Supplemental Limited Site
Investigation
Lot 22
SW Quadrant Orange Avenue at Mary Louis Lane
Kissimmee, Osceola County, Florida
June 29, 2018
Terracon Project No. H1177166A
Prepared for:
Deerfield Land Corporation
Orlando, Florida
Prepared by:
Terracon Consultants, Inc.
Winter Park, Florida
TABLE OF CONTENTS
ii
1.0 SITE DESCRIPTION ....................................................................................................... 1 2.0 PREVIOUS ASSESSMENT ............................................................................................ 1 3.0 SCOPE OF SERVICES ................................................................................................... 2
3.1 Standard of Care.................................................................................................. 2 3.2 Additional Scope Limitations ................................................................................ 2 3.3 Reliance ............................................................................................................... 3
4.0 SUPPLEMENTAL SOIL TESTING .................................................................................. 3 5.0 CONCLUSIONS .............................................................................................................. 4
APPENDIX A – EXHIBITS
Exhibit 1 – Topographic Map
Exhibit 2 – Soil Sample Locations Map
APPENDIX B – TABLES
Table 1 – Soil Arsenic Analytical Summary
APPENDIX C – PREVIOUS SOURCE REMOVAL REPORT EXCERPTS
APPENDIX D – ANALYTICAL REPORT AND CHAIN OF CUSTODY
Responsive ■ Resourceful ■ Reliable
SUPPLEMENTAL LIMITED SITE INVESTIGATION
LOT 22
SW QUADRANT ORANGE AVENUE AT MARY LOUIS LANE
KISSIMMEE, OSCEOLA COUNTY, FLORIDA
Terracon Project No. H1177166A
June 29, 2018
1.0 SITE DESCRIPTION
The site is approximately 19.2 acres of vacant land located approximately 500 feet south of the
Mary Louis Lane and 300 feet west of Orange Avenue in Kissimmee, Osceola County, Florida.
The site is approximately 19.2 acres identified by the Osceola County property appraiser as parcel
03-25-29-4586-0001-0020. A topographic map showing the site location is included as Exhibit 1
and a site diagram is included as Exhibit 2 in Appendix A. We understand the intended future
use of the site is commercial development.
2.0 PREVIOUS ASSESSMENT
Terracon previously completed a Phase I Environmental Site Assessment report dated March 8,
2017 (Terracon Project No. H1177125) for 37.2 acres that included the site and adjoining property
to the east and south. Based on a review of the historical information, a golf course was present
onsite from the 1970s to late-1980s or early-1990s. Potential impacts to soil and shallow
groundwater attributed to the historical pesticide and herbicide application associated with the
golf course turf maintenance was deemed a recognized environmental condition. A 1984 aerial
photograph from the Phase I Environmental Assessment report is contained in Appendix C.
Terracon prepared a Limited Site Investigation, Lots 22 & 23 dated April 28, 2017 (Terracon
Project No. H1177166) discussing initial soil and groundwater testing conducted to evaluate
potential pesticide and arsenic impacts associated with the former golf course. Arsenic was
identified at a relict golf course hole green area (sample location B8) at Lot 22 in the top 2 feet of
soil at concentrations exceeding Florida’s soil cleanup target level (SCTL) for residential direct
exposure (RSCTL) of 2.1 milligrams per kilogram (mg/kg) listed in Chapter 62-777, Florida
Administrative Code (FAC). The reported arsenic concentrations in soil did not exceed the
commercial/industrial direct exposure SCTL (CSCTL) of 12 mg/kg. Organochlorine pesticide
concentrations reported in soil samples did not exceed SCTLs. Arsenic concentrations detected
in a groundwater sample (TMW-8) collected at Lot 21 did not exceed the groundwater cleanup
target level (GCTL) of 10 micrograms per liter (ug/L) established for arsenic in Chapter 62-777,
FAC. Diagrams indicating the location of boring B8 and temporary monitoring well TMW-8 are
contained in Appendix C.
Terracon prepared a Limited Site Investigation Report and No Further Action Proposal dated
March 2, 2018 (Terracon Project No. H1177166A), for the site and south adjoining San Mateo
Supplemental Limited Site Investigation
Lot 22 ■ Kissimmee, Florida
June 29, 2018 ■ Terracon Project No. H1177166A
Responsive ■ Resourceful ■ Reliable 2
property, which was submitted to the Florida Department of Environmental Protection (FDEP)
Central District for review and concurrence with the no further action proposal. The reported
included documentation of additional soil testing for arsenic at Lot 22.
