Post on 30-Aug-2018
August 2017 Project No. 1656790
APPENDIX B
GROUNDWATER MONITORING FORMS & ANALYTICAL LABORATORY RESULTS
October 06, 2016
Anne Faeth-BoydGolder Associates820 South Main St.Suite 100St Charles, MO 63301
The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Results are expressed as "as received" unless otherwise noted.
QC sample results for this data met EPA or laboratory specifications except as noted in the Case Narrative or as noted with qualifiers in the QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained by ALS Environmental. Samples will be disposed in 30 days unless storage arrangements are made.
If you have any questions regarding this report, please feel free to call me.
Sincerely,
ALS Environmental received 6 sample(s) on Sep 29, 2016 for the analysis presented in the following report.
Laboratory Results for: City of Camdenton
Dear Anne,
Work Order: HS16091367
Generated By: Jumoke.Lawal
Dane J. Wacasey
10450 Stancliff Rd. Suite 210 Houston, TX 77099 T: +1 281 530 5656 F: +1 281 530 5887 www.alsglobal.com
Page 1 of 30
Client: Golder Associates
Work Order: HS16091367Project: City of Camdenton SAMPLE SUMMARY
Lab Samp ID Client Sample ID Collection DateMatrix TagNo Date Received Hold
HS16091367-01 28-Sep-2016 11:30 29-Sep-2016 08:20Mulberry Well (437-472) Water
HS16091367-02 27-Sep-2016 18:35 29-Sep-2016 08:20Mulberry Well (564-598) Water
HS16091367-03 27-Sep-2016 14:08 29-Sep-2016 08:20Mulberry Well (532-567) Water
HS16091367-04 27-Sep-2016 11:00 29-Sep-2016 08:20Mulberry Well (511-546) Water
HS16091367-05 26-Sep-2016 18:25 29-Sep-2016 08:20Mulberry Well (395-429) Water
HS16091367-06 28-Sep-2016 00:00 29-Sep-2016 08:20Trip Blank Water
ALS Group USA, Corp 06-Oct-16Date:
Page 2 of 30
Client: CASE NARRATIVE
Work Order:City of CamdentonGolder Associates
Project:HS16091367
GCMS Volatiles by Method SW8260
Batch ID: R282565Sample ID: Mulberry Well (564-598) (HS16091367-02MSD)
Some compounds outside recovery limits on MS/MSD.•
Sample ID: VLCSW-161005cis-1,3-Dichloropropene and Methylcyclohexane exceeded %recovery limits on LCS. Samples are non detect in the batch•
Sample ID: VSTD050Dichlorodifluoromethane, cis-1,3-Dichloropropene and Methylcyclohexane exceeded %D limits on CCV. Samples are non detect•
ALS Group USA, Corp 06-Oct-16Date:
Page 3 of 30
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonMulberry Well (437-472)
WorkOrder:Lab ID:
Collection Date:
HS16091367HS16091367-01
28-Sep-2016 11:30 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 05-Oct-2016 14:300.201,1,1-Trichloroethane 1.0U
1ug/L 05-Oct-2016 14:300.501,1,2,2-Tetrachloroethane 1.0U
1ug/L 05-Oct-2016 14:301.01,1,2-Trichlor-1,2,2-trifluoroethane 1.0U
1ug/L 05-Oct-2016 14:300.301,1,2-Trichloroethane 1.0U
1ug/L 05-Oct-2016 14:300.201,1-Dichloroethane 1.0U
1ug/L 05-Oct-2016 14:300.201,1-Dichloroethene 1.0U
1ug/L 05-Oct-2016 14:300.501,2,4-Trichlorobenzene 1.0U
1ug/L 05-Oct-2016 14:301.01,2-Dibromo-3-chloropropane 1.0U
1ug/L 05-Oct-2016 14:300.201,2-Dibromoethane 1.0U
1ug/L 05-Oct-2016 14:300.501,2-Dichlorobenzene 1.0U
1ug/L 05-Oct-2016 14:300.201,2-Dichloroethane 1.0U
1ug/L 05-Oct-2016 14:300.501,2-Dichloropropane 1.0U
1ug/L 05-Oct-2016 14:300.401,3-Dichlorobenzene 1.0U
1ug/L 05-Oct-2016 14:300.401,4-Dichlorobenzene 1.0U
1ug/L 05-Oct-2016 14:300.502-Butanone 2.0U
1ug/L 05-Oct-2016 14:301.02-Hexanone 2.0U
1ug/L 05-Oct-2016 14:300.704-Methyl-2-pentanone 2.0U
1ug/L 05-Oct-2016 14:302.0Acetone 2.0U
1ug/L 05-Oct-2016 14:300.20Benzene 1.0U
1ug/L 05-Oct-2016 14:300.20Bromodichloromethane 1.0U
1ug/L 05-Oct-2016 14:300.40Bromoform 1.0U
1ug/L 05-Oct-2016 14:300.40Bromomethane 1.0U
1ug/L 05-Oct-2016 14:300.60Carbon disulfide 2.0U
1ug/L 05-Oct-2016 14:300.50Carbon tetrachloride 1.0U
1ug/L 05-Oct-2016 14:300.30Chlorobenzene 1.0U
1ug/L 05-Oct-2016 14:300.30Chloroethane 1.0U
1ug/L 05-Oct-2016 14:300.20Chloroform 1.0U
1ug/L 05-Oct-2016 14:300.20Chloromethane 1.0U
1ug/L 05-Oct-2016 14:300.20cis-1,2-Dichloroethene 1.08.2
1ug/L 05-Oct-2016 14:300.10cis-1,3-Dichloropropene 1.0U
1ug/L 05-Oct-2016 14:300.30Cyclohexane 1.0U
1ug/L 05-Oct-2016 14:300.30Dibromochloromethane 1.0U
1ug/L 05-Oct-2016 14:300.30Dichlorodifluoromethane 1.0U
1ug/L 05-Oct-2016 14:300.30Ethylbenzene 1.0U
1ug/L 05-Oct-2016 14:300.30Isopropylbenzene 1.0U
1ug/L 05-Oct-2016 14:300.50m,p-Xylene 2.0U
1ug/L 05-Oct-2016 14:301.0Methyl acetate 1.0U
1ug/L 05-Oct-2016 14:300.20Methyl tert-butyl ether 1.0U
1ug/L 05-Oct-2016 14:300.30Methylcyclohexane 1.0U
06-Oct-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 4 of 30
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonMulberry Well (437-472)
WorkOrder:Lab ID:
Collection Date:
HS16091367HS16091367-01
28-Sep-2016 11:30 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 05-Oct-2016 14:301.0Methylene chloride 2.0U
1ug/L 05-Oct-2016 14:300.30o-Xylene 1.0U
1ug/L 05-Oct-2016 14:300.30Styrene 1.0U
1ug/L 05-Oct-2016 14:300.30Tetrachloroethene 1.0U
1ug/L 05-Oct-2016 14:300.20Toluene 1.01.2
1ug/L 05-Oct-2016 14:300.20trans-1,2-Dichloroethene 1.0U
1ug/L 05-Oct-2016 14:300.20trans-1,3-Dichloropropene 1.0U
1ug/L 05-Oct-2016 14:300.20Trichloroethene 1.0140
1ug/L 05-Oct-2016 14:300.30Trichlorofluoromethane 1.0U
1ug/L 05-Oct-2016 14:300.20Vinyl chloride 1.0U
1ug/L 05-Oct-2016 14:300.50Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 05-Oct-2016 14:3098.4 71-125
Surr: 4-Bromofluorobenzene 1%REC 05-Oct-2016 14:3090.0 70-125
Surr: Dibromofluoromethane 1%REC 05-Oct-2016 14:3079.0 74-125
Surr: Toluene-d8 1%REC 05-Oct-2016 14:30104 75-125
06-Oct-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 5 of 30
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonMulberry Well (564-598)
WorkOrder:Lab ID:
Collection Date:
HS16091367HS16091367-02
27-Sep-2016 18:35 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 05-Oct-2016 12:210.201,1,1-Trichloroethane 1.0U
1ug/L 05-Oct-2016 12:210.501,1,2,2-Tetrachloroethane 1.0U
1ug/L 05-Oct-2016 12:211.01,1,2-Trichlor-1,2,2-trifluoroethane 1.0U
1ug/L 05-Oct-2016 12:210.301,1,2-Trichloroethane 1.0U
1ug/L 05-Oct-2016 12:210.201,1-Dichloroethane 1.0U
1ug/L 05-Oct-2016 12:210.201,1-Dichloroethene 1.0U
1ug/L 05-Oct-2016 12:210.501,2,4-Trichlorobenzene 1.0U
1ug/L 05-Oct-2016 12:211.01,2-Dibromo-3-chloropropane 1.0U
1ug/L 05-Oct-2016 12:210.201,2-Dibromoethane 1.0U
1ug/L 05-Oct-2016 12:210.501,2-Dichlorobenzene 1.0U
1ug/L 05-Oct-2016 12:210.201,2-Dichloroethane 1.0U
1ug/L 05-Oct-2016 12:210.501,2-Dichloropropane 1.0U
1ug/L 05-Oct-2016 12:210.401,3-Dichlorobenzene 1.0U
1ug/L 05-Oct-2016 12:210.401,4-Dichlorobenzene 1.0U
1ug/L 05-Oct-2016 12:210.502-Butanone 2.0U
1ug/L 05-Oct-2016 12:211.02-Hexanone 2.0U
1ug/L 05-Oct-2016 12:210.704-Methyl-2-pentanone 2.0U
1ug/L 05-Oct-2016 12:212.0Acetone 2.0U
1ug/L 05-Oct-2016 12:210.20Benzene 1.0U
1ug/L 05-Oct-2016 12:210.20Bromodichloromethane 1.0U
1ug/L 05-Oct-2016 12:210.40Bromoform 1.0U
1ug/L 05-Oct-2016 12:210.40Bromomethane 1.0U
1ug/L 05-Oct-2016 12:210.60Carbon disulfide 2.0U
1ug/L 05-Oct-2016 12:210.50Carbon tetrachloride 1.0U
1ug/L 05-Oct-2016 12:210.30Chlorobenzene 1.0U
1ug/L 05-Oct-2016 12:210.30Chloroethane 1.0U
1ug/L 05-Oct-2016 12:210.20Chloroform 1.0U
1ug/L 05-Oct-2016 12:210.20Chloromethane 1.0U
1ug/L 05-Oct-2016 12:210.20cis-1,2-Dichloroethene 1.03.2
1ug/L 05-Oct-2016 12:210.10cis-1,3-Dichloropropene 1.0U
1ug/L 05-Oct-2016 12:210.30Cyclohexane 1.0U
1ug/L 05-Oct-2016 12:210.30Dibromochloromethane 1.0U
1ug/L 05-Oct-2016 12:210.30Dichlorodifluoromethane 1.0U
1ug/L 05-Oct-2016 12:210.30Ethylbenzene 1.0U
1ug/L 05-Oct-2016 12:210.30Isopropylbenzene 1.0U
1ug/L 05-Oct-2016 12:210.50m,p-Xylene 2.0U
1ug/L 05-Oct-2016 12:211.0Methyl acetate 1.0U
1ug/L 05-Oct-2016 12:210.20Methyl tert-butyl ether 1.0U
1ug/L 05-Oct-2016 12:210.30Methylcyclohexane 1.0U
06-Oct-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 6 of 30
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonMulberry Well (564-598)
WorkOrder:Lab ID:
Collection Date:
HS16091367HS16091367-02
27-Sep-2016 18:35 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 05-Oct-2016 12:211.0Methylene chloride 2.0U
1ug/L 05-Oct-2016 12:210.30o-Xylene 1.0U
1ug/L 05-Oct-2016 12:210.30Styrene 1.0U
1ug/L 05-Oct-2016 12:210.30Tetrachloroethene 1.0U
1ug/L 05-Oct-2016 12:210.20Toluene 1.01.8
1ug/L 05-Oct-2016 12:210.20trans-1,2-Dichloroethene 1.0U
1ug/L 05-Oct-2016 12:210.20trans-1,3-Dichloropropene 1.0U
1ug/L 05-Oct-2016 12:210.20Trichloroethene 1.052
1ug/L 05-Oct-2016 12:210.30Trichlorofluoromethane 1.0U
1ug/L 05-Oct-2016 12:210.20Vinyl chloride 1.0U
1ug/L 05-Oct-2016 12:210.50Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 05-Oct-2016 12:21100 71-125
Surr: 4-Bromofluorobenzene 1%REC 05-Oct-2016 12:2189.0 70-125
Surr: Dibromofluoromethane 1%REC 05-Oct-2016 12:2182.4 74-125
Surr: Toluene-d8 1%REC 05-Oct-2016 12:21102 75-125
06-Oct-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 7 of 30
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonMulberry Well (532-567)
WorkOrder:Lab ID:
Collection Date:
HS16091367HS16091367-03
27-Sep-2016 14:08 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 05-Oct-2016 14:560.201,1,1-Trichloroethane 1.0U
1ug/L 05-Oct-2016 14:560.501,1,2,2-Tetrachloroethane 1.0U
1ug/L 05-Oct-2016 14:561.01,1,2-Trichlor-1,2,2-trifluoroethane 1.0U
1ug/L 05-Oct-2016 14:560.301,1,2-Trichloroethane 1.0U
1ug/L 05-Oct-2016 14:560.201,1-Dichloroethane 1.0U
1ug/L 05-Oct-2016 14:560.201,1-Dichloroethene 1.0U
1ug/L 05-Oct-2016 14:560.501,2,4-Trichlorobenzene 1.0U
1ug/L 05-Oct-2016 14:561.01,2-Dibromo-3-chloropropane 1.0U
1ug/L 05-Oct-2016 14:560.201,2-Dibromoethane 1.0U
1ug/L 05-Oct-2016 14:560.501,2-Dichlorobenzene 1.0U
1ug/L 05-Oct-2016 14:560.201,2-Dichloroethane 1.0U
1ug/L 05-Oct-2016 14:560.501,2-Dichloropropane 1.0U
1ug/L 05-Oct-2016 14:560.401,3-Dichlorobenzene 1.0U
1ug/L 05-Oct-2016 14:560.401,4-Dichlorobenzene 1.0U
1ug/L 05-Oct-2016 14:560.502-Butanone 2.0U
1ug/L 05-Oct-2016 14:561.02-Hexanone 2.0U
1ug/L 05-Oct-2016 14:560.704-Methyl-2-pentanone 2.0U
1ug/L 05-Oct-2016 14:562.0Acetone 2.0U
1ug/L 05-Oct-2016 14:560.20Benzene 1.0U
1ug/L 05-Oct-2016 14:560.20Bromodichloromethane 1.0U
1ug/L 05-Oct-2016 14:560.40Bromoform 1.0U
1ug/L 05-Oct-2016 14:560.40Bromomethane 1.0U
1ug/L 05-Oct-2016 14:560.60Carbon disulfide 2.0U
1ug/L 05-Oct-2016 14:560.50Carbon tetrachloride 1.0U
1ug/L 05-Oct-2016 14:560.30Chlorobenzene 1.0U
1ug/L 05-Oct-2016 14:560.30Chloroethane 1.0U
1ug/L 05-Oct-2016 14:560.20Chloroform 1.0U
1ug/L 05-Oct-2016 14:560.20Chloromethane 1.0U
1ug/L 05-Oct-2016 14:560.20cis-1,2-Dichloroethene 1.03.3
1ug/L 05-Oct-2016 14:560.10cis-1,3-Dichloropropene 1.0U
1ug/L 05-Oct-2016 14:560.30Cyclohexane 1.0U
1ug/L 05-Oct-2016 14:560.30Dibromochloromethane 1.0U
1ug/L 05-Oct-2016 14:560.30Dichlorodifluoromethane 1.0U
1ug/L 05-Oct-2016 14:560.30Ethylbenzene 1.0U
1ug/L 05-Oct-2016 14:560.30Isopropylbenzene 1.0U
1ug/L 05-Oct-2016 14:560.50m,p-Xylene 2.0U
1ug/L 05-Oct-2016 14:561.0Methyl acetate 1.0U
1ug/L 05-Oct-2016 14:560.20Methyl tert-butyl ether 1.0U
1ug/L 05-Oct-2016 14:560.30Methylcyclohexane 1.0U
06-Oct-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 8 of 30
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonMulberry Well (532-567)
WorkOrder:Lab ID:
Collection Date:
HS16091367HS16091367-03
27-Sep-2016 14:08 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 05-Oct-2016 14:561.0Methylene chloride 2.0U
1ug/L 05-Oct-2016 14:560.30o-Xylene 1.0U
1ug/L 05-Oct-2016 14:560.30Styrene 1.0U
1ug/L 05-Oct-2016 14:560.30Tetrachloroethene 1.0U
1ug/L 05-Oct-2016 14:560.20Toluene 1.02.8
1ug/L 05-Oct-2016 14:560.20trans-1,2-Dichloroethene 1.0U
1ug/L 05-Oct-2016 14:560.20trans-1,3-Dichloropropene 1.0U
1ug/L 05-Oct-2016 14:560.20Trichloroethene 1.058
1ug/L 05-Oct-2016 14:560.30Trichlorofluoromethane 1.0U
1ug/L 05-Oct-2016 14:560.20Vinyl chloride 1.0U
1ug/L 05-Oct-2016 14:560.50Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 05-Oct-2016 14:5699.8 71-125
Surr: 4-Bromofluorobenzene 1%REC 05-Oct-2016 14:5689.3 70-125
Surr: Dibromofluoromethane 1%REC 05-Oct-2016 14:5682.4 74-125
Surr: Toluene-d8 1%REC 05-Oct-2016 14:56103 75-125
06-Oct-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 9 of 30
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonMulberry Well (511-546)
WorkOrder:Lab ID:
Collection Date:
HS16091367HS16091367-04
27-Sep-2016 11:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 05-Oct-2016 15:220.201,1,1-Trichloroethane 1.0U
1ug/L 05-Oct-2016 15:220.501,1,2,2-Tetrachloroethane 1.0U
1ug/L 05-Oct-2016 15:221.01,1,2-Trichlor-1,2,2-trifluoroethane 1.0U
1ug/L 05-Oct-2016 15:220.301,1,2-Trichloroethane 1.0U
1ug/L 05-Oct-2016 15:220.201,1-Dichloroethane 1.0U
1ug/L 05-Oct-2016 15:220.201,1-Dichloroethene 1.0U
1ug/L 05-Oct-2016 15:220.501,2,4-Trichlorobenzene 1.0U
1ug/L 05-Oct-2016 15:221.01,2-Dibromo-3-chloropropane 1.0U
1ug/L 05-Oct-2016 15:220.201,2-Dibromoethane 1.0U
1ug/L 05-Oct-2016 15:220.501,2-Dichlorobenzene 1.0U
1ug/L 05-Oct-2016 15:220.201,2-Dichloroethane 1.0U
1ug/L 05-Oct-2016 15:220.501,2-Dichloropropane 1.0U
1ug/L 05-Oct-2016 15:220.401,3-Dichlorobenzene 1.0U
1ug/L 05-Oct-2016 15:220.401,4-Dichlorobenzene 1.0U
1ug/L 05-Oct-2016 15:220.502-Butanone 2.0U
1ug/L 05-Oct-2016 15:221.02-Hexanone 2.0U
1ug/L 05-Oct-2016 15:220.704-Methyl-2-pentanone 2.0U
1ug/L 05-Oct-2016 15:222.0Acetone 2.0U
1ug/L 05-Oct-2016 15:220.20Benzene 1.0U
