Work package #2(DEVELOPMENT)
WARIALWeb Accessed Remote Instrumental Analytical Laboratory
FIRST OVERVIEW OF QUESTIONARIES:1. Laboratory Instrument Availability2. Your Computer & Your Suggestions
Darko & Tatjana AnđelkovićUniversity of Niš
Faculty of Science and [email protected]
INSTRUMENT in your Lab, eventually available for NETCHEMshort description: type of instrument, producer, model, e.g. GC-MS AGILENT 6893
with FID detector
Questionary no. 1 – Laboratory Instrument Availability
Institution Instrument
P-01 UN Thermo HR ESI MS LTQ Orbitrap & HPLC Thermo AccelaThermo ESI MS Advantage & HPLC Thermo AccelaThermo ESI MS Deca & HPLC Thermo SurveyorAgilent GC/MS single quad 6983/MSD 5973 with auto sampler
P-03 UoG Thermally stimulated current spectrometer (TSC)Thermal gravimetric analysator (TGA)JEOL FT NMR 500 MHz (ECA500)JEOL FT NMR 400 MHz
P-04 BUT GC×GC/TOF MS
P-06 UB Agilent GC-MS (GC 7890B, MSD 5977)WD-XRF Thermo Scientific ARL Performix XRF
INSTRUMENT in your Lab, eventually available for NETCHEMshort description: type of instrument, producer, model, e.g. GC-MS AGILENT 6893
with FID detector
Questionary no. 1 – Laboratory Instrument Availability
Institution Instrument
P-07 UNS HPLC DAD (Agilent Infinity 1260)GC-MS SHIMADZU Ultra QP-2010 with FID detector
P-08 UNIKG AAS Perkin Elmer 3300HPLC DAD (SDPM20A)GC-MS (GC6890N, MSD 5975B)UV-VIS Spectrometer Agilent CARRY 300
P-10 UT UV VIS spectrometer ShimadzuElectrochemical analyzer MEC-12B Jiangsu Jiangfen electrochemical instument inc.AAS GF, NovAA 400 Analytik Jena
OTHER INST. Still waiting for approval...
TOTAL: 20 instruments available
USAGE of instrumenthow it may be involved in NETCHEM educational programme
(you may choose both A and B answers)
Questionary no. 1 – Laboratory Instrument Availability
A) through WARIAL
internet access, remote meetings…e.g.
B) NOT WARIALnot on-line, for other OERs, video-clips…
1. Thermo HR ESI MS LTQ Orbitrap & HPLC Thermo Accela
2. Thermo ESI MS Advantage & HPLC Thermo Accela3. Thermo ESI MS Deca & HPLC Thermo Surveyor4. Agilent GC/MS single quad 6983/MSD 5973 with auto
sampler5. Thermally stimulated current spectrometer (TSC)6. Thermal gravimetric analysator (TGA) – MAYBE7. JEOL FT NMR 500 MHz (ECA500)8. JEOL FT NMR 400 MHz9. GC×GC/TOF MS10. Agilent GC-MS (GC 7890B, MSD 5977)11. WD-XRF Thermo Scientific ARL Performix XRF12. HPLC DAD (Agilent Infinity 1260)13. GC-MS SHIMADZU Ultra QP-2010 with FID14. AAS Perkin Elmer 3300 (no answer ?)15. HPLC DAD (SDPM20A)16. GC-MS (GC6890N, MSD 5975B)17. UV-VIS Spectrometer Agilent CARRY 30018. UV VIS spectrometer Shimadzu19. Electrochemical analyzer MEC-12B Jiangsu Jiangfen
electrochemical instument inc.20. AAS GF, NovAA 400 Analytik Jena
1. Thermo HR ESI MS LTQ Orbitrap & HPLC Thermo Accela2. Thermo ESI MS Advantage & HPLC Thermo Accela3. Thermo ESI MS Deca & HPLC Thermo Surveyor4. Agilent GC/MS single quad 6983/MSD 5973 with auto sampler5. Thermal gravimetric analysator (TGA)6. JEOL FT NMR 500 MHz (ECA500)7. JEOL FT NMR 400 MHz8. AAS Perkin Elmer 3300 (no answer ?)9. GC-MS (GC6890N, MSD 5975B)10. UV-VIS Spectrometer Agilent CARRY 30011. UV VIS spectrometer Shimadzu12. Electrochemical analyzer MEC-12B Jiangsu Jiangfen
electrochemical instument inc.13. AAS GF, NovAA 400 Analytik Jena
Characteristics of Instrumental PC & Extra PC in Labs
Questionary no. 1 – Laboratory Instrument Availability
Instrument PC (directly connected) Extra PC(near instrument)
Institution/Instrument Inter-net
Hardware OS Software TeamViewer
Camera &Headphone set
P01-UN/Thermo HR ESI MS LTQ Orbitrap & HPLC Accela
LAN & WiFi
4 GB RAM1920×1080
Win XP 32 bit
Thermo eXcalibur 2.4 YES Not now, can provide
P01-UN/Thermo ESI MS Advantage & HPLC Accela
LAN & WiFi
1 GB RAM1920×1080
Win XP SP2
Thermo eXcalibur 1.4 Maybe Not now, can provide
P01-UN/Thermo ESI MS Deca & HPLC Thermo Surveyor
LAN & WiFi
512 MB RAM1920×1080
Win 2000 Thermo eXcalibur 1.3 YES YES
P01-UN/Agilent GC/MS single quad 6983/MSD 5973 & AS
LAN & WIFi
512 MB RAM1280×1024
Win XP SP3
MSD ChemStation D02.00.275
YES Not now, can provide
P03-UoG/TSC – Thermally stimulated current spectr.