The FDEP then requested completion of soil source removal activities to remove soils identified
with arsenic concentrations exceeding the CSCTL at Lot 22, and to remove soils identified with
arsenic concentrations exceeding the RSCTL at the south adjoining San Mateo property. The
defined extent of soil containing arsenic concentrations exceeding the CSCTL identified at Lot 22
in the area of boring location B8 was excavated and disposed at a permitted landfill. The defined
extent of soil containing arsenic concentrations exceeding the RSCTL identified above the normal
groundwater elevation of 83 feet NGVD at the San Mateo property was then excavated and placed
at Lot 22 in the area around boring B8. Terracon documented performance of the source removal
activities in a Soil Source Removal report dated April 5, 2018. On May 10, 2018, the FDEP issued
No Further Assessment Required letter indicating that the FDEP would not require additional
assessment or remediation of the investigated areas. Appendix C contains copies of the FDEP
letter, and diagrams from the Soil Source Removal report showing the soil sampling and soil
source removal areas.
3.0 SCOPE OF SERVICES
This Supplemental LSI included soil sampling and analysis to evaluate arsenic concentrations in
soils above the groundwater at select areas on Lot 22 where previous golf course features (tees,
greens and fairways) were perceived based on review of aerial photographs and observations
during site reconnaissance at the time soil samples were collected. The current soil sampling
locations are indicated on Exhibit 2 in Appendix A.
3.1 Standard of Care
Terracon’s services were performed in a manner consistent with generally accepted practices of
the profession undertaken in similar studies in the same geographical area during the same time.
Terracon makes no warranties, either express or implied, regarding the findings, conclusions, or
recommendations. Please note that Terracon does not warrant the work of laboratories,
regulatory agencies, or other third parties supplying information used in the preparation of the
report. These LSI services were performed in accordance with the scope of work agreed with you,
our client, as reflected in our proposal.
3.2 Additional Scope Limitations
Findings, conclusions, and recommendations resulting from these services are based upon
information derived from the on-site activities and other services performed under this scope of
work; such information is subject to change over time. Certain indicators of the presence of
hazardous substances, petroleum products, or other constituents may have been latent,
Supplemental Limited Site Investigation
Lot 22 ■ Kissimmee, Florida
June 29, 2018 ■ Terracon Project No. H1177166A
Responsive ■ Resourceful ■ Reliable 3
inaccessible, unobservable, nondetectable, or not present during these services. We cannot
represent that the site contains no hazardous substances, toxic materials, petroleum products, or
other latent conditions beyond those identified during this LSI. Subsurface conditions may vary
from those encountered at specific borings or wells or during other surveys, tests, assessments,
investigations, or exploratory services. The data, interpretations, findings, and our
recommendations are based solely upon data obtained at the time and within the scope of these
services.
3.3 Reliance
This report has been prepared for the exclusive use of Deerfield Land Corporation. Any
authorization for use or reliance by any other party (except a governmental entity having
jurisdiction over the site) is prohibited without the express written authorization of Deerfield Land
Corporation and Terracon. Any unauthorized distribution or reuse is at Deerfield Land
Corporation’s sole risk. Notwithstanding the foregoing, reliance by authorized parties will be
subject to the terms, conditions, and limitations stated in the proposal, Supplemental LSI report,
and Terracon’s Agreement for Services. The limitation of liability defined in the terms and
conditions is the aggregate limit of Terracon’s liability to Deerfield Land Corporation and all relying
parties unless otherwise agreed in writing.
4.0 SUPPLEMENTAL SOIL TESTING
Terracon has a commitment to the safety of all its employees. As such, and in accordance with
our Incident and Injury Free® safety culture, a site safety pre-task plan was developed to identify
potential safety concerns and prepare our personnel to handle conditions during field services.
Prior to commencement of daily on-site activities, Terracon held a meeting with assigned staff to
review the proposed work sequence and evaluate work practices for safe completion of the
project. Fieldwork was conducted by environmental staff with OSHA 1910.120 training. Terracon
contacted Sunshine 811 to mark locations of underground utilities in the work area prior to
initiating intrusive activities. Soil sampling activities were conducted in general accordance with
the FDEP Standard Operating Procedures for Field Activities, DEP-SOP-001/01.
Soil sampling was conducted at 25 soil boring locations on June 21, 2018. Soil sampling locations
F1 to F25 are plotted on Exhibits 2 in Appendix A. Global positioning coordinates were recorded
at each soil boring location. Soil samples were collected using a decontaminated hand auger at
all of the boring locations at a depth 0 to 6 inches below ground surface (bgs). Deeper soil
samples above the groundwater table interface were collected at depths of 6 to 24 inches bgs
and 2 to 3 feet bgs or 2 to 4 feet bgs, depending on groundwater depth at the boring location.