1ug/L 05-Oct-2016 15:220.20Bromodichloromethane 1.0U
1ug/L 05-Oct-2016 15:220.40Bromoform 1.0U
1ug/L 05-Oct-2016 15:220.40Bromomethane 1.0U
1ug/L 05-Oct-2016 15:220.60Carbon disulfide 2.0U
1ug/L 05-Oct-2016 15:220.50Carbon tetrachloride 1.0U
1ug/L 05-Oct-2016 15:220.30Chlorobenzene 1.0U
1ug/L 05-Oct-2016 15:220.30Chloroethane 1.0U
1ug/L 05-Oct-2016 15:220.20Chloroform 1.0U
1ug/L 05-Oct-2016 15:220.20Chloromethane 1.0U
1ug/L 05-Oct-2016 15:220.20cis-1,2-Dichloroethene 1.01.6
1ug/L 05-Oct-2016 15:220.10cis-1,3-Dichloropropene 1.0U
1ug/L 05-Oct-2016 15:220.30Cyclohexane 1.0U
1ug/L 05-Oct-2016 15:220.30Dibromochloromethane 1.0U
1ug/L 05-Oct-2016 15:220.30Dichlorodifluoromethane 1.0U
1ug/L 05-Oct-2016 15:220.30Ethylbenzene 1.0U
1ug/L 05-Oct-2016 15:220.30Isopropylbenzene 1.0U
1ug/L 05-Oct-2016 15:220.50m,p-Xylene 2.0U
1ug/L 05-Oct-2016 15:221.0Methyl acetate 1.0U
1ug/L 05-Oct-2016 15:220.20Methyl tert-butyl ether 1.0U
1ug/L 05-Oct-2016 15:220.30Methylcyclohexane 1.0U
06-Oct-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 10 of 30
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonMulberry Well (511-546)
WorkOrder:Lab ID:
Collection Date:
HS16091367HS16091367-04
27-Sep-2016 11:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 05-Oct-2016 15:221.0Methylene chloride 2.0U
1ug/L 05-Oct-2016 15:220.30o-Xylene 1.0U
1ug/L 05-Oct-2016 15:220.30Styrene 1.0U
1ug/L 05-Oct-2016 15:220.30Tetrachloroethene 1.0U
1ug/L 05-Oct-2016 15:22J 0.20Toluene 1.00.84
1ug/L 05-Oct-2016 15:220.20trans-1,2-Dichloroethene 1.0U
1ug/L 05-Oct-2016 15:220.20trans-1,3-Dichloropropene 1.0U
1ug/L 05-Oct-2016 15:220.20Trichloroethene 1.030
1ug/L 05-Oct-2016 15:220.30Trichlorofluoromethane 1.0U
1ug/L 05-Oct-2016 15:220.20Vinyl chloride 1.0U
1ug/L 05-Oct-2016 15:220.50Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 05-Oct-2016 15:2299.4 71-125
Surr: 4-Bromofluorobenzene 1%REC 05-Oct-2016 15:2288.9 70-125
Surr: Dibromofluoromethane 1%REC 05-Oct-2016 15:2281.7 74-125
Surr: Toluene-d8 1%REC 05-Oct-2016 15:22104 75-125
06-Oct-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 11 of 30
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonMulberry Well (395-429)
WorkOrder:Lab ID:
Collection Date:
HS16091367HS16091367-05
26-Sep-2016 18:25 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 05-Oct-2016 12:470.201,1,1-Trichloroethane 1.0U
1ug/L 05-Oct-2016 12:470.501,1,2,2-Tetrachloroethane 1.0U
1ug/L 05-Oct-2016 12:471.01,1,2-Trichlor-1,2,2-trifluoroethane 1.0U
1ug/L 05-Oct-2016 12:470.301,1,2-Trichloroethane 1.0U
1ug/L 05-Oct-2016 12:470.201,1-Dichloroethane 1.0U
1ug/L 05-Oct-2016 12:470.201,1-Dichloroethene 1.0U
1ug/L 05-Oct-2016 12:470.501,2,4-Trichlorobenzene 1.0U
1ug/L 05-Oct-2016 12:471.01,2-Dibromo-3-chloropropane 1.0U
1ug/L 05-Oct-2016 12:470.201,2-Dibromoethane 1.0U
1ug/L 05-Oct-2016 12:470.501,2-Dichlorobenzene 1.0U
1ug/L 05-Oct-2016 12:470.201,2-Dichloroethane 1.0U
1ug/L 05-Oct-2016 12:470.501,2-Dichloropropane 1.0U
1ug/L 05-Oct-2016 12:470.401,3-Dichlorobenzene 1.0U
1ug/L 05-Oct-2016 12:470.401,4-Dichlorobenzene 1.0U
1ug/L 05-Oct-2016 12:470.502-Butanone 2.0U
1ug/L 05-Oct-2016 12:471.02-Hexanone 2.0U
1ug/L 05-Oct-2016 12:470.704-Methyl-2-pentanone 2.0U
1ug/L 05-Oct-2016 12:472.0Acetone 2.0U
1ug/L 05-Oct-2016 12:470.20Benzene 1.0U
1ug/L 05-Oct-2016 12:470.20Bromodichloromethane 1.0U
1ug/L 05-Oct-2016 12:470.40Bromoform 1.0U
1ug/L 05-Oct-2016 12:470.40Bromomethane 1.0U
1ug/L 05-Oct-2016 12:470.60Carbon disulfide 2.0U
1ug/L 05-Oct-2016 12:470.50Carbon tetrachloride 1.0U
1ug/L 05-Oct-2016 12:470.30Chlorobenzene 1.0U
1ug/L 05-Oct-2016 12:470.30Chloroethane 1.0U
1ug/L 05-Oct-2016 12:470.20Chloroform 1.0U
1ug/L 05-Oct-2016 12:470.20Chloromethane 1.0U
1ug/L 05-Oct-2016 12:470.20cis-1,2-Dichloroethene 1.016
1ug/L 05-Oct-2016 12:470.10cis-1,3-Dichloropropene 1.0U
1ug/L 05-Oct-2016 12:470.30Cyclohexane 1.0U
1ug/L 05-Oct-2016 12:470.30Dibromochloromethane 1.0U
1ug/L 05-Oct-2016 12:470.30Dichlorodifluoromethane 1.0U
1ug/L 05-Oct-2016 12:470.30Ethylbenzene 1.0U
1ug/L 05-Oct-2016 12:470.30Isopropylbenzene 1.0U
1ug/L 05-Oct-2016 12:470.50m,p-Xylene 2.0U
1ug/L 05-Oct-2016 12:471.0Methyl acetate 1.0U
1ug/L 05-Oct-2016 12:470.20Methyl tert-butyl ether 1.0U
1ug/L 05-Oct-2016 12:470.30Methylcyclohexane 1.0U
06-Oct-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 12 of 30
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonMulberry Well (395-429)
WorkOrder:Lab ID:
Collection Date:
HS16091367HS16091367-05
26-Sep-2016 18:25 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 05-Oct-2016 12:471.0Methylene chloride 2.0U
1ug/L 05-Oct-2016 12:470.30o-Xylene 1.0U
1ug/L 05-Oct-2016 12:470.30Styrene 1.0U
1ug/L 05-Oct-2016 12:470.30Tetrachloroethene 1.0U
1ug/L 05-Oct-2016 12:47J 0.20Toluene 1.00.70
1ug/L 05-Oct-2016 12:470.20trans-1,2-Dichloroethene 1.0U
1ug/L 05-Oct-2016 12:470.20trans-1,3-Dichloropropene 1.0U
10ug/L 05-Oct-2016 14:052.0Trichloroethene 10240
1ug/L 05-Oct-2016 12:470.30Trichlorofluoromethane 1.0U
1ug/L 05-Oct-2016 12:470.20Vinyl chloride 1.0U
1ug/L 05-Oct-2016 12:470.50Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 05-Oct-2016 12:47101 71-125
Surr: 1,2-Dichloroethane-d4 10%REC 05-Oct-2016 14:0595.4 71-125
Surr: 4-Bromofluorobenzene 10%REC 05-Oct-2016 14:0590.4 70-125
Surr: 4-Bromofluorobenzene 1%REC 05-Oct-2016 12:4788.8 70-125
Surr: Dibromofluoromethane 1%REC 05-Oct-2016 12:4784.0 74-125
Surr: Dibromofluoromethane 10%REC 05-Oct-2016 14:0593.7 74-125
Surr: Toluene-d8 10%REC 05-Oct-2016 14:05104 75-125
Surr: Toluene-d8 1%REC 05-Oct-2016 12:47105 75-125
06-Oct-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 13 of 30
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonTrip Blank
WorkOrder:Lab ID:
Collection Date:
HS16091367HS16091367-06
28-Sep-2016 00:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 05-Oct-2016 15:480.201,1,1-Trichloroethane 1.0U
1ug/L 05-Oct-2016 15:480.501,1,2,2-Tetrachloroethane 1.0U
1ug/L 05-Oct-2016 15:481.01,1,2-Trichlor-1,2,2-trifluoroethane 1.0U
1ug/L 05-Oct-2016 15:480.301,1,2-Trichloroethane 1.0U
1ug/L 05-Oct-2016 15:480.201,1-Dichloroethane 1.0U
1ug/L 05-Oct-2016 15:480.201,1-Dichloroethene 1.0U
1ug/L 05-Oct-2016 15:480.501,2,4-Trichlorobenzene 1.0U
1ug/L 05-Oct-2016 15:481.01,2-Dibromo-3-chloropropane 1.0U
1ug/L 05-Oct-2016 15:480.201,2-Dibromoethane 1.0U
1ug/L 05-Oct-2016 15:480.501,2-Dichlorobenzene 1.0U
1ug/L 05-Oct-2016 15:480.201,2-Dichloroethane 1.0U
1ug/L 05-Oct-2016 15:480.501,2-Dichloropropane 1.0U
1ug/L 05-Oct-2016 15:480.401,3-Dichlorobenzene 1.0U
1ug/L 05-Oct-2016 15:480.401,4-Dichlorobenzene 1.0U
1ug/L 05-Oct-2016 15:480.502-Butanone 2.0U
1ug/L 05-Oct-2016 15:481.02-Hexanone 2.0U
1ug/L 05-Oct-2016 15:480.704-Methyl-2-pentanone 2.0U
1ug/L 05-Oct-2016 15:482.0Acetone 2.0U
1ug/L 05-Oct-2016 15:480.20Benzene 1.0U
1ug/L 05-Oct-2016 15:480.20Bromodichloromethane 1.0U
1ug/L 05-Oct-2016 15:480.40Bromoform 1.0U
1ug/L 05-Oct-2016 15:480.40Bromomethane 1.0U
1ug/L 05-Oct-2016 15:480.60Carbon disulfide 2.0U
1ug/L 05-Oct-2016 15:480.50Carbon tetrachloride 1.0U
1ug/L 05-Oct-2016 15:480.30Chlorobenzene 1.0U
1ug/L 05-Oct-2016 15:480.30Chloroethane 1.0U
1ug/L 05-Oct-2016 15:480.20Chloroform 1.0U
1ug/L 05-Oct-2016 15:480.20Chloromethane 1.0U
1ug/L 05-Oct-2016 15:480.20cis-1,2-Dichloroethene 1.0U
1ug/L 05-Oct-2016 15:480.10cis-1,3-Dichloropropene 1.0U
1ug/L 05-Oct-2016 15:480.30Cyclohexane 1.0U
1ug/L 05-Oct-2016 15:480.30Dibromochloromethane 1.0U
1ug/L 05-Oct-2016 15:480.30Dichlorodifluoromethane 1.0U
1ug/L 05-Oct-2016 15:480.30Ethylbenzene 1.0U
1ug/L 05-Oct-2016 15:480.30Isopropylbenzene 1.0U
1ug/L 05-Oct-2016 15:480.50m,p-Xylene 2.0U
1ug/L 05-Oct-2016 15:481.0Methyl acetate 1.0U
1ug/L 05-Oct-2016 15:480.20Methyl tert-butyl ether 1.0U
1ug/L 05-Oct-2016 15:480.30Methylcyclohexane 1.0U
06-Oct-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 14 of 30
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonTrip Blank
WorkOrder:Lab ID:
Collection Date:
HS16091367HS16091367-06
28-Sep-2016 00:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 05-Oct-2016 15:481.0Methylene chloride 2.0U
1ug/L 05-Oct-2016 15:480.30o-Xylene 1.0U
1ug/L 05-Oct-2016 15:480.30Styrene 1.0U
1ug/L 05-Oct-2016 15:480.30Tetrachloroethene 1.0U
1ug/L 05-Oct-2016 15:480.20Toluene 1.0U
1ug/L 05-Oct-2016 15:480.20trans-1,2-Dichloroethene 1.0U
1ug/L 05-Oct-2016 15:480.20trans-1,3-Dichloropropene 1.0U
1ug/L 05-Oct-2016 15:480.20Trichloroethene 1.0U
1ug/L 05-Oct-2016 15:480.30Trichlorofluoromethane 1.0U
1ug/L 05-Oct-2016 15:480.20Vinyl chloride 1.0U
1ug/L 05-Oct-2016 15:480.50Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 05-Oct-2016 15:4899.7 71-125
Surr: 4-Bromofluorobenzene 1%REC 05-Oct-2016 15:4888.0 70-125
Surr: Dibromofluoromethane 1%REC 05-Oct-2016 15:4874.4 74-125
Surr: Toluene-d8 1%REC 05-Oct-2016 15:48103 75-125
06-Oct-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 15 of 30
Client:City of CamdentonGolder Associates
WorkOrder:Project:
HS16091367DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID TCLP Date DF
Batch ID R282565 Test Name : LOW LEVEL VOLATILES BY SW8260C Matrix: Water
05 Oct 2016 14:30HS16091367-01 28 Sep 2016 11:30 1Mulberry Well (437-472)
05 Oct 2016 12:21HS16091367-02 27 Sep 2016 18:35 1Mulberry Well (564-598)
05 Oct 2016 14:56HS16091367-03 27 Sep 2016 14:08 1Mulberry Well (532-567)
05 Oct 2016 15:22HS16091367-04 27 Sep 2016 11:00 1Mulberry Well (511-546)
05 Oct 2016 14:05HS16091367-05 26 Sep 2016 18:25 10Mulberry Well (395-429)
05 Oct 2016 12:47HS16091367-05 26 Sep 2016 18:25 1Mulberry Well (395-429)
05 Oct 2016 15:48HS16091367-06 28 Sep 2016 00:00 1Trip Blank
06-Oct-16Date: ALS Group USA, Corp
Page 16 of 30
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16091367
QC BATCH REPORT
Batch ID: R282565 Instrument: VOA4 Method: SW8260
Sample ID: VBLKW-161005 Units: ug/L Analysis Date: 05-Oct-2016 11:30
Run ID: VOA4_282565 SeqNo: 3849954 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MBLK
Client ID:
1,1,1-Trichloroethane U 1.0
1,1,2,2-Tetrachloroethane U 1.0
1,1,2-Trichlor-1,2,2-trifluoroethane U 1.0
1,1,2-Trichloroethane U 1.0
1,1-Dichloroethane U 1.0
1,1-Dichloroethene U 1.0
1,2,4-Trichlorobenzene U 1.0
1,2-Dibromo-3-chloropropane U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichlorobenzene U 1.0
1,2-Dichloroethane U 1.0
1,2-Dichloropropane U 1.0
1,3-Dichlorobenzene U 1.0
1,4-Dichlorobenzene U 1.0
2-Butanone U 2.0
2-Hexanone U 2.0
4-Methyl-2-pentanone U 2.0
Acetone U 2.0
Benzene U 1.0
Bromodichloromethane U 1.0
Bromoform U 1.0
Bromomethane U 1.0
Carbon disulfide U 2.0
Carbon tetrachloride U 1.0
Chlorobenzene U 1.0
Chloroethane U 1.0
Chloroform U 1.0
Chloromethane U 1.0
cis-1,2-Dichloroethene U 1.0
cis-1,3-Dichloropropene U 1.0
Cyclohexane U 1.0
Dibromochloromethane U 1.0
Dichlorodifluoromethane U 1.0
Ethylbenzene U 1.0
ALS Group USA, Corp Date: 06-Oct-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 17 of 30
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16091367
QC BATCH REPORT
Batch ID: R282565 Instrument: VOA4 Method: SW8260
Sample ID: VBLKW-161005 Units: ug/L Analysis Date: 05-Oct-2016 11:30
Run ID: VOA4_282565 SeqNo: 3849954 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MBLK
Client ID:
Isopropylbenzene U 1.0
m,p-Xylene U 2.0
Methyl acetate U 1.0
Methyl tert-butyl ether U 1.0
Methylcyclohexane U 1.0
Methylene chloride U 2.0
o-Xylene U 1.0
Styrene U 1.0
Tetrachloroethene U 1.0
Toluene U 1.0
trans-1,2-Dichloroethene U 1.0
trans-1,3-Dichloropropene U 1.0
Trichloroethene U 1.0
Trichlorofluoromethane U 1.0
Vinyl chloride U 1.0
Xylenes, Total U 3.0
47.8 50 0 95.6 71 - 1251.0Surr: 1,2-Dichloroethane-d4
44.48 50 0 89.0 70 - 1251.0Surr: 4-Bromofluorobenzene
48.62 50 0 97.2 74 - 1251.0Surr: Dibromofluoromethane
51.05 50 0 102 75 - 1251.0Surr: Toluene-d8
ALS Group USA, Corp Date: 06-Oct-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 18 of 30
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16091367
QC BATCH REPORT
Batch ID: R282565 Instrument: VOA4 Method: SW8260
Sample ID: VLCSW-161005 Units: ug/L Analysis Date: 05-Oct-2016 10:13
Run ID: VOA4_282565 SeqNo: 3849953 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
LCS
Client ID:
1,1,1-Trichloroethane 57.99 50 0 116 75 - 1301.0
1,1,2,2-Tetrachloroethane 43.19 50 0 86.4 74 - 1231.0
1,1,2-Trichlor-1,2,2-trifluoroethane 59.79 50 0 120 70 - 1301.0
1,1,2-Trichloroethane 50.38 50 0 101 80 - 1201.0
1,1-Dichloroethane 53.88 50 0 108 76 - 1201.0
1,1-Dichloroethene 56.45 50 0 113 75 - 1301.0
1,2,4-Trichlorobenzene 51.99 50 0 104 75 - 1261.0
1,2-Dibromo-3-chloropropane 52.09 50 0 104 65 - 1251.0
1,2-Dibromoethane 54.35 50 0 109 80 - 1211.0
1,2-Dichlorobenzene 49.95 50 0 99.9 80 - 1201.0
1,2-Dichloroethane 52.65 50 0 105 76 - 1201.0
1,2-Dichloropropane 51.56 50 0 103 80 - 1201.0
1,3-Dichlorobenzene 52.16 50 0 104 80 - 1201.0
1,4-Dichlorobenzene 49.23 50 0 98.5 80 - 1201.0
2-Butanone 109.3 100 0 109 60 - 1402.0
2-Hexanone 115.4 100 0 115 60 - 1312.0
4-Methyl-2-pentanone 96.73 100 0 96.7 60 - 1352.0
Acetone 97.46 100 0 97.5 60 - 1402.0
Benzene 55.06 50 0 110 75 - 1221.0
Bromodichloromethane 56.31 50 0 113 75 - 1251.0
Bromoform 53.48 50 0 107 70 - 1301.0
Bromomethane 55.77 50 0 112 60 - 1401.0
Carbon disulfide 112.4 100 0 112 70 - 1302.0
Carbon tetrachloride 54.02 50 0 108 75 - 1251.0
Chlorobenzene 50.85 50 0 102 80 - 1201.0
Chloroethane 54.74 50 0 109 70 - 1301.0
Chloroform 51.61 50 0 103 70 - 1301.0
