisture
GENERAL CHEMISTRY
LabSampleID
D/F
Time
Analytes
%Sol
Moist
Type
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
FORM XIII-IN 06/03/2010Page 607 of 623
13-IN
ANALYSIS RUN LOG
Lab Name: Job No.:
SDG No.:
Instrument ID: Method:
Start Date: End Date:
TestAmerica Edison 460-13139-1
NOEQUIP
05/14/2010 21:47 05/14/2010 21:54
Moisture
GENERAL CHEMISTRY
LabSampleID
D/F
Time
Analytes
%Sol
Moist
Type
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:47ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
FORM XIII-IN 06/03/2010Page 608 of 623
13-IN
ANALYSIS RUN LOG
Lab Name: Job No.:
SDG No.:
Instrument ID: Method:
Start Date: End Date:
TestAmerica Edison 460-13139-1
NOEQUIP
05/14/2010 21:47 05/14/2010 21:54
Moisture
GENERAL CHEMISTRY
LabSampleID
D/F
Time
Analytes
%Sol
Moist
Type
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
FORM XIII-IN 06/03/2010Page 609 of 623
13-IN
ANALYSIS RUN LOG
Lab Name: Job No.:
SDG No.:
Instrument ID: Method:
Start Date: End Date:
TestAmerica Edison 460-13139-1
NOEQUIP
05/14/2010 21:47 05/14/2010 21:54
Moisture
GENERAL CHEMISTRY
LabSampleID
D/F
Time
Analytes
%Sol
Moist
Type
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:53ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
FORM XIII-IN 06/03/2010Page 610 of 623
13-IN
ANALYSIS RUN LOG
Lab Name: Job No.:
SDG No.:
Instrument ID: Method:
Start Date: End Date:
TestAmerica Edison 460-13139-1
NOEQUIP
05/14/2010 21:47 05/14/2010 21:54
Moisture
GENERAL CHEMISTRY
LabSampleID
D/F
Time
Analytes
%Sol
Moist
Type
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
21:54ZZZZZZ
Prep Types
T = Total/NA
FORM XIII-IN 06/03/2010Page 611 of 623
13-IN
ANALYSIS RUN LOG
Lab Name: Job No.:
SDG No.:
Instrument ID: Method:
Start Date: End Date:
TestAmerica Edison 460-13139-1
NOEQUIP
05/17/2010 19:56 05/17/2010 19:56
Moisture
GENERAL CHEMISTRY
LabSampleID
D/F
Time
Analytes
%Sol
Moist
Type
19:56ZZZZZZ
1 19:56 X X460-13139-7 T
19:56ZZZZZZ
19:56ZZZZZZ
19:56ZZZZZZ
19:56ZZZZZZ
1 19:56 X X460-13237-A-4 DU T
19:56ZZZZZZ
19:56ZZZZZZ
19:56ZZZZZZ
19:56ZZZZZZ
19:56ZZZZZZ
19:56ZZZZZZ
19:56ZZZZZZ
19:56ZZZZZZ
19:56ZZZZZZ
19:56ZZZZZZ
19:56ZZZZZZ
19:56ZZZZZZ
19:56ZZZZZZ
Prep Types
T = Total/NA
FORM XIII-IN 06/03/2010Page 612 of 623
General Chemistry Worksheet
Method: Moisture
Analyst: Dave, Virendra
Batch Number: 460-37508 Date Open:
Batch End:
May 14 2010 9:47PM
Lab ID Client ID Basis Empty Dish Weight Mass of wet Sample Mass of Dry SampleDish IDMethod Chain
PB~460-37508/1 13 1.01 g 1.01 g1.01 g
460-13148-A-1 T 15 1.04 g 8.01 g8.41 g
460-13120-A-1 T 14 1.04 g 5.92 g6.65 g
460-13120-A-2 T 83 1.02 g 5.62 g6.27 g
460-13187-D-1 T 165 1.01 g 6.35 g6.86 g
