OPRA - Twin Boro Field Phase 2 Lab Report

ANALYTICAL REPORT

Job Number: 460-13139-1

Job Description: Dumont Fields - Twin Boro

For:Duffield Associates

5400 Limestone RoadWilmington, DE 19808

Attention: Mr. Bradley Summerville

_____________________________________________

Approved for release.Jamie CapaciProject Manager I6/3/2010 3:55 PM

Jamie CapaciProject Manager I

[email protected]/03/2010

The test results in this report meet all NELAP requirements unless specified within the case narrative. Pursuant toNELAP, this report may not be reproduced, except in full, without the written approval of the laboratory. All questionsregarding this report should be directed to the TestAmerica Edison Project Manager.

TestAmerica Edison Certifications and Approvals: Connecticut: CTDOH #PH-0200, New Jersey: NJDEP (NELAP)#12028, New York: NYDOH (NELAP) #11452, NYDOH (ELAP) #11452, Pennsylvania: PADEP (NELAP) 68-00522 andRhode Island: RIDOH LAO00132

TestAmerica Laboratories, Inc.

TestAmerica Edison 777 New Durham Road, Edison, NJ 08817

Tel (732) 549-3900 Fax (732) 549-3679 www.testamericainc.com

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mailto:[email protected]

http://www.testamericainc.com

Table of ContentsCover Title Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Data Summaries . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Report Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

Executive Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12

Method / Analyst Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13

Sample Datasheets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62

QC Data Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 66

Data Qualifiers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 95

QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 97

Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 101

Organic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 106

GC/MS VOA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 106

Method 8260B . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 106Method 8260B QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 107Method 8260B Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 114Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 142

Method 8260B ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 142Method 8260B CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 154

Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 157Method 8260B Tune Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 157Method 8260B Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 165Method 8260B LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 171

Method 8260B Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 185

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Table of ContentsMethod 8260B Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 187

GC/MS Semi VOA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 189

Method 8270C . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 189Method 8270C QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 190Method 8270C Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 202Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 298

Method 8270C ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 298Method 8270C CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 309

Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 312Method 8270C Tune Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 312Method 8270C Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 320Method 8270C LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 329Method 8270C MS/MSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 336

Method 8270C Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 340Method 8270C Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 342

GC Semi VOA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 344

Method 8081A . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 344Method 8081A QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 345Method 8081A Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 360Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 389

Method 8081A ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 389Method 8081A PEM Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 409Method 8081A CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 417

Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 425Method 8081A Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 425Method 8081A LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 431

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Table of ContentsMethod 8081A MS/MSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 441

Method 8081A Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 445Method 8081A Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 448

Method 8082 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 450Method 8082 QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 451Method 8082 Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 464Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 488

Method 8082 ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 488Method 8082 CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 538

Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 546Method 8082 Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 546Method 8082 LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 552Method 8082 MS/MSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 563

Method 8082 Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 567Method 8082 Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 570

Inorganic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 572

Metals Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 572

Met Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 573

Met Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 574

Met QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 578Met ICV/CCV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 578Met Blanks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 580Met ICSA/ICSAB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 584Met MS/MSD/PDS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 588Met Duplicates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 589Met LCS/LCSD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 590

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Table of ContentsMet Serial Dilution . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 592

Met MDL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 593

Met Linear Ranges . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 595

Met Preparation Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 596

Met Analysis Run Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 598

Met Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 600

General Chemistry Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 603

Gen Chem Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 604

Gen Chem MDL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 605

Gen Chem Analysis Run Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 606

Gen Chem Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 613

Shipping and Receiving Documents . . . . . . . . . . . . . . . . . . . . . . . . . . . 621

Client Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 622

Sample Receipt Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 623

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CASE NARRATIVE

Client: Duffield Associates

Project: Dumont Fields - Twin Boro

Report Number: 460-13139-1

This case narrative is in the form of an exception report, where only the anomalies related to this report, method specific performance

and/or QA/QC issues are discussed. If there are no issues to report, this narrative will include a statement that documents that there are

no relevant data issues.

It should be noted that samples with elevated Reporting Limits (RLs) as a result of a dilution may not be able to satisfy customer reporting

limits in some cases. Such increases in the RLs are unavoidable but acceptable consequence of sample dilution that enables

quantification of target analytes or interferences which exceed the calibration range of the instrument.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the

individual sections below.

RECEIPT

The samples were received on 05/13/2010; the samples arrived in good condition, properly preserved and on ice. The temperature of the

coolers at receipt was 3.3 C.

Note: All samples which require thermal preservation are considered acceptable if the arrival temperature is within 2C of the required

temperature or method specified range. For samples with a specified temperature of 4C, samples with a temperature ranging from just

above freezing temperature of water to 6C shall be acceptable. Samples that are hand delivered immediately following collection may not

meet these criteria, however they will be deemed acceptable according to NELAC standards, if there is evidence that the chilling process

has begun, such as arrival on ice, etc.

TOTAL METALS

Samples 460-13139-2, 460-13139-4, 460-13139-5 and 460-13139-7 were analyzed for total metals in accordance with EPA SW-846

Method 6010B. The samples were prepared on 05/14/2010 and analyzed on 05/18/2010.

The matrix spike(MS) recoveries for antimony in batch 37477 was outside control limits. The associated laboratory control sample (LCS)

recovery met acceptance criteria.

Samples 460-13139-2(4X), 460-13139-4(4X), 460-13139-5(4X) and 460-13139-7(4X) required dilution prior to analysis. The reporting

limits have been adjusted accordingly.

As a standard practice all soil samples and related QC samples (i.e., MB, LCS, Dup, MS, SD) are diluted 2X-4X prior to analysis. Further

dilutions may be required dependent upon analyte levels in the samples. Refer to the analytical results forms for dilutions.

No other difficulties were encountered during the metals analyses.

All other quality control parameters were within the acceptance limits.

TOTAL MERCURY

Samples 460-13139-2, 460-13139-4, 460-13139-5 and 460-13139-7 were analyzed for total mercury in accordance with EPA SW-846

Method 7471A. The samples were prepared and analyzed on 05/14/2010.

No difficulties were encountered during the mercury analyses.

All quality control parameters were within the acceptance limits.

ORGANOCHLORINE PESTICIDES

Samples 460-13139-2, 460-13139-4, 460-13139-5 and 460-13139-7 were analyzed for organochlorine pesticides in accordance with EPA

SW-846 Method 8081A. The samples were prepared on 05/14/2010 and analyzed on 05/17/2010.

DCB surrogate recovery for the following sample(s) was outside control limits: 460-13139-4 on the primary column. Evidence of matrix

interference is present; therefore, re-extraction and/or re-analysis was not performed.

No other difficulties were encountered during the pesticides analyses.


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POLYCHLORINATED BIPHENYLS (PCBS)

Samples 460-13139-2, 460-13139-4, 460-13139-5 and 460-13139-7 were analyzed for polychlorinated biphenyls (PCBs) in accordance

with EPA SW-846 Method 8082. The samples were prepared and analyzed on 05/14/2010.

No difficulties were encountered during the PCBs analyses.


VOLATILE ORGANIC COMPOUNDS (GC-MS)

Samples 460-13139-2, 460-13139-4, 460-13139-5 and 460-13139-7 were analyzed for volatile organic compounds (GC-MS) in

accordance with EPA SW-846 Method 8260B. The samples were prepared on 05/14/2010 and analyzed on 05/18/2010.

No difficulties were encountered during the volatiles analyses.


SEMIVOLATILE ORGANIC COMPOUNDS (GC-MS)

Samples 460-13139-2, 460-13139-4, 460-13139-5 and 460-13139-7 were analyzed for semivolatile organic compounds (GC-MS) in

accordance with EPA SW-846 Method 8270C. The samples were prepared on 05/17/2010 and analyzed on 05/18/2010.

The laboratory control sample (LCS) for batch 37564 was outside control limits for the following analyte: Benzidine.

The matrix spike / matrix spike duplicate (MS/MSD) precision for batch 37564 was outside control limits for Benzidine.

The matrix spike / matrix spike duplicate (MS/MSD) recoveries for batch 37564 were outside control limits for 2,4-Dinitrophenol,

4,6-Dinitro-2-methylphenol and Benzidine.

No other difficulties were encountered during the semivolatiles analyses.


PERCENT SOLIDS

Samples 460-13139-1 through 460-13139-8 were analyzed for percent solids in accordance with ASTM D2974-87 Modified. The samples

were analyzed on 05/14/2010 and 05/17/2010.

No difficulties were encountered during the % solids analyses.


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SAMPLE SUMMARY

Client: Duffield Associates Job Number: 460-13139-1

Client Sample IDLab Sample ID Client Matrix

Date/Time

Sampled

Date/Time

Received

05/12/2010 0900 05/13/2010 1830TB-3 2-3460-13139-1 Soil

05/12/2010 0945 05/13/2010 1830TB-3 6-7460-13139-2 Soil

05/12/2010 1030 05/13/2010 1830TB-2 2-3460-13139-3 Soil

05/12/2010 1045 05/13/2010 1830TB-2 5-6460-13139-4 Soil

05/12/2010 1125 05/13/2010 1830TB-1 2-3460-13139-5 Soil

05/12/2010 1145 05/13/2010 1830TB-1 5-6460-13139-6 Soil

05/12/2010 1230 05/13/2010 1830TB-5 3-4460-13139-7 Soil

05/12/2010 1340 05/13/2010 1830TB-4 6-7460-13139-8 Soil

TestAmerica Edison

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EXECUTIVE SUMMARY - Detections


Analyte Result / Qualifier

Reporting

Limit Units Method

Lab Sample ID Client Sample ID

460-13139-1 TB-3 2-3

1.0 % Moisture17.9Percent Moisture

1.0 % Moisture82.1Percent Solids

460-13139-2 TB-3 6-7

41 ug/Kg 8270C28 JBenzo[a]anthracene

410 ug/Kg 8270C120 JBis(2-ethylhexyl) phthalate

1.2 mg/Kg 6010B1.9Arsenic

0.46 mg/Kg 6010B0.20 JBeryllium

2.3 mg/Kg 6010B9.1Chromium

5.8 mg/Kg 6010B13.9Copper

1.2 mg/Kg 6010B17.5Lead

9.3 mg/Kg 6010B7.0 JNickel

7.0 mg/Kg 6010B31.3Zinc



460-13139-3 TB-2 2-3



TestAmerica Edison

06/03/2010 of 623




Reporting

Limit Units Method


460-13139-4 TB-2 5-6

380 ug/Kg 8270C97 JAcenaphthylene

380 ug/Kg 8270C110 JAcenaphthene

380 ug/Kg 8270C150 JFluorene

380 ug/Kg 8270C1500Phenanthrene

380 ug/Kg 8270C240 JAnthracene

380 ug/Kg 8270C1800Fluoranthene

380 ug/Kg 8270C1500Pyrene

38 ug/Kg 8270C710Benzo[a]anthracene

380 ug/Kg 8270C960Chrysene


38 ug/Kg 8270C820Benzo[b]fluoranthene

38 ug/Kg 8270C300Benzo[k]fluoranthene

38 ug/Kg 8270C690Benzo[a]pyrene

38 ug/Kg 8270C610Indeno[1,2,3-cd]pyrene

38 ug/Kg 8270C130Dibenz(a,h)anthracene

380 ug/Kg 8270C680Benzo[g,h,i]perylene

77 ug/Kg 8081A170 pChlordane

7.7 ug/Kg 8081A554,4'-DDD

7.7 ug/Kg 8081A8.6 p4,4'-DDE

7.7 ug/Kg 8081A294,4'-DDT

7.7 ug/Kg 8081A5.5 J pDieldrin


0.46 mg/Kg 6010B0.37 JBeryllium

1.1 mg/Kg 6010B0.98 JCadmium



1.1 mg/Kg 6010B251Lead

9.2 mg/Kg 6010B11.9Nickel

2.3 mg/Kg 6010B4.9 BSilver

6.9 mg/Kg 6010B137Zinc

0.035 mg/Kg 7471A0.22Mercury



460-13139-5 TB-1 2-3




1.0 mg/Kg 6010B7.9Lead


6.1 mg/Kg 6010B19.2Zinc



TestAmerica Edison

06/03/2010 of 623




Reporting

Limit Units Method


460-13139-6 TB-1 5-6



460-13139-7 TB-5 3-4

860 ug/Kg 8270C200 JAcenaphthene

860 ug/Kg 8270C440 JFluorene

860 ug/Kg 8270C1800Phenanthrene

860 ug/Kg 8270C260 JAnthracene

860 ug/Kg 8270C1300Fluoranthene

860 ug/Kg 8270C790 JPyrene

86 ug/Kg 8270C380Benzo[a]anthracene

860 ug/Kg 8270C560 JChrysene


86 ug/Kg 8270C590Benzo[b]fluoranthene

86 ug/Kg 8270C230Benzo[k]fluoranthene

86 ug/Kg 8270C410Benzo[a]pyrene

86 ug/Kg 8270C460Indeno[1,2,3-cd]pyrene

860 ug/Kg 8270C460 JBenzo[g,h,i]perylene

17 ug/Kg 8081A16 J pgamma-BHC (Lindane)

170 ug/Kg 8081A1700Chlordane

17 ug/Kg 8081A18 p4,4'-DDE

17 ug/Kg 8081A28Dieldrin


2.5 mg/Kg 6010B1.1 JCadmium



2.5 mg/Kg 6010B222Lead


15.3 mg/Kg 6010B152Zinc

0.082 mg/Kg 7471A0.31Mercury



460-13139-8 TB-4 6-7



TestAmerica Edison

06/03/2010 of 623

METHOD SUMMARY

Job Number: 460-13139-1Client: Duffield Associates

Preparation MethodMethodLab LocationDescription

Matrix: Solid

SW846 8260BVolatile Organic Compounds (GC/MS) TAL EDI

SW846 5035TAL EDIClosed System Purge and Trap

SW846 8270CSemivolatile Compounds by Gas Chromatography/Mass

Spectrometry (GC/MS)

TAL EDI

SW846 3541TAL EDIAutomated Soxhlet Extraction

SW846 8081AOrganochlorine Pesticides (GC) TAL EDI


SW846 8082Polychlorinated Biphenyls (PCBs) by Gas Chromatography TAL EDI


SW846 6010BMetals (ICP) TAL EDI

SW846 3050BTAL EDIPreparation, Metals

SW846 7471AMercury (CVAA) TAL EDI

SW846 7471ATAL EDIPreparation, Mercury

EPA MoisturePercent Moisture TAL EDI

Lab References:

TAL EDI = TestAmerica Edison

Method References:

EPA = US Environmental Protection Agency

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

TestAmerica Edison

06/03/2010 of 623

METHOD / ANALYST SUMMARY


Method Analyst Analyst ID

Boykin, Kenneth KBSW846 8260B

Zhao, Chunxin CZSW846 8270C

Manlangit, Ferdie FMSW846 8081A

Diaz, Carol B CBDSW846 8082

Chang, Churn Der CDCSW846 6010B

Sheikh, Razia B RBSSW846 7471A

Dave, Virendra VDEPA Moisture

TestAmerica Edison

06/03/2010 of 623

Analytical Data


Client Sample ID:

Lab Sample ID:

TB-3 6-7

Client Matrix: % Moisture: 18.8

460-13139-2

Soil

Date Sampled: 05/12/2010 0945

Date Received: 05/13/2010 1830

8260B Volatile Organic Compounds (GC/MS)

Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

05/14/2010 0850

05/18/2010 0018

1.0

8260B Analysis Batch: 460-37643

Prep Batch: 460-37413

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID:

o37400.d

5.02 g

5 mL

5035

VOAMS12

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL

1.2 U 1.20.78Chloromethane

1.2 U 1.20.50Bromomethane

1.2 U 1.20.29Vinyl chloride

1.2 U 1.20.49Chloroethane

1.2 U 1.20.58Methylene Chloride

1.2 U 1.20.32Trichlorofluoromethane

1.2 U 1.20.451,1-Dichloroethene

1.2 U 1.20.311,1-Dichloroethane

1.2 U 1.20.35trans-1,2-Dichloroethene

1.2 U 1.20.29cis-1,2-Dichloroethene

1.2 U 1.20.29Chloroform


1.2 U 1.20.231,1,1-Trichloroethane

1.2 U 1.20.12Carbon tetrachloride

1.2 U 1.20.37Bromodichloromethane

1.2 U 1.20.391,2-Dichloropropane

1.2 U 1.20.25cis-1,3-Dichloropropene

1.2 U 1.20.45Trichloroethene

1.2 U 1.20.69Dibromochloromethane


1.2 U 1.20.91Benzene

1.2 U 1.20.27trans-1,3-Dichloropropene

6.1 U 6.11.62-Chloroethyl vinyl ether

1.2 U 1.20.86Bromoform

1.2 U 1.20.40Tetrachloroethene

1.2 U 1.20.931,1,2,2-Tetrachloroethane

1.2 U 1.20.37Toluene

1.2 U 1.20.59Chlorobenzene

1.2 U 1.20.23Ethylbenzene

3.7 U 3.70.96Xylenes, Total

Surrogate %Rec Acceptance LimitsQualifier

92 70 - 1381,2-Dichloroethane-d4 (Surr)

88 66 - 126Toluene-d8 (Surr)

102 72 - 132Bromofluorobenzene

TestAmerica Edison 06/03/2010 of 623

Analytical Data


Client Sample ID:

Lab Sample ID:

TB-3 6-7


460-13139-2

Soil

Date Sampled: 05/12/2010 0945



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

05/14/2010 0850

05/18/2010 0018

1.0





Lab File ID:

Instrument ID:

o37400.d

5.02 g

5 mL

5035

VOAMS12

Tentatively Identified Compounds

QualifierEst. Result (ug/Kg)RTAnalyteCas Number

0Number TIC's Found:

NoneTentatively Identified Compound


Analytical Data


Client Sample ID:

Lab Sample ID:

TB-2 5-6


460-13139-4

Soil

Date Sampled: 05/12/2010 1045



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

05/14/2010 0854

05/18/2010 0043

1.0





Lab File ID:

Instrument ID:

o37401.d

3.75 g

5 mL

5035

VOAMS12






















1.5 U 1.51.1Benzene















Analytical Data


Client Sample ID:

Lab Sample ID:

TB-2 5-6


460-13139-4

Soil

Date Sampled: 05/12/2010 1045



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

05/14/2010 0854

05/18/2010 0043

1.0





Lab File ID:

Instrument ID:

o37401.d

3.75 g

5 mL

5035

VOAMS12






Analytical Data


Client Sample ID:

Lab Sample ID:

TB-1 2-3


460-13139-5

Soil

Date Sampled: 05/12/2010 1125



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

05/14/2010 0855

05/18/2010 0108

1.0





Lab File ID:

Instrument ID:

o37402.d

3.09 g

5 mL

5035

VOAMS12






















1.7 U 1.71.3Benzene















Analytical Data


Client Sample ID:

Lab Sample ID:

TB-1 2-3


460-13139-5

Soil

Date Sampled: 05/12/2010 1125



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

05/14/2010 0855

05/18/2010 0108

1.0





Lab File ID:

Instrument ID:

o37402.d

3.09 g

5 mL

5035

VOAMS12






Analytical Data


Client Sample ID:

Lab Sample ID:

TB-5 3-4


460-13139-7

Soil

Date Sampled: 05/12/2010 1230



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

05/14/2010 0858

05/18/2010 0133

1.0





Lab File ID:

Instrument ID:

o37403.d

2.50 g

5 mL

5035

VOAMS12






















5.2 U 5.23.8Benzene


26 U 266.62-Chloroethyl vinyl ether




5.2 U 5.21.6Toluene



16 U 164.1Xylenes, Total






Analytical Data


Client Sample ID:

Lab Sample ID:

TB-5 3-4


460-13139-7

Soil

Date Sampled: 05/12/2010 1230



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

05/14/2010 0858

05/18/2010 0133

1.0





Lab File ID:

Instrument ID:

o37403.d

2.50 g

5 mL

5035

VOAMS12




67-64-1 1.94 1100Acetone

78-93-3 3.23 2202-Butanone (MEK)

10.68 28 T JUnknown


Analytical Data


Client Sample ID:

Lab Sample ID:

TB-3 6-7


460-13139-2

Soil

Date Sampled: 05/12/2010 0945


8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)

Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

05/17/2010 0900

05/18/2010 1500

1.0

8270C Analysis Batch: 460-37818


Injection Volume:



Lab File ID:

Instrument ID:

p2888.d

15.00 g

1 mL

3541

BNAMS10


410 U 41050Phenol

410 U 410542-Chlorophenol

410 U 410672-Nitrophenol

410 U 410652,4-Dimethylphenol

410 U 410652,4-Dichlorophenol

410 U 410684-Chloro-3-methylphenol

410 U 410732,4,6-Trichlorophenol

1200 U 1200862,4-Dinitrophenol


1200 U 12001904,6-Dinitro-2-methylphenol

1200 U 1200200Pentachlorophenol

410 U 41041N-Nitrosodimethylamine

41 U 418.5Bis(2-chloroethyl)ether

410 U 410561,3-Dichlorobenzene



41 U 415.4N-Nitrosodi-n-propylamine

41 U 416.9Hexachloroethane

41 U 419.1Nitrobenzene

410 U 41047Isophorone

410 U 41058Bis(2-chloroethoxy)methane

41 U 416.71,2,4-Trichlorobenzene

410 U 41060Naphthalene

83 U 8317Hexachlorobutadiene

410 U 410120Hexachlorocyclopentadiene

410 U 410582-Chloronaphthalene

410 U 41055Dimethyl phthalate

410 U 41058Acenaphthylene

83 U 83102,6-Dinitrotoluene

410 U 41058Acenaphthene


410 U 41055Diethyl phthalate

410 U 410704-Chlorophenyl phenyl ether

410 U 41069Fluorene

410 U 41066N-Nitrosodiphenylamine

410 U 410734-Bromophenyl phenyl ether

41 U 415.7Hexachlorobenzene

410 U 41071Phenanthrene

410 U 41072Anthracene

410 U 41062Di-n-butyl phthalate

410 U 41068Fluoranthene

410 U 41070Pyrene

410 U * 41087Benzidine

410 U 41048Butyl benzyl phthalate

830 U 830903,3'-Dichlorobenzidine

28 J 417.5Benzo[a]anthracene


Analytical Data


Client Sample ID:

Lab Sample ID:

TB-3 6-7


460-13139-2

Soil

Date Sampled: 05/12/2010 0945



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

05/17/2010 0900

05/18/2010 1500

1.0



Injection Volume:



Lab File ID:

Instrument ID:

p2888.d

15.00 g

1 mL

3541

BNAMS10


410 U 41059Chrysene

120 J 41054Bis(2-ethylhexyl) phthalate

410 U 41048Di-n-octyl phthalate

41 U 416.1Benzo[b]fluoranthene

41 U 415.7Benzo[k]fluoranthene

41 U 415.0Benzo[a]pyrene

41 U 416.5Indeno[1,2,3-cd]pyrene

41 U 414.9Dibenz(a,h)anthracene

410 U 41043Benzo[g,h,i]perylene

410 U 41053bis (2-chloroisopropyl) ether


80 38 - 105Nitrobenzene-d5

82 41 - 118Phenol-d5

100 16 - 151Terphenyl-d14

78 10 - 1202,4,6-Tribromophenol

76 37 - 1252-Fluorophenol

78 40 - 1092-Fluorobiphenyl


Analytical Data


Client Sample ID:

Lab Sample ID:

TB-3 6-7


460-13139-2

Soil

Date Sampled: 05/12/2010 0945



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

05/17/2010 0900

05/18/2010 1500

1.0



Injection Volume:



Lab File ID:

Instrument ID:

p2888.d

15.00 g

1 mL

3541

BNAMS10






Analytical Data


Client Sample ID:

Lab Sample ID:

TB-2 5-6


460-13139-4

Soil

Date Sampled: 05/12/2010 1045



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

05/17/2010 0900

05/18/2010 2025

1.0



Injection Volume:



Lab File ID:

Instrument ID:

p2900.d

15.05 g

1 mL

3541

BNAMS10


380 U 38046Phenol



























97 J 38054Acenaphthylene

77 U 779.62,6-Dinitrotoluene

110 J 38054Acenaphthene




150 J 38064Fluorene




1500 38066Phenanthrene

240 J 38067Anthracene


1800 38063Fluoranthene

1500 38065Pyrene




710 387.0Benzo[a]anthracene


Analytical Data


Client Sample ID:

Lab Sample ID:

TB-2 5-6


460-13139-4

Soil

Date Sampled: 05/12/2010 1045



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

05/17/2010 0900

05/18/2010 2025

1.0



Injection Volume:



Lab File ID:

Instrument ID:

p2900.d

15.05 g

1 mL

3541

BNAMS10


960 38055Chrysene



820 385.6Benzo[b]fluoranthene

300 385.3Benzo[k]fluoranthene

690 384.7Benzo[a]pyrene

610 386.0Indeno[1,2,3-cd]pyrene

130 384.5Dibenz(a,h)anthracene

680 38040Benzo[g,h,i]perylene




60 41 - 118Phenol-d5






Analytical Data


Client Sample ID:

Lab Sample ID:

TB-2 5-6


460-13139-4

Soil

Date Sampled: 05/12/2010 1045



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

05/17/2010 0900

05/18/2010 2025

1.0



Injection Volume:



Lab File ID:

Instrument ID:

p2900.d

15.05 g

1 mL

3541

BNAMS10




9.23 400 T JC15H12 PAH-1

9.25 440 T JC15H12 PAH-2

9.33 550 T JC15H10/C15H12 PAHs

9.36 320 T JC15H12 PAH-3

84-65-1 9.54 510 T J N9,10-Anthracenedione

9.77 330 T JC16H14 PAH

10.49 370 T JC17H12 PAH-1

10.60 380 T JC17H12 PAH-2

13.25 500 T JC20H12 PAH


Analytical Data


Client Sample ID:

Lab Sample ID:

TB-1 2-3


460-13139-5

Soil

Date Sampled: 05/12/2010 1125



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

05/17/2010 0900

05/18/2010 1152

1.0



Injection Volume:



Lab File ID:

Instrument ID:

p2881.d

15.02 g

1 mL

3541

BNAMS10


350 U 35043Phenol

































350 U 35060Fluorene








350 U 35061Pyrene




35 U 356.5Benzo[a]anthracene


Analytical Data


Client Sample ID:

Lab Sample ID:

TB-1 2-3


460-13139-5

Soil

Date Sampled: 05/12/2010 1125



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

05/17/2010 0900

05/18/2010 1152

1.0



Injection Volume:



Lab File ID:

Instrument ID:

p2881.d

15.02 g

1 mL

3541

BNAMS10


350 U 35051Chrysene

350 U 35047Bis(2-ethylhexyl) phthalate











68 41 - 118Phenol-d5






Analytical Data


Client Sample ID:

Lab Sample ID:

TB-1 2-3


460-13139-5

Soil

Date Sampled: 05/12/2010 1125



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

05/17/2010 0900

05/18/2010 1152

1.0



Injection Volume:



Lab File ID:

Instrument ID:

p2881.d

15.02 g

1 mL

3541

BNAMS10






Analytical Data


Client Sample ID:

Lab Sample ID:

TB-5 3-4


460-13139-7

Soil

Date Sampled: 05/12/2010 1230



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

05/17/2010 0900

05/18/2010 1958

1.0



Injection Volume:



Lab File ID:

Instrument ID:

p2899.d

15.01 g

1 mL

3541

BNAMS10


860 U 860110Phenol












86 U 8618Bis(2-chloroethyl)ether




86 U 8611N-Nitrosodi-n-propylamine

86 U 8614Hexachloroethane

86 U 8619Nitrobenzene



86 U 86141,2,4-Trichlorobenzene








200 J 860120Acenaphthene




440 J 860150Fluorene



86 U 8612Hexachlorobenzene

1800 860150Phenanthrene

260 J 860150Anthracene


1300 860140Fluoranthene

790 J 860150Pyrene




380 8616Benzo[a]anthracene


Analytical Data


Client Sample ID:

Lab Sample ID:

TB-5 3-4


460-13139-7

Soil

Date Sampled: 05/12/2010 1230



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

05/17/2010 0900

05/18/2010 1958

1.0



Injection Volume:



Lab File ID:

Instrument ID:

p2899.d

15.01 g

1 mL

3541

BNAMS10


560 J 860120Chrysene



590 8613Benzo[b]fluoranthene

230 8612Benzo[k]fluoranthene

410 8611Benzo[a]pyrene

460 8614Indeno[1,2,3-cd]pyrene

86 U 8610Dibenz(a,h)anthracene

460 J 86091Benzo[g,h,i]perylene




41 41 - 118Phenol-d5






Analytical Data


Client Sample ID:

Lab Sample ID:

TB-5 3-4


460-13139-7

Soil

Date Sampled: 05/12/2010 1230



Method:

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

05/17/2010 0900

05/18/2010 1958

1.0



Injection Volume:



Lab File ID:

Instrument ID:

p2899.d

15.01 g

1 mL

3541

BNAMS10




12.11 5400 T JUnknown-1

12.22 13000 T JUnknown Alkane-1


13.86 4200 T JUnknown-2

7616-22-0 13.96 8500 T J N.gamma.-Tocopherol


59-02-9 14.36 11000 T J NVitamin E

15.02 3800 T JUnknown-3

15.21 6500 T JUnknown-4

15.37 10000 T JUnknown-5

15.62 30000 T JUnknown-6

15.72 10000 T JUnknown Sterol

1000194-62-4 15.77 30000 T J N4,4,6a,6b,8a,11,11,14b-Octamethyl-1,4,4a

15.81 4700 T JUnknown-7

15.86 9800 T JUnknown-8

15.98 22000 T JUnknown-9

16.11 36000 T JUnknown-10

16.27 11000 T JUnknown-11

16.32 23000 T JUnknown-12

16.37 10000 T JUnknown-13

16.44 10000 T JUnknown-14

16.55 13000 T JUnknown-15

16.75 3400 T JUnknown-16

16.86 5100 T JUnknown-17

17.40 4500 T JUnknown-18


Analytical Data


Client Sample ID:

Lab Sample ID:

TB-3 6-7


460-13139-2

Soil

Date Sampled: 05/12/2010 0945


Method:

8081A Organochlorine Pesticides (GC)

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A

3541

1.0

05/17/2010 0800

05/14/2010 0915

Analysis Batch: 460-37575


Instrument ID:



Injection Volume:

Result Type: PRIMARY

15.00 g

10 mL

1 uL

PESTGC1


8.3 U 8.31.8Aldrin

8.3 U 8.31.5alpha-BHC

8.3 U 8.31.1beta-BHC

8.3 U 8.31.3delta-BHC

8.3 U 8.30.96gamma-BHC (Lindane)

83 U 8318Chlordane

8.3 U 8.30.994,4'-DDD

8.3 U 8.31.64,4'-DDE

8.3 U 8.31.04,4'-DDT

8.3 U 8.31.6Dieldrin

8.3 U 8.31.7Endosulfan I

8.3 U 8.31.2Endosulfan II

8.3 U 8.31.1Endosulfan sulfate

8.3 U 8.31.2Endrin

8.3 U 8.32.1Endrin aldehyde

8.3 U 8.31.2Heptachlor

8.3 U 8.31.7Heptachlor epoxide

83 U 8317Toxaphene


115 22 - 141Tetrachloro-m-xylene

125 10 - 165DCB Decachlorobiphenyl


Analytical Data


Client Sample ID:

Lab Sample ID:

TB-3 6-7


460-13139-2

Soil

Date Sampled: 05/12/2010 0945


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A

3541

1.0

05/17/2010 0800

05/14/2010 0915



Instrument ID:



Injection Volume:

Result Type: SECONDARY

15.00 g

10 mL

1 uL

PESTGC1





Analytical Data


Client Sample ID:

Lab Sample ID:

TB-2 5-6


460-13139-4

Soil

Date Sampled: 05/12/2010 1045


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A

3541

1.0

05/17/2010 0827

05/14/2010 0915



Instrument ID:



Injection Volume:


15.01 g

10 mL

1 uL

PESTGC1


7.7 U 7.71.7Aldrin


7.7 U 7.71.0beta-BHC



170 p 7717Chlordane

55 7.70.924,4'-DDD

8.6 p 7.71.54,4'-DDE

29 7.70.964,4'-DDT

5.5 J p 7.71.5Dieldrin




7.7 U 7.71.1Endrin




77 U 7716Toxaphene



168 10 - 165XDCB Decachlorobiphenyl


Analytical Data


Client Sample ID:

Lab Sample ID:

TB-2 5-6


460-13139-4

Soil

Date Sampled: 05/12/2010 1045


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A

3541

1.0

05/17/2010 0827

05/14/2010 0915



Instrument ID:



Injection Volume:


15.01 g

10 mL

1 uL

PESTGC1





Analytical Data


Client Sample ID:

Lab Sample ID:

TB-1 2-3


460-13139-5

Soil

Date Sampled: 05/12/2010 1125


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A

3541

1.0

05/17/2010 0841

05/14/2010 0915



Instrument ID:



Injection Volume:


15.00 g

10 mL

1 uL

PESTGC1


7.2 U 7.21.6Aldrin


7.2 U 7.20.97beta-BHC



72 U 7216Chlordane

7.2 U 7.20.864,4'-DDD

7.2 U 7.21.44,4'-DDE

7.2 U 7.20.904,4'-DDT





7.2 U 7.21.0Endrin




72 U 7215Toxaphene





Analytical Data


Client Sample ID:

Lab Sample ID:

TB-1 2-3


460-13139-5

Soil

Date Sampled: 05/12/2010 1125


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A

3541

1.0

05/17/2010 0841

05/14/2010 0915



Instrument ID:



Injection Volume:


15.00 g

10 mL

1 uL

PESTGC1





Analytical Data


Client Sample ID:

Lab Sample ID:

TB-5 3-4


460-13139-7

Soil

Date Sampled: 05/12/2010 1230


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A

3541

1.0

05/17/2010 0909

05/14/2010 0915



Instrument ID:



Injection Volume:


15.00 g

10 mL

1 uL

PESTGC1


17 U 173.8Aldrin

17 U 173.2alpha-BHC

17 U 172.4beta-BHC

17 U 172.7delta-BHC

16 J p 172.0gamma-BHC (Lindane)

1700 17038Chlordane

17 U 172.14,4'-DDD

18 p 173.44,4'-DDE

17 U 172.24,4'-DDT

28 173.4Dieldrin

17 U 173.7Endosulfan I

17 U 172.6Endosulfan II

17 U 172.2Endosulfan sulfate

17 U 172.4Endrin

17 U 174.3Endrin aldehyde

17 U 172.5Heptachlor

17 U 173.5Heptachlor epoxide

170 U 17036Toxaphene





Analytical Data


Client Sample ID:

Lab Sample ID:

TB-5 3-4


460-13139-7

Soil

Date Sampled: 05/12/2010 1230


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8081A

3541

1.0

05/17/2010 0909

05/14/2010 0915



Instrument ID:



Injection Volume:


15.00 g

10 mL

1 uL

PESTGC1





Analytical Data


Client Sample ID:

Lab Sample ID:

TB-3 6-7


460-13139-2

Soil

Date Sampled: 05/12/2010 0945


Method:

8082 Polychlorinated Biphenyls (PCBs) by Gas Chromatography

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8082

3541

1.0

05/14/2010 1959

05/14/2010 0719



Instrument ID:



Injection Volume:


15.00 g

10 mL

PESTGC7


83 U 8316Aroclor 1016

83 U 8325Aroclor 1221

83 U 8347Aroclor 1232

83 U 8316Aroclor 1242

83 U 8322Aroclor 1248

83 U 8328Aroclor 1254

83 U 839.2Aroclor 1260

83 U 8314Aroclor 1262

83 U 8314Aroclor 1268




Analytical Data


Client Sample ID:

Lab Sample ID:

TB-3 6-7


460-13139-2

Soil

Date Sampled: 05/12/2010 0945


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8082

3541

1.0

05/14/2010 1959

05/14/2010 0719



Instrument ID:



Injection Volume:


15.00 g

10 mL

PESTGC7




Analytical Data


Client Sample ID:

Lab Sample ID:

TB-2 5-6


460-13139-4

Soil

Date Sampled: 05/12/2010 1045


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8082

3541

1.0

05/14/2010 2032

05/14/2010 0719



Instrument ID:



Injection Volume:


15.03 g

10 mL

PESTGC7


77 U 7715Aroclor 1016

77 U 7723Aroclor 1221

77 U 7743Aroclor 1232

77 U 7715Aroclor 1242

77 U 7720Aroclor 1248

77 U 7726Aroclor 1254

77 U 778.6Aroclor 1260

77 U 7713Aroclor 1262

77 U 7713Aroclor 1268




Analytical Data


Client Sample ID:

Lab Sample ID:

TB-2 5-6


460-13139-4

Soil

Date Sampled: 05/12/2010 1045


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8082

3541

1.0

05/14/2010 2032

05/14/2010 0719



Instrument ID:



Injection Volume:


15.03 g

10 mL

PESTGC7




Analytical Data


Client Sample ID:

Lab Sample ID:

TB-1 2-3


460-13139-5

Soil

Date Sampled: 05/12/2010 1125


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8082

3541

1.0

05/14/2010 2048

05/14/2010 0719



Instrument ID:



Injection Volume:


15.02 g

10 mL

PESTGC7


72 U 7214Aroclor 1016

72 U 7222Aroclor 1221

72 U 7241Aroclor 1232

72 U 7214Aroclor 1242

72 U 7219Aroclor 1248

72 U 7224Aroclor 1254

72 U 728.0Aroclor 1260

72 U 7212Aroclor 1262

72 U 7212Aroclor 1268




Analytical Data


Client Sample ID:

Lab Sample ID:

TB-1 2-3


460-13139-5

Soil

Date Sampled: 05/12/2010 1125


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8082

3541

1.0

05/14/2010 2048

05/14/2010 0719



Instrument ID:



Injection Volume:


15.02 g

10 mL

PESTGC7




Analytical Data


Client Sample ID:

Lab Sample ID:

TB-5 3-4


460-13139-7

Soil

Date Sampled: 05/12/2010 1230


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8082

3541

1.0

05/14/2010 2121

05/14/2010 0719



Instrument ID:



Injection Volume:


15.02 g

10 mL

PESTGC7


170 U 17033Aroclor 1016

170 U 17052Aroclor 1221

170 U 17099Aroclor 1232

170 U 17033Aroclor 1242

170 U 17046Aroclor 1248

170 U 17059Aroclor 1254

170 U 17019Aroclor 1260

170 U 17030Aroclor 1262

170 U 17030Aroclor 1268




Analytical Data


Client Sample ID:

Lab Sample ID:

TB-5 3-4


460-13139-7

Soil

Date Sampled: 05/12/2010 1230


Method:


Preparation:

Dilution:

Date Analyzed:

Date Prepared:

8082

3541

1.0

05/14/2010 2121

05/14/2010 0719



Instrument ID:



Injection Volume:


15.02 g

10 mL

PESTGC7




Analytical Data


Client Sample ID:

Lab Sample ID:

TB-3 6-7


460-13139-2

Soil

Date Sampled: 05/12/2010 0945


6010B Metals (ICP)

Method: 6010B Analysis Batch: 460-37705 Instrument ID:

Preparation: Prep Batch: 460-37477 Lab File ID: 05182010A.txt

Dilution: 4.0 Initial Weight/Volume: 1.06 g

Date Analyzed: 05/18/2010 1155 Final Weight/Volume: 50 mL

Date Prepared: 05/14/2010 1542

3050B

ICP4

Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL

2.3 U 2.31.0Antimony

1.9 1.20.81Arsenic

0.20 J 0.460.20Beryllium

1.2 U 1.20.18Cadmium

9.1 2.31.4Chromium

13.9 5.80.95Copper

17.5 1.20.58Lead

7.0 J 9.30.62Nickel

2.3 U 2.31.1Selenium

2.3 U 2.30.18Silver

2.3 U 2.31.1Thallium

31.3 7.01.1Zinc

7471A Mercury (CVAA)

Method: 7471A Analysis Batch: 460-37472 Instrument ID:

Preparation: Prep Batch: 460-37424 Lab File ID: 37424hg1.PRN




7471A

LEEMAN5


0.039 U 0.0390.030Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

TB-2 5-6


460-13139-4

Soil

Date Sampled: 05/12/2010 1045


6010B Metals (ICP)






3050B

ICP4



4.5 1.10.80Arsenic

0.37 J 0.460.20Beryllium

0.98 J 1.10.18Cadmium

17.9 2.31.4Chromium

71.8 5.70.94Copper

251 1.10.57Lead

11.9 9.20.61Nickel


4.9 B 2.30.17Silver


137 6.91.1Zinc







7471A

LEEMAN5


0.22 0.0350.028Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

TB-1 2-3


460-13139-5

Soil

Date Sampled: 05/12/2010 1125


6010B Metals (ICP)






3050B

ICP4



1.4 1.00.70Arsenic

0.40 U 0.400.18Beryllium

1.0 U 1.00.16Cadmium

4.6 2.01.2Chromium

7.2 5.00.82Copper

7.9 1.00.50Lead

5.4 J 8.10.54Nickel


2.0 U 2.00.15Silver


19.2 6.10.99Zinc







7471A

LEEMAN5


0.035 U 0.0350.028Mercury


Analytical Data


Client Sample ID:

Lab Sample ID:

TB-5 3-4


460-13139-7

Soil

Date Sampled: 05/12/2010 1230


6010B Metals (ICP)






3050B

ICP4



3.2 2.51.8Arsenic


1.1 J 2.50.40Cadmium

6.7 5.13.0Chromium

22.0 12.72.1Copper

222 2.51.3Lead

7.0 J 20.41.4Nickel


5.1 U 5.10.39Silver


152 15.32.5Zinc







7471A

LEEMAN5


0.31 0.0820.064Mercury


Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

TB-3 2-3

Client Matrix:

460-13139-1

Soil

Date Sampled: 05/12/2010 0900


Analyte Result Qual Units RL RL Dil Method

Percent Moisture 17.9 % 1.0 1.0 1.0 Moisture

Analysis Batch: 460-37508 DryWt Corrected: NDate Analyzed: 05/14/2010 2147

Percent Solids 82.1 % 1.0 1.0 1.0 Moisture



Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

TB-3 6-7

Client Matrix:

460-13139-2

Soil

Date Sampled: 05/12/2010 0945








Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

TB-2 2-3

Client Matrix:

460-13139-3

Soil

Date Sampled: 05/12/2010 1030








Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

TB-2 5-6

Client Matrix:

460-13139-4

Soil

Date Sampled: 05/12/2010 1045








Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

TB-1 2-3

Client Matrix:

460-13139-5

Soil

Date Sampled: 05/12/2010 1125








Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

TB-1 5-6

Client Matrix:

460-13139-6

Soil

Date Sampled: 05/12/2010 1145








Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

TB-5 3-4

Client Matrix:

460-13139-7

Soil

Date Sampled: 05/12/2010 1230








Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

TB-4 6-7

Client Matrix:

460-13139-8

Soil

Date Sampled: 05/12/2010 1340








Quality Control Results


Surrogate Recovery Report


Client Matrix: Solid


DCA TOL BFB

%Rec %Rec %Rec

460-13139-2 TB-3 6-7 92 88 102

460-13139-4 TB-2 5-6 95 89 105

460-13139-5 TB-1 2-3 100 90 108

460-13139-7 TB-5 3-4 89 73 92

MB 460-37643/5 104 92 107

LCS 460-37643/3 89 90 108

LCSD 460-37643/4 90 95 106

Surrogate Acceptance Limits

DCA = 1,2-Dichloroethane-d4 (Surr) 70-138

TOL = Toluene-d8 (Surr) 66-126

BFB = Bromofluorobenzene 72-132

TestAmerica Edison

06/03/2010 of 623







2FP PHL NBZ FBP TBP TPH

%Rec %Rec %Rec %Rec %Rec %Rec

460-13139-2 TB-3 6-7 76 82 80 78 78 100

460-13139-4 TB-2 5-6 55 60 59 67 53 74

460-13139-5 TB-1 2-3 58 68 70 69 93 91

460-13139-7 TB-5 3-4 39 41 55 60 52 54

MB 460-37564/1-A 76 82 80 78 82 93

LCS 460-37564/2-A 74 78 82 80 99 89

460-13139-5 MS TB-1 2-3 MS 74 79 80 80 67 91

460-13139-5 MSD TB-1 2-3 MSD 72 75 81 82 66 89


2FP = 2-Fluorophenol 37-125

PHL = Phenol-d5 41-118

NBZ = Nitrobenzene-d5 38-105

FBP = 2-Fluorobiphenyl 40-109

TBP = 2,4,6-Tribromophenol 10-120

TPH = Terphenyl-d14 16-151

TestAmerica Edison

06/03/2010 of 623







TCX1 TCX2 DCB1 DCB2

%Rec %Rec %Rec %Rec

460-13139-2 TB-3 6-7 115 112 125 105

460-13139-4 TB-2 5-6 121 106 155 168X

460-13139-5 TB-1 2-3 117 113 138 118

460-13139-7 TB-5 3-4 84 76 78 75

MB 460-37420/1-A 76 75 145 118

LCS 460-37420/2-A 75 71 93 92

460-13147-A-2-B MS 107 94 132 123

460-13147-A-2-C

MSD

101 91 147 56p


TCX = Tetrachloro-m-xylene 22-141

DCB = DCB Decachlorobiphenyl 10-165

TestAmerica Edison

06/03/2010 of 623







DCB1 DCB2

%Rec %Rec

460-13139-2 TB-3 6-7 106 108

460-13139-4 TB-2 5-6 110 97

460-13139-5 TB-1 2-3 109 113

460-13139-7 TB-5 3-4 65 55

MB 460-37391/1-A 98 94

LCS 460-37391/2-A 104 110

460-13137-A-1-B MS 108 106

460-13137-A-1-C

MSD

91 91



TestAmerica Edison

06/03/2010 of 623



SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

05/17/2010 2011

Method Blank - Batch: 460-37643

Date Prepared:

Instrument ID:

Lab File ID:




Prep Batch: N/A o37390.d

5 mL

5 mL

N/A

Units: ug/Kg

Method: 8260B

Preparation: N/A

VOAMS12MB 460-37643/5

Analyte RLMDLQualResult





















1.0 U 1.00.74Benzene










Surrogate % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 104 70 - 138

Toluene-d8 (Surr) 92 66 - 126

Bromofluorobenzene 107 72 - 132

Method Blank TICs- Batch: 460-37643

Cas Number Analyte RT Est. Result Qual

Tentatively Identified Compound None




Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

05/17/2010 1746

05/17/2010 1810

Lab Control Sample/

Lab Control Sample Duplicate Recovery Report - Batch: 460-37643

1.0

1.0

Solid

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:




Date Prepared:

Units:

Instrument ID:

Lab File ID:



ug/Kg

Prep Batch: N/A


N/A

o37386.d

5 mL

5 mL

o37387.d

5 mL

5 mL

ug/Kg


Prep Batch: N/A

Method: 8260B

Preparation: N/A

N/A

VOAMS12

VOAMS12

LCS 460-37643/3

LCSD 460-37643/4

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

% Rec.

9696 50 - 151 0 30Chloromethane

111110 54 - 142 1 30Bromomethane

9897 67 - 133 0 30Vinyl chloride

10099 56 - 146 0 30Chloroethane

134120 74 - 137 11 30Methylene Chloride

105107 61 - 139 2 30Trichlorofluoromethane

116104 71 - 126 11 301,1-Dichloroethene

10899 76 - 125 8 301,1-Dichloroethane

10899 75 - 122 9 30trans-1,2-Dichloroethene

110100 80 - 120 10 30cis-1,2-Dichloroethene

10999 77 - 120 9 30Chloroform

10898 76 - 118 9 301,2-Dichloroethane

115103 78 - 117 11 301,1,1-Trichloroethane

116107 79 - 118 8 30Carbon tetrachloride

115100 79 - 119 14 30Bromodichloromethane

10598 82 - 122 8 301,2-Dichloropropane

10994 80 - 123 15 30cis-1,3-Dichloropropene

10699 79 - 119 7 30Trichloroethene

9183 68 - 120 9 30Dibromochloromethane

10089 73 - 118 12 301,1,2-Trichloroethane

11099 77 - 117 11 30Benzene

8776 67 - 121 14 30trans-1,3-Dichloropropene

8783 74 - 120 5 302-Chloroethyl vinyl ether

8473 59 - 125 13 30Bromoform

11193 80 - 120 18 30Tetrachloroethene

10195 79 - 122 7 301,1,2,2-Tetrachloroethane

10996 75 - 115 12 30Toluene

110100 80 - 120 9 30Chlorobenzene

111105 81 - 121 5 30Ethylbenzene

112103 82 - 122 8 30Xylenes, Total

Surrogate LCS % Rec LCSD % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 89 90 70 - 138

Toluene-d8 (Surr) 90 95 66 - 126




Surrogate LCS % Rec LCSD % Rec Acceptance Limits

Bromofluorobenzene 108 106 72 - 132

Solid

Date Analyzed: Date Analyzed:05/17/2010 1746 05/17/2010 1810

Dilution: Dilution:1.0 1.0

LCS Lab Sample ID:

Client Matrix:

Date Prepared:

LCSD Lab Sample ID:


Date Prepared:N/A N/A

Laboratory Control/

Laboratory Duplicate Data Report - Batch: 460-37643

Method: 8260B

Preparation: N/A

Units: ug/KgLCS 460-37643/3 LCSD 460-37643/4

LCSD

Result/Qual

LCS

Result/Qual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

19.219.220.0 20.0Chloromethane

22.322.020.0 20.0Bromomethane

19.519.520.0 20.0Vinyl chloride

19.919.920.0 20.0Chloroethane

26.823.920.0 20.0Methylene Chloride

21.121.520.0 20.0Trichlorofluoromethane

23.120.820.0 20.01,1-Dichloroethene

21.519.820.0 20.01,1-Dichloroethane

21.619.820.0 20.0trans-1,2-Dichloroethene

22.120.020.0 20.0cis-1,2-Dichloroethene

21.819.920.0 20.0Chloroform

21.519.620.0 20.01,2-Dichloroethane

23.020.520.0 20.01,1,1-Trichloroethane

23.321.520.0 20.0Carbon tetrachloride

23.120.120.0 20.0Bromodichloromethane

21.119.520.0 20.01,2-Dichloropropane

21.818.720.0 20.0cis-1,3-Dichloropropene

21.219.820.0 20.0Trichloroethene

18.316.720.0 20.0Dibromochloromethane

20.017.820.0 20.01,1,2-Trichloroethane

21.919.720.0 20.0Benzene

17.515.220.0 20.0trans-1,3-Dichloropropene

17.416.520.0 20.02-Chloroethyl vinyl ether

16.814.720.0 20.0Bromoform

22.318.620.0 20.0Tetrachloroethene

20.318.920.0 20.01,1,2,2-Tetrachloroethane

21.719.220.0 20.0Toluene

21.920.020.0 20.0Chlorobenzene

22.121.120.0 20.0Ethylbenzene

67.161.960.0 60.0Xylenes, Total




SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

05/18/2010 1057


Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:



05/17/2010 0900

p2879.d

15.02 g

1 mL

Units: ug/Kg

Method: 8270C

Preparation: 3541

BNAMS10MB 460-37564/1-A


330 U 33040Phenol

































330 U 33056Fluorene








330 U 33057Pyrene

330 U 33070Benzidine




SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

05/18/2010 1057


Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:



05/17/2010 0900

p2879.d

15.02 g

1 mL

Units: ug/Kg

Method: 8270C

Preparation: 3541

BNAMS10MB 460-37564/1-A




33 U 336.1Benzo[a]anthracene

330 U 33048Chrysene

330 U 33044Bis(2-ethylhexyl) phthalate










Nitrobenzene-d5 80 38 - 105

Phenol-d5 82 41 - 118

Terphenyl-d14 93 16 - 151

2,4,6-Tribromophenol 82 10 - 120

2-Fluorophenol 76 37 - 125

2-Fluorobiphenyl 78 40 - 109

Method Blank TICs- Batch: 460-37564

Cas Number Analyte RT Est. Result Qual

2.30Unknown Aldol Condensate-1 497 T A J

2.72Unknown Aldol Condensate-2 16600 T A J




Solid

1.0

05/18/2010 1125Date Analyzed:

Lab Control Sample - Batch: 460-37564

Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

p2880.d

05/17/2010 0900



15.00 g

1 mL

Units: ug/Kg

Method: 8270C

Preparation: 3541

BNAMS10LCS 460-37564/2-A

Analyte QualLimit% Rec.ResultSpike Amount

6670 4950 74 54 - 115Phenol

6670 5140 77 56 - 1102-Chlorophenol

6670 5640 85 55 - 1012-Nitrophenol

6670 5280 79 56 - 1122,4-Dimethylphenol

6670 5340 80 58 - 1152,4-Dichlorophenol

6670 5690 85 55 - 1174-Chloro-3-methylphenol

6670 5360 80 53 - 1182,4,6-Trichlorophenol

6670 1100 16 10 - 1292,4-Dinitrophenol

6670 6490 97 45 - 1144-Nitrophenol

6670 2180 33 10 - 1104,6-Dinitro-2-methylphenol

6670 4830 72 19 - 113Pentachlorophenol

3330 2550 77 40 - 84N-Nitrosodimethylamine

3330 3020 91 44 - 101Bis(2-chloroethyl)ether

3330 2490 75 47 - 841,3-Dichlorobenzene



3330 3040 91 42 - 107N-Nitrosodi-n-propylamine

3330 2480 74 45 - 90Hexachloroethane

3330 2640 79 42 - 106Nitrobenzene

3330 2850 86 48 - 97Isophorone

3330 2860 86 51 - 100Bis(2-chloroethoxy)methane

3330 2740 82 48 - 941,2,4-Trichlorobenzene

3330 2710 81 53 - 94Naphthalene

3330 2710 81 45 - 98Hexachlorobutadiene

3330 3110 93 24 - 98Hexachlorocyclopentadiene

3330 2700 81 51 - 1022-Chloronaphthalene

3330 2960 89 52 - 112Dimethyl phthalate

3330 2780 83 51 - 103Acenaphthylene

3330 3130 94 51 - 1152,6-Dinitrotoluene

3330 2840 85 46 - 100Acenaphthene

3330 3200 96 53 - 1102,4-Dinitrotoluene

3330 3000 90 52 - 114Diethyl phthalate

3330 2910 87 50 - 1064-Chlorophenyl phenyl ether

3330 2890 87 51 - 108Fluorene

3330 3110 93 49 - 106N-Nitrosodiphenylamine

3330 2910 87 44 - 1024-Bromophenyl phenyl ether

3330 2940 88 43 - 104Hexachlorobenzene

3330 2850 86 48 - 108Phenanthrene

3330 2870 86 50 - 107Anthracene

3330 2980 89 50 - 108Di-n-butyl phthalate

3330 3040 91 49 - 108Fluoranthene

3330 2850 85 49 - 116Pyrene

3330 169 5 J *10 - 61Benzidine

3330 3010 90 49 - 117Butyl benzyl phthalate




Solid

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

p2880.d

05/17/2010 0900



15.00 g

1 mL

Units: ug/Kg

Method: 8270C

Preparation: 3541

BNAMS10LCS 460-37564/2-A


3330 2870 86 24 - 1053,3'-Dichlorobenzidine

3330 2880 86 46 - 112Benzo[a]anthracene

3330 2900 87 45 - 114Chrysene

3330 3010 90 49 - 119Bis(2-ethylhexyl) phthalate

3330 3130 94 40 - 106Di-n-octyl phthalate

3330 3060 92 33 - 96Benzo[b]fluoranthene

3330 2990 90 35 - 115Benzo[k]fluoranthene

3330 2590 78 36 - 89Benzo[a]pyrene

3330 2870 86 43 - 109Indeno[1,2,3-cd]pyrene

3330 2900 87 43 - 107Dibenz(a,h)anthracene

3330 2980 89 43 - 106Benzo[g,h,i]perylene

3330 2700 81 45 - 102bis (2-chloroisopropyl) ether


Nitrobenzene-d5 82 38 - 105

Phenol-d5 78 41 - 118

Terphenyl-d14 89 16 - 151

2,4,6-Tribromophenol 99 10 - 120

2-Fluorophenol 74 37 - 125

2-Fluorobiphenyl 80 40 - 109




Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

05/18/2010 1218

05/18/2010 1246

Solid

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 460-37564

1.0

1.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

Instrument ID:

Lab File ID:



Injection Volume:




05/17/2010 0900

05/17/2010 0900



p2882.d

15.04 g

1 mL

p2883.d

15.03 g

1 mL

Method: 8270C

Preparation: 3541

BNAMS10

BNAMS10

460-13139-5

460-13139-5

Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS

% Rec.

76 73 54 - 115 5 30Phenol

76 75 56 - 110 1 302-Chlorophenol

81 79 55 - 101 3 302-Nitrophenol

78 75 56 - 112 4 302,4-Dimethylphenol

80 76 58 - 115 4 302,4-Dichlorophenol

86 80 55 - 117 7 304-Chloro-3-methylphenol

67 66 53 - 118 2 302,4,6-Trichlorophenol

0 0 10 - 129 NC 30 U F U F2,4-Dinitrophenol

65 65 45 - 114 0 304-Nitrophenol

3 0 10 - 110 NC 30 J F U F4,6-Dinitro-2-methylphenol

22 21 19 - 113 4 30Pentachlorophenol

74 75 40 - 84 1 30N-Nitrosodimethylamine

90 88 44 - 101 2 30Bis(2-chloroethyl)ether

66 67 47 - 84 2 301,3-Dichlorobenzene



91 87 42 - 107 5 30N-Nitrosodi-n-propylamine

66 68 45 - 90 2 30Hexachloroethane

76 76 42 - 106 0 30Nitrobenzene

84 81 48 - 97 3 30Isophorone

85 83 51 - 100 3 30Bis(2-chloroethoxy)methane

78 78 48 - 94 0 301,2,4-Trichlorobenzene

77 78 53 - 94 1 30Naphthalene

74 76 45 - 98 3 30Hexachlorobutadiene

85 89 24 - 98 4 30Hexachlorocyclopentadiene

79 80 51 - 102 1 302-Chloronaphthalene

85 86 52 - 112 1 30Dimethyl phthalate

82 83 51 - 103 1 30Acenaphthylene

90 90 51 - 115 0 302,6-Dinitrotoluene

84 83 46 - 100 0 30Acenaphthene

87 88 53 - 110 1 302,4-Dinitrotoluene

85 85 52 - 114 1 30Diethyl phthalate




Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

05/18/2010 1218

05/18/2010 1246

Solid

Matrix Spike/


1.0

1.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

Instrument ID:

Lab File ID:



Injection Volume:




05/17/2010 0900

05/17/2010 0900



p2882.d

15.04 g

1 mL

p2883.d

15.03 g

1 mL

Method: 8270C

Preparation: 3541

BNAMS10

BNAMS10

460-13139-5

460-13139-5


% Rec.

85 86 50 - 106 1 304-Chlorophenyl phenyl ether

84 85 51 - 108 2 30Fluorene

93 93 49 - 106 0 30N-Nitrosodiphenylamine

88 88 44 - 102 1 304-Bromophenyl phenyl ether

87 87 43 - 104 1 30Hexachlorobenzene

82 85 48 - 108 3 30Phenanthrene

84 85 50 - 107 2 30Anthracene

84 89 50 - 108 6 30Di-n-butyl phthalate

85 91 49 - 108 6 30Fluoranthene

87 84 49 - 116 4 30Pyrene

3 4 10 - 61 38 30 J F J FBenzidine

87 88 49 - 117 1 30Butyl benzyl phthalate

87 89 24 - 105 2 303,3'-Dichlorobenzidine

85 85 46 - 112 1 30Benzo[a]anthracene

87 87 45 - 114 0 30Chrysene

87 88 49 - 119 1 30Bis(2-ethylhexyl) phthalate

87 88 40 - 106 2 30Di-n-octyl phthalate

89 91 33 - 96 2 30Benzo[b]fluoranthene

87 89 35 - 115 3 30Benzo[k]fluoranthene

75 77 36 - 89 2 30Benzo[a]pyrene

88 88 43 - 109 1 30Indeno[1,2,3-cd]pyrene

84 85 43 - 107 1 30Dibenz(a,h)anthracene

87 89 43 - 106 2 30Benzo[g,h,i]perylene

78 79 45 - 102 0 30bis (2-chloroisopropyl) ether

Surrogate MS % Rec MSD % Rec Acceptance Limits

Nitrobenzene-d5 80 81 38 - 105

Phenol-d5 79 75 41 - 118

Terphenyl-d14 91 89 16 - 151

2,4,6-Tribromophenol 67 66 10 - 120

2-Fluorophenol 74 72 37 - 125

2-Fluorobiphenyl 80 82 40 - 109




Solid



MS Lab Sample ID:

Client Matrix:

Date Prepared:

MSD Lab Sample ID:


Date Prepared:05/17/2010 0900 05/17/2010 0900

Matrix Spike/

Matrix Spike Duplicate Data Report - Batch: 460-37564

Method: 8270C

Preparation: 3541

Units: ug/Kg460-13139-5 460-13139-5

MSD

Result/Qual

MS

Result/Qual

MSD Spike

Amount

MS Spike

Amount

Sample

Result/QualAnalyte

350 U 7110 7120 5410 5170Phenol

350 U 7110 7120 5430 53502-Chlorophenol

350 U 7110 7120 5770 56202-Nitrophenol

350 U 7110 7120 5560 53702,4-Dimethylphenol

350 U 7110 7120 5660 54402,4-Dichlorophenol

350 U 7110 7120 6080 56904-Chloro-3-methylphenol

350 U 7110 7120 4770 46702,4,6-Trichlorophenol

1100 U 7110 7120 1100 1100U F U F2,4-Dinitrophenol

1100 U 7110 7120 4630 46304-Nitrophenol

1100 U 7110 7120 191 1100J F U F4,6-Dinitro-2-methylphenol

1100 U 7110 7120 1600 1530Pentachlorophenol

350 U 3560 3560 2620 2660N-Nitrosodimethylamine

35 U 3560 3560 3190 3150Bis(2-chloroethyl)ether

350 U 3560 3560 2340 23901,3-Dichlorobenzene



35 U 3560 3560 3240 3100N-Nitrosodi-n-propylamine

35 U 3560 3560 2360 2420Hexachloroethane

35 U 3560 3560 2690 2700Nitrobenzene

350 U 3560 3560 2980 2900Isophorone

350 U 3560 3560 3020 2950Bis(2-chloroethoxy)methane

35 U 3560 3560 2760 27701,2,4-Trichlorobenzene

350 U 3560 3560 2740 2780Naphthalene

72 U 3560 3560 2630 2720Hexachlorobutadiene

350 U 3560 3560 3040 3150Hexachlorocyclopentadiene

350 U 3560 3560 2820 28602-Chloronaphthalene

350 U 3560 3560 3030 3060Dimethyl phthalate

350 U 3560 3560 2920 2940Acenaphthylene

72 U 3560 3560 3210 32002,6-Dinitrotoluene

350 U 3560 3560 2980 2970Acenaphthene

72 U 3560 3560 3110 31502,4-Dinitrotoluene

350 U 3560 3560 3010 3030Diethyl phthalate

350 U 3560 3560 3010 30504-Chlorophenyl phenyl ether

350 U 3560 3560 2970 3020Fluorene

350 U 3560 3560 3310 3320N-Nitrosodiphenylamine

350 U 3560 3560 3110 31304-Bromophenyl phenyl ether

35 U 3560 3560 3080 3110Hexachlorobenzene

350 U 3560 3560 2930 3030Phenanthrene

350 U 3560 3560 2970 3040Anthracene

350 U 3560 3560 2980 3160Di-n-butyl phthalate

350 U 3560 3560 3030 3230Fluoranthene




Solid



MS Lab Sample ID:

Client Matrix:

Date Prepared:

MSD Lab Sample ID:


Date Prepared:05/17/2010 0900 05/17/2010 0900

Matrix Spike/


Method: 8270C

Preparation: 3541

Units: ug/Kg460-13139-5 460-13139-5

MSD

Result/Qual

MS

Result/Qual

MSD Spike

Amount

MS Spike

Amount

Sample

Result/QualAnalyte

350 U 3560 3560 3110 2980Pyrene

350 U 3560 3560 89.3 131J F J FBenzidine

350 U 3560 3560 3090 3120Butyl benzyl phthalate

720 U 3560 3560 3100 31803,3'-Dichlorobenzidine

35 U 3560 3560 3010 3030Benzo[a]anthracene

350 U 3560 3560 3100 3080Chrysene

350 U 3560 3560 3100 3130Bis(2-ethylhexyl) phthalate

350 U 3560 3560 3080 3150Di-n-octyl phthalate

35 U 3560 3560 3160 3220Benzo[b]fluoranthene

35 U 3560 3560 3090 3180Benzo[k]fluoranthene

35 U 3560 3560 2660 2720Benzo[a]pyrene

35 U 3560 3560 3110 3150Indeno[1,2,3-cd]pyrene

35 U 3560 3560 3000 3030Dibenz(a,h)anthracene

350 U 3560 3560 3110 3170Benzo[g,h,i]perylene

350 U 3560 3560 2780 2800bis (2-chloroisopropyl) ether




SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

05/17/2010 0937


Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:



05/14/2010 0915

xr108835.d

15.00 g

10 mL

1 uL

Units: ug/Kg

Column ID: PRIMARY

Method: 8081A

Preparation: 3541

PESTGC1MB 460-37420/1-A


6.7 U 6.71.5Aldrin


6.7 U 6.70.91beta-BHC



67 U 6715Chlordane

6.7 U 6.70.804,4'-DDD

6.7 U 6.71.34,4'-DDE

6.7 U 6.70.844,4'-DDT





6.7 U 6.70.94Endrin




67 U 6714Toxaphene


Tetrachloro-m-xylene 76 22 - 141

DCB Decachlorobiphenyl 145 10 - 165







Solid

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

xf108820.d

05/14/2010 0915



15.00 g

10 mL

1 uL

Units: ug/Kg

Column ID: PRIMARY

Method: 8081A

Preparation: 3541

PESTGC1LCS 460-37420/2-A


133 88.9 67 32 - 152Aldrin

133 96.3 72 41 - 145alpha-BHC

133 104 78 28 - 155beta-BHC

133 121 91 31 - 154delta-BHC

133 98.6 74 33 - 152gamma-BHC (Lindane)

133 94.7 71 50 - 1544,4'-DDD

133 98.1 74 47 - 1504,4'-DDE

133 99.1 74 39 - 1544,4'-DDT

133 89.6 67 40 - 147Dieldrin

133 93.6 70 42 - 147Endosulfan I

133 101 76 32 - 150Endosulfan II

133 103 77 37 - 143Endosulfan sulfate

133 104 78 44 - 149Endrin

133 104 78 34 - 142Endrin aldehyde

133 93.0 70 32 - 152Heptachlor

133 97.0 73 33 - 149Heptachlor epoxide




Solid

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

xr108820.d

05/14/2010 0915



15.00 g

10 mL

1 uL

Units: ug/Kg

Column ID: SECONDARY

Method: 8081A

Preparation: 3541



133 82.2 62 32 - 152Aldrin

133 89.0 67 41 - 145alpha-BHC

133 102 76 28 - 155beta-BHC

133 109 82 31 - 154delta-BHC

133 90.2 68 33 - 152gamma-BHC (Lindane)

133 93.4 70 50 - 1544,4'-DDD

133 94.8 71 47 - 1504,4'-DDE

133 97.2 73 39 - 1544,4'-DDT

133 88.6 66 40 - 147Dieldrin




Solid

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

xr108820.d

05/14/2010 0915



15.00 g

10 mL

1 uL

Units: ug/Kg


Method: 8081A

Preparation: 3541



133 93.3 70 42 - 147Endosulfan I

133 101 75 32 - 150Endosulfan II

133 101 76 37 - 143Endosulfan sulfate

133 101 76 44 - 149Endrin

133 103 78 34 - 142Endrin aldehyde

133 87.2 65 32 - 152Heptachlor

133 93.5 70 33 - 149Heptachlor epoxide







Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

05/17/2010 0636

05/17/2010 0650

Solid

Matrix Spike/


1.0

1.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

Column ID:

Instrument ID:

Lab File ID:



Injection Volume:

Column ID:




05/14/2010 0915

05/14/2010 0915



xf108822.d

15.01 g

10 mL

1 uL

PRIMARY

xf108823.d

15.00 g

10 mL

1 uL

PRIMARY

Method: 8081A

Preparation: 3541

PESTGC1

PESTGC1

460-13147-A-2-B MS

460-13147-A-2-C MSD


% Rec.

99 95 32 - 152 4 30Aldrin

100 94 41 - 145 6 30alpha-BHC

100 94 28 - 155 6 30beta-BHC

109 103 31 - 154 5 30delta-BHC

101 96 33 - 152 5 30gamma-BHC (Lindane)

104 102 50 - 154 2 304,4'-DDD

110 105 47 - 150 5 304,4'-DDE

102 94 39 - 154 8 304,4'-DDT

98 91 40 - 147 7 30Dieldrin

94 89 42 - 147 5 30Endosulfan I

99 95 32 - 150 5 30Endosulfan II

96 96 37 - 143 0 30Endosulfan sulfate

109 106 44 - 149 3 30Endrin

95 89 34 - 142 6 30Endrin aldehyde

91 82 32 - 152 10 30Heptachlor

97 92 33 - 149 6 30Heptachlor epoxide


Tetrachloro-m-xylene 107 101 22 - 141

DCB Decachlorobiphenyl 132 56 10 - 165p




Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

05/17/2010 0636

05/17/2010 0650

Solid

Matrix Spike/


1.0

1.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

Column ID:

Instrument ID:

Lab File ID:



Injection Volume:

Column ID:




05/14/2010 0915

05/14/2010 0915



xr108822.d

15.01 g

10 mL

1 uL

SECONDARY

xr108823.d

15.00 g

10 mL

1 uL

SECONDARY

Method: 8081A

Preparation: 3541

PESTGC1

PESTGC1

460-13147-A-2-B MS

460-13147-A-2-C MSD


% Rec.

