Post on 04-Apr-2020
EPA Contract No. 68-W6-0042EPA Work Assignment No. 032-TATA-0105
EPA Project Officer: Diana KingEPA Remedial Project Manager: Richard Goehlert
DATA EVALUATIONSUMMARY REPORT
FOR"PHASE II SEDIMENT SAMPLING
Ottati and Goss/Kingston Steel DrumSuperfund Site
Kingston, New Hampshire
Metcalf & Eddy
TABLE OF CONTENTS
1.0 INTRODUCTION
2.0 SUMMARY OF FIELD ACTIVITIES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 2.1 Sediment Sampling . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
3.0 ANALYTICAL DATA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
4.0 REFERENCES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
APPENDIX A - SEDIMENT SAMPLING WORKSHEETS
APPENDIX B - ANALYTICAL DATA TABLES
LIST OF FIGURES AND TABLES
Figure 1 Phase I and II Sediment Sample Locations at the Ottati & Goss Superfiind Site . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
Figure 2 Samples Collected at Depth (24-30") from the "Ballfield" . . . . . . . . . . . . . . 3
Table 1 Sample Analyses and Quantities Collected During Phase II Sediment Sampling . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Table 2 Summary of Total PCBs, Total Pesticides, and Combined Total for Arsenic, Chromium, Lead, and Nickel . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
1.0 INTRODUCTION
In accordance with the scope of work for the Ottati & Goss/Kingston Steel Drum Superfund Site, dated May 1998 (M&E, 1998a), Metcalf & Eddy (M&E) performed field work associated with Phase I and II Sediment Sampling in Country Pond Marsh. The sampling occurred in two separate phases in order to characterize the wetlands beyond the previous sampling efforts and assess the potential for redistribution of sediments contaminated with polychlorinated biphenyls (PCBs) after a 100-year flood event. The first phase of sediment sampling took place from October 12 through 16,1998, during which time M&E collected sediment samples from thirty-two locations within the existing sampling grid established by ADL as part of their sediment sampling program. The results of the Phase I sampling event are summarized in the Data Evaluation Summary Report for Phase I Sediment Sampling (M&E, 1998c). Based on the outcome of a meeting held on December 14,1998, which was attended by representatives from the U.S. Environmental Protection Agency, U.S. Army Corps of Engineers, New Hampshire Department of Environmental Services, U.S. Fish and Wildlife Services, and M&E, a second phase of sediment sampling was initiated to better define the limits of excavation based on a cleanup goal of 10 ppm total PCBs. The second phase of sediment sampling took place from December 17 through 28,1998. During Phase II, M&E collected sediment samples from ninety-eight locations within the existing sampling grid and "ballfield" area. The sampling grid was previously established by ADL and the "ballfield" is a diamond-shaped area which is located on the east side of the culvert situated under Route 125.
The field work was conducted in accordance with M&E's Sampling and Analysis Plan (SAP) for Technical Assistance (1998b). The SAP was developed to cover field activities, data collection, and analytical activities associated with sediment sampling in Country Pond Marsh. The Phase I and II sampling locations within the existing grid are shown in Figure FG-1. Phase II sediment sampling locations from the "ballfield" area are shown on Figure FG-2.
2.0 SUMMARY OF FIELD ACTIVITIES
Phase II of the sediment sampling was performed by M&E from December 17 through 28, 1998. Upon arrival at the site on December 17th, M&E field personnel mobilized into teams of two personnel and initiated sampling activities. As a result of brush cutting activities conducted during Phase I and seasonally minimal vegetation, access to previously established travel routes through the marsh to sampling locations was readily available. Sample collection was performed in the same manner as during Phase I, with the field teams following the sample collection and drying procedures outlined in the M&E SAP (1998b). A total of ninety-eight sediment locations were sampled during the second event. A summary of the sample analyses and quantities collected during Phase II is presented in Table 1. Copies of the sediment sampling worksheets are included in Appendix A.
PIEZOMETER LOCATIONS BY METCALF & EDDY
PHASE I SEDIMENT SAMPLE LOCATION
PHASE II PESTICIDE / PCB AND METALS SAMPLE LOCATION
PHASE H PCB SAMPLE LOCATION
USAGE SPLIT AND / OR TOC SAMPLE
SAMPLE COLLECTED AT SURFACE AND DEPTH
PCB CONCENTRATIONS (199;>—1996 SAMPLES ONLYV
Between 1 ppm and 10 ppm •
| | Between 10 ppm and 20 ppm
m Greater than 20 ppm \
PCB CONCENTRATIONS (1992, SAMPLE ANALYSIS ONLY}: \
|%%1 Between 1 ppm and 20 ppm
^m Greater than 20 ppm
OTTAH ft OOSS G. STANLEY SUPERfUNO SHE METCALF & EDDY MNGSTDN. NEWHAMPSHRE
nUENO. PHASE I & II NOT10SCMC 0*0 nu: PIEZOMETER & SEDIMENT
SAMPLE LOCATIONS 1C KDLOCK-HUNT
T
GROUNDWATER WELL
STAKED LOCATION
PHASE II PESTICIDE / PCB AND METALS SAMPLE LOCATION
OTTATl * GOSS
METCALF & EDDY SUPERFUND SITE KINGSTON. NEW HAMPSHIRE
CAOOfl£ CGOTC006.D*
FG-_2__
TABLE 1. SUMMARY OF SAMPLE ANALYSES AND QUANTmES COLLECTED DURING PHASE U SEDIMENT SAMPLING
DAS Analyses High Moisture Methods
Pesticides/PCBs Metals ENVIRONMENTAL SAMPLES: Sediment Sampling:
Phase II Marsh Locations 105 66
Field Collected QC Samples: Equipment Blanks 6 4 Field Duplicates 6 4 PE Samples 6 4 Matrix Spike 6 4 Matrix Spike Duplicate 6
| Subtotal: 135 82 | Number ofSDGs: 6 4
| GRAND TOTAL: 135 82
NOTES: DAS - Delivery of Analytical Services QC - Quality Control PCBs - Polychlorinated Biphenyls SDG - Sample Delivery Group PE - Performance Evaluation
2.1 Sediment Sampling
Upon arrival at the site each day that sediment sampling was conducted, field instruments were calibrated and sampling equipment decontaminated following the procedures outlined in the M&E SAP (1998b). Prior to initiation of sample collection at each sediment location, organic vapor readings were taken with a photoionization detector (PID). Sediment samples were collected using the procedure adapted from the Wells G&H project for collecting samples with a high percent moisture (M&E, 1997).
During Phase II, samples were collected from locations within the area of the existing sampling grid which had previously been identified as an area of contamination (ADL, 1997) (Figure FG-1). Sediment samples were collected using a bulb planter, post-hole digger, or shovel, from the top 6 to 12 inches of the marsh, below the vegetation. In addition, seven locations were selected within the existing grid for sampling at the 6-12 inch depth and the 24-30 inch depth, to determine the potential vertical extent of contamination. Five locations were also designated in the "ballfield" area for sampling at the 24-30 inch depth, only. These locations were selected based on locations, previously sampled by ADL, which had the highest reported concentrations of PCBs. Upon collection, all samples were homogenized and standing water was removed from the sample by decanting or the use of filter paper as specified in the M&E SAP (1998b).
At the request of EPA, all samples were submitted to the laboratory for the analysis of PCBs. In addition at the request of EPA, approximately 70% of the samples submitted for PCB analysis were also submitted for the analysis of pesticides and metals. However, upon receipt of the data, it was determined that all of the samples submitted for PCB analysis were also analyzed for pesticides. Pesticide data has been tabulated for all samples along with the results of the required analyses.
At all sampling locations, the pesticide/PCB samples were collected first, then the bottles for the metals analysis were filled. Sediment samples were collected for the DAS parameters outlined in Table 1. All samples were labeled prior to sample collection and immediately placed on ice after the bottles were filled. Each day, samples were packaged for shipment and the chain-of-custodies prepared. Upon completion of the field activities each day, samples were submitted to an EPA-approved DAS laboratory for analysis.
3.0 ANALYTICAL DATA
Based on the results of the Phase I data validation and at the direction of EPA, all pesticide/PCB and metals analytical data from the Phase II sediment sampling event were validated to Tier II in accordance with Region I EPA-New England Data Validation Functional Guidelines (US EPA, 1996). The analytical data tables are presented in Appendix B. Figure FG-1 depicts the Phase I and II sediment sample locations in the vicinity of the previously identified area of contamination (ADL, 1997). Table 2 presents a summary of the total detected PCB concentrations, total detected pesticide concentrations, and combined total detected concentrations for arsenic, chromium, lead, and nickel.
TABLE2 SUMMARY OF TOTAL PCBs, TOTAL PESTICIDES, AND COMBINED TOTAL FOR
ARSENIC, CHROMIUM, LEAD, AND NICKEL
SAMPLE LOCATION
A300 A'300 C300
C'300
D300 D'300 A350 A'350
B350 (6-12") B350 (24-30")
B'350 C350 C'350 D350
F'350 G350 G'350 B400 B'400 C400 C'400 D400
E'400
TOTAL PCBs (Mg/Kg) '
630
1,602/2,203* 1,097
300
556
41
227
151
547
535
13,780 64
1,502
812
51
252
215
20,120
8,360
544
3,330 579
3,884
TOTAL PESTICIDES G"g/Kg)
81
134/200* 92
104
123
8
32
18
73
81
1,235
4
160
101
5
150
19
876
793
42
319
58
274
TOTAL As, Cr, Pb, and
Ni (mg/Kg)
NA
193.6/191.0* NA
11.2
NA
28.4
62.5
NA
89.7
62.1
NA
31.1
NA
53.7
23.9
NA
46.4
NA
141.8
NA
76.9
NA
119.5
TABLE 2 (Continued).
SAMPLE LOCATION
F400
F'400
G400 (6-12")
G400 (24-30")
G'400
B'450
C450
C'450 (6-12")
C'450 (24-30")
D450
D'450
E450
F450
F'450
G450
G'450
C500
C'500
D500
D'500
E500
E'500
F500
TOTAL PCBs
TABLE 2 (Continued).
SAMPLE LOCATION
G500
C'550
D550
D'550
E550
E'550 (6-12")
E'550 (24-30")
F550
F'550
G550
C600
D600(6-12")
D600 (24-30")
D'600
E'600
F600
F'600
G600 (6-12")
G600 (24-30")
C'650
E650
E'650
F650
F'650
TOTAL PCBs G'g/Kg)
1,864/1,025*
488
500
2,155
2,063
968
496
565
372
487
1,880
2,700
199
3,460
344
520
476
140
540
241
412
140
301
370/350*
TOTAL PESTICIDES 0/g/Kg)
69/103*
65
47
225
915
119
63
117
108
121
1181
475
12
490
52
150
128
24
101
56
47
26
44
60/41*
TOTAL As, Cr, Pb, and Ni (mg/Kg)
NA
17.6
NA
100.8
NA
42.4
23.2
NA
NA
96.2
125.3
193.3
28.2
NA
NA
63.5
NA
27.0
42.9
29.0
NA
21.8
NA
36.5/37.2*
TABLE 2 (Continued).
SAMPLE LOCATION
B700
C700
D700
E700
E'700
F700
B750
B'750
C750
C'750 (6-12")
C'750 (24-30")
E750
E'750
F750
B'800
C800
C'800
D800
D'800
E800
E'800
F800
C850
C'850
TOTAL PCBs G"g/Kg)
760
219
1,120
980
287
100
1,480
243
660
530
142
236
121
404
122
100
1,190
3,960
360
330/410*
380
255
109
1,030/1,251*
TOTAL PESTICIDES G*g/Kg)
88
97
124
62
137
"19
259
22
237
54
139
32
88
200
18
29
51
560
234
82/221*
50
35
16
160/196*
TOTAL As, Cr, Pb, and Ni (nig/Kg)
41.7
28.3
107.8
36.6
NA
45.4
60.3
48.3
NA
32.2
36.9
NA
41.4
NA
26.7
43.5
47.8
NA
52.2
48.7/55.8*
NA
25.6
59.3
NA
TABLE 2 (Continued).