The soil samples were placed in laboratory prepared glassware, labelled, and placed on ice in a
cooler sealed with custody tape. The sample coolers and completed chain-of-custody records
were relinquished to SGS North America Inc. – Orlando, for analysis of arsenic concentrations by
EPA Method 6010. The laboratory analytical report and chain-of-custody record are attached in
Supplemental Limited Site Investigation
Lot 22 ■ Kissimmee, Florida
June 29, 2018 ■ Terracon Project No. H1177166A
Responsive ■ Resourceful ■ Reliable 4
Appendix D. Table 1 in Appendix B contains a summary of soil sample locations with reference
to sample collection depths, date, groundwater depths, and measured arsenic concentrations.
Laboratory analytical results for soil samples were compared to SCTLs established for arsenic
listed in Chapter 62-777, FAC. In summary:
Arsenic concentrations reported in the soil samples did not exceed SCTLs, except at
sample location F11 where an arsenic concentration of 3.1 mg/kg was measured in the
sample collected from the surface to a depth of 6 inches bgs that exceeds the RSCTL for
direct exposure specified for residential settings of 2.1 mg/kg but does not exceed the
CSCTL for direct exposure specified for commercial settings of 12 mg/kg.
5.0 CONCLUSIONS
Based on the scope of services described in this report and subject to the limitations described
herein, Terracon concludes the following.
Arsenic concentrations reported in the soil samples did not exceed the SCTL applicable
for commercial settings. Based on our understanding that the site is proposed for
commercial development, additional assessment associated with the previous site use as
a golf course does not appear warranted.
APPENDIX A – EXHIBITS
NATIONAL GEODETIC VERTICAL DATUM OF 1929CONTOUR INTERVAL 5 FEET
RANGE:
Drawn By:
Checked By:
Approved By:
Project Mngr:
File No.
Date:
Scale:
Project No. EXHIBITTOPOGRAPHIC VICINITY MAP
1
1000090008000
1
6000
1000
0
5000 7000
2000
2
4000
0
0
3000
.5
1000
1
1000
0 2000
.5
1000
1
KILOMETERS
MILES
FEET
SCALE 1:24 000
7.5 MINUTE SERIES (QUADRANGLE)
N
EK
1
29 EAST
SW
EK
EK
H1177166A
AS SHOWN
H1177166A-1
6-25-18
SECTION:TOWNSHIP:
325 SOUTH
KISSIMMEE, FLORIDAISSUED: 1953 REVISED: 1987
Consulting Engineers and Scientists
1675 LEE ROAD WINTER PARK, FLORIDA 32789FAX. (407) 740-6112PH. (407) 740-6110 KISSIMMEE, OSCEOLA COUNTY, FLORIDA
SW QUADRANT ORANGE AVENUE AT MARY LOUIS LANE
LIMITED SITE INVESTIGATIONLOT 22
SITE
Drawn By:
Checked By:
Approved By:
Project Mngr:
File No.
Date:
Scale:
Project No. EXHIBITSOIL SAMPLE LOCATIONS MAPEK
2SW
EK
EK
H1177166A
AS SHOWN
H1177166A-2
6-29-18
Consulting Engineers and Scientists
1675 LEE ROAD WINTER PARK, FLORIDA 32789FAX. (407) 740-6112PH. (407) 740-6110 KISSIMMEE, OSCEOLA COUNTY, FLORIDA
SW QUADRANT ORANGE AVENUE AT MARY LOUIS LANE
LIMITED SITE INVESTIGATIONLOT 21
N
APPROXIMATE LOCATION OFSOIL BORING / SOIL SAMPLE
APPENDIX B – TABLES
F1-0.5 0 - 0.5 3 0.31 I
F1-2 0.5 - 2 3 0.088 U
F1-3 2 - 3 3 0.082 U
F2-0.5 0 - 0.5 2.9 0.11 U
F2-2 0.5 - 2 2.9 0.088 U
F2-3 2 - 3 2.9 0.11 U
F3-0.5 0 - 0.5 2.8 0.42 I
F3-2 0.5 - 2 2.8 1.3
F3-3 2 - 3 2.8 0.81
F4-0.5 0 - 0.5 3.8 0.090 I
F4-2 0.5 - 2 3.8 0.080 U
F4-4 2 - 4 3.8 0.12 U
F5-0.5 0 - 0.5 3.9 0.099 U
F5-2 0.5 - 2 3.9 0.083 U
F5-4 2 - 4 3.9 0.087 U
F6-0.5 0 - 0.5 1.9 0.11 U
F6-2 0.5 - 2 1.9 0.11 U
F7-0.5 0 - 0.5 2.2 0.30 I
F7-2 0.5 - 2 2.2 0.40 I
F8-0.5 0 - 0.5 1.8 0.46 I
F8-2 0.5 - 2 1.8 0.71
F9-0.5 0 - 0.5 1.8 0.11 U
F9-2 0.5 - 2 1.8 0.11 U
F10-0.5 0 - 0.5 1.8 0.12 U
F11-0.5 0 - 0.5 1.8 3.1
F11-2 0.5 - 2 2 0.098 U
F12-0.5 0 - 0.5 2 0.31 I
F12-2 0.5 - 2 2 0.077 U
F13-0.5 0 - 0.5 2.1 0.26 I
F13-2 0.5 - 2 2.1 0.096 U
F14-0.5 0 - 0.5 2 0.43 I
F14-2 0.5 - 2 2 0.11 I
F15-0.5 0 - 0.5 2 0.71
F15-2 0.5 - 2 2 0.29 I
F16-0.5 0 - 0.5 2.8 0.57
F16-2 0.5 - 2 2.8 0.43
F17-0.5 0 - 0.5 2 0.27 I
F17-2 0.5 - 2 2 0.11 U
F18-0.5 0 - 0.5 2 0.48 I
F18-2 0.5 - 2 2 0.15 I
F19-0.5 0 - 0.5 2 0.19 I
F19-2 0.5 - 2 2 0.10 U
F20-0.5 0 - 0.5 2 0.14 I
F20-2 0.5 - 2 2 0.099 U
Arsenic Concentration
(mg/kg)
Soil Sample
No.
Groundwater
Interface Depth
(ft)
Soil Arsenic Analytical Summary
Table 1
Lot 22
Soil Sample
Depth (ft)
Supplemental Limited Site Investigation
Arsenic Concentration
(mg/kg)
Soil Sample
No.
Groundwater
Interface Depth
(ft)
Soil Arsenic Analytical Summary
Table 1
Lot 22
Soil Sample
Depth (ft)
Supplemental Limited Site Investigation
F21-0.5 0 - 0.5 2 0.13 I
F21-2 0.5 - 2 2 0.24 I
F22-0.5 0 - 0.5 2 0.18 I
F22-2 0.5 - 2 2 0.087 I
F23-0.5 0 - 0.5 2 0.035 I
F23-2 0.5 - 2 2 0.10 U
F24-0.5 0 - 0.5 2 0.19 I
F24-2 0.5 - 2 2 0.062
F25-0.5 0 - 0.5 3.9 0.29 I
F25-2 0.5 - 2 3.9 0.123 I
F25-4 2 - 4 3.9 0.089 I
*
2.1
12
mg/kg = milligrams per kilogram
ft = feet below ground surface
Exceeds RSCTL
Exceeds CSCTL
** = Laboratory reported matrix interference
SCTL = Soil Cleanup Target Level per Chapter 62-777, Florida Administrative Code
Leachability Based on Groundwater Criteria (LSCTL)
Residential Direct Exposure SCTL (RSCTL)