460-13187-D-2 T 74 1.04 g 6.13 g6.65 g
460-13139-D-1 TB-3 2-3 T 66 1.00 g 6.04 g7.14 gMoisture
460-13139-D-2 TB-3 6-7 T 26 1.00 g 6.23 g7.44 gMoisture
460-13139-D-3 TB-2 2-3 T 57 0.98 g 6.80 g7.74 gMoisture
460-13139-D-4 TB-2 5-6 T 27 0.97 g 4.93 g5.51 gMoisture
460-13139-D-5 TB-1 2-3 T 71 0.95 g 8.85 g9.40 gMoisture
460-13139-D-6 TB-1 5-6 T 29 1.01 g 6.71 g7.48 gMoisture
460-13139-D-8 TB-4 6-7 T 84 1.03 g 5.70 g6.61 gMoisture
460-13137-D-9 T 36 0.98 g 6.54 g7.54 g
460-13137-D-10 T 80 1.01 g 5.92 g7.01 g
460-13137-D-11 T 43 0.99 g 6.15 g7.64 g
460-13137-D-12 T 82 1.03 g 8.84 g9.46 g
460-13137-D-13 T 87 0.98 g 9.69 g9.88 g
460-13137-D-14 T 276 0.99 g 5.39 g7.06 g
460-13146-A-1 T 39 0.98 g 5.84 g6.78 g
460-13146-A-1~DU T 28 0.99 g 5.94 g6.89 gMoisture
460-13131-A-1 T 69 0.97 g 5.81 g7.03 g
460-13131-A-2 T 36 0.97 g 6.28 g7.20 g
460-13131-A-3 T 35 1.00 g 6.47 g7.46 g
460-13131-A-4 T 13 0.99 g 7.47 g9.25 g
06/03/2010Page 613 of 623
General Chemistry Worksheet
Method: Moisture
Analyst: Dave, Virendra
Batch Number: 460-37508 Date Open:
Batch End:
May 14 2010 9:47PM
Lab ID Client ID Basis Empty Dish Weight Mass of wet Sample Mass of Dry SampleDish IDMethod Chain
460-13131-A-5 T 35 1.01 g 6.36 g7.38 g
460-13131-A-6 T 82 1.01 g 6.75 g7.24 g
460-13131-A-7 T 85 1.00 g 6.33 g7.26 g
460-13131-A-8 T 38 1.03 g 7.94 g8.97 g
460-13131-A-9 T 81 1.02 g 7.11 g7.89 g
460-13131-A-11 T 40 1.00 g 5.62 g6.56 g
460-13131-A-12 T 85 1.02 g 7.01 g8.40 g
460-13164-E-1 T 30 1.03 g 6.35 g7.75 g
460-13164-E-2 T 17 0.95 g 7.28 g8.23 g
460-13164-E-3 T 85 0.97 g 7.29 g8.68 g
460-13164-E-4 T 45 0.94 g 7.08 g7.81 g
460-13164-E-5 T 44 0.96 g 6.37 g7.35 g
460-13175-A-1 T 37 0.99 g 6.12 g7.13 g
460-13175-A-2 T 77 1.03 g 7.76 g8.48 g
460-13175-A-3 T 72 1.00 g 6.67 g7.72 g
460-13175-A-3~DU T 65 1.05 g 8.35 g9.61 g
460-13175-A-4 T 62 1.01 g 8.72 g9.92 g
460-13175-A-5 T 74 0.99 g 8.74 g9.91 g
460-13175-A-6 T 14 1.00 g 8.80 g9.62 g
460-13175-A-7 T 76 0.99 g 7.79 g8.78 g
460-13175-A-8 T 151 1.03 g 7.46 g8.19 g
460-13175-A-9 T 48 1.01 g 7.05 g7.57 g
460-13175-A-10 T 79 0.99 g 7.99 g9.51 g
460-13175-A-11 T 45 1.00 g 8.95 g9.87 g
460-13175-A-12 T 81 1.00 g 7.80 g8.61 g
06/03/2010Page 614 of 623
General Chemistry Worksheet
Method: Moisture
Analyst: Dave, Virendra
Batch Number: 460-37508 Date Open:
Batch End:
May 14 2010 9:47PM
Lab ID Client ID Basis Empty Dish Weight Mass of wet Sample Mass of Dry SampleDish IDMethod Chain
460-13176-A-1 T 5 1.01 g 6.03 g6.69 g
460-13176-A-2 T 85 1.01 g 5.52 g6.34 g
460-13176-A-3 T 47 0.97 g 5.66 g6.73 g
460-13176-A-4 T 4 0.98 g 6.48 g7.21 g
460-13176-A-5 T 79 1.01 g 7.44 g8.21 g
460-13176-A-6 T 72 1.01 g 7.43 g8.18 g