SAMPLE TOTAL PCBs TOTAL PESTICIDES TOTAL As, Cr, Pb, and LOCATION fag/Kg) G*g/Kg) Ni (mg/Kg)
D850 500 172 58.5
D'850 1,123 308 NA
E850 256 30 23.6
E'850 510 158 52.1
E'900 610 98 68.5
12N12E 2,910 214 44.2
12N22E 41,000 203 46.1
14N14E 26,400 4264 126.6
16N18E 3,300 790 64.4
20N20E 2,800 252 99.3
* - Data presented are the field sample and its associated duplicate result NA - Not Analyzed BOLD - Total PCB concentration exceeds site clean-up goal of 10 ppm
Based on a review of the data, several pesticides including 4,4'-DDD, 4,4'-DDE, 4,4-DDT, aldrin, alpha- and gawma-chlordane, dieldrin, endosulfan I, endrin, gamma-BHC, and heptachlor epoxide were detected in the sediment samples. A comparison with the data collected during Phase I shows that the frequency and concentrations of pesticides detected during Phase II increased over those detected during Phase I sediment sampling. The increase is attributed to sampling closer to the source area.
The total PCB concentrations calculated are presented on the analytical data tables (Appendix B) for comparison with the site clean-up goalof 10 parts per million (10,000 parts per billion) total PCBs. The total PCBs at each location are also presented on Table 2. The total PCB results detected during the Phase II sediment sampling were all less than 10 parts per million (ppm), with the exception of locations 12N22E and 14N14E, located within the "ballfield" area, and locations B'350 and B400, within the existing grid. In addition, at several locations, the reported concentrations of PCBs were greater than 1 ppm. A review of the results indicates that, with the exception of one pocket of contamination around the F'/G 450/500 grid area, the F grid line appears to be the eastern perimeter of the area of contamination which is reported as less than 1 ppm.
10
A review of the metals data indicates that arsenic, chromium, lead, and nickel were detected at all of the Phase II sediment sampling locations. Although these metals have been considered analytes of interest at the site, clean up goals for these metals have not been designated. Therefore, for correlation purposes with the PCBs and pesticides results, Table 2 has been prepared by M&E to present the tabulated results of the total PCBs, total pesticides, and combined totals for arsenic, chromium, lead, and nickel for each Phase II sediment sample location.
4.0 REFERENCES
Arthur D. Little (ADL). 1997. Final Report - Baseline Wetland Floristic Survey - Ottati & Goss/Great Lakes Container Corporation Site, Kingston, New Hampshire. December 1997.
Metcalf & Eddy (M&E). 1997. Draft Sampling and Analysis Plan for Wells G&H Superfund Site Aberjona River Study (Operable Unit 3). October 1997.
Metcalf & Eddy (M&E). 1998a. Draft Work Plan for Technical Assistance for Ottati and Goss/Kingston Steel Drum Superfund Site, Kingston, New Hampshire. July 1998.
Metcalf & Eddy (M&E). 1998b. Draft Sampling and Analysis Plan for Technical Assistance for Ottati and Goss/Kingston Steel Drum Superfund Site, Kingston, New Hampshire. August 1998.
Metcalf & Eddy (M&E). 1998c. Data Evaluation Summary Report for Phase I Sediment Sampling for Ottati and Goss/Kingston Steel Drum Superfund Site, Kingston, New Hampshire. December 1998.
U.S. Environmental Protection Agency (U.S. EPA). 1996. Region I, EPA-New England Data Validation Functional Guidelines for Evaluating Environmental Analyses. December 1996.
11
APPENDIX A
PHASE II SEDIMENT SAMPLING WORKSHEETS
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APPENDIX B
ANALYTICAL DATA TABLES
Ottati * Goss Site DATA SUMMARY TABLE Case 3M Sediment Pesticide / PCB Analysis SDGNo.: DAMF67
4,4'-DDD 0.33 0.33 UJ 0.33 UJ 10.4 J 0.33 UJ 11.3J 0.33 U 4,4'-DDE 0.33 0.33 UJ 1.56 J 19.1 J 0.33 UJ 11.1 J 3.0 J 4,4'-DDT 0.33 0.33 UJ 0.33 UJ 0.71 J 0.33 UJ 1.1 J 0.33 U Aldrin 0.17 0.17UJ 0.17UJ 1.97.J 0.17 UJ 2.12 J 0.16U alpha-BHC 0.17 0.17UJ 0.17UJ 0.27J 0.17 UJ 0.17 UJ 0.20 J alpha-Chlordane 0.17 1.19J 0.95 J 1.02J 0.17 UJ 0.96 J 0.39 J beta-BHC 0.17 0.17UJ 0.17 UJ 0.16 U 0.17 UJ 0.17 UJ 0.16U delta-BHC 0.17 0.17UJ 0.17 UJ 0.16 U 0.17 UJ 0.17 UJ 0.16U Dieldrin 0.33 66.7 J 8.14 J 113J 17.8 J 108 J 11.2J Endosulfan I 0.17 1.55 J 0.17UJ 0.41 J 0.47 J 1.34J 0.17U Endosulfan II 0.33 1.96J 0.33 UJ 0.32 U 0.33 UJ 0.33 UJ 0.33 U Endosulfan sulfate 0.33 0.33 UJ 0.33 UJ 0.32 U 0.33 UJ 0.49 J 0.33 U Endrin 0.33 18.5 J 3.79 J 19.9 5.24 J 18.7 J 1.87J Endrin aldehyde 0.33 4.26 J 0.33 UJ 0.32 U 2.53 J 0.33 UJ 0.33 U Endrin ketone 0.33 0.33 UJ 0.33 UJ 0.32 U 0.33 UJ 0.33 UJ 0.33 U gamma-BHC (Lindane) 0.17 0.21 J 0.33 J 0.49 J 0.17 UJ 0.36 J 0.17J gamma-Chlordane 0.17 2.15 J 0.90 J 3.43 J 3.79 J 2.55 J 0.85 J Heptachlor 0.17 0.21 J 0.17UJ 0.16 U 0.17 UJ 0.17 UJ 0.16U Heptachlor epoxide 0.17 0.97 J 0.17UJ 1.22 0.52 J 0.17 UJ 0.16U Methoxychlor 1.7 1.66 UJ 1.65UJ 1.62U 1.67 UJ 1.66UJ 1.64 U Toxaphene 17 4.14UJ 4.13UJ 4.05 U 4.18UJ 4.15 UJ 4.11U Aroclor-1016 3.3 3.3 U 3.3 U 3.2 UJ 3.3 U 3.3 U 3.3 U Aroclor-1221 6.6 6.6 U 6.6 U 6.4 UJ 6.6 U 6.6 U 6.6 U Aroclor-1232 3.3 3.3 U 3.3 U 3.2 UJ 3.3 U 3.3 U 3.3 U Aroclor-1242 3.3 3.3 U 3.3 U 3.2 UJ 3.3 U 3.3 U 3.3 U Aroclor-1248 3.3 180 J 41 J 160 J 76 J 140 J 42 J Aroclor-1254 3.3 3.3 U 3.3 U 3.2 UJ 3.3 U 3.3 U 3.3 U Aroclor-1260 3.3 430 J 68 J 340 J 180 J 370 J 80 J
Total PCBs: 610 109 500 256 510 122
Page 1 of4
Ottat' "• Goss Site Case 3M SDGNo.: DAMF67
4,4'-DDD 0.33 0.33 U 0.34 UJ 5.36 J 0.33 UJ 4.09 J 11.5J 4,4'-DDE 0.33 1.26J 5.28 J 11.5J 13.3 J 8.69 J 18.4J 4,4'-DDT 0.33 0.33 U 0.34 UJ 0.33 U 0.33 UJ 0.80 J 0.37 J Aldrin 0.17 0.16 U 0.17 UJ 0.17 U 1.15J 0.17 UJ 1.76 J a!pha-BHC 0.17 0.16 U 6.17 UJ 0.17 U 0.17UJ 6.17 UJ 0.16 U alpha-Chlordane 0.17 0.16U 0.89 J 0.17U 0.17 UJ 0.17 UJ 0.16 U beta-BHC 0.17 0.16U 0.17 UJ 0.17 U 0.17 UJ 0.17 UJ 0.16 U delta-BHC 0.17 0.16 U 0.17 UJ 0.17 U 0.17 UJ 0.17 UJ 0.16 U Dieldrin 0.33 19.7 J 0.34 UJ 198 J 49.1 J 11.2J 164J Endosulfan I 0.17 0.25 J 0.44 J 0.33 J 0.17 UJ 0.70 J 0.47 J Endosulfan II 0.33 0.33 U 0.34 UJ 0.33 U 0.33 UJ 0.33 UJ 0.33 U Endosulfan sulfate 0.33 0.33 U 0.34 UJ 0.33 U 0.33 UJ 0.33 UJ 0.48 J Endrin 0.33 4.35 32 J 11.7 15.7 J 6.4 J 17.2 Endrin aldehyde 0.33 0.33 U 5.12J 3.21 J 0.33 UJ 0.91 J 1.61 J Endrin ketone 0.33 0.33 U 0.34 UJ 0.33 U 0.33 UJ 0.33 UJ 0.33 U gamma-BHC (Lindane) gamma-Chlordane
0.17 0.17
0.16 U 3.15J
0.43 J 5.16 J
0.24 J 3.09 J
0.17UJ 2.42 J
0.17UJ 1.47 J
0.30 J 3.91 J
Heptachlor Heptachlor epoxide
0.17 0.17
0.16U 0.53 J
0.36 J 1.69J
0.17 U 0.82 J
0.17 UJ 0.76 J