Chloromethane 55.26 50 0 111 65 - 1301.0
cis-1,2-Dichloroethene 54.71 50 0 109 75 - 1251.0
cis-1,3-Dichloropropene 62.7 50 0 125 79 - 125 S 1.0
Cyclohexane 55.88 50 0 112 70 - 1301.0
Dibromochloromethane 53.14 50 0 106 70 - 1301.0
Dichlorodifluoromethane 60.6 50 0 121 60 - 1401.0
Ethylbenzene 54.83 50 0 110 80 - 1201.0
ALS Group USA, Corp Date: 06-Oct-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 19 of 30
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16091367
QC BATCH REPORT
Batch ID: R282565 Instrument: VOA4 Method: SW8260
Sample ID: VLCSW-161005 Units: ug/L Analysis Date: 05-Oct-2016 10:13
Run ID: VOA4_282565 SeqNo: 3849953 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
LCS
Client ID:
Isopropylbenzene 58.67 50 0 117 75 - 1301.0
m,p-Xylene 111.1 100 0 111 80 - 1202.0
Methyl acetate 53.76 50 0 108 76 - 1221.0
Methyl tert-butyl ether 56.73 50 0 113 70 - 1301.0
Methylcyclohexane 66.82 50 0 134 70 - 126 S 1.0
Methylene chloride 50.09 50 0 100 65 - 1332.0
o-Xylene 54.51 50 0 109 80 - 1201.0
Styrene 57.58 50 0 115 78 - 1221.0
Tetrachloroethene 53.84 50 0 108 75 - 1301.0
Toluene 52.73 50 0 105 75 - 1211.0
trans-1,2-Dichloroethene 55.89 50 0 112 75 - 1251.0
trans-1,3-Dichloropropene 50.1 50 0 100 76 - 1251.0
Trichloroethene 55.46 50 0 111 71 - 1251.0
Trichlorofluoromethane 58.05 50 0 116 67 - 1321.0
Vinyl chloride 55.55 50 0 111 70 - 1351.0
Xylenes, Total 165.6 150 0 110 79 - 1243.0
46.52 50 0 93.0 71 - 1251.0Surr: 1,2-Dichloroethane-d4
49.14 50 0 98.3 70 - 1251.0Surr: 4-Bromofluorobenzene
49.02 50 0 98.0 74 - 1251.0Surr: Dibromofluoromethane
50.96 50 0 102 75 - 1251.0Surr: Toluene-d8
ALS Group USA, Corp Date: 06-Oct-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 20 of 30
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16091367
QC BATCH REPORT
Batch ID: R282565 Instrument: VOA4 Method: SW8260
Sample ID: HS16091367-02MS Units: ug/L Analysis Date: 05-Oct-2016 13:13
Run ID: VOA4_282565 SeqNo: 3849958 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MS
Client ID: Mulberry Well (564-598)
1,1,1-Trichloroethane 59.37 50 0 119 75 - 1301.0
1,1,2,2-Tetrachloroethane 0.978 50 0 1.96 74 - 123 JS 1.0
1,1,2-Trichlor-1,2,2-trifluoroethane 65.78 50 0 132 70 - 130 S 1.0
1,1,2-Trichloroethane 46.34 50 0 92.7 80 - 1201.0
1,1-Dichloroethane 53.35 50 0 107 76 - 1201.0
1,1-Dichloroethene 62.89 50 0 126 75 - 1301.0
1,2,4-Trichlorobenzene 48.71 50 0 97.4 75 - 1261.0
1,2-Dibromo-3-chloropropane 45.39 50 0 90.8 65 - 1251.0
1,2-Dibromoethane 53.24 50 0 106 80 - 1211.0
1,2-Dichlorobenzene 47.55 50 0 95.1 80 - 1201.0
1,2-Dichloroethane 51.43 50 0 103 76 - 1201.0
1,2-Dichloropropane 50.57 50 0 101 80 - 1201.0
1,3-Dichlorobenzene 51.29 50 0 103 80 - 1201.0
1,4-Dichlorobenzene 47.45 50 0 94.9 80 - 1201.0
2-Butanone 111.3 100 0 111 60 - 1402.0
2-Hexanone 111.8 100 0 112 60 - 1312.0
4-Methyl-2-pentanone 94.67 100 0 94.7 60 - 1352.0
Acetone 96.42 100 0 96.4 60 - 1402.0
Benzene 54.77 50 0 110 75 - 1221.0
Bromodichloromethane 52.46 50 0 105 75 - 1251.0
Bromoform 51.75 50 0 104 70 - 1301.0
Bromomethane 53.88 50 0 108 60 - 1401.0
Carbon disulfide 116.5 100 0 116 70 - 1302.0
Carbon tetrachloride 54.85 50 0 110 79 - 1201.0
Chlorobenzene 49.76 50 0 99.5 80 - 1201.0
Chloroethane 54.94 50 0 110 70 - 1301.0
Chloroform 51.92 50 0 104 70 - 1301.0
Chloromethane 55.54 50 0 111 65 - 1301.0
cis-1,2-Dichloroethene 58.44 50 3.228 110 75 - 1251.0
cis-1,3-Dichloropropene 57.43 50 0 115 79 - 1251.0
Cyclohexane 60.91 50 0 122 70 - 1301.0
Dibromochloromethane 50.47 50 0 101 70 - 1301.0
Dichlorodifluoromethane 65.02 50 0 130 60 - 1401.0
Ethylbenzene 55.92 50 0 112 80 - 1201.0
ALS Group USA, Corp Date: 06-Oct-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 21 of 30
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16091367
QC BATCH REPORT
Batch ID: R282565 Instrument: VOA4 Method: SW8260
Sample ID: HS16091367-02MS Units: ug/L Analysis Date: 05-Oct-2016 13:13
Run ID: VOA4_282565 SeqNo: 3849958 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MS
Client ID: Mulberry Well (564-598)
Isopropylbenzene 59.79 50 0 120 75 - 1301.0
m,p-Xylene 112.4 100 0 112 80 - 1202.0
Methyl acetate U 50 0 0 76 - 122 S 1.0
Methyl tert-butyl ether 54.17 50 0 108 70 - 1301.0
Methylcyclohexane 70.3 50 0 141 70 - 126 S 1.0
Methylene chloride 50.19 50 0 100 65 - 1332.0
o-Xylene 55.27 50 0 111 80 - 1201.0
Styrene 56.49 50 0 113 78 - 1221.0
Tetrachloroethene 58.34 50 0 117 75 - 1301.0
Toluene 56.2 50 1.767 109 75 - 1211.0
trans-1,2-Dichloroethene 58.01 50 0 116 75 - 1251.0
trans-1,3-Dichloropropene 45.63 50 0 91.3 76 - 1251.0
Trichloroethene 155.8 50 52.25 207 71 - 125 S 1.0
Trichlorofluoromethane 62.87 50 0 126 67 - 1321.0
Vinyl chloride 61.01 50 0 122 70 - 1351.0
Xylenes, Total 167.7 150 0 112 80 - 1243.0
49.59 50 0 99.2 71 - 1251.0Surr: 1,2-Dichloroethane-d4
50.06 50 0 100 70 - 1251.0Surr: 4-Bromofluorobenzene
41.81 50 0 83.6 74 - 1251.0Surr: Dibromofluoromethane
52.24 50 0 104 75 - 1251.0Surr: Toluene-d8
ALS Group USA, Corp Date: 06-Oct-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 22 of 30
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16091367
QC BATCH REPORT
Batch ID: R282565 Instrument: VOA4 Method: SW8260
Sample ID: HS16091367-02MSD Units: ug/L Analysis Date: 05-Oct-2016 13:39
Run ID: VOA4_282565 SeqNo: 3849959 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MSD
Client ID: Mulberry Well (564-598)
1,1,1-Trichloroethane 58.28 50 0 117 75 - 130 59.37 1.85 201.0
1,1,2,2-Tetrachloroethane 1.003 50 0 2.01 74 - 123 0.978 2.51 20 S 1.0
1,1,2-Trichlor-1,2,2-trifluoroethane 61.91 50 0 124 70 - 130 65.78 6.06 201.0
1,1,2-Trichloroethane 42.77 50 0 85.5 80 - 120 46.34 8.02 201.0
1,1-Dichloroethane 50.73 50 0 101 76 - 120 53.35 5.02 201.0
1,1-Dichloroethene 64.02 50 0 128 75 - 130 62.89 1.78 201.0
1,2,4-Trichlorobenzene 50.99 50 0 102 75 - 126 48.71 4.56 201.0
1,2-Dibromo-3-chloropropane 49.02 50 0 98.0 65 - 125 45.39 7.68 201.0
1,2-Dibromoethane 49.8 50 0 99.6 80 - 121 53.24 6.67 201.0
1,2-Dichlorobenzene 48.46 50 0 96.9 80 - 120 47.55 1.91 201.0
1,2-Dichloroethane 48.52 50 0 97.0 76 - 120 51.43 5.83 201.0
1,2-Dichloropropane 48.16 50 0 96.3 80 - 120 50.57 4.89 201.0
1,3-Dichlorobenzene 51.67 50 0 103 80 - 120 51.29 0.74 201.0
1,4-Dichlorobenzene 48.13 50 0 96.3 80 - 120 47.45 1.43 201.0
2-Butanone 112.4 100 0 112 60 - 140 111.3 0.958 202.0
2-Hexanone 113.3 100 0 113 60 - 131 111.8 1.38 202.0
4-Methyl-2-pentanone 94.26 100 0 94.3 60 - 135 94.67 0.436 202.0
Acetone 97.28 100 0 97.3 60 - 140 96.42 0.887 202.0
Benzene 53.35 50 0 107 75 - 122 54.77 2.64 201.0
Bromodichloromethane 50.1 50 0 100 75 - 125 52.46 4.61 201.0
Bromoform 50.91 50 0 102 70 - 130 51.75 1.65 201.0
Bromomethane 52.18 50 0 104 60 - 140 53.88 3.2 201.0
Carbon disulfide 111.8 100 0 112 70 - 130 116.5 4.08 202.0
Carbon tetrachloride 52.86 50 0 106 75 - 125 54.85 3.69 201.0
Chlorobenzene 48.02 50 0 96.0 80 - 120 49.76 3.56 201.0
Chloroethane 54.65 50 0 109 70 - 130 54.94 0.545 201.0
Chloroform 49.98 50 0 100.0 70 - 130 51.92 3.8 201.0
Chloromethane 53.93 50 0 108 65 - 130 55.54 2.94 201.0
cis-1,2-Dichloroethene 56.12 50 3.228 106 75 - 125 58.44 4.05 201.0
cis-1,3-Dichloropropene 56.1 50 0 112 79 - 125 57.43 2.34 201.0
Cyclohexane 58.33 50 0 117 70 - 130 60.91 4.31 201.0
Dibromochloromethane 48.23 50 0 96.5 70 - 130 50.47 4.54 201.0
Dichlorodifluoromethane 63.21 50 0 126 60 - 140 65.02 2.81 201.0
Ethylbenzene 53.84 50 0 108 80 - 120 55.92 3.79 201.0
ALS Group USA, Corp Date: 06-Oct-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 23 of 30
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16091367
QC BATCH REPORT
Batch ID: R282565 Instrument: VOA4 Method: SW8260
Sample ID: HS16091367-02MSD Units: ug/L Analysis Date: 05-Oct-2016 13:39
Run ID: VOA4_282565 SeqNo: 3849959 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MSD
Client ID: Mulberry Well (564-598)
Isopropylbenzene 58.2 50 0 116 75 - 130 59.79 2.69 201.0
m,p-Xylene 106.6 100 0 107 80 - 120 112.4 5.31 202.0
Methyl acetate U 50 0 0 76 - 122 0 0 20 S 1.0
Methyl tert-butyl ether 53.32 50 0 107 70 - 130 54.17 1.58 201.0
Methylcyclohexane 67.83 50 0 136 70 - 126 70.3 3.58 20 S 1.0
Methylene chloride 48.84 50 0 97.7 65 - 133 50.19 2.74 202.0
o-Xylene 52.13 50 0 104 80 - 120 55.27 5.85 201.0
Styrene 55.03 50 0 110 78 - 122 56.49 2.62 201.0
Tetrachloroethene 54.44 50 0 109 75 - 130 58.34 6.92 201.0
Toluene 53.51 50 1.767 103 75 - 121 56.2 4.89 201.0
trans-1,2-Dichloroethene 55.52 50 0 111 75 - 125 58.01 4.39 201.0
trans-1,3-Dichloropropene 46.07 50 0 92.1 76 - 125 45.63 0.949 201.0
Trichloroethene 151.3 50 52.25 198 71 - 125 155.8 2.94 20 S 1.0
Trichlorofluoromethane 59.81 50 0 120 67 - 132 62.87 4.98 201.0
Vinyl chloride 58.84 50 0 118 70 - 135 61.01 3.62 201.0
Xylenes, Total 158.7 150 0 106 80 - 124 167.7 5.49 203.0
47.76 50 0 95.5 71 - 125 49.59 3.77 201.0Surr: 1,2-Dichloroethane-d4
49.01 50 0 98.0 70 - 125 50.06 2.13 201.0Surr: 4-Bromofluorobenzene
40.32 50 0 80.6 74 - 125 41.81 3.63 201.0Surr: Dibromofluoromethane
51.34 50 0 103 75 - 125 52.24 1.73 201.0Surr: Toluene-d8
The following samples were analyzed in this batch: HS16091367-01 HS16091367-02 HS16091367-03 HS16091367-04 HS16091367-05 HS16091367-06
ALS Group USA, Corp Date: 06-Oct-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 24 of 30
QUALIFIERS, ACRONYMS, UNITS
Client:Project:WorkOrder:
Golder AssociatesCity of CamdentonHS16091367
Qualifier Description* Value exceeds Regulatory Limit
a Not accredited
B Analyte detected in the associated Method Blank above the Reporting Limit
E Value above quantitation range
H Analyzed outside of Holding Time
J Analyte detected below quantitation limit
M Manually integrated, see raw data for justification
n Not offered for accreditation
ND Not Detected at the Reporting Limit
O Sample amount is > 4 times amount spiked
P Dual Column results percent difference > 40%
R RPD above laboratory control limit
S Spike Recovery outside laboratory control limits
U Analyzed but not detected above the MDL/SDL
Acronym DescriptionDCS Detectability Check Study
DUP Method Duplicate
LCS Laboratory Control Sample
LCSD Laboratory Control Sample Duplicate
MBLK Method Blank
MDL Method Detection Limit
MQL Method Quantitation Limit
MS Matrix Spike
MSD Matrix Spike Duplicate
PDS Post Digestion Spike
PQL Practical Quantitaion Limit
SD Serial Dilution
SDL Sample Detection Limit
TRRP Texas Risk Reduction Program
Unit Reported Descriptionµg/L Micrograms per Liter
ALS Group USA, Corp Date: 06-Oct-16
Page 25 of 30
CERTIFICATIONS,ACCREDITATIONS & LICENSES
Agency Number Expire Date
Arkansas 16-022-1 27-Mar-2017
California 2919 2016-2018 31-Jul-2018
Illinois 003872 09-May-2017
Kansas E-10352 2015-2016 30-Oct-2016
Kentucky 96 2016-2017 30-Apr-2017
Louisiana 03087 2016-2017 30-Jun-2017
North Carolina 624 - 2016 31-Dec-2016
North Dakota R193 2016-2017 30-Apr-2017
Oklahoma 2016-122 31-Aug-2017
Texas TX104704231-16-17 30-Apr-2017
06-Oct-16Date: ALS Group USA, Corp
Page 26 of 30
Client: Golder Associates
Work Order: HS16091367Project: City of Camdenton SAMPLE TRACKING
Lab Samp ID Client Sample ID Action Date Person New Location
HS16091367-01 Mulberry Well (437-472) Login 9/29/2016 11:43:32 AM JRM VW-3
HS16091367-02 Mulberry Well (564-598) Login 9/29/2016 11:43:32 AM JRM VW-3
HS16091367-03 Mulberry Well (532-567) Login 9/29/2016 11:43:32 AM JRM VW-3
HS16091367-04 Mulberry Well (511-546) Login 9/29/2016 11:43:33 AM JRM VW-3
HS16091367-05 Mulberry Well (395-429) Login 9/29/2016 11:43:33 AM JRM VW-3
HS16091367-06 Trip Blank Login 9/29/2016 11:43:33 AM JRM VW-3
ALS Group USA, Corp 06-Oct-16Date:
Page 27 of 30
RPG
29-Sep-2016 08:20Date/Time Received:
HS16091367
Golder St Louis
Work Order:
Client Name:
Sample Receipt Checklist
Received by:
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
Container/Temp Blank temperature in compliance?
Temperature(s)/Thermometer(s):
Cooler(s)/Kit(s):
Date/Time sample(s) sent to storage:
Water - VOA vials have zero headspace?
Water - pH acceptable upon receipt?
pH adjusted?
pH adjusted by:
Login Notes:
No Not Present
Yes No Not Present
Yes No Not Present
Yes No
Yes No
Yes No
Yes No
Yes No
Yes No
Yes No
Yes No
1.3c/2.0c UC/C IR11White09/29/2016 11:45
Yes No No VOA vials submitted
Yes No N/A
Yes No N/A
Checklist completed by: Jared R. MakanDateeSignatureDateeSignature
3-Oct-201629-Sep-2016
FedExWater Carrier name:Matrices:
Reviewed by: Dane J. Wacasey
Client Contacted: Date Contacted: Person Contacted:
Contacted By: Regarding:
Comments:
Corrective Action:
Yes
NoYesTX1005 solids received in hermetically sealed vials? N/A
ALS Group USA, Corp 06-Oct-16Date:
Page 28 of 30
Page 29 of 30
Page 30 of 30
November 07, 2016
Anne Faeth-BoydGolder Associates820 South Main St.Suite 100St Charles, MO 63301
The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Results are expressed as "as received" unless otherwise noted.
QC sample results for this data met EPA or laboratory specifications except as noted in the Case Narrative or as noted with qualifiers in the QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained by ALS Environmental. Samples will be disposed in 30 days unless storage arrangements are made.
If you have any questions regarding this report, please feel free to call me.
Sincerely,
ALS Environmental received 7 sample(s) on Oct 29, 2016 for the analysis presented in the following report.
