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Page 1: Supporting Information for Liu, Okamoto, Alexy, Hong, Tran ...authors.library.caltech.edu/66506/4/ja6b02153_si_002.pdf · Supporting Information for Liu, Okamoto, Alexy, Hong, Tran,

SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz

SI-67

1H NMR and 13C NMR Spectra of New Compounds

1 H N

MR

(500

MH

z, C

DC

l 3) o

f com

poun

d 3aa.

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SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz

SI-68

13C

NM

R (1

25 M

Hz,

CD

Cl 3)

of c

ompo

und 3aa.

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SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz

SI-69

1 H N

MR

(500

MH

z, C

DC

l 3) o

f com

poun

d 5aa.

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SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz

SI-70

13C

NM

R (1

25 M

Hz,

CD

Cl 3)

of c

ompo

und 5aa.

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SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz

SI-71

1 H N

MR

(500

MH

z, C

6D6)

of c

ompo

und 5ab.

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SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz

SI-72

13C

NM

R (1

25 M

Hz,

CD

Cl 3)

of c

ompo

und 5ab.

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SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz

SI-73

1 H N

MR

(500

MH

z, C

6D6)

of c

ompo

und 5ac.

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SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz

SI-74

13C

NM

R (1

25 M

Hz,

CD

Cl 3)

of c

ompo

und 5ac.

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SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz

SI-75

1 H N

MR

(500

MH

z, C

6D6)

of c

ompo

und 5ad.

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SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz

SI-76

13C

NM

R (1

25 M

Hz,

C6D

6) o

f com

poun

d 5ad.

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SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz

SI-77

1 H N

MR

(500

MH

z, C

DC

l 3) o

f com

poun

d 5ae.

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SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz

SI-78

13C

NM

R (1

25 M

Hz,

CD

Cl 3)

of c

ompo

und 3aa.

13C

NM

R (1

25 M

Hz,

CD

Cl 3)

of c

ompo

und 5ae.

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SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz

SI-79

1 H N

MR

(500

MH

z, C

DC

l 3) o

f com

poun

d 5af.

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SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz

SI-80

13C

NM

R (1

25 M

Hz,

CD

Cl 3)

of c

ompo

und 5af.

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SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz

SI-81

1 H N

MR

(400

MH

z, C

DC

l 3) o

f com

poun

d 5ag.

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SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz

SI-82

13C

NM

R (1

25 M

Hz,

CD

Cl 3)

of c

ompo

und 5ag.

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SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz

SI-83

1 H N

MR

(500

MH

z, C

DC

l 3) o

f com

poun

d 5ba.

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SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz

SI-84

13C

NM

R (1

25 M

Hz,

CD

Cl 3)

of c

ompo

und 5ba.

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SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz

SI-85

1 H N

MR

(500

MH

z, C

DC

l 3) o

f com

poun

d 5ca.

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SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz

SI-86

13C

NM

R (1

25 M

Hz,

CD

Cl 3)

of c

ompo

und 5ca.

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SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz

SI-87

1 H

NM

R (5

00 M

Hz,

CD

Cl 3)

of c

ompo

und 5da.

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SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz

SI-88

13C

NM

R (1

25 M

Hz,

CD

Cl 3)

of c

ompo

und 5da.

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SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz

SI-89

1 H N

MR

(400

MH

z, C

DC

l 3) o

f com

poun

d 5ea.

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SI-90

13C

NM

R (1

00 M

Hz,

CD

Cl 3)

of c

ompo

und 5ea.

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SI-91

1 H N

MR

(400

MH

z, C

DC

l 3) o

f com

poun

d 5fa.

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SI-92

13C

NM

R (1

00 M

Hz,

CD

Cl 3)

of c

ompo

und 5fa.

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SI-93

1 H

NM

R (4

00 M

Hz,

CD

Cl 3)

of c

ompo

und 1a

.

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SI-94

13C

NM

R (1

25 M

Hz,

CD

Cl 3)

of c

ompo

und 1a

.

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SI-95

1 H N

MR

(400

MH

z, C

DC

l 3) o

f com

poun

d 1d

.

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SI-96

13C

NM

R (1

25 M

Hz,

CD

Cl 3)

of c

ompo

und 1d

.

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SI-97

1 H N

MR

(400

MH

z, C

DC

l 3) o

f com

poun

d 1e

.

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SI-98

13

C N

MR

(100

MH

z, C

DC

l 3) o

f com

poun

d 1e

.

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SI-99

1 H N

MR

(400

MH

z, C

DC

l 3) o

f com

poun

d 1f.

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SI-100

13C

NM

R (1

00 M

Hz,

CD

Cl 3)

of c

ompo

und 1f

.

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SI-101

1 H N

MR

(400

MH

z, C

DC

l 3) o

f com

poun

d S5aa.

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SI-102

13C

NM

R (1

00 M

Hz,

CD

Cl 3)

of c

ompo

und S5aa

.

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SI-103

1 H N

MR

(500

MH

z, C

DC

l 3) o

f com

poun

d 7aa.

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SI-104

13

C N

MR

(125

MH

z, C

DC

l 3) o

f com

poun

d 7aa.

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SI-105

1 H N

MR

(500

MH

z, C

DC

l 3) o

f com

poun

d 7aa’.

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SI-106

13C

NM

R (1

25 M

Hz,

CD

Cl 3)

of c

ompo

und 7aa’

.

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SI-107

1 H N

MR

(500

MH

z, C

DC

l 3) o

f com

poun

d 7ba.

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SI-108

13C

NM

R (1

25 M

Hz,

CD

Cl 3)

of c

ompo

und 7ba.

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SI-109

1 H N

MR

(500

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z, C

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d 7ba’.

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SI-110

13C

NM

R (1

25 M

Hz,

CD

Cl 3)

of c

ompo

und 7ba’

.

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SI-111

1 H N

MR

(500

MH

z, C

DC

l 3) o

f com

poun

d 7ca.

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SI-112

13C

NM

R (1

25 M

Hz,

CD

Cl 3)

of c

ompo

und 7ca.

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SI-113

1 H N

MR

(500

MH

z, C

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poun

d 7ca’.

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SI-114

13C

NM

R (1

25 M

Hz,

CD

Cl 3)

of c

ompo

und 7ca’

.

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SI-115

1 H N

MR

(500

MH

z, C

DC

l 3) o

f com

poun

d 7da.

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SI-116

13C

NM

R (1

25 M

Hz,

CD

Cl 3)

of c

ompo

und 7da.

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SI-117

1 H N

MR

(500

MH

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d 7da’.

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SI-118

13C

NM

R (1

25 M

Hz,

CD

Cl 3)

of c

ompo

und 7da’

.

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SI-119

1 H N

MR

(500

MH

z, C

DC

l 3) o

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SI-120

13C

NM

R (1

25 M

Hz,

CD

Cl 3)

of c

ompo

und 7ab.

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SI-121

1 H N

MR

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d 7ab’.

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SI-122

13C

NM

R (1

25 M

Hz,

CD

Cl 3)

of c

ompo

und 7ab’

.

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SI-123

1 H N

MR

(500

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z, C

DC

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SI-124

13C

NM

R (1

25 M

Hz,

CD

Cl 3)

of c

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und 7ad.

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SI-125

1 H N

MR

(500

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SI-126

13C

NM

R (1

25 M

Hz,

CD

Cl 3)

of c

ompo

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