0.17 UJ 0.59 J
0.16 U 1.16J
Methoxychlor 1.7 1.64 U 1.67 UJ 1.66U 1.67 UJ 1.66 UJ 1.64 U Toxaphene Aroclor-1016
17 3.3
4.11 U 3.3 UJ
4.18UJ 3.3 U
4.16U 3.3 UJ
4.17 UJ 3.3 U
4.14UJ 3.3 U
4.09 U 3.3 U
Aroclor-1221 6.6 6.6 UJ 6.6 U 6.6 UJ 6.6 U 6.6 U 6.6 U Aroclor-1232 3.3 3.3 UJ 3.3 U 3.3 UJ 3.3 U 3.3 U 3.3 U Aroclor-1242 3.3 3.3 UJ 3.3 U 3.3 UJ 3.3 U 3.3 U 3.3 U Aroclor-1248 3.3 28 J 410 J 120 J 110J 85 J 140 J Aroclor-1254 3.3 3.3 UJ 3.3 U 3.3 UJ 3.3 U 3.3 U 3.3 U Aroclor-1260 3.3 72 J 780 J 240 J 220 J 170 J 270 J
Total PCBs: 100 1190 360 330 255 410
Page 2 of4
Otta*' * Goss Site Casl MM SDGNo.: DAMF67
4,4'-DDD 0.33 34.3 J 2.51 J 3.92 J 2.35 J 2.7 J 21.9 J 4,4'-DDE 0.33 34.7 J 2.35 J 9.08 J 1.09 J 5.27 J 32.5 J 4,4'-DDT 0.33 4.35 J 0.33 U 0.34 U 0.33 UJ 0.33 UJ 0.34 U Aldrin 0.17 2.85 J 0.17 U 0.85 J 0.17UJ 0.44 J 0.17 U alpha-BHC 0.17 0.17 U 0.17 U 0.17 U 0.17 UJ 0.17 UJ 0.17U alpha-Chlordane 0.17 1.14J 0.28 J 0.17 U 0.19J 0.17 UJ 0.55 J beta-BHC 0.17 0.17 U 0.17 U 0.17 U 0.17 UJ 0.17 UJ 0.17 U delta-BHC 0.17 0.17 U 0.17 U 0.17 U 0.17 UJ 0.17 UJ 0.17U Dieldrin 0.33 129 J 2.36 J 27.8 J 132 J 73.2 J 35.2 Endosulfan I 0.17 0.68 J 0.33 J 0.21 J 0.17 UJ 0.17J 0.17U Endosulfan II 0.33 0.34 U 0.33 U 0.34 U 0.33 UJ 0.33 UJ 0.34 U Endosulfan sulfate 0.33 0.34 U 0.33 U 0.34 U 0.33 UJ 0.33 UJ 0.34 U Endrin 0.33 41 J 11.4J 8.92 2.27 J 3.03 J 27.9 Endrin aldehyde 0.33 0.34 U 0.33 U 0.34 U 0.33 UJ 1.30 J 0.34 U Endrin ketone 0.33 0.34 U 0.33 U 0.34 U 0.33 UJ 0.33 UJ 0.34 U gamma-BHC (Lindane) 0.17 0.26 J 0.17 U 0.17 U 0.17UJ 0.17UJ 0.17U gamma-Chlordane 0.17 8.08 J 1.86 J 2.20 J 0.62 J 1.82J 4.43 J Heptachlor 0.17 0.17 U 0.17 U 0.17 U 0.17UJ 0.17 UJ 0.17 U Heptachlor epoxide 0.17 2.27 0.57 0.73 J 0.20 J 0.17 UJ 1.75 Methoxychlor 1.7 1.67U 1.65U 1.68 U 1.66UJ 1.67UJ 1.68 U Toxaphene 17 4.19 U 4.14 U 4.19 U 4.15 UJ 4.17 UJ 4.2 U Aroclor-1016 3.3 3.3 U 3.3 U 3.4 U 3.3 UJ 3.3 UJ 3.4 UJ Aroclor-1221 6.6 6.7 U 6.6 U 6.7 U 6.7 UJ 6.7 UJ 6.7 UJ Aroclor-1232 3.3 3.3 U 3.3 U 3.4 U 3.3 UJ 3.3 UJ 3.4 UJ Aroclor-1242 3.3 3.3 U 3.3 U 3.4 U 3.3 UJ 3.3 UJ 3.4 UJ Aroclor-1248 3.3 480 J 73 J 190 J 58 J 41 J 380 J Aroclor-1254 3.3 3.3 U 3.3 U 3.4 U 3.3 UJ 3.3 UJ 3.4 UJ Aroclor-1260 3.3 1000 J 170 J 340 J 84 J 80 J 740 J
Total PCBs: 1480 243 530 142 121 1120
Page 3 of 4 •o
Ottati & Goss Site Case 0083M SDGNo.: DAMF67
4,4'-DDD 0.33 0.33 U 2.29 J 0.01 U 4,4'-DDE 0.33 36.50 J 4.70 J 0.01 U 4,4'-DDT 0.33 0.33 U 0.34 UJ 0.01 U Aldrin 0.17 0.17 U 0.17UJ 0.005 U alpha-BHC alpha-Chlordane beta-BHC
0.17 0.17 0.17
0.170.170.17
U U U
0.17UJ 0.17 UJ 0.17 UJ
0.005 U 0.005 U 0.005 U
delta-BHC 0.17 0.17 U 0.17 UJ 0.005 U Dieldrin 0.33 4.11 J 7.74 J 0.01 U Endosulfan I 0.17 0.42 J 0.17UJ 0.005 U Endosulfan II 0.33 0.33 U 0.34 UJ 0.01 U Endosulfan sulfate 0.33 0.33 U 0.34 UJ 0.01 U Endrin 0.33 13.7 J 2.92 J 0.01 U Endrin aldehyde Endrin ketone
0.33 0.33
0.330.33
U U
0.440.34
J UJ
0.010.01
U U
gamma-BHC (Lindane) gamma-Chlordane Heptachlor Heptachlor epoxide
0.17 0.17 0.17 0.17
0.17 U 5.25 J 0.17 U 1.63
0.17 UJ 0.63 J 0.17UJ 0.25 J
0.005 U 0.005 U 0.005 U 0.005 U
Methoxychlor 1.7 1.65 U 1.67UJ 0.05 U Toxaphene ArocIor-1016
17 3.3
4.14U 3.3 U
4.18 UJ 3.3 UJ
0.125 U 0.1 U
Aroclor-1221 6.6 6.6 U 6.7 UJ 0.2 U Aroclor-1232 3.3 3.3 U 3.3 UJ 0.1 U Aroclor-1242 3.3 3.3 U 3.3 UJ 0.1 U Aroclor-1248 3.3 300 J 28 J 0.1 U Aroclor-1254 3.3 3.3 U 3.3 UJ 0.1 U Aroclor-1260 3.3 680 J 72 J 0.1 U
Total PCBs: 980 100 ND
Page 4 of4 O
Ottatli/- Ooss Site DATA ST^-HVIARY TABLE Case (. M Sediment Pi ide / PCB Analysis SDGNo.: DAMF69 ________ug/Kg________
4,4'-DDD 0.33 29 J 33 J 76 J 2.1 30 J 3.3 J 4,4'-DDE 0.33 46 J 55 J 130 J 15 J 47 J 11 J 4,4'-DDT 0.33 1.0 U 0.33 U 1.0 U 0.33 UJ 0.33 UJ 0.33 UJ Aldrin 0.17 1.0 U 1.7 J 5.2 J R 1.3 J 0.17 UJ alpha-BHC 0.17 1.0 U 0.17 J 0.70 J 0.17 U 0.18 J 0.17 UJ alpha-Chlordane 0.17 6.0 J 19 J 43 J 2.5 J 9.8 J 4.2 J beta-BHC 0.17 0.50 U 0.17U 0.50 U 0.17 U 0.17UJ 0.17 UJ delta-BHC 0.17 1.0 0.37 J 3.3 J 0.45 J 0.17 UJ 0.17 UJ Dieldrin 0.33 66 J 190 J 270 J 27 J 120 J 4.9 J Endosulfan I 0.17 0.72 J 0.32 J 0.94 J 0.17 J 0.17 UJ 0.17 J Endosulfan II 0.33 5.3 J 3.9 13 J 0.33 U 3.0 J 1.9 J Endosulfan sulfatc 0.33 1.0 U 0.33 U 1.0 U 0.33 U 0.33 UJ 0.33 UJ Endrin 0.33 1.4 J 2.3 J 5.9 J 0.65 J 1.4 J 0.9 J Endrin aldehyde 0.33 2.7 J 0.64 J 9.0 J 1.5 J 2.6 J 0.7 J Endrin ketone 0.33 1.0 U 0.33 U 1.0 U 0.33 U 0.33 UJ 0.33 UJ gamma-BHC (Lindane) 0.17 0.50 U 0.17 U 0.50 U 0.17 J 0.17 UJ 0.17 UJ gamma-Chlordane 0.17 0.50 U 0.17 U 0.50 U 0.17 U 21 J 4.4 J Heptachlor Heptachlor epoxide
0.17 0.17
0.50 U 2.8
0.17U 1.4
0.50 U 3.3 J
0.17 UJ 0.58
0.17 UJ 0.89 J
0.17 UJ 0.73 J
Methoxychlor Toxaphcne Aroclor-1016
1.7 17
3.3
5.0 U 13 U
3.3 U
1.7 U 4.2 U 3.3 U
5.0 U 13 U
3.3 U
1.7 U 4.2 U 3.3 U
1.7UJ 4.2 UJ 3.3 U
1.7 UJ 4.2 UJ 3.3 UJ
ArocIor-1221 6.6 6.7 U 6.7 U 6.7 U 6.7 U 6.7 U 6.7 UJ ArocIor-1232 3.3 3.3 U 3.3 U 3.3 U 3.3 U 3.3 U 3.3 UJ Aroclor-1242 3.3 3.3 U 3.3 U 3.3 U 3.3 U 3.3 U 3.3 UJ Aroclor-1248 3.3 346 J 378 J 1I30J 144 J 202 J 81.2 J Aroclor-1254 3.3 3.3 U 3.3 U 3.3 U 3.3 U 3.3 U 3.3 UJ Aroclor-1260 3.3 684 J 745 J 2830 J 236 J 458 J 155 J
Total PCBs: 1030 1123 3960 380 660 236
Page 1 of4
Ottat' * Goss Site Case 3M SDGNo.: DAMF69
4,4'-DDD 4,4'-DDE 4,4'-DDT Aldrin alpha-BHC alpha-Chlordane beta-BHC delta-BHC Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone gamma-BHC (Lindane) gamma-Chlordane Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Aroclor-1016 Aroclor-1221 Aroclor-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260
Total PCBs:
0.33 0.33 0.33 0.17 0.17 0.17 0.17 0.17 0.33 0.17 0.33 0.33 0.33 0.33 0.33 0.17 0.17 0.17 0.17 1.7 17
3.3 6.6 3.3 3.3 3.3 3.3 3.3
6.5 J 22 J 1.0 U 1.7 J
0.50 U 2.8
0.50 U 0.50 U 160
0.50 U 2.5 1.0 U 2.0 J 1.3 J 1.0 U
0.50 U 0.50 U 0.50 U 0.91
5.0 U 13 U
3.3 U 6.7 U 3.3 U 3.3 U 134 J 3.3 U
270 J
404
8.5 J 10J
1.0 U 2.0 J
0.50 U 1.6 J
0.50 U 0.59 J 110
0.50 U 1.2 J 1.0 U 1.5 J I.I J I .OU
0.50 U 0.50 U 0.50 U 0.52 J 5.0 U 13 U
3.3 U 6.7 U 3.3 U 3.3 U 111 J 3.3 U 176 J
287
Page 2 of4
3.8 J 28 J
0.63 J 0.17 UJ 0.17 UJ 8.3 J
O.I7UJ 0.17 UJ
1.1 J 0.17 UJ
1.4 J 0.33 UJ 0.43 J 2.2 J
0.33 UJ 0.17 UJ
1.7UJ 0.17 UJ 0.73 J
1.7 U 4.2 U 3.3 U 6.7 U 3.3 U 3.3 U 159 J 3.3 U
253 J
412
3.4 J 16J
0.43 J 0.17 UJ 0.17UJ 2.2 J
0.17 UJ 0.17UJ
18 J 0.24 J 0.86 J 0.33 UJ 0.65 J
1.3 J 0.33 UJ 0.17 UJ 0.17 UJ 0.17 UJ 0.60 J
1.7 UJ 4.2 UJ 3.3 U 6.7 U 3.3 U 3.3 U 124 J 3.3 U 177 J
301
230 J 180 J I.OU
0.50 U 1.5 J 45 J
0.50 U 1.3 J 7.0 J 0.85 J 9.4 J 2.1 J 6.2 J 1.4 J I.OU