In future
Old PC Win XP GPIB Cable NI Instruments National
NO Not now, can provide
P03-UoG/Thermal gravimetric analyser (TGA)
In future
Old PC Win XP GPIB Cable NI Instruments National
NO Not now, can provide
P03-UoG/JEOL FT NMR 500 MHz (ECA500)
LAN unknown Win 7 unknown NO Not now, can provide
P03-UoG/JEOL FT NMR 400 MHz
LAN unknown Win 7 unknown NO Not now, can provide
Characteristics of Instrumental PC & Extra PC in Labs
Questionary no. 1 – Laboratory Instrument Availability
Instrument PC (directly connected) Extra PC(near instrument)
Institution/Instrument Inter-net
Hardware OS Software TeamViewer
Camera &Headphone set
P04-BUT/GC×GC/TOF MS LAN 2 monitors Win 7 Chroma TOF (LECO) YES Not now, can provide
P06-UB/Agilent GC-MS (GC 7890B, MSD 5977),
In future
unknown unknown MSD Chem Station, Mass Hunter
No answer
Noanswer
P06-UB/WD-XRF Thermo Scientific ARL Performix XRF
YES PC year 2012 Win 7 OXAS, UniQuant YES YES
P07-UNS/HPLC DAD (Agilent Infinity 1260)
NO y. 2014, 4GB 1280×1024
Win 764 bit
Agilent OpenLab CDS Chemstation
YES Not now, can provide
P07-UNS/GC-MS SHIMADZU Ultra QP-2010 with FID
YES 4 GB RAM 1440×900
32-bit OS Lab Solutions GC-MS solutions Shimadzu
YES Not now, can provide
P08- UNIKG/AAS Perkin Elmer 3300
NO Year 1996 unknown unknown YES NO
P08- UNIKG/HPLC DAD (SDPM20A)
NO Year 2008 Win XP LC Solution NO NO
P08- UNIKG/UV-VIS Spectr. Agilent CARRY 300
LAN unknown Win 7 Agilent CARRY YES YES
P08- UNIKG/Agilent GC/MS 6890N/5975B
LAN Year 2007 Win XP 32 bit SP2
Agilent ChemStation Software
NO NO
Characteristics of Instrumental PC & Extra PC in Labs
Questionary no. 1 – Laboratory Instrument Availability
Instrument PC (directly connected) Extra PC(near instrument)
Institution/Instrument Inter-net
Hardware OS Software TeamViewer
Camera &Headphone set
P10-UT/UV-VIS spectrometer Shimadzu
LAN unknown Win XPWin 2000
UV Probe Versioni 1.11 NO Not now, can provide
P10-UT/Electrochem analyzer MEC-12B Jiangsu Jiangfe
LAN Year 2008 Win XPWin 2000
unknown No answer
Noanswer
P10-UT/AAS GF, NovAA 400 Analytik Jena
LAN unknown Win XP unknown NO Not now, can provide
Questionary no. 1 – Laboratory Instrument Availability
WARIAL Service... last 4 questions in the Questionary no. 1
14. What kind of educational service you may provide with this
instrument?• e.g. running HPLC sample for 15-20 min
• calibration of mass spectrometer
• procedure of cleaning/maintenance/replacement…
• sample preparation
• evaluation of analytical data
• consulting on chromatographic data, IR spectra
• on-line video call in scheduled time, but without remote control of instrument, etc.