83 80 32 - 152 4 30Aldrin

85 80 41 - 145 6 30alpha-BHC

84 82 28 - 155 2 30beta-BHC

93 87 31 - 154 6 30delta-BHC

85 79 33 - 152 7 30gamma-BHC (Lindane)

87 77 50 - 154 13 304,4'-DDD

88 79 47 - 150 11 304,4'-DDE

82 74 39 - 154 10 304,4'-DDT

83 78 40 - 147 7 30Dieldrin

88 82 42 - 147 7 30Endosulfan I

80 74 32 - 150 8 30Endosulfan II

77 71 37 - 143 8 30Endosulfan sulfate

96 87 44 - 149 10 30Endrin

76 63 34 - 142 19 30Endrin aldehyde

90 79 32 - 152 12 30Heptachlor

86 79 33 - 149 8 30Heptachlor epoxide


Tetrachloro-m-xylene 94 91 22 - 141

DCB Decachlorobiphenyl 123 147 10 - 165




Solid



MS Lab Sample ID:

Client Matrix:

Date Prepared:

MSD Lab Sample ID:


Date Prepared:05/14/2010 0915 05/14/2010 0915

Matrix Spike/


Method: 8081A

Preparation: 3541

Units: ug/Kg460-13147-A-2-B MS 460-13147-A-2-C MSD

MSD

Result/Qual

MS

Result/Qual

MSD Spike

Amount

MS Spike

Amount

Sample

Result/QualAnalyte

7.7 U 153 153 151 145Aldrin

7.7 U 153 153 154 145alpha-BHC

7.7 U 153 153 153 144beta-BHC

7.7 U 153 153 167 159delta-BHC

7.7 U 153 153 155 147gamma-BHC (Lindane)

7.7 U 153 153 159 1564,4'-DDD

7.7 U 153 153 169 1614,4'-DDE

6.4 J 153 153 162 1504,4'-DDT

7.7 U 153 153 150 140Dieldrin

7.7 U 153 153 144 137Endosulfan I

7.7 U 153 153 152 145Endosulfan II

7.7 U 153 153 147 147Endosulfan sulfate

7.7 U 153 153 168 163Endrin

7.7 U 153 153 145 137Endrin aldehyde

7.7 U 153 153 139 125Heptachlor

7.7 U 153 153 149 140Heptachlor epoxide




Solid



MS Lab Sample ID:

Client Matrix:

Date Prepared:

MSD Lab Sample ID:


Date Prepared:05/14/2010 0915 05/14/2010 0915

Matrix Spike/


Method: 8081A

Preparation: 3541


MSD

Result/Qual

MS

Result/Qual

MSD Spike

Amount

MS Spike

Amount

Sample

Result/QualAnalyte

7.7 U 153 153 127 122Aldrin

7.7 U 153 153 129 122alpha-BHC

7.7 U 153 153 128 125beta-BHC

7.7 U 153 153 142 134delta-BHC

7.7 U 153 153 130 121gamma-BHC (Lindane)

7.7 U 153 153 134 1184,4'-DDD

7.7 U 153 153 135 1224,4'-DDE

4.8 J 153 153 131 1184,4'-DDT

7.7 U 153 153 128 120Dieldrin

7.7 U 153 153 135 126Endosulfan I

7.7 U 153 153 123 113Endosulfan II

7.7 U 153 153 118 109Endosulfan sulfate

7.7 U 153 153 148 133Endrin

7.7 U 153 153 116 95.9Endrin aldehyde

7.7 U 153 153 137 122Heptachlor

7.7 U 153 153 132 122Heptachlor epoxide




SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

05/14/2010 1820


Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:



05/14/2010 0719

or077395.d

15.00 g

10 mL

Units: ug/Kg

Column ID: PRIMARY

Method: 8082

Preparation: 3541

PESTGC7MB 460-37391/1-A


67 U 6713Aroclor 1016

67 U 6720Aroclor 1221

67 U 6738Aroclor 1232

67 U 6713Aroclor 1242

67 U 6718Aroclor 1248

67 U 6723Aroclor 1254

67 U 677.5Aroclor 1260

67 U 6712Aroclor 1262

67 U 6712Aroclor 1268








Solid

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

of077396.d

05/14/2010 0719



15.00 g

10 mL

Units: ug/Kg

Column ID: PRIMARY

Method: 8082

Preparation: 3541



333 316 95 62 - 148Aroclor 1016

333 328 98 58 - 145Aroclor 1260



Solid

1.0



Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

or077396.d

05/14/2010 0719



15.00 g

10 mL

Units: ug/Kg


Method: 8082

Preparation: 3541



333 278 83 62 - 148Aroclor 1016

333 314 94 58 - 145Aroclor 1260






Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

05/14/2010 1909

05/14/2010 1926

Solid

Matrix Spike/


1.0

1.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

Column ID:

Instrument ID:

Lab File ID:



Injection Volume:

Column ID:




05/14/2010 0719

05/14/2010 0719



of077398.d

15.03 g

10 mL

PRIMARY

of077399.d

15.02 g

10 mL

PRIMARY

Method: 8082

Preparation: 3541

PESTGC7

PESTGC7

460-13137-A-1-B MS

460-13137-A-1-C MSD


% Rec.

104 106 62 - 148 2 30Aroclor 1016

106 110 58 - 145 4 30Aroclor 1260






Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

05/14/2010 1909

05/14/2010 1926

Solid

Matrix Spike/


1.0

1.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

Column ID:

Instrument ID:

Lab File ID:



Injection Volume:

Column ID:




05/14/2010 0719

05/14/2010 0719



or077398.d

15.03 g

10 mL

SECONDARY

or077399.d

15.02 g

10 mL

SECONDARY

Method: 8082

Preparation: 3541

PESTGC7

PESTGC7

460-13137-A-1-B MS

460-13137-A-1-C MSD


% Rec.

94 98 62 - 148 4 30Aroclor 1016

96 100 58 - 145 4 30Aroclor 1260






Solid



MS Lab Sample ID:

Client Matrix:

Date Prepared:

MSD Lab Sample ID:


Date Prepared:05/14/2010 0719 05/14/2010 0719

Matrix Spike/


Method: 8082

Preparation: 3541


MSD

Result/Qual

MS

Result/Qual

MSD Spike

Amount

MS Spike

Amount

Sample

Result/QualAnalyte

69 U 343 343 357 364Aroclor 1016

69 U 343 343 362 376Aroclor 1260

Solid



MS Lab Sample ID:

Client Matrix:

Date Prepared:

MSD Lab Sample ID:


Date Prepared:05/14/2010 0719 05/14/2010 0719

Matrix Spike/


Method: 8082

Preparation: 3541


MSD

Result/Qual

MS

Result/Qual

MSD Spike

Amount

MS Spike

Amount

Sample

Result/QualAnalyte

69 U 343 343 321 335Aroclor 1016

69 U 343 343 331 343Aroclor 1260




SolidClient Matrix:

2.0Dilution:

Date Analyzed:

Lab Sample ID:

05/18/2010 1120


Date Prepared:

Instrument ID:

Lab File ID:





05/14/2010 1542

05182010A.txt

1.00 g

50 mL

Units: mg/Kg

Method: 6010B

Preparation: 3050B

ICP4MB 460-37477/1-A ^2



0.50 U 0.500.35Arsenic


0.50 U 0.500.078Cadmium

1.0 U 1.00.59Chromium

2.5 U 2.50.41Copper

0.50 U 0.500.25Lead

4.0 U 4.00.27Nickel


0.0811 J 1.00.076Silver


3.0 U 3.00.49Zinc

Solid

4.0


LCS-Standard Reference Material - Batch:

Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



05182010A.txt

05/14/2010 1542



1.02 g

50 mL

Units: mg/Kg

Method: 6010B

Preparation: 3050B

ICP4LCSSRM 460-37477/2-A ^4


66.1 68.57 104 32.0 - 353Antimony

102 93.00 91 69.7 - 131Arsenic

76.1 73.49 97 74.0 - 126Beryllium

59.5 53.69 90 73.3 - 127Cadmium

231 228.8 99 70.8 - 129Chromium

171 171.5 101 75.3 - 124Copper

84.3 86.10 102 69.8 - 130Lead

131 123.8 94 73.2 - 127Nickel

280 249.4 89 69.6 - 130Selenium

29.5 29.73 101 65.1 - 135Silver

119 124.3 105 67.8 - 133Thallium

582 538.2 92 73.6 - 127Zinc




SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

05/14/2010 1222


Date Prepared:

Instrument ID:

Lab File ID:





05/14/2010 0925

37424hg1.PRN

0.60 g

100 mL

Units: mg/Kg

Method: 7471A

Preparation: 7471A

LEEMAN5MB 460-37424/1-A


0.033 U 0.0330.026Mercury

Solid

10


LCS-Standard Reference Material - Batch:

Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



37424hg1.PRN

05/14/2010 0925



0.60 g

100 mL

Units: mg/Kg

Method: 7471A

Preparation: 7471A

LEEMAN5LCSSRM 460-37424/2-A ^10


8.46 9.15 108 51.3 - 149Mercury

Solid

1.0


Matrix Spike - Batch: 460-37424

Lab Sample ID:

Client Matrix:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



05/14/2010 0925

37424hg1.PRN



0.60 g

100 mL

Units: mg/Kg

Method: 7471A

Preparation: 7471A

LEEMAN5460-13139-5

QualLimit% Rec.ResultSpike AmountSample Result/QualAnalyte

0.035 U 0.178 0.214 120 75 - 125Mercury




mg/KgUnits:

Solid

Dilution: 1.0

Date Analyzed:

Duplicate - Batch: 460-37424

Lab Sample ID:

Client Matrix:

Date Prepared:

05/14/2010 1228

05/14/2010 0925

Instrument ID:

Lab File ID:




Prep Batch: 460-37424 37424hg1.PRN

0.60 g

100 mL

Method: 7471A

Preparation: 7471A

LEEMAN5460-13139-5

Analyte QualLimitRPDResultSample Result/Qual

0.0350.035 U NC 20 UMercury




%Units:

Solid

Dilution: 1.0

Date Analyzed:


Lab Sample ID:

Client Matrix:

Date Prepared:

05/14/2010 2147

Instrument ID:

Lab File ID:




Prep Batch: N/A

N/A

Method: Moisture

Preparation: N/A

N/A

No Equipment Assigned460-13146-A-1 DU


16.116.2 1 20Percent Moisture

83.983.8 0 20Percent Solids




%Units:

Solid

Dilution: 1.0

Date Analyzed:


Lab Sample ID:

Client Matrix:

Date Prepared:

05/17/2010 1956

Instrument ID:

Lab File ID:




Prep Batch: N/A

N/A

Method: Moisture

Preparation: N/A

N/A

No Equipment Assigned460-13237-A-4 DU


16.215.8 2 20Percent Moisture

83.884.2 0 20Percent Solids


DATA REPORTING QUALIFIERS


Lab Section Qualifier Description

GC/MS VOA

Indicates an Estimated Value for TICsJ

Indicates the analyte was analyzed for but not detected.U

Result is a tentatively identified compound (TIC) and an

estimated value.

T

GC/MS Semi VOA

Indicates an Estimated Value for TICsJ


MS/MSD Recovery or RPD exceeds the control limitsF

Recovery or RPD exceeds control limits*

Result is a tentatively identified compound (TIC) and an

estimated value.

T

Result is less than the RL but greater than or equal to the MDL

and the concentration is an approximate value.

J

The tentatively identified compound is a suspected

aldol-condensation product.

A

This flag indicates the presumptive evidence of a compound.N

GC Semi VOA




J

Surrogate is outside control limitsX

The %RPD between the primary and confirmation

column/detector is >40%. The lower value has been reported.

p

TestAmerica Edison

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DATA REPORTING QUALIFIERS


Lab Section Qualifier Description

Metals

Compound was found in the blank and sample.B




J

TestAmerica Edison

06/03/2010 of 623



QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

GC/MS VOA


SolidTB-3 6-7 5035460-13139-2 T

SolidTB-2 5-6 5035460-13139-4 T

SolidTB-1 2-3 5035460-13139-5 T

SolidTB-5 3-4 5035460-13139-7 T

Analysis Batch:460-37643

Lab Control Sample Solid 8260BLCS 460-37643/3 T

Lab Control Sample Duplicate Solid 8260BLCSD 460-37643/4 T

Method Blank Solid 8260BMB 460-37643/5 T

Solid 460-37413TB-3 6-7 8260B460-13139-2 T

Solid 460-37413TB-2 5-6 8260B460-13139-4 T

Solid 460-37413TB-1 2-3 8260B460-13139-5 T

Solid 460-37413TB-5 3-4 8260B460-13139-7 T

Report Basis

T = Total

GC/MS Semi VOA


Lab Control Sample Solid 3541LCS 460-37564/2-A T

Method Blank Solid 3541MB 460-37564/1-A T

SolidTB-3 6-7 3541460-13139-2 T

SolidTB-2 5-6 3541460-13139-4 T

SolidTB-1 2-3 3541460-13139-5 T

Matrix Spike Solid 3541460-13139-5MS T

Matrix Spike Duplicate Solid 3541460-13139-5MSD T

SolidTB-5 3-4 3541460-13139-7 T


Lab Control Sample Solid 460-375648270CLCS 460-37564/2-A T

Method Blank Solid 460-375648270CMB 460-37564/1-A T

Solid 460-37564TB-3 6-7 8270C460-13139-2 T

Solid 460-37564TB-2 5-6 8270C460-13139-4 T

Solid 460-37564TB-1 2-3 8270C460-13139-5 T

Matrix Spike Solid 460-375648270C460-13139-5MS T

Matrix Spike Duplicate Solid 460-375648270C460-13139-5MSD T

Solid 460-37564TB-5 3-4 8270C460-13139-7 T

Report Basis

T = Total

TestAmerica Edison

06/03/2010 of 623





Report

Basis

GC Semi VOA




Matrix Spike Solid 3541460-13137-A-1-B MS T

Matrix Spike Duplicate Solid 3541460-13137-A-1-C MSD T

SolidTB-3 6-7 3541460-13139-2 T

SolidTB-2 5-6 3541460-13139-4 T

SolidTB-1 2-3 3541460-13139-5 T

SolidTB-5 3-4 3541460-13139-7 T




SolidTB-3 6-7 3541460-13139-2 T

SolidTB-2 5-6 3541460-13139-4 T

SolidTB-1 2-3 3541460-13139-5 T

SolidTB-5 3-4 3541460-13139-7 T

Matrix Spike Solid 3541460-13147-A-2-B MS T

Matrix Spike Duplicate Solid 3541460-13147-A-2-C MSD T


Lab Control Sample Solid 460-373918082LCS 460-37391/2-A T

Method Blank Solid 460-373918082MB 460-37391/1-A T

Matrix Spike Solid 460-373918082460-13137-A-1-B MS T

Matrix Spike Duplicate Solid 460-373918082460-13137-A-1-C MSD T

Solid 460-37391TB-3 6-7 8082460-13139-2 T

Solid 460-37391TB-2 5-6 8082460-13139-4 T

Solid 460-37391TB-1 2-3 8082460-13139-5 T

Solid 460-37391TB-5 3-4 8082460-13139-7 T


Lab Control Sample Solid 460-374208081ALCS 460-37420/2-A T

Method Blank Solid 460-374208081AMB 460-37420/1-A T

Solid 460-37420TB-3 6-7 8081A460-13139-2 T

Solid 460-37420TB-2 5-6 8081A460-13139-4 T

Solid 460-37420TB-1 2-3 8081A460-13139-5 T

Solid 460-37420TB-5 3-4 8081A460-13139-7 T

Matrix Spike Solid 460-374208081A460-13147-A-2-B MS T

Matrix Spike Duplicate Solid 460-374208081A460-13147-A-2-C MSD T

Report Basis

T = Total

TestAmerica Edison

06/03/2010 of 623





Report

Basis

Metals


LCS-Standard Reference Material Solid 7471ALCSSRM 460-37424/2-A ^10 T

Method Blank Solid 7471AMB 460-37424/1-A T

SolidTB-3 6-7 7471A460-13139-2 T

SolidTB-2 5-6 7471A460-13139-4 T

SolidTB-1 2-3 7471A460-13139-5 T

Duplicate Solid 7471A460-13139-5DU T

Matrix Spike Solid 7471A460-13139-5MS T

SolidTB-5 3-4 7471A460-13139-7 T


LCS-Standard Reference Material Solid 460-374247471ALCSSRM 460-37424/2-A ^10 T

Method Blank Solid 460-374247471AMB 460-37424/1-A T

Solid 460-37424TB-3 6-7 7471A460-13139-2 T

Solid 460-37424TB-2 5-6 7471A460-13139-4 T

Solid 460-37424TB-1 2-3 7471A460-13139-5 T

Duplicate Solid 460-374247471A460-13139-5DU T

Matrix Spike Solid 460-374247471A460-13139-5MS T

Solid 460-37424TB-5 3-4 7471A460-13139-7 T


LCS-Standard Reference Material Solid 3050BLCSSRM 460-37477/2-A ^4 T

Method Blank Solid 3050BMB 460-37477/1-A ^2 T

SolidTB-3 6-7 3050B460-13139-2 T

SolidTB-2 5-6 3050B460-13139-4 T

SolidTB-1 2-3 3050B460-13139-5 T

SolidTB-5 3-4 3050B460-13139-7 T


LCS-Standard Reference Material Solid 460-374776010BLCSSRM 460-37477/2-A ^4 T

Method Blank Solid 460-374776010BMB 460-37477/1-A ^2 T

Solid 460-37477TB-3 6-7 6010B460-13139-2 T

Solid 460-37477TB-2 5-6 6010B460-13139-4 T

Solid 460-37477TB-1 2-3 6010B460-13139-5 T

Solid 460-37477TB-5 3-4 6010B460-13139-7 T

Report Basis

T = Total

TestAmerica Edison

06/03/2010 of 623





Report

Basis

General Chemistry


SolidTB-3 2-3 Moisture460-13139-1 T







Duplicate Solid Moisture460-13146-A-1 DU T



Duplicate Solid Moisture460-13237-A-4 DU T

Report Basis

T = Total

TestAmerica Edison

06/03/2010 of 623



Laboratory Chronicle

05/13/2010 18:30

Lab ID:

Method Bottle ID Run

Analysis

Batch Prep Batch

Date Prepared /

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: Received Date/Time:05/12/2010 09:00

460-13139-1 TB-3 2-3

A:Moisture 460-13139-D-1 460-37508 05/14/2010 21:47 VDTAL EDI1

05/13/2010 18:30

Lab ID:


Analysis

Batch Prep Batch

Date Prepared /


Client ID:


460-13139-2 TB-3 6-7

P:5035 460-13139-B-2-A 460-37643 460-37413 05/14/2010 08:50 MMDTAL EDI1

A:8260B 460-13139-B-2-A 460-37643 460-37413 05/18/2010 00:18 KBTAL EDI1

P:3541 460-13139-E-2-E 460-37818 460-37564 05/17/2010 09:00 cmTAL EDI1

A:8270C 460-13139-E-2-E 460-37818 460-37564 05/18/2010 15:00 CZTAL EDI1

P:3541 460-13139-E-2-B 460-37575 460-37420 05/14/2010 09:15 hpTAL EDI1

A:8081A 460-13139-E-2-B 460-37575 460-37420 05/17/2010 08:00 FMTAL EDI1

P:3541 460-13139-E-2-A 460-37531 460-37391 05/14/2010 07:19 ARATAL EDI1

A:8082 460-13139-E-2-A 460-37531 460-37391 05/14/2010 19:59 CBDTAL EDI1

P:3050B 460-13139-E-2-D ^4 460-37705 460-37477 05/14/2010 15:42 ARCTAL EDI4

A:6010B 460-13139-E-2-D ^4 460-37705 460-37477 05/18/2010 11:55 CDCTAL EDI4

P:7471A 460-13139-E-2-C 460-37472 460-37424 05/14/2010 09:25 RBSTAL EDI1

A:7471A 460-13139-E-2-C 460-37472 460-37424 05/14/2010 12:52 RBSTAL EDI1


05/13/2010 18:30

Lab ID:


Analysis

Batch Prep Batch

Date Prepared /


Client ID:


460-13139-3 TB-2 2-3


A = Analytical Method P = Prep Method TestAmerica Edison

06/03/2010 of 623




05/13/2010 18:30

Lab ID:


Analysis

Batch Prep Batch

Date Prepared /


Client ID:


460-13139-4 TB-2 5-6

P:5035 460-13139-B-4-A 460-37643 460-37413 05/14/2010 08:54 MMDTAL EDI1

A:8260B 460-13139-B-4-A 460-37643 460-37413 05/18/2010 00:43 KBTAL EDI1

P:3541 460-13139-E-4-E 460-37818 460-37564 05/17/2010 09:00 cmTAL EDI1

A:8270C 460-13139-E-4-E 460-37818 460-37564 05/18/2010 20:25 CZTAL EDI1

P:3541 460-13139-E-4-B 460-37575 460-37420 05/14/2010 09:15 hpTAL EDI1

A:8081A 460-13139-E-4-B 460-37575 460-37420 05/17/2010 08:27 FMTAL EDI1

P:3541 460-13139-E-4-A 460-37531 460-37391 05/14/2010 07:19 ARATAL EDI1

A:8082 460-13139-E-4-A 460-37531 460-37391 05/14/2010 20:32 CBDTAL EDI1

P:3050B 460-13139-E-4-D ^4 460-37705 460-37477 05/14/2010 15:42 ARCTAL EDI4

A:6010B 460-13139-E-4-D ^4 460-37705 460-37477 05/18/2010 12:01 CDCTAL EDI4

P:7471A 460-13139-E-4-C 460-37472 460-37424 05/14/2010 09:25 RBSTAL EDI1

A:7471A 460-13139-E-4-C 460-37472 460-37424 05/14/2010 12:55 RBSTAL EDI1


05/13/2010 18:30

Lab ID:


Analysis

Batch Prep Batch

Date Prepared /


Client ID:


460-13139-5 TB-1 2-3

P:5035 460-13139-B-5-A 460-37643 460-37413 05/14/2010 08:55 MMDTAL EDI1

A:8260B 460-13139-B-5-A 460-37643 460-37413 05/18/2010 01:08 KBTAL EDI1

P:3541 460-13139-E-5-G 460-37818 460-37564 05/17/2010 09:00 cmTAL EDI1

A:8270C 460-13139-E-5-G 460-37818 460-37564 05/18/2010 11:52 CZTAL EDI1

P:3541 460-13139-E-5-B 460-37575 460-37420 05/14/2010 09:15 hpTAL EDI1

A:8081A 460-13139-E-5-B 460-37575 460-37420 05/17/2010 08:41 FMTAL EDI1

P:3541 460-13139-E-5-A 460-37531 460-37391 05/14/2010 07:19 ARATAL EDI1

A:8082 460-13139-E-5-A 460-37531 460-37391 05/14/2010 20:48 CBDTAL EDI1

P:3050B 460-13139-E-5-F ^4 460-37705 460-37477 05/14/2010 15:42 ARCTAL EDI4

A:6010B 460-13139-E-5-F ^4 460-37705 460-37477 05/18/2010 12:04 CDCTAL EDI4

P:7471A 460-13139-E-5-C 460-37472 460-37424 05/14/2010 09:25 RBSTAL EDI1

A:7471A 460-13139-E-5-C 460-37472 460-37424 05/14/2010 12:26 RBSTAL EDI1


05/13/2010 18:30

Lab ID:


Analysis

Batch Prep Batch

Date Prepared /


Client ID:


460-13139-5 MS TB-1 2-3

P:3541 460-13139-E-5-H MS 460-37818 460-37564 05/17/2010 09:00 cmTAL EDI1

A:8270C 460-13139-E-5-H MS 460-37818 460-37564 05/18/2010 12:18 CZTAL EDI1

P:7471A 460-13139-E-5-E MS 460-37472 460-37424 05/14/2010 09:25 RBSTAL EDI1

A:7471A 460-13139-E-5-E MS 460-37472 460-37424 05/14/2010 12:31 RBSTAL EDI1


06/03/2010 of 623




05/13/2010 18:30

Lab ID:


Analysis

Batch Prep Batch

Date Prepared /


Client ID:


460-13139-5 MSD TB-1 2-3

P:3541 460-13139-E-5-I MSD 460-37818 460-37564 05/17/2010 09:00 cmTAL EDI1

A:8270C 460-13139-E-5-I MSD 460-37818 460-37564 05/18/2010 12:46 CZTAL EDI1

05/13/2010 18:30

Lab ID:


Analysis

Batch Prep Batch

Date Prepared /


Client ID:


460-13139-5 DU TB-1 2-3

P:7471A 460-13139-E-5-D DU 460-37472 460-37424 05/14/2010 09:25 RBSTAL EDI1

A:7471A 460-13139-E-5-D DU 460-37472 460-37424 05/14/2010 12:28 RBSTAL EDI1

05/13/2010 18:30

Lab ID:


Analysis

Batch Prep Batch

Date Prepared /


Client ID:


460-13139-6 TB-1 5-6


05/13/2010 18:30

Lab ID:


Analysis

Batch Prep Batch

Date Prepared /


Client ID:


460-13139-7 TB-5 3-4

P:5035 460-13139-B-7-A 460-37643 460-37413 05/14/2010 08:58 MMDTAL EDI1

A:8260B 460-13139-B-7-A 460-37643 460-37413 05/18/2010 01:33 KBTAL EDI1

P:3541 460-13139-E-7-E 460-37818 460-37564 05/17/2010 09:00 cmTAL EDI1

A:8270C 460-13139-E-7-E 460-37818 460-37564 05/18/2010 19:58 CZTAL EDI1

P:3541 460-13139-E-7-B 460-37575 460-37420 05/14/2010 09:15 hpTAL EDI1

A:8081A 460-13139-E-7-B 460-37575 460-37420 05/17/2010 09:09 FMTAL EDI1

P:3541 460-13139-E-7-A 460-37531 460-37391 05/14/2010 07:19 ARATAL EDI1

A:8082 460-13139-E-7-A 460-37531 460-37391 05/14/2010 21:21 CBDTAL EDI1

P:3050B 460-13139-E-7-D ^4 460-37705 460-37477 05/14/2010 15:42 ARCTAL EDI4

A:6010B 460-13139-E-7-D ^4 460-37705 460-37477 05/18/2010 12:10 CDCTAL EDI4

P:7471A 460-13139-E-7-C 460-37472 460-37424 05/14/2010 09:25 RBSTAL EDI1

A:7471A 460-13139-E-7-C 460-37472 460-37424 05/14/2010 12:59 RBSTAL EDI1

A:Moisture 460-13139-E-7 460-37639 05/17/2010 19:56 VDTAL EDI1

05/13/2010 18:30

Lab ID:


Analysis

Batch Prep Batch

Date Prepared /


Client ID:


460-13139-8 TB-4 6-7



06/03/2010 of 623




Lab ID:


Analysis

Batch Prep Batch

Date Prepared /


Client ID:

Sample Date/Time: N/A Received Date/Time: N/A

MB N/A

A:8260B MB 460-37643/5 460-37643 05/17/2010 20:11 KBTAL EDI1

P:3541 MB 460-37564/1-A 460-37818 460-37564 05/17/2010 09:00 cmTAL EDI1

A:8270C MB 460-37564/1-A 460-37818 460-37564 05/18/2010 10:57 CZTAL EDI1

P:3541 MB 460-37420/1-A 460-37575 460-37420 05/14/2010 09:15 hpTAL EDI1

A:8081A MB 460-37420/1-A 460-37575 460-37420 05/17/2010 09:37 FMTAL EDI1

P:3541 MB 460-37391/1-A 460-37531 460-37391 05/14/2010 07:19 ARATAL EDI1

A:8082 MB 460-37391/1-A 460-37531 460-37391 05/14/2010 18:20 CBDTAL EDI1

P:3050B MB 460-37477/1-A ^2 460-37705 460-37477 05/14/2010 15:42 ARCTAL EDI2

A:6010B MB 460-37477/1-A ^2 460-37705 460-37477 05/18/2010 11:20 CDCTAL EDI2

P:7471A MB 460-37424/1-A 460-37472 460-37424 05/14/2010 09:25 RBSTAL EDI1

A:7471A MB 460-37424/1-A 460-37472 460-37424 05/14/2010 12:22 RBSTAL EDI1

Lab ID:


Analysis

Batch Prep Batch

Date Prepared /


Client ID:


LCS N/A

A:8260B LCS 460-37643/3 460-37643 05/17/2010 17:46 KBTAL EDI1

P:3541 LCS 460-37564/2-A 460-37818 460-37564 05/17/2010 09:00 cmTAL EDI1

A:8270C LCS 460-37564/2-A 460-37818 460-37564 05/18/2010 11:25 CZTAL EDI1

P:3541 LCS 460-37420/2-A 460-37575 460-37420 05/14/2010 09:15 hpTAL EDI1

A:8081A LCS 460-37420/2-A 460-37575 460-37420 05/17/2010 05:43 FMTAL EDI1

P:3541 LCS 460-37391/2-A 460-37531 460-37391 05/14/2010 07:19 ARATAL EDI1

A:8082 LCS 460-37391/2-A 460-37531 460-37391 05/14/2010 18:37 CBDTAL EDI1

Lab ID:


Analysis

Batch Prep Batch

Date Prepared /


Client ID:


LCSD N/A

A:8260B LCSD 460-37643/4 460-37643 05/17/2010 18:10 KBTAL EDI1

Lab ID:


Analysis

Batch Prep Batch

Date Prepared /


Client ID:


LCSSRM N/A

P:3050B LCSSRM

460-37477/2-A ^4

460-37705 460-37477 05/14/2010 15:42 ARCTAL EDI4

A:6010B LCSSRM

460-37477/2-A ^4

460-37705 460-37477 05/18/2010 11:23 CDCTAL EDI4

P:7471A LCSSRM

460-37424/2-A ^10

460-37472 460-37424 05/14/2010 09:25 RBSTAL EDI10

A:7471A LCSSRM

460-37424/2-A ^10

460-37472 460-37424 05/14/2010 12:24 RBSTAL EDI10


06/03/2010 of 623




05/13/2010 18:00

Lab ID:


Analysis

Batch Prep Batch

Date Prepared /


Client ID:


MS N/A

P:3541 460-13147-A-2-B MS 460-37575 460-37420 05/14/2010 09:15 hpTAL EDI1

A:8081A 460-13147-A-2-B MS 460-37575 460-37420 05/17/2010 06:36 FMTAL EDI1

P:3541 460-13137-A-1-B MS 460-37531 460-37391 05/14/2010 07:19 ARATAL EDI1

A:8082 460-13137-A-1-B MS 460-37531 460-37391 05/14/2010 19:09 CBDTAL EDI1

05/13/2010 18:00

Lab ID:


Analysis

Batch Prep Batch

Date Prepared /


Client ID:


MSD N/A

P:3541 460-13147-A-2-C

MSD

460-37575 460-37420 05/14/2010 09:15 hpTAL EDI1

A:8081A 460-13147-A-2-C

MSD

460-37575 460-37420 05/17/2010 06:50 FMTAL EDI1

P:3541 460-13137-A-1-C

MSD

460-37531 460-37391 05/14/2010 07:19 ARATAL EDI1

A:8082 460-13137-A-1-C

MSD

460-37531 460-37391 05/14/2010 19:26 CBDTAL EDI1

05/13/2010 18:00

Lab ID:


Analysis

Batch Prep Batch

Date Prepared /


Client ID:


DU N/A

A:Moisture 460-13146-A-1 DU 460-37508 05/14/2010 21:47 VDTAL EDI1

A:Moisture 460-13237-A-4 DU 460-37639 05/17/2010 19:56 VDTAL EDI1

Lab References:TAL EDI = TestAmerica Edison


06/03/2010 of 623

Method 8260BVolatile Organic Compounds (GC/MS)

by Method 8260B

06/03/2010 of 623

FORM II

GC/MS VOA SURROGATE RECOVERY

Lab Name: Job No.: 460-13139-1

SDG No.:

Matrix: Solid Level: Low

TestAmerica Edison

GC Column (1): DB-624 ID: 0.18(mm)

#Lab Sample IDClient Sample ID # #DCA TOL BFB

460-13139-2TB-3 6-7 92 88 102

460-13139-4TB-2 5-6 95 89 105

460-13139-5TB-1 2-3 100 90 108

460-13139-7TB-5 3-4 89 73 92

MB 460-37643/5 104 92 107

LCS 460-37643/3 89 90 108

LCSD 460-37643/4 90 95 106

QC LIMITSQC LIMITSDCA = 1,2-Dichloroethane-d4 (Surr) 70-138

TOL = Toluene-d8 (Surr) 66-126BFB = Bromofluorobenzene 72-132

FORM II 8260B

# Column to be used to flag recovery values

06/03/2010 of 623

GC/MS VOA LAB CONTROL SAMPLE RECOVERY

FORM III

Job No.:Lab Name:

SDG No.:

Level:Matrix:Matrix:

Low

460-13139-1

Lab File ID: o37386.dSolid

Lab ID: LCS 460-37643/3 Client ID:

TestAmerica Edison

REC

%

REC

QC

LIMITSCONCENTRATION

(ug/Kg)

SPIKE

ADDED

(ug/Kg)

#

LCS LCS

COMPOUND

Chloromethane 20.0 19.2 50-15196

Bromomethane 20.0 22.0 54-142110

Vinyl chloride 20.0 19.5 67-13397

Chloroethane 20.0 19.9 56-14699

Methylene Chloride 20.0 23.9 74-137120

Trichlorofluoromethane 20.0 21.5 61-139107

1,1-Dichloroethene 20.0 20.8 71-126104

1,1-Dichloroethane 20.0 19.8 76-12599

trans-1,2-Dichloroethene 20.0 19.8 75-12299

cis-1,2-Dichloroethene 20.0 20.0 80-120100

Chloroform 20.0 19.9 77-12099

1,2-Dichloroethane 20.0 19.6 76-11898

1,1,1-Trichloroethane 20.0 20.5 78-117103

Carbon tetrachloride 20.0 21.5 79-118107

Bromodichloromethane 20.0 20.1 79-119100

1,2-Dichloropropane 20.0 19.5 82-12298

cis-1,3-Dichloropropene 20.0 18.7 80-12394

Trichloroethene 20.0 19.8 79-11999

Dibromochloromethane 20.0 16.7 68-12083

1,1,2-Trichloroethane 20.0 17.8 73-11889

Benzene 20.0 19.7 77-11799

trans-1,3-Dichloropropene 20.0 15.2 67-12176

2-Chloroethyl vinyl ether 20.0 16.5 74-12083

Bromoform 20.0 14.7 59-12573

Tetrachloroethene 20.0 18.6 80-12093

1,1,2,2-Tetrachloroethane 20.0 18.9 79-12295

Toluene 20.0 19.2 75-11596

Chlorobenzene 20.0 20.0 80-120100

Ethylbenzene 20.0 21.1 81-121105

Xylenes, Total 60.0 61.9 82-122103

FORM III 8260B

# Column to be used to flag recovery and RPD values

06/03/2010 of 623

GC/MS VOA LAB CONTROL SAMPLE DUPLICATE RECOVERY

FORM III

Job No.:Lab Name:

SDG No.:


Low

460-13139-1

Lab File ID: o37387.dSolid

Lab ID: LCSD 460-37643/4 Client ID:

TestAmerica Edison

COMPOUND

SPIKE

ADDED CONCENTRATION %

REC

%

RPD

QC LIMITS

RPD REC (ug/Kg) (ug/Kg)

#

LCSD LCSD

20.0 19.2 30 50-151Chloromethane 096

20.0 22.3 30 54-142Bromomethane 1111

20.0 19.5 30 67-133Vinyl chloride 098

20.0 19.9 30 56-146Chloroethane 0100

20.0 26.8 30 74-137Methylene Chloride 11134

20.0 21.1 30 61-139Trichlorofluoromethane 2105

20.0 23.1 30 71-1261,1-Dichloroethene 11116

20.0 21.5 30 76-1251,1-Dichloroethane 8108

20.0 21.6 30 75-122trans-1,2-Dichloroethene 9108

20.0 22.1 30 80-120cis-1,2-Dichloroethene 10110

20.0 21.8 30 77-120Chloroform 9109

20.0 21.5 30 76-1181,2-Dichloroethane 9108

20.0 23.0 30 78-1171,1,1-Trichloroethane 11115

20.0 23.3 30 79-118Carbon tetrachloride 8116

20.0 23.1 30 79-119Bromodichloromethane 14115

20.0 21.1 30 82-1221,2-Dichloropropane 8105

20.0 21.8 30 80-123cis-1,3-Dichloropropene 15109

20.0 21.2 30 79-119Trichloroethene 7106

20.0 18.3 30 68-120Dibromochloromethane 991

20.0 20.0 30 73-1181,1,2-Trichloroethane 12100

20.0 21.9 30 77-117Benzene 11110

20.0 17.5 30 67-121trans-1,3-Dichloropropene 1487

20.0 17.4 30 74-1202-Chloroethyl vinyl ether 587

20.0 16.8 30 59-125Bromoform 1384

20.0 22.3 30 80-120Tetrachloroethene 18111

20.0 20.3 30 79-1221,1,2,2-Tetrachloroethane 7101

20.0 21.7 30 75-115Toluene 12109

20.0 21.9 30 80-120Chlorobenzene 9110

20.0 22.1 30 81-121Ethylbenzene 5111

60.0 67.1 30 82-122Xylenes, Total 8112

FORM III 8260B


06/03/2010 of 623

FORM IV

GC/MS VOA METHOD BLANK SUMMARY

Lab Name:

SDG No.:

Job No.: 460-13139-1TestAmerica Edison

Date Analyzed:

GC Column: ID:

Instrument ID: 05/17/2010 20:11

DB-624

YHeated Purge:(Y/N)

VOAMS12

o37390.dLab File ID: Lab Sample ID: MB 460-37643/5

SolidMatrix:

0.18(mm)

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:

LAB SAMPLE ID

LAB

FILE ID DATE ANALYZEDCLIENT SAMPLE ID

05/17/2010 17:46o37386.dLCS 460-37643/3

05/17/2010 18:10o37387.dLCSD 460-37643/4

05/18/2010 00:18o37400.d460-13139-2TB-3 6-7

05/18/2010 00:43o37401.d460-13139-4TB-2 5-6

05/18/2010 01:08o37402.d460-13139-5TB-1 2-3

05/18/2010 01:33o37403.d460-13139-7TB-5 3-4

FORM IV 8260B

06/03/2010 of 623

FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 460-13139-1

Lab File ID:

Instrument ID:

o36289.d

VOAMS12

04/15/2010

13:12

BFB Injection Date:

BFB Injection Time:

M/E ION ABUNDANCE CRITERIA% RELATIVEABUNDANCE

Analysis Batch No.: 34969

50 15.0 - 40.0 % of mass 95 15.8

75 30.0 - 60.0 % of mass 95 47.6

95 Base Peak, 100% relative abundance 100.0

96 5.0 - 9.0 % of mass 95 6.5

173 Less than 2.0 % of mass 174 0.0 (0.0)1

174 50.0 - 120.00 % of mass 95 74.4

175 5.0 - 9.0 % of mass 174 6.1 (8.2)1

176 95.0 - 101.0 % of mass 174 73.8 (99.2)1

177 5.0 - 9.0 % of mass 176 5.0 (6.8)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:

GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Edison

CLIENT SAMPLE IDLAB

FILE IDLAB SAMPLE IDDATE

ANALYZEDTIME

ANALYZED

o36292.d 04/15/2010 14:24IC 460-34969/2

o36294.d 04/15/2010 15:13IC 460-34969/3

o36295.d 04/15/2010 15:38ICIS 460-34969/19

o36296.d 04/15/2010 16:03IC 460-34969/20

o36297.d 04/15/2010 16:27IC 460-34969/6

o36298.d 04/15/2010 16:52IC 460-34969/7

FORM V 8260B 06/03/2010 of 623

FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 460-13139-1

Lab File ID:

Instrument ID:

o37384.d

VOAMS12

05/17/2010

16:42

BFB Injection Date:

BFB Injection Time:



50 15.0 - 40.0 % of mass 95 16.0

75 30.0 - 60.0 % of mass 95 49.0

95 Base Peak, 100% relative abundance 100.0

96 5.0 - 9.0 % of mass 95 6.5

173 Less than 2.0 % of mass 174 0.6 (0.9)1

174 50.0 - 120.00 % of mass 95 68.7

175 5.0 - 9.0 % of mass 174 5.2 (7.6)1

176 95.0 - 101.0 % of mass 174 66.0 (96.2)1

177 5.0 - 9.0 % of mass 176 3.6 (5.5)2



GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Edison

CLIENT SAMPLE IDLAB


ANALYZEDTIME

ANALYZED

o37385.d 05/17/2010 17:02CCVIS 460-37643/2

o37386.d 05/17/2010 17:46LCS 460-37643/3

o37387.d 05/17/2010 18:10LCSD 460-37643/4

o37390.d 05/17/2010 20:11MB 460-37643/5

TB-3 6-7 o37400.d 05/18/2010 00:18460-13139-2

TB-2 5-6 o37401.d 05/18/2010 00:43460-13139-4

TB-1 2-3 o37402.d 05/18/2010 01:08460-13139-5

TB-5 3-4 o37403.d 05/18/2010 01:33460-13139-7

FORM V 8260B 06/03/2010 of 623

GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Edison 460-13139-1

Sample No.: CCVIS 460-37643/2 Date Analyzed: 05/17/2010 17:02

Lab File ID (Standard): o37385.d

Instrument ID: VOAMS12 GC Column: DB-624 ID: 0.18(mm)

Heated Purge: (Y/N) Y

Calibration ID: 5832

AREA # RT # AREA RT # AREA # RT ##

FB CBZ DCB

UPPER LIMIT

LOWER LIMIT

2954680

738670 542177

2168708

292159

1168634

4.26 8.05 11.7312/24 HOUR STD

4.76

3.76

8.55

7.55

12.23

11.23

1477340 1084354 584317

LAB SAMPLE ID CLIENT SAMPLE ID

LCS 460-37643/3 1596386 1094145 577641 4.26 8.05 11.73

LCSD 460-37643/4 1620590 1107274 586808 4.26 8.05 11.74

MB 460-37643/5 1237424 1154369 545686 4.26 8.05 11.73

460-13139-2 TB-3 6-7 1493462 1272951 616746 4.26 8.05 11.74

460-13139-4 TB-2 5-6 1437887 1144265 567459 4.26 8.05 11.73

460-13139-5 TB-1 2-3 1396875 1243273 600118 4.26 8.05 11.73

460-13139-7 TB-5 3-4 1175155 1039684 426343 4.26 8.05 11.73

FB = Fluorobenzene

CBZ = Chlorobenzene-d5

DCB = 1,4-Dichlorobenzene-d4

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

06/03/2010 of 623

FORM IForm 1GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

TB-3 6-7

SDG No.:

460-13139-1

Lab Sample ID: 460-13139-2

Matrix: o37400.dLab File ID:

Date Collected:8260BAnalysis Method:

Soil

TestAmerica Edison

05/12/2010 09:45

Sample wt/vol:

% Moisture:

GC Column:Soil Extract Vol.:

Dilution Factor:Soil Aliquot Vol:

18.8

1

Level: (low/med) Low

5.02(g)

0.18(mm)

Date Analyzed: 05/18/2010 00:18

ID:DB-624

Analysis Batch No.: 37643 ug/KgUnits:

CAS NO. COMPOUND NAME RESULT Q MDLRL

Chloromethane74-87-3 1.2 1.2 0.78U

Bromomethane74-83-9 1.2 1.2 0.50U

Vinyl chloride75-01-4 1.2 1.2 0.29U

Chloroethane75-00-3 1.2 1.2 0.49U

Methylene Chloride75-09-2 1.2 1.2 0.58U

Trichlorofluoromethane75-69-4 1.2 1.2 0.32U

1,1-Dichloroethene75-35-4 1.2 1.2 0.45U

1,1-Dichloroethane75-34-3 1.2 1.2 0.31U

trans-1,2-Dichloroethene156-60-5 1.2 1.2 0.35U

cis-1,2-Dichloroethene156-59-2 1.2 1.2 0.29U

Chloroform67-66-3 1.2 1.2 0.29U


1,1,1-Trichloroethane71-55-6 1.2 1.2 0.23U

Carbon tetrachloride56-23-5 1.2 1.2 0.12U

Bromodichloromethane75-27-4 1.2 1.2 0.37U

1,2-Dichloropropane78-87-5 1.2 1.2 0.39U

cis-1,3-Dichloropropene10061-01-5 1.2 1.2 0.25U

Trichloroethene79-01-6 1.2 1.2 0.45U

Dibromochloromethane124-48-1 1.2 1.2 0.69U


Benzene71-43-2 1.2 1.2 0.91U

trans-1,3-Dichloropropene10061-02-6 1.2 1.2 0.27U

2-Chloroethyl vinyl ether110-75-8 6.1 6.1 1.6U

Bromoform75-25-2 1.2 1.2 0.86U

Tetrachloroethene127-18-4 1.2 1.2 0.40U

1,1,2,2-Tetrachloroethane79-34-5 1.2 1.2 0.93U

Toluene108-88-3 1.2 1.2 0.37U

Chlorobenzene108-90-7 1.2 1.2 0.59U

Ethylbenzene100-41-4 1.2 1.2 0.23U

Xylenes, Total1330-20-7 3.7 3.7 0.96U

FORM I 8260B

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-3 6-7

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 09:45

Sample wt/vol:

% Moisture:



18.8

1


5.02(g)

0.18(mm)

Date Analyzed: 05/18/2010 00:18

ID:DB-624


SURROGATE %RECCAS NO. LIMITS Q

17060-07-0 1,2-Dichloroethane-d4 (Surr) 92 70-138

2037-26-5 Toluene-d8 (Surr) 88 66-126

460-00-4 Bromofluorobenzene 102 72-132

FORM I 8260B

06/03/2010 of 623


TENTATIVELY IDENTIFIED COMPOUNDS

Client Sample ID:

Lab Name: Job No.:

TB-3 6-7

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 09:45

Sample wt/vol:

% Moisture:



18.8

1


5.02(g)

0.18(mm)

Date Analyzed: 05/18/2010 00:18

ID:DB-624


Number TICs Found: TIC Result Total: 00

QRTCOMPOUND NAME RESULTCAS NO.


FORM I-TIC 8260B

06/03/2010 of 623

Data File: /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37400.dReport Date: 18-May-2010 09:27

TestAmerica

VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37400.dLab Smp Id: 460-13139-B-2-A Client Smp ID: TB-3 6-7Inj Date : 18-MAY-2010 00:18 Operator : VOAMS 9 Inst ID: VOAMS12.iSmp Info : 460-13139-B-2-A;;;5.02;5Misc Info : 460-13139-B-2-AComment : Method : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/8260L_10.mMeth Date : 17-May-2010 18:29 ken Quant Type: ISTDCal Date : 15-APR-2010 16:52 Cal File: o36298.dAls bottle: 16 Dil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd2

Concentration Formula: Amt * DF * ((Vt/Ws)/((100-M)/100)) * CpndVariable

Name Value Description-------------- -------------- -----------------------

DF 1.00000 Dilution FactorVt 5.00000 Volume of final extract (mL)Ws 5.02000 Weight of sample extracted (g)M 18.78882 % Moisture (not decanted)

Cpnd Variable Local Compound Variable

CONCENTRATIONS

QUANT SIG ON-COLUMN FINAL

Compounds MASS RT EXP RT REL RT RESPONSE ( ug/L) (ug/Kg)

========================== ==== == ====== ====== ======== ======= =======

$ 16 1,2-Dichloroethane-d4 (SUR) 65 3.933 3.933 (0.923) 308316 45.9493 56

* 69 Fluorobenzene 96 4.262 4.262 (1.000) 1493462 50.0000

$ 37 Toluene-d8 (SUR) 98 6.072 6.073 (0.754) 1191531 43.8335 54

* 32 Chlorobenzene-d5 117 8.054 8.054 (1.000) 1272951 50.0000

$ 41 Bromofluorobenzene (SUR) 174 9.913 9.913 (0.845) 400760 50.9986 62

* 91 1,4-Dichlorobenzene-d4 152 11.736 11.730 (1.000) 616746 50.0000

06/03/2010 of 623


TestAmerica


- NO TENTATIVELY IDENTIFIED COMPOUNDS -

06/03/2010 of 623

Data File: o37400.d

Date: 18-MAY-2010 00:18

Client ID: TB-3 6-7 Instrument: VOAMS12.i

Sample Info: 460-13139-B-2-A;;;5.02;5 Operator: VOAMS 9

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-2 5-6

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 10:45

Sample wt/vol:

% Moisture:



12.8

1


3.75(g)

0.18(mm)

Date Analyzed: 05/18/2010 00:43

ID:DB-624




Bromomethane74-83-9 1.5 1.5 0.63U


Chloroethane75-00-3 1.5 1.5 0.61U







Chloroform67-66-3 1.5 1.5 0.36U










Benzene71-43-2 1.5 1.5 1.1U



Bromoform75-25-2 1.5 1.5 1.1U



Toluene108-88-3 1.5 1.5 0.46U


Ethylbenzene100-41-4 1.5 1.5 0.29U

Xylenes, Total1330-20-7 4.6 4.6 1.2U

FORM I 8260B

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-2 5-6

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 10:45

Sample wt/vol:

% Moisture:



12.8

1


3.75(g)

0.18(mm)

Date Analyzed: 05/18/2010 00:43

ID:DB-624




2037-26-5 Toluene-d8 (Surr) 89 66-126


FORM I 8260B

06/03/2010 of 623



Client Sample ID:

Lab Name: Job No.:

TB-2 5-6

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 10:45

Sample wt/vol:

% Moisture:



12.8

1


3.75(g)

0.18(mm)

Date Analyzed: 05/18/2010 00:43

ID:DB-624





FORM I-TIC 8260B

06/03/2010 of 623


TestAmerica






CONCENTRATIONS



========================== ==== == ====== ====== ======== ======= =======


* 69 Fluorobenzene 96 4.262 4.262 (1.000) 1437887 50.0000

$ 37 Toluene-d8 (SUR) 98 6.073 6.073 (0.754) 1088814 44.5595 68

* 32 Chlorobenzene-d5 117 8.054 8.054 (1.000) 1144265 50.0000



06/03/2010 of 623


TestAmerica



06/03/2010 of 623

Data File: o37401.d

Date: 18-MAY-2010 00:43



06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-1 2-3

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 11:25

Sample wt/vol:

% Moisture:



6.5

1


3.09(g)

0.18(mm)

Date Analyzed: 05/18/2010 01:08

ID:DB-624




Bromomethane74-83-9 1.7 1.7 0.71U


Chloroethane75-00-3 1.7 1.7 0.69U







Chloroform67-66-3 1.7 1.7 0.41U










Benzene71-43-2 1.7 1.7 1.3U



Bromoform75-25-2 1.7 1.7 1.2U



Toluene108-88-3 1.7 1.7 0.52U


Ethylbenzene100-41-4 1.7 1.7 0.33U

Xylenes, Total1330-20-7 5.2 5.2 1.4U

FORM I 8260B

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-1 2-3

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 11:25

Sample wt/vol:

% Moisture:



6.5

1


3.09(g)

0.18(mm)

Date Analyzed: 05/18/2010 01:08

ID:DB-624




2037-26-5 Toluene-d8 (Surr) 90 66-126


FORM I 8260B

06/03/2010 of 623



Client Sample ID:

Lab Name: Job No.:

TB-1 2-3

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 11:25

Sample wt/vol:

% Moisture:



6.5

1


3.09(g)

0.18(mm)

Date Analyzed: 05/18/2010 01:08

ID:DB-624





FORM I-TIC 8260B

06/03/2010 of 623


TestAmerica






CONCENTRATIONS



========================== ==== == ====== ====== ======== ======= =======


* 69 Fluorobenzene 96 4.262 4.262 (1.000) 1396875 50.0000

$ 37 Toluene-d8 (SUR) 98 6.073 6.073 (0.754) 1200401 45.2140 78

* 32 Chlorobenzene-d5 117 8.054 8.054 (1.000) 1243273 50.0000



06/03/2010 of 623


TestAmerica



06/03/2010 of 623

Data File: o37402.d

Date: 18-MAY-2010 01:08



06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-5 3-4

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 12:30

Sample wt/vol:

% Moisture:



61.5

1


2.50(g)

0.18(mm)

Date Analyzed: 05/18/2010 01:33

ID:DB-624




Bromomethane74-83-9 5.2 5.2 2.1U


Chloroethane75-00-3 5.2 5.2 2.1U







Chloroform67-66-3 5.2 5.2 1.2U










Benzene71-43-2 5.2 5.2 3.8U


2-Chloroethyl vinyl ether110-75-8 26 26 6.6U

Bromoform75-25-2 5.2 5.2 3.6U



Toluene108-88-3 5.2 5.2 1.6U


Ethylbenzene100-41-4 5.2 5.2 0.99U

Xylenes, Total1330-20-7 16 16 4.1U

FORM I 8260B

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-5 3-4

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 12:30

Sample wt/vol:

% Moisture:



61.5

1


2.50(g)

0.18(mm)

Date Analyzed: 05/18/2010 01:33

ID:DB-624




2037-26-5 Toluene-d8 (Surr) 73 66-126


FORM I 8260B

06/03/2010 of 623



Client Sample ID:

Lab Name: Job No.:

TB-5 3-4

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 12:30

Sample wt/vol:

% Moisture:



61.5

1


2.50(g)

0.18(mm)

Date Analyzed: 05/18/2010 01:33

ID:DB-624




67-64-1 Acetone 1100 1.94

78-93-3 2-Butanone (MEK) 220 3.23

Unknown 28 10.68 T J

FORM I-TIC 8260B

06/03/2010 of 623


TestAmerica






CONCENTRATIONS



========================== ==== == ====== ====== ======== ======= =======

7 Acetone 43 1.939 1.939 (0.455) 364133 218.087 440

8 Carbon Disulfide 76 2.043 2.037 (0.479) 79922 3.20859 6.4

18 2-Butanone 72 3.226 3.213 (0.757) 38209 42.9502 86


* 69 Fluorobenzene 96 4.262 4.262 (1.000) 1175155 50.0000

$ 37 Toluene-d8 (SUR) 98 6.073 6.073 (0.754) 809402 36.4566 73

* 32 Chlorobenzene-d5 117 8.054 8.054 (1.000) 1039684 50.0000


112 n-Propylbenzene 91 10.377 10.377 (0.885) 41788 0.89175 1.8(a)


70 Naphthalene 128 14.016 14.016 (1.195) 59928 2.13807 4.3

06/03/2010 of 623


QC Flag Legend

a - Target compound detected but, quantitated amountBelow Limit Of Quantitation(BLOQ).

06/03/2010 of 623


TestAmerica






ISTD RT AREA AMOUNT======== ==== ====== ======

* 91 1,4-Dichlorobenzene-d4 11.730 2775259 50.000

CONCENTRATIONS QUANT

RT AREA ON-COL( ug/L) FINAL(ug/Kg) QUAL LIBRARY LIB ENTRY CPND #

==== ==== ============= ============ ==== ======= ========= ======

Unknown CAS #:

10.675 296942 5.34980704 11 0 0 91

06/03/2010 of 623

Data File: o37403.d

Date: 18-MAY-2010 01:33



06/03/2010 of 623

Data File: o37403.d

Date: 18-MAY-2010 01:33



7 Acetone

06/03/2010 of 623

Data File: o37403.d

Date: 18-MAY-2010 01:33



18 2-Butanone

06/03/2010 of 623

Data File: o37403.d

Date: 18-MAY-2010 01:33



Retention Time: 10.68

Library Search Compound Match CAS Number Library Entry Quality Formula Weight

Unknown

Bicyclo[2.2.1]heptane, 2-ethyl- 2146-41-0 NIST02.l 10368 53 C9H16 124

Bicyclo[2.2.1]heptane, 2,2,3-trime 473-19-8 NIST02.l 16369 49 C10H18 138

06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA


VOAMS12

Analy Batch No.: 34969

5832Calibration Start Date: Calibration End Date:04/15/2010 14:24

Y

04/15/2010 16:52

0.18(mm)DB-624 ID:

INTERNAL STANDARD CURVE EVALUTION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-34969/2 o36292.d2Level IC 460-34969/3 o36294.d3Level ICIS 460-34969/19 o36295.d4Level IC 460-34969/20 o36296.d5Level IC 460-34969/6 o36297.d6Level IC 460-34969/7 o36298.d

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVETYPE

COEFFICIENT

B M1 M2

# %RSD # MAX%RSD

R^2OR COD

# MIN R^2OR COD

MIN RRF

LVL 6

1-Chloropropane +++++ +++++ +++++ +++++ +++++ Ave+++++

15.0

2-Chloropropane +++++ +++++ +++++ +++++ +++++ Ave+++++

15.0

Propene +++++ +++++ +++++ +++++ +++++ Ave+++++

15.0

Dichlorodifluoromethane 0.5422 0.5230 0.4719 0.4493 0.3392 LinF 0.99800.3324

0.99000.3350

Chloromethane 0.7369 0.6514 0.6123 0.5870 0.4788 LinF 0.99750.4445

0.99000.4514

Vinyl chloride 0.6601 0.6229 0.5878 0.5762 0.4739 LinF 0.99770.4412

0.99000.4477

Bromomethane 0.5004 0.4223 0.3596 0.3414 0.2989 LinF 0.99970.3024

0.99000.3024

Chloroethane 0.4318 0.3538 0.3330 0.3191 0.2733 LinF 0.99890.2611

0.1000 0.99000.2636

Trichlorofluoromethane 0.8600 0.7309 0.7035 0.6806 0.5835 LinF 0.99940.5714

0.99000.5744

n-Pentane 0.0786 0.0654 0.0729 0.0691 0.0621 Ave 9.50.0624

15.00.0684

Ethanol 0.0021 0.0025 0.0021 0.0022 0.0019 Ave 11.10.0019

15.00.0021

Ethyl ether 0.3123 0.2860 0.2487 0.2510 0.2423 Ave 11.20.2380

15.00.2631

Isopropene 0.5603 0.5498 0.5790 0.5747 0.5229 Ave 5.40.5045

15.00.5485

Acrolein 0.0326 0.0383 0.0348 0.0342 0.0432 Ave 11.60.0419

15.00.0375

Freon TF 0.4614 0.4173 0.3915 0.3885 0.3381 Ave 12.10.3393

15.00.3893

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




VOAMS12



Y

04/15/2010 16:52

0.18(mm)DB-624 ID:


ANALYTE RRF


CURVETYPE

COEFFICIENT

B M1 M2

# %RSD # MAX%RSD

R^2OR COD

# MIN R^2OR COD

MIN RRF

LVL 6

1,1-Dichloroethene 0.3567 0.3868 0.3609 0.3527 0.2925 Ave 12.70.2780

30.00.3379

Acetone 0.2171 0.1630 0.1347 0.1050 0.0764 LinF 0.99740.0705

0.99000.0710

Iodomethane 0.4149 0.4209 0.4047 0.4057 0.3919 Ave 5.40.3611

15.00.3999

Carbon disulfide 1.1556 1.1071 0.9874 0.9904 1.0476 Ave 6.21.0708

15.01.0598

Isopropanol 0.0335 0.0285 0.0263 0.0252 0.0223 QuaF 0.99390.0224

0.990027.334 6.7713

Acetonitrile 0.0797 0.0687 0.0555 0.0514 0.0413 LinF 0.99710.0383

0.99000.0389

Methyl acetate 0.1414 0.1031 0.0986 0.0946 0.0739 LinF 0.99820.0714

0.99000.0721

Methylene Chloride 0.6993 0.4490 0.4137 0.3900 0.3457 LinF 0.99890.3276

0.99000.3310

TBA 0.0449 0.0371 0.0363 0.0324 0.0315 Ave 14.30.0319

15.00.0357

Acrylonitrile 0.1378 0.1573 0.1442 0.1383 0.1202 Ave 10.00.1230

15.00.1368

trans-1,2-Dichloroethene 0.4591 0.3997 0.4069 0.3867 0.3531 Ave 10.80.3413

15.00.3911

MTBE 0.7522 0.7264 0.7701 0.7537 0.8260 Ave 5.40.8293

15.00.7763

Hexane 0.2712 0.2468 0.2783 0.3051 0.2725 Ave 7.00.2879

15.00.2770

1,1-Dichloroethane 0.7985 0.6736 0.6844 0.6636 0.6035 Ave 11.40.5809

0.1000 15.00.6674

Vinyl acetate 0.7102 0.6659 0.6585 0.7316 0.8552 Ave 12.10.8631

15.00.7474

DIPE 0.9238 0.8739 0.9124 0.9208 0.9686 Ave 4.30.9825

15.00.9303

Tert-butyl ethyl ether 0.8043 0.7458 0.7718 0.7954 0.8662 Ave 6.80.8894

15.00.8122

2,2-Dichloropropane 0.4367 0.4241 0.4810 0.4947 0.4619 Ave 5.90.4469

15.00.4576

cis-1,2-Dichloroethene 0.4420 0.4127 0.3905 0.3782 0.3555 Ave 9.40.3441

15.00.3871

2-Butanone (MEK) 0.0402 0.0413 0.0418 0.0358 0.0356 Ave 9.90.0325

15.00.0379

FORM VI 8260B


06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




VOAMS12



Y

04/15/2010 16:52

0.18(mm)DB-624 ID:


ANALYTE RRF


CURVETYPE

COEFFICIENT

B M1 M2

# %RSD # MAX%RSD

R^2OR COD

# MIN R^2OR COD

MIN RRF

LVL 6

Ethyl acetate 0.0343 0.0270 0.0273 0.0270 0.0272 Ave 10.30.0274

15.00.0284

Bromochloromethane 0.1824 0.1690 0.1589 0.1525 0.1433 Ave 10.80.1362

15.00.1570

Chloroform 0.7318 0.6185 0.6128 0.5890 0.5544 Ave 10.90.5499

30.00.6094

1,1,1-Trichloroethane 0.5194 0.4678 0.5175 0.5211 0.4874 Ave 4.90.4747

15.00.4980

Cyclohexane 0.7209 0.7001 0.6953 0.6890 0.6215 Ave 5.90.6323

15.00.6765

Carbon tetrachloride 0.3909 0.3596 0.4181 0.4239 0.4178 Ave 6.10.4124

15.00.4038

1,1-Dichloropropene 0.4333 0.4166 0.4845 0.4915 0.4867 Ave 6.70.4623

15.00.4625

Benzene 1.4368 1.2625 1.4254 1.4012 1.3909 Ave 7.11.2032

15.01.3534

1,2-Dichloroethane 0.5055 0.4206 0.3973 0.3883 0.3803 Ave 11.90.3750

15.00.4112

Isopropyl acetate 0.5114 0.4721 0.4965 0.5065 0.5711 Ave 8.80.5917

15.00.5249

Tert-amyl methyl ether 0.7638 0.6725 0.6680 0.6704 0.7741 Ave 8.70.8091

15.00.7263

2,4,4-Trimethyl-1-pentene 0.1589 0.1533 0.1271 0.1094 0.1244 LinF 0.99860.1145

0.99000.1160

n-Butanol 0.0056 0.0051 0.0049 0.0051 0.0059 Ave 7.9+++++

15.00.0053

Trichloroethene 0.3853 0.2935 0.3554 0.3502 0.3483 Ave 8.70.3348

15.00.3446

Ethyl acrylate 0.2788 0.3205 0.3000 0.2903 0.3398 Ave 11.50.3775

15.00.3178

Methylcyclohexane 0.6899 0.6140 0.6233 0.6729 0.6673 Ave 4.80.6806

15.00.6580

1,2-Dichloropropane 0.3272 0.3162 0.3472 0.3397 0.3525 Ave 4.00.3412

30.00.3373

Dibromomethane 0.2263 0.1838 0.1837 0.1683 0.1706 Ave 12.90.1605

15.00.1822

Methyl methacrylate 0.2304 0.1751 0.1533 0.1547 0.1778 LinF 0.99970.1806

0.99000.1800

1,4-Dioxane 0.0053 0.0050 0.0047 0.0048 0.0040 Ave 10.90.0040

15.00.0046

FORM VI 8260B


06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




VOAMS12



Y

04/15/2010 16:52

0.18(mm)DB-624 ID:


ANALYTE RRF


CURVETYPE

COEFFICIENT

B M1 M2

# %RSD # MAX%RSD

R^2OR COD

# MIN R^2OR COD

MIN RRF

LVL 6

Propyl acetate 0.6412 0.4143 0.3513 0.3249 0.3538 LinF 0.99980.3615

0.99000.3602

Bromodichloromethane 0.3759 0.3509 0.3764 0.3816 0.4128 Ave 5.90.4072

15.00.3841

2-Chloroethyl vinyl ether 0.1481 0.1363 0.1568 0.1534 0.1721 Ave 9.10.1731

15.00.1566

Epichlorohydrin 0.0353 0.0318 0.0313 0.0314 0.0298 Ave 6.90.0291

15.00.0314

cis-1,3-Dichloropropene 0.4131 0.3734 0.4403 0.4623 0.5085 Ave 11.70.5047

15.00.4504

4-Methyl-2-pentanone 0.2698 0.2986 0.2259 0.2063 0.2312 Ave 13.50.2440

15.00.2460

Toluene 2.3018 1.9052 2.1270 2.1672 2.2207 Ave 9.01.8199

30.02.0903

trans-1,3-Dichloropropene 0.3710 0.3293 0.4953 0.6079 0.6839 LinF 0.99940.6555

0.99000.6590

1,1,2-Trichloroethane 0.2547 0.2126 0.2863 0.3296 0.3372 LinF 0.99920.3160

0.99000.3191

Tetrachloroethene 0.4564 0.3454 0.4757 0.5142 0.5068 Ave 13.20.4744

15.00.4622

1,3-Dichloropropane 0.5130 0.4647 0.6361 0.7046 0.7217 LinF 0.99890.6696

0.99000.6775

2-Hexanone 0.2538 0.2803 0.2756 0.2502 0.2560 Ave 4.70.2622

15.00.2630

Dibromochloromethane 0.2869 0.2226 0.3072 0.3707 0.4176 LinF 0.99960.4085

0.99000.4093

Butyl acetate 0.5680 0.5336 0.5756 0.5675 0.5791 Ave 3.40.5902

15.00.5690

1,2-Dibromoethane 0.3063 0.2340 0.3332 0.3706 0.3860 LinF 0.99880.3569

0.99000.3613

Chlorobenzene 1.2679 1.1200 1.2725 1.2968 1.3206 Ave 5.71.2848

0.3000 15.01.2604

1,1,1,2-Tetrachloroethane 0.2799 0.2352 0.3204 0.3925 0.4407 LinF 0.99970.4357

0.99000.4359

Ethylbenzene 0.7265 0.6553 0.8122 0.7992 0.7490 Ave 7.60.7259

30.00.7447

m&p-Xylene 0.8901 0.7708 0.9340 1.0419 0.9389 Ave 9.80.8795

15.00.9092

o-Xylene 0.7751 0.6844 0.8605 0.9569 0.8858 Ave 11.30.8442

15.00.8345

FORM VI 8260B


06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




VOAMS12



Y

04/15/2010 16:52

0.18(mm)DB-624 ID:


ANALYTE RRF


CURVETYPE

COEFFICIENT

B M1 M2

# %RSD # MAX%RSD

R^2OR COD

# MIN R^2OR COD

MIN RRF

LVL 6

Styrene 1.2501 1.2182 1.4946 1.6541 1.5547 Ave 12.01.4868

15.01.4431

Butyl acrylate 1.3787 1.2580 1.4226 1.5065 1.5332 Ave 10.21.6981

15.01.4662

Bromoform 0.1386 0.1208 0.1751 0.2106 0.2513 LinF 0.99940.2460

0.1000 0.99000.2464

Amly acetate 0.4099 0.3020 0.3435 0.3906 0.3512 Ave 10.50.3574

15.00.3591

Isopropylbenzene 2.1964 2.0047 2.4498 2.6946 2.3715 Ave 11.1+++++

15.02.3434

Camphene, Total 2.2489 1.9256 2.1205 2.0478 1.9104 Ave 6.22.1013

15.02.0591

Monobromobenzene 0.9530 0.8847 0.9827 0.9396 0.9594 Ave 3.60.9675

15.00.9478

1,1,2,2-Tetrachloroethane 0.8387 0.8089 0.8413 0.8148 0.9519 Ave 7.70.9550

0.3000 15.00.8684

1,2,3-Trichloropropane 0.2734 0.2262 0.2388 0.2331 0.2634 Ave 7.50.2556

15.00.2484

trans-1,4-Dichloro-2-butene 0.1289 0.1059 0.0854 0.0864 0.0933 LinF 0.99960.0970

0.99000.0964

N-Propylbenzene 5.4669 5.0455 5.9803 5.9824 5.9666 Ave 11.04.5322

15.05.4957

2-Chlorotoluene 2.9808 2.8955 3.1492 3.1611 3.2284 Ave 4.33.2030

15.03.1030

4-Chlorotoluene 3.4495 3.1411 3.6488 3.5594 3.4194 Ave 5.13.3468

15.03.4275

1,3,5-Trimethylbenzene 3.4507 3.2570 3.6512 3.6565 3.9036 Ave 6.13.6355

15.03.5924

Butyl Methacrylate 1.2020 1.1220 1.2390 1.2626 1.3882 Ave 10.61.5005

15.01.2857

tert-Butylbenzene 2.8468 2.9677 3.4949 3.4946 3.4726 Ave 8.93.3642

15.03.2735

1,2,4-Trimethylbenzene 3.8350 3.2180 3.6764 3.6460 3.9729 Ave 7.43.4518

15.03.6334

2-Octanone 1.1732 1.0771 1.1937 1.0591 1.0825 Ave 5.01.0923

15.01.1130

sec-Butylbenzene 4.7292 4.7248 5.5718 5.5007 5.5211 Ave 13.03.9449

15.04.9987

1,3-Dichlorobenzene 2.2056 1.7788 2.0167 1.9751 2.0327 Ave 6.82.0180

15.02.0045

FORM VI 8260B


06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




VOAMS12



Y

04/15/2010 16:52

0.18(mm)DB-624 ID:


ANALYTE RRF


CURVETYPE

COEFFICIENT

B M1 M2

# %RSD # MAX%RSD

R^2OR COD

# MIN R^2OR COD

MIN RRF

LVL 6

2-Octanol 0.2304 0.1953 0.2458 0.2713 0.2585 Ave 14.40.3007

15.00.2503


15.02.0602

p-Isopropyltoluene 3.8704 3.7613 4.5046 4.4095 4.6907 Ave 13.03.3025

15.04.0898

Benzyl chloride 1.2846 1.0362 1.3102 1.4331 1.7114 LinF 0.99851.8267

0.99001.8086


15.01.8859

n-Butylbenzene 4.0798 3.8435 4.5477 4.4464 4.6438 Ave 14.13.0968

15.04.1097

1,2-Dibromo-3-Chloropropane 0.2351 0.1691 0.1723 0.1811 0.1894 Ave 13.10.1761

15.00.1872

Camphor 0.1451 0.1046 0.1229 0.1290 0.1077 Ave 12.90.1103

15.00.1199

1,2,4-Trichlorobenzene 1.5255 1.3520 1.4523 1.3933 1.4237 Ave 4.91.3351

15.01.4136

Hexachlorobutadiene 0.7886 0.7609 0.8828 0.8772 0.8562 Ave 6.20.8012

15.00.8278

Naphthalene 3.7939 3.3083 3.5240 3.3931 3.3446 Ave 14.82.3591

15.03.2871


15.01.3309

1,2-Dichloroethane-d4 (Surr) 0.2481 0.2510 0.2240 0.2169 0.2022 Ave 9.30.2056

15.00.2246

Toluene-d8 (Surr) 1.0332 0.9949 1.0658 1.0999 1.0968 Ave 4.31.1157

15.01.0677

Bromofluorobenzene 0.6140 0.6436 0.6675 0.6346 0.6129 Ave 3.30.6497

15.00.6371

FORM VI 8260B


06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)



VOAMS12



Y

04/15/2010 16:52

GC Column: DB-624 ID: 0.18(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-34969/2 o36292.dLevel 2 IC 460-34969/3 o36294.dLevel 3 ICIS 460-34969/19 o36295.dLevel 4 IC 460-34969/20 o36296.dLevel 5 IC 460-34969/6 o36297.dLevel 6 IC 460-34969/7 o36298.d

ANALYTE CURVETYPE

ISREF

RESPONSE


CONCENTRATION (UG/L)