0.50 U 0.50 U 0.50 U 5.3 J 5.0 U 12 U 3.3 U 6.7 U 3.3 U 3.3 U
1380J 3.3 U
2080J
3460
16 J 24
0.33 UJ 0.17 UJ 0.21 J 1.9 J
0.17 UJ 0.30J 6.0 J 0.17J 1.1 J
0.33 UJ 0.76 J 1.3 J
0.33 UJ 0.17 UJ 0.17UJ 0.17 UJ 0.52J 1.7 UJ 4.2 UJ 3.3 U 6.7U 3.3 U 3.3 U 132 J 3.3 U 212 J
344
Ottat' "- Goss Site Case* 3M SDGNo.: DAMF69
4,4'-DDD 0.33 29 J 5.7 J 280 J 27 J 13 J 29 J 4,4'-DDE 0.33 40 J 22 J 210J 34 J 15J 46 J 4,4'-DDT 0.33 0.33 UJ 0.33 UJ 1.0 U 0.33 UJ 1.0 UJ 1.0 UJ Aldrin 0.17 0.17 UJ 0.17 UJ 21 J 0.76 J 1.7 J 0.50 UJ alpha-BHC 0.17 0.17 UJ 0.40 J 1.5 0.17 UJ 0.50 UJ 0.50 UJ alpha-Chlordane 0.17 10 J 8.8 38 7.8 J 2.6 J 6.3 J beta-BHC 0.17 0.17 UJ 0.17 UJ 0.50 U 0.17 UJ 0.50 UJ 0.50 UJ delta-BHC 0.17 0.37 J 0.17UJ I.I J 0.77 J 0.50 UJ 1.1 J Dieldrin 0.33 40 J 6.4 J 310J 42 J 62 J 100 J Endosulfan I 0.17 0.47 J 0.22 J 0.59 J 0.20 J 0.50 UJ 0.72 J Endosulfan II 0.33 2.3 J 1.7 J 8.1 1.9 J 2.0 J 5.5 J Endosulfan sulfate 0.33 0.33 UJ 0.33 UJ 1.0 U 0.33 UJ 1.0 UJ 1.0 UJ Endrin 0.33 0.51 J 0.33 UJ 39 J 0.39 J 8.3 J 1.2 J Endrin aldehyde 0.33 4.1 J 0.88 J 1.7 J 1.8 J 1.0 UJ 3.6 J Endrin ketone 0.33 0.33 UJ 0.33 UJ 1.0 U 0.33 UJ 1.0 UJ 1.0 UJ gamma-BHC (Lindane) 0.17 0.26 J 0.17 UJ 0.50 U 0.17 UJ 0.50 UJ 0.50 UJ gamma-Chlordane 0.17 0.17 UJ 0.17 UJ 0.50 U 0.17 UJ 2.7 J 0.50 UJ Heptachlor 0.17 0.17 UJ 0.17 UJ 0.50 U 0.17 U 0.50 UJ 0.50 UJ Heptachlor epoxide 0.17 1.0 J 1.1 J 3.6 0.70 J 0.89 J 2.7 J Methoxychlor 1.7 1.7UJ 1.7UJ 5.0 U 1.7UJ 5.0 UJ 5.0 UJ Toxaphene 17 4.2 UJ 4.2 UJ 13 U 4.2 UJ 12 UJ 12 UJ Aroclor-1016 3.3 3.3 U 3.3 U 3.3 U 3.3 U 3.3 UJ 3.3 U ArocIor-1221 6.6 6.7 U 6.7U 6.7 U 6.7 U 6.7 UJ 6.6 U Aroclor-1232 3.3 3.3 U 3.3 U 3.3 U 3.3 U 3.3 UJ 3.3 U Aroclor-1242 3.3 3.3 U 3.3 U 3.3 U 3.3 U 3.3 UJ 3.3 U Aroclor-1248 3.3 194 J 224 J 823 J 216 J 149 J 431 J Aroclor-1254 3.3 3.3 U 3.3 U 3.3 U 3.3 U 3.3 UJ 3.3 U Aroclor-1260 3.3 282 J 276 J 1240J 349 J 223 J 820 J
Total PCBs: 476 500 2063 565 372 1251
Page 3 of4
Ottati & Goss Site Case 0083M SDGNo.: DAMF69
4,4'-DDD 0.33 26 J 24 J 74 J 0.01 U 4,4'-DDE 0.33 24 J 39 J 35 J 0.01 U 4,4'-DDT 0.33 3.1 J 1.1 J 1.7 J 0.01 U Aldrin 0.17 0.17 U 0.64 J 0.17 U 0.005 U alpha-BHC 0.17 0.59 J 0.32 J 0.27 J 0.005 U alpha-Chlordane 0.17 7.1 J 13 J 0.92 J 0.005 U beta-BHC 0.17 0.17U 0.17 U 0.17U 0.005 U delta-BHC 0.17 0.17U 1.3 J 0.17U 0.005 U Dieldrin 0.33 15 J 4.8 J 4.3 J 0.01 U Endosulfan I 0.17 0.17U 0.47 J 0.17 U 0.005 U Endosulfan II 0.33 0.73 J 2.1 J 0.56 J 0.01 U Endosulfan sulfate 0.33 0.33 U 0.33 U 0.38 J 0.01 U Endrin 0.33 3.2 J 1.3 J 1.7 J 0.01 U Endrin aldehyde 0.33 1.1 J 2.6 J 1.6 J 0.01 U Endrin ketone 0.33 0.33 U 0.33 U 0.33 U 0.01 U gamma-BHC (Lindane) 0.17 0.17 U 0.17 U 0.17 U 0.005 U gamma-Chlordane 0.17 0.17 U 0.17 U 0.17 U 0.005 U Heptachlor 0.17 0.17U 0.17U 0.17U 0.005 U Heptachlor epoxide 0.17 0.26 J 1.6 J 0.45 J 0.005 U Methoxychlor 1.7 1.7 U 1.7 U 1.8 J 0.05 U Toxaphene 17 4.2 U 4.2 U 4.2 U 0.13 U Aroclor-1016 3.3 3.3 U 3.3 U 3.3 U 0.1 U Aroclor-1221 6.6 6.7 U 6.7 U 6.7 U 0.2 U Aroclor-1232 3.3 3.3 U 3.3 U 3.3 U 0. U Aroclor-1242 3.3 3.3 U 3.3 U 3.3 U 0. Aroclor-1248 3.3 477 J 659 J 380 J 0. Aroclor-1254 3.3 3.3 U 3.3 U 3.3 U 0. Aroclor-1260 3.3 153 J 438 J 176 J 0.
Total PCBs: 630 1097 556 ND
Page 4 of4
Ottatl °- Goss Site DATA SUMMARY TABLE Case JM merit Pesticide/PCB Analysis SDG No.: DAMF87
4,4'-DDD 0.33 17 J 5.3 J 3.8 J 4.4 J 0.33 UJ 4,4'-DDE 0.33 26 J 16 J 13 J 13 J 17 J 4,4'-DDT 0.33 3.3 J 1.2 J 0.33 UJ 0.33 UJ 1.1 J Aldrin 0.17 0.17 U 2.4 J 0.73 J R 0.16 UJ alpha-BHC alpha-Chlordanc beta-BHC
0.17 0.17 0.17
0.17 U 10 J
0.17 U
0.17 UJ 1.5 J
0.17 UJ
0.18 J 1.9 J
0.17UJ
0.17 UJ 0.79 J 0.17UJ
0.17 J 1.9 J
0.16 UJ delta-BHC 0.17 0.17 U 0.17UJ 0.85 J 0.17 UJ 0.16UJ Dieldrin 0.33 7.9 J 66 J 26 J 2.3 J 37 J Endosulfan I 0.17 0.3 J 0.17UJ 0.17 UJ 0.17 UJ 0.33 J Endosulfan II 0.33 4.1 1.2 J 1.4 J 0.64 J 1.1 J Endosulfan sulfate 0.33 0.33 U 0.33 UJ 0.33 UJ 0.33 UJ 0.33 UJ Endrin 0.33 17 J 0.87 J 5.6 J 3.2 J 0.38 J Endrin aldehyde Endrin ketone
0.33 0.33
1.2 J 0.33 U
2.3 J 0.33 UJ
2.2 J 0.33 UJ
1.4 J 0.33 UJ
0.67 J 0.33 UJ
gamma-BHC (Lindane) gamma-Chlordane
0.17 0.17
0.17U 0.17 U
0.17UJ 0.17 UJ
0.17 UJ 0.17 UJ
R 0.17UJ
0.16 UJ 0.16UJ
Heptachlor Heptachlor epoxide
0.17 0.17
0.17 U 1.5
0.17UJ 0.38 J
0.17UJ 0.39 J
R 0.34 UJ
0.16 UJ 0.53 UJ
Methoxychlor 1.7 1.7 U 1.7UJ 1.7UJ 1.7UJ 1.6UJ Toxaphene 4.2 4.2 U 4.2 UJ 4.2 UJ 4.2 UJ 4.1 UJ Aroclor-1016 3.3 3.3 UJ 3.3 UJ 3.3 U 3.3 U 3.3 UJ ArocIor-1221 6.6 6.7 UJ 6.7 UJ 6.7 U 6.7 U 6.7 UJ Aroclor-1232 3.3 3.3 UJ 3.3 UJ 3.3 U R 3.3 UJ Aroclor-1242 3.3 3.3 UJ 3.3 UJ 3.3 U 3.3 U 3.3 UJ Aroclor-1248 3.3 280 J 89 J 91 J 49 J 140 J Aroclor-1254 3.3 3.3 UJ 3.3 UJ 3.3 U 3.3 U 3.3 UJ Aroclor-1260 3.3 480 J 130 J 150 91 230 J
Total PCBs: 760 219 241 140 370
1.8 J 9.9 J
0.74 J 0.17 UJ 0.17 UJ
1.6 J 0.17UJ 0.17 UJ
21 J 0.27 J 0.87 J 0.33 UJ 4.1 J
0.52 J 0.33 UJ 0.17 UJ 0.17 UJ 0.17 UJ 0.45 J
1.7UJ 4.2 UJ 3.3 UJ 6.7 UJ 3.3 UJ 3.3 UJ 130 J 3.3 UJ 220 J
Page 1 of4 350
Ottatl " Goss Site Case' JM SDG No.: DAMF87
4,4'-DDD4,4'-DDE4,4'-DDTAldrinalpha-BHCalpha-Chlordanebeta-BHCdelta-BHCDieldrinEndosulfan IEndosulfan IIEndosulfan sulfateEndrinEndrin aldehydeEndrin ketonegamma-BHC (Lindane)gamma-ChlordaneHeptachlorHeptachlor epoxideMethoxychlorToxapheneAroclor-1016Aroclor-1221Aroclor-1232Aroclor-1242Aroclor-1248Aroclor-1254Aroclor-1260
Total PCBs:
0.33 0.33 0.33
0.17 0.17
0.17 0.17 0.17
0.33 0.17 0.33
0.33 0.33
0.33 0.33
0.17 0.17
0.17 0.17
1.7 4.2
3.3 6.6 3.3 3.3 3.3 3.3 3.3
150 J 230 J 0.4 J 5.4 J
0.17 U 94 J
0.17U 0.72 J 680 J
0.53 J 13
0.33 U 0.33 U
2 J 0.33 U 0.17U 0.17 U 0.17 U 4.5 1.7 U 4.2 U 3.3 UJ 6.7 UJ 3.3 UJ 3.3 UJ 780 J 3.3 UJ
1100J
1880
130 J 130 J
0.33 U 0.17 U 0.34 J
57 0.17 U
1.0 J 120 J
0.82 J 30
0.54 J 0.33 U 0.91 J 0.33 U 0.17 U 0.17U 0.17 U 4.1 1.7 U 4.2 U 3.3 UJ 6.7 UJ 3.3 UJ 3.3 UJ
1300J 3.3 UJ
1400J
2700 Page 2 of4
1.6 J 1.3 J
0.33 UJ 0.17 U 0.17U 0.67 J 0.17 U 0.17 U 3.1 J
0.17 U 0.57 J 0.33 UJ 3.0 J 1.3 J
0.33 UJ 0.17 U 0.17 U 0.17 U 0.44 1.7 UJ 4.2 UJ 3.3 UJ 6.7 UJ 3.3 UJ 3.3 UJ 89 J 3.3 UJ 110J
199
35 J 40 J
0.33 U 1.2 J
0.29 J 2.0 J
0.17U 0.48 J
65 J 0.21 J 2.2
0.33 U 1.3 J 1.8 J
0.33 U 0.17 U 0.17 U 0.17 U 0.89 J
1.7 U 4.2 U 3.3 UJ 6.7 UJ 3.3 UJ 3.3 UJ
200 J 3.3 UJ
320 J
520
5.1 J 9.6 J
0.56 J 0.17U 0.17 U 0.71 J 0.17 U 0.73 J 0.94 J 0.17 U 0.81 0.33 U
4.1 0.57 J 0.33 U 0.24 0.17 U 0.17 U 0.42
1.7 U 4.2 U 3.3 U 6.7 U 3.3 U 3.3 U 53 J
3.3 U 87
140
30 J 34 J
1 J 0.17 UJ 0.17 UJ
9J 0.17UJ 0.19J
17J 0.78 J
1.7 J 0.33 UJ 4.6 J 1.3 J
0.33 UJ 0.19 J 0.17 UJ 0.25 J 0.83 J