460-13176-A-7 T 91 1.00 g 6.25 g7.06 g
460-13176-A-8 T 75 1.04 g 5.86 g6.81 g
460-13176-A-8~DU T 7 0.98 g 6.11 g6.96 g
460-13176-A-9 T 161 1.02 g 6.12 g6.87 g
460-13173-A-1 T 22 0.97 g 5.63 g6.54 g
460-13173-A-2 T 80 1.01 g 6.08 g7.36 g
460-13173-A-3 T 86 0.98 g 7.04 g8.51 g
460-13173-A-4 T 99 1.04 g 8.80 g9.36 g
460-13173-A-5 T 50 0.98 g 7.78 g8.27 g
460-13173-A-6 T 56 1.02 g 6.73 g7.47 g
460-13173-A-7 T 62 1.00 g 5.23 g6.20 g
460-13173-A-8 T 52 1.03 g 7.46 g8.65 g
460-13173-A-9 T 31 0.95 g 6.10 g6.84 g
460-13173-A-10 T 84 0.99 g 7.80 g9.30 g
460-13173-A-11 T 51 1.04 g 7.78 g9.35 g
460-13173-A-12 T 40 0.96 g 5.33 g6.34 g
460-13173-A-13 T 68 1.02 g 6.83 g7.99 g
460-13173-A-14 T 63 1.00 g 5.53 g6.23 g
460-13173-A-15 T 70 1.00 g 6.15 g7.04 g
06/03/2010Page 615 of 623
General Chemistry Worksheet
Method: Moisture
Analyst: Dave, Virendra
Batch Number: 460-37508 Date Open:
Batch End:
May 14 2010 9:47PM
Lab ID Client ID Basis Empty Dish Weight Mass of wet Sample Mass of Dry SampleDish IDMethod Chain
460-13173-A-16 T 37 1.00 g 5.25 g6.10 g
460-13173-A-17 T 72 0.97 g 4.28 g4.88 g
460-13173-A-18 T 21 1.03 g 7.51 g8.65 g
460-13173-A-19 T 71 1.01 g 5.53 g6.51 g
460-13173-A-20 T 86 1.00 g 7.08 g8.31 g
460-13173-A-21 T 28 1.01 g 7.14 g8.27 g
460-13173-A-22 T 54 0.99 g 6.56 g7.58 g
460-13173-A-23 T 67 1.02 g 7.67 g9.31 g
460-13173-A-24 T 66 1.04 g 8.21 g9.79 g
460-13173-A-25 T 50 1.02 g 7.97 g9.51 g
460-13173-A-26 T 75 0.99 g 7.41 g8.96 g
460-13173-A-27 T 73 1.02 g 6.74 g7.97 g
460-13173-A-28 T 91 0.98 g 9.97 g9.98 g
460-13173-A-28~DU T 90 1.00 g 7.73 g7.74 g
460-13179-A-1 T 81 1.00 g 7.33 g8.40 g
460-13179-A-2 T 100 1.02 g 7.61 g8.29 g
460-13179-A-3 T 24 1.02 g 5.72 g6.25 g
460-13179-A-4 T 25 1.02 g 7.62 g8.05 g
460-13179-A-5 T 34 0.98 g 7.85 g9.12 g
460-13179-A-6 T 37 1.01 g 6.46 g6.75 g
460-13179-A-7 T 49 1.02 g 7.58 g8.32 g
460-13179-A-8 T 11 0.97 g 6.53 g7.04 g
460-13179-A-9 T 4 1.03 g 7.11 g7.45 g
460-13179-A-10 T 23 0.98 g 5.77 g6.12 g
460-13179-A-11 T 29 0.98 g 8.66 g9.20 g
06/03/2010Page 616 of 623
General Chemistry Worksheet
Method: Moisture
Analyst: Dave, Virendra
Batch Number: 460-37508 Date Open:
Batch End:
May 14 2010 9:47PM
Lab ID Client ID Basis Empty Dish Weight Mass of wet Sample Mass of Dry SampleDish IDMethod Chain
460-13179-A-12 T 14 0.96 g 8.99 g9.66 g
460-13179-A-12~DU T 96 1.03 g 7.75 g8.35 g
460-13179-A-13 T 74 0.99 g 8.23 g8.96 g
460-13179-A-14 T 39 0.97 g 6.86 g7.81 g
460-13179-A-15 T 30 0.98 g 8.30 g8.83 g
460-13179-A-16 T 16 1.00 g 8.83 g9.56 g
460-13179-A-17 T 77 0.99 g 7.79 g8.26 g
460-13179-A-18 T 8 1.02 g 8.44 g9.08 g
460-13179-A-19 T 164 0.99 g 8.06 g8.34 g
460-13179-A-20 T 27 1.02 g 7.89 g8.30 g