15. Do you use this instrument for student exercises now?lecture in classical way – directly with student group on the site/lab where instrument is installed
16. How frequently this instrument can be used remotely through
WARIAL, within your institution?e.g. 8 × 60 min per semester for student exercises, including me and 3 other professors &
assistants…
17. How frequently this instrument can be offered (WARIAL connected) to
other – remote – institutions?• e.g. approx. 3 × 45 min per semester for remote student exercises;
• up to 2 hours per month to give professional consulting to colleagues from other Universities or
SMEs
WARIAL Service in your institution and for external users
Questionary no. 1 – Laboratory Instrument Availability
Institution/Instrument 14. 15. 16. (inside) 17. (outside)
P01-UN/Thermo HR ESI MS LTQ Orbitrap & HPLC Accela
Running HR MS analysis, calibration of instrument, evaluation of data
NO 4×45 min per semestar 4×45 min per semestar
P01-UN/Thermo ESI MS Advantage & HPLC Accela
Running ESI MS analysis, efects of instrument parameters
YES 3×45 min per semestar 2×45 min per semestar
P01-UN/Thermo ESI MS Deca & HPLC Thermo Surveyor
Running MS analysis, evaluation of data, instrument tunning
NO 3×45 min per semestar 2×45 min per semestar
P01-UN/Agilent GC/MS single quad 6983/MSD 5973 & AS
Running GC analysis, evaluation of data, EI MS library search
NO 5×60 min per semestar 4×60 min per semestar
P03-UoG/TSC – Thermally stimulated current spectr.
Running calibration, evaluation of data
NO As many as we agree Would depend on availability of instrument and staff
P03-UoG/Thermal gravimetric analysator (TGA)
Running calibration, evaluation of data
NO As many as we agree Would depend on availability of instrument and staff
P03-UoG/JEOL FT NMR 500 MHz (ECA500)
Running NMR samples, sample preparation, evaluation
YES 8×60 min per semestar 6×60 min per semestar
P03-UoG/JEOL FT NMR 400 MHz
Running NMR samples, sample preparation, evaluation
YES 8×60 min per semestar 6×60 min per semestar
WARIAL Service in your institution and for external users
Questionary no. 1 – Laboratory Instrument Availability
Institution/Instrument 14. 15. 16. (inside) 17. (outside)
P04-BUT/GC×GC/TOF MS Running sample in in 2d-GC (GC×GC), data evaluation
YES Depends on assesment Depends on assesment
P06-UB/Agilent GC-MS (GC 7890B, MSD 5977),
Sample analysis, data evaluation YES No answer No answer
P06-UB/WD-XRF Thermo Scientific ARL Performix XRF
Sample preparation, analysis, data evaluation
YES 5× per semestar 3×120 min per semestar
P07-UNS/HPLC DAD (Agilent Infinity 1260)
Running sample for 15 – 20 min, procedure of cleaning, mainte-nance and replacement, sample preparation, data evaluation
YES 5×60 min per semestar 2×45 min per semestar
P07-UNS/GC-MS SHIMADZU Ultra QP-2010 with FID
Sample preparation, evaluation of data, running GC analysis
YES 5×60 min per semestar 2×45 min per semestar
P08- UNIKG/AAS Perkin Elmer 3300
Evaluation of analytical data YES 8×60 min per semestar 4×60 min per semestar
P08- UNIKG/HPLC DAD (SDPM20A)
Running of HPLC sample, evaluation of data
YES Few times per month Few times per month
P08- UNIKG/UV-VIS Spectr. Agilent CARRY 300
Running UV-VIS sample, biochemical interactions noble metals – ligands; stabil. const. etc
YES Approx. 4×60 min per week
Approx. 4×60 min per week
P08- UNIKG/Agilent GC/MS 6890N/5975B
Calibration of MSD, cleaning, replacement of septa, gold seal cleaning of inlet, GC col. replac.