1.7UJ 4.2 UJ 3.3 U 6.7 U 3.3 U 3.3 U 190 J 3.3 U 350
540
Ottati/ ^o Case d A SDG No.: DAMF87
4,4'-DDD 0.33 12 J 660 J 120 J 61 J 27 J 37 J 4,4'-DDE 0.33 39 J 1500J 160 J 100 J 110J 27 J 4,4'-DDT 0.33 3.3 U 3.3 U 0.33 U 0.44 J 3.3 U 2J Aldrin 0.17 1.7 U 1.7 U 0.17 U 4.3 J 1.7 U 0.17U alpha-BHC 0.17 1.7 U 2.2 " 0.23 J 0.17 U 1.7 U 0.17 U alpha-Chlordane 0.17 18 780 J 65 J 8.6 J 1.7 U 1.6 J beta-BHC 0.17 1.7 U 1.7 U 0.17 U 0.17 U 1.7 U 0.17 U delta-BHC 0.17 1.7 U 1.7 U 0.95 J 1.2 J 1.7 U 0.17 U Dicldrin 0.33 120 J 410 390 J 33 J 36 J 13 J Endosulfan I 0.17 2 J 110J 1.2 J 0.61 J 4.5 J 0.72 J Endosulfan II 0.33 7.4 J 450 J 40 J 5.8 J 3.3 U 0.89 J Endosulfan sulfate 0.33 3.3 U 3.3 U 0.97 J 2.2 3.3 U 0.33 U Endrin 0.33 3.3 U 11 J 0.33 U 27 J 3.3 U 17 J Endrin aldehyde 0.33 9 31 4.7 1.4 J 11 1.6 J Endrin ketone 0.33 3.3 U 3.3 U 0.33 U 0.33 U 3.3 U 0.33 U gamma-BHC (Lindane) 0.17 1.7 U 1.7 U 0.17 U 0.17 U 1.7 U 0.17 U gamma-Chlordane 0.17 1.7 U 1.7 U 0.17 U 0.17 U 1.7 U 0.17 U Heptachlor 0.17 1.7 U 1.7 U 0.17U 0.17 U 1.7 U 0.17U Heptachlor cpoxide 0.17 6.1 J 310J 7.2 J 6 14 J 0.45 J Methoxychlor 1.7 17 U 17U 1.7 U 1.7 U 17U 2.6 J Toxaphene 4.2 42 U 42 U 4.2 U 4.2 U 42 U 4.2 U Aroclor-1016 3.3 3.3 U 3.3 U 3.3 U 3.3 UJ 3.3 U 3.3 U Aroclor-1221 6.6 6.7 U 6.7 U 6.7 U 6.7 UJ 6.7 U 6.6 U Aroclor-1232 3.3 3.3 U 3.3 U 3.3 U 3.3 UJ 3.3 U 3.3 U Aroclor-1242 3.3 3.3 U 3.3 U 3.3 U 3.3 UJ 3.3 U 3.3 U Aroclor-1248 3.3 2500 J 22000 J 2300 J 1400 J 29000 J 190 J Aroclor-1254 3.3 3.3 U 3.3 U 3.3 U 3.3 UJ 3.3 U 3.3 U Aroclor-1260 3.3 410 4400 J 1000J 1400 J 12000 J 110
Total PCBs: 2910 26400 3300 2800 41000 300 Page 3 of4
Ottati & Goss Site Case 0083M SDG No.: DAMF87
4,4'-DDD4,4'-DDE4,4'-DDTAldrinalpha-BHCalpha-Chlordanebeta-BHCdelta-BHCDieldrinEndosulfan IEndosulfan IIEndosulfan sulfateEndrinEndrin aldehydeEndrin ketonegamma-BHC (Lindane)gamma-ChlordaneHeptachlorHeptachlor epoxideMethoxychlorToxapheneAroclor-1016Aroclor-1221Aroclor-1232Aroclor-1242Aroclor-1248Aroclor-1254Aroclor-1260
Total PCBs:
0.33 0.33 0.33
0.17 0.17
0.17 0.17 0.17
0.33 0.17 0.33
0.33 0.33
0.33 0.33
0.17 0.17
0.17 0.17
1.7 4.2
3.3 6.6 3.3 3.3 3.3 3.3 3.3
Page 4 of4
3.6 J 1.2 J
0.58 J 0.17UJ 0.17 UJ 0.30 J 0.17 UJ 0.19 J 0.33 UJ 0.17J 0.33 UJ 0.33 UJ
I.I J 0.33 UJ 0.33 UJ 0.29 J 0.17 UJ 0.17 J 0.17UJ
1.7UJ 4.2 UJ 3.3 U 6.7 U 3.3 U 3.3 U 26 J
3.3 U 15
41
0.01 U 0.01 U 0.01 U
0.005 U 0.005 U
0.01 U 0.005 U 0.005 U
0.01 U 0.005 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U
0.005 U 0.005 U 0.005 U 0.005 U 0.05 U 0.13U 0.1 U 0.2 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U
ND
Ottatj •• Goss Site DATA STTMMARY TABLE Case JM Sediment k .cide/PCB Analysis SDG No.: DAMG16 tig/Kg
4,4'-DDD 0.33 6.8 J 52 J 14 J 24 J 9.1 J 23J 4,4'-DDE 0.33 13 J 68 J 28 J 22 J 21 J 32 J 4,4'-DDT 0.33 R R R R R 9.2 J Aldrin 0.17 R R R R R R a!pha-BHC 0.17 R R R R R R alpha-Chlordanebeta-BHC
0.17 0.17
5.4 J R
11 J R
9.3 J R
5.1 J R
4.2 J R
9.8 J R
delta-BHC 0.17 R R R R R R Dieldrin 0.33 22 J 27 J 32 J 38 J 19 J 26 J Endosulfan I 0.17 R 1.9 J R R R R Endosulfan II 0.33 3.6 J 9.5 J 6.4 J 4.5 J 4.0 J R Endosulfan sulfate 0.33 R 3.7 J R R R 3.6 J Endrin 0.33 12 J 46 J 21 J 22 J R 22 J Endrin aldehydeEndrin ketone
0.33 0.33
3.5 J R
R R
7.2 J R
3.4 J R
4.0 J R
6.0 J R
gamma-BHC (Lindane)gamma-Chlordane
0.17 0.17
R R
R R
R R
R R
R R
R R
Heptachlor 0.17 R R R R R R Heptachlor epoxideMethoxychlorToxapheneAroclor-1016
0.17 1.7
4.2 3.3
R R R R
5.5 J R R R
2.3 J R R R
2.2 J R R R
1.7 J R R R
2.3 J R R R
Aroclor-1221 6.6 R R R R R R ArocIor-1232 3.3 R R R R R R Aroclor-1242 3.3 R R R R R R Aroclor-1248 3.3 230 J 875 J 427 J 159 J 224 J 1070 J Aroclor-1254 3.3 R R R R R R Aroclor-1260 3.3 258 J 1280 J 541 J 328 J 272] 532 J
Total PCBs: 488 2155 968 487 496 1602
Page 1 of4
Ottat« •• Goss Site Cast/ 3M SDG No.: DAMG16
4,4'-DDD 4,4'-DDE 4,4'-DDT Aldrin alpha-BHC alpha-Chlordanc bcta-BHC delta-BHC Dicldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone gamma-BHC (Lindane) gamma-Chlordane Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Aroclor-1016 Aroclor-1221 Aroclor-1232 Aroclor-1242 Aroclor-1248 ArocIor-1254 Aroclor-1260
Total PCBs:
0.33 0.33 0.33 0.17 0.17 0.17 0.17 0.17 0.33 0.17 0.33 0.33 0.33 0.33 0.33 0.17 0.17 0.17 0.17 1.7 4.2 3.3 6.6 3.3 3.3 3.3 3.3 3.3
16 J 41 J 3.4 J
R R
13 J R R
34 J 26 J 7.3 J 6.4 J 40 J
9.3 J R R R R
4.0 J R R R R R R
1440 J R
763 J
2203
84 J 130 J
R 11 J
R 46 J
R R
120 J 3.0 J 23 J
R 130 J 5.4 J
R R R R
11 J R R R R R R
2230 J R
2740 J
4970
100 J 110J
R R R
10J R R
29 J 1.9 J 10J 15 J 53 J
R R R R R
5.8 J R R R R R R
1510J R
1920 J
3430
18 J 90 J
R 12 J
R 19 J
R R
200 J 2.2 J 18J
R 70 J 7.8 J
R R R R
7.4 J R R R R R R
1350J R
1660 J
3010
R 8.7 J
R R R
4.2 J R R
9.5 J R R R
10J 4.7 J
R R R R R R R R R R R
127 J R
194 J
321
59 J 160 J
R R R
85 J R R
200 J 5.0 J 40 J
R 210 J
14 J R R R R
20 J R R R R R R
5240 J R
3120J
Page 2 of4
8360
OttatJ * Goss Site Case 3M SDG No.: DAMG16
4,4'-DDD 0.33 18 J 43 J 4.9 J R R 8.3 J 4,4'-DDE 0.33 78 J 49 J 12 J 8.4 J 7.0 J 3.8 J 4,4'-DDT 0.33 R R R R R R Aldrin 0.17 R R R R R R a!pha-BHC 0.17 R R R R R R alpha-Chlordane 0.17 24 J 13 J 4.2 J 4.2 J 2.2 J 4.6 J bcta-BHC 0.17 R R R R R R delta-BHC 0.17 R R R R R R Dieldrin 0.33 48 J 24 J 8.1 J R 5.1 J 9.6 J Endosulfan I 0.17 2.1 J R R R R R Endosulfan II 0.33 22 J 25 J 4.2 J R R 5.0 J Endosulfan sulfate 0.33 R R R R R 7.0 J Endrin 0.33 110J 110J 17J 8.5 J 7.0 J 19 J Endrin aldehyde 0.33 7.8 J 4.1 J 3.4 J R R R Endrin ketone 0.33 R R R R R R gamma-BHC (Lindane) 0.17 R R R R R R gamma-Chlordane 0.17 R R R R R R Heptachlor 0.17 R R R R R R Heptachlor cpoxide 0.17 9.5 J 6.5 J R R R R Methoxychlor 1.7 R R R R R R Toxaphene 4.2 R R R R R R Aroclor-1016 3.3 R R R R R R Aroclor-1221 6.6 R R R R R R Aroclor-1232 3.3 R R R R R R Aroclor-1242 3.3 R R R R R R Aroclor-1248 3.3 1740 J 794 J 222 J 70 J 68 J 183 J Aroclor-1254 3.3 R R R R R R Aroclor-1260 3.3 1590J 3090 J 396 J 142 J 124 J 298 J
Total PCBs: 3330 3884 618 212 192 481
Page 3 of4
Ottati & Goss Site Case 0083M SDG No.: DAMG16
4,4'-DDD 4,4'-DDE 4,4'-DDT Aldrin alpha-BHC alpha-Chlordane beta-BHC delta-BHC Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone gamma-BHC (Lindane) gamma-Chlordane Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Aroclor-1016 Aroclor-1221 Aroclor-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260
0.33 0.33 0.33 0.17 0.17 0.17 0.17 0.17 0.33 0.17 0.33 0.33 0.33 0.33 0.33 0.17 0.17 0.17 0.17 1.7 4.2 3.3 6.6 3.3 . 3.3 3.3 3.3 3.3