460-13179-A-21 T 76 1.04 g 7.25 g7.68 g
460-13179-A-22 T 20 0.98 g 8.25 g8.73 g
460-13179-A-23 T 3 1.03 g 8.49 g9.12 g
460-13179-A-24 T 87 0.99 g 9.00 g9.85 g
460-13144-A-3 T 9 0.97 g 6.90 g7.39 g
460-13147-B-1 T 49 1.00 g 7.77 g8.92 g
460-13147-A-2 T 26 1.05 g 7.67 g8.66 g
460-13147-A-2~DU T 70 1.03 g 7.97 g8.89 g
460-13149-A-1 T 33 0.98 g 7.28 g8.81 g
460-13168-A-1 T 80 0.99 g 7.95 g8.93 g
460-13144-A-1 T 18 1.00 g 7.87 g8.35 g
460-13144-A-2 T 78 1.02 g 8.06 g8.79 g
460-13152-A-1 T 98 1.00 g 7.35 g8.88 g
460-13152-A-2 T 97 1.02 g 7.74 g9.58 g
460-13152-A-3 T 8 0.99 g 6.92 g8.16 g
06/03/2010Page 617 of 623
General Chemistry Worksheet
Method: Moisture
Analyst: Dave, Virendra
Batch Number: 460-37508 Date Open:
Batch End:
May 14 2010 9:47PM
Lab ID Client ID Basis Empty Dish Weight Mass of wet Sample Mass of Dry SampleDish IDMethod Chain
460-12815-A-1 T 11 0.99 g 9.46 g9.75 g
460-13137-A-1 T 80 1.04 g 6.94 g7.12 g
460-13137-A-2 T 53 1.04 g 7.83 g8.08 g
460-13137-A-3 T 92 1.01 g 6.88 g7.00 g
460-13137-A-4 T 21 0.98 g 7.22 g7.36 g
460-13137-A-5 T 1 0.99 g 8.70 g9.25 g
460-13137-A-6 T 3 0.98 g 9.01 g9.13 g
460-13137-A-7 T 73 0.98 g 7.23 g7.44 g
460-13137-A-8 T 6 1.00 g 6.52 g6.74 g
460-13136-B-1 T 5 0.96 g 6.20 g6.53 g
460-13136-A-2 T 12 0.98 g 8.77 g9.55 g
460-13136-A-2~DU T 46 0.97 g 7.46 g8.09 g
460-13173-A-29 T 48 0.97 g 7.50 g8.95 g
460-13173-B-30 T 7 0.98 g 8.38 g9.90 g
460-13173-A-31 T 9 0.96 g 7.83 g8.84 g
460-13173-A-32 T 56 0.97 g 8.10 g9.52 g
460-13173-A-33 T 1 1.06 g 7.13 g8.47 g
460-13173-A-34 T 55 0.98 g 6.58 g7.20 g
460-13173-A-35 T 21 1.01 g 7.07 g8.45 g
460-13173-A-36 T 25 0.97 g 7.28 g8.43 g
460-13173-A-37 T 23 1.00 g 6.28 g7.41 g
460-13173-A-38 T 69 1.02 g 7.96 g8.76 g
460-13173-A-39 T 41 0.99 g 7.61 g8.78 g
460-13173-A-40 T 1 1.03 g 6.53 g7.83 g
460-13173-A-41 T 38 1.00 g 6.48 g7.14 g
06/03/2010Page 618 of 623
General Chemistry Worksheet
Method: Moisture
Analyst: Dave, Virendra
Batch Number: 460-37508 Date Open:
Batch End:
May 14 2010 9:47PM
Lab ID Client ID Basis Empty Dish Weight Mass of wet Sample Mass of Dry SampleDish IDMethod Chain
460-13173-A-42 T 24 0.98 g 5.73 g7.01 g
460-13173-A-43 T 77 1.00 g 6.14 g7.05 g
460-13173-A-44 T 22 1.00 g 5.34 g6.11 g
460-13173-A-44~DU T 12 1.00 g 5.78 g6.63 g
460-13183-B-1 T 89 0.99 g 5.39 g7.27 g
460-13183-B-2 T 89 1.04 g 7.11 g8.61 g
460-13183-B-3 T 59 0.99 g 7.09 g8.05 g
460-13181-A-1 T 15 1.03 g 7.95 g9.89 g
460-13189-A-1 T 42 1.00 g 7.17 g8.25 g
460-13174-A-1 T 88 1.00 g 8.17 g9.27 g
460-13192-A-1 T 31 1.03 g 4.56 g6.08 g
460-13192-A-2 T 14 0.98 g 6.72 g7.26 g
460-13192-A-3 T 17 0.97 g 6.23 g7.03 g
460-13192-A-3~DU T 36 1.01 g 7.19 g8.17 g
Balance ID: 101 No Unit