YES No answer 2×60 min per month
WARIAL Service in your institution and for external users
Questionary no. 1 – Laboratory Instrument Availability
Institution/Instrument 14. 15. 16. (inside) 17. (outside)
P10-UT/UV-VIS spectrometer Shimadzu
Calibration, procedure of cleaning, maintence & replacement, sample preparation, evaluation of analytical data
YES 15×60 min per semester for student excercises
3×45 min per semester for remote student exercises;up to 2 hours per month to give professional consulting to coleagues from other Universities or SMEs
P10-UT/Electrochem analyzer MEC-12B Jiangsu Jiangfe
Calibration, procedure of cleaning, maintence & replacement, sample preparation, evaluation of analytical data
YES 15×60 min per semester for student excercises
3×45 min per semester for remote student exercises;up to 2 hours per month to give professional consulting to coleagues from other Universities or SMEs
P10-UT/AAS GF, NovAA 400 Analytik Jena
Sample preparation, analysis, data evaluation
YES 8×60 min per semester for student excercises
3×45 min per semester for remote student exercises;up to 2 hours per month to give professional consulting to coleagues from other Universities or SMEs
Questionary no. 2 – Your computer and Your suggestions(24 received answers)
1/7: On your own computer(s), do you have and use:hardware & software on personal home/business computer/laptop, not on PC connected to the Instrument
Microsoft Windows 10 operating
system?
YES: ●●●●●●●●●●●●●●●●● 71%
NO: ●●●●●● 25%
Partially: ● 4%
Microsoft Account to log on your
computer?
YES: ●●●●●●●●●●●●●●●●●● 75%
NO: ●●●●●● 25%
Partially: 0%
MS OneDrive (15 GB – 1 TB cloud data
storage)
YES: ●●●●●●●●●● 42%
NO: ●●●●●●●●●●●● 50%
Partially: ●● 8%
MS Office 2016 (desktop) or Office 365YES: ●●●●●●●●●● 42%
NO: ●●●●●●●●●●●●●● 58%
Partially: 0%
MS Outlook 2016/365 – contacts and
calendars
YES: ●●●●●●●●●● 42%
NO: ●●●●●●●●●●●●●● 58%
Partially: 0%
MS OneNote (.one files) – notebooksYES: ●●●●●● 25%
NO: ●●●●●●●●●●●●●●●●● 71%
Partially: ● 4%
Questionary no. 2 – Your computer and Your suggestions
2/7: On your own computer(s), do you have and use:hardware & software on personal home/business computer/laptop, not on PC connected to the Instrument
MS Windows Ink – tool for free-hand
drawing
YES ●● 8%
NO ●●●●●●●●●●●●●●●●●●●●● 88%
Partially ● 4%
Are you familiar with TeamViewer
software?
YES ●●●●●●●●●●●●●●●● 67%
NO ●●●●● 21%
Partially ●●● 12%
Are you familiar with SKYPE software?YES ●●●●●●●●●●●●●●●●●●●●● 88%
NO 0%
Partially ●●● 12%
Some other PC/mobile communication
software that may be of interest for
NETCHEM/WARIAL
P-01 UN WhatsUp, Viber, Messenger
P-02 UPMC (no answer)
P-03 UoG (no answer)
P-04 BUT (no answer)
P-06 UB (no answer)
P-07 UNS (no answer)
P-08 UNIKG (no answer)
P-10 UT WhatsUp, Viber, Messenger
Questionary no. 2 – Your computer and Your suggestions
3/7: WARIAL OFFERS & DEMANDSWhat kind of specialized Instrument
Driver Software are you familiar with?
• e.g. Agilent GC MSD ChemStation Quant Method
Translator
• nothing special, other colleagues work with it
• not personally, but in the lab we have installed THERMO
MS 4.0.28
P-01 UN Agilent GC-MS MSD ChemStation
Thermo eXcalibur
Perkin Elmer AAS AAnalyst 300
UV-VIS GBC Cintra 1010
P-02 UPMC (no answer)
P-03 UoG Origin
Microcal
JEOL Delta
Mestrec Generic NMR Software
(no answer)
P-04 BUT (no answer)
P-06 UB Oxas
UniQuant
Agilent GC MSD ChemStation
P-07 UNS (no answer)
Agilent OpenLab CDS ChemStation
P-08 UNIKG UV WinLab and Pro-Data
LC Solution, Shimadzy
P-10 UT Win AAS; MEC-12
UV probe ver. 1.11
Analyst, Sciex
(no answer)
Agilent GC-MSD Chemstation
Questionary no. 2 – Your computer and Your suggestions
4/7: WARIAL OFFERS & DEMANDSWhat kind of WARIAL content would you like to add in your lectures?
e.g. remote instrument access FT-IR for solid samples;GC-MS for multiple pesticide residues (student Master 2 level);tunning of High Res Mass Spectrometer (for my own education/consulting)I cannot decide nowyou may give several answers for you and what expected for your colleagues
P-01 UN GC-MS phthalates and pesticides quantificat.