0.01 UJ 0.01 UJ 0.01 UJ
0.005 UJ 0.005 UJ 0.005 UJ 0.005 UJ 0.005 UJ 0.01 UJ
0.005 UJ 0.01 UJ 0.01 UJ 0.01 UJ 0.01 UJ 0.01 UJ
0.005 UJ 0.005 UJ 0.005 UJ 0.005 UJ
0.05 UJ 0.125UJ
0.1 U 0.2 U 0. 0. 0. 0. 0.
Total PCBs: ND
Page 4 of4
Ottati *- Goss Site DATA SUMMARY TABLE Case ( M Sediment F :ide/PCB Analysis SDG No.: DAMG27
4,4'-DDD 0.33 38 J 100 J R 33 J 4.7 J 8.5 J 4,4'-DDE 0.33 111 170 J 20.0 J 43 J 27 J 42 J 4,4'-DDT 0.33 R R R R R R Aldrin 0.17 8.1 J R R R R R alpha-BHC 0.17 R R R R R R alpha-Chlordane 0.17 22 J 42 J 6.3 J 6.9 J 3.6 J 5.5 J beta-BHC 0.17 R R R R R R delta-BHC 0.17 R R R R R R Dieldrin 0.33 160 J 360 J 7.3 J 23 J 5.0 J 7.6 J EndosulfanI 0.17 R 2.7 J R R R R Endosulfan II 0.33 12J 24 J 4.9 J 8.7 J 4.4 J 6.7 J Endosulfan sulfate 0.33 R 100 J R R R R Endrin 0.33 5.8 J 33 J 18 J 32 J 20 J 29 J Endrin aldehyde 0.33 R R 4.9 J R R R Endrin ketone 0.33 R R R R R R gamma-BHC (Lindane) 0.17 R R R R R R gamma-Chlordane 0.17 R R R R 1.7 R R Heptachlor 0.17 R R R R R R Heptachlor epoxide 0.17 6.9 J 13 J 2.0 J 2.0 J 2.4 J 3.6 J Methoxychlor 1.7 R R R R R R Toxaphene 4.2 R R R R R R Aroclor-1016 3.3 R R R R R R Aroclor-1221 6.6 R R R R R R Aroclor-1232 3.3 R R R R R R Aroclor-1242 3.3 R R R R R R Aroclor-1248 3.3 2220 J 4670 J 320 J 422 J 724 J 377 J Aroclor-1254 3.3 R R R R R R Aroclor-1260 3.3 1410 J 3260 J 408 J 741 J 1140J 648 J
Total PCBs: 3630 7930 728 1163 1864 1025
Page 1 of4
Otta" 4 Goss Site Cas 33M SDG No.: DAMG27
4,4'-DDD 4,4'-DDE 4,4'-DDT Aldrin alpha-BHC alpha-Chlordane beta-BHC delta-BHC Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone gamma-BHC (Lindane) gamma-Chlordane Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Aroclor-1016 Arocior-1221 Aroclor-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260
Total PCBs:
0.33 0.33 0.33 0.17 0.17 0.17 0.17 0.17 0.33 0.17 0.33 0.33 0.33 0.33 0.33 0.17 0.17 0.17 0.17 1.7 4.2 3.3 6.6 3.3 3.3 3.3 3.3 3.3
160 J 320 J
R R R
130 J R R
150 J 4.6 J 52 J
R R
11 J R R R R
48 J R R R R R R
13000 J R
7120 J
20120
R 11 J
R R R
5.8 J R R
5.6 J R
4.5 J R
13 J R R R R R
1.8 J R R R R R R
319 J R
225 J
544
R 13 J
R R R
6.5 J R R
9.4 J R
4.3 J R
16J 7.1 J
R R R R
1.8 J R R R
6.7 R R R
275 J R
304 J
579
R 5.9 J
R R R
4.1 J R R R R R R
7.2 J R R R R R R R R R R R R
137 J R
151 J
288
R 17 J
R R R
8.3 J R R
11 J R
6.1 J R
21 J 3.4 J
R R R R
1.8 J R R R R R R
214 J R
349 J
563
R R R R R R R R R R R R
4.3 J R R R R R R R R R R R R
65.2 J R
75.1 J
140
Page 2 of4
Otta*' "' Goss Site Cast ,3M SDG No.: DAMG27
4,4'-DDD 4,4'-DDE 4,4'-DDT Aldrin alpha-BHC alpha-Chlordane bcta-BHC delta-BHC Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone gamma-BHC (Lindane) gamma-Chlordane Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Aroclor-1016 Aroclor-1221 Aroclor-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260
Total PCBs:
0.33 0.33 0.33 0.17 0.17 0.17 0.17 0.17 0.33 0.17 0.33 0.33 0.33 0.33 0.33 0.17 0.17 0.17 0.17 1.7 4.2 3.3 6.6 3.3 3.3 3.3 3.3 3.3
13 J 38 J
R R R
18 J R R
10 J R
9.4 J R
37 J R R R R R
6.3 J R R R R R R
1780J R
692 J
2472
32 J 81 J
R R R
27 J R R
24 J 1.9 J 19 J
R 95 J
R R R R R
9.6 J R R R R R R
2680 J R
1900J
4580
15 J 39 J
R R R
16J R R
19 J R
12 J R
45 J 3.5 J
R R R R
6.0 J R R R R R R
651 J R
784 J
1435
14 J 25 J
R R R
7.4 J R R
11 J R
3.3 UJ R R R R R R R
3.1 J R R R R R R
537 J R
640 J
1177
37 J 54 J
R R R
23 J R R
27 J R
14 J R R
4.0 J R R R R
7.4 J R R R R R R
1500J R
1450 J
2950
R 4.1 J 4.1 J
R R
2.4 J R R R R R R
5.2 J R R R R R
1.7UJ R R R R R R
81.5 J R
69.8 J
Page 3 of4
151
Ottati & Goss Site Case 0083M SDG No.: DAMG27
4,4'-DDD 4,4'-DDE 4,4'-DDT Aldrin alpha-BHC alpha-Chlordane beta-BHC delta-BHC Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone gamma-BHC (Lindane) gamma-Chlordane Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Aroclor-1016 Aroclor-1221 Aroclor-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260
Total PCBs:
0.33 0.33 0.33 0.17 0.17 0.17 0.17 0.17 0.33 0.17 0.33 0.33 0.33 0.33 0.33 0.17 0.17 0.17 0.17 1.7 4.2 3.3 6.6 3.3 3.3 3.3 3.3 3.3
120 J 260 J 3.3 UJ 1.7UJ 1.7UJ
150 J 1.7UJ 1.7UJ
180 J 4.9 J 42 J 3.3 UJ
360 J 14 J
3.3 UJ 1.7UJ 1.7UJ 1.7UJ 23 J 17 UJ 42 UJ 3.3 UJ 6.7 UJ 3.3 UJ 3.3 UJ
6160 J 3.3 UJ
7620 J
13780
15 J 18 J
3.3 UJ 1.7 UJ 1.7UJ 10 J
1.7UJ I.7UJ 16 J
1.7UJ 4.6 J 3.3 UJ 3.3 UJ 6.9 J 3.3 UJ 1.7 UJ 1.7UJ 1.7UJ 3.2 J 17 UJ 42 UJ 3.3 UJ 6.7 UJ 3.3 UJ 3.3 UJ
1050J 3.3 UJ
452 J
1502
26 J 14 J
3.3 UJ 1.7 UJ 1.7UJ 2.3 J 1.7UJ 1.7UJ 7.2 J 1.7UJ 3.3 UJ 3.3 UJ 9.7 J 3.3 UJ 3.3 UJ 1.7 UJ 1.7UJ 1.7UJ 1.7UJ 17 UJ 42 UJ 3.3 UJ 6.7 UJ 3.3 UJ 3.3 UJ
98.8 J 3.3 UJ 153 J
252
0.01 U 0.01 U 0.01 U
0.005 U 0.005 U 0.005 U 0.005 U 0.005 U
0.01 U 0.005 U
0.01 U 0.01 U 0.01 U 0.01 U 0.01 U
0.005 U 0.005 U 0.005 U 0.005 U
0.05 U 0.13 U
0.1 U 0.2 U 0. 0. 0. 0. 0.
ND
Page 4 of4
Ottati ' "ossSite ~ \TA SUMMARY TABLE Case 01 M S* lent Pesticide/PCB Analysis SDG No.: DAMG28 ug/Kg
1 4,4'-DDD 4,4'-DDE 4,4'-DDT Aldrin alpha-BHC alpha-Chlordanc beta-BHC delta-BHC Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone gamma-BHC (Lindane) gamma-Chlordane Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Aroclor-1016 Aroclor-1221 Aroclor-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260
Total PCBs:
0.33 0.33 0.33 0.17 0.17 0.17 0.17 0.17 0.33 0.17 0.33 0.33 0.33 0.33 0.33 0.17 0.17 0.17 0.17 1.7 4.2 3.3 6.6 3.3 3.3 3.3 3.3 3.3
37 J 87 J
R R R
47 J R R
33 J 2.3 J 26 J
R 120 J 14 J
R R R R
13 J R R R R R R
3280 J R
2980 J
6260
42 J 78 J
R R R
42 J R R
37 J 2.5 J 25 J
R 9.8 J 19 J
R R R R
12 J R R R R R R
1420 J R
1120J
2540
30 J 85 J
R R R
43 J R R
22 J 2.5 J 23 J
R 85 J
R R R R R
12 J R R R R R R
1070J R
664 J
1734
54 J 110J
R R R
51 J R R
78 J 2.2 J 32 J
R 120 J 6.3 J
R R R R
11 J R R R R R R
3840 J R
5550 J
9390
25 J 71 J
R R R
36 J R R
19 J 2.1 J 19 J
R 87 J
R R R R R
10 J R R R R R R
1070 J R
620 J
1690
R 6.7 J
R R R
4.5 J R R
8.0 J R
3.6 J R
8.7 J R R R R R R R R R R R R
114J R
113J
Page 1 of3
227
Ott, "c Goss Site Cast ->/83M SDG No.: DAMG28
4,4'-DDD 4,4'-DDE 4,4'-DDT Aldrin alpha-BHC alpha-Chlordane bcta-BHC delta-BHC Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone gamma-BHC (Lindane) gamma-Chlordane Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Aroclor-1016 Aroclor-1221 Aroclor-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260
Total PCBs:
0.33 0.33 0.33 0.17 0.17 0.17 0.17 0.17 0.33 0.17 0.33 0.33 0.33 0.33 0.33 0.17 0.17 0.17 0.17 1.7 4.2 3.3 6.6 3.3 3.3 3.3 3.3 3.3
6.2 J 23 J 3.7 J
R R
5.3 J R R
8.5 J R
4.7 J R
22 J R R R R R R R R R R R R
236 J R
311 J
547
4.6 J 23 J
R R R
10 J R R
7.6 J R
5.6 J R
23 J 4.8 J
R R R R
2.6 J R R R R R R
196 J R
339 J
535
R 12 J R R R 23 J R 6.8 J R R R R R R R R R R R R R 9.9 J R 2.6 J R R R R R R R R R 16 J 4.7 J R R R R R R 5.1 J R R R R R R R 28 J R 9.8 J R 4.0 J R R R R R R R R R R