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5LVL 6 LVL 6

1-Chloropropane AveCBZ +++++ +++++ +++++ +++++ ++++++++++

+++++ +++++ +++++ +++++ ++++++++++

2-Chloropropane AveFB +++++ +++++ +++++ +++++ ++++++++++

+++++ +++++ +++++ +++++ ++++++++++

Propene AveFB +++++ +++++ +++++ +++++ ++++++++++

+++++ +++++ +++++ +++++ ++++++++++

Dichlorodifluoromethane LinFFB 9829 51094 209388 506957 19808165162135

1.00 5.00 20.0 50.0 200500

Chloromethane LinFFB 13358 63632 271705 662255 27957136903964

1.00 5.00 20.0 50.0 200500

Vinyl chloride LinFFB 11966 60847 260836 650079 27674276851705

1.00 5.00 20.0 50.0 200500

Bromomethane LinFFB 9071 41254 159558 385155 17452934696427

1.00 5.00 20.0 50.0 200500

Chloroethane LinFFB 7827 34561 147753 359969 15955594055833

1.00 5.00 20.0 50.0 200500

Trichlorofluoromethane LinFFB 15590 71397 312150 767854 34073618874740

1.00 5.00 20.0 50.0 200500

n-Pentane AveFB 1424 6387 32359 78006 362390968730

1.00 5.00 20.0 50.0 200500

Ethanol AveFB 38307 98550 142293 197624 275689349834

1000 2000 3000 4000 50006000

Ethyl ether AveFB 5662 27938 110374 283184 14150743696360

1.00 5.00 20.0 50.0 200500

Isopropene AveFB 10157 53707 256913 648374 30535577835552

1.00 5.00 20.0 50.0 200500

Acrolein AveFB 59019 149526 231470 308394 629909781848

100 200 300 400 500600

Freon TF AveFB 8364 40760 173734 438279 19741885270220

1.00 5.00 20.0 50.0 200500

1,1-Dichloroethene AveFB 6467 37786 160155 397935 17077694317065

1.00 5.00 20.0 50.0 200500

FORM VI 8260B 06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




VOAMS12



Y

04/15/2010 16:52



ANALYTE CURVETYPE

ISREF

RESPONSE




Acetone LinFFB 39351 47775 59779 118448 4463382191135

10.0 15.0 20.0 50.0 2001000

Iodomethane AveFB 7522 41118 179591 457708 22886415607660

1.00 5.00 20.0 50.0 200500

Carbon disulfide AveFB 20948 108150 438107 1117367 611712316630794

1.00 5.00 20.0 50.0 200500

Isopropanol QuaFFB 607480 1113792 1749554 2278520 32541834167051

1000 2000 3000 4000 50006000

Acetonitrile LinFFB 28912 134192 492092 1160085 482225511905866

20.0 100 400 1000 400010000

Methyl acetate LinFFB 2564 10076 43755 106674 4317731109552

1.00 5.00 20.0 50.0 200500

Methylene Chloride LinFFB 12677 43858 183554 440031 20185365088257

1.00 5.00 20.0 50.0 200500

TBA AveFB 16289 72467 322329 730139 36831819907107

20.0 100 400 1000 400010000

Acrylonitrile AveFB 124913 307269 479998 624185 8774371146198

50.0 100 150 200 250300

trans-1,2-Dichloroethene AveFB 8322 39047 180556 436305 20619325301198

1.00 5.00 20.0 50.0 200500

MTBE AveFB 13636 70955 341696 850298 482340312880704

1.00 5.00 20.0 50.0 200500

Hexane AveFB 4917 24105 123471 344172 15912144471278

1.00 5.00 20.0 50.0 200500

1,1-Dichloroethane AveFB 14475 65799 303680 748689 35236609022002

1.00 5.00 20.0 50.0 200500

Vinyl acetate AveFB 12875 65052 292196 825367 499389613405213

1.00 5.00 20.0 50.0 200500

DIPE AveFB 16747 85364 404838 1038836 565594115260277

1.00 5.00 20.0 50.0 200500

Tert-butyl ethyl ether AveFB 14581 72855 342469 897352 505802813814023

1.00 5.00 20.0 50.0 200500

2,2-Dichloropropane AveFB 7917 41430 213438 558153 26972996940846

1.00 5.00 20.0 50.0 200500

cis-1,2-Dichloroethene AveFB 8012 40310 173250 426651 20760355343818

1.00 5.00 20.0 50.0 200500

2-Butanone (MEK) AveFB 7281 12096 18549 40377 2076681009784

10.0 15.0 20.0 50.0 2001000

Ethyl acetate AveFB 1244 5268 24213 61001 318096850152

2.00 10.0 40.0 100 4001000

Bromochloromethane AveFB 3306 16505 70511 172015 8368402115548

1.00 5.00 20.0 50.0 200500

FORM VI 8260B 06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




VOAMS12



Y

04/15/2010 16:52



ANALYTE CURVETYPE

ISREF

RESPONSE




Chloroform AveFB 13266 60420 271900 664487 32370828541410

1.00 5.00 20.0 50.0 200500

1,1,1-Trichloroethane AveFB 9415 45699 229638 587888 28459317373424

1.00 5.00 20.0 50.0 200500

Cyclohexane AveFB 13068 68390 308504 777281 36287769820423

1.00 5.00 20.0 50.0 200500

Carbon tetrachloride AveFB 7086 35128 185522 478191 24396586405906

1.00 5.00 20.0 50.0 200500

1,1-Dichloropropene AveFB 7854 40700 215002 554490 28421917179727

1.00 5.00 20.0 50.0 200500

Benzene AveFB 26047 123328 632459 1580850 812180918688215

1.00 5.00 20.0 50.0 200500

1,2-Dichloroethane AveFB 9163 41087 176271 438030 22205455824849

1.00 5.00 20.0 50.0 200500

Isopropyl acetate AveFB 18542 92236 440643 1142906 667003118380366

2.00 10.0 40.0 100 4001000

Tert-amyl methyl ether AveFB 13847 65690 296423 756316 452019312567064

1.00 5.00 20.0 50.0 200500

2,4,4-Trimethyl-1-pentene LinFFB 2880 14973 56393 123454 7263291778966

1.00 5.00 20.0 50.0 200500

n-Butanol AveFB 50719 100546 163835 229028 433389+++++

500 1000 1500 2000 2500+++++

Trichloroethene AveFB 6984 28668 157706 395065 20335265200531

1.00 5.00 20.0 50.0 200500

Ethyl acrylate AveFB 5054 31305 133126 327562 19841185863032

1.00 5.00 20.0 50.0 200500

Methylcyclohexane AveFB 12506 59982 276571 759186 389657610569957

1.00 5.00 20.0 50.0 200500

1,2-Dichloropropane AveFB 5931 30886 154070 383264 20584975299536

1.00 5.00 20.0 50.0 200500

Dibromomethane AveFB 4103 17950 81516 189900 9963672492277

1.00 5.00 20.0 50.0 200500

Methyl methacrylate LinFFB 4177 17107 68043 174550 10384152804649

1.00 5.00 20.0 50.0 200500

1,4-Dioxane AveFB 95558 194311 311068 430938 587679751736

1000 2000 3000 4000 50006000

Propyl acetate LinFFB 23248 80944 311765 733128 413153211229348

2.00 10.0 40.0 100 4001000

Bromodichloromethane AveFB 6814 34281 167023 430487 24106556324586

1.00 5.00 20.0 50.0 200500

2-Chloroethyl vinyl ether AveFB 2685 13317 69580 173060 10047082689127

1.00 5.00 20.0 50.0 200500

FORM VI 8260B 06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




VOAMS12



Y

04/15/2010 16:52



ANALYTE CURVETYPE

ISREF

RESPONSE




Epichlorohydrin AveFB 12794 62116 277498 709199 34753469034273

20.0 100 400 1000 400010000

cis-1,3-Dichloropropene AveFB 7489 36479 195348 521566 29692157838898

1.00 5.00 20.0 50.0 200500

4-Methyl-2-pentanone AveFB 48901 87506 100225 232775 13502757579276

10.0 15.0 20.0 50.0 2001000

Toluene AveCBZ 35372 169702 653762 1476565 827436719110155

1.00 5.00 20.0 50.0 200500

trans-1,3-Dichloropropene LinFCBZ 5701 29332 152245 414159 25481866883355

1.00 5.00 20.0 50.0 200500

1,1,2-Trichloroethane LinFCBZ 3914 18939 87997 224539 12562863317800

1.00 5.00 20.0 50.0 200500

Tetrachloroethene AveCBZ 7013 30765 146217 350365 18884034981279

1.00 5.00 20.0 50.0 200500

1,3-Dichloropropane LinFCBZ 7884 41392 195511 480075 26892197031925

1.00 5.00 20.0 50.0 200500

2-Hexanone AveCBZ 39000 74898 84694 170489 9540335507288

10.0 15.0 20.0 50.0 2001000

Dibromochloromethane LinFCBZ 4409 19824 94435 252590 15560834289334

1.00 5.00 20.0 50.0 200500

Butyl acetate AveCBZ 17457 95060 353843 773295 431534112396122

2.00 10.0 40.0 100 4001000

1,2-Dibromoethane LinFCBZ 4707 20839 102404 252470 14381853748152

1.00 5.00 20.0 50.0 200500

Chlorobenzene AveCBZ 19484 99759 391122 883565 492042813491058

1.00 5.00 20.0 50.0 200500

1,1,1,2-Tetrachloroethane LinFCBZ 4301 20949 98481 267402 16421794574855

1.00 5.00 20.0 50.0 200500

Ethylbenzene AveCBZ 11165 58368 249628 544539 27908627622609

1.00 5.00 20.0 50.0 200500

m&p-Xylene AveCBZ 27357 137315 574126 1419678 699687518471786

2.00 10.0 40.0 100 4001000

o-Xylene AveCBZ 11912 60960 264498 651941 33005128864989

1.00 5.00 20.0 50.0 200500

Styrene AveCBZ 19210 108506 459380 1126968 579281615613202

1.00 5.00 20.0 50.0 200500

Butyl acrylate AveDCB 11389 56933 233518 610553 31154079103920

1.00 5.00 20.0 50.0 200500

Bromoform LinFCBZ 2130 10756 53806 143454 9364692583583

1.00 5.00 20.0 50.0 200500

Amly acetate AveCBZ 6299 26904 105586 266112 13083853753042

1.00 5.00 20.0 50.0 200500

FORM VI 8260B 06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




VOAMS12



Y

04/15/2010 16:52



ANALYTE CURVETYPE

ISREF

RESPONSE




Isopropylbenzene AveCBZ 33753 178564 752969 1835860 8836094+++++

1.00 5.00 20.0 50.0 200+++++

Camphene, Total AveDCB 18577 87150 348075 829962 388182911265636

1.00 5.00 20.0 50.0 200500

Monobromobenzene AveDCB 7872 40040 161302 380811 19493385186993

1.00 5.00 20.0 50.0 200500

1,1,2,2-Tetrachloroethane AveDCB 6928 36609 138101 330226 19341665119877

1.00 5.00 20.0 50.0 200500

1,2,3-Trichloropropane AveDCB 2258 10239 39196 94478 5352431370300

1.00 5.00 20.0 50.0 200500

trans-1,4-Dichloro-2-butene LinFFB 2337 10349 37887 97438 5449651506749

1.00 5.00 20.0 50.0 200500

N-Propylbenzene AveDCB 45159 228351 981644 2424606 1212370324298694

1.00 5.00 20.0 50.0 200500

2-Chlorotoluene AveDCB 24623 131044 516934 1281161 655983017172189

1.00 5.00 20.0 50.0 200500

4-Chlorotoluene AveDCB 28494 142158 598938 1442568 694807017942950

1.00 5.00 20.0 50.0 200500

1,3,5-Trimethylbenzene AveDCB 28504 147405 599323 1481917 793181119490914

1.00 5.00 20.0 50.0 200500

Butyl Methacrylate AveDCB 9929 50780 203371 511721 28207928044647

1.00 5.00 20.0 50.0 200500

tert-Butylbenzene AveDCB 23516 134310 573676 1416333 705616818036505

1.00 5.00 20.0 50.0 200500

1,2,4-Trimethylbenzene AveDCB 31679 145642 603459 1477665 807272818506249

1.00 5.00 20.0 50.0 200500

2-Octanone AveDCB 9691 48748 195932 429220 21996455855978

1.00 5.00 20.0 50.0 200500

sec-Butylbenzene AveDCB 39065 213837 914577 2229359 1121849821149703

1.00 5.00 20.0 50.0 200500

1,3-Dichlorobenzene AveDCB 18219 80505 331029 800495 413024510819131

1.00 5.00 20.0 50.0 200500

2-Octanol AveDCB 1903 8840 40343 109959 5252051612316

1.00 5.00 20.0 50.0 200500


1.00 5.00 20.0 50.0 200500

p-Isopropyltoluene AveDCB 31971 170228 739407 1787116 953128917705621

1.00 5.00 20.0 50.0 200500

Benzyl chloride LinFDCB 10611 46895 215067 580809 34774279793596

1.00 5.00 20.0 50.0 200500


1.00 5.00 20.0 50.0 200500

FORM VI 8260B 06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




VOAMS12



Y

04/15/2010 16:52



ANALYTE CURVETYPE

ISREF

RESPONSE




n-Butylbenzene AveDCB 33701 173948 746484 1802086 943599716602685

1.00 5.00 20.0 50.0 200500

1,2-Dibromo-3-Chloropropane AveDCB 1942 7653 28277 73411 384903944195

1.00 5.00 20.0 50.0 200500

Camphor AveDCB 5993 23678 100851 261323 10946122957724

5.00 25.0 100 250 10002500

1,2,4-Trichlorobenzene AveDCB 12601 61188 238386 564686 28929087158001

1.00 5.00 20.0 50.0 200500

Hexachlorobutadiene AveDCB 6514 34437 144905 355509 17396844295340

1.00 5.00 20.0 50.0 200500

Naphthalene AveDCB 31339 149725 578445 1375171 679593912647892

1.00 5.00 20.0 50.0 200500

1,2,3-Trichlorobenzene AveDCB 11972 60124 218509 539501 26708096600362

1.00 5.00 20.0 50.0 200500

1,2-Dichloroethane-d4 (Surr) AveFB 224919 245158 248478 244690 295209319383

50.0 50.0 50.0 50.0 50.050.0

Toluene-d8 (Surr) AveCBZ 793858 886156 818959 749412 10216651171616

50.0 50.0 50.0 50.0 50.050.0

Bromofluorobenzene AveDCB 253605 291292 273931 257206 311348348336

50.0 50.0 50.0 50.0 50.050.0

Curve Type Legend:Ave = Average ISTDLinF = Linear ISTD forced zeroQuaF = Quadratic ISTD forced zero

FORM VI 8260B 06/03/2010 of 623

FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

Calib End Date:GC Column: ID:

GC/MS VOA CONTINUING CALIBRATION DATA

0.18(mm)

460-13139-1

VOAMS12

05/17/2010 17:02

04/15/2010 14:24

04/15/2010 16:52

CCVIS 460-37643/2

DB-624

TestAmerica Edison

Lab File ID: o37385.d Heated Purge: (Y/N) YConc. Units: ug/L

ANALYTE CURVE AVE RRF RRF MIN RRF CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

Dichlorodifluoromethane LinF 0.41800.4430 25.0 20.0 24.8 50.0

Chloromethane LinF 0.48360.5852 0.1000 21.4 20.0 7.1 50.0

Vinyl chloride LinF 0.47800.5604 21.4 20.0 6.8 20.0

Bromomethane LinF 0.37510.3708 24.8 20.0 24.0 50.0

Chloroethane LinF 0.28350.3287 21.5 20.0 7.5 50.0

Trichlorofluoromethane LinF 0.65520.6883 22.8 20.0 14.1 50.0

n-Pentane Ave 0.07170.0684 20.9 20.0 4.7 50.0

Ethanol Ave 0.00180.0021 2500 3000 -16.6 50.0

Ethyl ether Ave 0.23550.2631 17.9 20.0 -10.5 50.0

Isopropene Ave 0.52120.5485 19.0 20.0 -5.0 50.0

Acrolein Ave 0.02350.0375 188 300 -37.4 99.0

1,1-Dichloroethene Ave 0.33320.3379 19.7 20.0 -1.4 20.0

Freon TF Ave 0.40410.3893 20.8 20.0 3.8 50.0

Acetone LinF 0.07800.1278 22.0 20.0 9.8 50.0

Iodomethane Ave 0.42010.3999 21.0 20.0 5.1 50.0

Carbon disulfide Ave 1.0841.060 20.5 20.0 2.3 50.0

Isopropanol QuaF 0.01920.0264 2030 3000 -32.5 50.0

Acetonitrile LinF 0.03930.0558 404 400 0.9 50.0

Methyl acetate LinF 0.06270.0972 17.4 20.0 -13.1 50.0

Methylene Chloride LinF 0.37850.4375 22.9 20.0 14.3 50.0

TBA Ave 0.02740.0357 307 400 -23.3 50.0

Acrylonitrile Ave 0.11640.1368 128 150 -14.9 50.0

trans-1,2-Dichloroethene Ave 0.37090.3911 19.0 20.0 -5.2 50.0

MTBE Ave 0.66530.7763 17.1 20.0 -14.3 50.0

Hexane Ave 0.23940.2770 17.3 20.0 -13.6 50.0

1,1-Dichloroethane Ave 0.61940.6674 0.1000 18.6 20.0 -7.2 50.0

Vinyl acetate Ave 0.58000.7474 15.5 20.0 -22.4 50.0

DIPE Ave 0.80570.9303 17.3 20.0 -13.4 50.0

Tert-butyl ethyl ether Ave 0.66770.8122 0.0100 16.4 20.0 -17.8 50.0

2,2-Dichloropropane Ave 0.46630.4576 20.4 20.0 1.9 50.0

cis-1,2-Dichloroethene Ave 0.37420.3871 19.3 20.0 -3.4 50.0

2-Butanone (MEK) Ave 0.03720.0379 19.6 20.0 -1.7 50.0

Ethyl acetate Ave 0.02090.0284 29.5 40.0 -26.3 50.0

Bromochloromethane Ave 0.15780.1570 20.1 20.0 0.5 50.0

Chloroform Ave 0.59640.6094 19.6 20.0 -2.1 20.0

1,1,1-Trichloroethane Ave 0.48570.4980 19.5 20.0 -2.5 50.0

Cyclohexane Ave 0.62250.6765 18.4 20.0 -8.0 50.0

1,1-Dichloropropene Ave 0.42070.4625 18.2 20.0 -9.0 50.0

Carbon tetrachloride Ave 0.41010.4038 20.3 20.0 1.6 50.0

Benzene Ave 1.2271.353 18.1 20.0 -9.3 50.0

1,2-Dichloroethane Ave 0.38750.4112 18.9 20.0 -5.7 50.0

FORM VII 8260B

06/03/2010 of 623

FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:



0.18(mm)

460-13139-1

VOAMS12

05/17/2010 17:02

04/15/2010 14:24

04/15/2010 16:52

CCVIS 460-37643/2

DB-624

TestAmerica Edison




Isopropyl acetate Ave 0.40850.5249 31.1 40.0 -22.2 50.0

Tert-amyl methyl ether Ave 0.53480.7263 14.7 20.0 -26.4 50.0

2,4,4-Trimethyl-1-pentene LinF 0.11040.1313 19.0 20.0 -4.8 50.0

n-Butanol Ave 0.00340.0053 950 1500 -36.7 50.0

Trichloroethene Ave 0.29620.3446 17.2 20.0 -14.0 50.0

Ethyl acrylate Ave 0.24840.3178 15.6 20.0 -21.9 50.0

Methylcyclohexane Ave 0.51820.6580 15.8 20.0 -21.2 50.0

1,2-Dichloropropane Ave 0.29020.3373 17.2 20.0 -14.0 20.0

Dibromomethane Ave 0.17910.1822 19.7 20.0 -1.7 50.0

1,4-Dioxane Ave 0.00360.0046 2360 3000 -21.3 50.0

Methyl methacrylate LinF 0.12180.1787 13.5 20.0 -32.3 50.0

Propyl acetate LinF 0.27590.4078 30.6 40.0 -23.4 50.0

Bromodichloromethane Ave 0.37080.3841 19.3 20.0 -3.5 50.0

2-Chloroethyl vinyl ether Ave 0.12090.1566 15.4 20.0 -22.8 50.0

Epichlorohydrin Ave 0.02650.0314 337 400 -15.7 50.0

cis-1,3-Dichloropropene Ave 0.39650.4504 17.6 20.0 -12.0 50.0

4-Methyl-2-pentanone Ave 0.18510.2460 15.0 20.0 -24.8 50.0

Toluene Ave 1.7372.090 16.6 20.0 -16.9 20.0

trans-1,3-Dichloropropene LinF 0.42640.5238 12.9 20.0 -35.3 50.0

1,1,2-Trichloroethane LinF 0.24440.2894 15.3 20.0 -23.4 50.0

Tetrachloroethene Ave 0.36340.4622 15.7 20.0 -21.4 50.0

1,3-Dichloropropane LinF 0.53000.6183 15.6 20.0 -21.8 50.0

2-Hexanone Ave 0.21450.2630 16.3 20.0 -18.5 50.0

Dibromochloromethane LinF 0.29310.3356 14.3 20.0 -28.4 50.0

Butyl acetate Ave 0.49720.5690 35.0 40.0 -12.6 50.0

1,2-Dibromoethane LinF 0.29370.3312 16.3 20.0 -18.7 50.0

Chlorobenzene Ave 1.1681.260 0.3000 18.5 20.0 -7.4 50.0

1,1,1,2-Tetrachloroethane LinF 0.28210.3507 12.9 20.0 -35.3 50.0

Ethylbenzene Ave 0.72790.7447 19.6 20.0 -2.2 20.0

m&p-Xylene Ave 0.87690.9092 38.6 40.0 -3.5 50.0

o-Xylene Ave 0.81620.8345 19.6 20.0 -2.2 50.0

Styrene Ave 1.4011.443 19.4 20.0 -2.9 50.0

Butyl acrylate Ave 1.2691.466 17.3 20.0 -13.4 50.0

Bromoform LinF 0.16450.1904 0.1000 13.4 20.0 -33.2 50.0

Amly acetate Ave 0.55200.3591 30.7 20.0 53.7* 50.0

Isopropylbenzene Ave 2.2832.343 19.5 20.0 -2.6 50.0

Camphene, Total Ave 1.9722.059 19.2 20.0 -4.2 50.0

Monobromobenzene Ave 0.94120.9478 19.9 20.0 -0.7 50.0

1,1,2,2-Tetrachloroethane Ave 0.72320.8684 0.3000 16.7 20.0 -16.7 50.0

1,2,3-Trichloropropane Ave 0.20330.2484 16.4 20.0 -18.2 50.0

trans-1,4-Dichloro-2-butene LinF 0.07820.0995 16.2 20.0 -18.9 50.0

FORM VII 8260B

06/03/2010 of 623

FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:



0.18(mm)

460-13139-1

VOAMS12

05/17/2010 17:02

04/15/2010 14:24

04/15/2010 16:52

CCVIS 460-37643/2

DB-624

TestAmerica Edison




N-Propylbenzene Ave 5.4005.496 19.7 20.0 -1.7 50.0

2-Chlorotoluene Ave 2.9613.103 19.1 20.0 -4.6 50.0

4-Chlorotoluene Ave 3.3363.427 19.5 20.0 -2.7 50.0

1,3,5-Trimethylbenzene Ave 3.2513.592 18.1 20.0 -9.5 50.0

Butyl Methacrylate Ave 1.1141.286 17.3 20.0 -13.4 50.0

tert-Butylbenzene Ave 3.1293.273 19.1 20.0 -4.4 50.0

1,2,4-Trimethylbenzene Ave 3.3353.633 18.4 20.0 -8.2 50.0

2-Octanone Ave 0.87981.113 15.8 20.0 -21.0 50.0

sec-Butylbenzene Ave 4.9924.999 20.0 20.0 -0.1 50.0

1,3-Dichlorobenzene Ave 1.8752.004 18.7 20.0 -6.5 50.0

2-Octanol Ave 0.15030.2503 12.0 20.0 -40.0 50.0


p-Isopropyltoluene Ave 3.9804.090 19.5 20.0 -2.7 50.0

Benzyl chloride LinF 1.3721.434 15.2 20.0 -24.1 50.0


n-Butylbenzene Ave 4.0244.110 19.6 20.0 -2.1 50.0

1,2-Dibromo-3-Chloropropane Ave 0.14400.1872 15.4 20.0 -23.1 50.0

Camphor Ave 0.08880.1199 74.0 100 -26.0 50.0

1,2,4-Trichlorobenzene Ave 1.4201.414 20.1 20.0 0.5 50.0

Hexachlorobutadiene Ave 0.80380.8278 19.4 20.0 -2.9 50.0

Naphthalene Ave 3.1203.287 19.0 20.0 -5.1 50.0

1,2,3-Trichlorobenzene Ave 1.2891.331 19.4 20.0 -3.1 50.0

1,2-Dichloroethane-d4 (Surr) Ave 0.21560.2246 48.0 50.0 -4.0 50.0

Toluene-d8 (Surr) Ave 0.94631.068 44.3 50.0 -11.4 50.0

Bromofluorobenzene Ave 0.69300.6371 54.4 50.0 8.8 50.0

FORM VII 8260B

06/03/2010 of 623

Data File: /chem/VOAMS12.i/8260L_10/04-15-10/15apr10.b/o36289.d Report Date: 15-Apr-2010 13:20

TestAmerica

Data file : /chem/VOAMS12.i/8260L_10/04-15-10/15apr10.b/o36289.dLab Smp Id: BFB-VMBFB Inj Date : 15-APR-2010 13:12 Operator : VOAMS 1 Inst ID: VOAMS12.iSmp Info : BFB-VMBFBMisc Info : Comment : Method : /chem/VOAMS12.i/8260L_10/04-15-10/15apr10.b/VOABFB.mMeth Date : 24-Feb-2010 18:04 ken Quant Type: ISTDCal Date : Cal File: Als bottle: 2 QC Sample: BFBDil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Sample Matrix: WATERProcessing Host: hpd2

Concentration Formula: Amt * DF * Uf * Vf * VI * CpndVariable


DF 1.00000 Dilution FactorUf 1.00000 ng unit correction factorVf 1.00000 Volumetric correction factorVI 1.00000 Injection Volume


CONCENTRATIONS

ON-COL FINAL

RT EXP RT (REL RT) MASS RESPONSE ( ug/L) ( ug/L) TARGET RANGE RATIO

== ====== ======== ==== ======== ======= ======= ============ =====

1 BFB CAS #: 460-00-4

2.700 2.700 (0.000) 95 84592 0.00- 100.00 100.00

2.700 2.700 (0.000) 50 13379 15.00- 40.00 15.82

2.700 2.700 (0.000) 75 40224 30.00- 60.00 47.55

2.700 2.700 (0.000) 96 5536 5.00- 9.00 6.54

2.700 2.700 (0.000) 173 0 0.00- 2.00 0.00

2.700 2.700 (0.000) 174 62952 50.00- 100.00 74.42

2.700 2.700 (0.000) 175 5162 5.00- 9.00 8.20

2.700 2.700 (0.000) 176 62464 95.00- 101.00 99.22

2.700 2.700 (0.000) 177 4244 5.00- 9.00 6.79

-------------------------------------------------------------------------------

06/03/2010 of 623

Data File: o36289.d

Date: 15-APR-2010 13:12

Client ID: Instrument: VOAMS12.i

Sample Info: BFB-VMBFB Operator: VOAMS 1

06/03/2010 of 623

Data File: o36289.d

Date: 15-APR-2010 13:12



1 BFB

% RELATIVE m/e ION ABUNDANCE CRITERIA ABUNDANCE

+-----+------------------------------------------+---------------------+| | | || 95 | Base Peak, 100% relative abundance | 100.00 || 50 | 15.00 - 40.00% of mass 95 | 15.82 || 75 | 30.00 - 60.00% of mass 95 | 47.55 || 96 | 5.00 - 9.00% of mass 95 | 6.54 || 173 | Less than 2.00% of mass 174 | 0.00 ( 0.00) || 174 | 50.00 - 100.00% of mass 95 | 74.42 || 175 | 5.00 - 9.00% of mass 174 | 6.10 ( 8.20) || 176 | 95.00 - 101.00% of mass 174 | 73.84 ( 99.22) || 177 | 5.00 - 9.00% of mass 176 | 5.02 ( 6.79) |+-----+------------------------------------------+---------------------+

06/03/2010 of 623

Data File: o36289.d

Date: 15-APR-2010 13:12



Data File: /chem/VOAMS12.i/8260L_10/04-15-10/15apr10.b/o36289.dSpectrum: Avg. Scans 101-103 ( 2.70), Background Scan 95

Location of Maximum: 95.00Number of points: 114

m/z Y m/z Y m/z Y m/z Y+------------------+------------------+------------------+------------------+| 36.00 736 | 70.00 557 | 109.00 124 | 149.00 118 || 37.00 3445 | 72.00 728 | 110.00 73 | 150.00 155 || 38.00 3000 | 73.00 3066 | 111.00 134 | 152.00 43 || 39.00 1397 | 74.00 12308 | 113.00 44 | 155.00 118 || 40.00 53 | 75.00 40224 | 114.00 36 | 157.00 118 |+------------------+------------------+------------------+------------------+| 41.00 36 | 76.00 3465 | 115.00 125 | 158.00 66 || 43.00 179 | 77.00 698 | 116.00 187 | 159.00 44 || 44.00 345 | 78.00 448 | 117.00 502 | 171.00 60 || 45.00 613 | 79.00 1486 | 118.00 350 | 172.00 305 || 47.00 1041 | 80.00 447 | 119.00 377 | 174.00 62952 |+------------------+------------------+------------------+------------------+| 48.00 406 | 81.00 1625 | 121.00 61 | 175.00 5162 || 49.00 3190 | 82.00 448 | 123.00 34 | 176.00 62464 || 50.00 13379 | 83.00 37 | 125.00 52 | 177.00 4244 || 51.00 4498 | 85.00 37 | 126.00 84 | 178.00 172 || 52.00 299 | 86.00 118 | 128.00 254 | 182.00 82 |+------------------+------------------+------------------+------------------+| 53.00 37 | 87.00 3555 | 129.00 219 | 186.00 44 || 55.00 348 | 88.00 2888 | 130.00 265 | 191.00 46 || 56.00 1150 | 89.00 64 | 131.00 37 | 192.00 49 || 57.00 1781 | 91.00 187 | 134.00 156 | 193.00 62 || 58.00 33 | 92.00 2154 | 136.00 37 | 207.00 46 |+------------------+------------------+------------------+------------------+| 59.00 97 | 93.00 3190 | 137.00 40 | 208.00 41 || 60.00 516 | 94.00 8659 | 141.00 570 | 232.00 43 || 61.00 3467 | 95.00 84592 | 142.00 49 | 241.00 42 || 62.00 3370 | 96.00 5536 | 143.00 628 | 253.00 82 || 63.00 2925 | 97.00 214 | 144.00 38 | 258.00 40 |+------------------+------------------+------------------+------------------+| 64.00 357 | 104.00 199 | 145.00 58 | 280.00 34 || 67.00 458 | 105.00 172 | 146.00 47 | 281.00 90 || 68.00 7550 | 106.00 219 | 147.00 106 | || 69.00 8092 | 107.00 56 | 148.00 108 | |+------------------+------------------+------------------+------------------+

06/03/2010 of 623


TestAmerica

Data file : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37384.dLab Smp Id: BFB-VMBFB Inj Date : 17-MAY-2010 16:42 Operator : VOAMS 1 Inst ID: VOAMS12.iSmp Info : BFB-VMBFBMisc Info : Comment : Method : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/VOABFB.mMeth Date : 24-Feb-2010 18:04 ken Quant Type: ISTDCal Date : Cal File: Als bottle: 2 QC Sample: BFBDil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Sample Matrix: WATERProcessing Host: hpd2

Concentration Formula: Amt * DF * Uf * Vf * VI * CpndVariable


DF 1.00000 Dilution FactorUf 1.00000 ng unit correction factorVf 1.00000 Volumetric correction factorVI 1.00000 Injection Volume


CONCENTRATIONS

ON-COL FINAL

RT EXP RT (REL RT) MASS RESPONSE ( ug/L) ( ug/L) TARGET RANGE RATIO

== ====== ======== ==== ======== ======= ======= ============ =====

1 BFB CAS #: 460-00-4

2.688 2.700 (0.000) 95 177984 0.00- 100.00 100.00

2.688 2.700 (0.000) 50 28472 15.00- 40.00 16.00

2.688 2.700 (0.000) 75 87240 30.00- 60.00 49.02

2.688 2.700 (0.000) 96 11563 5.00- 9.00 6.50

2.688 2.700 (0.000) 173 1134 0.00- 2.00 0.93

2.688 2.700 (0.000) 174 122192 50.00- 100.00 68.65

2.688 2.700 (0.000) 175 9308 5.00- 9.00 7.62

2.688 2.700 (0.000) 176 117512 95.00- 101.00 96.17

2.688 2.700 (0.000) 177 6472 5.00- 9.00 5.51

-------------------------------------------------------------------------------

06/03/2010 of 623

Data File: o37384.d

Date: 17-MAY-2010 16:42



06/03/2010 of 623

Data File: o37384.d

Date: 17-MAY-2010 16:42



1 BFB


+-----+------------------------------------------+---------------------+| | | || 95 | Base Peak, 100% relative abundance | 100.00 || 50 | 15.00 - 40.00% of mass 95 | 16.00 || 75 | 30.00 - 60.00% of mass 95 | 49.02 || 96 | 5.00 - 9.00% of mass 95 | 6.50 || 173 | Less than 2.00% of mass 174 | 0.64 ( 0.93) || 174 | 50.00 - 100.00% of mass 95 | 68.65 || 175 | 5.00 - 9.00% of mass 174 | 5.23 ( 7.62) || 176 | 95.00 - 101.00% of mass 174 | 66.02 ( 96.17) || 177 | 5.00 - 9.00% of mass 176 | 3.64 ( 5.51) |+-----+------------------------------------------+---------------------+

06/03/2010 of 623

Data File: o37384.d

Date: 17-MAY-2010 16:42



Data File: /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37384.dSpectrum: HP MS o37384.d, Scan 100: 2.688 min.


m/z Y m/z Y m/z Y m/z Y+------------------+------------------+------------------+------------------+| 36.10 1183 | 71.90 685 | 111.70 258 | 155.80 121 || 37.00 6748 | 73.00 6936 | 112.60 142 | 156.90 521 || 37.90 5948 | 74.00 28936 | 114.60 174 | 159.40 260 || 39.00 2292 | 75.00 87240 | 115.10 126 | 160.90 349 || 39.80 286 | 76.00 7153 | 115.80 549 | 169.40 287 |+------------------+------------------+------------------+------------------+| 43.30 431 | 76.70 1061 | 116.80 1311 | 170.10 246 || 44.10 953 | 77.10 900 | 117.80 598 | 170.50 285 || 44.70 669 | 77.90 381 | 118.90 869 | 171.00 200 || 45.10 872 | 78.80 4831 | 119.70 169 | 171.70 408 || 46.20 198 | 80.00 1427 | 124.60 402 | 172.70 1134 |+------------------+------------------+------------------+------------------+| 47.00 1409 | 80.80 4094 | 126.00 146 | 173.90 122192 || 48.00 788 | 81.90 840 | 127.20 179 | 174.90 9308 || 49.00 6150 | 82.90 272 | 128.10 610 | 175.90 117512 || 50.00 28472 | 86.10 317 | 128.80 106 | 177.00 6472 || 51.00 10415 | 87.00 8860 | 129.90 793 | 178.00 563 |+------------------+------------------+------------------+------------------+| 52.00 280 | 88.00 8092 | 130.80 544 | 204.30 177 || 55.00 706 | 89.00 105 | 133.70 173 | 207.10 109 || 55.90 2362 | 90.40 629 | 134.70 215 | 209.00 159 || 57.00 4501 | 90.90 624 | 135.80 155 | 218.20 120 || 57.70 138 | 91.90 5401 | 139.20 239 | 230.70 160 |+------------------+------------------+------------------+------------------+| 58.20 122 | 93.00 7018 | 139.70 234 | 231.90 103 || 58.90 145 | 94.00 19008 | 140.80 1482 | 252.40 167 || 60.00 1563 | 95.00 177984 | 141.80 211 | 266.10 139 || 60.90 7246 | 96.00 11563 | 142.70 1970 | 267.20 136 || 62.00 7224 | 96.80 601 | 144.00 196 | 270.80 110 |+------------------+------------------+------------------+------------------+| 63.00 6053 | 100.10 128 | 145.00 317 | 274.80 155 || 64.00 607 | 102.90 280 | 145.70 253 | 277.70 129 || 64.70 223 | 103.80 966 | 146.80 125 | 280.80 168 || 66.50 320 | 105.20 140 | 147.80 624 | 281.20 104 || 68.00 15623 | 105.80 521 | 148.40 236 | 282.30 102 |+------------------+------------------+------------------+------------------+| 69.00 13446 | 106.40 140 | 149.10 210 | 294.80 175 || 70.00 2010 | 106.80 249 | 152.50 113 | 299.60 134 || 70.70 183 | 109.80 104 | 153.70 217 | || 71.10 156 | 111.00 148 | 154.80 610 | |+------------------+------------------+------------------+------------------+

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1

Lab Sample ID: MB 460-37643/5



Solid

TestAmerica Edison

Sample wt/vol:

% Moisture:


Dilution Factor:Soil Aliquot Vol: 1


5(mL)

0.18(mm)

Date Analyzed: 05/17/2010 20:11

ID:DB-624




Bromomethane74-83-9 1.0 1.0 0.41U


Chloroethane75-00-3 1.0 1.0 0.40U







Chloroform67-66-3 1.0 1.0 0.24U










Benzene71-43-2 1.0 1.0 0.74U



Bromoform75-25-2 1.0 1.0 0.70U



Toluene108-88-3 1.0 1.0 0.30U


Ethylbenzene100-41-4 1.0 1.0 0.19U

Xylenes, Total1330-20-7 3.0 3.0 0.79U

FORM I 8260B

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1




Solid

TestAmerica Edison

Sample wt/vol:

% Moisture:




5(mL)

0.18(mm)

Date Analyzed: 05/17/2010 20:11

ID:DB-624




2037-26-5 Toluene-d8 (Surr) 92 66-126


FORM I 8260B

06/03/2010 of 623



Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1




Solid

TestAmerica Edison

Sample wt/vol:

% Moisture:




5(mL)

0.18(mm)

Date Analyzed: 05/17/2010 20:11

ID:DB-624





FORM I-TIC 8260B

06/03/2010 of 623


TestAmerica

VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37390.dLab Smp Id: MB Inj Date : 17-MAY-2010 20:11 Operator : VOAMS 9 Inst ID: VOAMS12.iSmp Info : MBMisc Info : Comment : Method : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/8260L_10.mMeth Date : 17-May-2010 18:29 ken Quant Type: ISTDCal Date : 15-APR-2010 16:52 Cal File: o36298.dAls bottle: 6 QC Sample: BLANKDil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd2





CONCENTRATIONS



========================== ==== == ====== ====== ======== ======= =======


* 69 Fluorobenzene 96 4.262 4.262 (1.000) 1237424 50.0000

$ 37 Toluene-d8 (SUR) 98 6.073 6.073 (0.754) 1133872 45.9973 46

* 32 Chlorobenzene-d5 117 8.054 8.054 (1.000) 1154369 50.0000



06/03/2010 of 623


TestAmerica

VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37390.dLab Smp Id: MB Inj Date : 17-MAY-2010 20:11 Operator : VOAMS 9 Inst ID: VOAMS12.iSmp Info : MBMisc Info : Comment : Method : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/8260L_10.mMeth Date : 17-May-2010 18:29 ken Quant Type: ISTDCal Date : 15-APR-2010 16:52 Cal File: o36298.dAls bottle: 6 QC Sample: BLANKDil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd2


06/03/2010 of 623

Data File: o37390.d

Date: 17-MAY-2010 20:11


Sample Info: MB Operator: VOAMS 9

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1

Lab Sample ID: LCS 460-37643/3



Solid

TestAmerica Edison

Sample wt/vol:

% Moisture:




5(mL)

0.18(mm)

Date Analyzed: 05/17/2010 17:46

ID:DB-624



Chloromethane74-87-3 19.2 1.0 0.63

Bromomethane74-83-9 22.0 1.0 0.41

Vinyl chloride75-01-4 19.5 1.0 0.23

Chloroethane75-00-3 19.9 1.0 0.40

Methylene Chloride75-09-2 23.9 1.0 0.47

Trichlorofluoromethane75-69-4 21.5 1.0 0.26

1,1-Dichloroethene75-35-4 20.8 1.0 0.37

1,1-Dichloroethane75-34-3 19.8 1.0 0.25

trans-1,2-Dichloroethene156-60-5 19.8 1.0 0.28

cis-1,2-Dichloroethene156-59-2 20.0 1.0 0.24

Chloroform67-66-3 19.9 1.0 0.24

1,2-Dichloroethane107-06-2 19.6 1.0 0.39

1,1,1-Trichloroethane71-55-6 20.5 1.0 0.19

Carbon tetrachloride56-23-5 21.5 1.0 0.10

Bromodichloromethane75-27-4 20.1 1.0 0.30

1,2-Dichloropropane78-87-5 19.5 1.0 0.32

cis-1,3-Dichloropropene10061-01-5 18.7 1.0 0.20

Trichloroethene79-01-6 19.8 1.0 0.36

Dibromochloromethane124-48-1 16.7 1.0 0.56


Benzene71-43-2 19.7 1.0 0.74

trans-1,3-Dichloropropene10061-02-6 15.2 1.0 0.22

2-Chloroethyl vinyl ether110-75-8 16.5 5.0 1.3

Bromoform75-25-2 14.7 1.0 0.70

Tetrachloroethene127-18-4 18.6 1.0 0.33

1,1,2,2-Tetrachloroethane79-34-5 18.9 1.0 0.76

Toluene108-88-3 19.2 1.0 0.30

Chlorobenzene108-90-7 20.0 1.0 0.48

Ethylbenzene100-41-4 21.1 1.0 0.19

Xylenes, Total1330-20-7 61.9 3.0 0.79

FORM I 8260B

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1

Lab Sample ID: LCS 460-37643/3



Solid

TestAmerica Edison

Sample wt/vol:

% Moisture:




5(mL)

0.18(mm)

Date Analyzed: 05/17/2010 17:46

ID:DB-624




2037-26-5 Toluene-d8 (Surr) 90 66-126


FORM I 8260B

06/03/2010 of 623


TestAmerica

VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37386.dLab Smp Id: LCS Inj Date : 17-MAY-2010 17:46 Operator : VOAMS 9 Inst ID: VOAMS12.iSmp Info : LCSMisc Info : Comment : Method : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/8260L_10.mMeth Date : 17-May-2010 18:29 ken Quant Type: ISTDCal Date : 15-APR-2010 16:52 Cal File: o36298.dAls bottle: 2 QC Sample: BSDil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd2





CONCENTRATIONS



========================== ==== == ====== ====== ======== ======= =======

M 14 1,2-Dichloroethene (total) 100 495021 39.8435 40

90 Dichlorodifluoromethane 85 1.012 1.013 (0.238) 241035 22.5387 22

1 Chloromethane 50 1.141 1.147 (0.268) 276534 19.1871 19

4 Vinyl Chloride 62 1.183 1.183 (0.278) 278276 19.4693 19

3 Bromomethane 94 1.372 1.372 (0.322) 212412 22.0007 22

5 Chloroethane 64 1.451 1.445 (0.341) 167312 19.8808 20

9 Trichlorofluoromethane 101 1.573 1.574 (0.369) 393716 21.4673 21

121 n-Pentane 72 1.616 1.616 (0.379) 42637 19.5222 20

127 Ethanol 46 1.707 1.708 (0.401) 161075 2378.15 2400

46 Ethyl Ether 59 1.756 1.756 (0.412) 144204 17.1687 17

119 Isoprene 67 1.762 1.762 (0.414) 324026 18.5014 18

47 Acrolein 56 1.835 1.836 (0.431) 191273 159.847 160

10 1,1-Dichloroethene 96 1.896 1.897 (0.445) 224018 20.7623 21

48 Freon TF 101 1.896 1.897 (0.445) 238620 19.1956 19

06/03/2010 of 623


CONCENTRATIONS



========================== ==== == ====== ====== ======== ======= =======

7 Acetone 43 1.939 1.939 (0.455) 53210 23.4599 23

142 Iodomethane 142 2.000 2.000 (0.469) 254463 19.9308 20

8 Carbon Disulfide 76 2.037 2.037 (0.478) 641152 18.9482 19

50 Acetonitrile 41 2.128 2.128 (0.499) 507349 408.034 410

125 Methyl acetate 74 2.153 2.159 (0.505) 42999 18.6780 19

6 Methylene Chloride 84 2.226 2.226 (0.522) 252844 23.9265 24

51 TBA 59 2.323 2.323 (0.545) 318591 279.598 280

52 Acrylonitrile 53 2.402 2.403 (0.564) 500440 114.570 110

12 trans-1,2-Dichloroethene 96 2.415 2.415 (0.567) 247497 19.8181 20

53 MTBE 73 2.421 2.421 (0.568) 434306 17.5230 18

49 Isopropanol 45 2.043 2.043 (0.479) 1993860 2235.11 2200(A)

54 Hexane 56 2.616 2.616 (0.614) 152512 17.2476 17

11 1,1-Dichloroethane 63 2.726 2.726 (0.640) 422554 19.8302 20

57 Vinyl Acetate 43 2.787 2.787 (0.654) 369414 15.4800 15

55 DIPE 45 2.793 2.793 (0.655) 512977 17.2699 17

149 tert-Butyl ethyl ether 59 3.085 3.085 (0.724) 420393 16.2122 16

104 2,2-Dichloropropane 77 3.189 3.189 (0.748) 311135 21.2972 21

13 cis-1,2-Dichloroethene 96 3.195 3.195 (0.750) 247523 20.0254 20

18 2-Butanone 72 3.225 3.213 (0.757) 20665 17.1005 17

56 Ethyl Acetate 70 3.280 3.274 (0.770) 26897 29.6978 30

108 Bromochloromethane 128 3.402 3.402 (0.798) 104478 20.8377 21

15 Chloroform 83 3.475 3.476 (0.815) 386341 19.8565 20

20 1,1,1-Trichloroethane 97 3.634 3.634 (0.853) 326415 20.5297 20

59 Cyclohexane 56 3.683 3.677 (0.864) 386708 17.9041 18

21 Carbon Tetrachloride 117 3.786 3.787 (0.888) 277101 21.4941 21

92 1,1-Dichloropropene 75 3.786 3.787 (0.888) 289303 19.5922 20


28 Benzene 78 3.981 3.982 (0.934) 852061 19.7194 20

17 1,2-Dichloroethane 62 4.000 4.000 (0.938) 257436 19.6110 20

61 Isopropyl Acetate 43 4.091 4.091 (0.960) 542308 32.3590 32

140 tert-Amylmethyl Ether 73 4.109 4.116 (0.964) 342824 14.7832 15(R)

* 69 Fluorobenzene 96 4.262 4.262 (1.000) 1596386 50.0000

156 2,4,4-Trimethyl-1-pentene 112 4.603 4.603 (1.080) 66928 18.0764 18

25 Trichloroethene 95 4.640 4.640 (1.089) 217624 19.7816 20

63 n-Butanol 43 4.634 4.634 (1.087) 192947 1132.63 1100

96 Ethyl Acrylate 55 4.798 4.798 (1.126) 165126 16.2730 16

126 Methyl cyclohexane 83 4.841 4.847 (1.136) 355777 16.9350 17


109 Dibromomethane 93 5.012 5.012 (1.176) 111801 19.2186 19

95 1,4-Dioxane 88 5.067 5.061 (1.189) 385825 2612.67 2600

146 Methyl methacrylate 69 5.060 5.061 (1.187) 86806 15.1057 15(R)

64 Propyl Acetate 43 5.140 5.140 (1.206) 364108 31.6625 32

22 Bromodichloromethane 83 5.207 5.207 (1.222) 246277 20.0800 20

30 2-Chloroethyl Vinyl Ether 63 5.597 5.597 (1.313) 82665 16.5291 16

118 Epichlorohydrin 57 5.652 5.652 (1.326) 318383 317.201 320

24 cis-1,3-Dichloropropene 75 5.749 5.750 (1.349) 269574 18.7467 19

33 4-Methyl-2-Pentanone 43 5.969 5.969 (1.401) 112446 14.3186 14

06/03/2010 of 623


CONCENTRATIONS



========================== ==== == ====== ====== ======== ======= =======

$ 37 Toluene-d8 (SUR) 98 6.072 6.073 (0.754) 1047591 44.8363 45

38 Toluene 91 6.158 6.158 (0.765) 879315 19.2234 19

29 trans-1,3-Dichloropropene 75 6.475 6.475 (0.804) 219864 15.2470 15


35 Tetrachloroethene 166 6.871 6.871 (0.853) 188075 18.5970 18


34 2-Hexanone 43 7.103 7.103 (0.882) 89741 15.5918 16

26 Dibromochloromethane 129 7.231 7.231 (0.898) 149446 16.6837 17

65 Butyl Acetate 43 7.322 7.322 (0.909) 414275 33.2711 33

66 1,2-Dibromoethane 107 7.359 7.359 (0.914) 145193 18.3664 18

* 32 Chlorobenzene-d5 117 8.054 8.054 (1.000) 1094145 50.0000

39 Chlorobenzene 112 8.096 8.097 (1.005) 550809 19.9701 20

97 1,1,1,2-Tetrachloroethane 131 8.243 8.243 (1.023) 149108 15.6317 16

40 Ethylbenzene 106 8.298 8.298 (1.030) 343579 21.0836 21

43 m+p-Xylene 106 8.487 8.487 (1.054) 817376 41.0826 41

44 o-Xylene 106 9.084 9.090 (1.128) 379766 20.7963 21

42 Styrene 104 9.115 9.115 (1.132) 652197 20.6530 21

147 Butyl Acrylate 55 9.157 9.157 (0.781) 287824 16.9922 17

31 Bromoform 173 9.358 9.359 (1.162) 79223 14.6906 15

145 Amyl Acetate 43 9.553 9.554 (1.186) 240392 30.5914 30

110 Isopropylbenzene 105 9.700 9.700 (1.204) 1062867 20.7267 21


150 Camphene 93 10.066 10.060 (0.858) 438409 18.4295 18

107 Bromobenzene 156 10.114 10.115 (0.862) 235634 21.5195 22


99 1,2,3-Trichloropropane 110 10.255 10.255 (0.874) 53405 18.6088 19

143 trans-1,4-Dichloro-2-butene 53 10.322 10.322 (2.422) 48569 15.7752 16

112 n-Propylbenzene 91 10.377 10.377 (0.885) 1329321 20.9373 21

105 2-Chlorotoluene 91 10.462 10.462 (0.892) 739182 20.6196 21

106 4-Chlorotoluene 91 10.651 10.651 (0.908) 846941 21.3889 21

102 1,3,5-Trimethylbenzene 105 10.700 10.694 (0.912) 826159 19.9063 20

148 Butyl methacrylate 69 10.974 10.968 (0.936) 247235 16.6447 17

115 tert-Butylbenzene 119 11.218 11.212 (0.956) 793519 20.9826 21


151 2-Octanone 43 11.535 11.529 (0.983) 248258 19.3078 19

114 sec-Butylbenzene 105 11.541 11.541 (0.984) 1265453 21.9128 22

67 1,3-Dichlorobenzene 146 11.632 11.633 (0.992) 478397 20.6585 21

153 2-Octanol 45 11.681 11.675 (0.996) 37750 13.0531 13(R)



113 p-Isopropyltoluene 119 11.766 11.767 (1.003) 1014389 21.4689 21


117 Benzyl chloride 91 11.962 11.962 (1.020) 298675 14.2946 14

111 n-Butylbenzene 91 12.272 12.267 (1.046) 1041415 21.9345 22

101 1,2-Dibromo-3-chloropropane 75 13.065 13.059 (1.114) 35475 16.4046 16

152 Camphor 95 13.730 13.736 (1.170) 111841 80.7128 81

93 1,2,4-Trichlorobenzene 180 13.821 13.821 (1.178) 346356 21.2077 21

06/03/2010 of 623


CONCENTRATIONS



========================== ==== == ====== ====== ======== ======= =======

94 Hexachlorobutadiene 225 13.986 13.986 (1.192) 199223 20.8319 21

70 Naphthalene 128 14.022 14.016 (1.195) 812454 21.3940 21


M 45 Xylene (Total) 100 1197143 61.8789 62

QC Flag Legend

A - Target compound detected but, quantitated amountexceeded maximum amount.

R - Spike/Surrogate failed recovery limits.

06/03/2010 of 623

Data File: o37386.d

Date: 17-MAY-2010 17:46


Sample Info: LCS Operator: VOAMS 9

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1

Lab Sample ID: LCSD 460-37643/4



Solid

TestAmerica Edison

Sample wt/vol:

% Moisture:




5(mL)

0.18(mm)

Date Analyzed: 05/17/2010 18:10

ID:DB-624



Chloromethane74-87-3 19.2 1.0 0.63

Bromomethane74-83-9 22.3 1.0 0.41

Vinyl chloride75-01-4 19.5 1.0 0.23

Chloroethane75-00-3 19.9 1.0 0.40

Methylene Chloride75-09-2 26.8 1.0 0.47

Trichlorofluoromethane75-69-4 21.1 1.0 0.26

1,1-Dichloroethene75-35-4 23.1 1.0 0.37

1,1-Dichloroethane75-34-3 21.5 1.0 0.25

trans-1,2-Dichloroethene156-60-5 21.6 1.0 0.28

cis-1,2-Dichloroethene156-59-2 22.1 1.0 0.24

Chloroform67-66-3 21.8 1.0 0.24

1,2-Dichloroethane107-06-2 21.5 1.0 0.39


Carbon tetrachloride56-23-5 23.3 1.0 0.10

Bromodichloromethane75-27-4 23.1 1.0 0.30

1,2-Dichloropropane78-87-5 21.1 1.0 0.32

cis-1,3-Dichloropropene10061-01-5 21.8 1.0 0.20

Trichloroethene79-01-6 21.2 1.0 0.36

Dibromochloromethane124-48-1 18.3 1.0 0.56


Benzene71-43-2 21.9 1.0 0.74

trans-1,3-Dichloropropene10061-02-6 17.5 1.0 0.22

2-Chloroethyl vinyl ether110-75-8 17.4 5.0 1.3

Bromoform75-25-2 16.8 1.0 0.70

Tetrachloroethene127-18-4 22.3 1.0 0.33

1,1,2,2-Tetrachloroethane79-34-5 20.3 1.0 0.76

Toluene108-88-3 21.7 1.0 0.30

Chlorobenzene108-90-7 21.9 1.0 0.48

Ethylbenzene100-41-4 22.1 1.0 0.19

Xylenes, Total1330-20-7 67.1 3.0 0.79

FORM I 8260B

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1

Lab Sample ID: LCSD 460-37643/4



Solid

TestAmerica Edison

Sample wt/vol:

% Moisture:




5(mL)

0.18(mm)

Date Analyzed: 05/17/2010 18:10

ID:DB-624




2037-26-5 Toluene-d8 (Surr) 95 66-126


FORM I 8260B

06/03/2010 of 623


TestAmerica

VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/o37387.dLab Smp Id: LCSD Inj Date : 17-MAY-2010 18:10 Operator : VOAMS 9 Inst ID: VOAMS12.iSmp Info : LCSDMisc Info : Comment : Method : /chem/VOAMS12.i/8260L_10/04-15-10/17may10a.b/8260L_10.mMeth Date : 17-May-2010 18:29 ken Quant Type: ISTDCal Date : 15-APR-2010 16:52 Cal File: o36298.dAls bottle: 3 QC Sample: BSDDil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd2





CONCENTRATIONS



========================== ==== == ====== ====== ======== ======= =======

M 14 1,2-Dichloroethene (total) 100 551170 43.7014 44

90 Dichlorodifluoromethane 85 1.007 1.013 (0.236) 246011 22.6604 23

1 Chloromethane 50 1.141 1.147 (0.268) 280679 19.1838 19

4 Vinyl Chloride 62 1.183 1.183 (0.278) 283367 19.5293 20

3 Bromomethane 94 1.372 1.372 (0.322) 218172 22.2598 22

5 Chloroethane 64 1.439 1.445 (0.338) 170390 19.9442 20

9 Trichlorofluoromethane 101 1.573 1.574 (0.369) 392325 21.0719 21

121 n-Pentane 72 1.622 1.616 (0.381) 47960 21.6313 22

127 Ethanol 46 1.708 1.708 (0.401) 165851 2412.10 2400

46 Ethyl Ether 59 1.756 1.756 (0.412) 160563 18.8309 19

119 Isoprene 67 1.769 1.762 (0.415) 352393 19.8206 20

47 Acrolein 56 1.836 1.836 (0.431) 193625 159.396 160

10 1,1-Dichloroethene 96 1.897 1.897 (0.445) 253166 23.1134 23

48 Freon TF 101 1.903 1.897 (0.446) 262458 20.7979 21

06/03/2010 of 623


CONCENTRATIONS



========================== ==== == ====== ====== ======== ======= =======

7 Acetone 43 1.939 1.939 (0.455) 49861 21.6549 22

142 Iodomethane 142 2.000 2.000 (0.469) 280315 21.6277 22

8 Carbon Disulfide 76 2.043 2.037 (0.479) 687938 20.0272 20

50 Acetonitrile 41 2.128 2.128 (0.499) 557084 441.342 440

125 Methyl acetate 74 2.159 2.159 (0.506) 44775 19.1589 19

6 Methylene Chloride 84 2.226 2.226 (0.522) 287754 26.8234 27

51 TBA 59 2.323 2.323 (0.545) 346571 299.611 300

52 Acrylonitrile 53 2.403 2.403 (0.564) 511031 115.248 120

12 trans-1,2-Dichloroethene 96 2.415 2.415 (0.567) 274203 21.6287 22

53 MTBE 73 2.421 2.421 (0.568) 467729 18.5896 18

49 Isopropanol 45 2.043 2.043 (0.479) 2018158 2227.02 2200(A)

54 Hexane 56 2.616 2.616 (0.614) 172880 19.2591 19

11 1,1-Dichloroethane 63 2.726 2.726 (0.640) 465976 21.5413 22

57 Vinyl Acetate 43 2.787 2.787 (0.654) 411856 17.0008 17

55 DIPE 45 2.793 2.793 (0.655) 575539 19.0867 19

149 tert-Butyl ethyl ether 59 3.085 3.085 (0.724) 474276 18.0170 18


13 cis-1,2-Dichloroethene 96 3.195 3.195 (0.750) 276966 22.0727 22

18 2-Butanone 72 3.226 3.213 (0.757) 23076 18.8101 19

56 Ethyl Acetate 70 3.274 3.274 (0.768) 29035 31.5804 32

108 Bromochloromethane 128 3.402 3.402 (0.798) 119530 23.4837 23

15 Chloroform 83 3.476 3.476 (0.815) 430231 21.7820 22


59 Cyclohexane 56 3.683 3.677 (0.864) 417907 19.0596 19

21 Carbon Tetrachloride 117 3.786 3.787 (0.888) 304647 23.2779 23

92 1,1-Dichloropropene 75 3.786 3.787 (0.888) 321297 21.4338 21


28 Benzene 78 3.982 3.982 (0.934) 961260 21.9143 22

17 1,2-Dichloroethane 62 4.006 4.000 (0.940) 287138 21.5470 22

61 Isopropyl Acetate 43 4.091 4.091 (0.960) 607798 35.7251 36

140 tert-Amylmethyl Ether 73 4.110 4.116 (0.964) 414461 17.6054 18

* 69 Fluorobenzene 96 4.262 4.262 (1.000) 1620590 50.0000

156 2,4,4-Trimethyl-1-pentene 112 4.603 4.603 (1.080) 67250 17.8921 18

25 Trichloroethene 95 4.646 4.640 (1.090) 236502 21.1765 21

63 n-Butanol 43 4.634 4.634 (1.087) 201766 1166.71 1200

96 Ethyl Acrylate 55 4.798 4.798 (1.126) 190787 18.5211 18

126 Methyl cyclohexane 83 4.847 4.847 (1.137) 410422 19.2443 19


109 Dibromomethane 93 5.012 5.012 (1.176) 129261 21.8880 22

95 1,4-Dioxane 88 5.067 5.061 (1.189) 386053 2575.17 2600

146 Methyl methacrylate 69 5.055 5.061 (1.186) 95473 16.3658 16

64 Propyl Acetate 43 5.140 5.140 (1.206) 398938 34.1731 34

22 Bromodichloromethane 83 5.207 5.207 (1.222) 287481 23.0894 23

30 2-Chloroethyl Vinyl Ether 63 5.597 5.597 (1.313) 88101 17.3529 17

118 Epichlorohydrin 57 5.652 5.652 (1.326) 334583 328.362 330

24 cis-1,3-Dichloropropene 75 5.750 5.750 (1.349) 318223 21.7994 22

33 4-Methyl-2-Pentanone 43 5.975 5.969 (1.402) 129514 16.2458 16

06/03/2010 of 623


CONCENTRATIONS



========================== ==== == ====== ====== ======== ======= =======

$ 37 Toluene-d8 (SUR) 98 6.073 6.073 (0.754) 1121982 47.4508 47

38 Toluene 91 6.158 6.158 (0.765) 1005590 21.7234 22

29 trans-1,3-Dichloropropene 75 6.475 6.475 (0.804) 255319 17.4957 17


35 Tetrachloroethene 166 6.871 6.871 (0.853) 227891 22.2669 22


34 2-Hexanone 43 7.103 7.103 (0.882) 92348 15.8544 16

26 Dibromochloromethane 129 7.231 7.231 (0.898) 165525 18.2596 18

65 Butyl Acetate 43 7.322 7.322 (0.909) 435485 34.5598 34

66 1,2-Dibromoethane 107 7.359 7.359 (0.914) 169638 21.2041 21

* 32 Chlorobenzene-d5 117 8.054 8.054 (1.000) 1107274 50.0000

39 Chlorobenzene 112 8.097 8.097 (1.005) 612134 21.9303 22


40 Ethylbenzene 106 8.298 8.298 (1.030) 365157 22.1420 22

43 m+p-Xylene 106 8.487 8.487 (1.054) 897827 44.5911 44

44 o-Xylene 106 9.084 9.090 (1.128) 415434 22.4797 22

42 Styrene 104 9.115 9.115 (1.132) 721987 22.5920 22

147 Butyl Acrylate 55 9.157 9.157 (0.780) 322044 18.7154 19

31 Bromoform 173 9.359 9.359 (1.162) 91554 16.7759 17

145 Amyl Acetate 43 9.554 9.554 (1.186) 264814 33.2997 33(R)

110 Isopropylbenzene 105 9.700 9.700 (1.204) 1157095 22.2966 22


150 Camphene 93 10.066 10.060 (0.858) 448780 18.5707 18

107 Bromobenzene 156 10.115 10.115 (0.862) 259509 23.3297 23


99 1,2,3-Trichloropropane 110 10.255 10.255 (0.874) 60531 20.7624 21

143 trans-1,4-Dichloro-2-butene 53 10.328 10.322 (2.423) 54348 17.3886 17

112 n-Propylbenzene 91 10.377 10.377 (0.884) 1506239 23.3532 23

105 2-Chlorotoluene 91 10.462 10.462 (0.891) 832256 22.8532 23

106 4-Chlorotoluene 91 10.651 10.651 (0.908) 937455 23.3049 23


148 Butyl methacrylate 69 10.974 10.968 (0.935) 285817 18.9415 19

115 tert-Butylbenzene 119 11.218 11.212 (0.956) 881519 22.9454 23


151 2-Octanone 43 11.529 11.529 (0.982) 242654 18.5772 18

114 sec-Butylbenzene 105 11.541 11.541 (0.983) 1413705 24.0975 24


153 2-Octanol 45 11.675 11.675 (0.995) 39257 13.3621 13(R)



113 p-Isopropyltoluene 119 11.767 11.767 (1.003) 1133180 23.6084 24


117 Benzyl chloride 91 11.962 11.962 (1.019) 327428 15.4259 15

111 n-Butylbenzene 91 12.273 12.267 (1.046) 1169584 24.2492 24

101 1,2-Dibromo-3-chloropropane 75 13.059 13.059 (1.113) 40554 18.4601 18

152 Camphor 95 13.736 13.736 (1.170) 115450 82.0159 82


06/03/2010 of 623


CONCENTRATIONS



========================== ==== == ====== ====== ======== ======= =======


70 Naphthalene 128 14.016 14.016 (1.194) 908248 23.5428 24


M 45 Xylene (Total) 100 1313261 67.0709 67

QC Flag Legend

A - Target compound detected but, quantitated amountexceeded maximum amount.