Commercial/Industrial Direct Exposure (CSCTL)
* = Leachability value may be determined using Synthetic Precipitation Leachability Procedure
Notes:
APPENDIX C – PREVIOUS SOURCE REMOVAL REPORT
EXCERPTS
APPENDIX D – ANALYTICAL REPORTS AND CHAIN OF
CUSTODY
06/27/18
Technical Report for
Terracon Consulting
San Mateo; Kissimmee, FL
H1177166A
SGS Job Number: FA55261
Sampling Date: 06/21/18
Report to:
Terracon1675 Lee RdWinter Park, FL [email protected]
ATTN: Eric Krebill
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Ken Overstreet 407-425-6700
Caitlin Brice, M.S.General Manager
Orlando, FL 06/27/18
e-Hardcopy 2.0Automated Report
102
SGS is the sole authority for authorizing edits or modifications to this document.Unauthorized modification of this report is strictly prohibited.Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas abouthow we can serve you better at:[email protected]
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Table of Contents-1-
Sections:
Section 1: Sample Summary ................................................................................................... 4Section 2: Summary of Hits .................................................................................................... 9Section 3: Sample Results ........................................................................................................ 14
3.1: FA55261-1: F1-0.5 ........................................................................................................ 153.2: FA55261-2: F1-2 ........................................................................................................... 163.3: FA55261-3: F1-3 ........................................................................................................... 173.4: FA55261-4: F2-0.5 ........................................................................................................ 183.5: FA55261-5: F2-2 ........................................................................................................... 193.6: FA55261-6: F2-3 ........................................................................................................... 203.7: FA55261-7: F3-0.5 ........................................................................................................ 213.8: FA55261-8: F3-2 ........................................................................................................... 223.9: FA55261-9: F3-3 ........................................................................................................... 233.10: FA55261-10: F4-0.5 .................................................................................................... 243.11: FA55261-11: F4-2 ....................................................................................................... 253.12: FA55261-12: F4-4 ....................................................................................................... 263.13: FA55261-13: F5-0.5 .................................................................................................... 273.14: FA55261-14: F5-2 ....................................................................................................... 283.15: FA55261-15: F5-4 ....................................................................................................... 293.16: FA55261-16: F6-0.5 .................................................................................................... 303.17: FA55261-17: F6-2 ....................................................................................................... 313.18: FA55261-18: F7-0.5 .................................................................................................... 323.19: FA55261-19: F7-2 ....................................................................................................... 333.20: FA55261-20: F8-0.5 .................................................................................................... 343.21: FA55261-21: F8-2 ....................................................................................................... 353.22: FA55261-22: F9-0.5 .................................................................................................... 363.23: FA55261-23: F9-2' ...................................................................................................... 373.24: FA55261-24: F10-0.5 .................................................................................................. 383.25: FA55261-25: F11-0.5 .................................................................................................. 393.26: FA55261-26: F11-2 ..................................................................................................... 403.27: FA55261-27: F12-0.5 .................................................................................................. 413.28: FA55261-28: F12-2 ..................................................................................................... 