4.2 J R R R R R R R R 3.4 J R R R R R R R R R R R R R R R R R R R R R R R R R R
33.8 J 426 J 22.7 J 94.3 J R R R R
30.4 J 386 J 28.6 J 121 J
64 812 51 215
Page 2 of 3
Ottati & Goss Site Case 0083M SDG No.: DAMG28
4,4'-DDD 4,4'-DDE 4,4'-DDT Aldrin alpha-BHC alpha-Chlordane beta-BHC delta-BHC Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone gamma-BHC (Lindane) gamma-Chlordane Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Aroclor-1016 Aroclor-1221 Aroclor-1232 ArocIor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260
Total PCBs:
0.33 0.33 0.33 0.17 0.17 0.17 0.17 0.17 0.33 0.17 0.33 0.33 0.33 0.33 0.33 0.17 0.17 0.17 0.17 1.7 4.2 3.3 6.6 3.3 3.3 3.3 3.3 3.3
0.01 UJ 0.01 UJ 0.01 UJ
0.005 UJ 0.005 UJ 0.005 UJ 0.005 UJ 0.005 UJ 0.01 UJ
0.005 UJ 0.01 UJ 0.01 UJ 0.01 UJ 0.01 UJ 0.01 UJ
0.005 UJ 0.005 UJ 0.005 UJ 0.005 UJ 0.05 UJ 0.13 UJ 0.1 UJ 0.2 UJ 0.1 UJ 0.1 UJ 0.1 UJ 0.1 UJ 0.1 UJ
ND
Page 3 of3
SITE: Ottati & Goss DATA SUMMARY TABLE CASE NO.: 0083M DAS METALS SDG NO.: DAMF67
Metals (mg/kg) Aluminum 200 2440 2380 Antimony Arsenic
60 10
0.29 3.1 J
0.25 U 3.5 J
Barium 200 78.2 61.8 Beryllium Cadmium
5.0 5.0
0.63 0.98 J
0.52 0.88 J
Calcium 5000 14400 10500 Chromium 10 5.6 J 6.4 J Cobalt 50 3.0 2.8 Copper Iron
25 100
9.3 3440
10.8 3430
Lead 3.0 55.7 45.4 Magnesium Manganese Mercury Nickel
5000 15
0.20 40
1560 407
0.07 J 4.1
996 357
0.02 J 4.0
Potassium 5000 149 J 109J Selenium 5.0 2.7 2.5 Silver 10 0.19 UJ 0.17 UJ Sodium 5000 574 504 Thallium 10 0.38 U 0.34 U Vanadium 50 7.4 J 6.0 J Zinc 20 32.9 35.8
2710 2350 2470 4080 3150 4350 0.30 0.25 U 0.42 0.33 J 0.47 0.27 U
2.9 J 1.2 J 2.7 J 3.2 J 4.4 J 1.9 J 74.9 60.4 67.5 57.6 64.7 47.9 0.54 0.52 0.36 1.0 0.70 0.58
1.9 J 0.53 J 1.7 J 1.9 J 1.0 J 1.7 J 12900 11300 11600 12500 11400 6940
5.9 J 3.4 J 4.9 J 5.5 J 5.5 J 10.7 J 2.2 1.1 2.0 2.4 3.3 1.4 9.6 10.3 8.6 8.6 9.9 9.7
2990 2030 2760 3150 3510 2040 45.5 15.8 40.9 12.1 29.1 31.5 1330 1120 1200 1100 984 576
171 70.7 160 229 567 167 0.05 J 0.03 J 0.02 J 0.03 J 0.02 J 0.08 J 4.2 3.2 3.6 5.9 4.5 3.7 135 J 98.9 J 124 J 134 J 99.8 J 154 J 2.6 3.4 2.4 5.5 3.6 33
0.03 J 0.02 UJ 0.02 UJ 0.1U 0.17 UJ 0.02 UJ 523 425 474 1080 786 299
0.36 U 0.34 U 0.37 U 0.36 U 0.35 U 036 U 62 J 3.7 J 5.8 J 6.8 J 6.3 J 5.8 J
35.1 11.5 31.5 10.1 24.1 20.0
Page 1 of3
or
SITE: Ottati & Goss CASE NO.: 0083M SDG NO.: DAMF67
Metals (mg/kg) Aluminum Antimony Arsenic Banum Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
200 60 10
200 5.0 5.0
5000 10 50 25 100 3.0
5000 15
0.20 40
5000 5.0 10
5000 10 50 20
3520 0.39 2.7 J
69.0 0.68
1.6 J 10600
7.1 J 2.5
15.0 3190 37.9 1290 247
0.05 J 4.5 105 J 3.7
0.02 UJ 430 0.38 U
6.5 J 34.2
3510 0.42 32}
71.5 0.55 UJ
11400 5.3 J 2.6
13.2 3160 35.5 1070 250 0.02 J 4.7
99.1J 3.3
0.02 UJ 385
0.36 U 7.2 J
34.8
2550 0.28 U
1.2 J 75.9 0.48 0.92 J
12900 3.3 J 1.3 9.8
2530 17.9
1360 108
0.05 J 3.2
98.8 J 3.0
0.02 UJ 409
0.37 U 4.3 J
15.0
3480 0.47
3.4 J 70.9 0.68
1.7 J 11200
6.5 J 2.7
13.6 3230 40.8 1050 261 0.06 J
5.1 101 J 3.2
0.02 UJ 386
0.36 U 7.4 J
41.4
4560 0.37 UJ
4.1 J 67.4 0.56 2.0 J
12300 10.4 J 2.8
11.7 3020 40.2 1120 214 0.01 UJ 5.6 146 J 2.7
0.02 UJ 738
0.49 U 8.3 J
35.1
5080 0.28 U
4.2 J 52.0 0.80 0.70 J
17000 10.7 J 3.4 8.7
1010 26.8 1200 169
0.01 UJ 6.6
240 J 7.1
0.04 J 2080 0.37 U
8.3 J 21.0
4490 0.35 J
2.2 J 65.3 0.88
1.7 J 9960
6.1 J 1.9
12.4 3060 19.7 1040 131
0.07 J 4.2 108 J 3.6
0.11 J 479 0.34 U 5.9 J
21.7
4120 035 J 4JJ
82.8 0.91 2.0 J
11300 5.9 J 2.6
12.5 3380 20.2 958 206 0.01 UJ 6.5
94.5 J 3.4
0.07 J 406
0.37 UJ 6.8 J
27.1
Page 2 of3
SITE: Ottati & Goss CASE NO.: 0083M SDG NO.: DAMF67
Metals (mg/kg) Aluminum 200 3140 3470 3320 3130 40.0 U Antimony 60 0.64 0.83 J 0.31 J 0.27 3.0 U Arsenic 10 3.5 J 4.6; 4.9 J 4.1 J 2.0 U Barium 200 75.9 67.2 71.8 70.9 5.0 U Beryllium 5.0 0.73 0.34 0.78 0.67 0.40 U Cadmium 5.0 1.4 J 5.3 J 0.96 J 1.5 J 0.10U Calcium 5000 11200 9480 11600 11600 50.0 U Chromium 10 5.3 J 14.3 J 5.7 J 6.6 J 5.0 UJ Cobalt 50 2.9 2.7 4.2 32 5.0 UJ Copper 25 12.4 15.1 12.6 12.5 5.0 UJ Iron 100 3990 3200 4580 3770 40.0 U Lead 3.0 27.8 83.6 21.0 29.6 3.0 U Magnesium 5000 1180 1080 1210 1260 50.0 U Manganese 15 371 270 643 383 5.0 U Mercury 0.20 0.01 UJ 0.03 J 0.10 J 0.11 J 0.20 UJ Nickel 40 4.8 5.3 5.0 5.1 5.0 UJ Potassium 5000 101 J 116J 101 J 80.7 J 100 U Selenium 5.0 3.4 3.2 4.1 3.7 5.0 U Silver 10 0.17 UJ 0.10 J 0.17 UJ 0.02 UJ 0.20 U Sodium 5000 387 362 415 385 250U Thallium 10 0.34 U 0.37 U 0.34 U 0.37 U 4.0 U Vanadium 50 6.0 J 7.5 J 5.9 J 6.0 J 5.0 UJ Zinc 20 32.0 77.3 25.0 26.7 5.0 UJ
Page 3 of3
0-55
SITE: Ottati & Goss DATA SUMMARY TABLE CASE NO.: 0083M DAS METALS SDG NO.: DAMF87
Metals (mg/kg) Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
200 60 10
200 5.0 5.0
5000 10 50 25 100 3.0
5000 15
0.20 40
5000 5.0 10
5000 10 50 20
4610 0.27 UJ
2.9 J 53.6 J 0.49
1.3 J 7710 11.3J 1.6
10.6 1780 23.6 734 S9.8 0.01 J 3.9 173 3.5
0.02 UJ 732
0.36 UJ 5.6
22.1
4170 0.31 J
3.3 J 71.4 J 0.67
1.1 J 9380
6.3 J 2.5
11.1 3470 14.9 904 320 0.01 J 3.8
91.4 3.6
0.02 UJ 327
0.37 UJ 6.6
12.4
3680 0.29 UJ
3.5 J 71.9 J 0.71 J
1.3 J 11200
5.9 J 2.8
12.1 3670 15.1
1340 336
R 4.5
83.2 4.5
0.02 UJ 420
0.39 UJ 5.9
15.6
3030 0.29 UJ
2.6 J 66.8 J 0.70 0.83 J
11600 3.8 J 2.2
II.1 2940 11.5 1240 289 0.01 J 3.9
93.0 3.8
0.02 UJ 397
0.39 UJ 5.2
12.8
2950 0.27 UJ
3.4 J 65.2 J 0.65
1.4 J 10400
4.5 J 3.1
10.8 4220 24.5 1120 462
R 4.1
91.4 3.3
0.02 UJ 400
0.35 UJ 5.2
28.6
2990 0.27 UJ
3.7 J 66.1 J 0.73 . 1.5 J
10600 4.4 J 3.1
11.0 4290 24.9 1150 468 0.04 J 4.2
97.0 3.6
0.02 UJ 413
0.35 UJ 52
33.5
4280 0.73 J
4.2 J 78.8 J 0.71 J
3.2 J 10600
22.7 J 3.0
18.1 4080 92.7 1200 285
R 5.7 154 3.6
0.02 UJ 339 0.34 UJ 8.4
78.0
4590 1.1 J
35.4 J 96.9 J 0.80 J 3.9 J
13800 22.5 J 8.6 19.7
16100 125
1100 1590
R 10.4 136 6.3
0.05 J 473 0.36 UJ 13.0 142
Page 1 of3
SITE: Ottati & Goss CASE NO.: 0083M SDG NO.: DAMF87
Metals (mg/kg) Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
3880 0.27 UJ 4.5 J
79.5 J l .OJ 1.4 J
16100 7.1 J 3.1
13.2 3560 11.5
1670 410
0.05 J 5.1 103 6.3
0.02 UJ 517
0.35 UJ 6.6
18.1
3220 0.55 J ll .OJ 80.8 J 0.63 2.6 J
12800 7.0 J 5.7
11.2 7520 39J 1160 1030 0.06 J 62
89.2 3.8
0.02 UJ 366
0.39 UJ 7.9
44.2
2380 0.26 UJ
4.5 J 82.0 J 0.65
1.2 J 15000
3.9 J 1.2 9.2
3150 13.4
1510 175
0.02 J 5.2
227 3J
0.02 UJ 2720 0.35 UJ
6.4 14.9
3060 0.26 UJ
4.0 J 77.9 J 0.62
1.5 J 13400
5.3 J 1.9
11.0 3610 29.6 1440 317
0.08 J 4.0 150 3.7
0.02 UJ 1610 0.34 UJ
6.1 27.8
5530 0.26 UJ
1.1 J 22.8 J 0.23 0.62 J 896 14.1 J 1.5 3.3
4370 23.4 1290 54.9 0.17 J 5.6
253 0.71 0.02 UJ 101
0.35 UJ 8.3
25.8
8350 0.27 UJ
3.1 J 48.1 J 0.36 J 6.0 J
1780 39.8 J 2.5
10.2 5170 75.7 1800 80.1 0.91 J 8.0
307 1.0
0.09 J 166
0.36 UJ 12.7 91.4
6970 0.29 UJ
2.6 J 47.3 J 0.36 J
1.3 J 3750 20.7 J
1.7 7.0