Laboratory Results for: City of Camdenton
Dear Anne,
Work Order: HS16101339
Generated By: Jumoke.Lawal
Dane J. Wacasey
10450 Stancliff Rd. Suite 210 Houston, TX 77099 T: +1 281 530 5656 F: +1 281 530 5887 www.alsglobal.com
Page 1 of 47
Client: Golder Associates
Work Order: HS16101339Project: City of Camdenton SAMPLE SUMMARY
Lab Samp ID Client Sample ID Collection DateMatrix TagNo Date Received Hold
HS16101339-01 25-Oct-2016 16:30 29-Oct-2016 09:30MWPT-1 Water
HS16101339-02 25-Oct-2016 00:00 29-Oct-2016 09:30DUP-1 Water
HS16101339-03 27-Oct-2016 16:00 29-Oct-2016 09:30MWPT-3 Water
HS16101339-04 27-Oct-2016 16:00 29-Oct-2016 09:30FB-1 Water
HS16101339-05 28-Oct-2016 11:30 29-Oct-2016 09:30MWPT-4 Water
HS16101339-06 28-Oct-2016 13:05 29-Oct-2016 09:30RB-1 Water
HS16101339-07 25-Oct-2016 00:00 29-Oct-2016 09:30TRIP BLANK Water
ALS Group USA, Corp 07-Nov-16Date:
Page 2 of 47
Client: CASE NARRATIVE
Work Order:City of CamdentonGolder Associates
Project:HS16101339
GCMS Volatiles by Method SW8260
Batch ID: R283946Sample ID: HS16101295-03MS
MS and MSD are for an unrelated sample•
Batch ID: R283975
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
Metals by Method M2340 B
Batch ID: R284356
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
Metals by Method SW7470
Batch ID: 109499Sample ID: HS16110059-01MS
MS and MSD are for an unrelated sample•
Metals by Method SW6020
Batch ID: 109425Sample ID: HS16101322-10MS
MS/MSD and DUPs are for an unrelated sample•
WetChemistry by Method SW9060
Batch ID: R284304
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method SM2320B
Batch ID: R284076
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Group USA, Corp 07-Nov-16Date:
Page 3 of 47
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonMWPT-1
WorkOrder:Lab ID:
Collection Date:
HS16101339HS16101339-01
25-Oct-2016 16:30 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 31-Oct-2016 19:330.201,1,1-Trichloroethane 1.0U
1ug/L 31-Oct-2016 19:330.501,1,2,2-Tetrachloroethane 1.0U
1ug/L 31-Oct-2016 19:331.01,1,2-Trichlor-1,2,2-trifluoroethane 1.0U
1ug/L 31-Oct-2016 19:330.301,1,2-Trichloroethane 1.0U
1ug/L 31-Oct-2016 19:330.201,1-Dichloroethane 1.0U
1ug/L 31-Oct-2016 19:330.201,1-Dichloroethene 1.0U
1ug/L 31-Oct-2016 19:330.501,2,4-Trichlorobenzene 1.0U
1ug/L 31-Oct-2016 19:331.01,2-Dibromo-3-chloropropane 1.0U
1ug/L 31-Oct-2016 19:330.201,2-Dibromoethane 1.0U
1ug/L 31-Oct-2016 19:330.501,2-Dichlorobenzene 1.0U
1ug/L 31-Oct-2016 19:330.201,2-Dichloroethane 1.0U
1ug/L 31-Oct-2016 19:330.501,2-Dichloropropane 1.0U
1ug/L 31-Oct-2016 19:330.401,3-Dichlorobenzene 1.0U
1ug/L 31-Oct-2016 19:330.401,4-Dichlorobenzene 1.0U
1ug/L 31-Oct-2016 19:330.502-Butanone 2.0U
1ug/L 31-Oct-2016 19:331.02-Hexanone 2.0U
1ug/L 31-Oct-2016 19:330.704-Methyl-2-pentanone 2.0U
1ug/L 31-Oct-2016 19:332.0Acetone 2.0U
1ug/L 31-Oct-2016 19:330.20Benzene 1.0U
1ug/L 31-Oct-2016 19:330.20Bromodichloromethane 1.0U
1ug/L 31-Oct-2016 19:330.40Bromoform 1.0U
1ug/L 31-Oct-2016 19:330.40Bromomethane 1.0U
1ug/L 31-Oct-2016 19:330.60Carbon disulfide 2.0U
1ug/L 31-Oct-2016 19:330.50Carbon tetrachloride 1.0U
1ug/L 31-Oct-2016 19:330.30Chlorobenzene 1.0U
1ug/L 31-Oct-2016 19:330.30Chloroethane 1.0U
1ug/L 31-Oct-2016 19:330.20Chloroform 1.0U
1ug/L 31-Oct-2016 19:330.20Chloromethane 1.0U
1ug/L 31-Oct-2016 19:330.20cis-1,2-Dichloroethene 1.03.5
1ug/L 31-Oct-2016 19:330.10cis-1,3-Dichloropropene 1.0U
1ug/L 31-Oct-2016 19:330.30Cyclohexane 1.0U
1ug/L 31-Oct-2016 19:330.30Dibromochloromethane 1.0U
1ug/L 31-Oct-2016 19:330.30Dichlorodifluoromethane 1.0U
1ug/L 31-Oct-2016 19:330.30Ethylbenzene 1.0U
1ug/L 31-Oct-2016 19:330.30Isopropylbenzene 1.0U
1ug/L 31-Oct-2016 19:330.50m,p-Xylene 2.0U
1ug/L 31-Oct-2016 19:331.0Methyl acetate 1.0U
1ug/L 31-Oct-2016 19:330.20Methyl tert-butyl ether 1.0U
1ug/L 31-Oct-2016 19:330.30Methylcyclohexane 1.0U
07-Nov-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 4 of 47
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonMWPT-1
WorkOrder:Lab ID:
Collection Date:
HS16101339HS16101339-01
25-Oct-2016 16:30 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 31-Oct-2016 19:331.0Methylene chloride 2.0U
1ug/L 31-Oct-2016 19:330.30o-Xylene 1.0U
1ug/L 31-Oct-2016 19:330.30Styrene 1.0U
1ug/L 31-Oct-2016 19:330.30Tetrachloroethene 1.0U
1ug/L 31-Oct-2016 19:330.20Toluene 1.0U
1ug/L 31-Oct-2016 19:330.20trans-1,2-Dichloroethene 1.0U
1ug/L 31-Oct-2016 19:330.20trans-1,3-Dichloropropene 1.0U
1ug/L 31-Oct-2016 19:330.20Trichloroethene 1.058
1ug/L 31-Oct-2016 19:330.30Trichlorofluoromethane 1.0U
1ug/L 31-Oct-2016 19:330.20Vinyl chloride 1.0U
1ug/L 31-Oct-2016 19:330.50Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 31-Oct-2016 19:3397.8 71-125
Surr: 4-Bromofluorobenzene 1%REC 31-Oct-2016 19:3389.7 70-125
Surr: Dibromofluoromethane 1%REC 31-Oct-2016 19:3382.6 74-125
Surr: Toluene-d8 1%REC 31-Oct-2016 19:3398.1 75-125HARDNESS, TOTAL AS CACO3 BY SM2340B
Method:M2340 B Analyst: DQ
1mg/L 07-Nov-2016 15:302.00Hardness (As CaCO3) 2.00327
ICP-MS METALS BY SW6020A Method:SW6020 Analyst: JDEPrep:SW3010A / 01-Nov-2016
1mg/L 04-Nov-2016 18:070.000400Arsenic 0.00500U
1mg/L 04-Nov-2016 18:070.00190Barium 0.005000.0489
1mg/L 04-Nov-2016 18:070.000200Cadmium 0.00200U
1mg/L 04-Nov-2016 18:070.0340Calcium 0.50067.6
1mg/L 04-Nov-2016 18:070.000400Chromium 0.00500U
1mg/L 04-Nov-2016 18:07J 0.000600Lead 0.005000.00399
1mg/L 04-Nov-2016 18:070.0100Magnesium 0.20038.5
1mg/L 04-Nov-2016 18:070.00110Selenium 0.00500U
1mg/L 04-Nov-2016 18:070.000200Silver 0.00500U
MERCURY BY SW7470A Method:SW7470 Analyst: JCJPrep:SW7470 / 03-Nov-2016
1mg/L 03-Nov-2016 15:270.0000400Mercury 0.000200U
ALKALINITY BY SM2320B Method:SM2320B Analyst: KMU1mg/L 02-Nov-2016 11:075.00Alkalinity, Bicarbonate (As
CaCO3)5.00324
1mg/L 02-Nov-2016 11:075.00Alkalinity, Carbonate (As CaCO3) 5.00U
1mg/L 02-Nov-2016 11:075.00Alkalinity, Hydroxide (As CaCO3) 5.00U
1mg/L 02-Nov-2016 11:075.00Alkalinity, Total (As CaCO3) 5.00324
TOTAL ORGANIC CARBON BY SW9060A Method:SW9060 Analyst: KMU1mg/L 06-Nov-2016 17:230.500Organic Carbon, Total 1.00U
07-Nov-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 5 of 47
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonDUP-1
WorkOrder:Lab ID:
Collection Date:
HS16101339HS16101339-02
25-Oct-2016 00:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 31-Oct-2016 19:580.201,1,1-Trichloroethane 1.0U
1ug/L 31-Oct-2016 19:580.501,1,2,2-Tetrachloroethane 1.0U
1ug/L 31-Oct-2016 19:581.01,1,2-Trichlor-1,2,2-trifluoroethane 1.0U
1ug/L 31-Oct-2016 19:580.301,1,2-Trichloroethane 1.0U
1ug/L 31-Oct-2016 19:580.201,1-Dichloroethane 1.0U
1ug/L 31-Oct-2016 19:580.201,1-Dichloroethene 1.0U
1ug/L 31-Oct-2016 19:580.501,2,4-Trichlorobenzene 1.0U
1ug/L 31-Oct-2016 19:581.01,2-Dibromo-3-chloropropane 1.0U
1ug/L 31-Oct-2016 19:580.201,2-Dibromoethane 1.0U
1ug/L 31-Oct-2016 19:580.501,2-Dichlorobenzene 1.0U
1ug/L 31-Oct-2016 19:580.201,2-Dichloroethane 1.0U
1ug/L 31-Oct-2016 19:580.501,2-Dichloropropane 1.0U
1ug/L 31-Oct-2016 19:580.401,3-Dichlorobenzene 1.0U
1ug/L 31-Oct-2016 19:580.401,4-Dichlorobenzene 1.0U
1ug/L 31-Oct-2016 19:580.502-Butanone 2.0U
1ug/L 31-Oct-2016 19:581.02-Hexanone 2.0U
1ug/L 31-Oct-2016 19:580.704-Methyl-2-pentanone 2.0U
1ug/L 31-Oct-2016 19:582.0Acetone 2.0U
1ug/L 31-Oct-2016 19:580.20Benzene 1.0U
1ug/L 31-Oct-2016 19:580.20Bromodichloromethane 1.0U
1ug/L 31-Oct-2016 19:580.40Bromoform 1.0U
1ug/L 31-Oct-2016 19:580.40Bromomethane 1.0U
1ug/L 31-Oct-2016 19:580.60Carbon disulfide 2.0U
1ug/L 31-Oct-2016 19:580.50Carbon tetrachloride 1.0U
1ug/L 31-Oct-2016 19:580.30Chlorobenzene 1.0U
1ug/L 31-Oct-2016 19:580.30Chloroethane 1.0U
1ug/L 31-Oct-2016 19:580.20Chloroform 1.0U
1ug/L 31-Oct-2016 19:580.20Chloromethane 1.0U
1ug/L 31-Oct-2016 19:580.20cis-1,2-Dichloroethene 1.03.0
1ug/L 31-Oct-2016 19:580.10cis-1,3-Dichloropropene 1.0U
1ug/L 31-Oct-2016 19:580.30Cyclohexane 1.0U
1ug/L 31-Oct-2016 19:580.30Dibromochloromethane 1.0U
1ug/L 31-Oct-2016 19:580.30Dichlorodifluoromethane 1.0U
1ug/L 31-Oct-2016 19:580.30Ethylbenzene 1.0U
1ug/L 31-Oct-2016 19:580.30Isopropylbenzene 1.0U
1ug/L 31-Oct-2016 19:580.50m,p-Xylene 2.0U
1ug/L 31-Oct-2016 19:581.0Methyl acetate 1.0U
1ug/L 31-Oct-2016 19:580.20Methyl tert-butyl ether 1.0U
1ug/L 31-Oct-2016 19:580.30Methylcyclohexane 1.0U
07-Nov-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 6 of 47
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonDUP-1
WorkOrder:Lab ID:
Collection Date:
HS16101339HS16101339-02
25-Oct-2016 00:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 31-Oct-2016 19:581.0Methylene chloride 2.0U
1ug/L 31-Oct-2016 19:580.30o-Xylene 1.0U
1ug/L 31-Oct-2016 19:580.30Styrene 1.0U
1ug/L 31-Oct-2016 19:580.30Tetrachloroethene 1.0U
1ug/L 31-Oct-2016 19:580.20Toluene 1.0U
1ug/L 31-Oct-2016 19:580.20trans-1,2-Dichloroethene 1.0U
1ug/L 31-Oct-2016 19:580.20trans-1,3-Dichloropropene 1.0U
1ug/L 31-Oct-2016 19:580.20Trichloroethene 1.058
1ug/L 31-Oct-2016 19:580.30Trichlorofluoromethane 1.0U
1ug/L 31-Oct-2016 19:580.20Vinyl chloride 1.0U
1ug/L 31-Oct-2016 19:580.50Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 31-Oct-2016 19:5895.2 71-125
Surr: 4-Bromofluorobenzene 1%REC 31-Oct-2016 19:5890.1 70-125
Surr: Dibromofluoromethane 1%REC 31-Oct-2016 19:5884.9 74-125
Surr: Toluene-d8 1%REC 31-Oct-2016 19:5898.7 75-125
07-Nov-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 7 of 47
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonMWPT-3
WorkOrder:Lab ID:
Collection Date:
HS16101339HS16101339-03
27-Oct-2016 16:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 31-Oct-2016 20:230.201,1,1-Trichloroethane 1.0U
1ug/L 31-Oct-2016 20:230.501,1,2,2-Tetrachloroethane 1.0U
1ug/L 31-Oct-2016 20:231.01,1,2-Trichlor-1,2,2-trifluoroethane 1.0U
1ug/L 31-Oct-2016 20:230.301,1,2-Trichloroethane 1.0U
1ug/L 31-Oct-2016 20:230.201,1-Dichloroethane 1.0U
1ug/L 31-Oct-2016 20:230.201,1-Dichloroethene 1.0U
1ug/L 31-Oct-2016 20:230.501,2,4-Trichlorobenzene 1.0U
1ug/L 31-Oct-2016 20:231.01,2-Dibromo-3-chloropropane 1.0U
1ug/L 31-Oct-2016 20:230.201,2-Dibromoethane 1.0U
1ug/L 31-Oct-2016 20:230.501,2-Dichlorobenzene 1.0U
1ug/L 31-Oct-2016 20:230.201,2-Dichloroethane 1.0U
1ug/L 31-Oct-2016 20:230.501,2-Dichloropropane 1.0U
1ug/L 31-Oct-2016 20:230.401,3-Dichlorobenzene 1.0U
1ug/L 31-Oct-2016 20:230.401,4-Dichlorobenzene 1.0U
1ug/L 31-Oct-2016 20:230.502-Butanone 2.0U
1ug/L 31-Oct-2016 20:231.02-Hexanone 2.0U
1ug/L 31-Oct-2016 20:230.704-Methyl-2-pentanone 2.0U
1ug/L 31-Oct-2016 20:232.0Acetone 2.0U
1ug/L 31-Oct-2016 20:230.20Benzene 1.0U
1ug/L 31-Oct-2016 20:230.20Bromodichloromethane 1.0U
1ug/L 31-Oct-2016 20:230.40Bromoform 1.0U
1ug/L 31-Oct-2016 20:230.40Bromomethane 1.0U
1ug/L 31-Oct-2016 20:230.60Carbon disulfide 2.0U
1ug/L 31-Oct-2016 20:230.50Carbon tetrachloride 1.0U
1ug/L 31-Oct-2016 20:230.30Chlorobenzene 1.0U
1ug/L 31-Oct-2016 20:230.30Chloroethane 1.0U
1ug/L 31-Oct-2016 20:230.20Chloroform 1.0U
1ug/L 31-Oct-2016 20:230.20Chloromethane 1.0U
1ug/L 31-Oct-2016 20:230.20cis-1,2-Dichloroethene 1.03.3
1ug/L 31-Oct-2016 20:230.10cis-1,3-Dichloropropene 1.0U
1ug/L 31-Oct-2016 20:230.30Cyclohexane 1.0U
1ug/L 31-Oct-2016 20:230.30Dibromochloromethane 1.0U
1ug/L 31-Oct-2016 20:230.30Dichlorodifluoromethane 1.0U
1ug/L 31-Oct-2016 20:230.30Ethylbenzene 1.0U
1ug/L 31-Oct-2016 20:230.30Isopropylbenzene 1.0U
1ug/L 31-Oct-2016 20:230.50m,p-Xylene 2.0U
1ug/L 31-Oct-2016 20:231.0Methyl acetate 1.0U
1ug/L 31-Oct-2016 20:230.20Methyl tert-butyl ether 1.0U
1ug/L 31-Oct-2016 20:230.30Methylcyclohexane 1.0U
07-Nov-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 8 of 47
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonMWPT-3
WorkOrder:Lab ID:
Collection Date:
HS16101339HS16101339-03
27-Oct-2016 16:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 31-Oct-2016 20:231.0Methylene chloride 2.0U
1ug/L 31-Oct-2016 20:230.30o-Xylene 1.0U
1ug/L 31-Oct-2016 20:230.30Styrene 1.0U
1ug/L 31-Oct-2016 20:230.30Tetrachloroethene 1.0U
1ug/L 31-Oct-2016 20:230.20Toluene 1.0U
1ug/L 31-Oct-2016 20:230.20trans-1,2-Dichloroethene 1.0U
1ug/L 31-Oct-2016 20:230.20trans-1,3-Dichloropropene 1.0U
1ug/L 31-Oct-2016 20:230.20Trichloroethene 1.059
1ug/L 31-Oct-2016 20:230.30Trichlorofluoromethane 1.0U
1ug/L 31-Oct-2016 20:230.20Vinyl chloride 1.0U
1ug/L 31-Oct-2016 20:230.50Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 31-Oct-2016 20:2396.3 71-125
Surr: 4-Bromofluorobenzene 1%REC 31-Oct-2016 20:2390.2 70-125
Surr: Dibromofluoromethane 1%REC 31-Oct-2016 20:2386.4 74-125
Surr: Toluene-d8 1%REC 31-Oct-2016 20:2399.4 75-125HARDNESS, TOTAL AS CACO3 BY SM2340B
Method:M2340 B Analyst: DQ
1mg/L 07-Nov-2016 15:302.00Hardness (As CaCO3) 2.00326
ICP-MS METALS BY SW6020A Method:SW6020 Analyst: JDEPrep:SW3010A / 01-Nov-2016
1mg/L 04-Nov-2016 18:100.000400Arsenic 0.00500U
1mg/L 04-Nov-2016 18:100.00190Barium 0.005000.0476
1mg/L 04-Nov-2016 18:100.000200Cadmium 0.00200U
1mg/L 04-Nov-2016 18:100.0340Calcium 0.50067.8
1mg/L 04-Nov-2016 18:100.000400Chromium 0.00500U
1mg/L 04-Nov-2016 18:100.000600Lead 0.005000.00531
1mg/L 04-Nov-2016 18:100.0100Magnesium 0.20038.1
1mg/L 04-Nov-2016 18:100.00110Selenium 0.00500U
1mg/L 04-Nov-2016 18:100.000200Silver 0.00500U
MERCURY BY SW7470A Method:SW7470 Analyst: JCJPrep:SW7470 / 03-Nov-2016
1mg/L 03-Nov-2016 15:280.0000400Mercury 0.000200U
ALKALINITY BY SM2320B Method:SM2320B Analyst: KMU1mg/L 02-Nov-2016 11:145.00Alkalinity, Bicarbonate (As
CaCO3)5.00326
1mg/L 02-Nov-2016 11:145.00Alkalinity, Carbonate (As CaCO3) 5.00U
1mg/L 02-Nov-2016 11:145.00Alkalinity, Hydroxide (As CaCO3) 5.00U
1mg/L 02-Nov-2016 11:145.00Alkalinity, Total (As CaCO3) 5.00326
TOTAL ORGANIC CARBON BY SW9060A Method:SW9060 Analyst: KMU1mg/L 06-Nov-2016 17:550.500Organic Carbon, Total 1.00U
07-Nov-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 9 of 47
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonFB-1
WorkOrder:Lab ID:
Collection Date:
HS16101339HS16101339-04
27-Oct-2016 16:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 31-Oct-2016 20:480.201,1,1-Trichloroethane 1.0U
1ug/L 31-Oct-2016 20:480.501,1,2,2-Tetrachloroethane 1.0U
1ug/L 31-Oct-2016 20:481.01,1,2-Trichlor-1,2,2-trifluoroethane 1.0U
1ug/L 31-Oct-2016 20:480.301,1,2-Trichloroethane 1.0U
1ug/L 31-Oct-2016 20:480.201,1-Dichloroethane 1.0U
1ug/L 31-Oct-2016 20:480.201,1-Dichloroethene 1.0U
1ug/L 31-Oct-2016 20:480.501,2,4-Trichlorobenzene 1.0U
1ug/L 31-Oct-2016 20:481.01,2-Dibromo-3-chloropropane 1.0U
1ug/L 31-Oct-2016 20:480.201,2-Dibromoethane 1.0U
1ug/L 31-Oct-2016 20:480.501,2-Dichlorobenzene 1.0U
1ug/L 31-Oct-2016 20:480.201,2-Dichloroethane 1.0U
1ug/L 31-Oct-2016 20:480.501,2-Dichloropropane 1.0U
1ug/L 31-Oct-2016 20:480.401,3-Dichlorobenzene 1.0U
1ug/L 31-Oct-2016 20:480.401,4-Dichlorobenzene 1.0U
1ug/L 31-Oct-2016 20:480.502-Butanone 2.0U
1ug/L 31-Oct-2016 20:481.02-Hexanone 2.0U
1ug/L 31-Oct-2016 20:480.704-Methyl-2-pentanone 2.0U
1ug/L 31-Oct-2016 20:482.0Acetone 2.0U
1ug/L 31-Oct-2016 20:480.20Benzene 1.0U
1ug/L 31-Oct-2016 20:480.20Bromodichloromethane 1.0U
1ug/L 31-Oct-2016 20:480.40Bromoform 1.0U
1ug/L 31-Oct-2016 20:480.40Bromomethane 1.0U
1ug/L 31-Oct-2016 20:480.60Carbon disulfide 2.0U
1ug/L 31-Oct-2016 20:480.50Carbon tetrachloride 1.0U
1ug/L 31-Oct-2016 20:480.30Chlorobenzene 1.0U
1ug/L 31-Oct-2016 20:480.30Chloroethane 1.0U
1ug/L 31-Oct-2016 20:48J 0.20Chloroform 1.00.45
1ug/L 31-Oct-2016 20:480.20Chloromethane 1.01.1
1ug/L 31-Oct-2016 20:480.20cis-1,2-Dichloroethene 1.0U
1ug/L 31-Oct-2016 20:480.10cis-1,3-Dichloropropene 1.0U
1ug/L 31-Oct-2016 20:480.30Cyclohexane 1.0U
1ug/L 31-Oct-2016 20:480.30Dibromochloromethane 1.0U
1ug/L 31-Oct-2016 20:480.30Dichlorodifluoromethane 1.0U
1ug/L 31-Oct-2016 20:480.30Ethylbenzene 1.0U
1ug/L 31-Oct-2016 20:480.30Isopropylbenzene 1.0U
1ug/L 31-Oct-2016 20:480.50m,p-Xylene 2.0U
1ug/L 31-Oct-2016 20:481.0Methyl acetate 1.0U
1ug/L 31-Oct-2016 20:480.20Methyl tert-butyl ether 1.0U
1ug/L 31-Oct-2016 20:480.30Methylcyclohexane 1.0U
07-Nov-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 10 of 47
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonFB-1
WorkOrder:Lab ID:
Collection Date:
HS16101339HS16101339-04
27-Oct-2016 16:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 31-Oct-2016 20:481.0Methylene chloride 2.0U
1ug/L 31-Oct-2016 20:480.30o-Xylene 1.0U
1ug/L 31-Oct-2016 20:480.30Styrene 1.0U
1ug/L 31-Oct-2016 20:480.30Tetrachloroethene 1.0U
1ug/L 31-Oct-2016 20:480.20Toluene 1.0U
1ug/L 31-Oct-2016 20:480.20trans-1,2-Dichloroethene 1.0U
1ug/L 31-Oct-2016 20:480.20trans-1,3-Dichloropropene 1.0U
1ug/L 31-Oct-2016 20:480.20Trichloroethene 1.0U
1ug/L 31-Oct-2016 20:480.30Trichlorofluoromethane 1.0U
1ug/L 31-Oct-2016 20:480.20Vinyl chloride 1.0U
1ug/L 31-Oct-2016 20:480.50Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 31-Oct-2016 20:4898.3 71-125
Surr: 4-Bromofluorobenzene 1%REC 31-Oct-2016 20:4888.5 70-125
Surr: Dibromofluoromethane 1%REC 31-Oct-2016 20:4875.4 74-125
Surr: Toluene-d8 1%REC 31-Oct-2016 20:4895.5 75-125
07-Nov-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 11 of 47
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonMWPT-4
WorkOrder:Lab ID:
Collection Date:
HS16101339HS16101339-05
28-Oct-2016 11:30 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 31-Oct-2016 21:130.201,1,1-Trichloroethane 1.0U
1ug/L 31-Oct-2016 21:130.501,1,2,2-Tetrachloroethane 1.0U
1ug/L 31-Oct-2016 21:131.01,1,2-Trichlor-1,2,2-trifluoroethane 1.0U
1ug/L 31-Oct-2016 21:130.301,1,2-Trichloroethane 1.0U
1ug/L 31-Oct-2016 21:130.201,1-Dichloroethane 1.0U
1ug/L 31-Oct-2016 21:130.201,1-Dichloroethene 1.0U
1ug/L 31-Oct-2016 21:130.501,2,4-Trichlorobenzene 1.0U
1ug/L 31-Oct-2016 21:131.01,2-Dibromo-3-chloropropane 1.0U
1ug/L 31-Oct-2016 21:130.201,2-Dibromoethane 1.0U
1ug/L 31-Oct-2016 21:130.501,2-Dichlorobenzene 1.0U
1ug/L 31-Oct-2016 21:130.201,2-Dichloroethane 1.0U
1ug/L 31-Oct-2016 21:130.501,2-Dichloropropane 1.0U
1ug/L 31-Oct-2016 21:130.401,3-Dichlorobenzene 1.0U
1ug/L 31-Oct-2016 21:130.401,4-Dichlorobenzene 1.0U
1ug/L 31-Oct-2016 21:130.502-Butanone 2.0U
1ug/L 31-Oct-2016 21:131.02-Hexanone 2.0U
1ug/L 31-Oct-2016 21:130.704-Methyl-2-pentanone 2.0U
1ug/L 31-Oct-2016 21:132.0Acetone 2.0U
1ug/L 31-Oct-2016 21:130.20Benzene 1.0U
1ug/L 31-Oct-2016 21:130.20Bromodichloromethane 1.0U
1ug/L 31-Oct-2016 21:130.40Bromoform 1.0U
1ug/L 31-Oct-2016 21:130.40Bromomethane 1.0U
1ug/L 31-Oct-2016 21:130.60Carbon disulfide 2.0U
1ug/L 31-Oct-2016 21:130.50Carbon tetrachloride 1.0U
1ug/L 31-Oct-2016 21:130.30Chlorobenzene 1.0U
1ug/L 31-Oct-2016 21:130.30Chloroethane 1.0U
1ug/L 31-Oct-2016 21:130.20Chloroform 1.0U
1ug/L 31-Oct-2016 21:130.20Chloromethane 1.0U
1ug/L 31-Oct-2016 21:130.20cis-1,2-Dichloroethene 1.03.4
1ug/L 31-Oct-2016 21:130.10cis-1,3-Dichloropropene 1.0U
1ug/L 31-Oct-2016 21:130.30Cyclohexane 1.0U
1ug/L 31-Oct-2016 21:130.30Dibromochloromethane 1.0U
1ug/L 31-Oct-2016 21:130.30Dichlorodifluoromethane 1.0U
1ug/L 31-Oct-2016 21:130.30Ethylbenzene 1.0U
1ug/L 31-Oct-2016 21:130.30Isopropylbenzene 1.0U
1ug/L 31-Oct-2016 21:130.50m,p-Xylene 2.0U
1ug/L 31-Oct-2016 21:131.0Methyl acetate 1.0U
1ug/L 31-Oct-2016 21:130.20Methyl tert-butyl ether 1.0U
1ug/L 31-Oct-2016 21:130.30Methylcyclohexane 1.0U
07-Nov-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 12 of 47
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonMWPT-4
WorkOrder:Lab ID:
Collection Date:
HS16101339HS16101339-05
28-Oct-2016 11:30 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 31-Oct-2016 21:131.0Methylene chloride 2.0U
1ug/L 31-Oct-2016 21:130.30o-Xylene 1.0U
1ug/L 31-Oct-2016 21:130.30Styrene 1.0U
1ug/L 31-Oct-2016 21:130.30Tetrachloroethene 1.0U
1ug/L 31-Oct-2016 21:130.20Toluene 1.0U
1ug/L 31-Oct-2016 21:130.20trans-1,2-Dichloroethene 1.0U
1ug/L 31-Oct-2016 21:130.20trans-1,3-Dichloropropene 1.0U
1ug/L 31-Oct-2016 21:130.20Trichloroethene 1.060
1ug/L 31-Oct-2016 21:130.30Trichlorofluoromethane 1.0U
1ug/L 31-Oct-2016 21:130.20Vinyl chloride 1.0U
1ug/L 31-Oct-2016 21:130.50Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 31-Oct-2016 21:13100 71-125
Surr: 4-Bromofluorobenzene 1%REC 31-Oct-2016 21:1391.0 70-125
Surr: Dibromofluoromethane 1%REC 31-Oct-2016 21:1383.3 74-125
Surr: Toluene-d8 1%REC 31-Oct-2016 21:1399.5 75-125HARDNESS, TOTAL AS CACO3 BY SM2340B
Method:M2340 B Analyst: DQ
1mg/L 07-Nov-2016 15:302.00Hardness (As CaCO3) 2.00326
ICP-MS METALS BY SW6020A Method:SW6020 Analyst: JDEPrep:SW3010A / 01-Nov-2016
1mg/L 04-Nov-2016 18:130.000400Arsenic 0.00500U
1mg/L 04-Nov-2016 18:130.00190Barium 0.005000.0489
1mg/L 04-Nov-2016 18:130.000200Cadmium 0.00200U
1mg/L 04-Nov-2016 18:130.0340Calcium 0.50068.0
1mg/L 04-Nov-2016 18:130.000400Chromium 0.00500U
1mg/L 04-Nov-2016 18:13J 0.000600Lead 0.005000.00415
1mg/L 04-Nov-2016 18:130.0100Magnesium 0.20037.9
1mg/L 04-Nov-2016 18:130.00110Selenium 0.00500U
1mg/L 04-Nov-2016 18:130.000200Silver 0.00500U
MERCURY BY SW7470A Method:SW7470 Analyst: JCJPrep:SW7470 / 03-Nov-2016
1mg/L 03-Nov-2016 15:300.0000400Mercury 0.000200U
ALKALINITY BY SM2320B Method:SM2320B Analyst: KMU1mg/L 02-Nov-2016 11:365.00Alkalinity, Bicarbonate (As
CaCO3)5.00324
1mg/L 02-Nov-2016 11:365.00Alkalinity, Carbonate (As CaCO3) 5.00U
1mg/L 02-Nov-2016 11:365.00Alkalinity, Hydroxide (As CaCO3) 5.00U
1mg/L 02-Nov-2016 11:365.00Alkalinity, Total (As CaCO3) 5.00324
TOTAL ORGANIC CARBON BY SW9060A Method:SW9060 Analyst: KMU1mg/L 06-Nov-2016 18:13J 0.500Organic Carbon, Total 1.000.510
07-Nov-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 13 of 47
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonRB-1
WorkOrder:Lab ID:
Collection Date:
HS16101339HS16101339-06
28-Oct-2016 13:05 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 01-Nov-2016 00:340.201,1,1-Trichloroethane 1.0U
1ug/L 01-Nov-2016 00:340.501,1,2,2-Tetrachloroethane 1.0U
1ug/L 01-Nov-2016 00:341.01,1,2-Trichlor-1,2,2-trifluoroethane 1.0U
1ug/L 01-Nov-2016 00:340.301,1,2-Trichloroethane 1.0U
1ug/L 01-Nov-2016 00:340.201,1-Dichloroethane 1.0U
1ug/L 01-Nov-2016 00:340.201,1-Dichloroethene 1.0U
1ug/L 01-Nov-2016 00:340.501,2,4-Trichlorobenzene 1.0U
1ug/L 01-Nov-2016 00:341.01,2-Dibromo-3-chloropropane 1.0U
1ug/L 01-Nov-2016 00:340.201,2-Dibromoethane 1.0U
1ug/L 01-Nov-2016 00:340.501,2-Dichlorobenzene 1.0U
1ug/L 01-Nov-2016 00:340.201,2-Dichloroethane 1.0U
1ug/L 01-Nov-2016 00:340.501,2-Dichloropropane 1.0U
1ug/L 01-Nov-2016 00:340.401,3-Dichlorobenzene 1.0U
1ug/L 01-Nov-2016 00:340.401,4-Dichlorobenzene 1.0U
1ug/L 01-Nov-2016 00:340.502-Butanone 2.0U
1ug/L 01-Nov-2016 00:341.02-Hexanone 2.0U
1ug/L 01-Nov-2016 00:340.704-Methyl-2-pentanone 2.0U
1ug/L 01-Nov-2016 00:342.0Acetone 2.0U
1ug/L 01-Nov-2016 00:340.20Benzene 1.0U
1ug/L 01-Nov-2016 00:340.20Bromodichloromethane 1.0U
1ug/L 01-Nov-2016 00:340.40Bromoform 1.0U
1ug/L 01-Nov-2016 00:340.40Bromomethane 1.0U
1ug/L 01-Nov-2016 00:340.60Carbon disulfide 2.0U
1ug/L 01-Nov-2016 00:340.50Carbon tetrachloride 1.0U
1ug/L 01-Nov-2016 00:340.30Chlorobenzene 1.0U
1ug/L 01-Nov-2016 00:340.30Chloroethane 1.0U
1ug/L 01-Nov-2016 00:34J 0.20Chloroform 1.00.37
1ug/L 01-Nov-2016 00:340.20Chloromethane 1.0U
1ug/L 01-Nov-2016 00:340.20cis-1,2-Dichloroethene 1.0U
1ug/L 01-Nov-2016 00:340.10cis-1,3-Dichloropropene 1.0U
1ug/L 01-Nov-2016 00:340.30Cyclohexane 1.0U
1ug/L 01-Nov-2016 00:340.30Dibromochloromethane 1.0U
1ug/L 01-Nov-2016 00:340.30Dichlorodifluoromethane 1.0U
1ug/L 01-Nov-2016 00:340.30Ethylbenzene 1.0U
1ug/L 01-Nov-2016 00:340.30Isopropylbenzene 1.0U
1ug/L 01-Nov-2016 00:340.50m,p-Xylene 2.0U
1ug/L 01-Nov-2016 00:341.0Methyl acetate 1.0U
1ug/L 01-Nov-2016 00:340.20Methyl tert-butyl ether 1.0U
1ug/L 01-Nov-2016 00:340.30Methylcyclohexane 1.0U
07-Nov-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 14 of 47
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonRB-1
WorkOrder:Lab ID:
Collection Date:
HS16101339HS16101339-06
28-Oct-2016 13:05 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 01-Nov-2016 00:341.0Methylene chloride 2.0U
1ug/L 01-Nov-2016 00:340.30o-Xylene 1.0U
1ug/L 01-Nov-2016 00:340.30Styrene 1.0U
1ug/L 01-Nov-2016 00:340.30Tetrachloroethene 1.0U
1ug/L 01-Nov-2016 00:340.20Toluene 1.0U
1ug/L 01-Nov-2016 00:340.20trans-1,2-Dichloroethene 1.0U
1ug/L 01-Nov-2016 00:340.20trans-1,3-Dichloropropene 1.0U
1ug/L 01-Nov-2016 00:340.20Trichloroethene 1.0U
1ug/L 01-Nov-2016 00:340.30Trichlorofluoromethane 1.0U
1ug/L 01-Nov-2016 00:340.20Vinyl chloride 1.0U
1ug/L 01-Nov-2016 00:340.50Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 01-Nov-2016 00:3496.3 71-125
Surr: 4-Bromofluorobenzene 1%REC 01-Nov-2016 00:3490.9 70-125
Surr: Dibromofluoromethane 1%REC 01-Nov-2016 00:3475.6 74-125
Surr: Toluene-d8 1%REC 01-Nov-2016 00:3498.7 75-125
07-Nov-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 15 of 47
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonTRIP BLANK
WorkOrder:Lab ID:
Collection Date:
HS16101339HS16101339-07
25-Oct-2016 00:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 01-Nov-2016 00:090.201,1,1-Trichloroethane 1.0U
1ug/L 01-Nov-2016 00:090.501,1,2,2-Tetrachloroethane 1.0U
1ug/L 01-Nov-2016 00:091.01,1,2-Trichlor-1,2,2-trifluoroethane 1.0U
1ug/L 01-Nov-2016 00:090.301,1,2-Trichloroethane 1.0U
1ug/L 01-Nov-2016 00:090.201,1-Dichloroethane 1.0U
1ug/L 01-Nov-2016 00:090.201,1-Dichloroethene 1.0U
1ug/L 01-Nov-2016 00:090.501,2,4-Trichlorobenzene 1.0U
1ug/L 01-Nov-2016 00:091.01,2-Dibromo-3-chloropropane 1.0U
1ug/L 01-Nov-2016 00:090.201,2-Dibromoethane 1.0U
1ug/L 01-Nov-2016 00:090.501,2-Dichlorobenzene 1.0U
1ug/L 01-Nov-2016 00:090.201,2-Dichloroethane 1.0U
1ug/L 01-Nov-2016 00:090.501,2-Dichloropropane 1.0U
1ug/L 01-Nov-2016 00:090.401,3-Dichlorobenzene 1.0U
1ug/L 01-Nov-2016 00:090.401,4-Dichlorobenzene 1.0U
1ug/L 01-Nov-2016 00:090.502-Butanone 2.0U
1ug/L 01-Nov-2016 00:091.02-Hexanone 2.0U
1ug/L 01-Nov-2016 00:090.704-Methyl-2-pentanone 2.0U
1ug/L 01-Nov-2016 00:092.0Acetone 2.0U
1ug/L 01-Nov-2016 00:090.20Benzene 1.0U
1ug/L 01-Nov-2016 00:090.20Bromodichloromethane 1.0U
1ug/L 01-Nov-2016 00:090.40Bromoform 1.0U
1ug/L 01-Nov-2016 00:090.40Bromomethane 1.0U
1ug/L 01-Nov-2016 00:090.60Carbon disulfide 2.0U
1ug/L 01-Nov-2016 00:090.50Carbon tetrachloride 1.0U
1ug/L 01-Nov-2016 00:090.30Chlorobenzene 1.0U
1ug/L 01-Nov-2016 00:090.30Chloroethane 1.0U
1ug/L 01-Nov-2016 00:090.20Chloroform 1.0U
1ug/L 01-Nov-2016 00:090.20Chloromethane 1.0U
1ug/L 01-Nov-2016 00:090.20cis-1,2-Dichloroethene 1.0U
1ug/L 01-Nov-2016 00:090.10cis-1,3-Dichloropropene 1.0U
1ug/L 01-Nov-2016 00:090.30Cyclohexane 1.0U
1ug/L 01-Nov-2016 00:090.30Dibromochloromethane 1.0U
1ug/L 01-Nov-2016 00:090.30Dichlorodifluoromethane 1.0U
1ug/L 01-Nov-2016 00:090.30Ethylbenzene 1.0U
1ug/L 01-Nov-2016 00:090.30Isopropylbenzene 1.0U
1ug/L 01-Nov-2016 00:090.50m,p-Xylene 2.0U
1ug/L 01-Nov-2016 00:091.0Methyl acetate 1.0U
1ug/L 01-Nov-2016 00:090.20Methyl tert-butyl ether 1.0U
1ug/L 01-Nov-2016 00:090.30Methylcyclohexane 1.0U
07-Nov-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 16 of 47
Client:Project:Sample ID:
Golder AssociatesCity of CamdentonTRIP BLANK
WorkOrder:Lab ID:
Collection Date:
HS16101339HS16101339-07
25-Oct-2016 00:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT LIMIT
DILUTION FACTORUNITS
DATE ANALYZEDQUAL MDL
LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1ug/L 01-Nov-2016 00:091.0Methylene chloride 2.0U
1ug/L 01-Nov-2016 00:090.30o-Xylene 1.0U
1ug/L 01-Nov-2016 00:090.30Styrene 1.0U
1ug/L 01-Nov-2016 00:090.30Tetrachloroethene 1.0U
1ug/L 01-Nov-2016 00:090.20Toluene 1.0U
1ug/L 01-Nov-2016 00:090.20trans-1,2-Dichloroethene 1.0U
1ug/L 01-Nov-2016 00:090.20trans-1,3-Dichloropropene 1.0U
1ug/L 01-Nov-2016 00:090.20Trichloroethene 1.0U
1ug/L 01-Nov-2016 00:090.30Trichlorofluoromethane 1.0U
1ug/L 01-Nov-2016 00:090.20Vinyl chloride 1.0U