06/03/2010 of 623

Data File: o37387.d

Date: 17-MAY-2010 18:10


Sample Info: LCSD Operator: VOAMS 9

06/03/2010 of 623

Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR

COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID


VOAMS12

34969

Start Date:

End Date: 04/16/2010 00:55

04/15/2010 13:12

BFB 460-34969/1 DB-624 0.18(mm)104/15/2010 13:12 o36289.d

IC 460-34969/2 DB-624 0.18(mm)104/15/2010 14:24 o36292.d

IC 460-34969/3 DB-624 0.18(mm)104/15/2010 15:13 o36294.d

ZZZZZ DB-624 0.18(mm)104/15/2010 15:38

ICIS 460-34969/19 DB-624 0.18(mm)104/15/2010 15:38 o36295.d

ZZZZZ DB-624 0.18(mm)104/15/2010 16:03

IC 460-34969/20 DB-624 0.18(mm)104/15/2010 16:03 o36296.d

IC 460-34969/6 DB-624 0.18(mm)104/15/2010 16:27 o36297.d

IC 460-34969/7 DB-624 0.18(mm)104/15/2010 16:52 o36298.d

ZZZZZ DB-624 0.18(mm)104/15/2010 19:52

ZZZZZ DB-624 0.18(mm)104/15/2010 19:52

ZZZZZ DB-624 0.18(mm)104/15/2010 20:17

ZZZZZ DB-624 0.18(mm)104/15/2010 21:13

ZZZZZ DB-624 0.18(mm)104/15/2010 21:38

ZZZZZ DB-624 0.18(mm)104/15/2010 22:02

ZZZZZ DB-624 0.18(mm)104/15/2010 22:27

ZZZZZ DB-624 0.18(mm)104/15/2010 22:52

ZZZZZ DB-624 0.18(mm)104/15/2010 23:16

ZZZZZ DB-624 0.18(mm)104/15/2010 23:41

ZZZZZ DB-624 0.18(mm)104/16/2010 00:06

ZZZZZ DB-624 0.18(mm)104/16/2010 00:30

ZZZZZ DB-624 0.18(mm)104/16/2010 00:55

8260B

06/03/2010 of 623

Lab Name: Job No.:

SDG No.:

Instrument ID:


GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR



VOAMS12

37643

Start Date:

End Date: 05/18/2010 03:36

05/17/2010 16:42

BFB 460-37643/1 DB-624 0.18(mm)105/17/2010 16:42 o37384.d

CCVIS 460-37643/2 DB-624 0.18(mm)105/17/2010 17:02 o37385.d

LCS 460-37643/3 DB-624 0.18(mm)105/17/2010 17:46 o37386.d

LCSD 460-37643/4 DB-624 0.18(mm)105/17/2010 18:10 o37387.d

MB 460-37643/5 DB-624 0.18(mm)105/17/2010 20:11 o37390.d

ZZZZZ DB-624 0.18(mm)105/17/2010 20:36

ZZZZZ DB-624 0.18(mm)105/17/2010 21:25

ZZZZZ DB-624 0.18(mm)105/17/2010 22:15

ZZZZZ DB-624 0.18(mm)105/17/2010 22:40

ZZZZZ DB-624 0.18(mm)105/17/2010 23:04

ZZZZZ DB-624 0.18(mm)105/17/2010 23:29

ZZZZZ DB-624 0.18(mm)105/17/2010 23:54

460-13139-2 TB-3 6-7 DB-624 0.18(mm)105/18/2010 00:18 o37400.d

460-13139-4 TB-2 5-6 DB-624 0.18(mm)105/18/2010 00:43 o37401.d

460-13139-5 TB-1 2-3 DB-624 0.18(mm)105/18/2010 01:08 o37402.d

460-13139-7 TB-5 3-4 DB-624 0.18(mm)105/18/2010 01:33 o37403.d

ZZZZZ DB-624 0.18(mm)105/18/2010 02:22

ZZZZZ DB-624 0.18(mm)105/18/2010 02:47

ZZZZZ DB-624 0.18(mm)105/18/2010 03:36

8260B

06/03/2010 of 623

GC/MS VOA Worksheet

Method: 5035

Analyst: D'Almeida, Melissa M

Batch Number: 460-37413 Date Open:

Batch End:

May 14 2010 8:38AM

May 14 2010 9:02AM

Lab ID Client ID Basis Final weight/volume of

sample

Initial weight/volume of

sample

Method Chain

LB3~460-37413/1 5 g 5 mL

460-13119-A-1 T 5.11 g 5 mL

460-13119-A-1 T 5.05 g 5 mL

460-13119-B-3 T 5.18 g 5 mL

460-13119-B-3 T 5.22 g 5 mL

460-13119-B-5 T 5.01 g 5 mL

460-13119-B-5 T 5.01 g 5 mL

460-13147-B-2 T 5.01 g 5 mL

460-13147-B-2 T 5.09 g 5 mL

460-13147-A-1 T 5.20 g 5 mL

460-13147-A-1 T 5.23 g 5 mL

460-13148-C-1 T 5.13 g 5 mL

460-13148-C-1 T 5.08 g 5 mL

460-13139-B-1 TB-3 2-3 T 3.67 g 5 mL

460-13139-C-1 TB-3 2-3 T 3.88 g 5 mL

460-13139-B-2 TB-3 6-7 T 5.02 g 5 mL5035, 8260B

460-13139-C-2 TB-3 6-7 T 5.05 g 5 mL

460-13139-B-3 TB-2 2-3 T 3.80 g 5 mL

460-13139-C-3 TB-2 2-3 T 2.46 g 5 mL

460-13139-B-4 TB-2 5-6 T 3.75 g 5 mL5035, 8260B

460-13139-C-4 TB-2 5-6 T 3.07 g 5 mL

460-13139-B-5 TB-1 2-3 T 3.09 g 5 mL5035, 8260B

460-13139-C-5 TB-1 2-3 T 3.20 g 5 mL

460-13139-B-6 TB-1 5-6 T 4.01 g 5 mL

460-13139-C-6 TB-1 5-6 T 3.02 g 5 mL

06/03/2010 of 623

GC/MS VOA Worksheet

Method: 5035

Analyst: D'Almeida, Melissa M


Batch End:

May 14 2010 8:38AM

May 14 2010 9:02AM


sample

Initial weight/volume of

sample

Method Chain

460-13139-B-7 TB-5 3-4 T 2.50 g 5 mL5035, 8260B

460-13139-C-7 TB-5 3-4 T 2.73 g 5 mL

460-13139-B-8 TB-4 6-7 T 4.14 g 5 mL

460-13139-C-8 TB-4 6-7 T 4.68 g 5 mL

06/03/2010 of 623

Method 8270CSemivolatile Organic Compounds

(GC/MS) by Method 8270C

06/03/2010 of 623

FORM II

GC/MS SEMI VOA SURROGATE RECOVERY


SDG No.:


TestAmerica Edison

GC Column (1): Rtx-5MS ID: 0.25(mm)

#Lab Sample IDClient Sample ID # # # # #2FP PHL NBZ FBP TBP TPH

460-13139-2TB-3 6-7 76 82 80 78 78 100

460-13139-4TB-2 5-6 55 60 59 67 53 74

460-13139-5TB-1 2-3 58 68 70 69 93 91

460-13139-7TB-5 3-4 39 41 55 60 52 54

MB 460-37564/1-A 76 82 80 78 82 93

LCS 460-37564/2-A

74 78 82 80 99 89

460-13139-5 MSTB-1 2-3 MS 74 79 80 80 67 91

460-13139-5 MSDTB-1 2-3 MSD 72 75 81 82 66 89

QC LIMITSQC LIMITS2FP = 2-Fluorophenol 37-125

PHL = Phenol-d5 41-118NBZ = Nitrobenzene-d5 38-105FBP = 2-Fluorobiphenyl 40-109TBP = 2,4,6-Tribromophenol 10-120TPH = Terphenyl-d14 16-151

FORM II 8270C


06/03/2010 of 623

GC/MS SEMI VOA LAB CONTROL SAMPLE RECOVERY

FORM III

Job No.:Lab Name:

SDG No.:


Low

460-13139-1

Lab File ID: p2880.dSolid

Lab ID: LCS 460-37564/2-A Client ID:

TestAmerica Edison

REC

%

REC

QC

LIMITSCONCENTRATION

(ug/Kg)

SPIKE

ADDED

(ug/Kg)

#

LCS LCS

COMPOUND

Phenol 6670 4950 54-11574

2-Chlorophenol 6670 5140 56-11077

2-Nitrophenol 6670 5640 55-10185

2,4-Dimethylphenol 6670 5280 56-11279

2,4-Dichlorophenol 6670 5340 58-11580

4-Chloro-3-methylphenol 6670 5690 55-11785

2,4,6-Trichlorophenol 6670 5360 53-11880

2,4-Dinitrophenol 6670 1100 10-12916

4-Nitrophenol 6670 6490 45-11497

4,6-Dinitro-2-methylphenol 6670 2180 10-11033

Pentachlorophenol 6670 4830 19-11372

N-Nitrosodimethylamine 3330 2550 40-8477

Bis(2-chloroethyl)ether 3330 3020 44-10191

1,3-Dichlorobenzene 3330 2490 47-8475



N-Nitrosodi-n-propylamine 3330 3040 42-10791

Hexachloroethane 3330 2480 45-9074

Nitrobenzene 3330 2640 42-10679

Isophorone 3330 2850 48-9786

Bis(2-chloroethoxy)methane 3330 2860 51-10086

1,2,4-Trichlorobenzene 3330 2740 48-9482

Naphthalene 3330 2710 53-9481

Hexachlorobutadiene 3330 2710 45-9881

Hexachlorocyclopentadiene 3330 3110 24-9893

2-Chloronaphthalene 3330 2700 51-10281

Dimethyl phthalate 3330 2960 52-11289

Acenaphthylene 3330 2780 51-10383

2,6-Dinitrotoluene 3330 3130 51-11594

Acenaphthene 3330 2840 46-10085

2,4-Dinitrotoluene 3330 3200 53-11096

Diethyl phthalate 3330 3000 52-11490

4-Chlorophenyl phenyl ether 3330 2910 50-10687

Fluorene 3330 2890 51-10887

N-Nitrosodiphenylamine 3330 3110 49-10693

4-Bromophenyl phenyl ether 3330 2910 44-10287

Hexachlorobenzene 3330 2940 43-10488

Phenanthrene 3330 2850 48-10886

Anthracene 3330 2870 50-10786

Di-n-butyl phthalate 3330 2980 50-10889

Fluoranthene 3330 3040 49-10891

Pyrene 3330 2850 49-11685

FORM III 8270C


06/03/2010 of 623

GC/MS SEMI VOA LAB CONTROL SAMPLE RECOVERY

FORM III

Job No.:Lab Name:

SDG No.:


Low

460-13139-1



TestAmerica Edison

REC

%

REC

QC

LIMITSCONCENTRATION

(ug/Kg)

SPIKE

ADDED

(ug/Kg)

#

LCS LCS

COMPOUND

Benzidine 3330 169 10-615J *

Butyl benzyl phthalate 3330 3010 49-11790

3,3'-Dichlorobenzidine 3330 2870 24-10586

Benzo[a]anthracene 3330 2880 46-11286

Chrysene 3330 2900 45-11487

Bis(2-ethylhexyl) phthalate 3330 3010 49-11990

Di-n-octyl phthalate 3330 3130 40-10694

Benzo[b]fluoranthene 3330 3060 33-9692

Benzo[k]fluoranthene 3330 2990 35-11590

Benzo[a]pyrene 3330 2590 36-8978

Indeno[1,2,3-cd]pyrene 3330 2870 43-10986

Dibenz(a,h)anthracene 3330 2900 43-10787

Benzo[g,h,i]perylene 3330 2980 43-10689

bis (2-chloroisopropyl) ether 3330 2700 45-10281

FORM III 8270C


06/03/2010 of 623

GC/MS SEMI VOA MATRIX SPIKE RECOVERY

FORM III

Job No.:Lab Name:

SDG No.:


Low

460-13139-1


Lab ID: 460-13139-5 MS Client ID: TB-1 2-3 MS

TestAmerica Edison

LIMITS

COMPOUND

CONCENTRATION %

REC

QC

REC

SAMPLE

CONCENTRATION

SPIKE

ADDED

(ug/Kg) (ug/Kg) (ug/Kg)

#

MS MS

7110 5410 54-115Phenol 76350 U

7110 5430 56-1102-Chlorophenol 76350 U

7110 5770 55-1012-Nitrophenol 81350 U

7110 5560 56-1122,4-Dimethylphenol 78350 U

7110 5660 58-1152,4-Dichlorophenol 80350 U

7110 6080 55-1174-Chloro-3-methylphenol 86350 U

7110 4770 53-1182,4,6-Trichlorophenol 67350 U

7110 1100 10-1292,4-Dinitrophenol 01100 UU F

7110 4630 45-1144-Nitrophenol 651100 U

7110 191 10-1104,6-Dinitro-2-methylphenol 31100 JU F

7110 1600 19-113Pentachlorophenol 221100 U

3560 2620 40-84N-Nitrosodimethylamine 74350 U

3560 3190 44-101Bis(2-chloroethyl)ether 9035 U

3560 2340 47-841,3-Dichlorobenzene 66350 U



3560 3240 42-107N-Nitrosodi-n-propylamine 9135 U

3560 2360 45-90Hexachloroethane 6635 U

3560 2690 42-106Nitrobenzene 7635 U

3560 2980 48-97Isophorone 84350 U

3560 3020 51-100Bis(2-chloroethoxy)methane 85350 U

3560 2760 48-941,2,4-Trichlorobenzene 7835 U

3560 2740 53-94Naphthalene 77350 U

3560 2630 45-98Hexachlorobutadiene 7472 U

3560 3040 24-98Hexachlorocyclopentadiene 85350 U

3560 2820 51-1022-Chloronaphthalene 79350 U

3560 3030 52-112Dimethyl phthalate 85350 U

3560 2920 51-103Acenaphthylene 82350 U

3560 3210 51-1152,6-Dinitrotoluene 9072 U

3560 2980 46-100Acenaphthene 84350 U

3560 3110 53-1102,4-Dinitrotoluene 8772 U

3560 3010 52-114Diethyl phthalate 85350 U

3560 3010 50-1064-Chlorophenyl phenyl ether 85350 U

3560 2970 51-108Fluorene 84350 U

3560 3310 49-106N-Nitrosodiphenylamine 93350 U

3560 3110 44-1024-Bromophenyl phenyl ether 88350 U

3560 3080 43-104Hexachlorobenzene 8735 U

3560 2930 48-108Phenanthrene 82350 U

3560 2970 50-107Anthracene 84350 U

3560 2980 50-108Di-n-butyl phthalate 84350 U

3560 3030 49-108Fluoranthene 85350 U

3560 3110 49-116Pyrene 87350 U

FORM III 8270C


06/03/2010 of 623

GC/MS SEMI VOA MATRIX SPIKE RECOVERY

FORM III

Job No.:Lab Name:

SDG No.:


Low

460-13139-1


Lab ID: 460-13139-5 MS Client ID: TB-1 2-3 MS

TestAmerica Edison

LIMITS

COMPOUND

CONCENTRATION %

REC

QC

REC

SAMPLE

CONCENTRATION

SPIKE

ADDED


#

MS MS

3560 89.3 10-61Benzidine 3350 JU F

3560 3090 49-117Butyl benzyl phthalate 87350 U

3560 3100 24-1053,3'-Dichlorobenzidine 87720 U

3560 3010 46-112Benzo[a]anthracene 8535 U

3560 3100 45-114Chrysene 87350 U

3560 3100 49-119Bis(2-ethylhexyl) phthalate 87350 U

3560 3080 40-106Di-n-octyl phthalate 87350 U

3560 3160 33-96Benzo[b]fluoranthene 8935 U

3560 3090 35-115Benzo[k]fluoranthene 8735 U

3560 2660 36-89Benzo[a]pyrene 7535 U

3560 3110 43-109Indeno[1,2,3-cd]pyrene 8835 U

3560 3000 43-107Dibenz(a,h)anthracene 8435 U

3560 3110 43-106Benzo[g,h,i]perylene 87350 U

3560 2780 45-102bis (2-chloroisopropyl) ether 78350 U

FORM III 8270C


06/03/2010 of 623

GC/MS SEMI VOA MATRIX SPIKE DUPLICATE RECOVERY

FORM III

Job No.:Lab Name:

SDG No.:


Low

460-13139-1


Lab ID: 460-13139-5 MSD Client ID: TB-1 2-3 MSD

TestAmerica Edison

COMPOUND

SPIKE


REC

%

RPD

QC LIMITS


#

MSD MSD

7120 5170 30 54-115Phenol 573

7120 5350 30 56-1102-Chlorophenol 175

7120 5620 30 55-1012-Nitrophenol 379

7120 5370 30 56-1122,4-Dimethylphenol 475

7120 5440 30 58-1152,4-Dichlorophenol 476

7120 5690 30 55-1174-Chloro-3-methylphenol 780

7120 4670 30 53-1182,4,6-Trichlorophenol 266

7120 1100 30 10-1292,4-Dinitrophenol NC0U F

7120 4630 30 45-1144-Nitrophenol 065

7120 1100 30 10-1104,6-Dinitro-2-methylphenol NC0U F

7120 1530 30 19-113Pentachlorophenol 421

3560 2660 30 40-84N-Nitrosodimethylamine 175

3560 3150 30 44-101Bis(2-chloroethyl)ether 288

3560 2390 30 47-841,3-Dichlorobenzene 267



3560 3100 30 42-107N-Nitrosodi-n-propylamine 587

3560 2420 30 45-90Hexachloroethane 268

3560 2700 30 42-106Nitrobenzene 076

3560 2900 30 48-97Isophorone 381

3560 2950 30 51-100Bis(2-chloroethoxy)methane 383

3560 2770 30 48-941,2,4-Trichlorobenzene 078

3560 2780 30 53-94Naphthalene 178

3560 2720 30 45-98Hexachlorobutadiene 376

3560 3150 30 24-98Hexachlorocyclopentadiene 489

3560 2860 30 51-1022-Chloronaphthalene 180

3560 3060 30 52-112Dimethyl phthalate 186

3560 2940 30 51-103Acenaphthylene 183

3560 3200 30 51-1152,6-Dinitrotoluene 090

3560 2970 30 46-100Acenaphthene 083

3560 3150 30 53-1102,4-Dinitrotoluene 188

3560 3030 30 52-114Diethyl phthalate 185

3560 3050 30 50-1064-Chlorophenyl phenyl ether 186

3560 3020 30 51-108Fluorene 285

3560 3320 30 49-106N-Nitrosodiphenylamine 093

3560 3130 30 44-1024-Bromophenyl phenyl ether 188

3560 3110 30 43-104Hexachlorobenzene 187

3560 3030 30 48-108Phenanthrene 385

3560 3040 30 50-107Anthracene 285

3560 3160 30 50-108Di-n-butyl phthalate 689

3560 3230 30 49-108Fluoranthene 691

3560 2980 30 49-116Pyrene 484

FORM III 8270C


06/03/2010 of 623

GC/MS SEMI VOA MATRIX SPIKE DUPLICATE RECOVERY

FORM III

Job No.:Lab Name:

SDG No.:


Low

460-13139-1


Lab ID: 460-13139-5 MSD Client ID: TB-1 2-3 MSD

TestAmerica Edison

COMPOUND

SPIKE


REC

%

RPD

QC LIMITS


#

MSD MSD

3560 131 30 10-61Benzidine 384J F

3560 3120 30 49-117Butyl benzyl phthalate 188

3560 3180 30 24-1053,3'-Dichlorobenzidine 289

3560 3030 30 46-112Benzo[a]anthracene 185

3560 3080 30 45-114Chrysene 087

3560 3130 30 49-119Bis(2-ethylhexyl) phthalate 188

3560 3150 30 40-106Di-n-octyl phthalate 288

3560 3220 30 33-96Benzo[b]fluoranthene 291

3560 3180 30 35-115Benzo[k]fluoranthene 389

3560 2720 30 36-89Benzo[a]pyrene 277

3560 3150 30 43-109Indeno[1,2,3-cd]pyrene 188

3560 3030 30 43-107Dibenz(a,h)anthracene 185

3560 3170 30 43-106Benzo[g,h,i]perylene 289

3560 2800 30 45-102bis (2-chloroisopropyl) ether 079

FORM III 8270C


06/03/2010 of 623

FORM IV

GC/MS SEMI VOA METHOD BLANK SUMMARY

Lab Name:

SDG No.:


Instrument ID:

Level:(Low/Med)

Date Extracted:

Date Analyzed: 05/18/2010 10:57

05/17/2010 09:00

Low

BNAMS10

Lab File ID: p2879.d Lab Sample ID: MB 460-37564/1-A

Matrix: Solid


LAB SAMPLE ID

LAB

FILE ID DATE ANALYZEDCLIENT SAMPLE ID

05/18/2010 11:25p2880.dLCS 460-37564/2-A

05/18/2010 11:52p2881.d460-13139-5TB-1 2-3

05/18/2010 12:18p2882.d460-13139-5 MSTB-1 2-3 MS

05/18/2010 12:46p2883.d460-13139-5 MSDTB-1 2-3 MSD

05/18/2010 15:00p2888.d460-13139-2TB-3 6-7

05/18/2010 19:58p2899.d460-13139-7TB-5 3-4

05/18/2010 20:25p2900.d460-13139-4TB-2 5-6

FORM IV 8270C

06/03/2010 of 623

FORM V

DECAFLUOROTRIPHENYLPHOSPHINE (DFTPP)

Lab Name:

SDG No.:

Job No.: 460-13139-1

DFTPP Injection Date: 05/11/2010Lab File ID:

Instrument ID: DFTPP Injection Time: 13:45

p2720.d

BNAMS10



51 30.0 - 60.0 % of mass 198 36.5

68 Less than 2.0 % of mass 69 0.0 (0.0)1

69 Mass 69 relative abundance 42.0

70 Less than 2.0 % of mass 69 0.0 (0.0)1

127 40.0 - 60.0 % of mass 198 58.3

197 Less than 1.0 % of mass 198 0.0

198 Base Peak, 100 % relative abundance 100.0

199 5.0- 9.0 % of mass 198 7.0

275 10.0 - 30.0 % of mass 198 25.9

365 Greater than 1.0 % of mass 198 3.2

441 Present but less than mass 443 12.5


443 17.0 - 23.0 % of mass 442 16.9 (20.0)2



GC/MS SEMI VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Edison

CLIENT SAMPLE IDLAB


ANALYZEDTIME

ANALYZED

p2721.d 05/11/2010 14:17ICIS 460-37184/2

p2722.d 05/11/2010 14:43IC 460-37184/3

p2723.d 05/11/2010 15:10IC 460-37184/4

p2724.d 05/11/2010 15:36IC 460-37184/5

p2725.d 05/11/2010 16:03IC 460-37184/6

p2726.d 05/11/2010 16:30IC 460-37184/7

FORM V 8270C 06/03/2010 of 623

FORM V

DECAFLUOROTRIPHENYLPHOSPHINE (DFTPP)

Lab Name:

SDG No.:

Job No.: 460-13139-1

DFTPP Injection Date: 05/18/2010Lab File ID:

Instrument ID: DFTPP Injection Time: 10:12

p2877.d

BNAMS10



51 30.0 - 60.0 % of mass 198 33.4

68 Less than 2.0 % of mass 69 0.0 (0.0)1

69 Mass 69 relative abundance 37.4

70 Less than 2.0 % of mass 69 0.0 (0.0)1

127 40.0 - 60.0 % of mass 198 54.9

197 Less than 1.0 % of mass 198 0.0

198 Base Peak, 100 % relative abundance 100.0

199 5.0- 9.0 % of mass 198 7.0

275 10.0 - 30.0 % of mass 198 27.1


441 Present but less than mass 443 14.4


443 17.0 - 23.0 % of mass 442 19.7 (19.3)2



GC/MS SEMI VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Edison

CLIENT SAMPLE IDLAB


ANALYZEDTIME

ANALYZED

p2878.d 05/18/2010 10:30CCVIS 460-37818/2

p2879.d 05/18/2010 10:57MB 460-37564/1-A

p2880.d 05/18/2010 11:25LCS 460-37564/2-A

TB-1 2-3 p2881.d 05/18/2010 11:52460-13139-5

TB-1 2-3 MS p2882.d 05/18/2010 12:18460-13139-5 MS

TB-1 2-3 MSD p2883.d 05/18/2010 12:46460-13139-5 MSD

TB-3 6-7 p2888.d 05/18/2010 15:00460-13139-2

TB-5 3-4 p2899.d 05/18/2010 19:58460-13139-7

TB-2 5-6 p2900.d 05/18/2010 20:25460-13139-4

FORM V 8270C 06/03/2010 of 623

GC/MS SEMI VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII



Lab File ID (Standard): p2878.d

Instrument ID: BNAMS10 GC Column: Rtx-5MS ID: 0.25(mm)

Heated Purge: (Y/N) N



DCB NPT ANT

UPPER LIMIT

LOWER LIMIT

379576

94894 307798

1231190

149907

599628

4.21 5.51 7.2612/24 HOUR STD

4.71

3.71

6.01

5.01

7.76

6.76

189788 615595 299814


MB 460-37564/1-A 194268 691224 369280 4.21 5.50 7.26

LCS 460-37564/2-A 175899 596977 306055 4.21 5.50 7.26

460-13139-5 TB-1 2-3 178089 635778 340945 4.21 5.50 7.26

460-13139-5 MS TB-1 2-3 MS 181935 635955 330807 4.21 5.50 7.26

460-13139-5 MSD TB-1 2-3 MSD 176230 597654 296797 4.21 5.50 7.26

460-13139-2 TB-3 6-7 179231 625848 328055 4.21 5.50 7.26

460-13139-7 TB-5 3-4 166401 504685 215742 4.21 5.50 7.26

460-13139-4 TB-2 5-6 184940 594577 269984 4.21 5.50 7.26

DCB = 1,4-Dichlorobenzene-d4

NPT = Naphthalene-d8

ANT = Acenaphthene-d10




FORM VIII 8270C

06/03/2010 of 623

GC/MS SEMI VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII



Lab File ID (Standard): p2878.d

Instrument ID: BNAMS10 GC Column: Rtx-5MS ID: 0.25(mm)

Heated Purge: (Y/N) N



PHN CRY PRY

UPPER LIMIT

LOWER LIMIT

775318

193830 110816

443264

73549

294196

8.73 11.49 13.4012/24 HOUR STD

9.23

8.23

11.99

10.99

13.90

12.90

387659 221632 147098


MB 460-37564/1-A 486284 267422 185780 8.73 11.48 13.40

LCS 460-37564/2-A 392818 220418 164936 8.73 11.49 13.40

460-13139-5 TB-1 2-3 465487 282918 186032 8.73 11.49 13.40

460-13139-5 MS TB-1 2-3 MS 406314 207230 152357 8.73 11.49 13.40

460-13139-5 MSD TB-1 2-3 MSD 366053 206096 152929 8.73 11.49 13.40

460-13139-2 TB-3 6-7 434676 225779 149045 8.73 11.48 13.40

460-13139-7 TB-5 3-4 245292 175541 185914 8.73 11.49 13.41

460-13139-4 TB-2 5-6 309230 191087 186699 8.73 11.49 13.41

PHN = Phenanthrene-d10

CRY = Chrysene-d12

PRY = Perylene-d12




FORM VIII 8270C

06/03/2010 of 623

FORM IForm 1GC/MS SEMI VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

TB-3 6-7

SDG No.:

460-13139-1


Matrix: p2888.dLab File ID:

Date Collected:8270CAnalysis Method:

Soil

TestAmerica Edison

05/12/2010 09:45

Level: (low/med)

Con. Extract Vol.:Volume:Injection Volume:

GPC Cleanup:(Y/N)

Date Analyzed:

Date Extracted:

Dilution Factor:

Extract. Method: 05/17/2010 09:00

1

3541

05/18/2010 15:00

Low

N

1(mL)

% Moisture: 18.8

Sample wt/vol: 15.00(g)



Phenol108-95-2 410 410 50U

2-Chlorophenol95-57-8 410 410 54U

2-Nitrophenol88-75-5 410 410 67U

2,4-Dimethylphenol105-67-9 410 410 65U

2,4-Dichlorophenol120-83-2 410 410 65U

4-Chloro-3-methylphenol59-50-7 410 410 68U

2,4,6-Trichlorophenol88-06-2 410 410 73U

2,4-Dinitrophenol51-28-5 1200 1200 86U

4-Nitrophenol100-02-7 1200 1200 100U

4,6-Dinitro-2-methylphenol534-52-1 1200 1200 190U

Pentachlorophenol87-86-5 1200 1200 200U

N-Nitrosodimethylamine62-75-9 410 410 41U

Bis(2-chloroethyl)ether111-44-4 41 41 8.5U

1,3-Dichlorobenzene541-73-1 410 410 56U



N-Nitrosodi-n-propylamine621-64-7 41 41 5.4U

Hexachloroethane67-72-1 41 41 6.9U

Nitrobenzene98-95-3 41 41 9.1U

Isophorone78-59-1 410 410 47U

Bis(2-chloroethoxy)methane111-91-1 410 410 58U

1,2,4-Trichlorobenzene120-82-1 41 41 6.7U

Naphthalene91-20-3 410 410 60U

Hexachlorobutadiene87-68-3 83 83 17U

Hexachlorocyclopentadiene77-47-4 410 410 120U

2-Chloronaphthalene91-58-7 410 410 58U

Dimethyl phthalate131-11-3 410 410 55U

Acenaphthylene208-96-8 410 410 58U

2,6-Dinitrotoluene606-20-2 83 83 10U

Acenaphthene83-32-9 410 410 58U


Diethyl phthalate84-66-2 410 410 55U

4-Chlorophenyl phenyl ether7005-72-3 410 410 70U

Fluorene86-73-7 410 410 69U

FORM I 8270C

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-3 6-7

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 09:45

Level: (low/med)


GPC Cleanup:(Y/N)

Date Analyzed:

Date Extracted:

Dilution Factor:

Extract. Method: 05/17/2010 09:00

1

3541

05/18/2010 15:00

Low

N

1(mL)

% Moisture: 18.8




N-Nitrosodiphenylamine86-30-6 410 410 66U

4-Bromophenyl phenyl ether101-55-3 410 410 73U

Hexachlorobenzene118-74-1 41 41 5.7U

Phenanthrene85-01-8 410 410 71U

Anthracene120-12-7 410 410 72U

Di-n-butyl phthalate84-74-2 410 410 62U

Fluoranthene206-44-0 410 410 68U

Pyrene129-00-0 410 410 70U

Benzidine92-87-5 410 410 87U *

Butyl benzyl phthalate85-68-7 410 410 48U

3,3'-Dichlorobenzidine91-94-1 830 830 90U

Benzo[a]anthracene56-55-3 28 41 7.5J

Chrysene218-01-9 410 410 59U

Bis(2-ethylhexyl) phthalate117-81-7 120 410 54J

Di-n-octyl phthalate117-84-0 410 410 48U

Benzo[b]fluoranthene205-99-2 41 41 6.1U

Benzo[k]fluoranthene207-08-9 41 41 5.7U

Benzo[a]pyrene50-32-8 41 41 5.0U

Indeno[1,2,3-cd]pyrene193-39-5 41 41 6.5U

Dibenz(a,h)anthracene53-70-3 41 41 4.9U

Benzo[g,h,i]perylene191-24-2 410 410 43U

bis (2-chloroisopropyl) ether108-60-1 410 410 53U


4165-60-0 Nitrobenzene-d5 80 38-105

4165-62-2 Phenol-d5 82 41-118

1718-51-0 Terphenyl-d14 100 16-151

118-79-6 2,4,6-Tribromophenol 78 10-120

367-12-4 2-Fluorophenol 76 37-125

321-60-8 2-Fluorobiphenyl 78 40-109

FORM I 8270C

06/03/2010 of 623



Client Sample ID:

Lab Name: Job No.:

TB-3 6-7

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 09:45

Level: (low/med)


GPC Cleanup:(Y/N)

Date Analyzed:

Date Extracted:

Dilution Factor:

Extract. Method: 05/17/2010 09:00

1

3541

05/18/2010 15:00

Low

N

1(mL)

% Moisture: 18.8






FORM I-TIC 8270C

06/03/2010 of 623

Data File: /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2888.d Report Date: 19-May-2010 14:53

TestAmerica

SEMI-VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2888.dLab Smp Id: 460-13139-E-2-E Client Smp ID: TB-3 6-7Inj Date : 18-MAY-2010 15:00 Operator : BNAMS 4 Inst ID: BNAMS10.iSmp Info : 460-13139-E-2-EMisc Info : 460-13139-E-2-EComment : Method : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/8270C_08SP.mMeth Date : 18-May-2010 11:53 czhao Quant Type: ISTDCal Date : 11-MAY-2010 16:30 Cal File: p2726.dAls bottle: 12 Dil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd1

Concentration Formula: Amt * DF * Uf*1000*Vt/(Ws*(100-M)/100) * CpndVariable


DF 1.00000 Dilution FactorUf 1.00000 ng unit correction factorVt 1.00000 Volume of final extract (ml)Ws 15.00000 Weight of sample extracted (g)M 18.78882 % Moisture


CONCENTRATIONS


Compounds MASS RT EXP RT REL RT RESPONSE (ug/ml) (ug/Kg)

========================== ==== == ====== ====== ======== ======= =======

$ 16 2-Fluorophenol (SUR) 112 2.963 2.928 (0.704) 455839 75.5200 6200

$ 17 Phenol-d5 (SUR) 99 3.850 3.862 (0.915) 554955 81.5177 6700


$ 76 Nitrobenzene-d5 (SUR) 82 4.767 4.778 (0.867) 243860 39.9973 3300

* 80 Naphthalene-d8 136 5.495 5.507 (1.000) 625848 40.0000

$ 77 2-Fluorobiphenyl (SUR) 172 6.588 6.594 (0.908) 467628 39.0913 3200

* 82 Acenaphthene-d10 164 7.258 7.264 (1.000) 328055 40.0000

$ 18 2,4,6-Tribromophenol (SUR) 330 8.039 8.045 (1.108) 84491 77.7534 6400

* 83 Phenanthrene-d10 188 8.727 8.733 (1.000) 434676 40.0000

52 Phenanthrene 178 8.744 8.756 (1.002) 6679 0.54067 44(a)

56 Fluoranthene 202 9.919 9.925 (1.137) 7957 0.81229 67(a)

57 Pyrene 202 10.143 10.149 (0.883) 7245 0.76175 62(a)

$ 78 Terphenyl-d14 244 10.307 10.307 (0.898) 296258 49.8339 4100

06/03/2010 of 623


CONCENTRATIONS



========================== ==== == ====== ====== ======== ======= =======

61 Benzo(a)anthracene 228 11.471 11.476 (0.999) 2160 0.34075 28(aH)

* 81 Chrysene-d12 240 11.482 11.494 (1.000) 225779 40.0000

62 Chrysene 228 11.512 11.524 (1.003) 2636 0.45893 38(a)

63 bis(2-Ethylhexyl)phthalate 149 11.523 11.524 (1.004) 6582 1.40436 120(a)

* 84 Perylene-d12 264 13.398 13.404 (1.000) 149045 40.0000

QC Flag Legend


H - Operator selected an alternate compound hit.

06/03/2010 of 623


TestAmerica



06/03/2010 of 623

Data File: p2888.d

Date: 18-MAY-2010 15:00

Client ID: TB-3 6-7 Instrument: BNAMS10.i

Sample Info: 460-13139-E-2-E Operator: BNAMS 4

06/03/2010 of 623

Data File: p2888.d

Date: 18-MAY-2010 15:00



61 Benzo(a)anthracene

06/03/2010 of 623

Data File: p2888.d

Date: 18-MAY-2010 15:00



63 bis(2-Ethylhexyl)phthalate

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-2 5-6

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 10:45

Level: (low/med)


GPC Cleanup:(Y/N)

Date Analyzed:

Date Extracted:

Dilution Factor:

Extract. Method: 05/17/2010 09:00

1

3541

05/18/2010 20:25

Low

N

1(mL)

% Moisture: 12.8




Phenol108-95-2 380 380 46U

2-Chlorophenol95-57-8 380 380 51U

2-Nitrophenol88-75-5 380 380 62U





2,4-Dinitrophenol51-28-5 1100 1100 80U

4-Nitrophenol100-02-7 1100 1100 97U











Isophorone78-59-1 380 380 43U








Acenaphthylene208-96-8 97 380 54J

2,6-Dinitrotoluene606-20-2 77 77 9.6U

Acenaphthene83-32-9 110 380 54J




Fluorene86-73-7 150 380 64J

FORM I 8270C

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-2 5-6

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 10:45

Level: (low/med)


GPC Cleanup:(Y/N)

Date Analyzed:

Date Extracted:

Dilution Factor:

Extract. Method: 05/17/2010 09:00

1

3541

05/18/2010 20:25

Low

N

1(mL)

% Moisture: 12.8







Phenanthrene85-01-8 1500 380 66

Anthracene120-12-7 240 380 67J


Fluoranthene206-44-0 1800 380 63

Pyrene129-00-0 1500 380 65

Benzidine92-87-5 380 380 80U *



Benzo[a]anthracene56-55-3 710 38 7.0

Chrysene218-01-9 960 380 55



Benzo[b]fluoranthene205-99-2 820 38 5.6

Benzo[k]fluoranthene207-08-9 300 38 5.3

Benzo[a]pyrene50-32-8 690 38 4.7

Indeno[1,2,3-cd]pyrene193-39-5 610 38 6.0

Dibenz(a,h)anthracene53-70-3 130 38 4.5

Benzo[g,h,i]perylene191-24-2 680 380 40



4165-60-0 Nitrobenzene-d5 59 38-105

4165-62-2 Phenol-d5 60 41-118

1718-51-0 Terphenyl-d14 74 16-151

118-79-6 2,4,6-Tribromophenol 53 10-120

367-12-4 2-Fluorophenol 55 37-125


FORM I 8270C

06/03/2010 of 623



Client Sample ID:

Lab Name: Job No.:

TB-2 5-6

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 10:45

Level: (low/med)


GPC Cleanup:(Y/N)

Date Analyzed:

Date Extracted:

Dilution Factor:

Extract. Method: 05/17/2010 09:00

1

3541

05/18/2010 20:25

Low

N

1(mL)

% Moisture: 12.8





C15H12 PAH-1 400 9.23 T J

C15H12 PAH-2 440 9.25 T J

C15H10/C15H12 PAHs 550 9.33 T J

C15H12 PAH-3 320 9.36 T J

84-65-1 9,10-Anthracenedione 510 9.54 T J N

C16H14 PAH 330 9.77 T J

C17H12 PAH-1 370 10.49 T J

C17H12 PAH-2 380 10.60 T J

C20H12 PAH 500 13.25 T J

FORM I-TIC 8270C

06/03/2010 of 623


TestAmerica






CONCENTRATIONS



========================== ==== == ====== ====== ======== ======= =======


$ 17 Phenol-d5 (SUR) 99 3.844 3.862 (0.913) 424868 60.4826 4600



* 80 Naphthalene-d8 136 5.495 5.507 (1.000) 594577 40.0000

31 Naphthalene 128 5.513 5.525 (1.003) 10806 0.64724 49(a)

34 2-Methylnaphthalene 142 6.218 6.224 (1.132) 6613 0.66751 51(a)



125 1,3-Dimethylnaphthalene 156 6.923 6.929 (0.954) 8728 1.29127 98(a)

39 Acenaphthylene 152 7.117 7.123 (0.981) 16669 1.27219 97(a)

* 82 Acenaphthene-d10 164 7.258 7.264 (1.000) 269984 40.0000

42 Acenaphthene 154 7.287 7.299 (1.004) 10589 1.44946 110(a)

06/03/2010 of 623


CONCENTRATIONS



========================== ==== == ====== ====== ======== ======= =======

43 Dibenzofuran 168 7.463 7.469 (1.028) 7214 0.68263 52(a)

47 Fluorene 166 7.798 7.810 (1.074) 15499 1.99010 150(a)


* 83 Phenanthrene-d10 188 8.727 8.733 (1.000) 309230 40.0000

52 Phenanthrene 178 8.750 8.756 (1.003) 168574 19.1821 1500

53 Anthracene 178 8.797 8.803 (1.008) 27584 3.13888 240(a)

54 Carbazole 167 8.956 8.962 (1.026) 11111 1.50609 110(a)

56 Fluoranthene 202 9.925 9.925 (1.137) 164552 23.6129 1800

57 Pyrene 202 10.148 10.149 (0.883) 161026 20.0043 1500

$ 78 Terphenyl-d14 244 10.307 10.307 (0.897) 185531 36.8743 2800

61 Benzo(a)anthracene 228 11.476 11.476 (0.999) 50160 9.34969 710

* 81 Chrysene-d12 240 11.488 11.494 (1.000) 191087 40.0000

62 Chrysene 228 11.518 11.524 (1.003) 61507 12.6525 960


65 Benzo(b)fluoranthene 252 12.881 12.881 (0.961) 56029 10.6991 820

66 Benzo(k)fluoranthene 252 12.916 12.922 (0.963) 22834 3.98923 300(H)

67 Benzo(a)pyrene 252 13.327 13.327 (0.994) 43147 9.00779 690

* 84 Perylene-d12 264 13.409 13.404 (1.000) 186699 40.0000

68 Indeno(1,2,3-cd)pyrene 276 14.908 14.908 (1.112) 31411 8.07262 610

69 Dibenz(a,h)anthracene 278 14.937 14.943 (1.114) 6725 1.70164 130

70 Benzo(g,h,i)perylene 276 15.319 15.319 (1.142) 35090 8.91008 680

QC Flag Legend



06/03/2010 of 623


TestAmerica







* 83 Phenanthrene-d10 8.727 825818 40.000

* 81 Chrysene-d12 11.488 685646 40.000

* 84 Perylene-d12 13.409 567337 40.000


RT AREA ON-COL(ug/ml) FINAL(ug/Kg) QUAL LIBRARY LIB ENTRY CPND #

==== ==== ============= ============ ==== ======= ========= ======

C15H12 PAH-1 CAS #:

9.226 108287 5.24507341 400 0 0 83

06/03/2010 of 623




==== ==== ============= ============ ==== ======= ========= ======

C15H12 PAH-2 CAS #:

9.250 120317 5.82777654 440 0 0 83

C15H10/C15H12 PAHs CAS #:

9.332 149704 7.25117045 550 0 0 83

C15H12 PAH-3 CAS #:

9.355 87084 4.21807501 320 0 0 83

9,10-Anthracenedione CAS #: 84-65-1

9.537 136921 6.63203860 500 98 NIST02.l 61654 83

C16H14 PAH CAS #:

9.772 88982 4.31002595 330 0 0 83

C17H12 PAH-1 CAS #:

10.489 82559 4.81641662 370 0 0 81

C17H12 PAH-2 CAS #:

10.601 85236 4.97259894 380 0 0 81

C20H12 PAH CAS #:

13.251 93427 6.58707981 500 0 0 84

06/03/2010 of 623

Data File: p2900.d

Date: 18-MAY-2010 20:25



06/03/2010 of 623

Data File: p2900.d

Date: 18-MAY-2010 20:25



39 Acenaphthylene

06/03/2010 of 623

Data File: p2900.d

Date: 18-MAY-2010 20:25



42 Acenaphthene

06/03/2010 of 623

Data File: p2900.d

Date: 18-MAY-2010 20:25



47 Fluorene

06/03/2010 of 623

Data File: p2900.d

Date: 18-MAY-2010 20:25



52 Phenanthrene

06/03/2010 of 623

Data File: p2900.d

Date: 18-MAY-2010 20:25



53 Anthracene

06/03/2010 of 623

Data File: p2900.d

Date: 18-MAY-2010 20:25



56 Fluoranthene

06/03/2010 of 623

Data File: p2900.d

Date: 18-MAY-2010 20:25



57 Pyrene

06/03/2010 of 623

Data File: p2900.d

Date: 18-MAY-2010 20:25




06/03/2010 of 623

Data File: p2900.d

Date: 18-MAY-2010 20:25



62 Chrysene

06/03/2010 of 623

Data File: p2900.d

Date: 18-MAY-2010 20:25




06/03/2010 of 623

Data File: p2900.d

Date: 18-MAY-2010 20:25



65 Benzo(b)fluoranthene

06/03/2010 of 623

Data File: p2900.d

Date: 18-MAY-2010 20:25



66 Benzo(k)fluoranthene

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Data File: p2900.d

Date: 18-MAY-2010 20:25



67 Benzo(a)pyrene

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Data File: p2900.d

Date: 18-MAY-2010 20:25



68 Indeno(1,2,3-cd)pyrene

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Data File: p2900.d

Date: 18-MAY-2010 20:25



69 Dibenz(a,h)anthracene

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Data File: p2900.d

Date: 18-MAY-2010 20:25



70 Benzo(g,h,i)perylene

06/03/2010 of 623

Data File: p2900.d

Date: 18-MAY-2010 20:25





C15H12 PAH-1

Anthracene, 2-methyl- 613-12-7 NIST02.l 50612 96 C15H12 192

Phenanthrene, 2-methyl- 2531-84-2 NIST02.l 50626 96 C15H12 192

06/03/2010 of 623

Data File: p2900.d

Date: 18-MAY-2010 20:25





C15H12 PAH-2

1H-Cyclopropa[l]phenanthrene,1a,9b 949-41-7 NIST02.l 50641 94 C15H12 192


06/03/2010 of 623

Data File: p2900.d

Date: 18-MAY-2010 20:25





C15H10/C15H12 PAHs

6H-Cyclobuta[jk]phenanthrene 83469-43-6 NIST02.l 49336 46 C15H10 190


06/03/2010 of 623

Data File: p2900.d

Date: 18-MAY-2010 20:25





C15H12 PAH-3



06/03/2010 of 623

Data File: p2900.d

Date: 18-MAY-2010 20:25





9,10-Anthracenedione 84-65-1 NIST02.l 61654 98 C14H8O2 208



06/03/2010 of 623

Data File: p2900.d

Date: 18-MAY-2010 20:25





C16H14 PAH

Phenanthrene, 2,5-dimethyl- 3674-66-6 NIST02.l 60352 96 C16H14 206

9,10-Dimethylanthracene 781-43-1 NIST02.l 60343 96 C16H14 206

06/03/2010 of 623

Data File: p2900.d

Date: 18-MAY-2010 20:25





C17H12 PAH-1

11H-Benzo[b]fluorene 243-17-4 NIST02.l 67030 90 C17H12 216

11H-Benzo[a]fluorene 238-84-6 NIST02.l 67031 87 C17H12 216

06/03/2010 of 623

Data File: p2900.d

Date: 18-MAY-2010 20:25





C17H12 PAH-2

Fluoranthene, 2-methyl- 33543-31-6 NIST02.l 67037 93 C17H12 216

Pyrene, 4-methyl- 3353-12-6 NIST02.l 67026 92 C17H12 216

06/03/2010 of 623

Data File: p2900.d

Date: 18-MAY-2010 20:25





C20H12 PAH

Perylene 198-55-0 NIST02.l 89813 98 C20H12 252

Perylene 198-55-0 NIST02.l 89814 98 C20H12 252

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-1 2-3

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 11:25

Level: (low/med)


GPC Cleanup:(Y/N)

Date Analyzed:

Date Extracted:

Dilution Factor:

Extract. Method: 05/17/2010 09:00

1

3541

05/18/2010 11:52

Low

N

1(mL)

% Moisture: 6.5




Phenol108-95-2 350 350 43U

2-Chlorophenol95-57-8 350 350 47U

2-Nitrophenol88-75-5 350 350 58U





2,4-Dinitrophenol51-28-5 1100 1100 75U

4-Nitrophenol100-02-7 1100 1100 91U











Isophorone78-59-1 350 350 41U














Fluorene86-73-7 350 350 60U

FORM I 8270C

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-1 2-3

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 11:25

Level: (low/med)


GPC Cleanup:(Y/N)

Date Analyzed:

Date Extracted:

Dilution Factor:

Extract. Method: 05/17/2010 09:00

1

3541

05/18/2010 11:52

Low

N

1(mL)

% Moisture: 6.5








Anthracene120-12-7 350 350 62U



Pyrene129-00-0 350 350 61U

Benzidine92-87-5 350 350 75U *



Benzo[a]anthracene56-55-3 35 35 6.5U

Chrysene218-01-9 350 350 51U

Bis(2-ethylhexyl) phthalate117-81-7 350 350 47U










4165-60-0 Nitrobenzene-d5 70 38-105

4165-62-2 Phenol-d5 68 41-118

1718-51-0 Terphenyl-d14 91 16-151

118-79-6 2,4,6-Tribromophenol 93 10-120

367-12-4 2-Fluorophenol 58 37-125


FORM I 8270C

06/03/2010 of 623



Client Sample ID:

Lab Name: Job No.:

TB-1 2-3

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 11:25

Level: (low/med)


GPC Cleanup:(Y/N)

Date Analyzed:

Date Extracted:

Dilution Factor:

Extract. Method: 05/17/2010 09:00

1

3541

05/18/2010 11:52

Low

N

1(mL)

% Moisture: 6.5






FORM I-TIC 8270C

06/03/2010 of 623


TestAmerica

SEMI-VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2881.dLab Smp Id: 460-13139-E-5-G Client Smp ID: TB-1 2-3Inj Date : 18-MAY-2010 11:52 Operator : BNAMS 4 Inst ID: BNAMS10.iSmp Info : 460-13139-E-5-GMisc Info : 460-13139-E-5-GComment : Method : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/8270C_08SP.mMeth Date : 18-May-2010 11:53 czhao Quant Type: ISTDCal Date : 11-MAY-2010 16:30 Cal File: p2726.dAls bottle: 5 Dil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd1





CONCENTRATIONS



========================== ==== == ====== ====== ======== ======= =======


$ 17 Phenol-d5 (SUR) 99 3.850 3.862 (0.915) 461525 68.2284 4800



* 80 Naphthalene-d8 136 5.495 5.507 (1.000) 635778 40.0000


* 82 Acenaphthene-d10 164 7.258 7.264 (1.000) 340945 40.0000


* 83 Phenanthrene-d10 188 8.727 8.733 (1.000) 465487 40.0000

$ 78 Terphenyl-d14 244 10.307 10.307 (0.897) 337666 45.3279 3200

* 81 Chrysene-d12 240 11.488 11.494 (1.000) 282918 40.0000

* 84 Perylene-d12 264 13.404 13.404 (1.000) 186032 40.0000

06/03/2010 of 623


TestAmerica

SEMI-VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2881.dLab Smp Id: 460-13139-E-5-G Client Smp ID: TB-1 2-3Inj Date : 18-MAY-2010 11:52 Operator : BNAMS 4 Inst ID: BNAMS10.iSmp Info : 460-13139-E-5-GMisc Info : 460-13139-E-5-GComment : Method : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/8270C_08SP.mMeth Date : 18-May-2010 11:53 czhao Quant Type: ISTDCal Date : 11-MAY-2010 16:30 Cal File: p2726.dAls bottle: 5 Dil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd1


06/03/2010 of 623

Data File: p2881.d

Date: 18-MAY-2010 11:52


Sample Info: 460-13139-E-5-G Operator: BNAMS 4

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-5 3-4

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 12:30

Level: (low/med)


GPC Cleanup:(Y/N)

Date Analyzed:

Date Extracted:

Dilution Factor:

Extract. Method: 05/17/2010 09:00

1

3541

05/18/2010 19:58

Low

N

1(mL)

% Moisture: 61.5




Phenol108-95-2 860 860 110U

2-Chlorophenol95-57-8 860 860 110U

2-Nitrophenol88-75-5 860 860 140U





2,4-Dinitrophenol51-28-5 2600 2600 180U

4-Nitrophenol100-02-7 2600 2600 220U




Bis(2-chloroethyl)ether111-44-4 86 86 18U




N-Nitrosodi-n-propylamine621-64-7 86 86 11U

Hexachloroethane67-72-1 86 86 14U

Nitrobenzene98-95-3 86 86 19U

Isophorone78-59-1 860 860 99U


1,2,4-Trichlorobenzene120-82-1 86 86 14U

Naphthalene91-20-3 860 860 130U







Acenaphthene83-32-9 200 860 120J




Fluorene86-73-7 440 860 150J

FORM I 8270C

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-5 3-4

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 12:30

Level: (low/med)


GPC Cleanup:(Y/N)

Date Analyzed:

Date Extracted:

Dilution Factor:

Extract. Method: 05/17/2010 09:00

1

3541

05/18/2010 19:58

Low

N

1(mL)

% Moisture: 61.5






Hexachlorobenzene118-74-1 86 86 12U

Phenanthrene85-01-8 1800 860 150

Anthracene120-12-7 260 860 150J


Fluoranthene206-44-0 1300 860 140

Pyrene129-00-0 790 860 150J

Benzidine92-87-5 860 860 180U *



Benzo[a]anthracene56-55-3 380 86 16

Chrysene218-01-9 560 860 120J



Benzo[b]fluoranthene205-99-2 590 86 13

Benzo[k]fluoranthene207-08-9 230 86 12

Benzo[a]pyrene50-32-8 410 86 11

Indeno[1,2,3-cd]pyrene193-39-5 460 86 14

Dibenz(a,h)anthracene53-70-3 86 86 10U

Benzo[g,h,i]perylene191-24-2 460 860 91J



4165-60-0 Nitrobenzene-d5 55 38-105

4165-62-2 Phenol-d5 41 41-118

1718-51-0 Terphenyl-d14 54 16-151

118-79-6 2,4,6-Tribromophenol 52 10-120

367-12-4 2-Fluorophenol 39 37-125


FORM I 8270C

06/03/2010 of 623



Client Sample ID:

Lab Name: Job No.:

TB-5 3-4

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 12:30

Level: (low/med)


GPC Cleanup:(Y/N)

Date Analyzed:

Date Extracted:

Dilution Factor:

Extract. Method: 05/17/2010 09:00

1

3541

05/18/2010 19:58

Low

N

1(mL)

% Moisture: 61.5





Unknown-1 5400 12.11 T J

Unknown Alkane-1 13000 12.22 T J


Unknown-2 4200 13.86 T J

7616-22-0 .gamma.-Tocopherol 8500 13.96 T J N


59-02-9 Vitamin E 11000 14.36 T J N

Unknown-3 3800 15.02 T J

Unknown-4 6500 15.21 T J

Unknown-5 10000 15.37 T J

Unknown-6 30000 15.62 T J

Unknown Sterol 10000 15.72 T J

1000194-62-4 4,4,6a,6b,8a,11,11,14b-Octamethyl-1,4,4a 30000 15.77 T J N

Unknown-7 4700 15.81 T J

Unknown-8 9800 15.86 T J

Unknown-9 22000 15.98 T J

Unknown-10 36000 16.11 T J

Unknown-11 11000 16.27 T J

Unknown-12 23000 16.32 T J

Unknown-13 10000 16.37 T J

Unknown-14 10000 16.44 T J

Unknown-15 13000 16.55 T J

Unknown-16 3400 16.75 T J

Unknown-17 5100 16.86 T J

Unknown-18 4500 17.40 T J

FORM I-TIC 8270C

06/03/2010 of 623


TestAmerica






CONCENTRATIONS



========================== ==== == ====== ====== ======== ======= =======


$ 17 Phenol-d5 (SUR) 99 3.844 3.862 (0.913) 258523 40.9026 7100(R)



* 80 Naphthalene-d8 136 5.495 5.507 (1.000) 504685 40.0000

31 Naphthalene 128 5.519 5.525 (1.004) 3709 0.26173 45(a)




125 1,3-Dimethylnaphthalene 156 6.917 6.929 (0.953) 2136 0.39546 68(a)

* 82 Acenaphthene-d10 164 7.258 7.264 (1.000) 215742 40.0000

42 Acenaphthene 154 7.287 7.299 (1.004) 6749 1.15609 200(a)

43 Dibenzofuran 168 7.458 7.469 (1.028) 7619 0.90221 160(a)

06/03/2010 of 623


CONCENTRATIONS



========================== ==== == ====== ====== ======== ======= =======

47 Fluorene 166 7.798 7.810 (1.074) 15977 2.56725 440(a)


* 83 Phenanthrene-d10 188 8.727 8.733 (1.000) 245292 40.0000

52 Phenanthrene 178 8.750 8.756 (1.003) 70548 10.1202 1800

53 Anthracene 178 8.797 8.803 (1.008) 10271 1.47343 260(a)

54 Carbazole 167 8.956 8.962 (1.026) 1635 0.27939 48(aH)

56 Fluoranthene 202 9.919 9.925 (1.137) 41324 7.47562 1300

57 Pyrene 202 10.143 10.149 (0.883) 33542 4.53596 780(a)

$ 78 Terphenyl-d14 244 10.307 10.307 (0.897) 123790 26.7822 4600


* 81 Chrysene-d12 240 11.488 11.494 (1.000) 175541 40.0000

62 Chrysene 228 11.518 11.524 (1.003) 14455 3.23685 560(a)



66 Benzo(k)fluoranthene 252 12.916 12.922 (0.963) 7456 1.30811 230

67 Benzo(a)pyrene 252 13.321 13.327 (0.993) 11271 2.36298 410

* 84 Perylene-d12 264 13.409 13.404 (1.000) 185914 40.0000

68 Indeno(1,2,3-cd)pyrene 276 14.908 14.908 (1.112) 10238 2.65562 460

70 Benzo(g,h,i)perylene 276 15.331 15.319 (1.143) 10400 2.65193 460(a)

QC Flag Legend


R - Spike/Surrogate failed recovery limits.H - Operator selected an alternate compound hit.

06/03/2010 of 623


TestAmerica







* 81 Chrysene-d12 11.488 536862 40.000

* 84 Perylene-d12 13.409 567669 40.000



==== ==== ============= ============ ==== ======= ========= ======

Unknown-1 CAS #:

12.111 417217 31.0855978 5400 0 0 81

06/03/2010 of 623




==== ==== ============= ============ ==== ======= ========= ======

Unknown Alkane-1 CAS #:

12.223 1043719 77.7643864 13000 0 0 81


13.157 1853159 130.580201 23000 0 0 84

Unknown-2 CAS #:

13.856 345601 24.3522478 4200 0 0 84

.gamma.-Tocopherol CAS #: 7616-22-0

13.956 699767 49.3080528 8500 97 NIST02.l 159683 84


14.132 1280041 90.1962735 16000 0 0 84

Vitamin E CAS #: 59-02-9

14.361 917147 64.6254471 11000 99 NIST02.l 161945 84

Unknown-3 CAS #:

15.019 312618 22.0281906 3800 0 0 84

Unknown-4 CAS #:

15.207 531423 37.4459666 6500 0 0 84

Unknown-5 CAS #:

15.372 821264 57.8691920 10000 0 0 84

Unknown-6 CAS #:

15.625 2439669 171.907769 30000 0 0 84

Unknown Sterol CAS #:

15.719 849198 59.8375162 10000 0 0 84

4,4,6a,6b,8a,11,11,14b-Octamethyl-1,4,4a CAS #: 1000194-62-4

15.766 2452198 172.790624 30000 86 NIST02.l 160977 84

Unknown-7 CAS #:

15.813 382367 26.9429338 4700 0 0 84

Unknown-8 CAS #:

15.860 803654 56.6283559 9800 0 0 84

Unknown-9 CAS #:

15.983 1834546 129.268630 22000 0 0 84

06/03/2010 of 623




==== ==== ============= ============ ==== ======= ========= ======

Unknown-10 CAS #:

16.106 2969630 209.250683 36000 0 0 84

Unknown-11 CAS #:

16.265 876283 61.7460238 11000 0 0 84

Unknown-12 CAS #:

16.324 1905580 134.273981 23000 0 0 84

Unknown-13 CAS #:

16.371 840203 59.2036779 10000 0 0 84

Unknown-14 CAS #:

16.441 839864 59.1797935 10000 0 0 84

Unknown-15 CAS #:

16.553 1046819 73.7626199 13000 0 0 84

Unknown-16 CAS #:

16.753 280252 19.7475552 3400 0 0 84

Unknown-17 CAS #:

16.858 417152 29.3940269 5100 0 0 84

Unknown-18 CAS #:

17.405 372516 26.2488193 4500 0 0 84

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58



06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58



42 Acenaphthene

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58



47 Fluorene

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58



52 Phenanthrene

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58



53 Anthracene

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58



56 Fluoranthene

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58



57 Pyrene

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58




06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58



62 Chrysene

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58




06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58



65 Benzo(b)fluoranthene

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58



66 Benzo(k)fluoranthene

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58



67 Benzo(a)pyrene

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58



68 Indeno(1,2,3-cd)pyrene

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58



70 Benzo(g,h,i)perylene

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58





Unknown-1

2(1H)-Phenanthrenone, 3,4,4a,4b,5, 7715-44-8 NIST02.l 103086 62 C19H30O 274

7H-Furo[3,2-g][1]benzopyran-7-one, 54087-32-0 NIST02.l 102803 58 C15H14O5 274

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58





Unknown Alkane-1

Hexadecane 544-76-3 NIST02.l 73968 90 C16H34 226

Hexadecane 544-76-3 NIST02.l 73966 68 C16H34 226

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58





Unknown Alkane-2

Nonacosane 630-03-5 NIST02.l 158131 97 C29H60 408

Tetracosane 646-31-1 NIST02.l 136482 97 C24H50 338

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58





Unknown-2

1,19-Eicosadiene 14811-95-1 NIST02.l 105307 90 C20H38 278

Oxirane, heptadecyl- 67860-04-2 NIST02.l 107629 70 C19H38O 282

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58





.gamma.-Tocopherol 7616-22-0 NIST02.l 159683 97 C28H48O2 416

3,4-Dihydro-3,5,8-trimethyl-3-(4,8 1000105-71-9 NIST02.l 165270 64 C30H50O3 458

Benzenepropanenitrile, 3,4-dimetho 49621-56-9 NIST02.l 49753 55 C11H13NO2 191

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58





Unknown Alkane-3

Heptadecane 629-78-7 NIST02.l 82607 96 C17H36 240

Hexadecane, 1-iodo- 544-77-4 NIST02.l 141774 95 C16H33I 352

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58





Vitamin E 59-02-9 NIST02.l 161945 99 C29H50O2 430



06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58





Unknown-3

2H,8H-Benzo[1,2-b:5,4-b']dipyran-2 55334-39-9 NIST02.l 130818 55 C20H22O4 326

Acetic acid, [2,5-bis(trimethylsil 27798-63-6 NIST02.l 130548 46 C15H26O4Si2 326

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58





Unknown-4

1,1'-Biphenyl, 2,2',3,4,5-Pentachl 55312-69-1 NIST02.l 129478 90 C12H5Cl5 324

Bis(pentamethylcyclopentadienyl)ir 12126-50-0 NIST02.l 130845 50 C20H30Fe 326

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58





Unknown-5

Ergostanol 6538-02-9 NIST02.l 157084 90 C28H50O 402

Cholestane, 3-ethoxy-, (3.beta.,5. 2089-02-3 NIST02.l 159710 72 C29H52O 416

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58





Unknown-6

.beta.-Sitosterol 83-46-5 NIST02.l 159282 98 C29H50O 414

Stigmasterol, 22,23-dihydro- 1000214-20-7 NIST02.l 159291 96 C29H50O 414

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58





Unknown Sterol

Cholestane, 3-ethoxy-, (3.beta.,5. 2089-02-3 NIST02.l 159710 41 C29H52O 416

Stigmastanol 19466-47-8 NIST02.l 159708 41 C29H52O 416

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58





4,4,6a,6b,8a,11,11,14b-Octamethyl- 1000194-62-4 NIST02.l 160977 86 C30H48O 424

Benzenamine, 2,6-dimethyl-N-(4,4-d 281211-68-5 NIST02.l 68040 64 C13H18N2O 218

Urs-12-ene 464-97-1 NIST02.l 158505 58 C30H50 410

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58





Unknown-7

p-(N-(Dimethylcarbamoylmethyl)acet 92703-70-3 NIST02.l 112574 27 C15H21N3O3 291

Phenol, 2,5-bis(1-methylpropyl)- 54932-77-3 NIST02.l 60195 25 C14H22O 206

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58





Unknown-8

Androst-5-en-17-ol, 4,4-dimethyl- 1000195-76-3 NIST02.l 118836 43 C21H34O 302

2-Methyl-3-n-heptyl-6-methoxy-1,5- 1000250-74-6 NIST02.l 110925 25 C17H24N2O2 288

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58





Unknown-9

.alpha.-Amyrin 638-95-9 NIST02.l 161264 91 C30H50O 426

2(1H)Naphthalenone, 3,5,6,7,8,8a-h 1000188-66-5 NIST02.l 68225 89 C15H22O 218

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58





Unknown-10


D:C-Friedoolean-8-en-3-one 22611-26-3 NIST02.l 160967 64 C30H48O 424

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58





Unknown-11

3-Methylcholanthrene 56-49-5 NIST02.l 99514 48 C21H16 268

Ethyl .alpha.-oximidostearate 1000126-75-7 NIST02.l 137659 46 C20H39NO3 341

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58





Unknown-12


.beta.-Amyrin 559-70-6 NIST02.l 161263 49 C30H50O 426

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58





Unknown-13

Ethanone, 1-[5-(5-trifluoromethyl- 1000266-44-5 NIST02.l 102545 43 C11H9F3N2OS 274

10H-Phenoxaphosphine, 2-ethyl-10-h 36360-91-5 NIST02.l 102822 38 C15H15O3P 274

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58





Unknown-14

Androstan-6-one, (5.alpha.)- 3676-06-0 NIST02.l 103060 43 C19H30O 274

2(1H)-Phenanthrenone, 3,4,4a,4b,5, 7715-44-8 NIST02.l 103086 43 C19H30O 274

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58





Unknown-15

Stigmast-4-en-3-one 1058-61-3 NIST02.l 158845 66 C29H48O 412

Cholest-5-en-3-one, 4,4-dimethyl- 2220-42-0 NIST02.l 158848 35 C29H48O 412

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58





Unknown-16

Azulene, 1,4-dimethyl-7-(1-methyle 489-84-9 NIST02.l 55042 51 C15H18 198

Naphthalene, 1,6-dimethyl-4-(1-met 483-78-3 NIST02.l 55043 38 C15H18 198

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58





Unknown-17

1,3-Diethyl-2-hydroxybenzothiazolo 1000227-15-3 NIST02.l 102705 43 C14H14N2O2S 274

10H-Phenoxaphosphine, 2-ethyl-10-h 36360-91-5 NIST02.l 102822 43 C15H15O3P 274

06/03/2010 of 623

Data File: p2899.d

Date: 18-MAY-2010 19:58





Unknown-18

.alpha.-Cedrene oxide 1000159-39-1 NIST02.l 69499 55 C15H24O 220

Friedelan-3-one 559-74-0 NIST02.l 161267 43 C30H50O 426

06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:


GC/MS SEMI VOA INITIAL CALIBRATION DATA


BNAMS10



N

05/11/2010 16:30

0.25(mm)Rtx-5MS ID:


Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-37184/4 p2723.d2Level IC 460-37184/7 p2726.d3Level IC 460-37184/6 p2725.d4Level ICIS 460-37184/2 p2721.d5Level IC 460-37184/5 p2724.d6Level IC 460-37184/3 p2722.d

ANALYTE RRF


CURVETYPE

COEFFICIENT

B M1 M2

# %RSD # MAX%RSD

R^2OR COD

# MIN R^2OR COD

MIN RRF

LVL 6

1,4-Dioxane 0.3344 0.2903 0.3185 0.2742 0.3041 Ave 7.00.3140

15.00.3059

2,3,7,8-TCDD (Screen) +++++ +++++ +++++ 0.1162 +++++ Ave+++++

15.00.1162

N-Nitrosodimethylamine 0.7958 0.7918 0.7605 0.7352 0.7200 Ave 4.00.7668

15.00.7617

Pyridine 1.5172 1.4777 1.4043 1.3267 1.3012 Ave 5.91.3964

15.01.4039

Benzaldehyde 0.8555 0.8922 0.6746 0.3984 0.2195 Ave 48.0+++++

* 15.00.6080

Phenol 1.8646 1.7991 1.6198 1.5352 1.4505 Ave 10.01.5320

30.01.6335

Aniline 2.1491 2.1648 1.9550 1.9105 1.7726 Ave 14.11.4427

15.01.8991

Bis(2-chloroethyl)ether 1.5055 1.4088 1.3203 1.2604 1.2286 QuaF 0.99661.8387

0.99000.9479 -0.073

2-Chlorophenol 1.6385 1.5763 1.4663 1.3419 1.2380 Ave 11.61.2722

15.01.4222

Decane 1.2704 1.2423 1.1654 1.1137 1.0305 Ave 10.80.9546

15.01.1295


15.01.6722


30.01.6514

Benzyl alcohol 0.8469 0.8728 0.8204 0.8191 0.7730 Ave 6.80.7184

15.00.8084


15.01.5551

2-Methylphenol 1.3383 1.2827 1.1732 1.0830 0.9986 Ave 12.01.0302

15.01.1510

FORM VI 8270C


06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




BNAMS10



N

05/11/2010 16:30

0.25(mm)Rtx-5MS ID:


ANALYTE RRF


CURVETYPE

COEFFICIENT

B M1 M2

# %RSD # MAX%RSD

R^2OR COD

# MIN R^2OR COD

MIN RRF

LVL 6

bis (2-chloroisopropyl) ether 1.4549 1.3999 1.3266 1.2394 1.1317 Ave 10.91.1177

15.01.2783

o-Toluidine 2.8826 2.7880 2.5140 2.3417 2.2140 Ave 11.2+++++

15.02.5481

Acetophenone 1.8303 1.8975 1.6444 1.5196 1.4083 Ave 12.81.4223

15.01.6204

3 & 4 Methylphenol 1.4050 1.3202 1.1862 1.0648 0.9922 Ave 13.71.0749

15.01.1739

4-Methylphenol 1.4050 1.3168 1.1790 1.0648 0.9922 Ave 13.71.0749

15.01.1721

N-Nitrosodi-n-propylamine 0.8446 0.8860 0.7934 0.7404 0.6671 Ave 11.90.6657

0.0500 15.00.7662

Hexachloroethane 0.6620 0.6496 0.6226 0.6050 0.5553 Ave 7.80.5476

15.00.6070

Nitrobenzene 0.6306 0.5806 0.5472 0.4898 0.4545 QuaF 0.99980.4070

0.99001.5964 0.6970

n,n'-Dimethylaniline 2.4040 2.2483 2.0634 1.8870 1.7586 Ave 13.51.7338

15.02.0159

Isophorone 0.6875 0.6968 0.6583 0.6277 0.6099 Ave 5.30.6352

15.00.6526

2-Nitrophenol 0.2097 0.2172 0.2118 0.2035 0.1993 Ave 3.20.2032

30.00.2074

2,4-Dimethylphenol 0.3756 0.3687 0.3420 0.3123 0.2929 Ave 11.30.2900

15.00.3302

Bis(2-chloroethoxy)methane 0.4292 0.4335 0.4079 0.3908 0.3729 Ave 6.20.3815

15.00.4026

Benzoic acid 0.1117 0.1532 0.1477 0.1430 0.1539 Ave 11.40.1545

15.00.1440

2,4-Dichlorophenol 0.3240 0.3223 0.2995 0.2779 0.2604 Ave 10.80.2500

30.00.2890


15.00.3311

Naphthalene 1.2625 1.2417 1.1826 1.0725 1.0183 Ave 11.00.9614

15.01.1232

4-Chloroaniline 0.4669 0.4747 0.4460 0.4155 0.3859 Ave 9.00.3882

15.00.4295

Hexachlorobutadiene 0.2068 0.1968 0.1888 0.1724 0.1643 Ave 10.00.1624

30.00.1819

Caprolactam 0.0720 0.0918 0.0794 0.0911 0.0792 Ave 9.20.0820

15.00.0826

FORM VI 8270C


06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




BNAMS10



N

05/11/2010 16:30

0.25(mm)Rtx-5MS ID:


ANALYTE RRF


CURVETYPE

COEFFICIENT

B M1 M2

# %RSD # MAX%RSD

R^2OR COD

# MIN R^2OR COD

MIN RRF

LVL 6

4-Chloro-3-methylphenol 0.3008 0.3171 0.2829 0.2731 0.2561 Ave 8.80.2554

30.00.2809

2-Methylnaphthalene 0.7637 0.7341 0.6805 0.6319 0.5906 Ave 10.80.5981

15.00.6665

1-Methylnaphthalene 0.7273 0.7477 0.6762 0.6289 0.5898 Ave 11.10.5685

15.00.6564

Hexachlorocyclopentadiene 0.2850 0.2637 0.2977 0.3481 0.3599 Ave 14.70.3835

0.0500 15.00.3230

2-tertbutyl-4-methylphenol 0.4897 0.5036 0.4567 0.4288 0.3989 QuaF 0.99090.3185

0.99001.4154 1.6687

2,4,6-Trichlorophenol 0.3931 0.3817 0.3704 0.3515 0.3577 Ave 6.30.4155

30.00.3783

2,4,5-Trichlorophenol 0.3852 0.3989 0.3911 0.3614 0.3545 Ave 7.30.3279

15.00.3698

Diphenyl 1.7136 1.7409 1.6333 1.4791 1.3908 Ave 14.61.1614

15.01.5199

2-Chloronaphthalene 1.3439 1.3326 1.2805 1.1639 1.1049 Ave 9.51.0802

15.01.2177

Diphenyl ether 0.9676 0.9598 0.9136 0.8331 0.8131 Ave 8.20.8140

15.00.8835

2-Nitroaniline 0.3559 0.4077 0.3840 0.3749 0.3538 Ave 11.40.2868

15.00.3605

Dimethylnaphthalene, total 1.0787 1.0835 1.0293 0.9443 0.9243 Ave 7.10.9485

15.01.0014

Dimethyl phthalate 1.2279 1.2744 1.2011 1.1561 1.0957 Ave 5.71.1248

15.01.1800

Coumarin 0.1909 0.2103 0.1868 0.1944 0.1713 Ave 8.10.1700

15.00.1873

2,6-Dinitrotoluene 0.2557 0.2876 0.2762 0.2816 0.2627 Ave 4.40.2749

15.00.2731

Acenaphthylene 2.1544 2.0838 1.9949 1.8523 1.7729 Ave 8.21.7892

15.01.9412


15.00.2879

3,5-di-tert-butyl-4-hydroxytol 1.0743 1.0917 1.0563 0.9555 0.9045 Ave 9.80.8616

15.00.9906

Acenaphthene 1.3092 1.1826 1.1267 1.0065 0.9419 Ave 13.90.9273

30.01.0824

2,4-Dinitrophenol 0.0693 0.0870 0.0932 0.1206 0.1216 QuaF 0.99470.1255

0.0500 0.99009.5223 -4.359

FORM VI 8270C


06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




BNAMS10



N

05/11/2010 16:30

0.25(mm)Rtx-5MS ID:


ANALYTE RRF


CURVETYPE

COEFFICIENT

B M1 M2

# %RSD # MAX%RSD

R^2OR COD

# MIN R^2OR COD

MIN RRF

LVL 6

4-Nitrophenol 0.1471 0.1550 0.1538 0.1708 0.1577 Ave 6.20.1720

0.0500 15.00.1594

2,4-Dinitrotoluene 0.3001 0.3403 0.3232 0.3272 0.2964 Ave 6.20.2932

15.00.3134

Dibenzofuran 1.7460 1.7462 1.6300 1.4998 1.3910 Ave 10.61.3813

15.01.5657

1-Naphthylamine 0.6314 0.7429 0.7934 0.8769 0.7729 Ave 10.70.8146

30.00.7720

2-Naphthylamine 0.8391 0.9325 0.8713 0.8843 0.8072 Ave 5.00.8501

15.00.8641

Diethyl phthalate 1.1532 1.2021 1.1333 1.0991 1.0349 Ave 7.60.9721

15.01.0991

4-Chlorophenyl phenyl ether 0.5800 0.5749 0.5370 0.4879 0.4542 Ave 10.90.4589

15.00.5155

Fluorene 1.2972 1.2905 1.2256 1.0989 1.0078 Ave 11.71.0032

15.01.1539


15.00.2420

4,6-Dinitro-2-methylphenol 0.0918 0.1030 0.1092 0.1184 0.1233 Ave 10.40.1151

15.00.1102

N-Nitrosodiphenylamine 0.6518 0.6783 0.6537 0.6015 0.6078 Ave 4.80.6185

30.00.6353

1,2-Diphenylhydrazine 1.1710 1.1698 1.0985 0.9985 0.9776 Ave 7.91.0275

15.01.0738

4-Bromophenyl phenyl ether 0.2512 0.2510 0.2393 0.2245 0.2239 Ave 5.20.2326

15.00.2371

Hexachlorobenzene 0.2621 0.2664 0.2460 0.2307 0.2309 Ave 6.20.2397

15.00.2460

Atrazine 0.1900 0.2050 0.1883 0.1864 0.1802 Ave 8.30.1580

15.00.1847

Pentachlorophenol 0.0991 0.1070 0.1093 0.1207 0.1219 Ave 10.10.1305

30.00.1147

n-Octadecane 0.5101 0.5404 0.5039 0.4540 0.4645 Ave 8.90.4239

15.00.4828

Phenanthrene 1.2423 1.2307 1.1658 1.0952 1.0414 Ave 7.91.0453

15.01.1368

Anthracene 1.2077 1.2242 1.1769 1.1108 1.0470 Ave 6.81.0539

15.01.1367

Carbazole 1.0121 1.0142 0.9757 0.9493 0.8875 Ave 6.00.8869

15.00.9543

FORM VI 8270C


06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




BNAMS10



N

05/11/2010 16:30

0.25(mm)Rtx-5MS ID:


ANALYTE RRF


CURVETYPE

COEFFICIENT

B M1 M2

# %RSD # MAX%RSD

R^2OR COD

# MIN R^2OR COD

MIN RRF

LVL 6

Di-n-butyl phthalate 1.1027 1.1829 1.1721 1.1526 1.0958 Ave 3.51.0964

15.01.1337

Fluoranthene 0.9159 0.9414 0.9319 0.9242 0.8490 Ave 4.70.8462

30.00.9014

Benzidine 0.0851 0.2413 0.1918 0.0988 0.0659 Ave 55.6+++++

* 15.00.1366

Pyrene 1.7105 1.8847 1.6665 1.6234 1.5613 Ave 6.51.6635

15.01.6850

Butyl benzyl phthalate 0.6096 0.6456 0.6396 0.6790 0.6734 Ave 5.70.7176

15.00.6608

Carbamazepine 0.2818 0.3992 0.4412 0.4980 0.5410 QuaF 0.99910.5480

0.99002.0817 -0.164

3,3'-Dichlorobenzidine 0.3069 0.3441 0.3277 0.3052 0.2954 Ave 6.80.2870

15.00.3111

Benzo[a]anthracene 1.2527 1.1088 1.0816 1.0904 1.0678 Ave 6.01.1369

15.01.1230

Bis(2-ethylhexyl) phthalate 0.8133 0.8447 0.8074 0.8253 0.8232 Ave 2.70.8681

15.00.8303

Chrysene 1.0900 1.0443 1.0478 1.0063 0.9683 Ave 5.20.9489

15.01.0176

Di-n-octyl phthalate 1.1765 1.4012 1.4005 1.6095 1.6475 QuaF 0.99971.8204

0.99000.6874 -0.025

Benzo[b]fluoranthene 0.8828 1.0698 1.1304 1.1936 1.2085 Ave 11.81.2468

15.01.1220

Benzo[k]fluoranthene 0.9836 1.3256 1.2367 1.2744 1.2573 Ave 10.01.2804

15.01.2263

Benzo[a]pyrene 0.9730 0.9980 1.0532 1.0313 1.0493 Ave 3.31.0526

30.01.0262

Indeno[1,2,3-cd]pyrene 0.5157 0.7363 0.7771 0.8835 0.9027 QuaF 0.99970.9446

0.99001.2085 -0.054

Dibenz(a,h)anthracene 0.4732 0.6915 0.8277 0.8965 0.9027 QuaF 0.99970.9390

0.99001.1825 -0.042

Benzo[g,h,i]perylene 0.7385 0.7848 0.8445 0.8735 0.8983 Ave 8.30.9231

15.00.8438

2-Fluorophenol 1.4987 1.4708 1.3674 1.2624 1.1903 Ave 9.01.2929

15.01.3471

Phenol-d5 1.7447 1.7117 1.5431 1.4345 1.3243 Ave 11.81.3577

15.01.5193

Nitrobenzene-d5 0.4151 0.4270 0.4021 0.3893 0.3689 Ave 8.60.3356

15.00.3897

FORM VI 8270C


06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




BNAMS10



N

05/11/2010 16:30

0.25(mm)Rtx-5MS ID:


ANALYTE RRF


CURVETYPE

COEFFICIENT

B M1 M2

# %RSD # MAX%RSD

R^2OR COD

# MIN R^2OR COD

MIN RRF

LVL 6

2-Fluorobiphenyl 1.5827 1.6097 1.5251 1.3955 1.3242 Ave 9.01.3144

15.01.4586

2,4,6-Tribromophenol 0.1217 0.1347 0.1322 0.1371 0.1295 Ave 4.80.1397

15.00.1325

Terphenyl-d14 1.0769 1.1483 1.0172 1.0334 0.9919 Ave 5.21.0516

15.01.0532

FORM VI 8270C


06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




BNAMS10



N

05/11/2010 16:30

GC Column: Rtx-5MS ID: 0.25(mm)


Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-37184/4 p2723.dLevel 2 IC 460-37184/7 p2726.dLevel 3 IC 460-37184/6 p2725.dLevel 4 ICIS 460-37184/2 p2721.dLevel 5 IC 460-37184/5 p2724.dLevel 6 IC 460-37184/3 p2722.d