3670 362 960 353
0.30 J 4.9 223 2.0
0.02 UJ 384
0.39 UJ 7.6
32.0
10800 0.25 J 4.9 J
49.6 J 0.57
1.7 J 5710 30.9 J 3.0
10.1 7770 52.9
2160 965
R 10.6 436 32
0.05 J 510
OJ3UJ 15.3 47.6
200 60 10
200 5.0 5.0
5000 10 50 25 100 3.0
5000 15
0.20 40
5000 5.0 10
5000 10 50 20
Page 2 of3
O
SITE: Ottati & Goss CASE NO.: 0083M SDG NO.: DAMF87
Metals (mg/kg) Aluminum 200 5210 3560 1730 40.0 U Antimony 60 0.26 UJ -0.62 J 0.28 UJ 3.0 U Arsenic 10 1.3 J 16.4 J 3.9 J 2.0 U Barium 200 42.4 J 77.1 J 46.5 J 5.0 U Beryllium 5.0 0.34 J 0.62 J 0.34 0.40 U Cadmium 5.0 1.8 J 0.53 J 0.51 J 0.10 U Calcium 5000 2420 22600 21800 59.7 Chromium 10 19.9 J 8.1 J 2.9 J 5.0 UJ Cobalt 50 0.91 5.6 1.5 5.0 UJ Copper Iron
25 100
5.2 1780
13.3 6210
5.1 2490
5.0 UJ 40.0 U
Lead 3.0 22.3 75.0 15.5 3.0 U Magnesium 5000 450 1830 1550 50.0 U Manganese 15 55.1 1100 251 5.0 U Mercury 0.20 0.38 J 0.04 J 0.04 J 0.20 UJ Nickel 40 2.6 11.7 6.1 5.0 UJ Potassium 5000 164 198 118 100 U Selenium 5.0 2.0 5.3 3.2 5.0 U Silver 10 0.06 J 0.02 UJ 0.02 UJ 0.20 U Sodium 5000 184 733 325 250 U Thallium 10 0.34 UJ 0.30 UJ 0.37 UJ 4.0 U Vanadium 50 4.9 13.3 6.1 5.0 UJ Zinc 20 20.8 71.9 18.9 5.0 UJ
Page 3 of3
SITE: Ottati & Goss DATA SUMMARY TABLE CASE NO.: 0083M DAS METALS SDG NO.: DAMG16 ______mg/kg
Metals (mg/kg) Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
200 60 10
200 5.0 5.0
5000 10 50 25 100 3.0
5000 15
0.20 40
5000 5.0 10
5000 10 50 20
3310 0.25 UJ
3.8 42.9 0.86 J 0.67
9340 U 3.9 1.3 8.1 U
2650 5.8
954 U 131
R 4.1
74.8 U 3.5
0.02 UJ 394 U
0.34 U 4.9 8.0
3930 I.5 J
22.7 912 0.78 4.7
16200 II.5 6.6
14.7 11100
58.2 1360 U 928
0.07 J 8.4 125 U 4.5
0.05 J 511 U 2.3 U
10.1 93.8
3440 0.40 J
4.3 69.2 0.70 J 2.5
12400 6.4 2.2
12.7 U 3380 27.2 1350 U 282
R 4.5
99.2 U 3.7
0.02 UJ 464 U
0.38 U 5.9
36.4
3370 0.71 J
7.9 78.4 0.59 J 3.5
13500 10.3 3.5
14.1 4310 71.7 1470 U 508
R 6.3 161 U 2.9
0.03 J 843 U
0.36 UJ 8.6
66.6
2860 027 UJ
2.9 78.7 0.61
1.2 15700
4.4 1.3 8.5 U
3990 11.0
1410 U 161
R 4.9
97.4 U 3.5
0.02 UJ 467 U
0.36 UJ 4.8
15.5
14400 0.28 J 47.0 85.9
1.0 1.8
7390 U 34.9 14.7 17.9
23300 88.7
3900 1880 0.01 J 23.0 1090 U
4.2 0.08 J 359 U
0.33 UJ 35.8 114
14500 0.27 J 42.7 80.0
1.1 1.8
7710 U 35.7 15.3 17.2
20300 89.7
4020 1920 0.01 J 22.9 1030 U
4.5 0.08 J 369 U
0.33 UJ 37.0 108
4110 0.65 J
7.1 73J 0.82 J 9J
10500 24.1 4.0
18.7 4740
102 1180U 767
0.01 J 6.8 136 U 3.8 0.7 J 460 U
036 UJ 8.4
82.8
Page 1 of3
a
SITE: Ottati & Goss CASE NO.: 0083M SDG NO.: DAMG16
Metils (mg/kg) Aluminum 200 Antimony 60 Arsenic 10 Barium 200 Beryllium 5.0 Cadmium 5.0 Calcium 5000 Chromium 10 Cobalt 50 Copper 25 Iron 100 Lead 3.0 Magnesium 5000 Manganese 15 Mercury 0.20 Nickel 40 Potassium 5000 Selenium 5.0 Silver 10 Sodium 5000 Thallium 10 Vanadium 50 Zinc 20
4980 1.3 J
45.8 100 1.2 8.1
14700 19.6 12.8 16.6
16100 74.9 1130U 1330 0.02 J 15.3 142 U 8.0
0.07 J 602 U 2.2 U
10.7 89.0
3050 0.59 J
5.6 62.1 0.56 J 4.4
11500 9.9 2.2
14.6 3390 57.6 1130U 346
R 4.7 100 U 3.4
0.04 J 404 U
0.33 UJ 6.4
54.4
2960 0.31 J
4.0 83.3 0.86 J
1.8 14300
6.5 2.7
11.4U 4320 30.8 1460 U 796
0.01 J 5.0 136 U 3.7
0.02 UJ 577 U
0.34 UJ 4.8
26.8
5620 1.7 J 6.5
80.3 0.90 J 5.5
9800 U 34.2 3.3
22.9 5100 94.4 1380 U 570
R 6.7
229 U 5.0
0.42 J 505 U
0.33 UJ 9.3
72.5
6920 0.59 J
5.5 61.2 0.59 2.8
7490 U 21.2 2.4
12.4 U 3630 44.3 1070 U 350
0.03 J 5.9 187 U 3.1
0.08 J 393 U
0.37 UJ 12.0 31.0
15800 0.28 UJ
6.7 70.9 0.69 4.0
5900 U 37.1 5.5
13.4 U 8900 60.6
3250 578
0.01 J 15.1 494 U 2.8
0.06 J 357 U 2.2 UJ
23.6 66.0
8700 0.26 UJ
5.1 57.9 0.56
1.4 9020 U 18.5 3.1
13.0 U 4170 44.7 1650 U 371
R 9.5
281 U 2.5
0.03 J 384 U
OJ5UJ 12.8 44.7
4460 079 UJ 5.1
65.4 0.74 J
1.2 13300
10.4 2.7
10.9 U 3350 19.0
1280 U 254 0.01 J 97 157 U 4.7
0.02 UJ 439 U
0.39 U 7.9
31.3
Page 2 of3
SITE: Ottati & Goss CASE NO.: 0083M SDG NO.: DAMG16
Metals (mg/kg) Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
200 60 10
200 5.0 5.0
5000 10 50 25 100 3.0
5000 15
0.20 40
5000 5.0 10
5000 10 50 20
4200 0.26 UJ 3.7
89.1 0.88 J 0.81
15400 6.1 2.7 9.3 U
5040 9.5
1670 U 472
R 6.5 158 U 4.2
0.02 UJ 535 U
0.34 UJ 5.4
12.9
3940 0.45 J 45.8 76.1 0.78 J 2.6
18000 7.8 5.1
10.9 U 7320 31.3 1400 U 1490
R 12.2 179 U 4.2
0.02 UJ 1200 U 0.38 UJ 7.9
43.6
40.0 U 3.0 U 2.0 U
22.3 0.40 U 0.10 U
22400 5.0 UJ 5.0 UJ
27.1 J 44.2 3.0 U
3770 5.0 U
0.20 UJ 5.0 UJ
3170 5.0 U
0.20 U 11500
4.0 U 5.0 UJ
13.6 J
Page 3 of3
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Metils (mg/kg) Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
SITE: Ottati & Goss DATA SUMMARY TABLE CASE NO.: 0083M DAS METALS SDG NO.: DAMG28 ______mg/kg______
6310 0.39 J
5.5 J 76.1 0.67 J 4.5 J
11300 29.0 3.8
19.4 5080
136 J 1490 406
0.02 J 8.2
280 J 3.1 J
0.09 J 461 J
0.34 UJ 12.1 81.3
3510 0.27 UJ
1.6 J 22.5 0.17 J 2.2 J
2090 19.1 U 73
2770 38.1 J 1110 76.0 0.32 J 4.2 255 J
0.71 J 0.02 J 141 J
0.36 U 6.3
27.2
3630 0.62 J
4.1 J 68.2 0.68 J 3.8 J
10300 17.0 2.7
14.6 3690 65.8 J 1270 477
R 4.6 174 J 3.3 J
0.07 J 491 J
0.35 UJ 6.9
56.9
200 60 10
200 5.0 5.0
5000 10 50 25 100 3.0
5000 15
0.20 40
5000 5.0 10
5000 10 50 20
3190 0.24 UJ
1.3 J 20.9 0.15 J
1.1 J 1930 19.0
1.1 7.6
2530 38.5 J 1010 73.5 0.21 J 4.0 223 J
0.64 J 0.02 UJ 143 J
0.32 U 5.9
27.1
3640 0.69 J
4.6 J 73.4 0.61 J 4.3 J
12100 19.3 3.0
17.5 4180 81.4 J 1480 497
R 4.9 160 J 3.0 J
0.06 J 495 J
0.37 UJ 7.2
73.0
10200 0.26 UJ
7.3 J 67.7 0.93 J 0.67 J
7120 20.8
5.5 9.3
10700 23.3 J 2090 1280
R 11.1 458 J 3.8 J
0.09 J 380 J 2.1 UJ
15.3 46.5
9030 0.32 J 10.4 J 67.9 0.63 J 2.6 J
10200 20.9 5.8
13.7 6440 48.5 J 1540 1680 0.01 J 9.9 332 J 3.1 J
0.08 J 387 J
0.35 UJ 17.1 54.7
5620 0.30 UJ 8.7 J
642 0.81 J 2JJ
14000 13.7 3.8
13.8 4400 32.2 J 1620 1210 0.03 J 7.5
247 J 5.7 J
0.10 J 470 J
0.40 UJ 10.6 48.2
Page 1 of2
SITE: Ottati & Goss CASE NO.: 0083M SDG NO.: DAMG28
Metals (mg/kg) Aluminum 200 40SO 2300 2030 3730 40.0 U
- Antimony 60 0.25 UJ 0.59 J 0.26 UJ 0.33 J 3.0 UJ Arsenic 10 7.3 J 7.8 J 2.2 J 5.3 J 2.0 U Barium 200 59.5 85.9 60.3 45.6 5.0 U Beryllium 5.0 0.46 J 0.46 J 0.54 J 0.67 J 0.40 UJ Cadmium 5.0 0.45 J 1.5 J 0.40 J 1.1 J 0.52 Calcium 5000 12200 21500 18400 14900 50.0 U Chromium 10 8.3 6.4 3.7 7.4 5.0 UJ Cobalt 50 3.3 9.3 1.6 2.2 5.0 UJ Copper 25 8.3 7.8 6.2 93 5.0 UJ Iron 100 6730 6750 2970 3360 40.0 U Lead 3.0 8.9 J 30.1 J 13.7 J 27.1 J 3.0 U Magnesium 5000 1320 1750 1570 1220 50.0 U Manganese 15 557 2240 380 234 5.0 U Mercury 0.20 0.02 J 0.06 J 0.03 J 0.03 J 0.20 UJ Nickel 40 6.6 9.4 43 6.6 5.0 UJ Potassium 5000 189 J 184 J 121 J 159 J 100 U Selenium 5.0 5.4 J 3.3 J 3.8 J 3.6 J 5.0 U Silver 10 0.05 J 0.03 J 0.02 J 0.04 J 0.20 U Sodium 5000 412 J 804 J 451 J 263 J 250 U Thallium 10 0.34 UJ 2.1 U 0.34 U 0.36 U 4.0 U Vanadium 50 7.7 7.3 3.8 8.8 5.0 UJ Zinc 20 14.7 58.2 12.8 28.7 5.0 UJ
Page 2 of2
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