MS MALDI for humic substances,
Calibration of Orbitrap
Running pesticides on HPLC HR ESI-MS,
Consulting/exprertise on specific
ESI-MS chromatogram/spectra for my own
P-02 UPMC (no lab, can provide names)
P-03 UoG I cannot decide nowP04 BUT Optimizing of GC×GC preparation
P06 UB I cannot decide now
(no answer)
P-07 UNS I cannot decide now
P-08 UNIKG I cannot decide now
Tuning of LC-MS instrument
for my own and student education,
Remote instrumental access for ESI-MS,
Remote instr. access for fluorimetric measur.
P-10 UT AAS-GF for heavy metals in water
and air samples,
Development of carbon paste electrodes,
I cannot decide now
Questionary no. 2 – Your computer and Your suggestions
5/7: WARIAL OFFERS & DEMANDSHow frequently would you like to utilize WARIAL from other Labs for your demands?
e.g. 2×1 hour per week for my PhD student on NMR 600 MHz;several hours per month for my own training on GC-MS Triple-Quadyou may give several answers for you and what expected for your colleagues
P-01 UN several hours per month
P-02 UPMC (no lab, can ask other persons)
P-03 UoG (no answer)P04 BUT will depend on offer
P06 UB few times in semester,
(no answer)
P-07 UNS 5×60 min per semester,
(no answer)
P-08 UNIKG Several hours per month,
2×60 min per month,
1×60 min per week,
2×60 min per week for my PhD student on
NMR 600 MHz,
several hours per month for my own training
on GC-MS Triple-Quad,
several hours per month for my own training
on GC-MS,
(no answer)
P-10 UT 2×60 min per week for MSc students AAS-GF1×60 min per week for MSc students
Questionary no. 2 – Your computer and Your suggestions
6/7: WARIAL OFFERS & DEMANDSWho may be the Contact person – coordinator for WARIAL working team in your Lab?
give one or two names of employees who will be coordinator(s) for WARIAL establishment and testing in front of your institution
P-01 UN Tatjana Anđelković, Ivana Kostić,
Milica Branković, Darko Anđelković
(but WHO is coordinator ???)
P-02 UPMC (no lab, can provide name)P-03 UoG Andy Mendham, Mark Allan, Milan AntonijevićP04 BUT Josef Časlavsky, Ludmila Mrav.P06 UB Jovana Orlić (za XRF)
P-07 UNS Ivana Mihajlović, Maja Đogo, (no laboratory)
P-08 UNIKG Jovana Bogojeski, Snežana Jovanović, Zorka Stanić,
Andrija Ćirić, Marina Ćendić, Verica Jevtić, Nenad Vuković
Milena Vukić, Ivan JakovljevićP-10 UT M. Vasjari, A. Shehu, N. Broli
Other person(s) FOR WARIAL
service in your Lab?
(members of WARIAL
working team)
give one or more suggestions – names &
contacts of employees
P-01 UN Tatjana Anđelković, Ivana Kostić,
Milica Branković, Darko Anđelković
P-02 UPMC (no lab, can provide names)
P-03 UoG (no answer), my PhD studentP04 BUT (no answer)P06 UB Jovana Orlić (za XRF), (no answer)
P-07 UNS Maja Sremački, Mladenka Novaković, (no laboratory)
P-08 UNIKG Andrija Ćirić, Zoran Simić, Ivan Jakovljević,
Marija Jeremić; Zoran Matović
P-10 UT MS.Duka, E. Begu, L. Vallja, S. Cenolli
Questionary no. 2 – Your computer and Your suggestions
7/7: WARIAL OFFERS & DEMANDSAny additional suggestion?
Thanks!
• no questions• no initiatives• no ideas• no suggestions• no discussion
TO-DO LIST1. Send ONE or TWO names of employees who will be coordinator(s) for WARIAL
establishment and testing in front of your institution.Send names to [email protected] until 20th July 2017.
2. Prepare yourselves and one of your team member for meeting in Tirana (Sep 2017)to present in 10 – 15 minutes your WARIAL remote access trial(each institution will have 10 – 15 minutes in Agenda of Tirana meeting).
Short presentation may be given in free-form and may comprise, for example:
a) description of your instrument in lab (one that will be involved in WARIAL)b) picture of lab site and instrumentc) describe configuration of PC with TeamViewer (instr.), PC for SKYPE
communication (extra PC)d) your experience with configuration, internet connectione) describe experience with first trial of WARIAL sessionf) experience of your WARIAL partner (from your institution or external one)g) video-clip of your lab, learning classroomh) video clip of recorded WARIAL session... etc.
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