Date samples were place in the oven: 5-14-10
Time samples were place in the oven: 22:30
Oven Temp when samples are put in oven: 104 104 Degrees C
Date samples were removed from oven: 5-15-10
Time Samples were removed from oven: 15:20
Oven Temp when samples removed from oven: 103 103 Degrees C
Oven ID: 1 2
ID number of the thermometer: 28212 29705
06/03/2010Page 619 of 623
General Chemistry Worksheet
Method: Moisture
Analyst: Dave, Virendra
Batch Number: 460-37639 Date Open:
Batch End:
May 17 2010 7:56PM
May 18 2010 9:38AM
Lab ID Client ID Basis Empty Dish Weight Mass of wet Sample Mass of Dry SampleDish IDMethod Chain
PB~460-37639/1 45 0.96 g 0.96 g0.96 g
460-13139-E-7 TB-5 3-4 T 27 0.99 g 3.29 g6.97 gMoisture
460-13238-A-1 T 57 0.97 g 6.90 g7.97 g
460-13238-A-2 T 43 0.98 g 6.52 g7.51 g
460-13237-A-3 T 80 1.01 g 5.73 g6.70 g
460-13237-A-4 T 36 1.02 g 5.38 g6.20 g
460-13237-A-4~DU T 56 1.03 g 5.32 g6.15 gMoisture
Balance ID: 101 No Unit
Date samples were place in the oven: 5-17-10
Time samples were place in the oven: 20:30
Oven Temp when samples are put in oven: 103 Degrees C
Oven Temp when samples removed from oven: 103°C Degrees C
Oven ID: 1
ID number of the thermometer: 28212
06/03/2010Page 620 of 623
Shipping and
Receiving
Documents
06/03/2010Page 621 of 623
06/03/2010Page 622 of 623
Login Sample Receipt Check List
Client: Duffield Associates Job Number: 460-13139-1
Login Number: 13139
Question T / F/ NA Comment
Creator: Hall, Alonzo
List Source: TestAmerica Edison
List Number: 1
Radioactivity either was not measured or, if measured, is at or below
background
N/A
The cooler's custody seal, if present, is intact. N/A
The cooler or samples do not appear to have been compromised or
tampered with.
True
Samples were received on ice. True
Cooler Temperature is acceptable. True
Cooler Temperature is recorded. True 3.3°C
COC is present. True
COC is filled out in ink and legible. True
COC is filled out with all pertinent information. True
There are no discrepancies between the sample IDs on the containers and
the COC.
True
Samples are received within Holding Time. True
Sample containers have legible labels. True
Containers are not broken or leaking. True
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
There is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
True
VOA sample vials do not have headspace or bubble is <6mm (1/4") in
diameter.
N/A
If necessary, staff have been informed of any short hold time or quick TAT
needs
True
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Is the Field Sampler's name present on COC? True
Sample Preservation Verified True
TestAmerica Edison 06/03/2010Page 623 of 623