1ug/L 01-Nov-2016 00:090.50Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 01-Nov-2016 00:0997.5 71-125
Surr: 4-Bromofluorobenzene 1%REC 01-Nov-2016 00:0990.1 70-125
Surr: Dibromofluoromethane 1%REC 01-Nov-2016 00:0978.1 74-125
Surr: Toluene-d8 1%REC 01-Nov-2016 00:0997.6 75-125
07-Nov-16Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 17 of 47
WEIGHT LOG
HS16101339City of CamdentonGolder Associates
WorkOrder:Project:Client:
Batch ID: 109425 Method: ICP-MS METALS BY SW6020A 3010APrep:
ContainerSampIDSample Wt/Vol
Final Volume
Prep Factor
HS16101339-01 1 50 50 (mL) 1HS16101339-03 1 50 50 (mL) 1HS16101339-05 1 50 50 (mL) 1
Batch ID: 109499 Method: MERCURY BY SW7470A HG_WPRPrep:
ContainerSampIDSample Wt/Vol
Final Volume
Prep Factor
HS16101339-01 1 40 40 (mL) 1HS16101339-03 1 40 40 (mL) 1HS16101339-05 1 40 40 (mL) 1
07-Nov-16Date: ALS Group USA, Corp
Page 18 of 47
Client:City of CamdentonGolder Associates
WorkOrder:Project:
HS16101339DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID TCLP Date DF
Batch ID 109425 Test Name : ICP-MS METALS BY SW6020A Matrix: Water
01 Nov 2016 10:00 04 Nov 2016 18:07HS16101339-01 25 Oct 2016 16:30 1MWPT-1
01 Nov 2016 10:00 04 Nov 2016 18:10HS16101339-03 27 Oct 2016 16:00 1MWPT-3
01 Nov 2016 10:00 04 Nov 2016 18:13HS16101339-05 28 Oct 2016 11:30 1MWPT-4
Batch ID 109499 Test Name : MERCURY BY SW7470A Matrix: Water
03 Nov 2016 09:52 03 Nov 2016 15:27HS16101339-01 25 Oct 2016 16:30 1MWPT-1
03 Nov 2016 09:52 03 Nov 2016 15:28HS16101339-03 27 Oct 2016 16:00 1MWPT-3
03 Nov 2016 09:52 03 Nov 2016 15:30HS16101339-05 28 Oct 2016 11:30 1MWPT-4
Batch ID R283946 Test Name : LOW LEVEL VOLATILES BY SW8260C Matrix: Water
31 Oct 2016 19:33HS16101339-01 25 Oct 2016 16:30 1MWPT-1
31 Oct 2016 19:58HS16101339-02 25 Oct 2016 00:00 1DUP-1
31 Oct 2016 20:23HS16101339-03 27 Oct 2016 16:00 1MWPT-3
31 Oct 2016 20:48HS16101339-04 27 Oct 2016 16:00 1FB-1
31 Oct 2016 21:13HS16101339-05 28 Oct 2016 11:30 1MWPT-4
Batch ID R283975 Test Name : LOW LEVEL VOLATILES BY SW8260C Matrix: Water
01 Nov 2016 00:34HS16101339-06 28 Oct 2016 13:05 1RB-1
01 Nov 2016 00:09HS16101339-07 25 Oct 2016 00:00 1TRIP BLANK
Batch ID R284076 Test Name : ALKALINITY BY SM2320B Matrix: Water
02 Nov 2016 11:07HS16101339-01 25 Oct 2016 16:30 1MWPT-1
02 Nov 2016 11:14HS16101339-03 27 Oct 2016 16:00 1MWPT-3
02 Nov 2016 11:36HS16101339-05 28 Oct 2016 11:30 1MWPT-4
Batch ID R284304 Test Name : TOTAL ORGANIC CARBON BY SW9060A Matrix: Water
06 Nov 2016 17:23HS16101339-01 25 Oct 2016 16:30 1MWPT-1
06 Nov 2016 17:55HS16101339-03 27 Oct 2016 16:00 1MWPT-3
06 Nov 2016 18:13HS16101339-05 28 Oct 2016 11:30 1MWPT-4
Batch ID R284356 Test Name : HARDNESS, TOTAL AS CACO3 BY SM2340B Matrix: Water
07 Nov 2016 15:30HS16101339-01 25 Oct 2016 16:30 1MWPT-1
07 Nov 2016 15:30HS16101339-03 27 Oct 2016 16:00 1MWPT-3
07 Nov 2016 15:30HS16101339-05 28 Oct 2016 11:30 1MWPT-4
07-Nov-16Date: ALS Group USA, Corp
Page 19 of 47
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16101339
QC BATCH REPORT
Batch ID: 109425 Instrument: ICPMS05 Method: SW6020
Sample ID: MBLK-109425 Units: mg/L Analysis Date: 04-Nov-2016 12:13
Run ID: ICPMS05_284197 SeqNo: 3881608 PrepDate: 01-Nov-2016 DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MBLK
Client ID:
Arsenic U 0.00500
Barium U 0.00500
Cadmium U 0.00200
Calcium U 0.500
Chromium U 0.00500
Lead U 0.00500
Magnesium U 0.200
Selenium U 0.00500
Silver U 0.00500
Sample ID: LCS-109425 Units: mg/L Analysis Date: 04-Nov-2016 12:16
Run ID: ICPMS05_284197 SeqNo: 3881609 PrepDate: 01-Nov-2016 DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
LCS
Client ID:
Arsenic 0.04997 0.05 0 99.9 80 - 1200.00500
Barium 0.05018 0.05 0 100 80 - 1200.00500
Cadmium 0.05127 0.05 0 103 80 - 1200.00200
Calcium 5.215 5 0 104 80 - 1200.500
Chromium 0.04782 0.05 0 95.6 80 - 1200.00500
Lead 0.04895 0.05 0 97.9 80 - 1200.00500
Magnesium 5.512 5 0 110 80 - 1200.200
Selenium 0.05048 0.05 0 101 80 - 1200.00500
Silver 0.04885 0.05 0 97.7 80 - 1200.00500
ALS Group USA, Corp Date: 07-Nov-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 20 of 47
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16101339
QC BATCH REPORT
Batch ID: 109425 Instrument: ICPMS05 Method: SW6020
Sample ID: HS16101322-10MS Units: mg/L Analysis Date: 04-Nov-2016 12:25
Run ID: ICPMS05_284197 SeqNo: 3881642 PrepDate: 01-Nov-2016 DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MS
Client ID:
Arsenic 0.05765 0.05 0.01165 92.0 80 - 1200.00500
Barium 0.2219 0.05 0.1563 131 80 - 120 S 0.00500
Cadmium 0.04517 0.05 0.000343 89.7 80 - 1200.00200
Calcium 130.7 5 120 215 80 - 120 SO 0.500
Chromium 0.08394 0.05 0.02858 111 80 - 1200.00500
Lead 0.05531 0.05 0.01085 88.9 80 - 1200.00500
Magnesium 17.46 5 12.78 93.6 80 - 1200.200
Selenium 0.04625 0.05 0 92.5 80 - 1200.00500
Silver 0.04424 0.05 0.000243 88.0 80 - 1200.00500
Sample ID: HS16101322-10MSD Units: mg/L Analysis Date: 04-Nov-2016 12:28
Run ID: ICPMS05_284197 SeqNo: 3881643 PrepDate: 01-Nov-2016 DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MSD
Client ID:
Arsenic 0.05727 0.05 0.01165 91.2 80 - 120 0.05765 0.668 200.00500
Barium 0.2265 0.05 0.1563 140 80 - 120 0.2219 2.07 20 S 0.00500
Cadmium 0.04618 0.05 0.000343 91.7 80 - 120 0.04517 2.2 200.00200
Calcium 131.1 5 120 223 80 - 120 130.7 0.312 20 SO 0.500
Chromium 0.08595 0.05 0.02858 115 80 - 120 0.08394 2.36 200.00500
Lead 0.05525 0.05 0.01085 88.8 80 - 120 0.05531 0.0977 200.00500
Magnesium 18.05 5 12.78 105 80 - 120 17.46 3.32 200.200
Selenium 0.04575 0.05 0 91.5 80 - 120 0.04625 1.08 200.00500
Silver 0.04361 0.05 0.000243 86.7 80 - 120 0.04424 1.44 200.00500
ALS Group USA, Corp Date: 07-Nov-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 21 of 47
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16101339
QC BATCH REPORT
Batch ID: 109425 Instrument: ICPMS05 Method: SW6020
Sample ID: HS16101322-10BS Units: mg/L Analysis Date: 04-Nov-2016 12:31
Run ID: ICPMS05_284197 SeqNo: 3881644 PrepDate: 01-Nov-2016 DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
PDS
Client ID:
Arsenic 0.104 0.1 0.01165 92.4 75 - 1250.00500
Barium 0.2504 0.1 0.1563 94.1 75 - 1250.00500
Cadmium 0.09216 0.1 0.000343 91.8 75 - 1250.00200
Calcium 129.9 10 120 99.8 75 - 125 O 0.500
Chromium 0.1112 0.1 0.02858 82.6 75 - 1250.00500
Lead 0.1017 0.1 0.01085 90.8 75 - 1250.00500
Magnesium 21.52 10 12.78 87.4 75 - 1250.200
Selenium 0.09148 0.1 0 91.5 75 - 1250.00500
Silver 0.08748 0.1 0.000243 87.2 75 - 1250.00500
Sample ID: HS16101322-10 DIL SX Units: mg/L Analysis Date: 04-Nov-2016 12:22
Run ID: ICPMS05_284197 SeqNo: 3881641 PrepDate: 01-Nov-2016 DF: 5
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %D%D Limit Qual
SD
Client ID:
Arsenic 0.01162 0.01165 0 10 J 0.0250
Barium 0.1571 0.1563 0.503 100.0250
Cadmium U 0.000343 0 100.0100
Calcium 119.9 120 0.058 102.50
Chromium 0.02974 0.02858 4.04 100.0250
Lead 0.01143 0.01085 0 10 J 0.0250
Selenium U 0 0 100.0250
Silver U 0.000243 0 100.0250
Sample ID: HS16101322-10 DIL SX Units: mg/L Analysis Date: 04-Nov-2016 16:58
Run ID: ICPMS05_284197 SeqNo: 3882201 PrepDate: 01-Nov-2016 DF: 5
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %D%D Limit Qual
SD
Client ID:
Magnesium 13.99 12.63 10.7 10 R 1.00
The following samples were analyzed in this batch: HS16101339-01 HS16101339-03 HS16101339-05
ALS Group USA, Corp Date: 07-Nov-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 22 of 47
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16101339
QC BATCH REPORT
Batch ID: 109499 Instrument: HG03 Method: SW7470
Sample ID: MBLK-109499 Units: mg/L Analysis Date: 03-Nov-2016 15:16
Run ID: HG03_284160 SeqNo: 3880458 PrepDate: 03-Nov-2016 DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MBLK
Client ID:
Mercury U 0.000200
Sample ID: LCS-109499 Units: mg/L Analysis Date: 03-Nov-2016 15:17
Run ID: HG03_284160 SeqNo: 3880459 PrepDate: 03-Nov-2016 DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
LCS
Client ID:
Mercury 0.00494 0.005 0 98.8 80 - 1240.000200
Sample ID: HS16110059-01MS Units: mg/L Analysis Date: 03-Nov-2016 15:59
Run ID: HG03_284160 SeqNo: 3880472 PrepDate: 03-Nov-2016 DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MS
Client ID:
Mercury 0.00115 0.005 -0.000011 23.2 80 - 124 S 0.000200
Sample ID: HS16101322-10MS Units: mg/L Analysis Date: 03-Nov-2016 15:23
Run ID: HG03_284160 SeqNo: 3880461 PrepDate: 03-Nov-2016 DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MS
Client ID:
Mercury 0.00499 0.005 -0.000004 99.9 80 - 1240.000200
Sample ID: HS16110059-01MSD Units: mg/L Analysis Date: 03-Nov-2016 16:01
Run ID: HG03_284160 SeqNo: 3880473 PrepDate: 03-Nov-2016 DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MSD
Client ID:
Mercury 0.00118 0.005 -0.000011 23.8 80 - 124 0.00115 2.58 20 S 0.000200
Sample ID: HS16101322-10MSD Units: mg/L Analysis Date: 03-Nov-2016 15:25
Run ID: HG03_284160 SeqNo: 3880462 PrepDate: 03-Nov-2016 DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MSD
Client ID:
Mercury 0.00492 0.005 -0.000004 98.5 80 - 124 0.00499 1.41 200.000200
The following samples were analyzed in this batch: HS16101339-01 HS16101339-03 HS16101339-05
ALS Group USA, Corp Date: 07-Nov-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 23 of 47
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16101339
QC BATCH REPORT
Batch ID: R283946 Instrument: VOA4 Method: SW8260
Sample ID: VBLKW-161031 Units: ug/L Analysis Date: 31-Oct-2016 11:34
Run ID: VOA4_283946 SeqNo: 3876203 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MBLK
Client ID:
1,1,1-Trichloroethane U 1.0
1,1,2,2-Tetrachloroethane U 1.0
1,1,2-Trichlor-1,2,2-trifluoroethane U 1.0
1,1,2-Trichloroethane U 1.0
1,1-Dichloroethane U 1.0
1,1-Dichloroethene U 1.0
1,2,4-Trichlorobenzene U 1.0
1,2-Dibromo-3-chloropropane U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichlorobenzene U 1.0
1,2-Dichloroethane U 1.0
1,2-Dichloropropane U 1.0
1,3-Dichlorobenzene U 1.0
1,4-Dichlorobenzene U 1.0
2-Butanone U 2.0
2-Hexanone U 2.0
4-Methyl-2-pentanone U 2.0
Acetone U 2.0
Benzene U 1.0
Bromodichloromethane U 1.0
Bromoform U 1.0
Bromomethane U 1.0
Carbon disulfide U 2.0
Carbon tetrachloride U 1.0
Chlorobenzene U 1.0
Chloroethane U 1.0
Chloroform U 1.0
Chloromethane U 1.0
cis-1,2-Dichloroethene U 1.0
cis-1,3-Dichloropropene U 1.0
Cyclohexane U 1.0
Dibromochloromethane U 1.0
Dichlorodifluoromethane U 1.0
Ethylbenzene U 1.0
ALS Group USA, Corp Date: 07-Nov-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 24 of 47
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16101339
QC BATCH REPORT
Batch ID: R283946 Instrument: VOA4 Method: SW8260
Sample ID: VBLKW-161031 Units: ug/L Analysis Date: 31-Oct-2016 11:34
Run ID: VOA4_283946 SeqNo: 3876203 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MBLK
Client ID:
Isopropylbenzene U 1.0
m,p-Xylene U 2.0
Methyl acetate U 1.0
Methyl tert-butyl ether U 1.0
Methylcyclohexane U 1.0
Methylene chloride U 2.0
o-Xylene U 1.0
Styrene U 1.0
Tetrachloroethene U 1.0
Toluene U 1.0
trans-1,2-Dichloroethene U 1.0
trans-1,3-Dichloropropene U 1.0
Trichloroethene U 1.0
Trichlorofluoromethane U 1.0
Vinyl chloride U 1.0
Xylenes, Total U 3.0
45.88 50 0 91.8 71 - 1251.0Surr: 1,2-Dichloroethane-d4
45.05 50 0 90.1 70 - 1251.0Surr: 4-Bromofluorobenzene
49.67 50 0 99.3 74 - 1251.0Surr: Dibromofluoromethane
49.8 50 0 99.6 75 - 1251.0Surr: Toluene-d8
ALS Group USA, Corp Date: 07-Nov-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 25 of 47
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16101339
QC BATCH REPORT
Batch ID: R283946 Instrument: VOA4 Method: SW8260
Sample ID: VLCSW-161031 Units: ug/L Analysis Date: 31-Oct-2016 10:45
Run ID: VOA4_283946 SeqNo: 3876202 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
LCS
Client ID:
1,1,1-Trichloroethane 56.41 50 0 113 75 - 1301.0
1,1,2,2-Tetrachloroethane 40 50 0 80.0 74 - 1231.0
1,1,2-Trichlor-1,2,2-trifluoroethane 49.81 50 0 99.6 70 - 1301.0
1,1,2-Trichloroethane 49.35 50 0 98.7 80 - 1201.0
1,1-Dichloroethane 51.01 50 0 102 76 - 1201.0
1,1-Dichloroethene 53.57 50 0 107 75 - 1301.0
1,2,4-Trichlorobenzene 47.46 50 0 94.9 75 - 1261.0
1,2-Dibromo-3-chloropropane 44.6 50 0 89.2 65 - 1251.0
1,2-Dibromoethane 53.8 50 0 108 80 - 1211.0
1,2-Dichlorobenzene 46.32 50 0 92.6 80 - 1201.0
1,2-Dichloroethane 49.8 50 0 99.6 76 - 1201.0
1,2-Dichloropropane 53.02 50 0 106 80 - 1201.0
1,3-Dichlorobenzene 49.25 50 0 98.5 80 - 1201.0
1,4-Dichlorobenzene 45.94 50 0 91.9 80 - 1201.0
2-Butanone 97.1 100 0 97.1 60 - 1402.0
2-Hexanone 86.04 100 0 86.0 60 - 1312.0
4-Methyl-2-pentanone 85.62 100 0 85.6 60 - 1352.0
Acetone 93.08 100 0 93.1 60 - 1402.0
Benzene 52.91 50 0 106 75 - 1221.0
Bromodichloromethane 55.3 50 0 111 75 - 1251.0
Bromoform 55.35 50 0 111 70 - 1301.0
Bromomethane 49.8 50 0 99.6 60 - 1401.0
Carbon disulfide 102.9 100 0 103 70 - 1302.0
Carbon tetrachloride 53.48 50 0 107 75 - 1251.0
Chlorobenzene 49.58 50 0 99.2 80 - 1201.0
Chloroethane 46.57 50 0 93.1 70 - 1301.0
Chloroform 50.25 50 0 100 70 - 1301.0
Chloromethane 45.39 50 0 90.8 65 - 1301.0
cis-1,2-Dichloroethene 52.74 50 0 105 75 - 1251.0
cis-1,3-Dichloropropene 53.34 50 0 107 79 - 1251.0
Cyclohexane 46.7 50 0 93.4 70 - 1301.0
Dibromochloromethane 52.92 50 0 106 70 - 1301.0
Dichlorodifluoromethane 48.1 50 0 96.2 60 - 1401.0
Ethylbenzene 52.77 50 0 106 80 - 1201.0
ALS Group USA, Corp Date: 07-Nov-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 26 of 47
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16101339
QC BATCH REPORT
Batch ID: R283946 Instrument: VOA4 Method: SW8260
Sample ID: VLCSW-161031 Units: ug/L Analysis Date: 31-Oct-2016 10:45
Run ID: VOA4_283946 SeqNo: 3876202 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
LCS
Client ID:
Isopropylbenzene 54.19 50 0 108 75 - 1301.0
m,p-Xylene 102.6 100 0 103 80 - 1202.0
Methyl acetate 45.94 50 0 91.9 76 - 1221.0
Methyl tert-butyl ether 54.28 50 0 109 70 - 1301.0