ANALYTE CURVETYPE

ISREF

RESPONSE


CONCENTRATION (UG/ML)


1,4-Dioxane AvePHN 11240 22497 33921 83612 135128270394

5.00 10.0 20.0 50.0 80.0120

2,3,7,8-TCDD (Screen) AveCRY +++++ +++++ +++++ 201 ++++++++++

+++++ +++++ +++++ 0.500 ++++++++++

N-Nitrosodimethylamine AveDCB 14340 30434 43821 110186 177396348575

5.00 10.0 20.0 50.0 80.0120

Pyridine AveDCB 27341 56800 80914 198833 320592634756

5.00 10.0 20.0 50.0 80.0120

Benzaldehyde AveDCB 15416 34294 38868 59710 54093+++++

5.00 10.0 20.0 50.0 80.0+++++

Phenol AveDCB 33600 69154 93332 230071 357392696410

5.00 10.0 20.0 50.0 80.0120

Aniline AveDCB 38727 83212 112648 286314 436758655809

5.00 10.0 20.0 50.0 80.0120

Bis(2-chloroethyl)ether QuaFDCB 2713 54151 76076 188896 302701835822

0.500 10.0 20.0 50.0 80.0120

2-Chlorophenol AveDCB 29526 60590 84489 201113 305031578327

5.00 10.0 20.0 50.0 80.0120

Decane AveDCB 22892 47754 67151 166905 253896433933

5.00 10.0 20.0 50.0 80.0120


5.00 10.0 20.0 50.0 80.0120


5.00 10.0 20.0 50.0 80.0120

Benzyl alcohol AveDCB 15262 33551 47273 122755 190447326576

5.00 10.0 20.0 50.0 80.0120


5.00 10.0 20.0 50.0 80.0120

2-Methylphenol AveDCB 24116 49304 67598 162311 246046468324

5.00 10.0 20.0 50.0 80.0120

bis (2-chloroisopropyl) ether AveDCB 26218 53809 76439 185741 278829508059

5.00 10.0 20.0 50.0 80.0120

FORM VI 8270C 06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




BNAMS10



N

05/11/2010 16:30



ANALYTE CURVETYPE

ISREF

RESPONSE




o-Toluidine AveDCB 51945 107169 144857 350940 545513+++++

5.00 10.0 20.0 50.0 80.0+++++

Acetophenone AveDCB 32983 72938 94753 227740 346994646534

5.00 10.0 20.0 50.0 80.0120

3 & 4 Methylphenol AveDCB 25319 50748 68352 159577 244458488609

5.00 10.0 20.0 50.0 80.0120

4-Methylphenol AveDCB 25319 50616 67932 159577 244458488609

5.00 10.0 20.0 50.0 80.0120

N-Nitrosodi-n-propylamine AveDCB 1522 34058 45716 110956 164360302592

0.500 10.0 20.0 50.0 80.0120

Hexachloroethane AveDCB 1193 24968 35876 90664 136813248912

0.500 10.0 20.0 50.0 80.0120

Nitrobenzene QuaFNPT 3859 77196 104246 247570 368229641389

0.500 10.0 20.0 50.0 80.0120

n,n'-Dimethylaniline AveDCB 4332 86423 118894 282801 433293788142

0.500 10.0 20.0 50.0 80.0120

Isophorone AveNPT 42075 92650 125399 317241 4941581000971

5.00 10.0 20.0 50.0 80.0120

2-Nitrophenol AveNPT 12831 28884 40349 102839 161449320228

5.00 10.0 20.0 50.0 80.0120

2,4-Dimethylphenol AveNPT 22983 49018 65148 157847 237353457019

5.00 10.0 20.0 50.0 80.0120

Bis(2-chloroethoxy)methane AveNPT 26264 57636 77698 197548 302150601104

5.00 10.0 20.0 50.0 80.0120

Benzoic acid AveNPT 6835 20370 28133 72294 124678243452

5.00 10.0 20.0 50.0 80.0120

2,4-Dichlorophenol AveNPT 19829 42859 57061 140455 210987393900

5.00 10.0 20.0 50.0 80.0120

1,2,4-Trichlorobenzene AveNPT 2106 47858 67115 162132 247105479659

0.500 10.0 20.0 50.0 80.0120

Naphthalene AveNPT 77263 165102 225280 542084 8250611514957

5.00 10.0 20.0 50.0 80.0120

4-Chloroaniline AveNPT 28570 63114 84965 210020 312652611799

5.00 10.0 20.0 50.0 80.0120

Hexachlorobutadiene AveNPT 2531 26169 35968 87146 133125255975

1.00 10.0 20.0 50.0 80.0120

Caprolactam AveNPT 4406 12205 15134 46028 64155129217

5.00 10.0 20.0 50.0 80.0120

4-Chloro-3-methylphenol AveNPT 18405 42159 53886 138012 207519402425

5.00 10.0 20.0 50.0 80.0120

2-Methylnaphthalene AveNPT 46734 97611 129639 319373 478513942529

5.00 10.0 20.0 50.0 80.0120

FORM VI 8270C 06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




BNAMS10



N

05/11/2010 16:30



ANALYTE CURVETYPE

ISREF

RESPONSE




1-Methylnaphthalene AveNPT 44511 99420 128821 317846 477852895898

5.00 10.0 20.0 50.0 80.0120

Hexachlorocyclopentadiene AveANT 8342 17302 26785 85502 135650277158

5.00 10.0 20.0 50.0 80.0120

2-tertbutyl-4-methylphenol QuaFNPT 29965 66956 86994 216729 323222501936

5.00 10.0 20.0 50.0 80.0120

2,4,6-Trichlorophenol AveANT 11507 25041 33330 86360 134821300269

5.00 10.0 20.0 50.0 80.0120

2,4,5-Trichlorophenol AveANT 11276 26170 35186 88777 133618236989

5.00 10.0 20.0 50.0 80.0120

Diphenyl AveANT 50166 114214 146952 363363 524191839368

5.00 10.0 20.0 50.0 80.0120

2-Chloronaphthalene AveANT 39343 87432 115207 285932 416432780728

5.00 10.0 20.0 50.0 80.0120

Diphenyl ether AveANT 28326 62972 82198 204654 306430588313

5.00 10.0 20.0 50.0 80.0120

2-Nitroaniline AveANT 20836 26746 34553 92096 133331207268

10.0 10.0 20.0 50.0 80.0120

Dimethylnaphthalene, total AveANT 31577 71084 92612 231987 348362685494

5.00 10.0 20.0 50.0 80.0120

Dimethyl phthalate AveANT 35947 83612 108065 284018 412960812920

5.00 10.0 20.0 50.0 80.0120

Coumarin AveNPT 11680 27957 35579 98245 138768267878

5.00 10.0 20.0 50.0 80.0120

2,6-Dinitrotoluene AveANT 1497 18866 24848 69187 98991198679

1.00 10.0 20.0 50.0 80.0120

Acenaphthylene AveANT 63070 136711 179491 455030 6681661293148

5.00 10.0 20.0 50.0 80.0120


10.0 10.0 20.0 50.0 80.0120

3,5-di-tert-butyl-4-hydroxytol AveANT 31450 71625 95036 234715 340885622746

5.00 10.0 20.0 50.0 80.0120

Acenaphthene AveANT 38326 77589 101369 247252 354979670223

5.00 10.0 20.0 50.0 80.0120

2,4-Dinitrophenol QuaFANT 6088 11411 12577 29626 4582790715

15.0 20.0 30.0 50.0 80.0120

4-Nitrophenol AveANT 12920 20332 20762 41966 59451124349

15.0 20.0 30.0 50.0 80.0120

2,4-Dinitrotoluene AveANT 1757 22325 29081 80387 111692211919

1.00 10.0 20.0 50.0 80.0120

Dibenzofuran AveANT 51114 114567 146660 368428 524234998346

5.00 10.0 20.0 50.0 80.0120

FORM VI 8270C 06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




BNAMS10



N

05/11/2010 16:30



ANALYTE CURVETYPE

ISREF

RESPONSE




1-Naphthylamine AveANT 18483 48739 71386 215410 291293588740

5.00 10.0 20.0 50.0 80.0120

2-Naphthylamine AveANT 24565 61178 78391 217236 304226614439

5.00 10.0 20.0 50.0 80.0120

Diethyl phthalate AveANT 33760 78864 101966 270013 390057702551

5.00 10.0 20.0 50.0 80.0120

4-Chlorophenyl phenyl ether AveANT 16978 37718 48319 119847 171192331646

5.00 10.0 20.0 50.0 80.0120

Fluorene AveANT 37974 84665 110268 269955 379831725070

5.00 10.0 20.0 50.0 80.0120


10.0 10.0 20.0 50.0 80.0120

4,6-Dinitro-2-methylphenol AvePHN 9258 15967 17449 36105 5481399111

15.0 20.0 30.0 50.0 80.0120

N-Nitrosodiphenylamine AvePHN 21910 52568 69616 183415 270082532569

5.00 10.0 20.0 50.0 80.0120

1,2-Diphenylhydrazine AvePHN 39363 90660 116988 304461 434441884689

5.00 10.0 20.0 50.0 80.0120

4-Bromophenyl phenyl ether AvePHN 8443 19455 25490 68465 99495200243

5.00 10.0 20.0 50.0 80.0120

Hexachlorobenzene AvePHN 881 20649 26198 70336 102624206404

0.500 10.0 20.0 50.0 80.0120

Atrazine AvePHN 6386 15890 20050 56849 80095136072

5.00 10.0 20.0 50.0 80.0120

Pentachlorophenol AvePHN 9996 16586 17454 36809 54159112373

15.0 20.0 30.0 50.0 80.0120

n-Octadecane AvePHN 17149 41882 53666 138422 206400365007

5.00 10.0 20.0 50.0 80.0120

Phenanthrene AvePHN 41761 95378 124157 333937 462778899985

5.00 10.0 20.0 50.0 80.0120

Anthracene AvePHN 40597 94876 125337 338699 465272907378

5.00 10.0 20.0 50.0 80.0120

Carbazole AvePHN 34022 78603 103916 289468 394382763600

5.00 10.0 20.0 50.0 80.0120

Di-n-butyl phthalate AvePHN 37067 91673 124828 351434 486959943979

5.00 10.0 20.0 50.0 80.0120

Fluoranthene AvePHN 30789 72957 99252 281801 377275728544

5.00 10.0 20.0 50.0 80.0120

Benzidine AvePHN 2860 37395 30641 30115 29293+++++

5.00 20.0 30.0 50.0 80.0+++++

Pyrene AveCRY 30421 74386 99692 280847 379631714441

5.00 10.0 20.0 50.0 80.0120

FORM VI 8270C 06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




BNAMS10



N

05/11/2010 16:30



ANALYTE CURVETYPE

ISREF

RESPONSE




Butyl benzyl phthalate AveCRY 10842 25479 38263 117469 163744308193

5.00 10.0 20.0 50.0 80.0120

Carbamazepine QuaFCRY 5011 15755 26391 86153 131540235332

5.00 10.0 20.0 50.0 80.0120

3,3'-Dichlorobenzidine AveCRY 10917 27163 29401 52807 71832123262

10.0 20.0 30.0 50.0 80.0120

Benzo[a]anthracene AveCRY 2228 43760 64700 188632 259636488256

0.500 10.0 20.0 50.0 80.0120

Bis(2-ethylhexyl) phthalate AveCRY 14465 33338 48297 142778 200167372822

5.00 10.0 20.0 50.0 80.0120

Chrysene AveCRY 19385 41216 62680 174091 235430407544

5.00 10.0 20.0 50.0 80.0120

Di-n-octyl phthalate QuaFPRY 15513 39057 63179 208803 296100560482

5.00 10.0 20.0 50.0 80.0120

Benzo[b]fluoranthene AvePRY 1164 29819 50994 154848 217207383883

0.500 10.0 20.0 50.0 80.0120

Benzo[k]fluoranthene AvePRY 1297 36950 55791 165327 225977394222

0.500 10.0 20.0 50.0 80.0120

Benzo[a]pyrene AvePRY 1283 27819 47514 133788 188595324081

0.500 10.0 20.0 50.0 80.0120

Indeno[1,2,3-cd]pyrene QuaFPRY 680 20524 35055 114626 162242290818

0.500 10.0 20.0 50.0 80.0120

Dibenz(a,h)anthracene QuaFPRY 624 19276 37340 116311 162253289112

0.500 10.0 20.0 50.0 80.0120

Benzo[g,h,i]perylene AvePRY 9737 21876 38095 113316 161451284212

5.00 10.0 20.0 50.0 80.0120

2-Fluorophenol AveDCB 27007 56536 78793 189188 293278587708

5.00 10.0 20.0 50.0 80.0120

Phenol-d5 AveDCB 31440 65796 88914 214979 326300617160

5.00 10.0 20.0 50.0 80.0120

Nitrobenzene-d5 AveNPT 25404 56772 76600 196791 298910528774

5.00 10.0 20.0 50.0 80.0120

2-Fluorobiphenyl AveANT 46332 105607 137214 342823 499061950013

5.00 10.0 20.0 50.0 80.0120

2,4,6-Tribromophenol AveANT 3562 8837 11894 33691 48819100994

5.00 10.0 20.0 50.0 80.0120

Terphenyl-d14 AveCRY 19152 45322 60848 178781 241181451642

5.00 10.0 20.0 50.0 80.0120

Curve Type Legend:Ave = Average ISTDQuaF = Quadratic ISTD forced zero

FORM VI 8270C 06/03/2010 of 623

FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:


GC/MS SEMI VOA CONTINUING CALIBRATION DATA

0.25(mm)

460-13139-1

BNAMS10

05/18/2010 10:30

05/11/2010 14:17

05/11/2010 16:30

CCVIS 460-37818/2

Rtx-5MS

TestAmerica Edison

Lab File ID: p2878.d Conc. Units: ug/L



1,4-Dioxane Ave 0.26100.3059 42700 50000 -14.7 20.0

N-Nitrosodimethylamine Ave 0.72500.7617 47600 50000 -4.8 20.0

Pyridine Ave 1.3171.404 46900 50000 -6.2 20.0

Benzaldehyde Ave 0.46970.6080 38600 50000 -22.7* 20.0

Phenol Ave 1.5291.634 46800 50000 -6.4 20.0

Aniline Ave 1.8231.899 48000 50000 -4.0 20.0

Bis(2-chloroethyl)ether QuaF 1.2431.427 51900 50000 3.7 20.0

2-Chlorophenol Ave 1.3321.422 46800 50000 -6.4 20.0

Decane Ave 1.0821.129 47900 50000 -4.2 20.0

1,3-Dichlorobenzene Ave 1.6011.672 47900 50000 -4.3 20.0


Benzyl alcohol Ave 0.76390.8084 47200 50000 -5.5 20.0


2-Methylphenol Ave 1.0531.151 45700 50000 -8.5 20.0

bis (2-chloroisopropyl) ether

Ave 1.1921.278 46600 50000 -6.8 20.0

Acetophenone Ave 1.4871.620 45900 50000 -8.3 20.0

N-Nitrosodi-n-propylamine Ave 0.66030.7662 0.0500 43100 50000 -13.8 20.0

3 & 4 Methylphenol Ave 1.0021.174 42700 50000 -14.6 20.0

4-Methylphenol Ave 1.0061.172 42900 50000 -14.2 20.0

o-Toluidine Ave 2.3582.548 46300 50000 -7.5 20.0

Hexachloroethane Ave 0.58220.6070 48000 50000 -4.1 20.0

Nitrobenzene QuaF 0.48210.5183 48600 50000 -2.8 20.0

n,n'-Dimethylaniline Ave 1.8542.016 46000 50000 -8.0 20.0

Isophorone Ave 0.61920.6526 47400 50000 -5.1 20.0

2-Nitrophenol Ave 0.21390.2074 51500 50000 3.1 20.0

2,4-Dimethylphenol Ave 0.31630.3302 47900 50000 -4.2 20.0

Bis(2-chloroethoxy)methane Ave 0.38840.4026 48200 50000 -3.5 20.0

Benzoic acid Ave 0.16100.1440 55900 50000 11.8 20.0

2,4-Dichlorophenol Ave 0.28110.2890 48600 50000 -2.7 20.0

1,2,4-Trichlorobenzene Ave 0.32830.3311 49600 50000 -0.9 20.0

Naphthalene Ave 1.0671.123 47500 50000 -5.0 20.0

4-Chloroaniline Ave 0.41000.4295 47700 50000 -4.5 20.0

Hexachlorobutadiene Ave 0.17680.1819 48600 50000 -2.8 20.0

Caprolactam Ave 0.08990.0826 54400 50000 8.9 20.0

4-Chloro-3-methylphenol Ave 0.27400.2809 48800 50000 -2.5 20.0

2-Methylnaphthalene Ave 0.63840.6665 47900 50000 -4.2 20.0

1-Methylnaphthalene Ave 0.63370.6564 48300 50000 -3.5 20.0

Hexachlorocyclopentadiene Ave 0.36530.3230 0.0500 56600 50000 13.1 20.0

2-tertbutyl-4-methylphenol QuaF 0.42730.4327 49300 50000 -1.4 20.0

2,4,6-Trichlorophenol Ave 0.36680.3783 48500 50000 -3.0 20.0

FORM VII 8270C

06/03/2010 of 623

FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:



0.25(mm)

460-13139-1

BNAMS10

05/18/2010 10:30

05/11/2010 14:17

05/11/2010 16:30

CCVIS 460-37818/2

Rtx-5MS

TestAmerica Edison




2,4,5-Trichlorophenol Ave 0.36610.3698 49500 50000 -1.0 20.0

Diphenyl Ave 1.4611.520 48100 50000 -3.9 20.0

2-Chloronaphthalene Ave 1.1481.218 47200 50000 -5.7 20.0

Diphenyl ether Ave 0.84750.8835 48000 50000 -4.1 20.0

2-Nitroaniline Ave 0.36920.3605 51200 50000 2.4 20.0

Dimethylnaphthalene, total Ave 0.94261.001 47100 50000 -5.9 20.0

Dimethyl phthalate Ave 1.1881.180 50300 50000 0.7 20.0

Coumarin Ave 0.19840.1873 53000 50000 5.9 20.0

2,6-Dinitrotoluene Ave 0.28810.2731 52800 50000 5.5 20.0

Acenaphthylene Ave 1.8411.941 47400 50000 -5.2 20.0


3,5-di-tert-butyl-4-hydroxytol

Ave 0.91860.9906 46400 50000 -7.3 20.0

Acenaphthene Ave 0.96521.082 44600 50000 -10.8 20.0

2,4-Dinitrophenol QuaF 0.14330.1029 0.0500 62600 50000 25.2* 20.0

4-Nitrophenol Ave 0.17830.1594 0.0500 55900 50000 11.9 20.0

2,4-Dinitrotoluene Ave 0.34030.3134 54300 50000 8.6 20.0

Dibenzofuran Ave 1.4841.566 47400 50000 -5.2 20.0

2-Naphthylamine Ave 0.90560.8641 52400 50000 4.8 20.0

Diethyl phthalate Ave 1.1361.099 51700 50000 3.3 20.0

4-Chlorophenyl phenyl ether Ave 0.49890.5155 48400 50000 -3.2 20.0

Fluorene Ave 1.1111.154 48100 50000 -3.7 20.0


4,6-Dinitro-2-methylphenol Ave 0.13600.1102 61700 50000 23.4* 20.0

N-Nitrosodiphenylamine Ave 0.60440.6353 47600 50000 -4.9 20.0

1,2-Diphenylhydrazine Ave 0.95561.074 44500 50000 -11.0 20.0

4-Bromophenyl phenyl ether Ave 0.23270.2371 49100 50000 -1.9 20.0

Hexachlorobenzene Ave 0.23840.2460 48500 50000 -3.1 20.0

Atrazine Ave 0.18780.1847 50900 50000 1.7 20.0

Pentachlorophenol Ave 0.12450.1147 54300 50000 8.5 20.0

n-Octadecane Ave 0.44850.4828 46400 50000 -7.1 20.0

Phenanthrene Ave 1.0831.137 47600 50000 -4.7 20.0

Anthracene Ave 1.1101.137 48800 50000 -2.3 20.0

Carbazole Ave 0.96730.9543 50700 50000 1.4 20.0

Di-n-butyl phthalate Ave 1.1891.134 52400 50000 4.9 20.0

Fluoranthene Ave 0.95860.9014 53200 50000 6.3 20.0

Benzidine Ave 0.09500.1366 34800 50000 -30.5* 20.0

Pyrene Ave 1.6661.685 49400 50000 -1.1 20.0

Butyl benzyl phthalate Ave 0.71400.6608 54000 50000 8.1 20.0

2,3,7,8-TCDD (Screen) Ave 0.16140.1162 694 500 38.9* 20.0

Carbamazepine QuaF 0.51210.4515 50600 50000 1.2 20.0

FORM VII 8270C

06/03/2010 of 623

FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:



0.25(mm)

460-13139-1

BNAMS10

05/18/2010 10:30

05/11/2010 14:17

05/11/2010 16:30

CCVIS 460-37818/2

Rtx-5MS

TestAmerica Edison




3,3'-Dichlorobenzidine Ave 0.32680.3111 52500 50000 5.1 20.0

Benzo[a]anthracene Ave 1.1041.123 49100 50000 -1.7 20.0

Bis(2-ethylhexyl) phthalate Ave 0.88510.8303 53300 50000 6.6 20.0

Chrysene Ave 0.99291.018 48800 50000 -2.4 20.0

Di-n-octyl phthalate QuaF 1.8711.509 58800 50000 17.6 20.0

Benzo[b]fluoranthene Ave 1.2181.122 54300 50000 8.6 20.0

Benzo[k]fluoranthene Ave 1.3061.226 53200 50000 6.5 20.0

Benzo[a]pyrene Ave 1.0401.026 50700 50000 1.4 20.0

Indeno[1,2,3-cd]pyrene QuaF 0.83640.7933 48200 50000 -3.6 20.0

Dibenz(a,h)anthracene QuaF 0.85780.7885 48800 50000 -2.4 20.0

Benzo[g,h,i]perylene Ave 0.83710.8438 49600 50000 -0.8 20.0

2-Fluorophenol Ave 1.2601.347 46800 50000 -6.5 20.0

Phenol-d5 Ave 1.4161.519 46600 50000 -6.8 20.0

Nitrobenzene-d5 Ave 0.39200.3897 50300 50000 0.6 20.0

2-Fluorobiphenyl Ave 1.3981.459 47900 50000 -4.2 20.0

2,4,6-Tribromophenol Ave 0.15310.1325 57800 50000 15.5 20.0

Terphenyl-d14 Ave 1.1111.053 52800 50000 5.5 20.0

FORM VII 8270C

06/03/2010 of 623


TestAmerica

Data file : /chem/BNAMS10.i/8270/05-11-10a/11may10.b/p2720.dLab Smp Id: DFTPP-459998 Inj Date : 11-MAY-2010 13:45 Operator : BNA2 Inst ID: BNAMS10.iSmp Info : DFTPP-459998Misc Info : Comment : Method : /chem/BNAMS10.i/8270/05-11-10a/11may10.b/BNADFTPP.mMeth Date : 11-May-2010 15:12 monica Quant Type: ESTDCal Date : Cal File: Als bottle: 1 QC Sample: DFTPPDil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Sample Matrix: None

CONCENTRATIONS

ON-COL FINAL

RT EXP RT DLT RT MASS RESPONSE ( ug/L) ( ug/L) TARGET RANGE RATIO

== ====== ======== ==== ======== ======= ======= ============ =====

1 dftpp CAS #:

4.598 4.700 -0.102 198 19020 0.00- 100.00 100.00

4.598 4.700 -0.102 51 6950 30.00- 60.00 36.54

4.598 4.700 -0.102 68 0 0.00- 2.00 0.00

4.598 4.700 -0.102 69 7985 0.00- 0.00 41.98

4.598 4.700 -0.102 70 0 0.00- 2.00 0.00

4.598 4.700 -0.102 127 11097 40.00- 60.00 58.34

4.598 4.700 -0.102 197 0 0.00- 1.00 0.00

4.598 4.700 -0.102 199 1335 5.00- 9.00 7.02

4.598 4.700 -0.102 275 4924 10.00- 30.00 25.89

4.598 4.700 -0.102 365 607 1.00- 0.00 3.19

4.598 4.700 -0.102 441 2378 0.01- 100.00 74.17

4.598 4.700 -0.102 442 16043 40.00- 110.00 84.35

4.598 4.700 -0.102 443 3206 17.00- 23.00 19.98

-------------------------------------------------------------------------------

06/03/2010 of 623

Data File: p2720.d

Date: 11-MAY-2010 13:45

Client ID: Instrument: BNAMS10.i

Sample Info: DFTPP-459998 Operator: BNA2

06/03/2010 of 623

Data File: p2720.d

Date: 11-MAY-2010 13:45



1 dftpp


+-----+------------------------------------------+---------------------+| | | || 198 | Base Peak, 100% relative abundance | 100.00 || 51 | 30.00 - 60.00% of mass 198 | 36.54 || 68 | Less than 2.00% of mass 69 | 0.00 ( 0.00) || 69 | Mass 69 relative abundance | 41.98 || 70 | Less than 2.00% of mass 69 | 0.00 ( 0.00) || 127 | 40.00 - 60.00% of mass 198 | 58.34 || 197 | Less than 1.00% of mass 198 | 0.00 || 199 | 5.00 - 9.00% of mass 198 | 7.02 || 275 | 10.00 - 30.00% of mass 198 | 25.89 || 365 | Greater than 1.00% of mass 198 | 3.19 || 441 | 0.01 - 100.00% of mass 443 | 12.50 ( 74.17) || 442 | 40.00 - 110.00% of mass 198 | 84.35 || 443 | 17.00 - 23.00% of mass 442 | 16.86 ( 19.98) |+-----+------------------------------------------+---------------------+

06/03/2010 of 623

Data File: p2720.d

Date: 11-MAY-2010 13:45



Data File: /chem/BNAMS10.i/8270/05-11-10a/11may10.b/p2720.dSpectrum: Average Spectrum: 4.592 to 4.604 min.


m/z Y m/z Y m/z Y m/z Y+------------------+------------------+------------------+------------------+| 39.00 444 | 101.00 174 | 186.00 2833 | 255.00 10406 || 50.00 1808 | 107.00 2857 | 187.00 685 | 256.00 1531 || 51.00 6950 | 108.00 220 | 196.00 467 | 258.00 470 || 52.00 225 | 110.00 5297 | 198.00 19016 | 273.00 168 || 57.00 234 | 111.00 805 | 199.00 1335 | 274.00 760 |+------------------+------------------+------------------+------------------+| 69.00 7985 | 117.00 2136 | 204.00 509 | 275.00 4924 || 74.00 884 | 127.00 11097 | 205.00 1205 | 276.00 598 || 75.00 1287 | 128.00 799 | 206.00 5093 | 277.00 195 || 76.00 239 | 129.00 4311 | 207.00 562 | 296.00 1307 || 77.00 9450 | 130.00 186 | 217.00 1211 | 323.00 406 |+------------------+------------------+------------------+------------------+| 78.00 526 | 141.00 221 | 221.00 959 | 365.00 607 || 79.00 557 | 148.00 454 | 223.00 168 | 423.00 816 || 80.00 236 | 156.00 191 | 224.00 2581 | 441.00 2378 || 81.00 339 | 167.00 1072 | 225.00 536 | 442.00 16043 || 93.00 1057 | 168.00 466 | 227.00 1040 | 443.00 3206 |+------------------+------------------+------------------+------------------+| 98.00 858 | 179.00 579 | 244.00 2009 | || 99.00 701 | 180.00 209 | 246.00 183 | |+------------------+------------------+------------------+------------------+

06/03/2010 of 623


TestAmerica

Data file : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2877.dLab Smp Id: DFTPP-459998 Inj Date : 18-MAY-2010 10:12 Operator : BNA2 Inst ID: BNAMS10.iSmp Info : DFTPP-459998Misc Info : Comment : Method : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/BNADFTPP.mMeth Date : 11-May-2010 15:12 monica Quant Type: ESTDCal Date : Cal File: Als bottle: 1 QC Sample: DFTPPDil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Sample Matrix: NoneProcessing Host: hpd1

CONCENTRATIONS

ON-COL FINAL

RT EXP RT DLT RT MASS RESPONSE ( ug/L) ( ug/L) TARGET RANGE RATIO

== ====== ======== ==== ======== ======= ======= ============ =====

1 dftpp CAS #:

4.492 4.700 -0.208 198 33776 0.00- 100.00 98.20

4.492 4.700 -0.208 51 11271 30.00- 60.00 33.37

4.492 4.700 -0.208 68 0 0.00- 2.00 0.00

4.492 4.700 -0.208 69 12632 0.00- 0.00 37.40

4.492 4.700 -0.208 70 0 0.00- 2.00 0.00

4.492 4.700 -0.208 127 18545 40.00- 60.00 54.91

4.492 4.700 -0.208 197 0 0.00- 1.00 0.00

4.492 4.700 -0.208 199 2362 5.00- 9.00 6.99

4.492 4.700 -0.208 275 9158 10.00- 30.00 27.11

4.492 4.700 -0.208 365 1228 1.00- 0.00 3.64

4.492 4.700 -0.208 441 4875 0.01- 100.00 73.43

4.492 4.700 -0.208 442 34394 40.00- 110.00 101.83

4.492 4.700 -0.208 443 6639 17.00- 23.00 19.30

-------------------------------------------------------------------------------

06/03/2010 of 623

Data File: p2877.d

Date: 18-MAY-2010 10:12



06/03/2010 of 623

Data File: p2877.d

Date: 18-MAY-2010 10:12



1 dftpp


+-----+------------------------------------------+---------------------+| | | || 198 | Base Peak, 100% relative abundance | 100.00 || 51 | 30.00 - 60.00% of mass 198 | 33.37 || 68 | Less than 2.00% of mass 69 | 0.00 ( 0.00) || 69 | Mass 69 relative abundance | 37.40 || 70 | Less than 2.00% of mass 69 | 0.00 ( 0.00) || 127 | 40.00 - 60.00% of mass 198 | 54.91 || 197 | Less than 1.00% of mass 198 | 0.00 || 199 | 5.00 - 9.00% of mass 198 | 6.99 || 275 | 10.00 - 30.00% of mass 198 | 27.11 || 365 | Greater than 1.00% of mass 198 | 3.64 || 441 | 0.01 - 100.00% of mass 443 | 14.43 ( 73.43) || 442 | 40.00 - 110.00% of mass 198 | 101.83 || 443 | 17.00 - 23.00% of mass 442 | 19.66 ( 19.30) |+-----+------------------------------------------+---------------------+

06/03/2010 of 623

Data File: p2877.d

Date: 18-MAY-2010 10:12



Data File: /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2877.dSpectrum: Average Spectrum: 4.486 to 4.498 min.


m/z Y m/z Y m/z Y m/z Y+------------------+------------------+------------------+------------------+| 39.00 830 | 108.00 721 | 180.00 884 | 245.00 231 || 50.00 3241 | 110.00 8893 | 181.00 223 | 246.00 534 || 51.00 11271 | 111.00 1318 | 185.00 521 | 255.00 18960 || 52.00 568 | 117.00 3401 | 186.00 4726 | 256.00 2865 || 56.00 357 | 122.00 190 | 187.00 1373 | 258.00 998 |+------------------+------------------+------------------+------------------+| 57.00 682 | 123.00 451 | 192.00 396 | 265.00 201 || 63.00 480 | 127.00 18544 | 193.00 205 | 273.00 517 || 69.00 12632 | 128.00 1517 | 196.00 894 | 274.00 1789 || 74.00 1100 | 129.00 7249 | 198.00 33776 | 275.00 9158 || 75.00 2261 | 130.00 466 | 199.00 2362 | 276.00 1221 |+------------------+------------------+------------------+------------------+| 76.00 638 | 135.00 502 | 204.00 1271 | 277.00 803 || 77.00 15462 | 141.00 844 | 205.00 2193 | 296.00 2403 || 78.00 948 | 147.00 462 | 206.00 8503 | 297.00 171 || 79.00 883 | 148.00 825 | 207.00 1251 | 323.00 862 || 80.00 626 | 155.00 446 | 208.00 200 | 334.00 262 |+------------------+------------------+------------------+------------------+| 81.00 1026 | 156.00 671 | 211.00 171 | 365.00 1228 || 86.00 167 | 161.00 172 | 217.00 2081 | 372.00 232 || 93.00 1728 | 165.00 356 | 221.00 1660 | 423.00 1908 || 98.00 1197 | 167.00 1898 | 223.00 492 | 424.00 203 || 99.00 982 | 168.00 634 | 224.00 4614 | 441.00 4875 |+------------------+------------------+------------------+------------------+| 101.00 511 | 174.00 174 | 225.00 1208 | 442.00 34392 || 104.00 169 | 175.00 518 | 227.00 1851 | 443.00 6639 || 105.00 350 | 177.00 180 | 229.00 176 | 444.00 311 || 107.00 4880 | 179.00 1212 | 244.00 3469 | |+------------------+------------------+------------------+------------------+

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1

Lab Sample ID: MB 460-37564/1-A



Solid

TestAmerica Edison

Level: (low/med)


GPC Cleanup:(Y/N)

Date Analyzed:

Date Extracted:

Dilution Factor:

Extract. Method: 05/17/2010 09:00

1

3541

05/18/2010 10:57

Low

N

1(mL)

% Moisture:




Phenol108-95-2 330 330 40U

2-Chlorophenol95-57-8 330 330 44U

2-Nitrophenol88-75-5 330 330 54U





2,4-Dinitrophenol51-28-5 1000 1000 70U

4-Nitrophenol100-02-7 1000 1000 85U











Isophorone78-59-1 330 330 38U














Fluorene86-73-7 330 330 56U

FORM I 8270C

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1




Solid

TestAmerica Edison

Level: (low/med)


GPC Cleanup:(Y/N)

Date Analyzed:

Date Extracted:

Dilution Factor:

Extract. Method: 05/17/2010 09:00

1

3541

05/18/2010 10:57

Low

N

1(mL)

% Moisture:








Anthracene120-12-7 330 330 58U



Pyrene129-00-0 330 330 57U

Benzidine92-87-5 330 330 70U



Benzo[a]anthracene56-55-3 33 33 6.1U

Chrysene218-01-9 330 330 48U

Bis(2-ethylhexyl) phthalate117-81-7 330 330 44U










4165-60-0 Nitrobenzene-d5 80 38-105

4165-62-2 Phenol-d5 82 41-118

1718-51-0 Terphenyl-d14 93 16-151

118-79-6 2,4,6-Tribromophenol 82 10-120

367-12-4 2-Fluorophenol 76 37-125


FORM I 8270C

06/03/2010 of 623



Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1




Solid

TestAmerica Edison

Level: (low/med)


GPC Cleanup:(Y/N)

Date Analyzed:

Date Extracted:

Dilution Factor:

Extract. Method: 05/17/2010 09:00

1

3541

05/18/2010 10:57

Low

N

1(mL)

% Moisture:





Unknown Aldol Condensate-1 497 2.30 T A J

Unknown Aldol Condensate-2 16600 2.72 T A J

FORM I-TIC 8270C

06/03/2010 of 623


TestAmerica

SEMI-VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2879.dLab Smp Id: MB 460-37564/1-A Inj Date : 18-MAY-2010 10:57 Operator : BNAMS 4 Inst ID: BNAMS10.iSmp Info : MB 460-37564/1-AMisc Info : Comment : Method : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/8270C_08SP.mMeth Date : 18-May-2010 11:53 czhao Quant Type: ISTDCal Date : 11-MAY-2010 16:30 Cal File: p2726.dAls bottle: 3 QC Sample: BLANKDil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd1





CONCENTRATIONS



========================== ==== == ====== ====== ======== ======= =======


$ 17 Phenol-d5 (SUR) 99 3.850 3.862 (0.915) 606994 82.2603 5500


23 1,2-Dichlorobenzene 146 4.379 4.385 (1.040) 2312 0.30611 20(aH)


* 80 Naphthalene-d8 136 5.495 5.507 (1.000) 691224 40.0000


* 82 Acenaphthene-d10 164 7.258 7.264 (1.000) 369280 40.0000


* 83 Phenanthrene-d10 188 8.727 8.733 (1.000) 486284 40.0000

$ 78 Terphenyl-d14 244 10.307 10.307 (0.898) 326248 46.3329 3100

* 81 Chrysene-d12 240 11.482 11.494 (1.000) 267422 40.0000

* 84 Perylene-d12 264 13.398 13.404 (1.000) 185780 40.0000

06/03/2010 of 623


QC Flag Legend



06/03/2010 of 623


TestAmerica

SEMI-VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2879.dLab Smp Id: MB 460-37564/1-A Inj Date : 18-MAY-2010 10:57 Operator : BNAMS 4 Inst ID: BNAMS10.iSmp Info : MB 460-37564/1-AMisc Info : Comment : Method : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/8270C_08SP.mMeth Date : 18-May-2010 11:53 czhao Quant Type: ISTDCal Date : 11-MAY-2010 16:30 Cal File: p2726.dAls bottle: 3 QC Sample: BLANKDil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd1






* 79 1,4-Dichlorobenzene-d4 4.208 1159126 40.000



==== ==== ============= ============ ==== ======= ========= ======

Unknown Aldol Condensate-1 CAS #:

2.305 216311 7.46463068 500 0 0 79

Unknown Aldol Condensate-2 CAS #:

2.716 7203501 248.583797 16000 0 0 79

06/03/2010 of 623

Data File: p2879.d

Date: 18-MAY-2010 10:57


Sample Info: MB 460-37564/1-A Operator: BNAMS 4

06/03/2010 of 623

Data File: p2879.d

Date: 18-MAY-2010 10:57





Unknown Aldol Condensate-1

3-Hexen-2-one 763-93-9 NIST02.l 3109 91 C6H10O 98

3-Penten-2-one, 4-methyl- 141-79-7 NIST02.l 3185 91 C6H10O 98

06/03/2010 of 623

Data File: p2879.d

Date: 18-MAY-2010 10:57





Unknown Aldol Condensate-2

2-Pentanone, 4-hydroxy-4-methyl- 123-42-2 NIST02.l 7951 50 C6H12O2 116

(+-)-4-Amino-4,5-dihydro-2(3H)-fur 16504-58-8 NIST02.l 3966 47 C4H7NO2 101

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1

Lab Sample ID: LCS 460-37564/2-A



Solid

TestAmerica Edison

Level: (low/med)


GPC Cleanup:(Y/N)

Date Analyzed:

Date Extracted:

Dilution Factor:

Extract. Method: 05/17/2010 09:00

1

3541

05/18/2010 11:25

Low

N

1(mL)

% Moisture:




Phenol108-95-2 4950 330 41

2-Chlorophenol95-57-8 5140 330 44

2-Nitrophenol88-75-5 5640 330 54

2,4-Dimethylphenol105-67-9 5280 330 53

2,4-Dichlorophenol120-83-2 5340 330 53

4-Chloro-3-methylphenol59-50-7 5690 330 56

2,4,6-Trichlorophenol88-06-2 5360 330 59

2,4-Dinitrophenol51-28-5 1100 1000 70

4-Nitrophenol100-02-7 6490 1000 85

4,6-Dinitro-2-methylphenol534-52-1 2180 1000 160

Pentachlorophenol87-86-5 4830 1000 160

N-Nitrosodimethylamine62-75-9 2550 330 34

Bis(2-chloroethyl)ether111-44-4 3020 33 6.9

1,3-Dichlorobenzene541-73-1 2490 330 45



N-Nitrosodi-n-propylamine621-64-7 3040 33 4.4

Hexachloroethane67-72-1 2480 33 5.6

Nitrobenzene98-95-3 2640 33 7.4

Isophorone78-59-1 2850 330 38

Bis(2-chloroethoxy)methane111-91-1 2860 330 47

1,2,4-Trichlorobenzene120-82-1 2740 33 5.4

Naphthalene91-20-3 2710 330 48

Hexachlorobutadiene87-68-3 2710 67 13

Hexachlorocyclopentadiene77-47-4 3110 330 97

2-Chloronaphthalene91-58-7 2700 330 47

Dimethyl phthalate131-11-3 2960 330 45

Acenaphthylene208-96-8 2780 330 47

2,6-Dinitrotoluene606-20-2 3130 67 8.4

Acenaphthene83-32-9 2840 330 47

2,4-Dinitrotoluene121-14-2 3200 67 9.7

Diethyl phthalate84-66-2 3000 330 44

4-Chlorophenyl phenyl ether7005-72-3 2910 330 57

Fluorene86-73-7 2890 330 56

FORM I 8270C

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1




Solid

TestAmerica Edison

Level: (low/med)


GPC Cleanup:(Y/N)

Date Analyzed:

Date Extracted:

Dilution Factor:

Extract. Method: 05/17/2010 09:00

1

3541

05/18/2010 11:25

Low

N

1(mL)

% Moisture:




N-Nitrosodiphenylamine86-30-6 3110 330 54

4-Bromophenyl phenyl ether101-55-3 2910 330 59

Hexachlorobenzene118-74-1 2940 33 4.6

Phenanthrene85-01-8 2850 330 58

Anthracene120-12-7 2870 330 58

Di-n-butyl phthalate84-74-2 2980 330 51

Fluoranthene206-44-0 3040 330 55

Pyrene129-00-0 2850 330 57

Benzidine92-87-5 169 330 70J

Butyl benzyl phthalate85-68-7 3010 330 39

3,3'-Dichlorobenzidine91-94-1 2870 670 73


Chrysene218-01-9 2900 330 48

Bis(2-ethylhexyl) phthalate117-81-7 3010 330 44

Di-n-octyl phthalate117-84-0 3130 330 39



Benzo[a]pyrene50-32-8 2590 33 4.1

Indeno[1,2,3-cd]pyrene193-39-5 2870 33 5.3



bis (2-chloroisopropyl) ether108-60-1 2700 330 43


4165-60-0 Nitrobenzene-d5 82 38-105

4165-62-2 Phenol-d5 78 41-118

1718-51-0 Terphenyl-d14 89 16-151

118-79-6 2,4,6-Tribromophenol 99 10-120

367-12-4 2-Fluorophenol 74 37-125


FORM I 8270C

06/03/2010 of 623


TestAmerica

SEMI-VOLATILE ORGANIC COMPOUND ANALYSISData file : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/p2880.dLab Smp Id: LCS 460-37564/2-A Inj Date : 18-MAY-2010 11:25 Operator : BNAMS 4 Inst ID: BNAMS10.iSmp Info : LCS 460-37564/2-AMisc Info : Comment : Method : /chem/BNAMS10.i/8270/05-11-10a/18may10.b/8270C_08SP.mMeth Date : 18-May-2010 11:53 czhao Quant Type: ISTDCal Date : 11-MAY-2010 16:30 Cal File: p2726.dAls bottle: 4 QC Sample: BSDil Factor: 1.00000 Integrator: HP RTE Compound Sublist: all.subTarget Version: 3.50 Processing Host: hpd1





CONCENTRATIONS



========================== ==== == ====== ====== ======== ======= =======

106 1,4-Dioxane 88 1.658 1.576 (0.190) 43993 14.6436 980

19 N-Nitrosodimethylamine 74 1.864 1.799 (0.442) 128281 38.2990 2600

71 Pyridine 79 1.893 1.829 (0.449) 167336 27.1048 1800


110 Benzaldehyde 77 3.773 3.768 (0.895) 49396 18.4739 1200

73 Aniline 93 3.885 3.885 (0.922) 252934 30.2868 2000

$ 17 Phenol-d5 (SUR) 99 3.862 3.862 (0.916) 520486 77.9028 5200

1 Phenol 94 3.879 3.874 (0.921) 533237 74.2322 4900

20 bis(2-Chloroethyl)ether 93 3.950 3.950 (0.937) 233807 45.2557 3000

2 2-Chlorophenol 128 4.009 4.009 (0.951) 481959 77.0624 5100




06/03/2010 of 623


CONCENTRATIONS



========================== ==== == ====== ====== ======== ======= =======

74 Benzyl Alcohol 108 4.355 4.361 (1.033) 157889 44.4117 3000


24 bis (2-chloroisopropyl) ether 45 4.490 4.496 (1.066) 227997 40.5580 2700

3 2-Methylphenol 108 4.473 4.479 (1.061) 390670 77.1847 5100

126 O-Toluidine 107 4.637 4.643 (1.100) 494679 44.1477 2900

104 Acetophenone 105 4.625 4.631 (1.098) 278784 39.1234 2600

25 N-Nitroso-di-n-propylamine 70 4.655 4.637 (1.105) 153582 45.5830 3000(M)

4 4-Methylphenol 108 4.637 4.643 (1.100) 398603 77.3341 5200

123 3 & 4 Methylphenol 108 4.637 4.643 (1.100) 398603 77.2164 5100

26 Hexachloroethane 117 4.725 4.731 (1.121) 99166 37.1507 2500


27 Nitrobenzene 77 4.796 4.802 (0.872) 303507 39.6708 2600

107 N,N-Dimethylaniline 120 4.802 4.808 (1.139) 339983 38.3526 2600

28 Isophorone 82 5.048 5.043 (0.918) 416526 42.7680 2800

5 2-Nitrophenol 139 5.119 5.119 (0.931) 261772 84.5523 5600

6 2,4-Dimethylphenol 122 5.172 5.172 (0.940) 390619 79.2531 5300

29 bis(2-Chloroethoxy)methane 93 5.260 5.266 (0.956) 257509 42.8542 2800

15 Benzoic Acid 122 5.284 5.313 (0.960) 47906 22.2915 1500

7 2,4-Dichlorophenol 162 5.366 5.366 (0.975) 345292 80.0479 5300


* 80 Naphthalene-d8 136 5.501 5.507 (1.000) 596977 40.0000

31 Naphthalene 128 5.524 5.525 (1.004) 680965 40.6236 2700

32 4-Chloroaniline 127 5.577 5.583 (1.014) 191385 29.8547 2000


111 Caprolactam 113 5.965 5.965 (1.084) 44462 36.0755 2400

8 4-Chloro-3-methylphenol 107 6.088 6.089 (1.107) 358022 85.4076 5700

34 2-Methylnaphthalene 142 6.218 6.224 (1.130) 431229 43.3529 2900

35 Hexachlorocyclopentadiene 237 6.388 6.388 (0.879) 115168 46.6046 3100

9 2,4,6-Trichlorophenol 196 6.512 6.512 (0.896) 232769 80.4132 5400

10 2,4,5-Trichlorophenol 196 6.553 6.553 (0.902) 229952 81.2645 5400


36 2-Chloronaphthalene 162 6.711 6.711 (0.924) 377950 40.5657 2700

102 Diphenyl 154 6.694 6.694 (0.922) 493491 42.4363 2800

103 Diphenyl Ether 170 6.794 6.800 (0.935) 276484 40.8990 2700

37 2-Nitroaniline 65 6.811 6.817 (0.938) 120656 43.7422 2900

38 Dimethylphthalate 163 6.999 7.005 (0.964) 401548 44.4747 3000

40 2,6-Dinitrotoluene 165 7.052 7.058 (0.971) 98206 46.9978 3100

39 Acenaphthylene 152 7.117 7.123 (0.980) 619163 41.6855 2800

41 3-Nitroaniline 138 7.222 7.223 (0.994) 78823 35.7801 2400

* 82 Acenaphthene-d10 164 7.264 7.264 (1.000) 306055 40.0000

42 Acenaphthene 154 7.293 7.299 (1.004) 352666 42.5846 2800

11 2,4-Dinitrophenol 184 7.322 7.328 (1.008) 13497 16.4582 1100

12 4-Nitrophenol 65 7.399 7.399 (1.019) 118788 97.3840 6500

43 Dibenzofuran 168 7.463 7.469 (1.028) 507113 42.3302 2800

44 2,4-Dinitrotoluene 165 7.452 7.458 (1.026) 115161 48.0253 3200

45 Diethylphthalate 149 7.698 7.704 (1.060) 378635 45.0233 3000

47 Fluorene 166 7.804 7.810 (1.074) 382181 43.2890 2900

06/03/2010 of 623


CONCENTRATIONS



========================== ==== == ====== ====== ======== ======= =======

46 4-Chlorophenyl-phenylether 204 7.804 7.810 (1.074) 172113 43.6381 2900

48 4-Nitroaniline 138 7.828 7.834 (1.078) 76473 41.2995 2800

13 4,6-Dinitro-2-methylphenol 198 7.857 7.863 (0.900) 35370 32.6973 2200

49 N-Nitrosodiphenylamine 169 7.922 7.928 (0.908) 290812 46.6150 3100

75 1,2-Diphenylhydrazine 77 7.963 7.963 (0.912) 413314 39.1939 2600


50 4-Bromophenyl-phenylether 248 8.286 8.292 (0.950) 101793 43.7193 2900

51 Hexachlorobenzene 284 8.356 8.357 (0.958) 106397 44.0462 2900

112 Atrazine 200 8.456 8.456 (0.969) 73116 40.3179 2700

14 Pentachlorophenol 266 8.550 8.550 (0.980) 81672 72.4759 4800

* 83 Phenanthrene-d10 188 8.727 8.733 (1.000) 392818 40.0000

52 Phenanthrene 178 8.750 8.756 (1.003) 477490 42.7720 2800

53 Anthracene 178 8.803 8.803 (1.009) 481158 43.1018 2900

54 Carbazole 167 8.962 8.962 (1.027) 405210 43.2382 2900

55 Di-n-butylphthalate 149 9.308 9.308 (1.067) 496960 44.6354 3000

56 Fluoranthene 202 9.925 9.925 (1.137) 403388 45.5680 3000

58 Benzidine 184 10.054 10.055 (1.152) 3394 2.53069 170(aR)

57 Pyrene 202 10.149 10.149 (0.883) 396245 42.6752 2800

$ 78 Terphenyl-d14 244 10.307 10.307 (0.897) 258602 44.5578 3000

59 Butylbenzylphthalate 149 10.830 10.830 (0.943) 164505 45.1765 3000


60 3,3'-Dichlorobenzidine 252 11.447 11.447 (0.996) 73696 42.9941 2900

* 81 Chrysene-d12 240 11.488 11.494 (1.000) 220418 40.0000

62 Chrysene 228 11.523 11.524 (1.003) 243635 43.4486 2900

63 bis(2-Ethylhexyl)phthalate 149 11.523 11.524 (1.003) 206823 45.2018 3000

64 Di-n-octylphthalate 149 12.381 12.381 (0.924) 301629 46.9031 3100


66 Benzo(k)fluoranthene 252 12.916 12.922 (0.964) 226488 44.7897 3000

67 Benzo(a)pyrene 252 13.321 13.327 (0.994) 164335 38.8351 2600

* 84 Perylene-d12 264 13.404 13.404 (1.000) 164936 40.0000

68 Indeno(1,2,3-cd)pyrene 276 14.908 14.908 (1.112) 153171 43.0472 2900

69 Dibenz(a,h)anthracene 278 14.943 14.943 (1.115) 157066 43.5201 2900

70 Benzo(g,h,i)perylene 276 15.319 15.319 (1.143) 155445 44.6788 3000

QC Flag Legend


R - Spike/Surrogate failed recovery limits.M - Compound response manually integrated.

06/03/2010 of 623

Data File: p2880.d

Date: 18-MAY-2010 11:25


Sample Info: LCS 460-37564/2-A Operator: BNAMS 4

06/03/2010 of 623

Manual Integration Report

Data File: p2880.dInj. Date and Time: 18-MAY-2010 11:25Instrument ID: BNAMS10.iClient ID: Compound: 25 N-Nitroso-di-n-propylamineCAS #: 621-64-7Report Date: 05/19/2010

Processing Integration Results

RT: 4.63

Response: 92099

Amount: 27

Conc: 1822

Manual Integration Results

RT: 4.65

Response: 153582

Amount: 46

Conc: 3039

Manually Integrated By: wahiedManual Integration Reason: Target Peak Misintegrated (extraneous area removed)

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-1 2-3 MS

SDG No.:

460-13139-1

Lab Sample ID: 460-13139-5 MS



Soil

TestAmerica Edison

05/12/2010 11:25

Level: (low/med)


GPC Cleanup:(Y/N)

Date Analyzed:

Date Extracted:

Dilution Factor:

Extract. Method: 05/17/2010 09:00

1

3541

05/18/2010 12:18

Low

N

1(mL)

% Moisture: 6.5




Phenol108-95-2 5410 350 43

2-Chlorophenol95-57-8 5430 350 47

2-Nitrophenol88-75-5 5770 350 58

2,4-Dimethylphenol105-67-9 5560 350 57

2,4-Dichlorophenol120-83-2 5660 350 57



2,4-Dinitrophenol51-28-5 1100 1100 75U

4-Nitrophenol100-02-7 4630 1100 91

4,6-Dinitro-2-methylphenol534-52-1 191 1100 170J









Nitrobenzene98-95-3 2690 35 7.9

Isophorone78-59-1 2980 350 41



Naphthalene91-20-3 2740 350 52






2,6-Dinitrotoluene606-20-2 3210 71 9.0

Acenaphthene83-32-9 2980 350 50

2,4-Dinitrotoluene121-14-2 3110 71 10



Fluorene86-73-7 2970 350 60

FORM I 8270C

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-1 2-3 MS

SDG No.:

460-13139-1

Lab Sample ID: 460-13139-5 MS



Soil

TestAmerica Edison

05/12/2010 11:25

Level: (low/med)


GPC Cleanup:(Y/N)

Date Analyzed:

Date Extracted:

Dilution Factor:

Extract. Method: 05/17/2010 09:00

1

3541

05/18/2010 12:18

Low

N

1(mL)

% Moisture: 6.5







Phenanthrene85-01-8 2930 350 62

Anthracene120-12-7 2970 350 62


Fluoranthene206-44-0 3030 350 59

Pyrene129-00-0 3110 350 61

Benzidine92-87-5 89.3 350 75J




Chrysene218-01-9 3100 350 51





Benzo[a]pyrene50-32-8 2660 35 4.3

Indeno[1,2,3-cd]pyrene193-39-5 3110 35 5.6





4165-60-0 Nitrobenzene-d5 80 38-105

4165-62-2 Phenol-d5 79 41-118

1718-51-0 Terphenyl-d14 91 16-151

118-79-6 2,4,6-Tribromophenol 67 10-120

367-12-4 2-Fluorophenol 74 37-125


FORM I 8270C

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-1 2-3 MSD

SDG No.:

460-13139-1

Lab Sample ID: 460-13139-5 MSD



Soil

TestAmerica Edison

05/12/2010 11:25

Level: (low/med)


GPC Cleanup:(Y/N)

Date Analyzed:

Date Extracted:

Dilution Factor:

Extract. Method: 05/17/2010 09:00

1

3541

05/18/2010 12:46

Low

N

1(mL)

% Moisture: 6.5




Phenol108-95-2 5170 350 43

2-Chlorophenol95-57-8 5350 350 47

2-Nitrophenol88-75-5 5620 350 58

2,4-Dimethylphenol105-67-9 5370 350 57

2,4-Dichlorophenol120-83-2 5440 350 57



2,4-Dinitrophenol51-28-5 1100 1100 75U

4-Nitrophenol100-02-7 4630 1100 91










Nitrobenzene98-95-3 2700 35 7.9

Isophorone78-59-1 2900 350 41



Naphthalene91-20-3 2780 350 52






2,6-Dinitrotoluene606-20-2 3200 72 9.0

Acenaphthene83-32-9 2970 350 50

2,4-Dinitrotoluene121-14-2 3150 72 10



Fluorene86-73-7 3020 350 60

FORM I 8270C

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-1 2-3 MSD

SDG No.:

460-13139-1

Lab Sample ID: 460-13139-5 MSD



Soil

TestAmerica Edison

05/12/2010 11:25

Level: (low/med)


GPC Cleanup:(Y/N)

Date Analyzed:

Date Extracted:

Dilution Factor:

Extract. Method: 05/17/2010 09:00

1

3541

05/18/2010 12:46

Low

N

1(mL)

% Moisture: 6.5







Phenanthrene85-01-8 3030 350 62

Anthracene120-12-7 3040 350 62


Fluoranthene206-44-0 3230 350 59

Pyrene129-00-0 2980 350 61

Benzidine92-87-5 131 350 75J




Chrysene218-01-9 3080 350 51





Benzo[a]pyrene50-32-8 2720 35 4.3

Indeno[1,2,3-cd]pyrene193-39-5 3150 35 5.6





4165-60-0 Nitrobenzene-d5 81 38-105

4165-62-2 Phenol-d5 75 41-118

1718-51-0 Terphenyl-d14 89 16-151

118-79-6 2,4,6-Tribromophenol 66 10-120

367-12-4 2-Fluorophenol 72 37-125


FORM I 8270C

06/03/2010 of 623

Lab Name: Job No.:

SDG No.:

Instrument ID:


GC/MS SEMI VOA ANALYSIS RUN LOG

DILUTION

FACTOR



BNAMS10

37184

Start Date:

End Date: 05/11/2010 16:30

05/11/2010 13:45

DFTPP 460-37184/1 Rtx-5MS 0.25(mm)105/11/2010 13:45 p2720.d

ICIS 460-37184/2 Rtx-5MS 0.25(mm)105/11/2010 14:17 p2721.d

IC 460-37184/3 Rtx-5MS 0.25(mm)105/11/2010 14:43 p2722.d

IC 460-37184/4 Rtx-5MS 0.25(mm)105/11/2010 15:10 p2723.d

IC 460-37184/5 Rtx-5MS 0.25(mm)105/11/2010 15:36 p2724.d

IC 460-37184/6 Rtx-5MS 0.25(mm)105/11/2010 16:03 p2725.d

IC 460-37184/7 Rtx-5MS 0.25(mm)105/11/2010 16:30 p2726.d

8270C

06/03/2010 of 623

Lab Name: Job No.:

SDG No.:

Instrument ID:


GC/MS SEMI VOA ANALYSIS RUN LOG

DILUTION

FACTOR



BNAMS10

37818

Start Date:

End Date: 05/18/2010 20:25

05/18/2010 10:12

DFTPP 460-37818/1 Rtx-5MS 0.25(mm)105/18/2010 10:12 p2877.d

CCVIS 460-37818/2 Rtx-5MS 0.25(mm)105/18/2010 10:30 p2878.d

MB 460-37564/1-A Rtx-5MS 0.25(mm)105/18/2010 10:57 p2879.d

LCS 460-37564/2-A Rtx-5MS 0.25(mm)105/18/2010 11:25 p2880.d

460-13139-5 TB-1 2-3 Rtx-5MS 0.25(mm)105/18/2010 11:52 p2881.d

460-13139-5 MS TB-1 2-3 MS Rtx-5MS 0.25(mm)105/18/2010 12:18 p2882.d

460-13139-5 MSD TB-1 2-3 MSD Rtx-5MS 0.25(mm)105/18/2010 12:46 p2883.d

ZZZZZ Rtx-5MS 0.25(mm)105/18/2010 13:12

ZZZZZ Rtx-5MS 0.25(mm)105/18/2010 13:39

ZZZZZ Rtx-5MS 0.25(mm)105/18/2010 14:06

ZZZZZ Rtx-5MS 0.25(mm)105/18/2010 14:33

460-13139-2 TB-3 6-7 Rtx-5MS 0.25(mm)105/18/2010 15:00 p2888.d

ZZZZZ Rtx-5MS 0.25(mm)105/18/2010 15:27

ZZZZZ Rtx-5MS 0.25(mm)10005/18/2010 15:54

ZZZZZ Rtx-5MS 0.25(mm)505/18/2010 16:21

ZZZZZ Rtx-5MS 0.25(mm)505/18/2010 16:48

ZZZZZ Rtx-5MS 0.25(mm)505/18/2010 17:16

ZZZZZ Rtx-5MS 0.25(mm)205/18/2010 17:42

ZZZZZ Rtx-5MS 0.25(mm)105/18/2010 18:10

ZZZZZ Rtx-5MS 0.25(mm)505/18/2010 18:36

ZZZZZ Rtx-5MS 0.25(mm)105/18/2010 19:03

ZZZZZ Rtx-5MS 0.25(mm)105/18/2010 19:30

460-13139-7 TB-5 3-4 Rtx-5MS 0.25(mm)105/18/2010 19:58 p2899.d

460-13139-4 TB-2 5-6 Rtx-5MS 0.25(mm)105/18/2010 20:25 p2900.d

8270C

06/03/2010 of 623

Organic Prep Worksheet

Method: 3541

Analyst: Masongo, Charles


Batch End:

May 17 2010 9:00AM

May 17 2010 3:00PM


sample

Position on the

SoxTherm

OP_Acid_SU_00010 OP_BN_SU_00010 OP8270SP_00012Initial weight/volume of

sample

Method Chain

MB~460-37564/1 15.02 g 1 mL 500 uL500 uL1033541, 8270C

LCS~460-37564/2 15.00 g 1 mL 500 uL500 uL500 uL1043541, 8270C

460-13139-E-5~MS TB-1 2-3 T 15.04 g 1 mL 500 uL500 uL500 uL1053541, 8270C

460-13139-E-5~MS

D

TB-1 2-3 T 15.03 g 1 mL 500 uL500 uL500 uL1063541, 8270C

460-13139-E-1 TB-3 2-3 15.00 g 1 mL 500 uL500 uL107

460-13139-E-2 TB-3 6-7 T 15.00 g 1 mL 500 uL500 uL1083541, 8270C

460-13139-E-3 TB-2 2-3 14.99 g 1 mL 500 uL500 uL109

460-13139-E-4 TB-2 5-6 T 15.05 g 1 mL 500 uL500 uL1103541, 8270C

460-13139-E-5 TB-1 2-3 T 15.02 g 1 mL 500 uL500 uL1113541, 8270C

460-13139-E-6 TB-1 5-6 15.02 g 1 mL 500 uL500 uL112

460-13139-E-7 TB-5 3-4 T 15.01 g 1 mL 500 uL500 uL1133541, 8270C

460-13139-E-8 TB-4 6-7 15.04 g 1 mL 500 uL500 uL114

460-13211-F-1 T 15.00 g 1 mL 500 uL500 uL1

460-13211-E-2 T 15.00 g 1 mL 500 uL500 uL2

First Start time: 9am

Person's name who did the prep: CM

Person's name who witnessed reagent drop: JR

First End time: 3pm

SOP Number: 3541

Balance ID: 28

Person's name who did the concentration: CM

Na2SO4 Lot Number: H52600

Solvent: MeCl2/Acetone mixture

Vendor lot number: G49E31

Blank Soil Lot Number: H52600

06/03/2010 of 623


Method: 3541

Analyst: Masongo, Charles


Batch End:

May 17 2010 9:00AM

May 17 2010 3:00PM

Lab ID Client ID Basis

Comments

Analysis commentMethod Chain

MB~460-37564/1 3541, 8270C

LCS~460-37564/2 3541, 8270C

460-13139-E-5~MS TB-1 2-3 T3541, 8270C

460-13139-E-5~MS

D

TB-1 2-3 T3541, 8270C

460-13139-E-1 TB-3 2-3

460-13139-E-2 TB-3 6-7 T3541, 8270C

460-13139-E-3 TB-2 2-3

460-13139-E-4 TB-2 5-6 T3541, 8270C

460-13139-E-5 TB-1 2-3 T3541, 8270C

460-13139-E-6 TB-1 5-6

460-13139-E-7 TB-5 3-4 T3541, 8270C

460-13139-E-8 TB-4 6-7

460-13211-F-1 T

460-13211-E-2 T

Batch Comment: BNA 8270C SOIL

06/03/2010 of 623

Method 8081AOrganochlorine Pesticides (GC) by

Method 8081A

06/03/2010 of 623

FORM II

GC SEMI VOA SURROGATE RECOVERY


SDG No.:


TestAmerica Edison

GC Column (1): ID: (mm) GC Column (2): ID: (mm)CLP-2 0.53 CLP-1 0.53

#Lab Sample IDClient Sample ID # # #TCX1 TCX2 DCB1 DCB2

460-13139-2TB-3 6-7 115 112 125 105

460-13139-4TB-2 5-6 121 106 155 168 X

460-13139-5TB-1 2-3 117 113 138 118

460-13139-7TB-5 3-4 84 76 78 75

MB 460-37420/1-A 76 75 145 118

LCS 460-37420/2-A

75 71 93 92

460-13147-A-2-B MS

107 94 132 123

460-13147-A-2-C MSD

101 91 147 56 p

QC LIMITSQC LIMITSTCX = Tetrachloro-m-xylene 22-141


FORM II 8081A


06/03/2010 of 623

GC SEMI VOA LAB CONTROL SAMPLE RECOVERY

FORM III

Job No.:Lab Name:

SDG No.:


Low

460-13139-1

Lab File ID: xf108820.dSolid


TestAmerica Edison

REC

%

REC

QC

LIMITSCONCENTRATION

(ug/Kg)

SPIKE

ADDED

(ug/Kg)

#

LCS LCS

COMPOUND

Aldrin 133 88.9 32-15267

alpha-BHC 133 96.3 41-14572

beta-BHC 133 104 28-15578

delta-BHC 133 121 31-15491

gamma-BHC (Lindane) 133 98.6 33-15274

4,4'-DDD 133 94.7 50-15471

4,4'-DDE 133 98.1 47-15074

4,4'-DDT 133 99.1 39-15474

Dieldrin 133 88.6 40-14766

Endosulfan I 133 93.6 42-14770

Endosulfan II 133 101 32-15076

Endosulfan sulfate 133 103 37-14377

Endrin 133 101 44-14976

Endrin aldehyde 133 103 34-14278

Heptachlor 133 93.0 32-15270

Heptachlor epoxide 133 97.0 33-14973

FORM III 8081A


06/03/2010 of 623


FORM III

Job No.:Lab Name:

SDG No.:


Low

460-13139-1

Lab File ID: xr108820.dSolid


TestAmerica Edison

REC

%

REC

QC

LIMITSCONCENTRATION

(ug/Kg)

SPIKE

ADDED

(ug/Kg)

#

LCS LCS

COMPOUND

Aldrin 133 82.2 32-15262

alpha-BHC 133 89.0 41-14567

beta-BHC 133 102 28-15576

delta-BHC 133 109 31-15482

gamma-BHC (Lindane) 133 90.2 33-15268

4,4'-DDD 133 93.4 50-15470

4,4'-DDE 133 94.8 47-15071

4,4'-DDT 133 97.2 39-15473

Dieldrin 133 89.6 40-14767

Endosulfan I 133 93.3 42-14770

Endosulfan II 133 101 32-15075

Endosulfan sulfate 133 101 37-14376

Endrin 133 104 44-14978

Endrin aldehyde 133 104 34-14278

Heptachlor 133 87.2 32-15265

Heptachlor epoxide 133 93.5 33-14970

FORM III 8081A


06/03/2010 of 623

GC SEMI VOA MATRIX SPIKE RECOVERY

FORM III

Job No.:Lab Name:

SDG No.:


Low

460-13139-1


Lab ID: 460-13147-A-2-B MS Client ID:

TestAmerica Edison

LIMITS

COMPOUND

CONCENTRATION %

REC

QC

REC

SAMPLE

CONCENTRATION

SPIKE

ADDED


#

MS MS

153 151 32-152Aldrin 997.7 U

153 154 41-145alpha-BHC 1007.7 U

153 153 28-155beta-BHC 1007.7 U

153 167 31-154delta-BHC 1097.7 U

153 155 33-152gamma-BHC (Lindane) 1017.7 U

153 159 50-1544,4'-DDD 1047.7 U

153 169 47-1504,4'-DDE 1107.7 U

153 162 39-1544,4'-DDT 1026.4 J

153 150 40-147Dieldrin 987.7 U

153 144 42-147Endosulfan I 947.7 U

153 152 32-150Endosulfan II 997.7 U

153 147 37-143Endosulfan sulfate 967.7 U

153 168 44-149Endrin 1097.7 U

153 145 34-142Endrin aldehyde 957.7 U

153 139 32-152Heptachlor 917.7 U

153 149 33-149Heptachlor epoxide 977.7 U

FORM III 8081A


06/03/2010 of 623


FORM III

Job No.:Lab Name:

SDG No.:


Low

460-13139-1



TestAmerica Edison

LIMITS

COMPOUND

CONCENTRATION %

REC

QC

REC

SAMPLE

CONCENTRATION

SPIKE

ADDED


#

MS MS

153 127 32-152Aldrin 837.7 U

153 129 41-145alpha-BHC 857.7 U

153 128 28-155beta-BHC 847.7 U

153 142 31-154delta-BHC 937.7 U

153 130 33-152gamma-BHC (Lindane) 857.7 U

153 134 50-1544,4'-DDD 877.7 U

153 135 47-1504,4'-DDE 887.7 U

153 131 39-1544,4'-DDT 824.8 J

153 128 40-147Dieldrin 837.7 U

153 135 42-147Endosulfan I 887.7 U

153 123 32-150Endosulfan II 807.7 U

153 118 37-143Endosulfan sulfate 777.7 U

153 148 44-149Endrin 967.7 U

153 116 34-142Endrin aldehyde 767.7 U

153 137 32-152Heptachlor 907.7 U

153 132 33-149Heptachlor epoxide 867.7 U

FORM III 8081A


06/03/2010 of 623

GC SEMI VOA MATRIX SPIKE DUPLICATE RECOVERY

FORM III

Job No.:Lab Name:

SDG No.:


Low

460-13139-1


Lab ID: 460-13147-A-2-C MSD Client ID:

TestAmerica Edison

COMPOUND

SPIKE


REC

%

RPD

QC LIMITS


#

MSD MSD

153 145 30 32-152Aldrin 495

153 145 30 41-145alpha-BHC 694

153 144 30 28-155beta-BHC 694

153 159 30 31-154delta-BHC 5103

153 147 30 33-152gamma-BHC (Lindane) 596

153 156 30 50-1544,4'-DDD 2102

153 161 30 47-1504,4'-DDE 5105

153 150 30 39-1544,4'-DDT 894

153 140 30 40-147Dieldrin 791

153 137 30 42-147Endosulfan I 589

153 145 30 32-150Endosulfan II 595

153 147 30 37-143Endosulfan sulfate 096

153 163 30 44-149Endrin 3106

153 137 30 34-142Endrin aldehyde 689

153 125 30 32-152Heptachlor 1082

153 140 30 33-149Heptachlor epoxide 692

FORM III 8081A


06/03/2010 of 623


FORM III

Job No.:Lab Name:

SDG No.:


Low

460-13139-1



TestAmerica Edison

COMPOUND

SPIKE


REC

%

RPD

QC LIMITS


#

MSD MSD

153 122 30 32-152Aldrin 480

153 122 30 41-145alpha-BHC 680

153 125 30 28-155beta-BHC 282

153 134 30 31-154delta-BHC 687

153 121 30 33-152gamma-BHC (Lindane) 779

153 118 30 50-1544,4'-DDD 1377

153 122 30 47-1504,4'-DDE 1179

153 118 30 39-1544,4'-DDT 1074

153 120 30 40-147Dieldrin 778

153 126 30 42-147Endosulfan I 782

153 113 30 32-150Endosulfan II 874

153 109 30 37-143Endosulfan sulfate 871

153 133 30 44-149Endrin 1087

153 95.9 30 34-142Endrin aldehyde 1963

153 122 30 32-152Heptachlor 1279

153 122 30 33-149Heptachlor epoxide 879

FORM III 8081A


06/03/2010 of 623

FORM IV

GC SEMI VOA METHOD BLANK SUMMARY

Lab Name:

SDG No.:


Date Analyzed:(1)

Instrument ID:(1)

GC Column:(1) ID:

Instrument ID:(2)

Date Extracted: 05/14/2010 09:15

Date Analyzed:(2)

GC Column:(2) ID:CLP-10.53(mm) 0.53(mm)

PESTGC1

05/17/2010 09:37

Lab File ID:(1) Lab File ID:(2)

Matrix: Solid

xr108835.d


xf108835.d

05/17/2010 09:37

PESTGC1

CLP-2


ANALYZED 2

DATEDATE

ANALYZED 1LAB SAMPLE IDCLIENT SAMPLE ID

LCS 460-37420/2-A 05/17/2010 05:43 05/17/2010 05:43

460-13147-A-2-B MS 05/17/2010 06:36 05/17/2010 06:36

460-13147-A-2-C MSD 05/17/2010 06:50 05/17/2010 06:50

460-13139-2TB-3 6-7 05/17/2010 08:00 05/17/2010 08:00

460-13139-4TB-2 5-6 05/17/2010 08:27 05/17/2010 08:27

460-13139-5TB-1 2-3 05/17/2010 08:41 05/17/2010 08:41

460-13139-7TB-5 3-4 05/17/2010 09:09 05/17/2010 09:09

FORM IV 8081A

06/03/2010 of 623

PESTICIDES ANALYTICAL SEQUENCE

Lab Name: Job No.:

SDG No.:

FORM VIII


Calibration ID:

Calibration Start Date:Instrument ID: PESTGC1

GC Column:

6135

Calibration End Date:

05/11/2010 12:47

05/11/2010 13:42CLP-2 ID: 0.53(mm)

THE ANALYTICAL SEQUENCE OF BLANKS, SAMPLES, STANDARDS, MS/MSDs AND LCSs IS GIVEN BELOW:

# #RT RT

TCX DCB

UPPER LIMIT

LOWER LIMIT

2.34

2.24

10.43

10.23

SURROGATE RT FROM CONTINUING CALIBRATION 2.29 10.33

LAB SAMPLE ID DATE ANALYZEDCLIENT SAMPLE ID LAB FILE ID

CCVRT 460-37575/5 05/17/2010 05:29 2.29 10.33xf108819.d

LCS 460-37420/2-A 05/17/2010 05:43 2.30 10.34xf108820.d

460-13147-A-2-B MS 05/17/2010 06:36 2.29 10.33xf108822.d

460-13147-A-2-C MSD 05/17/2010 06:50 2.29 10.33xf108823.d

460-13139-2 05/17/2010 08:00 2.29 10.33TB-3 6-7 xf108828.d

460-13139-4 05/17/2010 08:27 2.29 10.33TB-2 5-6 xf108830.d

460-13139-5 05/17/2010 08:41 2.28 10.33TB-1 2-3 xf108831.d

460-13139-7 05/17/2010 09:09 2.29 10.33TB-5 3-4 xf108833.d

MB 460-37420/1-A 05/17/2010 09:37 2.28 10.33xf108835.d

CCV 460-37575/23 05/17/2010 10:04 2.29 10.33xf108837.d

TCX = Tetrachloro-m-xylene

DCB = DCB Decachlorobiphenyl

TCX RT Limit = ± 0.05 minutes of surrogate RTDCB RT Limit = ± 0.10 minutes of surrogate RT


FORM VIII 8081A

06/03/2010 of 623

PESTICIDES ANALYTICAL SEQUENCE

Lab Name: Job No.:

SDG No.:

FORM VIII


Calibration ID:


GC Column:

6134


05/11/2010 12:47

05/11/2010 13:42CLP-1 ID: 0.53(mm)


# #RT RT

TCX DCB

UPPER LIMIT

LOWER LIMIT

2.04

1.94

9.61

9.41



CCVRT 460-37575/5 05/17/2010 05:29 1.99 9.51xr108819.d

LCS 460-37420/2-A 05/17/2010 05:43 1.98 9.52xr108820.d

460-13147-A-2-B MS 05/17/2010 06:36 1.99 9.51xr108822.d

460-13147-A-2-C MSD 05/17/2010 06:50 1.99 9.51xr108823.d

460-13139-2 05/17/2010 08:00 1.99 9.51TB-3 6-7 xr108828.d

460-13139-4 05/17/2010 08:27 1.99 9.51TB-2 5-6 xr108830.d

460-13139-5 05/17/2010 08:41 1.98 9.51TB-1 2-3 xr108831.d

460-13139-7 05/17/2010 09:09 1.99 9.51TB-5 3-4 xr108833.d

MB 460-37420/1-A 05/17/2010 09:37 1.98 9.51xr108835.d

CCV 460-37575/23 05/17/2010 10:04 1.98 9.51xr108837.d





FORM VIII 8081A

06/03/2010 of 623

FORM XForm 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:


Instrument ID (1): Instrument ID (2):

Date Analyzed (1): Date Analyzed (2):

GC Column (1): ID: GC Column (2): ID:

TB-2 5-6


IDENTIFICATION SUMMARYForm 1

0.53(mm) 0.53(mm)

05/17/2010 08:27 05/17/2010 08:27

PESTGC1 PESTGC1

CLP-2 CLP-1

ANALYTE COL PEAK RTRT WINDOW

FROM TO PEAK MEANRPD

CONCENTRATION

7.297.157.2214,4'-DDE 13 43.2

5.275.135.192 8.6

7.567.427.521Dieldrin 10 60.0

6.045.905.982 5.5

8.037.897.9614,4'-DDD 55 32.5

6.806.666.732 40

8.408.268.3314,4'-DDT 29 7.8

7.357.217.282 27

Chlordane 1 1 3.50 3.40 3.54 388 290 49.9

3 4.86 4.80 4.94 116

4 6.53 6.48 6.62 337

5 6.77 6.72 6.86 287

6 6.90 6.84 6.98 434

8 8.09 8.09 8.23 171

2 3 3.44 3.36 3.50 90.5 170

4 4.19 4.12 4.26 79.6

5 4.65 4.58 4.72 274

6 4.97 4.89 5.03 250

FORM X 8081A

06/03/2010 of 623

FORM XForm 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:





TB-5 3-4



0.53(mm) 0.53(mm)

05/17/2010 09:09 05/17/2010 09:09

PESTGC1 PESTGC1

CLP-2 CLP-1



CONCENTRATION

3.163.063.111gamma-BHC (Lindane) 16 55.8

2.662.562.582 28

7.297.157.2314,4'-DDE 35 65.2

5.275.135.202 18

7.567.427.491Dieldrin 22 23.2

6.045.905.982 28

Chlordane 1 1 3.47 3.40 3.54 926 1700 25.7

3 4.86 4.80 4.94 1120

4 6.53 6.48 6.62 1770

5 6.77 6.72 6.86 1860

6 6.90 6.84 6.98 1900

7 7.95 7.88 8.02 3800

8 8.12 8.09 8.23 368

2 1 2.92 2.84 2.98 608 1300

2 3.02 2.91 3.05 264

3 3.44 3.36 3.50 1410

4 4.19 4.12 4.26 1800

5 4.65 4.58 4.72 1180

6 4.95 4.89 5.03 1490

7 6.63 6.57 6.71 2310

FORM X 8081A

06/03/2010 of 623

FORM XForm 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:







0.53(mm) 0.53(mm)

05/17/2010 05:43 05/17/2010 05:43

PESTGC1 PESTGC1

CLP-2 CLP-1



CONCENTRATION

2.822.722.791alpha-BHC 96.3 7.9

2.432.332.382 89.0

3.163.063.131gamma-BHC (Lindane) 98.6 8.9

2.662.562.612 90.2

3.243.143.221beta-BHC 104 2.8

2.722.622.672 102

3.623.523.601delta-BHC 121 10.3

2.862.762.812 109

3.743.643.731Heptachlor 93.0 6.4

3.032.932.992 87.2

4.534.434.541Aldrin 88.9 7.9

3.323.223.282 82.2

6.105.966.101Heptachlor epoxide 97.0 3.7

4.414.274.362 93.5

7.106.967.081Endosulfan I 93.6 0.3

5.405.265.362 93.3

7.297.157.2614,4'-DDE 98.1 3.5

5.275.135.222 94.8

7.567.427.521Dieldrin 88.6 1.1

6.045.906.002 89.6

7.927.787.881Endrin 101 3.2

6.626.486.572 104

8.037.897.9914,4'-DDD 94.7 1.4

6.806.666.752 93.4

8.168.028.121Endosulfan II 101 0.9

7.136.997.082 101

8.408.268.3514,4'-DDT 99.1 2.0

7.357.217.302 97.2

8.558.418.501Endrin aldehyde 103 0.5

7.747.607.682 104

8.888.748.831Endosulfan sulfate 103 1.9

8.228.088.162 101

FORM X 8081A

06/03/2010 of 623

FORM XForm 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

Lab Sample ID: 460-13147-A-2-B MS






0.53(mm) 0.53(mm)

05/17/2010 06:36 05/17/2010 06:36

PESTGC1 PESTGC1

CLP-2 CLP-1



CONCENTRATION

2.822.722.771alpha-BHC 154 17.1

2.432.332.382 129


2.662.562.612 130

3.243.143.191beta-BHC 153 17.3

2.722.622.672 128

3.623.523.571delta-BHC 167 16.1

2.862.762.812 142

3.743.643.691Heptachlor 139 1.0

3.032.932.992 137

4.534.434.481Aldrin 151 17.6

3.323.223.282 127

6.105.966.041Heptachlor epoxide 149 12.4

4.414.274.352 132

7.106.967.041Endosulfan I 144 6.6

5.405.265.332 135

7.297.157.2314,4'-DDE 169 22.2

5.275.135.202 135

7.567.427.491Dieldrin 150 15.8

6.045.905.972 128

7.927.787.861Endrin 168 12.8

6.626.486.552 148

8.037.897.9614,4'-DDD 159 17.2

6.806.666.732 134

8.168.028.091Endosulfan II 152 21.4

7.136.997.072 123

8.408.268.3314,4'-DDT 162 21.7

7.357.217.292 131

8.558.418.481Endrin aldehyde 145 22.7

7.747.607.672 116


8.228.088.152 118

FORM X 8081A

06/03/2010 of 623

FORM XForm 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

Lab Sample ID: 460-13147-A-2-C MSD






0.53(mm) 0.53(mm)

05/17/2010 06:50 05/17/2010 06:50

PESTGC1 PESTGC1

CLP-2 CLP-1



CONCENTRATION

2.822.722.771alpha-BHC 145 17.0

2.432.332.382 122


2.662.562.612 121

3.243.143.191beta-BHC 144 13.8

2.722.622.672 125

3.623.523.571delta-BHC 159 16.8

2.862.762.812 134

3.743.643.691Heptachlor 125 3.0

3.032.932.982 122

4.534.434.481Aldrin 145 17.3

3.323.223.272 122

6.105.966.041Heptachlor epoxide 140 14.3

4.414.274.352 122

7.106.967.041Endosulfan I 137 8.0

5.405.265.332 126

7.297.157.2314,4'-DDE 161 27.6

5.275.135.202 122

7.567.427.491Dieldrin 140 15.4

6.045.905.972 120

7.927.787.861Endrin 163 20.0

6.626.486.552 133

8.037.897.9614,4'-DDD 156 27.8

6.806.666.732 118

8.168.028.091Endosulfan II 145 24.6

7.136.997.062 113

8.408.268.3314,4'-DDT 150 24.1

7.357.217.282 118

8.558.418.481Endrin aldehyde 137 35.3

7.747.607.672 95.9


8.228.088.152 109

FORM X 8081A

06/03/2010 of 623

FORM IForm 1PESTICIDES ORGANICS ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

TB-3 6-7

SDG No.:

460-13139-1


Matrix: xf108828.dLab File ID:

Date Collected:8081AAnalysis Method:

Soil

TestAmerica Edison

05/12/2010 09:45


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1

Extraction Method: 3541 05/14/2010 09:15

05/17/2010 08:00

N

10(mL)

1(uL)


% Moisture: 18.8

GC Column: ID: 0.53(mm)CLP-2



877-09-8 Tetrachloro-m-xylene 115 22-141

2051-24-3 DCB Decachlorobiphenyl 125 10-165

FORM I 8081A

06/03/2010 of 623

Data File: xf108828.d Report Date: 17-May-2010 11:17

TestAmerica

GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC1.i/8081T/front/May10/05-17-10/17may10a.b/xf108828.dLab Smp Id: 460-13139-e-2-b Inj Date : 17-MAY-2010 08:00 Operator : 462 Inst ID: PESTGC1.iSmp Info : 460-13139-e-2-bMisc Info : Comment : Method : /chem1/PESTGC1.i/8081T/front/May10/05-17-10/17may10a.b/09Xf8081.mMeth Date : 17-May-2010 11:16 ferdie Quant Type: ESTDCal Date : 11-MAY-2010 14:10 Cal File: xf108641.dAls bottle: 1 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: Allpest.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3

Concentration Formula: Amt * DF * Vt/(Ws*(100-M)/100) * CpndVariable


DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (uL)(1000 low, 2Ws 15.00000 Weight of sample extracted (g)M 0.00000 % Moisture


CONCENTRATIONS

ON-COL FINAL

RT EXP RT DLT RT RESPONSE ( ug/L) (ug/kg) TARGET RANGE RATIO

== ====== ======== ======== ======= ======= ============ =====

$ 28 Tetrachloro-m-xylene CAS #: 877-09-8

2.287 2.287 0.000 129307 57.5645 38 80.00- 120.00 100.00

-------------------------------------------------------------------------------

$ 30 Decachlorobiphenyl CAS #: 2051-24-3

10.333 10.333 0.000 81991 62.6568 42 80.00- 120.00 100.00

-------------------------------------------------------------------------------

06/03/2010 of 623

Data File: xf108828.d

Date: 17-MAY-2010 08:00

Client ID: Instrument: PESTGC1.i

Sample Info: 460-13139-e-2-b Operator: 462

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-3 6-7

SDG No.:

460-13139-1


Matrix: xr108828.dLab File ID:


Soil

TestAmerica Edison

05/12/2010 09:45


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/17/2010 08:00

N

10(mL)

1(uL)


% Moisture: 18.8




Aldrin309-00-2 8.3 8.3 1.8U

alpha-BHC319-84-6 8.3 8.3 1.5U

beta-BHC319-85-7 8.3 8.3 1.1U

delta-BHC319-86-8 8.3 8.3 1.3U

gamma-BHC (Lindane)58-89-9 8.3 8.3 0.96U

Chlordane57-74-9 83 83 18U

4,4'-DDD72-54-8 8.3 8.3 0.99U

4,4'-DDE72-55-9 8.3 8.3 1.6U

4,4'-DDT50-29-3 8.3 8.3 1.0U

Dieldrin60-57-1 8.3 8.3 1.6U

Endosulfan I959-98-8 8.3 8.3 1.7U

Endosulfan II33213-65-9 8.3 8.3 1.2U

Endosulfan sulfate1031-07-8 8.3 8.3 1.1U

Endrin72-20-8 8.3 8.3 1.2U

Endrin aldehyde7421-93-4 8.3 8.3 2.1U

Heptachlor76-44-8 8.3 8.3 1.2U

Heptachlor epoxide1024-57-3 8.3 8.3 1.7U

Toxaphene8001-35-2 83 83 17U




FORM I 8081A

06/03/2010 of 623

Data File: xr108828.d Page 1 Report Date: 17-May-2010 11:17

TestAmerica

GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC1.i/8081T/rear/May10/05-17-10/17may10a.b/xr108828.dLab Smp Id: 460-13139-e-2-b Inj Date : 17-MAY-2010 08:00 Operator : 462 Inst ID: PESTGC1.iSmp Info : 460-13139-e-2-bMisc Info : Comment : Method : /chem1/PESTGC1.i/8081T/rear/May10/05-17-10/17may10a.b/09Xr8081.mMeth Date : 17-May-2010 08:58 ferdie Quant Type: ESTDCal Date : 11-MAY-2010 14:10 Cal File: xr108641.dAls bottle: 1 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: Allpest.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3





CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====


1.987 1.987 0.000 227401 55.8844 37 80.00- 120.00 100.00

-------------------------------------------------------------------------------


9.513 9.513 0.000 132431 52.4024 35 80.00- 120.00 100.00

-------------------------------------------------------------------------------

06/03/2010 of 623

Data File: xr108828.d

Date: 17-MAY-2010 08:00



06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-2 5-6

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 10:45


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/17/2010 08:27

N

10(mL)

1(uL)


% Moisture: 12.8




4,4'-DDD72-54-8 55 7.7 0.92

4,4'-DDT50-29-3 29 7.7 0.96




FORM I 8081A

06/03/2010 of 623


TestAmerica






CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====


2.287 2.287 0.000 135629 60.3789 40 80.00- 120.00 100.00

-------------------------------------------------------------------------------

6 Chlordane CAS #: 57-74-9

3.503 3.470 0.033 56067 507.927 340 80.00- 120.00 100.00

3.697 3.700 -0.003 0 106.80- 160.20 0.00

4.860 4.870 -0.010 20965 151.507 100 100.29- 150.43 37.39

6.533 6.547 -0.014 154574 441.350 290 253.83- 380.74 275.70

6.770 6.787 -0.017 116242 376.157 250 223.96- 335.95 207.33

6.900 6.913 -0.013 162517 568.653 380 207.13- 310.69 289.86

7.960 7.953 0.007 0 38.42- 57.62 0.00

8.093 8.160 -0.067 22471 223.759 150 72.78- 109.17 40.08

Average of Peak Concentrations = 250

-------------------------------------------------------------------------------

06/03/2010 of 623


CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====

65 gamma-Chlordane CAS #: 5103-74-2

6.533 6.540 -0.007 154574 49.2684 33 80.00- 120.00 100.00

-------------------------------------------------------------------------------

66 alpha-Chlordane CAS #: 5103-71-9

6.900 6.903 -0.003 162517 56.3061 38 80.00- 120.00 100.00

-------------------------------------------------------------------------------

8 4,4'-DDE CAS #: 72-55-9

7.223 7.230 -0.007 41866 17.5219 12 80.00- 120.00 100.00

-------------------------------------------------------------------------------

10 Dieldrin CAS #: 60-57-1

7.520 7.490 0.030 33630 13.3142 8.9 80.00- 120.00 100.00

-------------------------------------------------------------------------------

7 4,4'-DDD CAS #: 72-54-8

7.960 7.967 -0.007 139431 72.5796 48 80.00- 120.00 100.00(M)

-------------------------------------------------------------------------------

9 4,4'-DDT CAS #: 50-29-3

8.327 8.330 -0.003 67783 38.0943 25 80.00- 120.00 100.00

-------------------------------------------------------------------------------


10.330 10.333 -0.003 101186 77.3255 52 80.00- 120.00 100.00

-------------------------------------------------------------------------------

QC Flag Legend

M - Compound response manually integrated.

06/03/2010 of 623


Date: 17-MAY-2010 08:27



06/03/2010 of 623


Data File: xf108830.dInj. Date and Time: 17-MAY-2010 08:27Instrument ID: PESTGC1.iClient ID: Compound: 7 4,4'-DDDCAS #: 72-54-8Report Date: 05/17/2010


Not Detected

Expected RT: 7.96


RT: 7.96

Response: 139431

Amount: 72.58

Conc: 48.39

Manually Integrated By: ferdieManual Integration Reason:

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-2 5-6

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 10:45


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/17/2010 08:27

N

10(mL)

1(uL)


% Moisture: 12.8




Aldrin309-00-2 7.7 7.7 1.7U

alpha-BHC319-84-6 7.7 7.7 1.4U

beta-BHC319-85-7 7.7 7.7 1.0U

delta-BHC319-86-8 7.7 7.7 1.2U


Chlordane57-74-9 170 77 17p

4,4'-DDE72-55-9 8.6 7.7 1.5p

Dieldrin60-57-1 5.5 7.7 1.5J p

Endosulfan I959-98-8 7.7 7.7 1.6U

Endosulfan II33213-65-9 7.7 7.7 1.2U


Endrin72-20-8 7.7 7.7 1.1U


Heptachlor76-44-8 7.7 7.7 1.1U


Toxaphene8001-35-2 77 77 16U



2051-24-3 DCB Decachlorobiphenyl X168 10-165

FORM I 8081A

06/03/2010 of 623


TestAmerica






CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====


1.987 1.987 0.000 216061 53.0976 35 80.00- 120.00 100.00

-------------------------------------------------------------------------------


2.917 2.913 0.004 0 80.00- 120.00 0.00(T)

0.000 2.983 -2.983 0 121.97- 182.95 0.00

3.440 3.433 0.007 30596 118.481 79 115.53- 173.30 347.95

4.190 4.193 -0.003 12263 104.189 69 52.66- 78.99 139.47

4.653 4.653 0.000 239639 358.874 240 298.74- 448.12 2725.28

4.967 4.963 0.004 343276 326.948 220 469.73- 704.59 3903.88

0.000 6.637 -6.637 0 64.26- 96.39 0.00

0.000 6.920 -6.920 0 102.24- 153.36 0.00


-------------------------------------------------------------------------------

06/03/2010 of 623


CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====


4.653 4.653 0.000 239639 44.8290 30 80.00- 120.00 100.00

-------------------------------------------------------------------------------


4.967 4.987 -0.020 343276 66.0699 44 80.00- 120.00 100.00

-------------------------------------------------------------------------------

8 4,4'-DDE CAS #: 72-55-9

5.193 5.203 -0.010 51169 11.2943 7.5 80.00- 120.00 100.00

-------------------------------------------------------------------------------


5.980 5.977 0.003 36344 7.16706 4.8 80.00- 120.00 100.00

-------------------------------------------------------------------------------

7 4,4'-DDD CAS #: 72-54-8

6.730 6.737 -0.007 206293 52.2907 35 80.00- 120.00 100.00

-------------------------------------------------------------------------------

9 4,4'-DDT CAS #: 50-29-3

7.283 7.287 -0.004 133598 35.2224 23 80.00- 120.00 100.00

-------------------------------------------------------------------------------


9.513 9.513 0.000 212206 83.9690 56 80.00- 120.00 100.00(R)

-------------------------------------------------------------------------------

QC Flag Legend

T - Target compound detected outside RT window.R - Spike/Surrogate failed recovery limits.

06/03/2010 of 623


Date: 17-MAY-2010 08:27



06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-1 2-3

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 11:25


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/17/2010 08:41

N

10(mL)

1(uL)


% Moisture: 6.5






FORM I 8081A

06/03/2010 of 623


TestAmerica






CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====


2.283 2.287 -0.004 131445 58.5163 39 80.00- 120.00 100.00

-------------------------------------------------------------------------------


10.333 10.333 0.000 90555 69.2013 46 80.00- 120.00 100.00

-------------------------------------------------------------------------------

06/03/2010 of 623


Date: 17-MAY-2010 08:41



06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-1 2-3

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 11:25


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/17/2010 08:41

N

10(mL)

1(uL)


% Moisture: 6.5




Aldrin309-00-2 7.2 7.2 1.6U

alpha-BHC319-84-6 7.2 7.2 1.3U

beta-BHC319-85-7 7.2 7.2 0.97U

delta-BHC319-86-8 7.2 7.2 1.1U


Chlordane57-74-9 72 72 16U

4,4'-DDD72-54-8 7.2 7.2 0.86U

4,4'-DDE72-55-9 7.2 7.2 1.4U

4,4'-DDT50-29-3 7.2 7.2 0.90U

Dieldrin60-57-1 7.2 7.2 1.4U

Endosulfan I959-98-8 7.2 7.2 1.5U

Endosulfan II33213-65-9 7.2 7.2 1.1U


Endrin72-20-8 7.2 7.2 1.0U


Heptachlor76-44-8 7.2 7.2 1.0U


Toxaphene8001-35-2 72 72 15U




FORM I 8081A

06/03/2010 of 623


TestAmerica






CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====


1.983 1.987 -0.004 230813 56.7229 38 80.00- 120.00 100.00

-------------------------------------------------------------------------------


9.513 9.513 0.000 148700 58.8399 39 80.00- 120.00 100.00

-------------------------------------------------------------------------------

06/03/2010 of 623


Date: 17-MAY-2010 08:41



06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-5 3-4

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 12:30


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/17/2010 09:09

N

10(mL)

1(uL)


% Moisture: 61.5




gamma-BHC (Lindane)58-89-9 16 17 2.0J p

Chlordane57-74-9 1700 170 38




FORM I 8081A

06/03/2010 of 623


TestAmerica






CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====


2.287 2.287 0.000 94721 42.1676 28 80.00- 120.00 100.00

-------------------------------------------------------------------------------

5 gamma-BHC (Lindane) CAS #: 58-89-9

3.110 3.110 0.000 26539 9.23526 6.2 80.00- 120.00 100.00

-------------------------------------------------------------------------------


3.470 3.470 0.000 58993 534.434 360 80.00- 120.00 100.00

3.740 3.700 0.040 0 106.80- 160.20 0.00

4.863 4.870 -0.007 89230 644.837 430 100.29- 150.43 151.26

6.533 6.547 -0.014 357199 1019.90 680 253.83- 380.74 605.49

6.773 6.787 -0.014 332123 1074.74 720 223.96- 335.95 562.99

6.900 6.913 -0.013 312475 1093.36 730 207.13- 310.69 529.68

06/03/2010 of 623


CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====

6 Chlordane (continued)

7.947 7.953 -0.006 116142 2191.11 1500 38.42- 57.62 196.87

8.117 8.160 -0.043 21339 212.487 140 72.78- 109.17 36.17


-------------------------------------------------------------------------------


6.533 6.540 -0.007 357199 113.852 76 80.00- 120.00 100.00

-------------------------------------------------------------------------------


6.900 6.903 -0.003 312475 108.261 72 80.00- 120.00 100.00

-------------------------------------------------------------------------------

8 4,4'-DDE CAS #: 72-55-9

7.227 7.230 -0.003 48425 20.2670 14 80.00- 120.00 100.00

-------------------------------------------------------------------------------


7.487 7.490 -0.003 31962 12.6539 8.4 80.00- 120.00 100.00

-------------------------------------------------------------------------------


10.333 10.333 0.000 51005 38.9776 26 80.00- 120.00 100.00

-------------------------------------------------------------------------------

06/03/2010 of 623


Date: 17-MAY-2010 09:09



06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-5 3-4

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 12:30


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/17/2010 09:09

N

10(mL)

1(uL)


% Moisture: 61.5




Aldrin309-00-2 17 17 3.8U

alpha-BHC319-84-6 17 17 3.2U

beta-BHC319-85-7 17 17 2.4U

delta-BHC319-86-8 17 17 2.7U

4,4'-DDD72-54-8 17 17 2.1U

4,4'-DDE72-55-9 18 17 3.4p

4,4'-DDT50-29-3 17 17 2.2U

Dieldrin60-57-1 28 17 3.4

Endosulfan I959-98-8 17 17 3.7U

Endosulfan II33213-65-9 17 17 2.6U

Endosulfan sulfate1031-07-8 17 17 2.2U

Endrin72-20-8 17 17 2.4U

Endrin aldehyde7421-93-4 17 17 4.3U

Heptachlor76-44-8 17 17 2.5U

Heptachlor epoxide1024-57-3 17 17 3.5U

Toxaphene8001-35-2 170 170 36U




FORM I 8081A

06/03/2010 of 623


TestAmerica






CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====


1.987 1.987 0.000 153679 37.7670 25 80.00- 120.00 100.00

-------------------------------------------------------------------------------


2.577 2.607 -0.030 85063 16.3746 11 80.00- 120.00 100.00

-------------------------------------------------------------------------------


2.917 2.913 0.004 62693 350.601 230 80.00- 120.00 100.00(T)

3.017 2.983 0.034 41598 152.587 100 121.97- 182.95 66.35

3.437 3.433 0.004 209490 811.235 540 115.53- 173.30 334.15

4.193 4.193 0.000 122302 1039.10 690 52.66- 78.99 195.08

4.650 4.653 -0.003 456141 683.099 460 298.74- 448.12 727.58

4.953 4.963 -0.010 904701 861.669 570 469.73- 704.59 1443.07

06/03/2010 of 623


CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====

6 Chlordane (continued)

6.633 6.637 -0.004 191468 1333.05 890 64.26- 96.39 305.41

0.000 6.920 -6.920 0 102.24- 153.36 0.00


-------------------------------------------------------------------------------


4.650 4.653 -0.003 456141 85.3297 57 80.00- 120.00 100.00

-------------------------------------------------------------------------------


4.953 4.987 -0.034 904701 174.127 120 80.00- 120.00 100.00

-------------------------------------------------------------------------------

8 4,4'-DDE CAS #: 72-55-9

5.197 5.203 -0.006 46677 10.3028 6.9 80.00- 120.00 100.00

-------------------------------------------------------------------------------


5.983 5.977 0.006 80996 15.9725 11 80.00- 120.00 100.00

-------------------------------------------------------------------------------


9.510 9.513 -0.003 94677 37.4633 25 80.00- 120.00 100.00

-------------------------------------------------------------------------------

QC Flag Legend

T - Target compound detected outside RT window.

06/03/2010 of 623


Date: 17-MAY-2010 09:09



06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:


GC SEMI VOA INITIAL CALIBRATION DATA


PESTGC1



N

05/11/2010 13:42

0.53(mm)GC Column: CLP-2 ID:

EXTERNAL STANDARD RETENTION TIME SUMMARY

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-37146/5 xf108635.dLevel 2 IC 460-37146/6 xf108636.dLevel 3 IC 460-37146/7 xf108637.dLevel 4 IC 460-37146/8 xf108638.dLevel 5 IC 460-37146/9 xf108639.d

ANALYTE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 AVG RTRT WINDOW

alpha-BHC 2.7782.727 - 2.8272.787 2.777 2.777 2.773 2.777gamma-BHC (Lindane) 3.1173.067 - 3.1673.127 3.113 3.117 3.113 3.113beta-BHC 3.2013.150 - 3.2503.210 3.200 3.200 3.197 3.197delta-BHC 3.5763.523 - 3.6233.590 3.573 3.573 3.570 3.573Heptachlor 3.7073.653 - 3.7533.723 3.703 3.703 3.700 3.703Aldrin 4.5014.447 - 4.5474.523 4.497 4.497 4.493 4.493Heptachlor epoxide 6.0555.980 - 6.1206.077 6.050 6.050 6.050 6.047gamma-Chlordane 6.5536.480 - 6.6206.573 6.550 6.550 6.547 6.547alpha-Chlordane 6.9176.843 - 6.9836.933 6.913 6.913 6.913 6.910Endosulfan I 7.0496.977 - 7.1177.063 7.047 7.047 7.047 7.0434,4'-DDE 7.2387.167 - 7.3077.250 7.237 7.237 7.233 7.233Dieldrin 7.4987.427 - 7.5677.507 7.497 7.497 7.497 7.493Endrin 7.8637.793 - 7.9337.870 7.863 7.863 7.860 7.8604,4'-DDD 7.9727.900 - 8.0407.980 7.970 7.970 7.970 7.970Endosulfan II 8.1038.030 - 8.1708.110 8.103 8.100 8.100 8.1004,4'-DDT 8.3368.263 - 8.4038.343 8.337 8.333 8.333 8.333Endrin aldehyde 8.4908.420 - 8.5608.497 8.490 8.490 8.487 8.487Endosulfan sulfate 8.8178.747 - 8.8878.823 8.817 8.817 8.817 8.813Methoxychlor 9.1319.060 - 9.2009.137 9.130 9.130 9.130 9.130Endrin ketone 9.4099.337 - 9.4779.413 9.410 9.407 9.407 9.407Tetrachloro-m-xylene 2.2882.237 - 2.3372.293 2.287 2.287 2.287 2.287DCB Decachlorobiphenyl 10.34110.240 - 10.44010.343 10.340 10.340 10.340 10.340

FORM VI 8081A 06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




PESTGC1



N

05/11/2010 13:42

0.53(mm)CLP-2 ID:

EXTERNAL STANDARD CURVE EVALUTION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-37146/5 xf108635.d2Level IC 460-37146/6 xf108636.d3Level IC 460-37146/7 xf108637.d4Level IC 460-37146/8 xf108638.d5Level IC 460-37146/9 xf108639.d

MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE

LVL 4LVL 3LVL 2LVL 1

RRFANALYTE MIN RRF

LVL 5

alpha-BHC Ave 9.5 20.031563642.8 3225.2 3035.5 2986.52889.3

gamma-BHC (Lindane) Ave 10.6 20.028743381.3 2925.0 2738.7 2712.52610.8

beta-BHC Ave 19.3 20.014541925.8 1488.7 1334.9 1292.41226.9

delta-BHC Ave 3.3 20.029643080.4 3041.6 2922.3 2939.12834.6

Heptachlor Ave 8.0 20.031493551.3 3222.3 3044.2 3019.92909.2

Aldrin Ave 3.3 20.031233286.2 3136.6 3068.7 3111.13013.3

Heptachlor epoxide Ave 10.6 20.030883637.2 3124.9 2960.7 2919.32798.4

gamma-Chlordane Ave 10.7 20.031373691.7 3164.0 2957.0 3062.22812.1

alpha-Chlordane Ave 12.8 20.028863503.7 2935.3 2736.8 2687.32568.5

Endosulfan I Ave 10.0 20.026453090.9 2661.6 2536.1 2516.02418.9

4,4'-DDE Ave 1.9 20.023892456.2 2378.2 2354.2 2414.32343.9

Dieldrin Ave 6.5 20.025262797.8 2549.6 2450.8 2458.92372.3

Endrin Ave 7.0 20.019792217.5 1979.7 1890.0 1924.01884.2

4,4'-DDD Ave 6.0 20.019212111.6 1935.2 1867.6 1876.71814.3

Endosulfan II Ave 10.8 20.021782576.2 2190.5 2086.6 2065.91970.5

FORM VI 8081A


06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




PESTGC1



N

05/11/2010 13:42

0.53(mm)CLP-2 ID:


MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE


RRFANALYTE MIN RRF

LVL 5

4,4'-DDT Ave 4.3 20.017791907.7 1746.1 1705.4 1774.61762.9

Endrin aldehyde Ave 13.5 20.017552163.5 1733.0 1670.2 1640.71566.6

Endosulfan sulfate Ave 10.9 20.019482306.6 1970.3 1860.8 1831.81769.8

Methoxychlor Ave 11.9 20.09991204.6 1003.1 935.69 927.02925.17

Endrin ketone Ave 12.2 20.022072653.4 2247.7 2106.0 2056.01973.1

Tetrachloro-m-xylene Ave 5.7 20.022462369.4 2378.1 2211.0 2196.92076.0

DCB Decachlorobiphenyl Ave 5.0 20.013091347.5 1377.5 1313.4 1298.31206.2

FORM VI 8081A


06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




PESTGC1



N

05/11/2010 13:42

GC Column: CLP-2 ID: 0.53(mm)

EXTERNAL STANDARD RESPONSE AND CONCENTRATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-37146/5 xf108635.dLevel 2 IC 460-37146/6 xf108636.dLevel 3 IC 460-37146/7 xf108637.dLevel 4 IC 460-37146/8 xf108638.dLevel 5 IC 460-37146/9 xf108639.d

CURVETYPE

RESPONSEANALYTE CONCENTRATION (UG/L)

LVL 1 LVL 1LVL 2 LVL 2LVL 3 LVL 3LVL 4 LVL 4LVL 5 LVL 5

alpha-BHC Ave 36428 161260 303553 746634 1444652 10.0 50.0 100 250 500gamma-BHC (Lindane) Ave 33813 146248 273872 678129 1305403 10.0 50.0 100 250 500beta-BHC Ave 19258 74437 133487 323092 613439 10.0 50.0 100 250 500delta-BHC Ave 30804 152081 292227 734786 1417324 10.0 50.0 100 250 500Heptachlor Ave 35513 161115 304423 754965 1454592 10.0 50.0 100 250 500Aldrin Ave 32862 156829 306871 777774 1506651 10.0 50.0 100 250 500Heptachlor epoxide Ave 36372 156243 296068 729816 1399176 10.0 50.0 100 250 500gamma-Chlordane Ave 36917 158200 295695 765545 1406046 10.0 50.0 100 250 500alpha-Chlordane Ave 35037 146766 273678 671826 1284233 10.0 50.0 100 250 500Endosulfan I Ave 30909 133078 253605 628993 1209466 10.0 50.0 100 250 5004,4'-DDE Ave 24562 118910 235417 603576 1171958 10.0 50.0 100 250 500Dieldrin Ave 27978 127479 245078 614720 1186157 10.0 50.0 100 250 500Endrin Ave 22175 98986 188999 480995 942121 10.0 50.0 100 250 5004,4'-DDD Ave 21116 96759 186757 469180 907157 10.0 50.0 100 250 500Endosulfan II Ave 25762 109525 208663 516465 985225 10.0 50.0 100 250 5004,4'-DDT Ave 19077 87305 170540 443648 881471 10.0 50.0 100 250 500Endrin aldehyde Ave 21635 86649 167018 410169 783293 10.0 50.0 100 250 500Endosulfan sulfate Ave 23066 98516 186083 457948 884919 10.0 50.0 100 250 500Methoxychlor Ave 12046 50153 93569 231756 462587 10.0 50.0 100 250 500Endrin ketone Ave 26534 112387 210601 514011 986528 10.0 50.0 100 250 500Tetrachloro-m-xylene Ave 59236 118907 221104 329529 415202 25.0 50.0 100 150 200DCB Decachlorobiphenyl Ave 33688 68873 131344 194739 241237 25.0 50.0 100 150 200

Curve Type Legend:Ave = Average

FORM VI 8081A 06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




PESTGC1



N

05/11/2010 13:42



Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-37146/5 xr108635.dLevel 2 IC 460-37146/6 xr108636.dLevel 3 IC 460-37146/7 xr108637.dLevel 4 IC 460-37146/8 xr108638.dLevel 5 IC 460-37146/9 xr108639.d


alpha-BHC 2.3812.330 - 2.4302.383 2.380 2.380 2.380 2.380gamma-BHC (Lindane) 2.6082.560 - 2.6602.610 2.607 2.610 2.607 2.607beta-BHC 2.6732.623 - 2.7232.677 2.673 2.673 2.670 2.673delta-BHC 2.8102.760 - 2.8602.813 2.810 2.810 2.807 2.810Heptachlor 2.9852.937 - 3.0372.987 2.983 2.987 2.983 2.983Aldrin 3.2753.227 - 3.3273.280 3.273 3.277 3.273 3.273Heptachlor epoxide 4.3514.280 - 4.4204.360 4.350 4.350 4.347 4.350gamma-Chlordane 4.6554.583 - 4.7234.663 4.653 4.653 4.650 4.653alpha-Chlordane 4.9904.917 - 5.0575.000 4.990 4.987 4.987 4.9874,4'-DDE 5.2055.133 - 5.2735.213 5.207 5.203 5.203 5.200Endosulfan I 5.3415.270 - 5.4105.350 5.340 5.340 5.337 5.337Dieldrin 5.9805.910 - 6.0505.987 5.980 5.980 5.977 5.977Endrin 6.5576.487 - 6.6276.563 6.557 6.557 6.557 6.5534,4'-DDD 6.7386.667 - 6.8076.743 6.740 6.737 6.737 6.733Endosulfan II 7.0707.000 - 7.1407.073 7.070 7.070 7.070 7.0674,4'-DDT 7.2897.220 - 7.3607.290 7.290 7.290 7.287 7.287Endrin aldehyde 7.6727.603 - 7.7437.673 7.673 7.673 7.670 7.670Methoxychlor 7.8857.813 - 7.9537.887 7.887 7.883 7.883 7.883Endosulfan sulfate 8.1558.087 - 8.2278.157 8.157 8.157 8.153 8.153Endrin ketone 8.4678.397 - 8.5378.470 8.467 8.467 8.467 8.463Tetrachloro-m-xylene 1.9841.937 - 2.0371.983 1.983 1.987 1.983 1.983DCB Decachlorobiphenyl 9.5179.417 - 9.6179.517 9.517 9.517 9.517 9.517

FORM VI 8081A 06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




PESTGC1



N

05/11/2010 13:42

0.53(mm)CLP-1 ID:


Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-37146/5 xr108635.d2Level IC 460-37146/6 xr108636.d3Level IC 460-37146/7 xr108637.d4Level IC 460-37146/8 xr108638.d5Level IC 460-37146/9 xr108639.d

MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE


RRFANALYTE MIN RRF

LVL 5

alpha-BHC Ave 13.6 20.059487207.4 6222.7 5718.8 5478.45114.7

gamma-BHC (Lindane) Ave 16.9 20.051956583.1 5459.6 4915.8 4689.44326.2

beta-BHC Ave 16.1 20.028383566.1 2951.4 2732.6 2550.92391.2

delta-BHC Ave 12.4 20.054726551.7 5640.6 5270.9 5119.94774.6

Heptachlor Ave 14.4 20.054136626.2 5650.1 5218.3 4965.14606.1

Aldrin Ave 10.3 20.051505951.2 5340.0 5023.9 4887.34548.9

Heptachlor epoxide Ave 12.0 20.052956311.3 5436.5 5111.5 4971.94642.6

gamma-Chlordane Ave 12.1 20.053466403.7 5446.6 5122.6 5025.94729.4

alpha-Chlordane Ave 11.8 20.051966170.5 5344.5 5020.5 4875.94566.9

4,4'-DDE Ave 3.6 20.045314725.9 4622.6 4504.6 4508.64290.8

Endosulfan I Ave 9.5 20.049545689.8 5057.7 4805.7 4785.34430.4

Dieldrin Ave 6.5 20.050715579.0 5137.4 4974.7 4977.44686.3

Endrin Ave 5.3 20.043004623.8 4407.6 4228.5 4220.74017.4

4,4'-DDD Ave 2.0 20.039454023.2 4007.4 3915.4 3954.83824.7

Endosulfan II Ave 11.1 20.043685152.0 4464.0 4225.2 4112.33884.9

FORM VI 8081A


06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




PESTGC1



N

05/11/2010 13:42

0.53(mm)CLP-1 ID:


MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE


RRFANALYTE MIN RRF

LVL 5

4,4'-DDT Ave 4.3 20.037934064.1 3807.1 3682.4 3756.43655.0

Endrin aldehyde Ave 14.1 20.033934191.1 3441.5 3227.9 3135.32970.7

Methoxychlor Ave 11.7 20.020062390.4 2063.2 1907.4 1863.51807.6

Endosulfan sulfate Ave 12.4 20.036964441.0 3786.4 3553.9 3443.33253.9

Endrin ketone Ave 12.4 20.043675212.8 4518.0 4241.2 4076.63786.0



FORM VI 8081A


06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




PESTGC1



N

05/11/2010 13:42



Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-37146/5 xr108635.dLevel 2 IC 460-37146/6 xr108636.dLevel 3 IC 460-37146/7 xr108637.dLevel 4 IC 460-37146/8 xr108638.dLevel 5 IC 460-37146/9 xr108639.d

CURVETYPE



alpha-BHC Ave 72074 311135 571876 1369592 2557369 10.0 50.0 100 250 500gamma-BHC (Lindane) Ave 65831 272981 491580 1172351 2163100 10.0 50.0 100 250 500beta-BHC Ave 35661 147570 273259 637728 1195601 10.0 50.0 100 250 500delta-BHC Ave 65517 282029 527092 1279970 2387292 10.0 50.0 100 250 500Heptachlor Ave 66262 282507 521826 1241271 2303062 10.0 50.0 100 250 500Aldrin Ave 59512 266999 502394 1221823 2274452 10.0 50.0 100 250 500Heptachlor epoxide Ave 63113 271825 511152 1242984 2321322 10.0 50.0 100 250 500gamma-Chlordane Ave 64037 272329 512255 1256480 2364701 10.0 50.0 100 250 500alpha-Chlordane Ave 61705 267224 502049 1218970 2283442 10.0 50.0 100 250 5004,4'-DDE Ave 47259 231132 450457 1127145 2145422 10.0 50.0 100 250 500Endosulfan I Ave 56898 252887 480568 1196330 2215214 10.0 50.0 100 250 500Dieldrin Ave 55790 256872 497473 1244342 2343168 10.0 50.0 100 250 500Endrin Ave 46238 220380 422846 1055167 2008700 10.0 50.0 100 250 5004,4'-DDD Ave 40232 200372 391542 988702 1912370 10.0 50.0 100 250 500Endosulfan II Ave 51520 223198 422515 1028068 1942470 10.0 50.0 100 250 5004,4'-DDT Ave 40641 190354 368241 939092 1827480 10.0 50.0 100 250 500Endrin aldehyde Ave 41911 172075 322789 783823 1485364 10.0 50.0 100 250 500Methoxychlor Ave 23904 103158 190743 465865 903822 10.0 50.0 100 250 500Endosulfan sulfate Ave 44410 189322 355394 860822 1626926 10.0 50.0 100 250 500Endrin ketone Ave 52128 225899 424117 1019160 1892989 10.0 50.0 100 250 500Tetrachloro-m-xylene Ave 107532 216323 400310 590211 756017 25.0 50.0 100 150 200DCB Decachlorobiphenyl Ave 63708 127382 257005 386160 479113 25.0 50.0 100 150 200


FORM VI 8081A 06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




PESTGC1



N

05/11/2010 13:56



Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-37146/10 xf108640.d

ANALYTE LVL 1 AVG RTRT WINDOW

Chlordane (technical) Peak 1 3.4703.400 - 3.5403.470Chlordane (technical) Peak 2 3.7003.630 - 3.7703.700Chlordane (technical) Peak 3 4.8704.800 - 4.9404.870Chlordane (technical) Peak 4 6.5476.477 - 6.6176.547Chlordane (technical) Peak 5 6.7876.717 - 6.8576.787Chlordane (technical) Peak 6 6.9136.843 - 6.9836.913Chlordane (technical) Peak 7 7.9537.883 - 8.0237.953Chlordane (technical) Peak 8 8.1608.090 - 8.2308.160

FORM VI 8081A 06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




PESTGC1



N

05/11/2010 13:56

0.53(mm)CLP-2 ID:


Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-37146/10 xf108640.d

MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE

LVL 1

RRFANALYTE MIN RRF

110.38Chlordane (technical) Peak Ave 110 20.0147.36Chlordane (technical) Peak Ave 147 20.0138.38Chlordane (technical) Peak Ave 138 20.0350.23Chlordane (technical) Peak Ave 350 20.0309.03Chlordane (technical) Peak Ave 309 20.0285.79Chlordane (technical) Peak Ave 286 20.053.006Chlordane (technical) Peak Ave 53 20.0100.43Chlordane (technical) Peak Ave 100 20.0

FORM VI 8081A


06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




PESTGC1



N

05/11/2010 13:56



Calibration Files:


CURVETYPE


LVL 1 LVL 1

Chlordane (technical) Peak 1 Ave 110384 1000Chlordane (technical) Peak 2 Ave 147359 1000Chlordane (technical) Peak 3 Ave 138376 1000Chlordane (technical) Peak 4 Ave 350230 1000Chlordane (technical) Peak 5 Ave 309025 1000Chlordane (technical) Peak 6 Ave 285793 1000Chlordane (technical) Peak 7 Ave 53006 1000Chlordane (technical) Peak 8 Ave 100425 1000


FORM VI 8081A 06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




PESTGC1



N

05/11/2010 13:56



Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-37146/10 xr108640.d


Chlordane (technical) Peak 1 2.9132.843 - 2.9832.913Chlordane (technical) Peak 2 2.9832.913 - 3.0532.983Chlordane (technical) Peak 3 3.4333.363 - 3.5033.433Chlordane (technical) Peak 4 4.1934.123 - 4.2634.193Chlordane (technical) Peak 5 4.6534.583 - 4.7234.653Chlordane (technical) Peak 6 4.9634.893 - 5.0334.963Chlordane (technical) Peak 7 6.6376.567 - 6.7076.637Chlordane (technical) Peak 8 6.9206.850 - 6.9906.920

FORM VI 8081A 06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




PESTGC1



N

05/11/2010 13:56

0.53(mm)CLP-1 ID:


Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-37146/10 xr108640.d

MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE

LVL 1

RRFANALYTE MIN RRF

178.82Chlordane (technical) Peak Ave 179 20.0272.62Chlordane (technical) Peak Ave 273 20.0258.24Chlordane (technical) Peak Ave 258 20.0117.70Chlordane (technical) Peak Ave 118 20.0667.75Chlordane (technical) Peak Ave 668 20.01049.9Chlordane (technical) Peak Ave 1050 20.0143.63Chlordane (technical) Peak Ave 144 20.0228.52Chlordane (technical) Peak Ave 229 20.0

FORM VI 8081A


06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




PESTGC1



N

05/11/2010 13:56



Calibration Files:


CURVETYPE


LVL 1 LVL 1

Chlordane (technical) Peak 1 Ave 178816 1000Chlordane (technical) Peak 2 Ave 272618 1000Chlordane (technical) Peak 3 Ave 258236 1000Chlordane (technical) Peak 4 Ave 117700 1000Chlordane (technical) Peak 5 Ave 667752 1000Chlordane (technical) Peak 6 Ave 1049940 1000Chlordane (technical) Peak 7 Ave 143631 1000Chlordane (technical) Peak 8 Ave 228523 1000


FORM VI 8081A 06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




PESTGC1



N

05/11/2010 14:10



Calibration Files:



Toxaphene Peak 1 8.1978.127 - 8.2678.197Toxaphene Peak 2 8.5008.430 - 8.5708.500Toxaphene Peak 3 8.6038.533 - 8.6738.603Toxaphene Peak 4 8.8108.740 - 8.8808.810Toxaphene Peak 5 9.1139.043 - 9.1839.113Toxaphene Peak 6 9.1779.107 - 9.2479.177Toxaphene Peak 7 9.5009.430 - 9.5709.500Toxaphene Peak 8 9.6409.570 - 9.7109.640

FORM VI 8081A 06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




PESTGC1



N

05/11/2010 14:10

0.53(mm)CLP-2 ID:


Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-37146/11 xf108641.d

MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE

LVL 1

RRFANALYTE MIN RRF

122.49Toxaphene Peak 1 Ave 122 20.0112.92Toxaphene Peak 2 Ave 113 20.098.212Toxaphene Peak 3 Ave 98 20.064.477Toxaphene Peak 4 Ave 64 20.0101.14Toxaphene Peak 5 Ave 101 20.0121.79Toxaphene Peak 6 Ave 122 20.050.603Toxaphene Peak 7 Ave 51 20.056.145Toxaphene Peak 8 Ave 56 20.0

FORM VI 8081A


06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




PESTGC1



N

05/11/2010 14:10



Calibration Files:


CURVETYPE


LVL 1 LVL 1

Toxaphene Peak 1 Ave 122493 1000Toxaphene Peak 2 Ave 112915 1000Toxaphene Peak 3 Ave 98212 1000Toxaphene Peak 4 Ave 64477 1000Toxaphene Peak 5 Ave 101138 1000Toxaphene Peak 6 Ave 121791 1000Toxaphene Peak 7 Ave 50603 1000Toxaphene Peak 8 Ave 56145 1000


FORM VI 8081A 06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




PESTGC1



N

05/11/2010 14:10



Calibration Files:



Toxaphene Peak 1 7.5637.493 - 7.6337.563Toxaphene Peak 2 7.6407.570 - 7.7107.640Toxaphene Peak 3 7.8177.747 - 7.8877.817Toxaphene Peak 4 7.9437.873 - 8.0137.943Toxaphene Peak 5 8.0377.967 - 8.1078.037Toxaphene Peak 6 8.1178.047 - 8.1878.117Toxaphene Peak 7 8.4408.370 - 8.5108.440Toxaphene Peak 8 8.6108.540 - 8.6808.610

FORM VI 8081A 06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




PESTGC1



N

05/11/2010 14:10

0.53(mm)CLP-1 ID:


Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-37146/11 xr108641.d

MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE

LVL 1

RRFANALYTE MIN RRF

318.65Toxaphene Peak 1 Ave 319 20.0228.60Toxaphene Peak 2 Ave 229 20.0249.56Toxaphene Peak 3 Ave 250 20.0189.17Toxaphene Peak 4 Ave 189 20.0203.69Toxaphene Peak 5 Ave 204 20.0346.52Toxaphene Peak 6 Ave 347 20.0142.50Toxaphene Peak 7 Ave 143 20.088.612Toxaphene Peak 8 Ave 89 20.0

FORM VI 8081A


06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




PESTGC1



N

05/11/2010 14:10



Calibration Files:


CURVETYPE


LVL 1 LVL 1

Toxaphene Peak 1 Ave 318647 1000Toxaphene Peak 2 Ave 228602 1000Toxaphene Peak 3 Ave 249559 1000Toxaphene Peak 4 Ave 189171 1000Toxaphene Peak 5 Ave 203690 1000Toxaphene Peak 6 Ave 346524 1000Toxaphene Peak 7 Ave 142501 1000Toxaphene Peak 8 Ave 88612 1000


FORM VI 8081A 06/03/2010 of 623

FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:


PESTICIDES PERFORMANCE EVALUATION MIXTURE (PEM)

0.53(mm)

460-13139-1

PESTGC1

05/17/2010 05:13

05/11/2010 12:47

05/11/2010 13:42

PEM 460-37575/4

CLP-2

TestAmerica Edison

Lab File ID: xf108818.d Conc. Units: ug/L

#LIMITBREAKDOWN (%)PEAK AREARTANALYTE

7.87Endrin 609276 6.41 15

8.50Endrin aldehyde 12596

9.41Endrin ketone 29168


8.344,4'-DDT 552424 4.78 15

7.984,4'-DDD 18240

7.264,4'-DDE 9472

FORM VII 8081A

06/03/2010 of 623


TestAmerica

GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC1.i/8081T/front/May10/05-17-10/17may10a.b/xf108818.dLab Smp Id: SGDDT/Ei_00009 Inj Date : 17-MAY-2010 05:13 Operator : 462 Inst ID: PESTGC1.iSmp Info : SGDDT/Ei_00009Misc Info : Comment : Method : /chem1/PESTGC1.i/8081T/front/May10/05-17-10/17may10a.b/09Xf8081.mMeth Date : 17-May-2010 11:16 ferdie Quant Type: ESTDCal Date : 11-MAY-2010 14:10 Cal File: xf108641.dAls bottle: 1 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: END_DDT.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3





CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====

7 4,4'-DDD CAS #: 72-54-8

7.983 7.967 0.016 18240 9.49468 6.3 80.00- 120.00 100.00(a)

-------------------------------------------------------------------------------

8 4,4'-DDE CAS #: 72-55-9

7.260 7.230 0.030 9472 3.96424 2.6 80.00- 120.00 100.00(a)

-------------------------------------------------------------------------------

9 4,4'-DDT CAS #: 50-29-3

8.343 8.330 0.013 552424 310.464 210 80.00- 120.00 100.00

-------------------------------------------------------------------------------

14 Endrin CAS #: 72-20-8

7.873 7.857 0.016 609276 307.857 200 80.00- 120.00 100.00

-------------------------------------------------------------------------------

15 Endrin aldehyde CAS #: 7421-93-4

8.500 8.483 0.017 12596 7.17809 4.8 80.00- 120.00 100.00(a)

-------------------------------------------------------------------------------

06/03/2010 of 623


CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====

16 Endrin ketone CAS #: 53494-70-5

9.413 9.403 0.010 29168 13.2146 8.8 80.00- 120.00 100.00

-------------------------------------------------------------------------------

QC Flag Legend


06/03/2010 of 623


Date: 17-MAY-2010 05:13


Sample Info: SGDDT/Ei_00009 Operator: 462

06/03/2010 of 623

FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:


PESTICIDES PERFORMANCE EVALUATION MIXTURE (PEM)

0.53(mm)

460-13139-1

PESTGC1

05/17/2010 05:13

05/11/2010 12:47

05/11/2010 13:42

PEM 460-37575/4

CLP-1

TestAmerica Edison

Lab File ID: xr108818.d Conc. Units: ug/L


6.57Endrin 1349360 4.96 15

7.68Endrin aldehyde 19144

8.47Endrin ketone 51211


7.294,4'-DDT 1136924 4.07 15

6.754,4'-DDD 30034

5.224,4'-DDE 18162

FORM VII 8081A

06/03/2010 of 623


TestAmerica

GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC1.i/8081T/rear/May10/05-17-10/17may10a.b/xr108818.dLab Smp Id: SGDDT/Ei_00009 Inj Date : 17-MAY-2010 05:13 Operator : 462 Inst ID: PESTGC1.iSmp Info : SGDDT/Ei_00009Misc Info : Comment : Method : /chem1/PESTGC1.i/8081T/rear/May10/05-17-10/17may10a.b/09Xr8081.mMeth Date : 17-May-2010 08:58 ferdie Quant Type: ESTDCal Date : 11-MAY-2010 14:10 Cal File: xr108641.dAls bottle: 1 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: END_DDT.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3





CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====

7 4,4'-DDD CAS #: 72-54-8

6.753 6.737 0.016 30034 7.61295 5.1 80.00- 120.00 100.00(a)

-------------------------------------------------------------------------------

8 4,4'-DDE CAS #: 72-55-9

5.220 5.203 0.017 18162 4.00882 2.7 80.00- 120.00 100.00(a)

-------------------------------------------------------------------------------

9 4,4'-DDT CAS #: 50-29-3

7.293 7.287 0.006 1136924 299.744 200 80.00- 120.00 100.00

-------------------------------------------------------------------------------

14 Endrin CAS #: 72-20-8

6.570 6.557 0.013 1349360 313.835 210 80.00- 120.00 100.00

-------------------------------------------------------------------------------


7.680 7.673 0.007 19144 5.64170 3.8 80.00- 120.00 100.00(a)

-------------------------------------------------------------------------------

06/03/2010 of 623


CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====


8.470 8.463 0.007 51211 11.7270 7.8 80.00- 120.00 100.00

-------------------------------------------------------------------------------

QC Flag Legend


06/03/2010 of 623


Date: 17-MAY-2010 05:13


Sample Info: SGDDT/Ei_00009 Operator: 462

06/03/2010 of 623

FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:


PESTICIDES CONTINUING CALIBRATION DATA

0.53(mm)

460-13139-1

PESTGC1

05/17/2010 05:29

05/11/2010 12:47

05/11/2010 13:42

CCVRT 460-37575/5

CLP-2

TestAmerica Edison




alpha-BHC Ave 32973156 104 100 4.5 15.0

gamma-BHC (Lindane) Ave 29512874 103 100 2.7 15.0

beta-BHC Ave 14351454 98.7 100 -1.3 15.0

delta-BHC Ave 31502964 106 100 6.3 15.0

Heptachlor Ave 32423149 103 100 3.0 15.0

Aldrin Ave 33743123 108 100 8.0 15.0

Heptachlor epoxide Ave 32123088 104 100 4.0 15.0

gamma-Chlordane Ave 34333137 109 100 9.4 15.0

alpha-Chlordane Ave 29642886 103 100 2.7 15.0

Endosulfan I Ave 27342645 103 100 3.4 15.0

4,4'-DDE Ave 25452389 107 100 6.5 15.0

Dieldrin Ave 26302526 104 100 4.1 15.0

Endrin Ave 20521979 104 100 3.7 15.0

4,4'-DDD Ave 19451921 101 100 1.2 15.0

Endosulfan II Ave 21942178 101 100 0.7 15.0

4,4'-DDT Ave 18601779 105 100 4.5 15.0

Endrin aldehyde Ave 17841755 102 100 1.6 15.0

Endosulfan sulfate Ave 19801948 102 100 1.7 15.0

Methoxychlor Ave 918.8999 92.0 100 -8.0 15.0

Endrin ketone Ave 22342207 101 100 1.2 15.0

Tetrachloro-m-xylene Ave 24642246 110 100 9.7 15.0

DCB Decachlorobiphenyl Ave 14171309 108 100 8.3 15.0

FORM VII 8081A

06/03/2010 of 623

FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:


PESTICIDES CONTINUING CALIBRATION RETENTION TIME SUMMARY

0.53(mm)

460-13139-1

PESTGC1

05/17/2010 05:29

05/11/2010 12:47

05/11/2010 13:42

CCVRT 460-37575/5

CLP-2

TestAmerica Edison

Lab File ID: xf108819.d

Analyte RTTO FROM

RT WINDOW

alpha-BHC 2.77 2.72 2.82

gamma-BHC (Lindane) 3.11 3.06 3.16

beta-BHC 3.20 3.14 3.24

delta-BHC 3.57 3.52 3.62

Heptachlor 3.70 3.64 3.74

Aldrin 4.49 4.43 4.53

Heptachlor epoxide 6.04 5.96 6.10

gamma-Chlordane 6.54 6.46 6.60

alpha-Chlordane 6.90 6.83 6.97

Endosulfan I 7.04 6.96 7.10

4,4'-DDE 7.23 7.15 7.29

Dieldrin 7.49 7.42 7.56

Endrin 7.86 7.78 7.92

4,4'-DDD 7.97 7.89 8.03

Endosulfan II 8.10 8.02 8.16

4,4'-DDT 8.33 8.26 8.40

Endrin aldehyde 8.48 8.41 8.55

Endosulfan sulfate 8.81 8.74 8.88

Methoxychlor 9.12 9.05 9.19

Endrin ketone 9.40 9.33 9.47

Tetrachloro-m-xylene 2.29 2.24 2.34

DCB Decachlorobiphenyl 10.33 10.23 10.43

Form VII 8081A

06/03/2010 of 623

FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:



0.53(mm)

460-13139-1

PESTGC1

05/17/2010 05:29

05/11/2010 12:47

05/11/2010 13:42

CCVRT 460-37575/5

CLP-1

TestAmerica Edison




alpha-BHC Ave 61405948 103 100 3.2 15.0


beta-BHC Ave 29512838 104 100 4.0 15.0

delta-BHC Ave 57055472 104 100 4.3 15.0

Heptachlor Ave 56315413 104 100 4.0 15.0

Aldrin Ave 54675150 106 100 6.1 15.0


gamma-Chlordane Ave 54605346 102 100 2.1 15.0

alpha-Chlordane Ave 49395196 95.1 100 -4.9 15.0

4,4'-DDE Ave 47704531 105 100 5.3 15.0

Endosulfan I Ave 52234954 105 100 5.4 15.0

Dieldrin Ave 53695071 106 100 5.9 15.0

Endrin Ave 46994300 109 100 9.3 15.0

4,4'-DDD Ave 40633945 103 100 3.0 15.0


4,4'-DDT Ave 41663793 110 100 9.8 15.0

Endrin aldehyde Ave 36283393 107 100 6.9 15.0

Methoxychlor Ave 21142006 105 100 5.3 15.0

Endosulfan sulfate Ave 38753696 105 100 4.9 15.0

Endrin ketone Ave 45364367 104 100 3.9 15.0



FORM VII 8081A

06/03/2010 of 623

FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:



0.53(mm)

460-13139-1

PESTGC1

05/17/2010 05:29

05/11/2010 12:47

05/11/2010 13:42

CCVRT 460-37575/5

CLP-1

TestAmerica Edison

Lab File ID: xr108819.d

Analyte RTTO FROM

RT WINDOW

alpha-BHC 2.38 2.33 2.43


beta-BHC 2.67 2.62 2.72

delta-BHC 2.81 2.76 2.86


Aldrin 3.28 3.22 3.32




4,4'-DDE 5.20 5.13 5.27


Dieldrin 5.98 5.90 6.04

Endrin 6.56 6.48 6.62

4,4'-DDD 6.74 6.66 6.80


4,4'-DDT 7.29 7.21 7.35







Form VII 8081A

06/03/2010 of 623

FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:



0.53(mm)

460-13139-1

PESTGC1

05/17/2010 10:04

05/11/2010 12:47

05/11/2010 13:42

CCV 460-37575/23

CLP-2

TestAmerica Edison




alpha-BHC Ave 31283156 99.1 100 -0.9 15.0

gamma-BHC (Lindane) Ave 28242874 98.3 100 -1.7 15.0

beta-BHC Ave 13851454 95.3 100 -4.7 15.0

delta-BHC Ave 29842964 101 100 0.7 15.0

Heptachlor Ave 30203149 95.9 100 -4.1 15.0

Aldrin Ave 31583123 101 100 1.1 15.0

Heptachlor epoxide Ave 29963088 97.0 100 -3.0 15.0

gamma-Chlordane Ave 30003137 95.6 100 -4.4 15.0

alpha-Chlordane Ave 27702886 96.0 100 -4.0 15.0

Endosulfan I Ave 25562645 96.7 100 -3.3 15.0

4,4'-DDE Ave 23772389 99.5 100 -0.5 15.0

Dieldrin Ave 24712526 97.8 100 -2.2 15.0

Endrin Ave 19251979 97.3 100 -2.7 15.0

4,4'-DDD Ave 19401921 101 100 1.0 15.0

Endosulfan II Ave 20592178 94.6 100 -5.4 15.0

4,4'-DDT Ave 15681779 88.1 100 -11.9 15.0

Endrin aldehyde Ave 16121755 91.9 100 -8.1 15.0

Endosulfan sulfate Ave 18371948 94.3 100 -5.7 15.0

Methoxychlor Ave 888.7999 88.9 100 -11.1 15.0

Endrin ketone Ave 20562207 93.2 100 -6.8 15.0


DCB Decachlorobiphenyl Ave 13071309 99.9 100 -0.1 15.0

FORM VII 8081A

06/03/2010 of 623

FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:



0.53(mm)

460-13139-1

PESTGC1

05/17/2010 10:04

05/11/2010 12:47

05/11/2010 13:42

CCV 460-37575/23

CLP-2

TestAmerica Edison

Lab File ID: xf108837.d

Analyte RTTO FROM

RT WINDOW

alpha-BHC 2.77 2.72 2.82


beta-BHC 3.19 3.14 3.24

delta-BHC 3.57 3.52 3.62


Aldrin 4.48 4.43 4.53





4,4'-DDE 7.22 7.15 7.29

Dieldrin 7.49 7.42 7.56

Endrin 7.85 7.78 7.92

4,4'-DDD 7.96 7.89 8.03


4,4'-DDT 8.33 8.26 8.40







Form VII 8081A

06/03/2010 of 623

FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:



0.53(mm)

460-13139-1

PESTGC1

05/17/2010 10:04

05/11/2010 12:47

05/11/2010 13:42

CCV 460-37575/23

CLP-1

TestAmerica Edison




alpha-BHC Ave 61885948 104 100 4.0 15.0


beta-BHC Ave 29502838 104 100 3.9 15.0

delta-BHC Ave 57205472 105 100 4.5 15.0

Heptachlor Ave 54575413 101 100 0.8 15.0

Aldrin Ave 53275150 103 100 3.4 15.0


gamma-Chlordane Ave 53045346 99.2 100 -0.8 15.0

alpha-Chlordane Ave 51965196 100 100 0.0 15.0

4,4'-DDE Ave 46334531 102 100 2.3 15.0

Endosulfan I Ave 50604954 102 100 2.1 15.0

Dieldrin Ave 51915071 102 100 2.4 15.0

Endrin Ave 44854300 104 100 4.3 15.0

4,4'-DDD Ave 42603945 108 100 8.0 15.0


4,4'-DDT Ave 35593793 93.8 100 -6.2 15.0

Endrin aldehyde Ave 32893393 96.9 100 -3.1 15.0

Methoxychlor Ave 19012006 94.7 100 -5.3 15.0

Endosulfan sulfate Ave 36073696 97.6 100 -2.4 15.0

Endrin ketone Ave 41254367 94.5 100 -5.5 15.0


DCB Decachlorobiphenyl Ave 24042527 95.1 100 -4.9 15.0

FORM VII 8081A

06/03/2010 of 623

FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:



0.53(mm)

460-13139-1

PESTGC1

05/17/2010 10:04

05/11/2010 12:47

05/11/2010 13:42

CCV 460-37575/23

CLP-1

TestAmerica Edison

Lab File ID: xr108837.d

Analyte RTTO FROM

RT WINDOW

alpha-BHC 2.38 2.33 2.43


beta-BHC 2.67 2.62 2.72

delta-BHC 2.81 2.76 2.86


Aldrin 3.27 3.22 3.32




4,4'-DDE 5.20 5.13 5.27


Dieldrin 5.97 5.90 6.04

Endrin 6.55 6.48 6.62

4,4'-DDD 6.73 6.66 6.80


4,4'-DDT 7.28 7.21 7.35







Form VII 8081A

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1




Solid

TestAmerica Edison


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/17/2010 09:37

N

10(mL)

1(uL)


% Moisture:






FORM I 8081A

06/03/2010 of 623


TestAmerica

GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC1.i/8081T/front/May10/05-17-10/17may10a.b/xf108835.dLab Smp Id: mb 460-37420/1-a Inj Date : 17-MAY-2010 09:37 Operator : 462 Inst ID: PESTGC1.iSmp Info : mb 460-37420/1-aMisc Info : Comment : Method : /chem1/PESTGC1.i/8081T/front/May10/05-17-10/17may10a.b/09Xf8081.mMeth Date : 17-May-2010 11:16 ferdie Quant Type: ESTDCal Date : 11-MAY-2010 14:10 Cal File: xf108641.dAls bottle: 1 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: Allpest.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3





CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====


2.283 2.287 -0.004 85900 38.2407 25 80.00- 120.00 100.00

-------------------------------------------------------------------------------


10.333 10.333 0.000 95179 72.7350 48 80.00- 120.00 100.00

-------------------------------------------------------------------------------

06/03/2010 of 623


Date: 17-MAY-2010 09:37


Sample Info: mb 460-37420/1-a Operator: 462

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1




Solid

TestAmerica Edison


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/17/2010 09:37

N

10(mL)

1(uL)


% Moisture:




Aldrin309-00-2 6.7 6.7 1.5U

alpha-BHC319-84-6 6.7 6.7 1.2U

beta-BHC319-85-7 6.7 6.7 0.91U

delta-BHC319-86-8 6.7 6.7 1.0U


Chlordane57-74-9 67 67 15U

4,4'-DDD72-54-8 6.7 6.7 0.80U

4,4'-DDE72-55-9 6.7 6.7 1.3U

4,4'-DDT50-29-3 6.7 6.7 0.84U

Dieldrin60-57-1 6.7 6.7 1.3U

Endosulfan I959-98-8 6.7 6.7 1.4U

Endosulfan II33213-65-9 6.7 6.7 1.0U


Endrin72-20-8 6.7 6.7 0.94U


Heptachlor76-44-8 6.7 6.7 0.96U


Toxaphene8001-35-2 67 67 14U




FORM I 8081A

06/03/2010 of 623


TestAmerica

GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC1.i/8081T/rear/May10/05-17-10/17may10a.b/xr108835.dLab Smp Id: mb 460-37420/1-a Inj Date : 17-MAY-2010 09:37 Operator : 462 Inst ID: PESTGC1.iSmp Info : mb 460-37420/1-aMisc Info : Comment : Method : /chem1/PESTGC1.i/8081T/rear/May10/05-17-10/17may10a.b/09Xr8081.mMeth Date : 17-May-2010 08:58 ferdie Quant Type: ESTDCal Date : 11-MAY-2010 14:10 Cal File: xr108641.dAls bottle: 1 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: Allpest.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3





CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====


1.983 1.987 -0.004 152446 37.4640 25 80.00- 120.00 100.00

-------------------------------------------------------------------------------


9.513 9.513 0.000 148995 58.9567 39 80.00- 120.00 100.00

-------------------------------------------------------------------------------

06/03/2010 of 623


Date: 17-MAY-2010 09:37


Sample Info: mb 460-37420/1-a Operator: 462

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1




Solid

TestAmerica Edison


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/17/2010 05:43

N

10(mL)

1(uL)


% Moisture:




Aldrin309-00-2 88.9 6.7 1.5

alpha-BHC319-84-6 96.3 6.7 1.2

beta-BHC319-85-7 104 6.7 0.91

delta-BHC319-86-8 121 6.7 1.0

gamma-BHC (Lindane)58-89-9 98.6 6.7 0.78

Chlordane57-74-9 67 67 15U

4,4'-DDD72-54-8 94.7 6.7 0.80

4,4'-DDE72-55-9 98.1 6.7 1.3

4,4'-DDT50-29-3 99.1 6.7 0.84

Dieldrin60-57-1 88.6 6.7 1.3

Endosulfan I959-98-8 93.6 6.7 1.4

Endosulfan II33213-65-9 101 6.7 1.0

Endosulfan sulfate1031-07-8 103 6.7 0.86

Endrin72-20-8 101 6.7 0.94

Endrin aldehyde7421-93-4 103 6.7 1.7

Heptachlor76-44-8 93.0 6.7 0.96

Heptachlor epoxide1024-57-3 97.0 6.7 1.4

Toxaphene8001-35-2 67 67 14U




FORM I 8081A

06/03/2010 of 623


TestAmerica

GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC1.i/8081T/front/May10/05-17-10/17may10a.b/xf108820.dLab Smp Id: lcs 460-37420/2-a Inj Date : 17-MAY-2010 05:43 Operator : 462 Inst ID: PESTGC1.iSmp Info : lcs 460-37420/2-aMisc Info : Comment : Method : /chem1/PESTGC1.i/8081T/front/May10/05-17-10/17may10a.b/09Xf8081.mMeth Date : 17-May-2010 11:24 ferdie Quant Type: ESTDCal Date : 11-MAY-2010 14:10 Cal File: xf108641.dAls bottle: 1 QC Sample: BSDil Factor: 1.00000 Integrator: Falcon Compound Sublist: Allpest.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3





CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====


2.297 2.287 0.010 84665 37.6912 25 80.00- 120.00 100.00

-------------------------------------------------------------------------------

2 alpha-BHC CAS #: 319-84-6

2.787 2.773 0.014 455846 144.444 96 80.00- 120.00 100.00

-------------------------------------------------------------------------------


3.130 3.110 0.020 424962 147.882 98 80.00- 120.00 100.00

-------------------------------------------------------------------------------

3 beta-BHC CAS #: 319-85-7

3.217 3.193 0.024 227814 156.710 100 80.00- 120.00 100.00

-------------------------------------------------------------------------------

4 delta-BHC CAS #: 319-86-8

3.600 3.567 0.033 539355 181.992 120 80.00- 120.00 100.00

-------------------------------------------------------------------------------

06/03/2010 of 623


CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====

17 Heptachlor CAS #: 76-44-8

3.733 3.693 0.040 439419 139.526 93 80.00- 120.00 100.00

-------------------------------------------------------------------------------

1 Aldrin CAS #: 309-00-2

4.540 4.480 0.060 416438 133.338 89 80.00- 120.00 100.00

-------------------------------------------------------------------------------

18 Heptachlor epoxide CAS #: 1024-57-3

6.100 6.033 0.067 449342 145.509 97 80.00- 120.00 100.00

-------------------------------------------------------------------------------


6.593 6.533 0.060 447261 142.559 95 80.00- 120.00 100.00

-------------------------------------------------------------------------------


6.953 6.897 0.056 399977 138.577 92 80.00- 120.00 100.00

-------------------------------------------------------------------------------

11 Endosulfan I CAS #: 959-98-8

7.080 7.033 0.047 371309 140.399 94 80.00- 120.00 100.00

-------------------------------------------------------------------------------

8 4,4'-DDE CAS #: 72-55-9

7.263 7.223 0.040 351669 147.181 98 80.00- 120.00 100.00

-------------------------------------------------------------------------------


7.517 7.487 0.030 335800 132.944 89 80.00- 120.00 100.00

-------------------------------------------------------------------------------

14 Endrin CAS #: 72-20-8

7.880 7.853 0.027 299228 151.195 100 80.00- 120.00 100.00

-------------------------------------------------------------------------------

7 4,4'-DDD CAS #: 72-54-8

7.987 7.963 0.024 272949 142.081 95 80.00- 120.00 100.00

-------------------------------------------------------------------------------

12 Endosulfan II CAS #: 33213-65-9

8.117 8.093 0.024 331407 152.166 100 80.00- 120.00 100.00

-------------------------------------------------------------------------------

9 4,4'-DDT CAS #: 50-29-3

8.350 8.327 0.023 264580 148.695 99 80.00- 120.00 100.00

-------------------------------------------------------------------------------


8.503 8.480 0.023 272239 155.141 100 80.00- 120.00 100.00

-------------------------------------------------------------------------------

13 Endosulfan sulfate CAS #: 1031-07-8

8.830 8.807 0.023 301417 154.742 100 80.00- 120.00 100.00

-------------------------------------------------------------------------------

19 Methoxychlor CAS #: 72-43-5

9.140 9.120 0.020 127407 127.521 85 80.00- 120.00 100.00

-------------------------------------------------------------------------------


9.417 9.400 0.017 310105 140.494 94 80.00- 120.00 100.00

-------------------------------------------------------------------------------

06/03/2010 of 623


CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====


10.343 10.333 0.010 60842 46.4952 31 80.00- 120.00 100.00

-------------------------------------------------------------------------------

06/03/2010 of 623


Date: 17-MAY-2010 05:43


Sample Info: lcs 460-37420/2-a Operator: 462

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1




Solid

TestAmerica Edison


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/17/2010 05:43

N

10(mL)

1(uL)


% Moisture:




Aldrin309-00-2 82.2 6.7 1.5

alpha-BHC319-84-6 89.0 6.7 1.2

beta-BHC319-85-7 102 6.7 0.91

delta-BHC319-86-8 109 6.7 1.0

gamma-BHC (Lindane)58-89-9 90.2 6.7 0.78

Chlordane57-74-9 67 67 15U

4,4'-DDD72-54-8 93.4 6.7 0.80

4,4'-DDE72-55-9 94.8 6.7 1.3

4,4'-DDT50-29-3 97.2 6.7 0.84

Dieldrin60-57-1 89.6 6.7 1.3

Endosulfan I959-98-8 93.3 6.7 1.4

Endosulfan II33213-65-9 101 6.7 1.0


Endrin72-20-8 104 6.7 0.94

Endrin aldehyde7421-93-4 104 6.7 1.7

Heptachlor76-44-8 87.2 6.7 0.96

Heptachlor epoxide1024-57-3 93.5 6.7 1.4

Toxaphene8001-35-2 67 67 14U




FORM I 8081A

06/03/2010 of 623


TestAmerica

GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC1.i/8081T/rear/May10/05-17-10/17may10a.b/xr108820.dLab Smp Id: lcs 460-37420/2-a Inj Date : 17-MAY-2010 05:43 Operator : 462 Inst ID: PESTGC1.iSmp Info : lcs 460-37420/2-aMisc Info : Comment : Method : /chem1/PESTGC1.i/8081T/rear/May10/05-17-10/17may10a.b/09Xr8081.mMeth Date : 17-May-2010 08:58 ferdie Quant Type: ESTDCal Date : 11-MAY-2010 14:10 Cal File: xr108641.dAls bottle: 1 QC Sample: BSDil Factor: 1.00000 Integrator: Falcon Compound Sublist: Allpest.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3





CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====


1.980 1.987 -0.007 144623 35.5415 24 80.00- 120.00 100.00

-------------------------------------------------------------------------------

2 alpha-BHC CAS #: 319-84-6

2.380 2.380 0.000 794220 133.518 89 80.00- 120.00 100.00

-------------------------------------------------------------------------------


2.607 2.607 0.000 702767 135.282 90 80.00- 120.00 100.00

-------------------------------------------------------------------------------

3 beta-BHC CAS #: 319-85-7

2.673 2.673 0.000 432408 152.340 100 80.00- 120.00 100.00

-------------------------------------------------------------------------------

4 delta-BHC CAS #: 319-86-8

2.810 2.810 0.000 897926 164.109 110 80.00- 120.00 100.00

-------------------------------------------------------------------------------

06/03/2010 of 623


CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====

17 Heptachlor CAS #: 76-44-8

2.987 2.987 0.000 708298 130.847 87 80.00- 120.00 100.00

-------------------------------------------------------------------------------

1 Aldrin CAS #: 309-00-2

3.277 3.277 0.000 634789 123.254 82 80.00- 120.00 100.00

-------------------------------------------------------------------------------

18 Heptachlor epoxide CAS #: 1024-57-3

4.363 4.350 0.013 742239 140.183 93 80.00- 120.00 100.00

-------------------------------------------------------------------------------


4.670 4.653 0.017 731852 136.907 91 80.00- 120.00 100.00

-------------------------------------------------------------------------------


5.003 4.987 0.016 713323 137.292 92 80.00- 120.00 100.00

-------------------------------------------------------------------------------

8 4,4'-DDE CAS #: 72-55-9

5.223 5.203 0.020 643942 142.135 95 80.00- 120.00 100.00

-------------------------------------------------------------------------------

11 Endosulfan I CAS #: 959-98-8

5.357 5.337 0.020 693640 140.022 93 80.00- 120.00 100.00

-------------------------------------------------------------------------------


5.997 5.977 0.020 681463 134.385 90 80.00- 120.00 100.00

-------------------------------------------------------------------------------

14 Endrin CAS #: 72-20-8

6.573 6.557 0.016 671332 156.139 100 80.00- 120.00 100.00

-------------------------------------------------------------------------------

7 4,4'-DDD CAS #: 72-54-8

6.753 6.737 0.016 552980 140.168 93 80.00- 120.00 100.00

-------------------------------------------------------------------------------

12 Endosulfan II CAS #: 33213-65-9

7.083 7.067 0.016 658465 150.759 100 80.00- 120.00 100.00

-------------------------------------------------------------------------------

9 4,4'-DDT CAS #: 50-29-3

7.300 7.287 0.013 552775 145.736 97 80.00- 120.00 100.00

-------------------------------------------------------------------------------


7.680 7.673 0.007 528827 155.844 100 80.00- 120.00 100.00

-------------------------------------------------------------------------------

19 Methoxychlor CAS #: 72-43-5

7.890 7.883 0.007 265576 132.363 88 80.00- 120.00 100.00

-------------------------------------------------------------------------------

13 Endosulfan sulfate CAS #: 1031-07-8

8.160 8.153 0.007 561203 151.853 100 80.00- 120.00 100.00

-------------------------------------------------------------------------------


8.473 8.463 0.010 616529 141.182 94 80.00- 120.00 100.00

-------------------------------------------------------------------------------

06/03/2010 of 623


CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====


9.520 9.513 0.007 116320 46.0273 31 80.00- 120.00 100.00

-------------------------------------------------------------------------------

06/03/2010 of 623


Date: 17-MAY-2010 05:43


Sample Info: lcs 460-37420/2-a Operator: 462

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1




Solid

TestAmerica Edison

05/12/2010 15:30


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/17/2010 06:36

N

10(mL)

1(uL)


% Moisture: 13.0




Aldrin309-00-2 151 7.7 1.7

alpha-BHC319-84-6 154 7.7 1.4

beta-BHC319-85-7 153 7.7 1.0

delta-BHC319-86-8 167 7.7 1.2

gamma-BHC (Lindane)58-89-9 155 7.7 0.90

Chlordane57-74-9 77 77 17U

4,4'-DDD72-54-8 159 7.7 0.92

4,4'-DDE72-55-9 169 7.7 1.5

4,4'-DDT50-29-3 162 7.7 0.96

Dieldrin60-57-1 150 7.7 1.5

Endosulfan I959-98-8 144 7.7 1.6

Endosulfan II33213-65-9 152 7.7 1.2


Endrin72-20-8 168 7.7 1.1

Endrin aldehyde7421-93-4 145 7.7 1.9

Heptachlor76-44-8 139 7.7 1.1

Heptachlor epoxide1024-57-3 149 7.7 1.6

Toxaphene8001-35-2 77 77 16U




FORM I 8081A

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1




Solid

TestAmerica Edison

05/12/2010 15:30


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/17/2010 06:36

N

10(mL)

1(uL)


% Moisture: 13.0




Aldrin309-00-2 127 7.7 1.7

alpha-BHC319-84-6 129 7.7 1.4

beta-BHC319-85-7 128 7.7 1.0

delta-BHC319-86-8 142 7.7 1.2


Chlordane57-74-9 77 77 17U

4,4'-DDD72-54-8 134 7.7 0.92

4,4'-DDE72-55-9 135 7.7 1.5

4,4'-DDT50-29-3 131 7.7 0.96

Dieldrin60-57-1 128 7.7 1.5

Endosulfan I959-98-8 135 7.7 1.6

Endosulfan II33213-65-9 123 7.7 1.2


Endrin72-20-8 148 7.7 1.1

Endrin aldehyde7421-93-4 116 7.7 1.9

Heptachlor76-44-8 137 7.7 1.1


Toxaphene8001-35-2 77 77 16U




FORM I 8081A

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1




Solid

TestAmerica Edison

05/12/2010 15:30


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/17/2010 06:50

N

10(mL)

1(uL)


% Moisture: 13.0




Aldrin309-00-2 145 7.7 1.7

alpha-BHC319-84-6 145 7.7 1.4

beta-BHC319-85-7 144 7.7 1.0

delta-BHC319-86-8 159 7.7 1.2


Chlordane57-74-9 77 77 17U

4,4'-DDD72-54-8 156 7.7 0.92

4,4'-DDE72-55-9 161 7.7 1.5

4,4'-DDT50-29-3 150 7.7 0.97

Dieldrin60-57-1 140 7.7 1.5

Endosulfan I959-98-8 137 7.7 1.6

Endosulfan II33213-65-9 145 7.7 1.2


Endrin72-20-8 163 7.7 1.1

Endrin aldehyde7421-93-4 137 7.7 1.9

Heptachlor76-44-8 125 7.7 1.1


Toxaphene8001-35-2 77 77 16U




FORM I 8081A

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1




Solid

TestAmerica Edison

05/12/2010 15:30


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/17/2010 06:50

N

10(mL)

1(uL)


% Moisture: 13.0




Aldrin309-00-2 122 7.7 1.7

alpha-BHC319-84-6 122 7.7 1.4

beta-BHC319-85-7 125 7.7 1.0

delta-BHC319-86-8 134 7.7 1.2


Chlordane57-74-9 77 77 17U

4,4'-DDD72-54-8 118 7.7 0.92

4,4'-DDE72-55-9 122 7.7 1.5

4,4'-DDT50-29-3 118 7.7 0.97

Dieldrin60-57-1 120 7.7 1.5

Endosulfan I959-98-8 126 7.7 1.6

Endosulfan II33213-65-9 113 7.7 1.2


Endrin72-20-8 133 7.7 1.1

Endrin aldehyde7421-93-4 95.9 7.7 1.9

Heptachlor76-44-8 122 7.7 1.1


Toxaphene8001-35-2 77 77 16U



2051-24-3 DCB Decachlorobiphenyl p56 10-165

FORM I 8081A

06/03/2010 of 623

Lab Name: Job No.:

SDG No.:

Instrument ID:


PESTICIDES ANALYSIS RUN LOG

DILUTION

FACTOR



PESTGC1

37146

Start Date:

End Date: 05/11/2010 14:23

05/11/2010 11:47

RINSE 460-37146/1 CLP-2 0.53(mm)105/11/2010 11:47

RINSE 460-37146/1 CLP-1 0.53(mm)105/11/2010 11:47

PIBLK 460-37146/2 CLP-2 0.53(mm)105/11/2010 12:04

PIBLK 460-37146/2 CLP-1 0.53(mm)105/11/2010 12:04

RESC 460-37146/3 CLP-2 0.53(mm)105/11/2010 12:18

RESC 460-37146/3 CLP-1 0.53(mm)105/11/2010 12:18

PEM 460-37146/4 CLP-2 0.53(mm)105/11/2010 12:32

PEM 460-37146/4 CLP-1 0.53(mm)105/11/2010 12:32

IC 460-37146/5 CLP-2 0.53(mm)105/11/2010 12:47 xf108635.d

IC 460-37146/5 CLP-1 0.53(mm)105/11/2010 12:47 xr108635.d

IC 460-37146/6 CLP-2 0.53(mm)105/11/2010 13:00 xf108636.d

IC 460-37146/6 CLP-1 0.53(mm)105/11/2010 13:00 xr108636.d

IC 460-37146/7 CLP-2 0.53(mm)105/11/2010 13:14 xf108637.d

IC 460-37146/7 CLP-1 0.53(mm)105/11/2010 13:14 xr108637.d

IC 460-37146/8 CLP-2 0.53(mm)105/11/2010 13:28 xf108638.d

IC 460-37146/8 CLP-1 0.53(mm)105/11/2010 13:28 xr108638.d

IC 460-37146/9 CLP-2 0.53(mm)105/11/2010 13:42 xf108639.d

IC 460-37146/9 CLP-1 0.53(mm)105/11/2010 13:42 xr108639.d

IC 460-37146/10 CLP-2 0.53(mm)105/11/2010 13:56 xf108640.d

IC 460-37146/10 CLP-1 0.53(mm)105/11/2010 13:56 xr108640.d

IC 460-37146/11 CLP-2 0.53(mm)105/11/2010 14:10 xf108641.d

IC 460-37146/11 CLP-1 0.53(mm)105/11/2010 14:10 xr108641.d

ICV 460-37146/12 CLP-2 0.53(mm)105/11/2010 14:23

ICV 460-37146/12 CLP-1 0.53(mm)105/11/2010 14:23

8081A

06/03/2010 of 623

Lab Name: Job No.:

SDG No.:

Instrument ID:



DILUTION

FACTOR



PESTGC1

37575

Start Date:

End Date: 05/17/2010 10:04

05/17/2010 04:31

RINSE 460-37575/1 CLP-2 0.53(mm)105/17/2010 04:31

RINSE 460-37575/1 CLP-1 0.53(mm)105/17/2010 04:31

PIBLK 460-37575/2 CLP-2 0.53(mm)105/17/2010 04:45

PIBLK 460-37575/2 CLP-1 0.53(mm)105/17/2010 04:45

ZZZZZ CLP-2 0.53(mm)105/17/2010 04:59

ZZZZZ CLP-1 0.53(mm)105/17/2010 04:59

PEM 460-37575/4 CLP-2 0.53(mm)105/17/2010 05:13 xf108818.d

PEM 460-37575/4 CLP-1 0.53(mm)105/17/2010 05:13 xr108818.d

CCVRT 460-37575/5 CLP-2 0.53(mm)105/17/2010 05:29 xf108819.d

CCVRT 460-37575/5 CLP-1 0.53(mm)105/17/2010 05:29 xr108819.d

LCS 460-37420/2-A CLP-2 0.53(mm)105/17/2010 05:43 xf108820.d

LCS 460-37420/2-A CLP-1 0.53(mm)105/17/2010 05:43 xr108820.d

ZZZZZ CLP-2 0.53(mm)105/17/2010 06:23

ZZZZZ CLP-1 0.53(mm)105/17/2010 06:23

460-13147-A-2-B MS CLP-2 0.53(mm)105/17/2010 06:36 xf108822.d

460-13147-A-2-B MS CLP-1 0.53(mm)105/17/2010 06:36 xr108822.d

460-13147-A-2-C MSD CLP-2 0.53(mm)105/17/2010 06:50 xf108823.d

460-13147-A-2-C MSD CLP-1 0.53(mm)105/17/2010 06:50 xr108823.d

ZZZZZ CLP-2 0.53(mm)105/17/2010 07:04

ZZZZZ CLP-1 0.53(mm)105/17/2010 07:04

ZZZZZ CLP-2 0.53(mm)105/17/2010 07:18

ZZZZZ CLP-1 0.53(mm)105/17/2010 07:18

ZZZZZ CLP-2 0.53(mm)105/17/2010 07:32

ZZZZZ CLP-1 0.53(mm)105/17/2010 07:32

ZZZZZ CLP-2 0.53(mm)105/17/2010 07:46

ZZZZZ CLP-1 0.53(mm)105/17/2010 07:46

460-13139-2 TB-3 6-7 CLP-2 0.53(mm)105/17/2010 08:00 xf108828.d

460-13139-2 TB-3 6-7 CLP-1 0.53(mm)105/17/2010 08:00 xr108828.d

ZZZZZ CLP-2 0.53(mm)105/17/2010 08:13

ZZZZZ CLP-1 0.53(mm)105/17/2010 08:13

460-13139-4 TB-2 5-6 CLP-2 0.53(mm)105/17/2010 08:27 xf108830.d

460-13139-4 TB-2 5-6 CLP-1 0.53(mm)105/17/2010 08:27 xr108830.d

460-13139-5 TB-1 2-3 CLP-2 0.53(mm)105/17/2010 08:41 xf108831.d

460-13139-5 TB-1 2-3 CLP-1 0.53(mm)105/17/2010 08:41 xr108831.d

ZZZZZ CLP-2 0.53(mm)105/17/2010 08:55

ZZZZZ CLP-1 0.53(mm)105/17/2010 08:55

460-13139-7 TB-5 3-4 CLP-2 0.53(mm)105/17/2010 09:09 xf108833.d

460-13139-7 TB-5 3-4 CLP-1 0.53(mm)105/17/2010 09:09 xr108833.d

ZZZZZ CLP-2 0.53(mm)105/17/2010 09:23

ZZZZZ CLP-1 0.53(mm)105/17/2010 09:23

MB 460-37420/1-A CLP-2 0.53(mm)105/17/2010 09:37 xf108835.d

MB 460-37420/1-A CLP-1 0.53(mm)105/17/2010 09:37 xr108835.d

PIBLK 460-37575/22 CLP-2 0.53(mm)105/17/2010 09:51

PIBLK 460-37575/22 CLP-1 0.53(mm)105/17/2010 09:51

CCV 460-37575/23 CLP-2 0.53(mm)105/17/2010 10:04 xf108837.d

8081A

06/03/2010 of 623

Lab Name: Job No.:

SDG No.:

Instrument ID:



DILUTION

FACTOR



PESTGC1

37575

Start Date:

End Date: 05/17/2010 10:04

05/17/2010 04:31

CCV 460-37575/23 CLP-1 0.53(mm)105/17/2010 10:04 xr108837.d

8081A

06/03/2010 of 623


Method: 3541

Analyst: Patel, Harsh


Batch End:

May 14 2010 9:15AM

May 14 2010 3:00PM


sample

Position on the

SoxTherm

OP_PESTSP_00004 OPPSTPCBSU_00014Initial weight/volume of

sample

Method Chain

MB~460-37420/1 15.00 g 10 mL 50 uL1213541, 8081A

LCS~460-37420/2 15.00 g 10 mL 50 uL100 uL1223541, 8081A

460-13147-A-2~MS T 15.01 g 10 mL 50 uL100 uL1233541, 8081A

460-13147-A-2~MS

D

T 15.00 g 10 mL 50 uL100 uL1243541, 8081A

460-13139-E-1 TB-3 2-3 T 15.02 g 10 mL 50 uL125

460-13139-E-2 TB-3 6-7 T 15.00 g 10 mL 50 uL1263541, 8081A

460-13139-E-3 TB-2 2-3 T 15.00 g 10 mL 50 uL67

460-13139-E-4 TB-2 5-6 T 15.01 g 10 mL 50 uL683541, 8081A

460-13139-E-5 TB-1 2-3 T 15.00 g 10 mL 50 uL693541, 8081A

460-13139-E-6 TB-1 5-6 T 15.00 g 10 mL 50 uL70

460-13139-E-7 TB-5 3-4 T 15.00 g 10 mL 50 uL713541, 8081A

460-13139-E-8 TB-4 6-7 T 15.01 g 10 mL 50 uL72

460-13146-G-1 T 15.00 g 10 mL 50 uL1

460-13147-B-1 T 15.00 g 10 mL 50 uL2

460-13147-A-2 T 15.02 g 10 mL 50 uL3

460-13148-B-1 T 15.00 g 10 mL 50 uL4

First Start time: 8.30am

Person's name who did the prep: hp

Person's name who witnessed reagent drop: JR

First End time: 3.00pm

Balance ID: 28

Person's name who did the concentration: hp

Na2SO4 Lot Number: H52600

Solvent: Acetone/Hexane mix

Vendor lot number: H35E05

Florisil Lot #: H38553

06/03/2010 of 623


Method: 3541

Analyst: Patel, Harsh


Batch End:

May 14 2010 9:15AM

May 14 2010 3:00PM


Comments


MB~460-37420/1 3541, 8081A

LCS~460-37420/2 3541, 8081A

460-13147-A-2~MS T3541, 8081A

460-13147-A-2~MS

D

T3541, 8081A

460-13139-E-1 TB-3 2-3 T

460-13139-E-2 TB-3 6-7 T3541, 8081A

460-13139-E-3 TB-2 2-3 T

460-13139-E-4 TB-2 5-6 T3541, 8081A

460-13139-E-5 TB-1 2-3 T3541, 8081A

460-13139-E-6 TB-1 5-6 T

460-13139-E-7 TB-5 3-4 T3541, 8081A

460-13139-E-8 TB-4 6-7 T

460-13146-G-1 T

460-13147-B-1 T

460-13147-A-2 T

460-13148-B-1 T

Batch Comment: PEST soil

06/03/2010 of 623

Method 8082Polychlorinated Biphenyls (PCBs) by

Gas Chromatography by Method 8082

06/03/2010 of 623

FORM II

GC SEMI VOA SURROGATE RECOVERY


SDG No.:


TestAmerica Edison

GC Column (1): ID: (mm) GC Column (2): ID: (mm)CLP-2 0.53 CLP-1 0.53

#Lab Sample IDClient Sample ID #DCB1 DCB2

460-13139-2TB-3 6-7 106 108

460-13139-4TB-2 5-6 110 97

460-13139-5TB-1 2-3 109 113

460-13139-7TB-5 3-4 65 55

MB 460-37391/1-A 98 94

LCS 460-37391/2-A

104 110

460-13137-A-1-B MS

108 106

460-13137-A-1-C MSD

91 91

QC LIMITSQC LIMITSDCB = DCB Decachlorobiphenyl 27-165

FORM II 8082


06/03/2010 of 623


FORM III

Job No.:Lab Name:

SDG No.:


Low

460-13139-1

Lab File ID: of077396.dSolid


TestAmerica Edison

REC

%

REC

QC

LIMITSCONCENTRATION

(ug/Kg)

SPIKE

ADDED

(ug/Kg)

#

LCS LCS

COMPOUND

Aroclor 1016 333 316 62-14895

Aroclor 1260 333 328 58-14598

FORM III 8082


06/03/2010 of 623


FORM III

Job No.:Lab Name:

SDG No.:


Low

460-13139-1

Lab File ID: or077396.dSolid


TestAmerica Edison

REC

%

REC

QC

LIMITSCONCENTRATION

(ug/Kg)

SPIKE

ADDED

(ug/Kg)

#

LCS LCS

COMPOUND

Aroclor 1016 333 278 62-14883

Aroclor 1260 333 314 58-14594

FORM III 8082


06/03/2010 of 623


FORM III

Job No.:Lab Name:

SDG No.:


Low

460-13139-1



TestAmerica Edison

LIMITS

COMPOUND

CONCENTRATION %

REC

QC

REC

SAMPLE

CONCENTRATION

SPIKE

ADDED


#

MS MS

343 357 62-148Aroclor 1016 10469 U

343 362 58-145Aroclor 1260 10669 U

FORM III 8082


06/03/2010 of 623


FORM III

Job No.:Lab Name:

SDG No.:


Low

460-13139-1



TestAmerica Edison

LIMITS

COMPOUND

CONCENTRATION %

REC

QC

REC

SAMPLE

CONCENTRATION

SPIKE

ADDED


#

MS MS

343 321 62-148Aroclor 1016 9469 U

343 331 58-145Aroclor 1260 9669 U

FORM III 8082


06/03/2010 of 623


FORM III

Job No.:Lab Name:

SDG No.:


Low

460-13139-1



TestAmerica Edison

COMPOUND

SPIKE


REC

%

RPD

QC LIMITS


#

MSD MSD

343 364 30 62-148Aroclor 1016 2106

343 376 30 58-145Aroclor 1260 4110

FORM III 8082


06/03/2010 of 623


FORM III

Job No.:Lab Name:

SDG No.:


Low

460-13139-1



TestAmerica Edison

COMPOUND

SPIKE


REC

%

RPD

QC LIMITS


#

MSD MSD

343 335 30 62-148Aroclor 1016 498

343 343 30 58-145Aroclor 1260 4100

FORM III 8082


06/03/2010 of 623

FORM IV

GC SEMI VOA METHOD BLANK SUMMARY

Lab Name:

SDG No.:


Date Analyzed:(1)

Instrument ID:(1)

GC Column:(1) ID:

Instrument ID:(2)

Date Extracted: 05/14/2010 07:19

Date Analyzed:(2)

GC Column:(2) ID:CLP-10.53(mm) 0.53(mm)

PESTGC7

05/14/2010 18:20

Lab File ID:(1) Lab File ID:(2)

Matrix: Solid

or077395.d


of077395.d

05/14/2010 18:20

PESTGC7

CLP-2


ANALYZED 2

DATEDATE

ANALYZED 1LAB SAMPLE IDCLIENT SAMPLE ID

LCS 460-37391/2-A 05/14/2010 18:37 05/14/2010 18:37

460-13137-A-1-B MS 05/14/2010 19:09 05/14/2010 19:09

460-13137-A-1-C MSD 05/14/2010 19:26 05/14/2010 19:26

460-13139-2TB-3 6-7 05/14/2010 19:59 05/14/2010 19:59

460-13139-4TB-2 5-6 05/14/2010 20:32 05/14/2010 20:32

460-13139-5TB-1 2-3 05/14/2010 20:48 05/14/2010 20:48

460-13139-7TB-5 3-4 05/14/2010 21:21 05/14/2010 21:21

FORM IV 8082

06/03/2010 of 623

PCBS ANALYTICAL SEQUENCE

Lab Name: Job No.:

SDG No.:

FORM VIII


Calibration ID:


GC Column:

6034


05/04/2010 16:54

05/04/2010 17:58CLP-2 ID: 0.53(mm)


# #RT RT

TCX DCB

UPPER LIMIT

LOWER LIMIT

2.14

2.04

10.31

10.11



CCVRT 460-37531/3 05/14/2010 17:55 2.09 10.21of077394.d

MB 460-37391/1-A 05/14/2010 18:20 10.21of077395.d

LCS 460-37391/2-A 05/14/2010 18:37 10.21of077396.d

460-13137-A-1-B MS 05/14/2010 19:09 10.21of077398.d

460-13137-A-1-C MSD 05/14/2010 19:26 10.21of077399.d

460-13139-2 05/14/2010 19:59 10.21TB-3 6-7 of077401.d

460-13139-4 05/14/2010 20:32 10.21TB-2 5-6 of077403.d

460-13139-5 05/14/2010 20:48 10.21TB-1 2-3 of077404.d

460-13139-7 05/14/2010 21:21 10.21TB-5 3-4 of077406.d

CCV 460-37531/25 05/15/2010 00:03 2.08 10.20of077416.d





FORM VIII 8082

06/03/2010 of 623

PCBS ANALYTICAL SEQUENCE

Lab Name: Job No.:

SDG No.:

FORM VIII


Calibration ID:


GC Column:

6042


05/04/2010 16:54

05/04/2010 17:58CLP-1 ID: 0.53(mm)


# #RT RT

TCX DCB

UPPER LIMIT

LOWER LIMIT

2.03

1.93

9.38

9.18



CCVRT 460-37531/3 05/14/2010 17:55 1.98 9.28or077394.d

MB 460-37391/1-A 05/14/2010 18:20 9.28or077395.d

LCS 460-37391/2-A 05/14/2010 18:37 9.28or077396.d

460-13137-A-1-B MS 05/14/2010 19:09 9.28or077398.d

460-13137-A-1-C MSD 05/14/2010 19:26 9.28or077399.d

460-13139-2 05/14/2010 19:59 9.28TB-3 6-7 or077401.d

460-13139-4 05/14/2010 20:32 9.28TB-2 5-6 or077403.d

460-13139-5 05/14/2010 20:48 9.28TB-1 2-3 or077404.d

460-13139-7 05/14/2010 21:21 9.28TB-5 3-4 or077406.d

CCV 460-37531/25 05/15/2010 00:03 1.98 9.28or077416.d





FORM VIII 8082

06/03/2010 of 623

FORM XForm 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:







0.53(mm) 0.53(mm)

05/14/2010 18:37 05/14/2010 18:37

PESTGC7 PESTGC7

CLP-2 CLP-1



CONCENTRATION

Aroclor 1016 1 1 2.57 2.49 2.63 285 316 12.7

2 3.01 2.92 3.06 309

3 3.27 3.19 3.33 331

4 3.52 3.44 3.58 306

5 3.68 3.60 3.74 316

6 3.97 3.89 4.03 329

7 4.24 4.16 4.30 308

8 4.39 4.31 4.45 344

2 1 2.28 2.19 2.33 258 278

2 2.59 2.51 2.65 279

3 2.78 2.70 2.84 278

4 3.04 2.97 3.11 287

5 3.19 3.11 3.25 285

6 3.25 3.17 3.31 272

7 3.62 3.54 3.68 291

8 3.71 3.64 3.78 274

Aroclor 1260 1 1 5.84 5.76 5.90 330 328 4.4

2 6.13 6.05 6.19 331

3 6.65 6.58 6.72 319

4 6.82 6.74 6.88 329

5 6.91 6.83 6.97 343

6 7.35 7.28 7.42 330

7 8.77 8.69 8.83 317

8 9.63 9.56 9.70 328

2 1 5.02 4.95 5.09 310 314

2 5.37 5.29 5.43 307

3 5.71 5.64 5.78 303

4 5.85 5.78 5.92 313

5 6.17 6.09 6.23 302

6 7.09 7.02 7.16 290

7 7.24 7.17 7.31 352

8 8.43 8.35 8.49 334

FORM X 8082

06/03/2010 of 623

FORM XForm 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:







0.53(mm) 0.53(mm)

05/14/2010 19:09 05/14/2010 19:09

PESTGC7 PESTGC7

CLP-2 CLP-1



CONCENTRATION

Aroclor 1016 1 1 2.57 2.49 2.63 352 357 10.7

2 3.00 2.92 3.06 350

3 3.26 3.19 3.33 354

4 3.51 3.44 3.58 347

5 3.67 3.60 3.74 355

6 3.96 3.89 4.03 389

7 4.23 4.16 4.30 330

8 4.39 4.31 4.45 380

2 1 2.27 2.19 2.33 300 321

2 2.59 2.51 2.65 323

3 2.78 2.70 2.84 318

4 3.04 2.97 3.11 329

5 3.19 3.11 3.25 326

6 3.25 3.17 3.31 309

7 3.62 3.54 3.68 324

8 3.71 3.64 3.78 339

Aroclor 1260 1 1 5.83 5.76 5.90 361 362 9.1

2 6.12 6.05 6.19 363

3 6.65 6.58 6.72 354

4 6.81 6.74 6.88 361

5 6.90 6.83 6.97 365

6 7.35 7.28 7.42 362

7 8.76 8.69 8.83 364

8 9.63 9.56 9.70 365

2 1 5.02 4.95 5.09 336 331

2 5.37 5.29 5.43 336

3 5.71 5.64 5.78 333

4 5.85 5.78 5.92 336

5 6.17 6.09 6.23 325

6 7.09 7.02 7.16 306

7 7.24 7.17 7.31 331

8 8.42 8.35 8.49 340

FORM X 8082

06/03/2010 of 623

FORM XForm 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:







0.53(mm) 0.53(mm)

05/14/2010 19:26 05/14/2010 19:26

PESTGC7 PESTGC7

CLP-2 CLP-1



CONCENTRATION

Aroclor 1016 1 1 2.57 2.49 2.63 349 364 8.1

2 3.00 2.92 3.06 352

3 3.27 3.19 3.33 369

4 3.52 3.44 3.58 361

5 3.68 3.60 3.74 370

6 3.96 3.89 4.03 365

7 4.24 4.16 4.30 349

8 4.39 4.31 4.45 394

2 1 2.28 2.19 2.33 297 335

2 2.59 2.51 2.65 326

3 2.78 2.70 2.84 327

4 3.04 2.97 3.11 345

5 3.19 3.11 3.25 342

6 3.25 3.17 3.31 332

7 3.62 3.54 3.68 343

8 3.71 3.64 3.78 371

Aroclor 1260 1 1 5.84 5.76 5.90 375 376 9.2

2 6.12 6.05 6.19 377

3 6.65 6.58 6.72 373

4 6.81 6.74 6.88 379

5 6.91 6.83 6.97 388

6 7.35 7.28 7.42 383

7 8.76 8.69 8.83 378

8 9.63 9.56 9.70 360

2 1 5.02 4.95 5.09 353 343

2 5.37 5.29 5.43 353

3 5.71 5.64 5.78 351

4 5.85 5.78 5.92 357

5 6.17 6.09 6.23 347

6 7.09 7.02 7.16 324

7 7.24 7.17 7.31 326

8 8.42 8.35 8.49 335

FORM X 8082

06/03/2010 of 623

FORM IForm 1PCBS ORGANICS ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

TB-3 6-7

SDG No.:

460-13139-1


Matrix: of077401.dLab File ID:

Date Collected:8082Analysis Method:

Soil

TestAmerica Edison

05/12/2010 09:45


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/14/2010 19:59

N

10(mL)


% Moisture: 18.8





FORM I 8082

06/03/2010 of 623

Data File: of077401.d Report Date: 16-May-2010 18:33

TestAmerica

GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC7.i/8082/front/May10/05-14-10/14may10a.b/of077401.dLab Smp Id: 460-13139-E-2-A Client Smp ID: TB-3 6-7Inj Date : 14-MAY-2010 19:59 Operator : 615 Inst ID: PESTGC7.iSmp Info : 460-13139-E-2-AMisc Info : 460-13139-E-2-AComment : Method : /chem1/PESTGC7.i/8082/front/May10/05-14-10/14may10a.b/08Of8082.mMeth Date : 05-May-2010 00:12 diazc Quant Type: ESTDCal Date : 04-MAY-2010 19:52 Cal File: of077121.dAls bottle: 10 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: AllPCB.subTarget Version: 3.50 Sample Matrix: SOLIDProcessing Host: hpd3



DF 1.00000 Dilution FactorVt 10.00000 Volume of final extract (mL)Ws 15.00000 Weight of sample extracted (g)M 0.00000 % Moisture


CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====

$ 30 Decachlorobiphenyl(surr) CAS #: 2051-24-3

10.205 10.205 0.000 184874 53.1503 35 80.00- 120.00 100.00

-------------------------------------------------------------------------------

06/03/2010 of 623

Data File: of077401.d

Date: 14-MAY-2010 19:59

Client ID: TB-3 6-7 Instrument: PESTGC7.i

Sample Info: 460-13139-E-2-A Operator: 615

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-3 6-7

SDG No.:

460-13139-1


Matrix: or077401.dLab File ID:


Soil

TestAmerica Edison

05/12/2010 09:45


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/14/2010 19:59

N

10(mL)


% Moisture: 18.8




Aroclor 101612674-11-2 83 83 16U

Aroclor 122111104-28-2 83 83 25U

Aroclor 123211141-16-5 83 83 47U

Aroclor 124253469-21-9 83 83 16U

Aroclor 124812672-29-6 83 83 22U

Aroclor 125411097-69-1 83 83 28U

Aroclor 126011096-82-5 83 83 9.2U

Aroclor 126237324-23-5 83 83 14U

Aroclor 126811100-14-4 83 83 14U



FORM I 8082

06/03/2010 of 623

Data File: or077401.d Page 1 Report Date: 16-May-2010 18:33

TestAmerica

GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC7.i/8082/rear/May10/05-14-10/14may10a.b/or077401.dLab Smp Id: 460-13139-E-2-A Client Smp ID: TB-3 6-7Inj Date : 14-MAY-2010 19:59 Operator : 615 Inst ID: PESTGC7.iSmp Info : 460-13139-E-2-AMisc Info : 460-13139-E-2-AComment : Method : /chem1/PESTGC7.i/8082/rear/May10/05-14-10/14may10a.b/08Or8082.mMeth Date : 05-May-2010 00:19 diazc Quant Type: ESTDCal Date : 04-MAY-2010 19:52 Cal File: or077121.dAls bottle: 10 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: AllPCB.subTarget Version: 3.50 Sample Matrix: SOLIDProcessing Host: hpd3





CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====


9.277 9.278 -0.001 130822 54.1694 80.00- 120.00 100.00(aR)

-------------------------------------------------------------------------------

QC Flag Legend



06/03/2010 of 623

Data File: or077401.d

Date: 14-MAY-2010 19:59



06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-2 5-6

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 10:45


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/14/2010 20:32

N

10(mL)


% Moisture: 12.8





FORM I 8082

06/03/2010 of 623


TestAmerica






CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====


10.205 10.205 0.000 190649 54.8106 36 80.00- 120.00 100.00

-------------------------------------------------------------------------------

06/03/2010 of 623


Date: 14-MAY-2010 20:32



06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-2 5-6

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 10:45


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/14/2010 20:32

N

10(mL)


% Moisture: 12.8




Aroclor 101612674-11-2 77 77 15U

Aroclor 122111104-28-2 77 77 23U

Aroclor 123211141-16-5 77 77 43U

Aroclor 124253469-21-9 77 77 15U

Aroclor 124812672-29-6 77 77 20U

Aroclor 125411097-69-1 77 77 26U

Aroclor 126011096-82-5 77 77 8.6U

Aroclor 126237324-23-5 77 77 13U

Aroclor 126811100-14-4 77 77 13U



FORM I 8082

06/03/2010 of 623


TestAmerica






CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====


9.277 9.278 -0.001 117209 48.5327 80.00- 120.00 100.00(aR)

-------------------------------------------------------------------------------

QC Flag Legend



06/03/2010 of 623


Date: 14-MAY-2010 20:32



06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-1 2-3

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 11:25


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/14/2010 20:48

N

10(mL)


% Moisture: 6.5





FORM I 8082

06/03/2010 of 623


TestAmerica






CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====


10.207 10.205 0.002 190389 54.7359 36 80.00- 120.00 100.00

-------------------------------------------------------------------------------

06/03/2010 of 623


Date: 14-MAY-2010 20:48



06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-1 2-3

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 11:25


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/14/2010 20:48

N

10(mL)


% Moisture: 6.5




Aroclor 101612674-11-2 72 72 14U

Aroclor 122111104-28-2 72 72 22U

Aroclor 123211141-16-5 72 72 41U

Aroclor 124253469-21-9 72 72 14U

Aroclor 124812672-29-6 72 72 19U

Aroclor 125411097-69-1 72 72 24U

Aroclor 126011096-82-5 72 72 8.0U

Aroclor 126237324-23-5 72 72 12U

Aroclor 126811100-14-4 72 72 12U



FORM I 8082

06/03/2010 of 623


TestAmerica






CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====


9.277 9.278 -0.001 136579 56.5532 80.00- 120.00 100.00(aR)

-------------------------------------------------------------------------------

QC Flag Legend



06/03/2010 of 623


Date: 14-MAY-2010 20:48



06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-5 3-4

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 12:30


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/14/2010 21:21

N

10(mL)


% Moisture: 61.5





FORM I 8082

06/03/2010 of 623


TestAmerica






CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====


10.205 10.205 0.000 112937 32.4688 22 80.00- 120.00 100.00

-------------------------------------------------------------------------------

06/03/2010 of 623


Date: 14-MAY-2010 21:21



06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

TB-5 3-4

SDG No.:

460-13139-1




Soil

TestAmerica Edison

05/12/2010 12:30


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/14/2010 21:21

N

10(mL)


% Moisture: 61.5




Aroclor 101612674-11-2 170 170 33U

Aroclor 122111104-28-2 170 170 52U

Aroclor 123211141-16-5 170 170 99U

Aroclor 124253469-21-9 170 170 33U

Aroclor 124812672-29-6 170 170 46U

Aroclor 125411097-69-1 170 170 59U

Aroclor 126011096-82-5 170 170 19U

Aroclor 126237324-23-5 170 170 30U

Aroclor 126811100-14-4 170 170 30U



FORM I 8082

06/03/2010 of 623


TestAmerica






CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====


9.277 9.278 -0.001 66819 27.6677 80.00- 120.00 100.00(aR)

-------------------------------------------------------------------------------

QC Flag Legend



06/03/2010 of 623


Date: 14-MAY-2010 21:21



06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




PESTGC7



N

05/04/2010 17:58



Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/4 of077110.dLevel 2 IC 460-36537/5 of077111.dLevel 3 IC 460-36537/6 of077112.dLevel 4 IC 460-36537/7 of077113.dLevel 5 IC 460-36537/8 of077114.d


PCB-1016 Peak 1 2.5572.485 - 2.6252.562 2.555 2.555 2.555 2.558PCB-1016 Peak 2 2.9922.920 - 3.0602.997 2.990 2.990 2.990 2.993PCB-1016 Peak 3 3.2583.185 - 3.3253.263 3.257 3.255 3.255 3.258PCB-1016 Peak 4 3.5073.435 - 3.5753.512 3.505 3.505 3.505 3.508PCB-1016 Peak 5 3.6673.595 - 3.7353.672 3.665 3.665 3.665 3.668PCB-1016 Peak 6 3.9573.885 - 4.0253.962 3.955 3.955 3.955 3.958PCB-1016 Peak 7 4.2294.157 - 4.2974.233 4.228 4.227 4.227 4.230PCB-1016 Peak 8 4.3824.310 - 4.4504.387 4.382 4.380 4.380 4.383PCB-1260 Peak 1 5.8325.762 - 5.9025.837 5.832 5.832 5.830 5.832PCB-1260 Peak 2 6.1196.048 - 6.1886.123 6.118 6.118 6.117 6.120PCB-1260 Peak 3 6.6476.575 - 6.7156.652 6.647 6.645 6.645 6.647PCB-1260 Peak 4 6.8086.737 - 6.8776.812 6.808 6.807 6.805 6.808PCB-1260 Peak 5 6.9016.830 - 6.9706.905 6.900 6.900 6.898 6.902PCB-1260 Peak 6 7.3467.275 - 7.4157.350 7.345 7.345 7.343 7.347PCB-1260 Peak 7 8.7598.688 - 8.8288.763 8.758 8.758 8.757 8.758PCB-1260 Peak 8 9.6289.557 - 9.6979.630 9.628 9.627 9.627 9.627Tetrachloro-m-xylene 2.0792.027 - 2.1272.083 2.077 2.077 2.078 2.080DCB Decachlorobiphenyl 10.20610.105 - 10.30510.208 10.207 10.205 10.205 10.205

FORM VI 8082 06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




PESTGC7



N

05/04/2010 17:58

0.53(mm)CLP-2 ID:


Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-36537/4 of077110.d2Level IC 460-36537/5 of077111.d3Level IC 460-36537/6 of077112.d4Level IC 460-36537/7 of077113.d5Level IC 460-36537/8 of077114.d

MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE


RRFANALYTE MIN RRF

LVL 5

PCB-1016 Peak 1 Ave 10.7 20.0113127.61 122.80 112.44 105.0698.465

PCB-1016 Peak 2 Ave 18.2 20.0236302.64 243.74 238.15 208.12189.69

PCB-1016 Peak 3 Ave 11.3 20.0110120.89 117.41 119.93 94.67299.372

PCB-1016 Peak 4 Ave 11.7 20.0428492.83 448.10 442.92 390.85365.56

PCB-1016 Peak 5 Ave 11.1 20.0201228.07 210.75 207.52 185.34171.51

PCB-1016 Peak 6 Ave 18.4 20.0133168.38 144.54 123.03 126.89103.18

PCB-1016 Peak 7 Ave 14.1 20.0154170.71 169.33 162.72 150.00118.28

PCB-1016 Peak 8 Ave 8.1 20.0156153.95 158.62 175.59 143.67146.53

PCB-1260 Peak 1 Ave 14.2 20.0304366.22 317.29 309.03 272.59254.89

PCB-1260 Peak 2 Ave 15.2 20.0340415.24 356.59 345.81 296.98286.16

PCB-1260 Peak 3 Ave 10.9 20.0484552.60 506.64 495.66 442.06420.61

PCB-1260 Peak 4 Ave 13.3 20.0243287.87 254.67 245.99 218.49205.73

PCB-1260 Peak 5 Ave 10.3 20.0146161.95 154.69 154.78 130.44130.01

PCB-1260 Peak 6 Ave 10.3 20.0266300.20 277.11 276.36 241.12234.86

PCB-1260 Peak 7 Ave 8.0 20.0371392.33 384.93 395.37 353.36327.05

FORM VI 8082


06/03/2010 of 623

FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:




PESTGC7



N

05/04/2010 17:58

0.53(mm)CLP-2 ID:


MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE


RRFANALYTE MIN RRF

LVL 5

PCB-1260 Peak 8 Ave 6.9 20.0125128.52 133.20 132.09 119.99112.83



FORM VI 8082


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PESTGC7



N

05/04/2010 17:58



Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/4 of077110.dLevel 2 IC 460-36537/5 of077111.dLevel 3 IC 460-36537/6 of077112.dLevel 4 IC 460-36537/7 of077113.dLevel 5 IC 460-36537/8 of077114.d

CURVETYPE



PCB-1016 Peak 1 Ave 12761 61402 112436 157593 246162 100 500 1000 1500 2500PCB-1016 Peak 2 Ave 30264 121868 238150 312174 474233 100 500 1000 1500 2500PCB-1016 Peak 3 Ave 12089 58707 119927 142008 248429 100 500 1000 1500 2500PCB-1016 Peak 4 Ave 49283 224051 442921 586273 913898 100 500 1000 1500 2500PCB-1016 Peak 5 Ave 22807 105377 207521 278004 428764 100 500 1000 1500 2500PCB-1016 Peak 6 Ave 16838 72269 123032 190341 257947 100 500 1000 1500 2500PCB-1016 Peak 7 Ave 17071 84666 162717 224998 295709 100 500 1000 1500 2500PCB-1016 Peak 8 Ave 15395 79310 175591 215509 366327 100 500 1000 1500 2500PCB-1260 Peak 1 Ave 36622 158643 309028 408879 637225 100 500 1000 1500 2500PCB-1260 Peak 2 Ave 41524 178297 345807 445464 715394 100 500 1000 1500 2500PCB-1260 Peak 3 Ave 55260 253320 495657 663088 1051514 100 500 1000 1500 2500PCB-1260 Peak 4 Ave 28787 127333 245987 327740 514318 100 500 1000 1500 2500PCB-1260 Peak 5 Ave 16195 77346 154781 195657 325031 100 500 1000 1500 2500PCB-1260 Peak 6 Ave 30020 138556 276362 361675 587157 100 500 1000 1500 2500PCB-1260 Peak 7 Ave 39233 192463 395372 530042 817635 100 500 1000 1500 2500PCB-1260 Peak 8 Ave 12852 66601 132085 179981 282076 100 500 1000 1500 2500Tetrachloro-m-xylene Ave 122947 256079 525659 733307 946740 25.0 50.0 100 150 200DCB Decachlorobiphenyl Ave 91938 184256 360298 492235 628886 25.0 50.0 100 150 200


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Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/4 or077110.dLevel 2 IC 460-36537/5 or077111.dLevel 3 IC 460-36537/6 or077112.dLevel 4 IC 460-36537/7 or077113.dLevel 5 IC 460-36537/8 or077114.d


PCB-1016 Peak 1 2.2642.193 - 2.3332.268 2.263 2.263 2.263 2.263PCB-1016 Peak 2 2.5832.512 - 2.6522.585 2.583 2.582 2.583 2.582PCB-1016 Peak 3 2.7722.702 - 2.8422.775 2.772 2.772 2.772 2.772PCB-1016 Peak 4 3.0362.965 - 3.1053.038 3.035 3.035 3.035 3.035PCB-1016 Peak 5 3.1783.107 - 3.2473.182 3.178 3.177 3.177 3.177PCB-1016 Peak 6 3.2393.168 - 3.3083.240 3.238 3.238 3.238 3.238PCB-1016 Peak 7 3.6113.540 - 3.6803.613 3.612 3.610 3.610 3.610PCB-1016 Peak 8 3.7083.637 - 3.7773.712 3.708 3.707 3.707 3.707PCB-1260 Peak 1 5.0194.948 - 5.0885.022 5.020 5.018 5.018 5.018PCB-1260 Peak 2 5.3635.292 - 5.4325.365 5.363 5.362 5.362 5.362PCB-1260 Peak 3 5.7085.637 - 5.7775.710 5.708 5.707 5.707 5.707PCB-1260 Peak 4 5.8505.778 - 5.9185.853 5.850 5.848 5.848 5.848PCB-1260 Peak 5 6.1636.093 - 6.2336.165 6.163 6.163 6.162 6.162PCB-1260 Peak 6 7.0857.015 - 7.1557.088 7.087 7.085 7.083 7.083PCB-1260 Peak 7 7.2367.167 - 7.3077.238 7.237 7.237 7.235 7.235PCB-1260 Peak 8 8.4228.352 - 8.4928.425 8.423 8.422 8.420 8.420Tetrachloro-m-xylene 1.9701.918 - 2.0181.972 1.970 1.968 1.970 1.970DCB Decachlorobiphenyl 9.2799.178 - 9.3789.280 9.278 9.278 9.278 9.278

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0.53(mm)CLP-1 ID:


Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-36537/4 or077110.d2Level IC 460-36537/5 or077111.d3Level IC 460-36537/6 or077112.d4Level IC 460-36537/7 or077113.d5Level IC 460-36537/8 or077114.d

MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE


RRFANALYTE MIN RRF

LVL 5

PCB-1016 Peak 1 Ave 17.8 20.07697.650 78.324 72.815 67.43562.786

PCB-1016 Peak 2 Ave 17.4 20.0131165.15 139.63 128.56 115.05106.79

PCB-1016 Peak 3 Ave 7.8 20.09298.330 96.916 94.289 86.39381.814

PCB-1016 Peak 4 Ave 6.7 20.0248259.63 259.90 261.00 235.62225.47

PCB-1016 Peak 5 Ave 11.8 20.0102117.49 107.59 104.68 92.29787.665

PCB-1016 Peak 6 Ave 3.3 20.07068.620 70.728 73.485 69.91767.436

PCB-1016 Peak 7 Ave 10.4 20.0107120.06 113.04 108.52 98.49492.460

PCB-1016 Peak 8 Ave 8.3 20.04542.210 46.350 50.679 46.16941.281

PCB-1260 Peak 1 Ave 15.9 20.0159196.35 167.43 155.77 142.08131.21

PCB-1260 Peak 2 Ave 16.0 20.0279346.02 293.32 274.62 248.75231.21

PCB-1260 Peak 3 Ave 10.0 20.0255288.49 268.85 258.77 237.06224.03

PCB-1260 Peak 4 Ave 14.4 20.0125153.18 130.39 122.95 113.59106.36

PCB-1260 Peak 5 Ave 12.4 20.0130152.44 137.14 128.84 117.31112.21

PCB-1260 Peak 6 Ave 5.1 20.0147150.48 145.81 158.32 144.34138.14

PCB-1260 Peak 7 Ave 4.7 20.09086.650 90.200 97.509 89.03687.752

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0.53(mm)CLP-1 ID:


MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE


RRFANALYTE MIN RRF

LVL 5

PCB-1260 Peak 8 Ave 9.7 20.07362.650 70.488 81.271 77.33274.842



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Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/4 or077110.dLevel 2 IC 460-36537/5 or077111.dLevel 3 IC 460-36537/6 or077112.dLevel 4 IC 460-36537/7 or077113.dLevel 5 IC 460-36537/8 or077114.d

CURVETYPE



PCB-1016 Peak 1 Ave 9765 39162 72815 101152 156966 100 500 1000 1500 2500PCB-1016 Peak 2 Ave 16515 69813 128558 172571 266964 100 500 1000 1500 2500PCB-1016 Peak 3 Ave 9833 48458 94289 129589 204534 100 500 1000 1500 2500PCB-1016 Peak 4 Ave 25963 129952 261001 353428 563686 100 500 1000 1500 2500PCB-1016 Peak 5 Ave 11749 53797 104682 138446 219162 100 500 1000 1500 2500PCB-1016 Peak 6 Ave 6862 35364 73485 104875 168591 100 500 1000 1500 2500PCB-1016 Peak 7 Ave 12006 56520 108515 147741 231150 100 500 1000 1500 2500PCB-1016 Peak 8 Ave 4221 23175 50679 69254 103203 100 500 1000 1500 2500PCB-1260 Peak 1 Ave 19635 83715 155769 213120 328021 100 500 1000 1500 2500PCB-1260 Peak 2 Ave 34602 146660 274615 373132 578023 100 500 1000 1500 2500PCB-1260 Peak 3 Ave 28849 134423 258774 355594 560083 100 500 1000 1500 2500PCB-1260 Peak 4 Ave 15318 65197 122945 170391 265894 100 500 1000 1500 2500PCB-1260 Peak 5 Ave 15244 68570 128841 175968 280519 100 500 1000 1500 2500PCB-1260 Peak 6 Ave 15048 72904 158321 216511 345343 100 500 1000 1500 2500PCB-1260 Peak 7 Ave 8665 45100 97509 133554 219380 100 500 1000 1500 2500PCB-1260 Peak 8 Ave 6265 35244 81271 115998 187104 100 500 1000 1500 2500Tetrachloro-m-xylene Ave 60210 139056 280394 397305 516858 25.0 50.0 100 150 200DCB Decachlorobiphenyl Ave 63041 131126 248257 342086 433591 25.0 50.0 100 150 200


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Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/9 of077115.d


PCB-1221 Peak 1 1.6731.603 - 1.7431.673PCB-1221 Peak 2 1.9881.918 - 2.0581.988PCB-1221 Peak 3 2.3532.283 - 2.4232.353PCB-1221 Peak 4 2.4952.425 - 2.5652.495PCB-1221 Peak 5 2.5582.488 - 2.6282.558PCB-1221 Peak 6 3.0602.990 - 3.1303.060PCB-1221 Peak 7 3.2623.192 - 3.3323.262PCB-1221 Peak 8 3.5103.440 - 3.5803.510

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0.53(mm)CLP-2 ID:


Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-36537/9 of077115.d

MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE

LVL 1

RRFANALYTE MIN RRF

64.656PCB-1221 Peak 1 Ave 65 20.012.481PCB-1221 Peak 2 Ave 12 20.060.208PCB-1221 Peak 3 Ave 60 20.039.669PCB-1221 Peak 4 Ave 40 20.0158.59PCB-1221 Peak 5 Ave 159 20.027.866PCB-1221 Peak 6 Ave 28 20.011.526PCB-1221 Peak 7 Ave 12 20.024.711PCB-1221 Peak 8 Ave 25 20.0

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CURVETYPE


LVL 1 LVL 1

PCB-1221 Peak 1 Ave 64656 1000PCB-1221 Peak 2 Ave 12481 1000PCB-1221 Peak 3 Ave 60208 1000PCB-1221 Peak 4 Ave 39669 1000PCB-1221 Peak 5 Ave 158588 1000PCB-1221 Peak 6 Ave 27866 1000PCB-1221 Peak 7 Ave 11526 1000PCB-1221 Peak 8 Ave 24711 1000


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LEVEL: LAB SAMPLE ID: LAB FILE ID:Level 1 IC 460-36537/9 or077115.d



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Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:1Level IC 460-36537/9 or077115.d

MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE

LVL 1

RRFANALYTE MIN RRF


FORM VI 8082


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Calibration Files:


CURVETYPE


LVL 1 LVL 1



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MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE

LVL 1

RRFANALYTE MIN RRF


FORM VI 8082


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CURVETYPE


LVL 1 LVL 1



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MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE

LVL 1

RRFANALYTE MIN RRF


FORM VI 8082


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Calibration Files:


CURVETYPE


LVL 1 LVL 1



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MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE

LVL 1

RRFANALYTE MIN RRF


FORM VI 8082


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CURVETYPE


LVL 1 LVL 1



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MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE

LVL 1

RRFANALYTE MIN RRF


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CURVETYPE


LVL 1 LVL 1



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Calibration Files:


MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE

LVL 1

RRFANALYTE MIN RRF


FORM VI 8082


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CURVETYPE


LVL 1 LVL 1



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MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE

LVL 1

RRFANALYTE MIN RRF


FORM VI 8082


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CURVETYPE


LVL 1 LVL 1



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MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE

LVL 1

RRFANALYTE MIN RRF


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CURVETYPE


LVL 1 LVL 1



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MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE

LVL 1

RRFANALYTE MIN RRF


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CURVETYPE


LVL 1 LVL 1



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MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE

LVL 1

RRFANALYTE MIN RRF


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CURVETYPE


LVL 1 LVL 1



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MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE

LVL 1

RRFANALYTE MIN RRF


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CURVETYPE


LVL 1 LVL 1



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MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE

LVL 1

RRFANALYTE MIN RRF


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CURVETYPE


LVL 1 LVL 1



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MIN R^2OR COD

#R^2OR COD

MAX%RSD

#%RSD#COEFFICIENT

M2M1B

CURVETYPE

LVL 1

RRFANALYTE MIN RRF


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CURVETYPE


LVL 1 LVL 1



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Calib Start Date:

Lab Sample ID:


PCBS CONTINUING CALIBRATION DATA

0.53(mm)

460-13139-1

PESTGC7

05/14/2010 17:55

05/04/2010 16:54

05/04/2010 17:58

CCVRT 460-37531/3

CLP-2

TestAmerica Edison

Lab File ID: of077394.d Conc. Units: ug/L



PCB-1016 Peak 1 Ave 118.1113.3 1040 1000 4.2 15.0

PCB-1016 Peak 2 Ave 251.8236.5 1060 1000 6.5 15.0

PCB-1016 Peak 3 Ave 131.8110.5 1190 1000 19.3* 15.0

PCB-1016 Peak 4 Ave 469.7428.1 1100 1000 9.7 15.0

PCB-1016 Peak 5 Ave 223.7200.6 1110 1000 11.5 15.0

PCB-1016 Peak 6 Ave 152.6133.2 1150 1000 14.6 15.0

PCB-1016 Peak 7 Ave 155.0154.2 1010 1000 0.5 15.0

PCB-1016 Peak 8 Ave 188.5155.7 1210 1000 21.1* 15.0

PCB-1260 Peak 1 Ave 333.3304.0 1100 1000 9.7 15.0

PCB-1260 Peak 2 Ave 374.5340.2 1100 1000 10.1 15.0

PCB-1260 Peak 3 Ave 542.2483.5 1120 1000 12.1 15.0

PCB-1260 Peak 4 Ave 268.1242.5 1110 1000 10.5 15.0

PCB-1260 Peak 5 Ave 168.4146.4 1150 1000 15.1* 15.0

PCB-1260 Peak 6 Ave 307.0265.9 1150 1000 15.4* 15.0

PCB-1260 Peak 7 Ave 417.6370.6 1130 1000 12.7 15.0

PCB-1260 Peak 8 Ave 148.5125.3 1180 1000 18.5* 15.0



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PCBS CONTINUING CALIBRATION RETENTION TIME SUMMARY

0.53(mm)

460-13139-1

PESTGC7

05/14/2010 17:55

05/04/2010 16:54

05/04/2010 17:58

CCVRT 460-37531/3

CLP-2

TestAmerica Edison

Lab File ID: of077394.d

Analyte RTTO FROM

RT WINDOW

PCB-1016 Peak 1 2.57 2.49 2.63

PCB-1016 Peak 2 3.00 2.92 3.06

PCB-1016 Peak 3 3.27 3.19 3.33

PCB-1016 Peak 4 3.52 3.44 3.58

PCB-1016 Peak 5 3.68 3.60 3.74

PCB-1016 Peak 6 3.97 3.89 4.03

PCB-1016 Peak 7 4.24 4.16 4.30

PCB-1016 Peak 8 4.39 4.31 4.45

PCB-1260 Peak 1 5.84 5.76 5.90

PCB-1260 Peak 2 6.13 6.05 6.19

PCB-1260 Peak 3 6.65 6.58 6.72

PCB-1260 Peak 4 6.81 6.74 6.88

PCB-1260 Peak 5 6.91 6.83 6.97

PCB-1260 Peak 6 7.35 7.28 7.42

PCB-1260 Peak 7 8.77 8.69 8.83

PCB-1260 Peak 8 9.63 9.56 9.70



Form VII 8082

06/03/2010 of 623

FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:



0.53(mm)

460-13139-1

PESTGC7

05/14/2010 17:55

05/04/2010 16:54

05/04/2010 17:58

CCVRT 460-37531/3

CLP-1

TestAmerica Edison

Lab File ID: or077394.d Conc. Units: ug/L



PCB-1016 Peak 1 Ave 74.9275.80 988 1000 -1.2 15.0

PCB-1016 Peak 2 Ave 132.2131.0 1010 1000 0.9 15.0

PCB-1016 Peak 3 Ave 97.0191.55 1060 1000 6.0 15.0

PCB-1016 Peak 4 Ave 267.8248.3 1080 1000 7.8 15.0

PCB-1016 Peak 5 Ave 106.5101.9 1040 1000 4.4 15.0

PCB-1016 Peak 6 Ave 76.4170.04 1090 1000 9.1 15.0

PCB-1016 Peak 7 Ave 112.4106.5 1060 1000 5.6 15.0

PCB-1016 Peak 8 Ave 49.1045.34 1080 1000 8.3 15.0

PCB-1260 Peak 1 Ave 163.1158.6 1030 1000 2.9 15.0

PCB-1260 Peak 2 Ave 288.1278.8 1030 1000 3.4 15.0

PCB-1260 Peak 3 Ave 270.6255.4 1060 1000 5.9 15.0

PCB-1260 Peak 4 Ave 128.4125.3 1030 1000 2.5 15.0

PCB-1260 Peak 5 Ave 132.9129.6 1030 1000 2.6 15.0

PCB-1260 Peak 6 Ave 162.4147.4 1100 1000 10.2 15.0

PCB-1260 Peak 7 Ave 95.3490.23 1060 1000 5.7 15.0

PCB-1260 Peak 8 Ave 84.3973.32 1150 1000 15.1* 15.0



FORM VII 8082

06/03/2010 of 623

FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:



0.53(mm)

460-13139-1

PESTGC7

05/14/2010 17:55

05/04/2010 16:54

05/04/2010 17:58

CCVRT 460-37531/3

CLP-1

TestAmerica Edison

Lab File ID: or077394.d

Analyte RTTO FROM

RT WINDOW

PCB-1016 Peak 1 2.27 2.19 2.33

PCB-1016 Peak 2 2.59 2.51 2.65

PCB-1016 Peak 3 2.78 2.70 2.84

PCB-1016 Peak 4 3.04 2.97 3.11

PCB-1016 Peak 5 3.19 3.11 3.25

PCB-1016 Peak 6 3.25 3.17 3.31

PCB-1016 Peak 7 3.62 3.54 3.68

PCB-1016 Peak 8 3.71 3.64 3.78

PCB-1260 Peak 1 5.02 4.95 5.09

PCB-1260 Peak 2 5.37 5.29 5.43

PCB-1260 Peak 3 5.71 5.64 5.78

PCB-1260 Peak 4 5.85 5.78 5.92

PCB-1260 Peak 5 6.17 6.09 6.23

PCB-1260 Peak 6 7.09 7.02 7.16

PCB-1260 Peak 7 7.24 7.17 7.31

PCB-1260 Peak 8 8.42 8.35 8.49



Form VII 8082

06/03/2010 of 623

FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:



0.53(mm)

460-13139-1

PESTGC7

05/15/2010 00:03

05/04/2010 16:54

05/04/2010 17:58

CCV 460-37531/25

CLP-2

TestAmerica Edison

Lab File ID: of077416.d Conc. Units: ug/L



PCB-1016 Peak 1 Ave 112.7113.3 995 1000 -0.5 15.0

PCB-1016 Peak 2 Ave 243.6236.5 1030 1000 3.0 15.0

PCB-1016 Peak 3 Ave 124.8110.5 1130 1000 13.0 15.0

PCB-1016 Peak 4 Ave 450.4428.1 1050 1000 5.2 15.0

PCB-1016 Peak 5 Ave 213.4200.6 1060 1000 6.4 15.0

PCB-1016 Peak 6 Ave 130.5133.2 980 1000 -2.0 15.0

PCB-1016 Peak 7 Ave 160.3154.2 1040 1000 4.0 15.0

PCB-1016 Peak 8 Ave 164.1155.7 1050 1000 5.4 15.0

PCB-1260 Peak 1 Ave 310.4304.0 1020 1000 2.1 15.0

PCB-1260 Peak 2 Ave 349.7340.2 1030 1000 2.8 15.0

PCB-1260 Peak 3 Ave 504.4483.5 1040 1000 4.3 15.0

PCB-1260 Peak 4 Ave 249.7242.5 1030 1000 2.9 15.0

PCB-1260 Peak 5 Ave 155.0146.4 1060 1000 5.9 15.0

PCB-1260 Peak 6 Ave 283.3265.9 1070 1000 6.5 15.0

PCB-1260 Peak 7 Ave 407.6370.6 1100 1000 10.0 15.0

PCB-1260 Peak 8 Ave 136.7125.3 1090 1000 9.0 15.0



FORM VII 8082

06/03/2010 of 623

FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:



0.53(mm)

460-13139-1

PESTGC7

05/15/2010 00:03

05/04/2010 16:54

05/04/2010 17:58

CCV 460-37531/25

CLP-2

TestAmerica Edison

Lab File ID: of077416.d

Analyte RTTO FROM

RT WINDOW

PCB-1016 Peak 1 2.56 2.49 2.63

PCB-1016 Peak 2 2.99 2.92 3.06

PCB-1016 Peak 3 3.26 3.19 3.33

PCB-1016 Peak 4 3.51 3.44 3.58

PCB-1016 Peak 5 3.67 3.60 3.74

PCB-1016 Peak 6 3.96 3.89 4.03

PCB-1016 Peak 7 4.23 4.16 4.30

PCB-1016 Peak 8 4.38 4.31 4.45

PCB-1260 Peak 1 5.83 5.76 5.90

PCB-1260 Peak 2 6.12 6.05 6.19

PCB-1260 Peak 3 6.64 6.58 6.72

PCB-1260 Peak 4 6.81 6.74 6.88

PCB-1260 Peak 5 6.90 6.83 6.97

PCB-1260 Peak 6 7.34 7.28 7.42

PCB-1260 Peak 7 8.76 8.69 8.83

PCB-1260 Peak 8 9.63 9.56 9.70



Form VII 8082

06/03/2010 of 623

FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:



0.53(mm)

460-13139-1

PESTGC7

05/15/2010 00:03

05/04/2010 16:54

05/04/2010 17:58

CCV 460-37531/25

CLP-1

TestAmerica Edison

Lab File ID: or077416.d Conc. Units: ug/L



PCB-1016 Peak 1 Ave 73.8175.80 974 1000 -2.6 15.0

PCB-1016 Peak 2 Ave 130.6131.0 996 1000 -0.4 15.0

PCB-1016 Peak 3 Ave 96.6391.55 1060 1000 5.5 15.0

PCB-1016 Peak 4 Ave 265.8248.3 1070 1000 7.0 15.0

PCB-1016 Peak 5 Ave 105.7101.9 1040 1000 3.6 15.0

PCB-1016 Peak 6 Ave 75.9670.04 1080 1000 8.5 15.0

PCB-1016 Peak 7 Ave 111.5106.5 1050 1000 4.7 15.0

PCB-1016 Peak 8 Ave 50.4445.34 1110 1000 11.2 15.0

PCB-1260 Peak 1 Ave 160.9158.6 1010 1000 1.5 15.0

PCB-1260 Peak 2 Ave 282.9278.8 1010 1000 1.5 15.0

PCB-1260 Peak 3 Ave 267.1255.4 1050 1000 4.5 15.0

PCB-1260 Peak 4 Ave 126.1125.3 1010 1000 0.6 15.0

PCB-1260 Peak 5 Ave 131.2129.6 1010 1000 1.3 15.0

PCB-1260 Peak 6 Ave 149.5147.4 1010 1000 1.4 15.0

PCB-1260 Peak 7 Ave 98.9690.23 1100 1000 9.7 15.0

PCB-1260 Peak 8 Ave 83.3073.32 1140 1000 13.6 15.0



FORM VII 8082

06/03/2010 of 623

FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:



0.53(mm)

460-13139-1

PESTGC7

05/15/2010 00:03

05/04/2010 16:54

05/04/2010 17:58

CCV 460-37531/25

CLP-1

TestAmerica Edison

Lab File ID: or077416.d

Analyte RTTO FROM

RT WINDOW

PCB-1016 Peak 1 2.27 2.19 2.33

PCB-1016 Peak 2 2.59 2.51 2.65

PCB-1016 Peak 3 2.78 2.70 2.84

PCB-1016 Peak 4 3.04 2.97 3.11

PCB-1016 Peak 5 3.18 3.11 3.25

PCB-1016 Peak 6 3.24 3.17 3.31

PCB-1016 Peak 7 3.61 3.54 3.68

PCB-1016 Peak 8 3.71 3.64 3.78

PCB-1260 Peak 1 5.02 4.95 5.09

PCB-1260 Peak 2 5.36 5.29 5.43

PCB-1260 Peak 3 5.71 5.64 5.78

PCB-1260 Peak 4 5.85 5.78 5.92

PCB-1260 Peak 5 6.16 6.09 6.23

PCB-1260 Peak 6 7.08 7.02 7.16

PCB-1260 Peak 7 7.23 7.17 7.31

PCB-1260 Peak 8 8.42 8.35 8.49



Form VII 8082

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1




Solid

TestAmerica Edison


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/14/2010 18:20

N

10(mL)


% Moisture:





FORM I 8082

06/03/2010 of 623


TestAmerica

GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC7.i/8082/front/May10/05-14-10/14may10a.b/of077395.dLab Smp Id: MB 460-37391/1-A Inj Date : 14-MAY-2010 18:20 Operator : 615 Inst ID: PESTGC7.iSmp Info : MB 460-37391/1-AMisc Info : Comment : Method : /chem1/PESTGC7.i/8082/front/May10/05-14-10/14may10a.b/08Of8082.mMeth Date : 05-May-2010 00:12 diazc Quant Type: ESTDCal Date : 04-MAY-2010 19:52 Cal File: of077121.dAls bottle: 4 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: AllPCB.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3





CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====


10.212 10.205 0.007 169651 48.7738 32 80.00- 120.00 100.00

-------------------------------------------------------------------------------

06/03/2010 of 623


Date: 14-MAY-2010 18:20


Sample Info: MB 460-37391/1-A Operator: 615

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1




Solid

TestAmerica Edison


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/14/2010 18:20

N

10(mL)


% Moisture:




Aroclor 101612674-11-2 67 67 13U

Aroclor 122111104-28-2 67 67 20U

Aroclor 123211141-16-5 67 67 38U

Aroclor 124253469-21-9 67 67 13U

Aroclor 124812672-29-6 67 67 18U

Aroclor 125411097-69-1 67 67 23U

Aroclor 126011096-82-5 67 67 7.5U

Aroclor 126237324-23-5 67 67 12U

Aroclor 126811100-14-4 67 67 12U



FORM I 8082

06/03/2010 of 623


TestAmerica

GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC7.i/8082/rear/May10/05-14-10/14may10a.b/or077395.dLab Smp Id: MB 460-37391/1-A Inj Date : 14-MAY-2010 18:20 Operator : 615 Inst ID: PESTGC7.iSmp Info : MB 460-37391/1-AMisc Info : Comment : Method : /chem1/PESTGC7.i/8082/rear/May10/05-14-10/14may10a.b/08Or8082.mMeth Date : 05-May-2010 00:19 diazc Quant Type: ESTDCal Date : 04-MAY-2010 19:52 Cal File: or077121.dAls bottle: 4 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: AllPCB.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3





CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====


9.280 9.278 0.002 113769 47.1083 80.00- 120.00 100.00(aR)

-------------------------------------------------------------------------------

QC Flag Legend



06/03/2010 of 623


Date: 14-MAY-2010 18:20


Sample Info: MB 460-37391/1-A Operator: 615

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1




Solid

TestAmerica Edison


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/14/2010 18:37

N

10(mL)


% Moisture:




Aroclor 101612674-11-2 316 67 13

Aroclor 122111104-28-2 67 67 20U

Aroclor 123211141-16-5 67 67 38U

Aroclor 124253469-21-9 67 67 13U

Aroclor 124812672-29-6 67 67 18U

Aroclor 125411097-69-1 67 67 23U

Aroclor 126011096-82-5 328 67 7.5

Aroclor 126237324-23-5 67 67 12U

Aroclor 126811100-14-4 67 67 12U



FORM I 8082

06/03/2010 of 623


TestAmerica

GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC7.i/8082/front/May10/05-14-10/14may10a.b/of077396.dLab Smp Id: LCS 460-37391/2-A Inj Date : 14-MAY-2010 18:37 Operator : 615 Inst ID: PESTGC7.iSmp Info : LCS 460-37391/2-AMisc Info : Comment : Method : /chem1/PESTGC7.i/8082/front/May10/05-14-10/14may10a.b/08Of8082.mMeth Date : 05-May-2010 00:12 diazc Quant Type: ESTDCal Date : 04-MAY-2010 19:52 Cal File: of077121.dAls bottle: 5 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: AllPCB.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3





CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====

21 Aroclor-1016 CAS #: 12674-11-2

2.570 2.555 0.015 48413 427.392 280 80.00- 120.00 100.00(M)

3.005 2.990 0.015 109671 463.790 310 154.12- 231.18 226.53

3.268 3.255 0.013 54836 496.456 330 80.74- 121.11 113.27

3.517 3.505 0.012 196527 459.119 310 297.01- 445.51 405.94

3.677 3.665 0.012 95218 474.578 320 139.34- 209.02 196.68

3.967 3.955 0.012 65663 492.949 330 83.83- 125.74 135.63

4.238 4.227 0.011 71216 461.817 310 96.10- 144.15 147.10

4.390 4.380 0.010 80281 515.703 340 119.05- 178.58 165.83


-------------------------------------------------------------------------------

27 Aroclor-1260 CAS #: 11096-82-5

5.838 5.832 0.006 150452 494.905 330 80.00- 120.00 100.00(M)

06/03/2010 of 623


CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====

27 Aroclor-1260 (continued)

6.125 6.118 0.007 168663 495.842 330 89.81- 134.72 112.10

6.653 6.645 0.008 231224 478.217 320 132.01- 198.02 153.69

6.815 6.807 0.008 119847 494.115 330 64.57- 96.85 79.66

6.908 6.900 0.008 75364 514.870 340 40.81- 61.21 50.09

7.353 7.345 0.008 131515 494.546 330 73.71- 110.57 87.41

8.765 8.758 0.007 175999 474.892 320 102.65- 153.97 116.98

9.632 9.627 0.005 61568 491.267 330 35.41- 53.12 40.92


-------------------------------------------------------------------------------


10.207 10.205 0.002 180882 52.0026 35 80.00- 120.00 100.00

-------------------------------------------------------------------------------

QC Flag Legend

M - Compound response manually integrated.

06/03/2010 of 623


Date: 14-MAY-2010 18:37


Sample Info: LCS 460-37391/2-A Operator: 615

06/03/2010 of 623


Data File: of077396.dInj. Date and Time: 14-MAY-2010 18:37Instrument ID: PESTGC7.iClient ID: Compound: 21 Aroclor-1016CAS #: 12674-11-2Report Date: 05/16/2010


Not Detected

Expected RT: 2.56


RT: 2.57

Response: 48413

Amount: 473.98

Conc: 320.00

Manually Integrated By: diazcManual Integration Reason: Baseline Event

06/03/2010 of 623


Data File: of077396.dInj. Date and Time: 14-MAY-2010 18:37Instrument ID: PESTGC7.iClient ID: Compound: 27 Aroclor-1260CAS #: 11096-82-5Report Date: 05/16/2010


Not Detected

Expected RT: 5.83


RT: 5.84

Response: 150452

Amount: 492.33

Conc: 330.00


06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1




Solid

TestAmerica Edison


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/14/2010 18:37

N

10(mL)


% Moisture:




Aroclor 101612674-11-2 278 67 13

Aroclor 122111104-28-2 67 67 20U

Aroclor 123211141-16-5 67 67 38U

Aroclor 124253469-21-9 67 67 13U

Aroclor 124812672-29-6 67 67 18U

Aroclor 125411097-69-1 67 67 23U

Aroclor 126011096-82-5 314 67 7.5

Aroclor 126237324-23-5 67 67 12U

Aroclor 126811100-14-4 67 67 12U



FORM I 8082

06/03/2010 of 623


TestAmerica

GC ORGANICS QUANTITATION REPORTData file : /chem1/PESTGC7.i/8082/rear/May10/05-14-10/14may10a.b/or077396.dLab Smp Id: LCS 460-37391/2-A Inj Date : 14-MAY-2010 18:37 Operator : 615 Inst ID: PESTGC7.iSmp Info : LCS 460-37391/2-AMisc Info : Comment : Method : /chem1/PESTGC7.i/8082/rear/May10/05-14-10/14may10a.b/08Or8082.mMeth Date : 05-May-2010 00:19 diazc Quant Type: ESTDCal Date : 04-MAY-2010 19:52 Cal File: or077121.dAls bottle: 5 Dil Factor: 1.00000 Integrator: Falcon Compound Sublist: AllPCB.subTarget Version: 3.50 Sample Matrix: SOILProcessing Host: hpd3





CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====

21 Aroclor-1016 CAS #: 12674-11-2

2.275 2.263 0.012 29358 387.298 80.00- 120.00 100.00(aM)

2.592 2.582 0.010 54887 418.878 136.06- 204.09 186.96

2.782 2.772 0.010 38222 417.507 104.24- 156.37 130.19

3.043 3.035 0.008 107031 431.011 287.29- 430.94 364.57

3.187 3.177 0.010 43575 427.434 111.70- 167.55 148.43

3.247 3.238 0.009 28586 408.154 85.92- 128.89 97.37

3.617 3.610 0.007 46506 436.619 117.81- 176.71 158.41

3.713 3.707 0.006 18656 411.488 52.60- 78.90 63.55

-------------------------------------------------------------------------------

27 Aroclor-1260 CAS #: 11096-82-5

5.023 5.018 0.005 73720 464.912 80.00- 120.00 100.00(a)

5.365 5.362 0.003 128572 461.189 140.97- 211.46 174.41

06/03/2010 of 623


CONCENTRATIONS

ON-COL FINAL


== ====== ======== ======== ======= ======= ============ =====

27 Aroclor-1260 (continued)

5.712 5.707 0.005 116240 455.056 136.60- 204.90 157.68

5.852 5.848 0.004 58772 469.072 64.85- 97.27 79.72

6.165 6.163 0.002 58784 453.622 68.41- 102.62 79.74

7.088 7.085 0.003 64104 434.847 84.22- 126.34 86.96

7.238 7.237 0.001 47649 528.087 53.50- 80.26 64.64

8.425 8.422 0.003 36769 501.510 45.63- 68.45 49.88

-------------------------------------------------------------------------------


9.278 9.278 0.000 132329 54.7934 80.00- 120.00 100.00(aR)

-------------------------------------------------------------------------------

QC Flag Legend


R - Spike/Surrogate failed recovery limits.M - Compound response manually integrated.

06/03/2010 of 623


Date: 14-MAY-2010 18:37


Sample Info: LCS 460-37391/2-A Operator: 615

06/03/2010 of 623


Data File: or077396.dInj. Date and Time: 14-MAY-2010 18:37Instrument ID: PESTGC7.iClient ID: Compound: 21 Aroclor-1016CAS #: 12674-11-2Report Date: 05/16/2010


Not Detected

Expected RT: 2.26


RT: 2.27

Response: 29358

Amount: 417.30

Conc: 0.00


06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1




Solid

TestAmerica Edison

05/12/2010 09:50


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/14/2010 19:09

N

10(mL)


% Moisture: 3.0




Aroclor 101612674-11-2 357 69 13

Aroclor 122111104-28-2 69 69 21U

Aroclor 123211141-16-5 69 69 39U

Aroclor 124253469-21-9 69 69 13U

Aroclor 124812672-29-6 69 69 18U

Aroclor 125411097-69-1 69 69 24U

Aroclor 126011096-82-5 362 69 7.7

Aroclor 126237324-23-5 69 69 12U

Aroclor 126811100-14-4 69 69 12U



FORM I 8082

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1




Solid

TestAmerica Edison

05/12/2010 09:50


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/14/2010 19:09

N

10(mL)


% Moisture: 3.0




Aroclor 101612674-11-2 321 69 13

Aroclor 122111104-28-2 69 69 21U

Aroclor 123211141-16-5 69 69 39U

Aroclor 124253469-21-9 69 69 13U

Aroclor 124812672-29-6 69 69 18U

Aroclor 125411097-69-1 69 69 24U

Aroclor 126011096-82-5 331 69 7.7

Aroclor 126237324-23-5 69 69 12U

Aroclor 126811100-14-4 69 69 12U



FORM I 8082

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1




Solid

TestAmerica Edison

05/12/2010 09:50


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/14/2010 19:26

N

10(mL)


% Moisture: 3.0




Aroclor 101612674-11-2 364 69 13

Aroclor 122111104-28-2 69 69 21U

Aroclor 123211141-16-5 69 69 39U

Aroclor 124253469-21-9 69 69 13U

Aroclor 124812672-29-6 69 69 18U

Aroclor 125411097-69-1 69 69 24U

Aroclor 126011096-82-5 376 69 7.7

Aroclor 126237324-23-5 69 69 12U

Aroclor 126811100-14-4 69 69 12U



FORM I 8082

06/03/2010 of 623


Client Sample ID:

Lab Name: Job No.:

SDG No.:

460-13139-1




Solid

TestAmerica Edison

05/12/2010 09:50


GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1


05/14/2010 19:26

N

10(mL)


% Moisture: 3.0




Aroclor 101612674-11-2 335 69 13

Aroclor 122111104-28-2 69 69 21U

Aroclor 123211141-16-5 69 69 39U

Aroclor 124253469-21-9 69 69 13U

Aroclor 124812672-29-6 69 69 18U

Aroclor 125411097-69-1 69 69 24U

Aroclor 126011096-82-5 343 69 7.7

Aroclor 126237324-23-5 69 69 12U

Aroclor 126811100-14-4 69 69 12U



FORM I 8082

06/03/2010 of 623

Lab Name: Job No.:

SDG No.:

Instrument ID:


PCBS ANALYSIS RUN LOG

DILUTION

FACTOR



PESTGC7

36537

Start Date:

End Date: 05/04/2010 20:08

05/04/2010 16:04

ZZZZZ CLP-2 0.53(mm)105/04/2010 16:04

ZZZZZ CLP-1 0.53(mm)105/04/2010 16:04

PIBLK 460-36537/2 CLP-2 0.53(mm)105/04/2010 16:21

PIBLK 460-36537/2 CLP-1 0.53(mm)105/04/2010 16:21

ZZZZZ CLP-2 0.53(mm)105/04/2010 16:37

ZZZZZ CLP-1 0.53(mm)105/04/2010 16:37

IC 460-36537/4 CLP-2 0.53(mm)105/04/2010 16:54 of077110.d

IC 460-36537/4 CLP-1 0.53(mm)105/04/2010 16:54 or077110.d

IC 460-36537/5 CLP-2 0.53(mm)105/04/2010 17:10 of077111.d

IC 460-36537/5 CLP-1 0.53(mm)105/04/2010 17:10 or077111.d

IC 460-36537/6 CLP-2 0.53(mm)105/04/2010 17:26 of077112.d

IC 460-36537/6 CLP-1 0.53(mm)105/04/2010 17:26 or077112.d

IC 460-36537/7 CLP-2 0.53(mm)105/04/2010 17:42 of077113.d

IC 460-36537/7 CLP-1 0.53(mm)105/04/2010 17:42 or077113.d

IC 460-36537/8 CLP-2 0.53(mm)105/04/2010 17:58 of077114.d

IC 460-36537/8 CLP-1 0.53(mm)105/04/2010 17:58 or077114.d

IC 460-36537/9 CLP-2 0.53(mm)105/04/2010 18:15 of077115.d

IC 460-36537/9 CLP-1 0.53(mm)105/04/2010 18:15 or077115.d

IC 460-36537/10 CLP-2 0.53(mm)105/04/2010 18:31 of077116.d

IC 460-36537/10 CLP-1 0.53(mm)105/04/2010 18:31 or077116.d

IC 460-36537/11 CLP-2 0.53(mm)105/04/2010 18:47 of077117.d

IC 460-36537/11 CLP-1 0.53(mm)105/04/2010 18:47 or077117.d

IC 460-36537/12 CLP-2 0.53(mm)105/04/2010 19:03 of077118.d

IC 460-36537/12 CLP-1 0.53(mm)105/04/2010 19:03 or077118.d

IC 460-36537/13 CLP-2 0.53(mm)105/04/2010 19:19 of077119.d

IC 460-36537/13 CLP-1 0.53(mm)105/04/2010 19:19 or077119.d

IC 460-36537/14 CLP-2 0.53(mm)105/04/2010 19:36 of077120.d

IC 460-36537/14 CLP-1 0.53(mm)105/04/2010 19:36 or077120.d

IC 460-36537/15 CLP-2 0.53(mm)105/04/2010 19:52 of077121.d

IC 460-36537/15 CLP-1 0.53(mm)105/04/2010 19:52 or077121.d

ZZZZZ CLP-2 0.53(mm)105/04/2010 20:08

ZZZZZ CLP-1 0.53(mm)105/04/2010 20:08

8082

06/03/2010 of 623

Lab Name: Job No.:

SDG No.:

Instrument ID:



DILUTION

FACTOR



PESTGC7

37531

Start Date:

End Date: 05/15/2010 00:03

05/14/2010 17:22

RINSE 460-37531/1 CLP-2 0.53(mm)105/14/2010 17:22

RINSE 460-37531/1 CLP-1 0.53(mm)105/14/2010 17:22

PIBLK 460-37531/2 CLP-2 0.53(mm)105/14/2010 17:39

PIBLK 460-37531/2 CLP-1 0.53(mm)105/14/2010 17:39

CCVRT 460-37531/3 CLP-2 0.53(mm)105/14/2010 17:55 of077394.d

CCVRT 460-37531/3 CLP-1 0.53(mm)105/14/2010 17:55 or077394.d

MB 460-37391/1-A CLP-2 0.53(mm)105/14/2010 18:20 of077395.d

MB 460-37391/1-A CLP-1 0.53(mm)105/14/2010 18:20 or077395.d

LCS 460-37391/2-A CLP-2 0.53(mm)105/14/2010 18:37 of077396.d

LCS 460-37391/2-A CLP-1 0.53(mm)105/14/2010 18:37 or077396.d

ZZZZZ CLP-2 0.53(mm)105/14/2010 18:53

ZZZZZ CLP-1 0.53(mm)105/14/2010 18:53

460-13137-A-1-B MS CLP-2 0.53(mm)105/14/2010 19:09 of077398.d

460-13137-A-1-B MS CLP-1 0.53(mm)105/14/2010 19:09 or077398.d

460-13137-A-1-C MSD CLP-2 0.53(mm)105/14/2010 19:26 of077399.d

460-13137-A-1-C MSD CLP-1 0.53(mm)105/14/2010 19:26 or077399.d

ZZZZZ CLP-2 0.53(mm)105/14/2010 19:43

ZZZZZ CLP-1 0.53(mm)105/14/2010 19:43

460-13139-2 TB-3 6-7 CLP-2 0.53(mm)105/14/2010 19:59 of077401.d

460-13139-2 TB-3 6-7 CLP-1 0.53(mm)105/14/2010 19:59 or077401.d

ZZZZZ CLP-2 0.53(mm)105/14/2010 20:15

ZZZZZ CLP-1 0.53(mm)105/14/2010 20:15

460-13139-4 TB-2 5-6 CLP-2 0.53(mm)105/14/2010 20:32 of077403.d

460-13139-4 TB-2 5-6 CLP-1 0.53(mm)105/14/2010 20:32 or077403.d

460-13139-5 TB-1 2-3 CLP-2 0.53(mm)105/14/2010 20:48 of077404.d

460-13139-5 TB-1 2-3 CLP-1 0.53(mm)105/14/2010 20:48 or077404.d

ZZZZZ CLP-2 0.53(mm)105/14/2010 21:05

ZZZZZ CLP-1 0.53(mm)105/14/2010 21:05

460-13139-7 TB-5 3-4 CLP-2 0.53(mm)105/14/2010 21:21 of077406.d

460-13139-7 TB-5 3-4 CLP-1 0.53(mm)105/14/2010 21:21 or077406.d

ZZZZZ CLP-2 0.53(mm)105/14/2010 21:38

ZZZZZ CLP-1 0.53(mm)105/14/2010 21:38

ZZZZZ CLP-2 0.53(mm)105/14/2010 21:54

ZZZZZ CLP-1 0.53(mm)105/14/2010 21:54

ZZZZZ CLP-2 0.53(mm)105/14/2010 22:10

ZZZZZ CLP-1 0.53(mm)105/14/2010 22:10

ZZZZZ CLP-2 0.53(mm)105/14/2010 22:27

ZZZZZ CLP-1 0.53(mm)105/14/2010 22:27

ZZZZZ CLP-2 0.53(mm)105/14/2010 22:43

ZZZZZ CLP-1 0.53(mm)105/14/2010 22:43

ZZZZZ CLP-2 0.53(mm)105/14/2010 22:58

ZZZZZ CLP-1 0.53(mm)105/14/2010 22:58

ZZZZZ CLP-2 0.53(mm)105/14/2010 23:15

ZZZZZ CLP-1 0.53(mm)105/14/2010 23:15

ZZZZZ CLP-2 0.53(mm)105/14/2010 23:31

8082

06/03/2010 of 623

Lab Name: Job No.:

SDG No.:

Instrument ID:



DILUTION

FACTOR



PESTGC7

37531

Start Date:

End Date: 05/15/2010 00:03

05/14/2010 17:22

ZZZZZ CLP-1 0.53(mm)105/14/2010 23:31

PIBLK 460-37531/24 CLP-2 0.53(mm)105/14/2010 23:47

PIBLK 460-37531/24 CLP-1 0.53(mm)105/14/2010 23:47

CCV 460-37531/25 CLP-2 0.53(mm)105/15/2010 00:03 of077416.d

CCV 460-37531/25 CLP-1 0.53(mm)105/15/2010 00:03 or077416.d

8082

06/03/2010 of 623


Method: 3541

Analyst: Alinea, Archilles R


Batch End:

May 14 2010 7:19AM

May 14 2010 2:30PM


sample

Position on the

SoxTherm

OP_PCBSP_00013 OPPSTPCBSU_00014Initial weight/volume of

sample

Method Chain

MB~460-37391/1 15.00 g 10 mL 50 uL733541, 8082

LCS~460-37391/2 15.00 g 10 mL 50 uL50 uL743541, 8082

460-13137-A-1~MS T 15.03 g 10 mL 50 uL50 uL753541, 8082

460-13137-A-1~MS

D

T 15.02 g 10 mL 50 uL50 uL763541, 8082

460-13139-E-1 TB-3 2-3 T 15.04 g 10 mL 50 uL77

460-13139-E-2 TB-3 6-7 T 15.00 g 10 mL 50 uL783541, 8082

460-13139-E-3 TB-2 2-3 T 15.05 g 10 mL 50 uL79

460-13139-E-4 TB-2 5-6 T 15.03 g 10 mL 50 uL803541, 8082

460-13139-E-5 TB-1 2-3 T 15.02 g 10 mL 50 uL813541, 8082

460-13139-E-6 TB-1 5-6 T 15.04 g 10 mL 50 uL82

460-13139-E-7 TB-5 3-4 T 15.02 g 10 mL 50 uL833541, 8082

460-13139-E-8 TB-4 6-7 T 15.01 g 10 mL 50 uL84

460-13137-A-1 T 15.00 g 10 mL 50 uL85

460-13137-A-2 T 15.02 g 10 mL 50 uL86

460-13137-A-3 T 15.03 g 10 mL 50 uL87

460-13137-A-4 T 15.03 g 10 mL 50 uL88

460-13137-A-5 T 15.02 g 10 mL 50 uL89

460-13137-A-6 T 15.01 g 10 mL 50 uL90

460-13137-A-7 T 15.00 g 10 mL 50 uL97

460-13137-A-8 T 15.04 g 10 mL 50 uL98

460-13146-G-1 T 15.01 g 10 mL 50 uL99

460-13147-A-1 T 15.03 g 10 mL 50 uL100

460-13147-B-2 T 15.02 g 10 mL 50 uL101

460-13148-B-1 T 15.05 g 10 mL 50 uL102

First Start time: 719am

Person's name who did the prep: archie

Person's name who witnessed reagent drop: juan r

First End time: 230pm

SOP Number: 3541

Balance ID: 30

Na2SO4 Lot Number: h39602

Solvent: hex./ace. mixed

Vendor lot number: h35e09

Blank Soil Lot Number: h39602

Florisil Lot #: n/a

TBA Lot #: op083

06/03/2010 of 623


Method: 3541

Analyst: Alinea, Archilles R


Batch End:

May 14 2010 7:19AM

May 14 2010 2:30PM


Comments


MB~460-37391/1 3541, 8082

LCS~460-37391/2 3541, 8082

460-13137-A-1~MS T3541, 8082

460-13137-A-1~MS

D

T3541, 8082

460-13139-E-1 TB-3 2-3 T

460-13139-E-2 TB-3 6-7 T3541, 8082

460-13139-E-3 TB-2 2-3 T

460-13139-E-4 TB-2 5-6 T3541, 8082

460-13139-E-5 TB-1 2-3 T3541, 8082

460-13139-E-6 TB-1 5-6 T

460-13139-E-7 TB-5 3-4 T3541, 8082

460-13139-E-8 TB-4 6-7 T

460-13137-A-1 T

460-13137-A-2 T

460-13137-A-3 T

460-13137-A-4 T

460-13137-A-5 T

460-13137-A-6 T

460-13137-A-7 T

460-13137-A-8 T

460-13146-G-1 T

460-13147-A-1 T

460-13147-B-2 T

460-13148-B-1 T

Batch Comment: pcb-soil

06/03/2010 of 623

METALS

06/03/2010 of 623

COVER PAGE

Lab Name: Job Number:

Client Sample ID Lab Sample ID

METALS


SDG No.:

460-13139-1TestAmerica Edison

TB-3 6-7 460-13139-2

TB-2 5-6 460-13139-4

TB-1 2-3 460-13139-5

TB-5 3-4 460-13139-7

Comments:

06/03/2010 of 623

1A-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:


Date Received: 05/13/2010 18:30

460-13139-1

TB-3 6-7

Soil 05/12/2010 09:45Date Sampled:

Reporting Basis: DRY

METALS

TestAmerica Edison

% Solids: 81.2

CAS No. Analyte Conc. CUnits Q MethodRL MDL DIL

7440-36-0 Antimony 2.3 Umg/Kg2.3 1.0 4 6010B

7440-38-2 Arsenic 1.9 mg/Kg1.2 0.81 4 6010B

7440-41-7 Beryllium 0.20 Jmg/Kg0.46 0.20 4 6010B

7440-43-9 Cadmium 1.2 Umg/Kg1.2 0.18 4 6010B

7440-47-3 Chromium 9.1 mg/Kg2.3 1.4 4 6010B

7440-50-8 Copper 13.9 mg/Kg5.8 0.95 4 6010B

7439-92-1 Lead 17.5 mg/Kg1.2 0.58 4 6010B

7440-02-0 Nickel 7.0 Jmg/Kg9.3 0.62 4 6010B

7782-49-2 Selenium 2.3 Umg/Kg2.3 1.1 4 6010B

7440-22-4 Silver 2.3 Umg/Kg2.3 0.18 4 6010B

7440-28-0 Thallium 2.3 Umg/Kg2.3 1.1 4 6010B

7440-66-6 Zinc 31.3 mg/Kg7.0 1.1 4 6010B

7439-97-6 Mercury 0.039 Umg/Kg0.039 0.030 1 7471A

FORM IA-IN 06/03/2010 of 623

1A-IN


Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:


Date Received: 05/13/2010 18:30

460-13139-1

TB-2 5-6



METALS

TestAmerica Edison

% Solids: 87.2


7440-36-0 Antimony 2.3 Umg/Kg2.3 1.0 4 6010B

7440-38-2 Arsenic 4.5 mg/Kg1.1 0.80 4 6010B

7440-41-7 Beryllium 0.37 Jmg/Kg0.46 0.20 4 6010B

7440-43-9 Cadmium 0.98 Jmg/Kg1.1 0.18 4 6010B

7440-47-3 Chromium 17.9 mg/Kg2.3 1.4 4 6010B

7440-50-8 Copper 71.8 mg/Kg5.7 0.94 4 6010B

7439-92-1 Lead 251 mg/Kg1.1 0.57 4 6010B

7440-02-0 Nickel 11.9 mg/Kg9.2 0.61 4 6010B

7782-49-2 Selenium 2.3 Umg/Kg2.3 1.1 4 6010B

7440-22-4 Silver 4.9 mg/Kg B2.3 0.17 4 6010B

7440-28-0 Thallium 2.3 Umg/Kg2.3 1.1 4 6010B

7440-66-6 Zinc 137 mg/Kg6.9 1.1 4 6010B

7439-97-6 Mercury 0.22 mg/Kg0.035 0.028 1 7471A

FORM IA-IN 06/03/2010 of 623

1A-IN


Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:


Date Received: 05/13/2010 18:30

460-13139-1

TB-1 2-3



METALS

TestAmerica Edison

% Solids: 93.5


7440-36-0 Antimony 2.0 Umg/Kg2.0 0.89 4 6010B

7440-38-2 Arsenic 1.4 mg/Kg1.0 0.70 4 6010B

7440-41-7 Beryllium 0.40 Umg/Kg0.40 0.18 4 6010B

7440-43-9 Cadmium 1.0 Umg/Kg1.0 0.16 4 6010B

7440-47-3 Chromium 4.6 mg/Kg2.0 1.2 4 6010B

7440-50-8 Copper 7.2 mg/Kg5.0 0.82 4 6010B

7439-92-1 Lead 7.9 mg/Kg1.0 0.50 4 6010B

7440-02-0 Nickel 5.4 Jmg/Kg8.1 0.54 4 6010B

7782-49-2 Selenium 2.0 Umg/Kg2.0 0.94 4 6010B

7440-22-4 Silver 2.0 Umg/Kg2.0 0.15 4 6010B

7440-28-0 Thallium 2.0 Umg/Kg2.0 0.98 4 6010B

7440-66-6 Zinc 19.2 mg/Kg6.1 0.99 4 6010B

7439-97-6 Mercury 0.035 Umg/Kg0.035 0.028 1 7471A

FORM IA-IN 06/03/2010 of 623

1A-IN


Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:


Date Received: 05/13/2010 18:30

460-13139-1

TB-5 3-4



METALS

TestAmerica Edison

% Solids: 38.5


7440-36-0 Antimony 5.1 Umg/Kg5.1 2.2 4 6010B

7440-38-2 Arsenic 3.2 mg/Kg2.5 1.8 4 6010B

7440-41-7 Beryllium 1.0 Umg/Kg1.0 0.45 4 6010B

7440-43-9 Cadmium 1.1 Jmg/Kg2.5 0.40 4 6010B

7440-47-3 Chromium 6.7 mg/Kg5.1 3.0 4 6010B

7440-50-8 Copper 22.0 mg/Kg12.7 2.1 4 6010B

7439-92-1 Lead 222 mg/Kg2.5 1.3 4 6010B

7440-02-0 Nickel 7.0 Jmg/Kg20.4 1.4 4 6010B

7782-49-2 Selenium 5.1 Umg/Kg5.1 2.4 4 6010B

7440-22-4 Silver 5.1 Umg/Kg5.1 0.39 4 6010B

7440-28-0 Thallium 5.1 Umg/Kg5.1 2.5 4 6010B

7440-66-6 Zinc 152 mg/Kg15.3 2.5 4 6010B

7439-97-6 Mercury 0.31 mg/Kg0.082 0.064 1 7471A

FORM IA-IN 06/03/2010 of 623

2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:


ug/LME_CCV_DUO_00013

ME_CCV_DUO_00013

Analyte

ICV 460-37705/6

05/18/2010 11:04

Found C True %R

CCV 460-37705/18

05/18/2010 11:40

CCV 460-37705/30

05/18/2010 12:16

Found FoundC CTrue %R True %R

Antimony 962 949 9451000 1000 100096 95 94

Arsenic 2370 2340 23302500 2500 250095 94 93

Beryllium 996 1000 9861000 1000 1000100 100 99

Cadmium 1200 1190 11801250 1250 125096 95 94

Chromium 5100 5000 50205000 5000 5000102 100 100

Copper 12480 12430 1241012500 12500 12500100 99 99

Lead 7240 7160 71207500 7500 750097 95 95

Nickel 2420 2390 23802500 2500 250097 96 95

Selenium 2390 2350 23402500 2500 250095 94 94

Silver 1240 1210 12201250 1250 125099 97 97

Thallium 2440 2480 24902500 2500 250098 99 100

Zinc 2410 2390 23802500 2500 250096 96 95

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

06/03/2010 of 623

2A-IN

Lab Name: Job No.:

SDG No.:


CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:


ug/LME_DCAL-IN_00284

ME_DCAL-IN_00284

Analyte

ICV 460-37424/26-A

05/14/2010 12:16

Found C True %R

CCV 460-37424/28-A

05/14/2010 12:42

CCV 460-37424/28-A

05/14/2010 13:06

Found FoundC CTrue %R True %R

Mercury 842 837 855833 833 833101 100 103

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.


06/03/2010 of 623

Lab Name: Job No.:


SDG No.:

INSTRUMENT BLANKS

METALS


ug/L

CFoundCFoundCFoundCFoundRLAnalyte

ICB 460-37705/7 CCB 460-37705/19 CCB 460-37705/31

05/18/2010 11:08 05/18/2010 11:44 05/18/2010 12:19

3-IN

Antimony 10.0 10.0 10.010.0 U U U

Arsenic 5.0 5.0 5.05.0 U U U

Beryllium 2.0 2.0 2.02.0 U U U

Cadmium 5.0 5.0 5.05.0 U U U

Chromium 10.0 10.0 10.010.0 U U U

Copper 25.0 11.6 25.025.0 U J U

Lead 5.0 5.0 5.05.0 U U U

Nickel 40.0 40.0 40.040.0 U U U

Selenium 10.0 10.0 10.010.0 U U U

Silver 10.0 1.35 10.010.0 U J U

Thallium 10.0 10.0 10.010.0 U U U

Zinc 30.0 30.0 30.030.0 U U U

FORM III-IN


06/03/2010 of 623

Lab Name: Job No.:


SDG No.:

INSTRUMENT BLANKS

METALS


ug/L

CFoundCFoundCFoundCFoundRLAnalyte

ICB 460-37472/8 CCB 460-37472/21 CCB 460-37472/33

05/14/2010 12:18 05/14/2010 12:44 05/14/2010 13:08

3-IN

Mercury 0.20 0.20 0.200.20 U U U

FORM III-IN


06/03/2010 of 623

Lab Name: Job No.:

SDG No.:

Lab Sample ID: MB 460-37477/1-A ^2Concentration Units: mg/Kg

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

460-13139-1

Instrument Code: ICP4

METHOD BLANK

METALS

37705

TestAmerica Edison

7440-36-0 Antimony 1.0 U 6010B

7440-38-2 Arsenic 0.50 U 6010B

7440-41-7 Beryllium 0.20 U 6010B

7440-43-9 Cadmium 0.50 U 6010B

7440-47-3 Chromium 1.0 U 6010B

7440-50-8 Copper 2.5 U 6010B

7439-92-1 Lead 0.50 U 6010B

7440-02-0 Nickel 4.0 U 6010B

7782-49-2 Selenium 1.0 U 6010B

7440-22-4 Silver 0.0811 J 6010B

7440-28-0 Thallium 1.0 U 6010B

7440-66-6 Zinc 3.0 U 6010B

FORM III-IN

06/03/2010 of 623

Lab Name: Job No.:

SDG No.:

Lab Sample ID: MB 460-37424/1-AConcentration Units: mg/Kg

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

460-13139-1

Instrument Code: LEEMAN5

METHOD BLANK

METALS

37472

TestAmerica Edison

7439-97-6 Mercury 0.033 U 7471A

FORM III-IN

06/03/2010 of 623

4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:


Analyte

True

PercentRecovery

Found

SDG No.:

Lab File ID:

Solution A Solution A

Lab Sample ID:


ICSA 460-37705/8

05182010A.txt

ug/L

ME_ICSA_Duo_00013

ICP4

INTERFERENCE CHECK STANDARD

METALS

-0.0551Antimony

1.34Arsenic

-0.165Beryllium

-0.674Cadmium

-1.85Chromium

9.81Copper

1.65Lead

5.93Nickel

-0.864Selenium

2.20Silver

1.72Thallium

-4.84Zinc

482000Aluminum 500000 96

0.0719Barium

475400Calcium 500000 95

1.70Cobalt

171600Iron 200000 86

436700Magnesium 500000 87

0.742Manganese

-1.82Molybdenum

100Potassium

33.3Sodium

5.06Strontium

-0.316Tin

0.619Titanium

1.41Vanadium

FORM IVA-IN


06/03/2010 of 623

4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:


Analyte

True

PercentRecovery

Found

SDG No.:

Lab File ID:

Solution AB Solution AB

Lab Sample ID:


ICSAB 460-37705/9

05182010A.txt

ug/L

ME_ICSAB_DUO_00011

ICP4


METALS

86.4Antimony 100 86

92.1Arsenic 100 92

96.5Beryllium 100 97

85.6Cadmium 100 86

98.4Chromium 100 98

97.1Copper 100 97

88.3Lead 100 88

91.9Nickel 100 92

88.0Selenium 100 88

102Silver 100 102

87.4Thallium 100 87

83.0Zinc 100 83

493700Aluminum 500000 99

91.5Barium 100 92

488500Calcium 500000 98

87.7Cobalt 100 88

172600Iron 200000 86

435600Magnesium 500000 87

99.7Manganese 100 100

85.2Molybdenum 100 85

10160Potassium 10000 102

10360Sodium 10000 104

104Strontium 100 104

85.0Tin 100 85

91.2Titanium 100 91

100Vanadium 100 100

FORM IVA-IN


06/03/2010 of 623

4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:


Analyte

True

PercentRecovery

Found

SDG No.:

Lab File ID:

Solution A Solution A

Lab Sample ID:


ICSA 460-37705/33

05182010A.txt

ug/L

ME_ICSA_Duo_00013

ICP4


METALS

-1.32Antimony

4.24Arsenic

-0.103Beryllium

-0.641Cadmium

-1.60Chromium

4.48Copper

1.61Lead

5.87Nickel

-2.41Selenium

0.247Silver

0.567Thallium

-5.18Zinc

485400Aluminum 500000 97

-0.160Barium

474000Calcium 500000 95

1.58Cobalt

168900Iron 200000 84

426200Magnesium 500000 85

0.404Manganese

-1.68Molybdenum

-50.9Potassium

-23.5Sodium

5.10Strontium

0.221Tin

-0.130Titanium

1.47Vanadium

FORM IVA-IN


06/03/2010 of 623

4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:


Analyte

True

PercentRecovery

Found

SDG No.:

Lab File ID:

Solution AB Solution AB

Lab Sample ID:


ICSAB 460-37705/34

05182010A.txt

ug/L

ME_ICSAB_DUO_00011

ICP4


METALS

88.5Antimony 100 88

94.4Arsenic 100 94

94.2Beryllium 100 94

86.5Cadmium 100 86

98.8Chromium 100 99

96.5Copper 100 96

87.3Lead 100 87

91.8Nickel 100 92

88.3Selenium 100 88

103Silver 100 103

88.8Thallium 100 89

84.7Zinc 100 85

486100Aluminum 500000 97

92.3Barium 100 92

478800Calcium 500000 96

88.4Cobalt 100 88

171800Iron 200000 86

437200Magnesium 500000 87

98.9Manganese 100 99

84.8Molybdenum 100 85

9650Potassium 10000 96

10080Sodium 10000 101

101Strontium 100 101

86.2Tin 100 86

91.0Titanium 100 91

100Vanadium 100 100

FORM IVA-IN


06/03/2010 of 623

MATRIX SPIKE SAMPLE RECOVERY

METALS

5A-IN

TB-1 2-3 MS

Lab Name: Job No.:

SDG No.:

Client ID: Lab ID: 460-13139-5 MS

460-13139-1

Matrix: Concentration Units: mg/KgSolid

TestAmerica Edison

% Solids: 93.5

ControlLimit%RAnalyte SSR

C

SampleResult (SR)

C

SpikeAdded (SA) %R Q Method

Mercury 75-1250.214 0.035 0.178 120 7471AU

SSR = Spiked Sample Result

FORM VA - IN

Note - Results and Reporting Limits have been adjusted for dry weight.


06/03/2010 of 623

6-IN

DUPLICATES

TB-1 2-3 DU

Lab Name: Job No.:

SDG No.:

Matrix: Concentration Units: mg/Kg

Analyte

ControlLimit Sample (S)

C

Duplicate (D)

CRPD Q Method

460-13139-1

Solid

METALS

% Solids for Sample: 93.5 % Solids for Duplicate:

Client ID: Lab ID: 460-13139-5 DU

93.5

TestAmerica Edison

Mercury 0.035 U0.0350.035 NC 7471AU

FORM VI-IN


06/03/2010 of 623

7A-IN

LCS-STANDARD REFERENCE MATERIAL

METALS

Lab ID: LCSSRM 460-37477/2-A ^4


Sample Matrix: Solid LCS Source: ME_LCSS_62_00002

TestAmerica Edison

Analyte

Solid(mg/Kg)

True Found C %R Limits Q Method

Antimony 66.1 68.57 104 6010B32.0 353

Arsenic 102 93.00 91 6010B69.7 131

Beryllium 76.1 73.49 97 6010B74.0 126

Cadmium 59.5 53.69 90 6010B73.3 127

Chromium 231 228.8 99 6010B70.8 129

Copper 171 171.5 101 6010B75.3 124

Lead 84.3 86.10 102 6010B69.8 130

Nickel 131 123.8 94 6010B73.2 127

Selenium 280 249.4 89 6010B69.6 130

Silver 29.5 29.73 101 6010B65.1 135

Thallium 119 124.3 105 6010B67.8 133

Zinc 582 538.2 92 6010B73.6 127


FORM VIIA - IN

06/03/2010 of 623

7A-IN

LCS-STANDARD REFERENCE MATERIAL

METALS

Lab ID: LCSSRM 460-37424/2-A ^10


Sample Matrix: Solid LCS Source: ME_LCSS_62_00002

TestAmerica Edison

Analyte

Solid(mg/Kg)

True Found C %R Limits Q Method

Mercury 8.46 9.15 108 7471A51.3 149


FORM VIIA - IN

06/03/2010 of 623

8-IN

Lab ID: 460-13139-5

Lab Name: Job No:

Matrix: Concentration Units: mg/Kg

Analyte

Initial SampleResult (I) C

SerialDilutionResult (S) C

%Difference Q Method

SDG No:

Solid

460-13139-1

ICP-AES AND ICP-MS SERIAL DILUTIONS

METALS

TestAmerica Edison

Mercury 0.035 U 0.18 U NC 7471A

FORM VIII-IN


06/03/2010 of 623

9-IN

12/30/2008 10:24

Instrument ID: ICP4

460-13139-1Job Number:

Solid

3050B

Leach Method:

Prep Method:

Analysis Method:

Matrix:

SDG Number:

Lab Name:

DETECTION LIMITS

Analyte Wavelength/Mass

RL MDL

6010B MDL Date:

(mg/Kg) (mg/Kg)

METALS

TestAmerica Edison

Antimony 206.8 0.220.5

Arsenic 189.0 0.1740.25

Beryllium 313.0 0.0440.1

Cadmium 226.5 0.0390.25

Chromium 267.7 0.2970.5

Copper 324.7 0.2041.25

Lead 220.6 0.1250.25

Nickel 231.6 0.1342

Selenium 196.0 0.2340.5

Silver 328.0 0.0380.5

Thallium 190.8 0.2420.5

Zinc 206.2 0.2451.5

FORM IX - IN

06/03/2010 of 623

9-IN

12/30/2008 14:33

Instrument ID: LEEMAN5


Solid

7471A

Leach Method:

Prep Method:

Analysis Method:

Matrix:

SDG Number:

Lab Name:

DETECTION LIMITS


RL MDL

7471A MDL Date:

(mg/Kg) (mg/Kg)

METALS

TestAmerica Edison

Mercury 0.0260.033

FORM IX - IN

06/03/2010 of 623

11-IN

Lab Name: TestAmerica Edison Job No: 460-13139-1

Instrument ID: Date:

Analyte

Integ.Time(Sec.)

Concentration

Method

ICP-AES AND ICP-MS LINEAR RANGES

ICP4

SDG No.:

(ug/L)

01/06/2009 11:38

METALS

Antimony 2000 6010B

Arsenic 10000 6010B

Beryllium 2000 6010B

Cadmium 5000 6010B

Chromium 10000 6010B

Copper 25000 6010B

Lead 20000 6010B

Nickel 5000 6010B

Selenium 10000 6010B

Silver 2500 6010B

Thallium 10000 6010B

Zinc 5000 6010B

FORM XI - IN

06/03/2010 of 623

12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

Preparation Method:

LabSampleID

PreparationDate

InitialWeight

Final Volume

PrepBatch

460-13139-1

METALS

3050B

InitialVolume

(g) (mL)

TestAmerica Edison

05/14/2010 15:42 37477MB 460-37477/1-A ^2 501.00

05/14/2010 15:42 37477LCSSRM 460-37477/2-A ^4

501.02

05/14/2010 15:42 37477460-13139-2 501.06

05/14/2010 15:42 37477460-13139-4 501.00

05/14/2010 15:42 37477460-13139-5 501.06

05/14/2010 15:42 37477460-13139-7 501.02

FORM XII-IN

06/03/2010 of 623

12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

Preparation Method:

LabSampleID

PreparationDate

InitialWeight

Final Volume

PrepBatch

460-13139-1

METALS

7471A

InitialVolume

(g) (mL)

TestAmerica Edison

05/14/2010 09:25 37424MB 460-37424/1-A 1000.60

05/14/2010 09:25 37424LCSSRM 460-37424/2-A ^10

1000.60

05/14/2010 09:25 37424460-13139-5 1000.60

05/14/2010 09:25 37424460-13139-5 DU 1000.60

05/14/2010 09:25 37424460-13139-5 MS 1000.60

05/14/2010 09:25 37424460-13139-2 1000.63

05/14/2010 09:25 37424460-13139-4 1000.64

05/14/2010 09:25 37424460-13139-7 1000.63

FORM XII-IN

06/03/2010 of 623

13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:


ICP4

05/18/2010 10:49 05/18/2010 12:34

6010B

METALS

LabSampleID

D/F

Time

Analytes

Ag

As

Be

Cd

Cr

Cu

Ni

Pb

Sb

Se

Tl

Zn

Type

10:49ZZZZZZ

10:52ZZZZZZ

10:55ZZZZZZ

10:58ZZZZZZ

11:01ZZZZZZ

1 11:04 X X X X X X X X X X X XICV 460-37705/6

1 11:08 X X X X X X X X X X X XICB 460-37705/7

1 11:11 X X X X X X X X X X X XICSA 460-37705/8

1 11:14 X X X X X X X X X X X XICSAB 460-37705/9

11:17ZZZZZZ

2 11:20 X X X X X X X X X X X XMB 460-37477/1-A ^2 T

4 11:23 X X X X X X X X X X X XLCSSRM 460-37477/2-A ^4

T

11:26ZZZZZZ

11:29ZZZZZZ

11:32ZZZZZZ

11:34ZZZZZZ

11:37ZZZZZZ

1 11:40 X X X X X X X X X X X XCCV 460-37705/18

1 11:44 X X X X X X X X X X X XCCB 460-37705/19

11:46ZZZZZZ

11:49ZZZZZZ

11:53ZZZZZZ

4 11:55 X X X X X X X X X X X X460-13139-2 T

11:58ZZZZZZ

4 12:01 X X X X X X X X X X X X460-13139-4 T

4 12:04 X X X X X X X X X X X X460-13139-5 T

12:07ZZZZZZ

4 12:10 X X X X X X X X X X X X460-13139-7 T

12:13ZZZZZZ

1 12:16 X X X X X X X X X X X XCCV 460-37705/30

1 12:19 X X X X X X X X X X X XCCB 460-37705/31

12:22ZZZZZZ

1 12:25 X X X X X X X X X X X XICSA 460-37705/33

1 12:28 X X X X X X X X X X X XICSAB 460-37705/34

12:31CCV 460-37705/35

12:34CCB 460-37705/36

Prep Types

T = Total/NA

FORM XIII-IN 06/03/2010 of 623

13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:




LEEMAN5

05/14/2010 12:04 05/14/2010 13:08

7471A

METALS

LabSampleID

D/F

Time

Analytes

Hg

Type

12:04 XIC 460-37424/20-A

12:06 XIC 460-37424/21-A

12:08 XIC 460-37424/22-A

12:10 XIC 460-37424/23-A

12:12 XIC 460-37424/24-A

12:14 XIC 460-37424/25-A

1 12:16 XICV 460-37424/26-A

1 12:18 XICB 460-37472/8

12:20ZZZZZZ

1 12:22 XMB 460-37424/1-A T

10 12:24 XLCSSRM 460-37424/2-A ^10

T

1 12:26 X460-13139-5 T

1 12:28 X460-13139-5 DU T

1 12:31 X460-13139-5 MS T

12:33ZZZZZZ

12:34ZZZZZZ

12:36ZZZZZZ

12:38ZZZZZZ

12:41ZZZZZZ

1 12:42 XCCV 460-37424/28-A

1 12:44 XCCB 460-37472/21

12:46ZZZZZZ

12:48ZZZZZZ

12:50ZZZZZZ

1 12:52 X460-13139-2 T

12:53ZZZZZZ

1 12:55 X460-13139-4 T

12:57ZZZZZZ

1 12:59 X460-13139-7 T

13:01ZZZZZZ

5 13:04 X460-13139-5 SD T

1 13:06 XCCV 460-37424/28-A

1 13:08 XCCB 460-37472/33

Prep Types

T = Total/NA


Metals Worksheet

Method: 7471A

Analyst: Sheikh, Razia B


Batch End:

May 14 2010 9:25AM


sample

ME_DCAL-IN_00284 ME_DICV-IN_00286 ME_LCSS_62_00002Initial weight/volume of

sample

Method Chain

MB~460-37424/1 0.60 g 100 mL7471A, 7471A

LCSSRM~460-3742

4/2

0.60 g 100 mL 0.60 g7471A, 7471A

460-13139-E-5 TB-1 2-3 T 0.60 g 100 mL7471A, 7471A

460-13139-E-5~DU TB-1 2-3 T 0.60 g 100 mL7471A, 7471A

460-13139-E-5~MS TB-1 2-3 T 0.60 g 100 mL 1.00 mL7471A, 7471A

460-13148-D-1 T 0.68 g 100 mL

460-13118-A-1 T 0.63 g 100 mL

460-13118-A-2 T 0.61 g 100 mL

460-13118-A-3 T 0.61 g 100 mL

460-13146-F-1 T 0.69 g 100 mL

460-13147-B-1 T 0.68 g 100 mL

460-13147-A-2 T 0.61 g 100 mL

460-13139-E-1 TB-3 2-3 T 0.66 g 100 mL

460-13139-E-2 TB-3 6-7 T 0.63 g 100 mL7471A, 7471A

460-13139-E-3 TB-2 2-3 T 0.65 g 100 mL

460-13139-E-4 TB-2 5-6 T 0.64 g 100 mL7471A, 7471A

460-13139-E-6 TB-1 5-6 T 0.65 g 100 mL

460-13139-E-7 TB-5 3-4 T 0.63 g 100 mL7471A, 7471A

460-13139-E-8 TB-4 6-7 T 0.70 g 100 mL

IC~460-37424/20 0.60 g 100 mL

IC~460-37424/21 0.60 g 100 mL 0.1 mL

IC~460-37424/22 0.60 g 100 mL 1.0 mL

IC~460-37424/23 0.60 g 100 mL 2.0 mL

IC~460-37424/24 0.60 g 100 mL 5.0 mL

IC~460-37424/25 0.60 g 100 mL 10.0 mL

06/03/2010 of 623

Metals Worksheet

Method: 7471A

Analyst: Sheikh, Razia B


Batch End:

May 14 2010 9:25AM


sample

ME_DCAL-IN_00284 ME_DICV-IN_00286 ME_LCSS_62_00002Initial weight/volume of

sample

Method Chain

ICV~460-37424/26 0.60 g 100 mL 5.0 mL7471A, 7471A

qcs 0.60 g 100 mL 5.0 mL

CCV~460-37424/28 0.60 g 100 mL 5.0 mL7471A, 7471A

Hood ID or number: 1

Balance ID: 33

Lot # of Nitric Acid: h51022

Lot # of hydrochloric acid: h42a18

Potassium Permanganate Lot Number: 00605lh

Sulfuric Acid Lot Number: h46f04

Stannous Chloride Lot Number: g37640

Oven, Bath or Block Temperature 1: 121c

NaCL Lot #: g28618

Hydroxylamine Hydrochloride Lot: g50470

06/03/2010 of 623

Metals Worksheet

Method: 3050B

Analyst: Cheema, Ali R


Batch End:

May 14 2010 3:42PM


sample

ME_LCS-int_00020 ME_LCSS_62_00002Initial weight/volume of

sample

Method Chain

MB~460-37477/1 1.00 g 50 mL3050B, 6010B

LCSSRM~460-3747

7/2

1.02 g 50 mL 1.00 g3050B, 6010B

460-13152-A-3 T 1.09 g 50 mL

460-13152-A-1 T 1.05 g 50 mL

460-13152-A-2 T 1.07 g 50 mL

460-13139-E-1 TB-3 2-3 T 1.02 g 50 mL

460-13139-E-2 TB-3 6-7 T 1.06 g 50 mL3050B, 6010B

460-13139-E-3 TB-2 2-3 T 1.06 g 50 mL

460-13139-E-4 TB-2 5-6 T 1.00 g 50 mL3050B, 6010B

460-13139-E-5 TB-1 2-3 T 1.06 g 50 mL3050B, 6010B

460-13139-E-6 TB-1 5-6 T 1.00 g 50 mL

460-13139-E-7 TB-5 3-4 T 1.02 g 50 mL3050B, 6010B

460-13139-E-8 TB-4 6-7 T 1.02 g 50 mL

460-13139-E-8~DU T 1.02 g 50 mL

460-13139-E-8~MS T 1.02 g 50 mL 2 mL

Balance ID: 35

Lot # of hydrochloric acid: H35A01

Lot # of Nitric Acid: J04031

Hydrogen peroxide lot number: H26J05

Temperature: 95 Degrees C

06/03/2010 of 623

GENERAL CHEMISTRY

06/03/2010 of 623

COVER PAGE

Lab Name: Job Number:

Client Sample ID Lab Sample ID

GENERAL CHEMISTRY


SDG No.:

460-13139-1TestAmerica Edison

TB-3 2-3 460-13139-1

TB-3 6-7 460-13139-2

TB-2 2-3 460-13139-3

TB-2 5-6 460-13139-4

TB-1 2-3 460-13139-5

TB-1 5-6 460-13139-6

TB-5 3-4 460-13139-7

TB-4 6-7 460-13139-8

Comments:

06/03/2010 of 623

9-IN

02/15/2007 17:07

Instrument ID: NOEQUIP


Solid

Leach Method:

Prep Method:

Analysis Method:

Matrix:

SDG Number:

Lab Name:

DETECTION LIMITS


RL

Moisture RL Date:

(%)

GENERAL CHEMISTRY

TestAmerica Edison

Percent Moisture 1

Percent Solids 1

FORM IX - IN

06/03/2010 of 623

13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:




NOEQUIP

05/14/2010 21:47 05/14/2010 21:54

Moisture

GENERAL CHEMISTRY

LabSampleID

D/F

Time

Analytes

%Sol

Moist

Type

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

1 21:47 X X460-13139-1 T

1 21:47 X X460-13139-2 T

1 21:47 X X460-13139-3 T

1 21:47 X X460-13139-4 T

1 21:47 X X460-13139-5 T

1 21:47 X X460-13139-6 T

1 21:47 X X460-13139-8 T

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

1 21:47 X X460-13146-A-1 DU T

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

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21:47ZZZZZZ

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21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ


13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:




NOEQUIP

05/14/2010 21:47 05/14/2010 21:54

Moisture

GENERAL CHEMISTRY

LabSampleID

D/F

Time

Analytes

%Sol

Moist

Type

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

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21:47ZZZZZZ

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21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ


13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:




NOEQUIP

05/14/2010 21:47 05/14/2010 21:54

Moisture

GENERAL CHEMISTRY

LabSampleID

D/F

Time

Analytes

%Sol

Moist

Type

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

21:47ZZZZZZ

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21:53ZZZZZZ

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21:53ZZZZZZ

21:53ZZZZZZ

21:53ZZZZZZ

21:53ZZZZZZ

21:53ZZZZZZ

21:53ZZZZZZ

21:53ZZZZZZ


13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:




NOEQUIP

05/14/2010 21:47 05/14/2010 21:54

Moisture

GENERAL CHEMISTRY

LabSampleID

D/F

Time

Analytes

%Sol

Moist

Type

21:53ZZZZZZ

21:53ZZZZZZ

21:53ZZZZZZ

21:53ZZZZZZ

21:53ZZZZZZ

21:53ZZZZZZ

21:53ZZZZZZ

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21:53ZZZZZZ

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21:53ZZZZZZ

21:53ZZZZZZ


13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:




NOEQUIP

05/14/2010 21:47 05/14/2010 21:54

Moisture

GENERAL CHEMISTRY

LabSampleID

D/F

Time

Analytes

%Sol

Moist

Type

21:53ZZZZZZ

21:53ZZZZZZ

21:53ZZZZZZ

21:53ZZZZZZ

21:53ZZZZZZ

21:53ZZZZZZ

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21:54ZZZZZZ


13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:




NOEQUIP

05/14/2010 21:47 05/14/2010 21:54

Moisture

GENERAL CHEMISTRY

LabSampleID

D/F

Time

Analytes

%Sol

Moist

Type

21:54ZZZZZZ

21:54ZZZZZZ

21:54ZZZZZZ

21:54ZZZZZZ

21:54ZZZZZZ

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Prep Types

T = Total/NA


13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:




NOEQUIP

05/17/2010 19:56 05/17/2010 19:56

Moisture

GENERAL CHEMISTRY

LabSampleID

D/F

Time

Analytes

%Sol

Moist

Type

19:56ZZZZZZ

1 19:56 X X460-13139-7 T

19:56ZZZZZZ

19:56ZZZZZZ

19:56ZZZZZZ

19:56ZZZZZZ

1 19:56 X X460-13237-A-4 DU T

19:56ZZZZZZ

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19:56ZZZZZZ

19:56ZZZZZZ

19:56ZZZZZZ

Prep Types

T = Total/NA


General Chemistry Worksheet

Method: Moisture

Analyst: Dave, Virendra


Batch End:

May 14 2010 9:47PM

Lab ID Client ID Basis Empty Dish Weight Mass of wet Sample Mass of Dry SampleDish IDMethod Chain

PB~460-37508/1 13 1.01 g 1.01 g1.01 g

460-13148-A-1 T 15 1.04 g 8.01 g8.41 g

460-13120-A-1 T 14 1.04 g 5.92 g6.65 g

460-13120-A-2 T 83 1.02 g 5.62 g6.27 g

460-13187-D-1 T 165 1.01 g 6.35 g6.86 g

460-13187-D-2 T 74 1.04 g 6.13 g6.65 g

460-13139-D-1 TB-3 2-3 T 66 1.00 g 6.04 g7.14 gMoisture







460-13137-D-9 T 36 0.98 g 6.54 g7.54 g

460-13137-D-10 T 80 1.01 g 5.92 g7.01 g

460-13137-D-11 T 43 0.99 g 6.15 g7.64 g

460-13137-D-12 T 82 1.03 g 8.84 g9.46 g

460-13137-D-13 T 87 0.98 g 9.69 g9.88 g

460-13137-D-14 T 276 0.99 g 5.39 g7.06 g

460-13146-A-1 T 39 0.98 g 5.84 g6.78 g

460-13146-A-1~DU T 28 0.99 g 5.94 g6.89 gMoisture

460-13131-A-1 T 69 0.97 g 5.81 g7.03 g

460-13131-A-2 T 36 0.97 g 6.28 g7.20 g

460-13131-A-3 T 35 1.00 g 6.47 g7.46 g

460-13131-A-4 T 13 0.99 g 7.47 g9.25 g

06/03/2010 of 623


Method: Moisture



Batch End:

May 14 2010 9:47PM


460-13131-A-5 T 35 1.01 g 6.36 g7.38 g

460-13131-A-6 T 82 1.01 g 6.75 g7.24 g

460-13131-A-7 T 85 1.00 g 6.33 g7.26 g

460-13131-A-8 T 38 1.03 g 7.94 g8.97 g

460-13131-A-9 T 81 1.02 g 7.11 g7.89 g

460-13131-A-11 T 40 1.00 g 5.62 g6.56 g

460-13131-A-12 T 85 1.02 g 7.01 g8.40 g

460-13164-E-1 T 30 1.03 g 6.35 g7.75 g

460-13164-E-2 T 17 0.95 g 7.28 g8.23 g

460-13164-E-3 T 85 0.97 g 7.29 g8.68 g

460-13164-E-4 T 45 0.94 g 7.08 g7.81 g

460-13164-E-5 T 44 0.96 g 6.37 g7.35 g

460-13175-A-1 T 37 0.99 g 6.12 g7.13 g

460-13175-A-2 T 77 1.03 g 7.76 g8.48 g

460-13175-A-3 T 72 1.00 g 6.67 g7.72 g

460-13175-A-3~DU T 65 1.05 g 8.35 g9.61 g

460-13175-A-4 T 62 1.01 g 8.72 g9.92 g

460-13175-A-5 T 74 0.99 g 8.74 g9.91 g

460-13175-A-6 T 14 1.00 g 8.80 g9.62 g

460-13175-A-7 T 76 0.99 g 7.79 g8.78 g

460-13175-A-8 T 151 1.03 g 7.46 g8.19 g

460-13175-A-9 T 48 1.01 g 7.05 g7.57 g

460-13175-A-10 T 79 0.99 g 7.99 g9.51 g

460-13175-A-11 T 45 1.00 g 8.95 g9.87 g

460-13175-A-12 T 81 1.00 g 7.80 g8.61 g

06/03/2010 of 623


Method: Moisture



Batch End:

May 14 2010 9:47PM


460-13176-A-1 T 5 1.01 g 6.03 g6.69 g

460-13176-A-2 T 85 1.01 g 5.52 g6.34 g

460-13176-A-3 T 47 0.97 g 5.66 g6.73 g

460-13176-A-4 T 4 0.98 g 6.48 g7.21 g

460-13176-A-5 T 79 1.01 g 7.44 g8.21 g

460-13176-A-6 T 72 1.01 g 7.43 g8.18 g

460-13176-A-7 T 91 1.00 g 6.25 g7.06 g

460-13176-A-8 T 75 1.04 g 5.86 g6.81 g

460-13176-A-8~DU T 7 0.98 g 6.11 g6.96 g

460-13176-A-9 T 161 1.02 g 6.12 g6.87 g

460-13173-A-1 T 22 0.97 g 5.63 g6.54 g

460-13173-A-2 T 80 1.01 g 6.08 g7.36 g

460-13173-A-3 T 86 0.98 g 7.04 g8.51 g

460-13173-A-4 T 99 1.04 g 8.80 g9.36 g

460-13173-A-5 T 50 0.98 g 7.78 g8.27 g

460-13173-A-6 T 56 1.02 g 6.73 g7.47 g

460-13173-A-7 T 62 1.00 g 5.23 g6.20 g

460-13173-A-8 T 52 1.03 g 7.46 g8.65 g

460-13173-A-9 T 31 0.95 g 6.10 g6.84 g

460-13173-A-10 T 84 0.99 g 7.80 g9.30 g

460-13173-A-11 T 51 1.04 g 7.78 g9.35 g

460-13173-A-12 T 40 0.96 g 5.33 g6.34 g

460-13173-A-13 T 68 1.02 g 6.83 g7.99 g

460-13173-A-14 T 63 1.00 g 5.53 g6.23 g

460-13173-A-15 T 70 1.00 g 6.15 g7.04 g

06/03/2010 of 623


Method: Moisture



Batch End:

May 14 2010 9:47PM


460-13173-A-16 T 37 1.00 g 5.25 g6.10 g

460-13173-A-17 T 72 0.97 g 4.28 g4.88 g

460-13173-A-18 T 21 1.03 g 7.51 g8.65 g

460-13173-A-19 T 71 1.01 g 5.53 g6.51 g

460-13173-A-20 T 86 1.00 g 7.08 g8.31 g

460-13173-A-21 T 28 1.01 g 7.14 g8.27 g

460-13173-A-22 T 54 0.99 g 6.56 g7.58 g

460-13173-A-23 T 67 1.02 g 7.67 g9.31 g

460-13173-A-24 T 66 1.04 g 8.21 g9.79 g

460-13173-A-25 T 50 1.02 g 7.97 g9.51 g

460-13173-A-26 T 75 0.99 g 7.41 g8.96 g

460-13173-A-27 T 73 1.02 g 6.74 g7.97 g

460-13173-A-28 T 91 0.98 g 9.97 g9.98 g

460-13173-A-28~DU T 90 1.00 g 7.73 g7.74 g

460-13179-A-1 T 81 1.00 g 7.33 g8.40 g

460-13179-A-2 T 100 1.02 g 7.61 g8.29 g

460-13179-A-3 T 24 1.02 g 5.72 g6.25 g

460-13179-A-4 T 25 1.02 g 7.62 g8.05 g

460-13179-A-5 T 34 0.98 g 7.85 g9.12 g

460-13179-A-6 T 37 1.01 g 6.46 g6.75 g

460-13179-A-7 T 49 1.02 g 7.58 g8.32 g

460-13179-A-8 T 11 0.97 g 6.53 g7.04 g

460-13179-A-9 T 4 1.03 g 7.11 g7.45 g

460-13179-A-10 T 23 0.98 g 5.77 g6.12 g

460-13179-A-11 T 29 0.98 g 8.66 g9.20 g

06/03/2010 of 623


Method: Moisture



Batch End:

May 14 2010 9:47PM


460-13179-A-12 T 14 0.96 g 8.99 g9.66 g

460-13179-A-12~DU T 96 1.03 g 7.75 g8.35 g

460-13179-A-13 T 74 0.99 g 8.23 g8.96 g

460-13179-A-14 T 39 0.97 g 6.86 g7.81 g

460-13179-A-15 T 30 0.98 g 8.30 g8.83 g

460-13179-A-16 T 16 1.00 g 8.83 g9.56 g

460-13179-A-17 T 77 0.99 g 7.79 g8.26 g

460-13179-A-18 T 8 1.02 g 8.44 g9.08 g

460-13179-A-19 T 164 0.99 g 8.06 g8.34 g

460-13179-A-20 T 27 1.02 g 7.89 g8.30 g

460-13179-A-21 T 76 1.04 g 7.25 g7.68 g

460-13179-A-22 T 20 0.98 g 8.25 g8.73 g

460-13179-A-23 T 3 1.03 g 8.49 g9.12 g

460-13179-A-24 T 87 0.99 g 9.00 g9.85 g

460-13144-A-3 T 9 0.97 g 6.90 g7.39 g

460-13147-B-1 T 49 1.00 g 7.77 g8.92 g

460-13147-A-2 T 26 1.05 g 7.67 g8.66 g

460-13147-A-2~DU T 70 1.03 g 7.97 g8.89 g

460-13149-A-1 T 33 0.98 g 7.28 g8.81 g

460-13168-A-1 T 80 0.99 g 7.95 g8.93 g

460-13144-A-1 T 18 1.00 g 7.87 g8.35 g

460-13144-A-2 T 78 1.02 g 8.06 g8.79 g

460-13152-A-1 T 98 1.00 g 7.35 g8.88 g

460-13152-A-2 T 97 1.02 g 7.74 g9.58 g

460-13152-A-3 T 8 0.99 g 6.92 g8.16 g

06/03/2010 of 623


Method: Moisture



Batch End:

May 14 2010 9:47PM


460-12815-A-1 T 11 0.99 g 9.46 g9.75 g

460-13137-A-1 T 80 1.04 g 6.94 g7.12 g

460-13137-A-2 T 53 1.04 g 7.83 g8.08 g

460-13137-A-3 T 92 1.01 g 6.88 g7.00 g

460-13137-A-4 T 21 0.98 g 7.22 g7.36 g

460-13137-A-5 T 1 0.99 g 8.70 g9.25 g

460-13137-A-6 T 3 0.98 g 9.01 g9.13 g

460-13137-A-7 T 73 0.98 g 7.23 g7.44 g

460-13137-A-8 T 6 1.00 g 6.52 g6.74 g

460-13136-B-1 T 5 0.96 g 6.20 g6.53 g

460-13136-A-2 T 12 0.98 g 8.77 g9.55 g

460-13136-A-2~DU T 46 0.97 g 7.46 g8.09 g

460-13173-A-29 T 48 0.97 g 7.50 g8.95 g

460-13173-B-30 T 7 0.98 g 8.38 g9.90 g

460-13173-A-31 T 9 0.96 g 7.83 g8.84 g

460-13173-A-32 T 56 0.97 g 8.10 g9.52 g

460-13173-A-33 T 1 1.06 g 7.13 g8.47 g

460-13173-A-34 T 55 0.98 g 6.58 g7.20 g

460-13173-A-35 T 21 1.01 g 7.07 g8.45 g

460-13173-A-36 T 25 0.97 g 7.28 g8.43 g

460-13173-A-37 T 23 1.00 g 6.28 g7.41 g

460-13173-A-38 T 69 1.02 g 7.96 g8.76 g

460-13173-A-39 T 41 0.99 g 7.61 g8.78 g

460-13173-A-40 T 1 1.03 g 6.53 g7.83 g

460-13173-A-41 T 38 1.00 g 6.48 g7.14 g

06/03/2010 of 623


Method: Moisture



Batch End:

May 14 2010 9:47PM


460-13173-A-42 T 24 0.98 g 5.73 g7.01 g

460-13173-A-43 T 77 1.00 g 6.14 g7.05 g

460-13173-A-44 T 22 1.00 g 5.34 g6.11 g

460-13173-A-44~DU T 12 1.00 g 5.78 g6.63 g

460-13183-B-1 T 89 0.99 g 5.39 g7.27 g

460-13183-B-2 T 89 1.04 g 7.11 g8.61 g

460-13183-B-3 T 59 0.99 g 7.09 g8.05 g

460-13181-A-1 T 15 1.03 g 7.95 g9.89 g

460-13189-A-1 T 42 1.00 g 7.17 g8.25 g

460-13174-A-1 T 88 1.00 g 8.17 g9.27 g

460-13192-A-1 T 31 1.03 g 4.56 g6.08 g

460-13192-A-2 T 14 0.98 g 6.72 g7.26 g

460-13192-A-3 T 17 0.97 g 6.23 g7.03 g

460-13192-A-3~DU T 36 1.01 g 7.19 g8.17 g

Balance ID: 101 No Unit

Date samples were place in the oven: 5-14-10

Time samples were place in the oven: 22:30

Oven Temp when samples are put in oven: 104 104 Degrees C

Date samples were removed from oven: 5-15-10

Time Samples were removed from oven: 15:20

Oven Temp when samples removed from oven: 103 103 Degrees C

Oven ID: 1 2

ID number of the thermometer: 28212 29705

06/03/2010 of 623


Method: Moisture



Batch End:

May 17 2010 7:56PM

May 18 2010 9:38AM


PB~460-37639/1 45 0.96 g 0.96 g0.96 g

460-13139-E-7 TB-5 3-4 T 27 0.99 g 3.29 g6.97 gMoisture

460-13238-A-1 T 57 0.97 g 6.90 g7.97 g

460-13238-A-2 T 43 0.98 g 6.52 g7.51 g

460-13237-A-3 T 80 1.01 g 5.73 g6.70 g

460-13237-A-4 T 36 1.02 g 5.38 g6.20 g

460-13237-A-4~DU T 56 1.03 g 5.32 g6.15 gMoisture

Balance ID: 101 No Unit

Date samples were place in the oven: 5-17-10

Time samples were place in the oven: 20:30

Oven Temp when samples are put in oven: 103 Degrees C

Oven Temp when samples removed from oven: 103°C Degrees C

Oven ID: 1

ID number of the thermometer: 28212

06/03/2010 of 623

Shipping and

Receiving

Documents

06/03/2010 of 623

06/03/2010 of 623

Login Sample Receipt Check List


Login Number: 13139

Question T / F/ NA Comment

Creator: Hall, Alonzo

List Source: TestAmerica Edison

List Number: 1

Radioactivity either was not measured or, if measured, is at or below

background

N/A

The cooler's custody seal, if present, is intact. N/A

The cooler or samples do not appear to have been compromised or

tampered with.

True

Samples were received on ice. True

Cooler Temperature is acceptable. True

Cooler Temperature is recorded. True 3.3°C

COC is present. True

COC is filled out in ink and legible. True

COC is filled out with all pertinent information. True

There are no discrepancies between the sample IDs on the containers and

the COC.

True

Samples are received within Holding Time. True

Sample containers have legible labels. True

Containers are not broken or leaking. True

Sample collection date/times are provided. True

Appropriate sample containers are used. True

Sample bottles are completely filled. True

There is sufficient vol. for all requested analyses, incl. any requested

MS/MSDs

True

VOA sample vials do not have headspace or bubble is <6mm (1/4") in

diameter.

N/A

If necessary, staff have been informed of any short hold time or quick TAT

needs

True

Multiphasic samples are not present. True

Samples do not require splitting or compositing. True

Is the Field Sampler's name present on COC? True

Sample Preservation Verified True


OPRA - Twin Boro Field Phase 2 Lab Report

Documents

Transcript of OPRA - Twin Boro Field Phase 2 Lab Report