Methylcyclohexane 47.3 50 0 94.6 61 - 1581.0
Methylene chloride 51.04 50 0 102 65 - 1332.0
o-Xylene 53.09 50 0 106 80 - 1201.0
Styrene 56.63 50 0 113 78 - 1221.0
Tetrachloroethene 54.47 50 0 109 75 - 1301.0
Toluene 51.68 50 0 103 75 - 1211.0
trans-1,2-Dichloroethene 52.51 50 0 105 75 - 1251.0
trans-1,3-Dichloropropene 53.71 50 0 107 76 - 1251.0
Trichloroethene 53.73 50 0 107 71 - 1251.0
Trichlorofluoromethane 56.18 50 0 112 67 - 1321.0
Vinyl chloride 49.09 50 0 98.2 70 - 1351.0
Xylenes, Total 155.6 150 0 104 79 - 1243.0
45.92 50 0 91.8 71 - 1251.0Surr: 1,2-Dichloroethane-d4
49.83 50 0 99.7 70 - 1251.0Surr: 4-Bromofluorobenzene
48.71 50 0 97.4 74 - 1251.0Surr: Dibromofluoromethane
49.66 50 0 99.3 75 - 1251.0Surr: Toluene-d8
ALS Group USA, Corp Date: 07-Nov-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 27 of 47
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16101339
QC BATCH REPORT
Batch ID: R283946 Instrument: VOA4 Method: SW8260
Sample ID: HS16101295-03MS Units: ug/L Analysis Date: 31-Oct-2016 14:31
Run ID: VOA4_283946 SeqNo: 3876210 PrepDate: DF: 10
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MS
Client ID:
1,1,1-Trichloroethane 565.2 500 0 113 75 - 13010
1,1,2,2-Tetrachloroethane 366.9 500 0 73.4 74 - 123 S 10
1,1,2-Trichlor-1,2,2-trifluoroethane 546.2 500 25.83 104 70 - 13010
1,1,2-Trichloroethane 471.5 500 0 94.3 80 - 12010
1,1-Dichloroethane 495.7 500 0 99.1 76 - 12010
1,1-Dichloroethene 545.9 500 0 109 75 - 13010
1,2,4-Trichlorobenzene 420 500 0 84.0 75 - 12610
1,2-Dibromo-3-chloropropane 380.4 500 0 76.1 65 - 12510
1,2-Dibromoethane 497.8 500 0 99.6 80 - 12110
1,2-Dichlorobenzene 443.4 500 0 88.7 80 - 12010
1,2-Dichloroethane 481.5 500 0 96.3 76 - 12010
1,2-Dichloropropane 513.1 500 0 103 80 - 12010
1,3-Dichlorobenzene 472.4 500 0 94.5 80 - 12010
1,4-Dichlorobenzene 449.8 500 0 90.0 80 - 12010
2-Butanone 872.4 1000 0 87.2 60 - 14020
2-Hexanone 706.2 1000 0 70.6 60 - 13120
4-Methyl-2-pentanone 786.3 1000 0 78.6 60 - 13520
Acetone 852.7 1000 0 85.3 60 - 14020
Benzene 523.6 500 0 105 75 - 12210
Bromodichloromethane 522.6 500 0 105 75 - 12510
Bromoform 505.5 500 0 101 70 - 13010
Bromomethane 475.7 500 0 95.1 60 - 14010
Carbon disulfide 1056 1000 0 106 70 - 13020
Carbon tetrachloride 543.8 500 0 109 79 - 12010
Chlorobenzene 477.8 500 0 95.6 80 - 12010
Chloroethane 454 500 0 90.8 70 - 13010
Chloroform 503 500 0 101 70 - 13010
Chloromethane 412.1 500 0 82.4 65 - 13010
cis-1,2-Dichloroethene 521.1 500 6.033 103 75 - 12510
cis-1,3-Dichloropropene 494.6 500 0 98.9 79 - 12510
Cyclohexane 482.2 500 0 96.4 70 - 13010
Dibromochloromethane 505 500 0 101 70 - 13010
Dichlorodifluoromethane 363 500 0 72.6 60 - 14010
Ethylbenzene 526.9 500 0 105 80 - 12010
ALS Group USA, Corp Date: 07-Nov-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 28 of 47
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16101339
QC BATCH REPORT
Batch ID: R283946 Instrument: VOA4 Method: SW8260
Sample ID: HS16101295-03MS Units: ug/L Analysis Date: 31-Oct-2016 14:31
Run ID: VOA4_283946 SeqNo: 3876210 PrepDate: DF: 10
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MS
Client ID:
Isopropylbenzene 556.3 500 0 111 75 - 13010
m,p-Xylene 1034 1000 0 103 80 - 12020
Methyl acetate 416 500 0 83.2 76 - 12210
Methyl tert-butyl ether 548.2 500 48.09 100 70 - 13010
Methylcyclohexane 490.1 500 0 98.0 61 - 15810
Methylene chloride 504.7 500 0 101 65 - 13320
o-Xylene 517.3 500 0 103 80 - 12010
Styrene 549.9 500 0 110 78 - 12210
Tetrachloroethene 563.5 500 0 113 75 - 13010
Toluene 515.6 500 0 103 75 - 12110
trans-1,2-Dichloroethene 529 500 0 106 75 - 12510
trans-1,3-Dichloropropene 498.8 500 0 99.8 76 - 12510
Trichloroethene 1183 500 638.3 109 71 - 12510
Trichlorofluoromethane 564.8 500 0 113 67 - 13210
Vinyl chloride 473.2 500 0 94.6 70 - 13510
Xylenes, Total 1551 1500 0 103 80 - 12430
455.7 500 0 91.1 71 - 12510Surr: 1,2-Dichloroethane-d4
487.2 500 0 97.4 70 - 12510Surr: 4-Bromofluorobenzene
493.1 500 0 98.6 74 - 12510Surr: Dibromofluoromethane
488.2 500 0 97.6 75 - 12510Surr: Toluene-d8
ALS Group USA, Corp Date: 07-Nov-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 29 of 47
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16101339
QC BATCH REPORT
Batch ID: R283946 Instrument: VOA4 Method: SW8260
Sample ID: HS16101295-03MSD Units: ug/L Analysis Date: 31-Oct-2016 14:56
Run ID: VOA4_283946 SeqNo: 3876211 PrepDate: DF: 10
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MSD
Client ID:
1,1,1-Trichloroethane 585.9 500 0 117 75 - 130 565.2 3.6 2010
1,1,2,2-Tetrachloroethane 397.5 500 0 79.5 74 - 123 366.9 8 2010
1,1,2-Trichlor-1,2,2-trifluoroethane 569.4 500 25.83 109 70 - 130 546.2 4.15 2010
1,1,2-Trichloroethane 489.1 500 0 97.8 80 - 120 471.5 3.65 2010
1,1-Dichloroethane 515.3 500 0 103 76 - 120 495.7 3.89 2010
1,1-Dichloroethene 569.1 500 0 114 75 - 130 545.9 4.17 2010
1,2,4-Trichlorobenzene 487.3 500 0 97.5 75 - 126 420 14.8 2010
1,2-Dibromo-3-chloropropane 446 500 0 89.2 65 - 125 380.4 15.9 2010
1,2-Dibromoethane 527.1 500 0 105 80 - 121 497.8 5.72 2010
1,2-Dichlorobenzene 474.5 500 0 94.9 80 - 120 443.4 6.79 2010
1,2-Dichloroethane 484.4 500 0 96.9 76 - 120 481.5 0.596 2010
1,2-Dichloropropane 521.2 500 0 104 80 - 120 513.1 1.57 2010
1,3-Dichlorobenzene 513.2 500 0 103 80 - 120 472.4 8.28 2010
1,4-Dichlorobenzene 493.4 500 0 98.7 80 - 120 449.8 9.25 2010
2-Butanone 938.4 1000 0 93.8 60 - 140 872.4 7.29 2020
2-Hexanone 844.3 1000 0 84.4 60 - 131 706.2 17.8 2020
4-Methyl-2-pentanone 840.9 1000 0 84.1 60 - 135 786.3 6.71 2020
Acetone 923.9 1000 0 92.4 60 - 140 852.7 8.02 2020
Benzene 533.5 500 0 107 75 - 122 523.6 1.87 2010
Bromodichloromethane 536.7 500 0 107 75 - 125 522.6 2.67 2010
Bromoform 534.8 500 0 107 70 - 130 505.5 5.64 2010
Bromomethane 487.7 500 0 97.5 60 - 140 475.7 2.5 2010
Carbon disulfide 1086 1000 0 109 70 - 130 1056 2.81 2020
Carbon tetrachloride 555.1 500 0 111 75 - 125 543.8 2.06 2010
Chlorobenzene 502.2 500 0 100 80 - 120 477.8 4.98 2010
Chloroethane 469.9 500 0 94.0 70 - 130 454 3.45 2010
Chloroform 507 500 0 101 70 - 130 503 0.793 2010
Chloromethane 427.6 500 0 85.5 65 - 130 412.1 3.69 2010
cis-1,2-Dichloroethene 538.7 500 6.033 107 75 - 125 521.1 3.33 2010
cis-1,3-Dichloropropene 508.9 500 0 102 79 - 125 494.6 2.84 2010
Cyclohexane 496.6 500 0 99.3 70 - 130 482.2 2.93 2010
Dibromochloromethane 522.6 500 0 105 70 - 130 505 3.41 2010
Dichlorodifluoromethane 354.7 500 0 70.9 60 - 140 363 2.32 2010
Ethylbenzene 547.7 500 0 110 80 - 120 526.9 3.88 2010
ALS Group USA, Corp Date: 07-Nov-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 30 of 47
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16101339
QC BATCH REPORT
Batch ID: R283946 Instrument: VOA4 Method: SW8260
Sample ID: HS16101295-03MSD Units: ug/L Analysis Date: 31-Oct-2016 14:56
Run ID: VOA4_283946 SeqNo: 3876211 PrepDate: DF: 10
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MSD
Client ID:
Isopropylbenzene 580.7 500 0 116 75 - 130 556.3 4.28 2010
m,p-Xylene 1083 1000 0 108 80 - 120 1034 4.66 2020
Methyl acetate 464.5 500 0 92.9 76 - 122 416 11 2010
Methyl tert-butyl ether 582.3 500 48.09 107 70 - 130 548.2 6.03 2010
Methylcyclohexane 501.8 500 0 100 61 - 158 490.1 2.34 2010
Methylene chloride 515.4 500 0 103 65 - 133 504.7 2.11 2020
o-Xylene 536 500 0 107 80 - 120 517.3 3.54 2010
Styrene 575 500 0 115 78 - 122 549.9 4.46 2010
Tetrachloroethene 591.2 500 0 118 75 - 130 563.5 4.8 2010
Toluene 531 500 0 106 75 - 121 515.6 2.94 2010
trans-1,2-Dichloroethene 549.1 500 0 110 75 - 125 529 3.74 2010
trans-1,3-Dichloropropene 517.7 500 0 104 76 - 125 498.8 3.71 2010
Trichloroethene 1190 500 638.3 110 71 - 125 1183 0.566 2010
Trichlorofluoromethane 573.6 500 0 115 67 - 132 564.8 1.55 2010
Vinyl chloride 495.6 500 0 99.1 70 - 135 473.2 4.62 2010
Xylenes, Total 1619 1500 0 108 80 - 124 1551 4.29 2030
462.1 500 0 92.4 71 - 125 455.7 1.39 2010Surr: 1,2-Dichloroethane-d4
485.3 500 0 97.1 70 - 125 487.2 0.395 2010Surr: 4-Bromofluorobenzene
494.1 500 0 98.8 74 - 125 493.1 0.199 2010Surr: Dibromofluoromethane
502.7 500 0 101 75 - 125 488.2 2.93 2010Surr: Toluene-d8
The following samples were analyzed in this batch: HS16101339-01 HS16101339-02 HS16101339-03 HS16101339-04 HS16101339-05
ALS Group USA, Corp Date: 07-Nov-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 31 of 47
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16101339
QC BATCH REPORT
Batch ID: R283975 Instrument: VOA4 Method: SW8260
Sample ID: VBLKW-161031 Units: ug/L Analysis Date: 31-Oct-2016 23:44
Run ID: VOA4_283975 SeqNo: 3876841 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MBLK
Client ID:
1,1,1-Trichloroethane U 1.0
1,1,2,2-Tetrachloroethane U 1.0
1,1,2-Trichlor-1,2,2-trifluoroethane U 1.0
1,1,2-Trichloroethane U 1.0
1,1-Dichloroethane U 1.0
1,1-Dichloroethene U 1.0
1,2,4-Trichlorobenzene U 1.0
1,2-Dibromo-3-chloropropane U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichlorobenzene U 1.0
1,2-Dichloroethane U 1.0
1,2-Dichloropropane U 1.0
1,3-Dichlorobenzene U 1.0
1,4-Dichlorobenzene U 1.0
2-Butanone U 2.0
2-Hexanone U 2.0
4-Methyl-2-pentanone U 2.0
Acetone U 2.0
Benzene U 1.0
Bromodichloromethane U 1.0
Bromoform U 1.0
Bromomethane U 1.0
Carbon disulfide U 2.0
Carbon tetrachloride U 1.0
Chlorobenzene U 1.0
Chloroethane U 1.0
Chloroform U 1.0
Chloromethane U 1.0
cis-1,2-Dichloroethene U 1.0
cis-1,3-Dichloropropene U 1.0
Cyclohexane U 1.0
Dibromochloromethane U 1.0
Dichlorodifluoromethane U 1.0
Ethylbenzene U 1.0
ALS Group USA, Corp Date: 07-Nov-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 32 of 47
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16101339
QC BATCH REPORT
Batch ID: R283975 Instrument: VOA4 Method: SW8260
Sample ID: VBLKW-161031 Units: ug/L Analysis Date: 31-Oct-2016 23:44
Run ID: VOA4_283975 SeqNo: 3876841 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MBLK
Client ID:
Isopropylbenzene U 1.0
m,p-Xylene U 2.0
Methyl acetate U 1.0
Methyl tert-butyl ether U 1.0
Methylcyclohexane U 1.0
Methylene chloride U 2.0
o-Xylene U 1.0
Styrene U 1.0
Tetrachloroethene U 1.0
Toluene U 1.0
trans-1,2-Dichloroethene U 1.0
trans-1,3-Dichloropropene U 1.0
Trichloroethene U 1.0
Trichlorofluoromethane U 1.0
Vinyl chloride U 1.0
Xylenes, Total U 3.0
47.98 50 0 96.0 71 - 1251.0Surr: 1,2-Dichloroethane-d4
45.42 50 0 90.8 70 - 1251.0Surr: 4-Bromofluorobenzene
49.99 50 0 100.0 74 - 1251.0Surr: Dibromofluoromethane
49.76 50 0 99.5 75 - 1251.0Surr: Toluene-d8
ALS Group USA, Corp Date: 07-Nov-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 33 of 47
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16101339
QC BATCH REPORT
Batch ID: R283975 Instrument: VOA4 Method: SW8260
Sample ID: VLCSW-161031 Units: ug/L Analysis Date: 31-Oct-2016 22:54
Run ID: VOA4_283975 SeqNo: 3876840 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
LCS
Client ID:
1,1,1-Trichloroethane 58.23 50 0 116 75 - 1301.0
1,1,2,2-Tetrachloroethane 40.88 50 0 81.8 74 - 1231.0
1,1,2-Trichlor-1,2,2-trifluoroethane 52.84 50 0 106 70 - 1301.0
1,1,2-Trichloroethane 50.88 50 0 102 80 - 1201.0
1,1-Dichloroethane 53.13 50 0 106 76 - 1201.0
1,1-Dichloroethene 56.49 50 0 113 75 - 1301.0
1,2,4-Trichlorobenzene 49.87 50 0 99.7 75 - 1261.0
1,2-Dibromo-3-chloropropane 45.98 50 0 92.0 65 - 1251.0
1,2-Dibromoethane 54.61 50 0 109 80 - 1211.0
1,2-Dichlorobenzene 46.93 50 0 93.9 80 - 1201.0
1,2-Dichloroethane 52.41 50 0 105 76 - 1201.0
1,2-Dichloropropane 54.44 50 0 109 80 - 1201.0
1,3-Dichlorobenzene 49.61 50 0 99.2 80 - 1201.0
1,4-Dichlorobenzene 45.82 50 0 91.6 80 - 1201.0
2-Butanone 104 100 0 104 60 - 1402.0
2-Hexanone 91.56 100 0 91.6 60 - 1312.0
4-Methyl-2-pentanone 90.22 100 0 90.2 60 - 1352.0
Acetone 101.8 100 0 102 60 - 1402.0
Benzene 54.38 50 0 109 75 - 1221.0
Bromodichloromethane 55.79 50 0 112 75 - 1251.0
Bromoform 56.2 50 0 112 70 - 1301.0
Bromomethane 52 50 0 104 60 - 1401.0
Carbon disulfide 109.2 100 0 109 70 - 1302.0
Carbon tetrachloride 54.35 50 0 109 75 - 1251.0
Chlorobenzene 49.31 50 0 98.6 80 - 1201.0
Chloroethane 49.1 50 0 98.2 70 - 1301.0
Chloroform 51.5 50 0 103 70 - 1301.0
Chloromethane 48.47 50 0 96.9 65 - 1301.0
cis-1,2-Dichloroethene 55.25 50 0 110 75 - 1251.0
cis-1,3-Dichloropropene 54.41 50 0 109 79 - 1251.0
Cyclohexane 50.08 50 0 100 70 - 1301.0
Dibromochloromethane 51.99 50 0 104 70 - 1301.0
Dichlorodifluoromethane 51.69 50 0 103 60 - 1401.0
Ethylbenzene 52.59 50 0 105 80 - 1201.0
ALS Group USA, Corp Date: 07-Nov-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 34 of 47
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16101339
QC BATCH REPORT
Batch ID: R283975 Instrument: VOA4 Method: SW8260
Sample ID: VLCSW-161031 Units: ug/L Analysis Date: 31-Oct-2016 22:54
Run ID: VOA4_283975 SeqNo: 3876840 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
LCS
Client ID:
Isopropylbenzene 55.59 50 0 111 75 - 1301.0
m,p-Xylene 103.8 100 0 104 80 - 1202.0
Methyl acetate 50.72 50 0 101 76 - 1221.0
Methyl tert-butyl ether 57.69 50 0 115 70 - 1301.0
Methylcyclohexane 50.2 50 0 100 61 - 1581.0
Methylene chloride 55.36 50 0 111 65 - 1332.0
o-Xylene 53.15 50 0 106 80 - 1201.0
Styrene 56.88 50 0 114 78 - 1221.0
Tetrachloroethene 54.29 50 0 109 75 - 1301.0
Toluene 51.58 50 0 103 75 - 1211.0
trans-1,2-Dichloroethene 54.25 50 0 108 75 - 1251.0
trans-1,3-Dichloropropene 54.09 50 0 108 76 - 1251.0
Trichloroethene 57.62 50 0 115 71 - 1251.0
Trichlorofluoromethane 57.61 50 0 115 67 - 1321.0
Vinyl chloride 52.36 50 0 105 70 - 1351.0
Xylenes, Total 157 150 0 105 79 - 1243.0
46.07 50 0 92.1 71 - 1251.0Surr: 1,2-Dichloroethane-d4
49.58 50 0 99.2 70 - 1251.0Surr: 4-Bromofluorobenzene
50.27 50 0 101 74 - 1251.0Surr: Dibromofluoromethane
49.08 50 0 98.2 75 - 1251.0Surr: Toluene-d8
ALS Group USA, Corp Date: 07-Nov-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 35 of 47
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16101339
QC BATCH REPORT
Batch ID: R283975 Instrument: VOA4 Method: SW8260
Sample ID: HS16101336-02MS Units: ug/L Analysis Date: 01-Nov-2016 01:49
Run ID: VOA4_283975 SeqNo: 3876846 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MS
Client ID:
1,1,1-Trichloroethane 60.68 50 0 121 75 - 1301.0
1,1,2,2-Tetrachloroethane 37.88 50 0 75.8 74 - 1231.0
1,1,2-Trichlor-1,2,2-trifluoroethane 56.8 50 0 114 70 - 1301.0
1,1,2-Trichloroethane 48.57 50 0 97.1 80 - 1201.0
1,1-Dichloroethane 54.2 50 0 108 76 - 1201.0
1,1-Dichloroethene 58.54 50 0 117 75 - 1301.0
1,2,4-Trichlorobenzene 44.08 50 0 88.2 75 - 1261.0
1,2-Dibromo-3-chloropropane 39.97 50 0 79.9 65 - 1251.0
1,2-Dibromoethane 52.62 50 0 105 80 - 1211.0
1,2-Dichlorobenzene 45.41 50 0 90.8 80 - 1201.0
1,2-Dichloroethane 48.61 50 0 97.2 76 - 1201.0
1,2-Dichloropropane 53.7 50 0 107 80 - 1201.0
1,3-Dichlorobenzene 48.96 50 0 97.9 80 - 1201.0
1,4-Dichlorobenzene 45.68 50 0 91.4 80 - 1201.0
2-Butanone 97.16 100 0 97.2 60 - 1402.0
2-Hexanone 81.47 100 0 81.5 60 - 1312.0
4-Methyl-2-pentanone 85.92 100 0 85.9 60 - 1352.0
Acetone 89.4 100 0 89.4 60 - 1402.0
Benzene 55.4 50 0 111 75 - 1221.0
Bromodichloromethane 54.54 50 0 109 75 - 1251.0
Bromoform 53.85 50 0 108 70 - 1301.0
Bromomethane 49.15 50 0 98.3 60 - 1401.0
Carbon disulfide 112.4 100 0 112 70 - 1302.0
Carbon tetrachloride 56.63 50 0 113 79 - 1201.0
Chlorobenzene 49.73 50 0 99.5 80 - 1201.0
Chloroethane 48.54 50 0 97.1 70 - 1301.0
Chloroform 53.64 50 0 107 70 - 1301.0
Chloromethane 44.25 50 0 88.5 65 - 1301.0
cis-1,2-Dichloroethene 55.52 50 0 111 75 - 1251.0
cis-1,3-Dichloropropene 50.21 50 0 100 79 - 1251.0
Cyclohexane 51.88 50 0 104 70 - 1301.0
Dibromochloromethane 52.67 50 0 105 70 - 1301.0
Dichlorodifluoromethane 37.84 50 0 75.7 60 - 1401.0
Ethylbenzene 54.77 50 0 110 80 - 1201.0
ALS Group USA, Corp Date: 07-Nov-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 36 of 47
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16101339
QC BATCH REPORT
Batch ID: R283975 Instrument: VOA4 Method: SW8260
Sample ID: HS16101336-02MS Units: ug/L Analysis Date: 01-Nov-2016 01:49
Run ID: VOA4_283975 SeqNo: 3876846 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MS
Client ID:
Isopropylbenzene 57.6 50 0 115 75 - 1301.0
m,p-Xylene 105.9 100 0 106 80 - 1202.0
Methyl acetate 47.52 50 0 95.0 76 - 1221.0
Methyl tert-butyl ether 53.98 50 0 108 70 - 1301.0
Methylcyclohexane 49.79 50 0 99.6 61 - 1581.0
Methylene chloride 54.46 50 0 109 65 - 1332.0
o-Xylene 54.34 50 0 109 80 - 1201.0
Styrene 56.77 50 0 114 78 - 1221.0
Tetrachloroethene 58.23 50 0 116 75 - 1301.0
Toluene 53.01 50 0 106 75 - 1211.0
trans-1,2-Dichloroethene 56.88 50 0 114 75 - 1251.0
trans-1,3-Dichloropropene 51 50 0 102 76 - 1251.0
Trichloroethene 57.39 50 0 115 71 - 1251.0
Trichlorofluoromethane 59.59 50 0 119 67 - 1321.0
Vinyl chloride 49.94 50 0 99.9 70 - 1351.0
Xylenes, Total 160.2 150 0 107 80 - 1243.0
45.58 50 0 91.2 71 - 1251.0Surr: 1,2-Dichloroethane-d4
48.21 50 0 96.4 70 - 1251.0Surr: 4-Bromofluorobenzene
50.72 50 0 101 74 - 1251.0Surr: Dibromofluoromethane
49.02 50 0 98.0 75 - 1251.0Surr: Toluene-d8
ALS Group USA, Corp Date: 07-Nov-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 37 of 47
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16101339
QC BATCH REPORT
Batch ID: R283975 Instrument: VOA4 Method: SW8260
Sample ID: HS16101336-02MSD Units: ug/L Analysis Date: 01-Nov-2016 02:14
Run ID: VOA4_283975 SeqNo: 3876847 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MSD
Client ID:
1,1,1-Trichloroethane 61.58 50 0 123 75 - 130 60.68 1.48 201.0
1,1,2,2-Tetrachloroethane 39.7 50 0 79.4 74 - 123 37.88 4.68 201.0
1,1,2-Trichlor-1,2,2-trifluoroethane 56.06 50 0 112 70 - 130 56.8 1.3 201.0
1,1,2-Trichloroethane 50.26 50 0 101 80 - 120 48.57 3.41 201.0
1,1-Dichloroethane 54.35 50 0 109 76 - 120 54.2 0.279 201.0
1,1-Dichloroethene 60.27 50 0 121 75 - 130 58.54 2.91 201.0
1,2,4-Trichlorobenzene 49.66 50 0 99.3 75 - 126 44.08 11.9 201.0
1,2-Dibromo-3-chloropropane 46.07 50 0 92.1 65 - 125 39.97 14.2 201.0
1,2-Dibromoethane 54.62 50 0 109 80 - 121 52.62 3.73 201.0
1,2-Dichlorobenzene 48.97 50 0 97.9 80 - 120 45.41 7.55 201.0
1,2-Dichloroethane 51.07 50 0 102 76 - 120 48.61 4.93 201.0
1,2-Dichloropropane 55.6 50 0 111 80 - 120 53.7 3.48 201.0
1,3-Dichlorobenzene 51.56 50 0 103 80 - 120 48.96 5.18 201.0
1,4-Dichlorobenzene 48.3 50 0 96.6 80 - 120 45.68 5.56 201.0
2-Butanone 101.9 100 0 102 60 - 140 97.16 4.76 202.0
2-Hexanone 93.18 100 0 93.2 60 - 131 81.47 13.4 202.0
4-Methyl-2-pentanone 87.98 100 0 88.0 60 - 135 85.92 2.37 202.0
Acetone 92.82 100 0 92.8 60 - 140 89.4 3.75 202.0
Benzene 57.37 50 0 115 75 - 122 55.4 3.51 201.0
Bromodichloromethane 56.08 50 0 112 75 - 125 54.54 2.79 201.0
Bromoform 55.59 50 0 111 70 - 130 53.85 3.18 201.0
Bromomethane 51.24 50 0 102 60 - 140 49.15 4.16 201.0
Carbon disulfide 113.3 100 0 113 70 - 130 112.4 0.811 202.0
Carbon tetrachloride 58.39 50 0 117 75 - 125 56.63 3.06 201.0
Chlorobenzene 50.59 50 0 101 80 - 120 49.73 1.72 201.0
Chloroethane 49.76 50 0 99.5 70 - 130 48.54 2.48 201.0
Chloroform 53.68 50 0 107 70 - 130 53.64 0.0751 201.0
Chloromethane 45.1 50 0 90.2 65 - 130 44.25 1.91 201.0
cis-1,2-Dichloroethene 57.17 50 0 114 75 - 125 55.52 2.92 201.0
cis-1,3-Dichloropropene 53.01 50 0 106 79 - 125 50.21 5.42 201.0
Cyclohexane 52.01 50 0 104 70 - 130 51.88 0.25 201.0
Dibromochloromethane 53.7 50 0 107 70 - 130 52.67 1.93 201.0
Dichlorodifluoromethane 37.03 50 0 74.1 60 - 140 37.84 2.17 201.0
Ethylbenzene 55.17 50 0 110 80 - 120 54.77 0.729 201.0
ALS Group USA, Corp Date: 07-Nov-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 38 of 47
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16101339
QC BATCH REPORT
Batch ID: R283975 Instrument: VOA4 Method: SW8260
Sample ID: HS16101336-02MSD Units: ug/L Analysis Date: 01-Nov-2016 02:14
Run ID: VOA4_283975 SeqNo: 3876847 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MSD
Client ID:
Isopropylbenzene 59.68 50 0 119 75 - 130 57.6 3.54 201.0
m,p-Xylene 109.3 100 0 109 80 - 120 105.9 3.21 202.0
Methyl acetate 47.28 50 0 94.6 76 - 122 47.52 0.498 201.0
Methyl tert-butyl ether 56.47 50 0 113 70 - 130 53.98 4.51 201.0
Methylcyclohexane 50.47 50 0 101 61 - 158 49.79 1.35 201.0
Methylene chloride 53.4 50 0 107 65 - 133 54.46 1.97 202.0
o-Xylene 55.67 50 0 111 80 - 120 54.34 2.41 201.0
Styrene 59 50 0 118 78 - 122 56.77 3.85 201.0
Tetrachloroethene 59.82 50 0 120 75 - 130 58.23 2.7 201.0
Toluene 54.42 50 0 109 75 - 121 53.01 2.64 201.0
trans-1,2-Dichloroethene 57.52 50 0 115 75 - 125 56.88 1.11 201.0
trans-1,3-Dichloropropene 52.75 50 0 106 76 - 125 51 3.39 201.0
Trichloroethene 61.07 50 0 122 71 - 125 57.39 6.22 201.0
Trichlorofluoromethane 60.04 50 0 120 67 - 132 59.59 0.76 201.0
Vinyl chloride 51.83 50 0 104 70 - 135 49.94 3.7 201.0
Xylenes, Total 165 150 0 110 80 - 124 160.2 2.94 203.0
45.9 50 0 91.8 71 - 125 45.58 0.702 201.0Surr: 1,2-Dichloroethane-d4
48.26 50 0 96.5 70 - 125 48.21 0.0971 201.0Surr: 4-Bromofluorobenzene
49.26 50 0 98.5 74 - 125 50.72 2.92 201.0Surr: Dibromofluoromethane
49.45 50 0 98.9 75 - 125 49.02 0.884 201.0Surr: Toluene-d8
The following samples were analyzed in this batch: HS16101339-06 HS16101339-07
ALS Group USA, Corp Date: 07-Nov-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 39 of 47
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16101339
QC BATCH REPORT
Batch ID: R284076 Instrument: ManTech01 Method: SM2320B
Sample ID: WBLKW1-161102 Units: mg/L Analysis Date: 02-Nov-2016 10:16
Run ID: ManTech01_284076 SeqNo: 3878729 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MBLK
Client ID:
Alkalinity, Bicarbonate (As CaCO3) U 5.00
Alkalinity, Carbonate (As CaCO3) U 5.00
Alkalinity, Hydroxide (As CaCO3) U 5.00
Alkalinity, Total (As CaCO3) U 5.00
Sample ID: LCS-ALK1-161102 Units: mg/L Analysis Date: 02-Nov-2016 10:25
Run ID: ManTech01_284076 SeqNo: 3878730 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
LCS
Client ID:
Alkalinity, Carbonate (As CaCO3) 1030 1000 0 103 80 - 1205.00
Alkalinity, Total (As CaCO3) 1056 1000 0 106 80 - 1205.00
Sample ID: LCSD-ALK1-161102 Units: mg/L Analysis Date: 02-Nov-2016 10:34
Run ID: ManTech01_284076 SeqNo: 3878731 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
LCSD
Client ID:
Alkalinity, Carbonate (As CaCO3) 1021 1000 0 102 80 - 120 1030 0.911 205.00
Alkalinity, Total (As CaCO3) 1048 1000 0 105 80 - 120 1056 0.729 205.00
Sample ID: HS16101161-01DUP Units: mg/L Analysis Date: 02-Nov-2016 10:49
Run ID: ManTech01_284076 SeqNo: 3878733 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
DUP
Client ID:
Alkalinity, Bicarbonate (As CaCO3) 108.8 110.8 1.77 205.00
Alkalinity, Carbonate (As CaCO3) U 0 0 205.00
Alkalinity, Hydroxide (As CaCO3) U 0 0 205.00
Alkalinity, Total (As CaCO3) 108.8 110.8 1.77 205.00
The following samples were analyzed in this batch: HS16101339-01 HS16101339-03 HS16101339-05
ALS Group USA, Corp Date: 07-Nov-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 40 of 47
Client:Project:
Golder AssociatesCity of Camdenton
WorkOrder: HS16101339
QC BATCH REPORT
Batch ID: R284304 Instrument: TOC_02 Method: SW9060
Sample ID: WBLKW1-110616 Units: mg/L Analysis Date: 06-Nov-2016 16:35
Run ID: TOC_02_284304 SeqNo: 3883060 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MBLK
Client ID:
Organic Carbon, Total U 1.00
Sample ID: WLCSW1-110616 Units: mg/L Analysis Date: 06-Nov-2016 16:52
Run ID: TOC_02_284304 SeqNo: 3883061 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
LCS
Client ID:
Organic Carbon, Total 9.639 10 0 96.4 80 - 1201.00
Sample ID: WLCSDW1-110616 Units: mg/L Analysis Date: 06-Nov-2016 17:07
Run ID: TOC_02_284304 SeqNo: 3883062 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
LCSD
Client ID:
Organic Carbon, Total 9.613 10 0 96.1 80 - 120 9.639 0.27 201.00
Sample ID: HS16101339-01MS Units: mg/L Analysis Date: 06-Nov-2016 17:40
Run ID: TOC_02_284304 SeqNo: 3883064 PrepDate: DF: 1
Analyte SPK ValPQLResultSPK Ref
Value %RECControl
LimitRPD Ref
Value %RPDRPD Limit Qual
MS
Client ID: MWPT-1
Organic Carbon, Total 9.797 10 0.449 93.5 80 - 1201.00
The following samples were analyzed in this batch: HS16101339-01 HS16101339-03 HS16101339-05
ALS Group USA, Corp Date: 07-Nov-16
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 41 of 47
QUALIFIERS, ACRONYMS, UNITS
Client:Project:WorkOrder:
Golder AssociatesCity of CamdentonHS16101339
Qualifier Description* Value exceeds Regulatory Limit
a Not accredited
B Analyte detected in the associated Method Blank above the Reporting Limit
E Value above quantitation range
H Analyzed outside of Holding Time
J Analyte detected below quantitation limit
M Manually integrated, see raw data for justification
n Not offered for accreditation
ND Not Detected at the Reporting Limit
O Sample amount is > 4 times amount spiked
P Dual Column results percent difference > 40%
R RPD above laboratory control limit
S Spike Recovery outside laboratory control limits
U Analyzed but not detected above the MDL/SDL
Acronym DescriptionDCS Detectability Check Study
DUP Method Duplicate
LCS Laboratory Control Sample
LCSD Laboratory Control Sample Duplicate
MBLK Method Blank
MDL Method Detection Limit
MQL Method Quantitation Limit
MS Matrix Spike
MSD Matrix Spike Duplicate
PDS Post Digestion Spike
PQL Practical Quantitaion Limit
SD Serial Dilution
SDL Sample Detection Limit
TRRP Texas Risk Reduction Program
Unit Reported Descriptionµg/L Micrograms per Liter
ALS Group USA, Corp Date: 07-Nov-16
Page 42 of 47
CERTIFICATIONS,ACCREDITATIONS & LICENSES
Agency Number Expire Date
Arkansas 16-022-1 27-Mar-2017
California 2919 2016-2018 31-Jul-2018
Illinois 003872 09-May-2017
Kansas E-10352 2016-2017 31-Jul-2017
Kentucky 96 2016-2017 30-Apr-2017
Louisiana 03087 2016-2017 30-Jun-2017
North Carolina 624 - 2016 31-Dec-2016
North Dakota R193 2016-2017 30-Apr-2017
Oklahoma 2016-122 31-Aug-2017
Texas TX104704231-16-17 30-Apr-2017
07-Nov-16Date: ALS Group USA, Corp
Page 43 of 47
Client: Golder Associates
Work Order: HS16101339Project: City of Camdenton SAMPLE TRACKING
Lab Samp ID Client Sample ID Action Date Person New Location
HS16101339-01 MWPT-1 Out 11/1/2016 3:34:37 PM PVL METPREP
HS16101339-03 MWPT-3 Out 11/1/2016 3:34:37 PM PVL METPREP
HS16101339-05 MWPT-4 Out 11/1/2016 3:34:37 PM PVL METPREP
HS16101339-01 MWPT-1 Return 11/1/2016 3:35:00 PM PVL 19A
HS16101339-03 MWPT-3 Return 11/1/2016 3:35:00 PM PVL 19A
HS16101339-05 MWPT-4 Return 11/1/2016 3:35:00 PM PVL 19A
HS16101339-01 MWPT-1 Out 11/3/2016 9:55:43 AM JCJ METPREP
HS16101339-03 MWPT-3 Out 11/3/2016 9:55:43 AM JCJ METPREP
HS16101339-05 MWPT-4 Out 11/3/2016 9:55:43 AM JCJ METPREP
HS16101339-01 MWPT-1 Return 11/3/2016 9:55:57 AM JCJ 19A
HS16101339-03 MWPT-3 Return 11/3/2016 9:55:57 AM JCJ 19A
HS16101339-05 MWPT-4 Return 11/3/2016 9:55:57 AM JCJ 19A
ALS Group USA, Corp 07-Nov-16Date:
Page 44 of 47
PMG
29-Oct-2016 09:30Date/Time Received:
HS16101339
Golder St Louis
Work Order:
Client Name:
Sample Receipt Checklist
Received by:
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
Container/Temp Blank temperature in compliance?
Temperature(s)/Thermometer(s):
Cooler(s)/Kit(s):
Date/Time sample(s) sent to storage:
Water - VOA vials have zero headspace?
Water - pH acceptable upon receipt?
pH adjusted?
pH adjusted by:
Login Notes:
No Not Present
Yes No Not Present
Yes No Not Present
Yes No
Yes No
Yes No
Yes No
Yes No
Yes No
Yes No
Yes No
2.0/2.7 uc/c 112483310/29/2016 01:30pm
Yes No No VOA vials submitted
Yes No N/A
Yes No N/A
Checklist completed by: Cesar A. LiraDateeSignatureDateeSignature
31-Oct-201629-Oct-2016
FedExWater Carrier name:Matrices:
Reviewed by: Dane J. Wacasey
Client Contacted: Date Contacted: Person Contacted:
Contacted By: Regarding:
Comments:
Corrective Action:
Yes
NoYesTX1005 solids received in hermetically sealed vials? N/A
ALS Group USA, Corp 07-Nov-16Date:
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