423.29: FA55261-29: F13-0.5 .................................................................................................. 433.30: FA55261-30: F13-2 ..................................................................................................... 443.31: FA55261-31: F14-0.5 .................................................................................................. 453.32: FA55261-32: F14-2 ..................................................................................................... 463.33: FA55261-33: F15-0.5 .................................................................................................. 473.34: FA55261-34: F15-2 ..................................................................................................... 483.35: FA55261-35: F16-0.5 .................................................................................................. 493.36: FA55261-36: F16-2 ..................................................................................................... 503.37: FA55261-37: F17-0.5 .................................................................................................. 513.38: FA55261-38: F17-2 ..................................................................................................... 523.39: FA55261-39: F18-0.5 .................................................................................................. 53
12
34
5
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Table of Contents-2-
Sections:
3.40: FA55261-40: F18-2 ..................................................................................................... 543.41: FA55261-41: F19-0.5 .................................................................................................. 553.42: FA55261-42: F19-2 ..................................................................................................... 563.43: FA55261-43: F20-0.5 .................................................................................................. 573.44: FA55261-44: F20-2 ..................................................................................................... 583.45: FA55261-45: F21-0.5 .................................................................................................. 593.46: FA55261-46: F21-2 ..................................................................................................... 603.47: FA55261-47: F22-0.5 .................................................................................................. 613.48: FA55261-48: F22-2 ..................................................................................................... 623.49: FA55261-49: F23-0.5 .................................................................................................. 633.50: FA55261-50: F23-2 ..................................................................................................... 643.51: FA55261-51: F24-0.5 .................................................................................................. 653.52: FA55261-52: F24-2 ..................................................................................................... 663.53: FA55261-53: F25-0.5 .................................................................................................. 673.54: FA55261-54: F25-2 ..................................................................................................... 683.55: FA55261-55: F25-4 ..................................................................................................... 69
Section 4: Misc. Forms ............................................................................................................ 704.1: Chain of Custody ........................................................................................................... 71
Section 5: Metals Analysis - QC Data Summaries ................................................................ 775.1: Prep QC MP33930: As .................................................................................................. 785.2: Prep QC MP33933: As .................................................................................................. 855.3: Prep QC MP33934: As .................................................................................................. 915.4: Prep QC MP33941: As .................................................................................................. 97
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Sample Summary
Terracon ConsultingJob No: FA55261
San Mateo; Kissimmee, FLProject No: H1177166A
Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID
FA55261-1 06/21/18 07:31 MBEK 06/21/18 SO Soil F1-0.5
FA55261-2 06/21/18 07:34 MBEK 06/21/18 SO Soil F1-2
FA55261-3 06/21/18 07:40 MBEK 06/21/18 SO Soil F1-3
FA55261-4 06/21/18 08:00 MBEK 06/21/18 SO Soil F2-0.5
FA55261-5 06/21/18 08:03 MBEK 06/21/18 SO Soil F2-2
FA55261-6 06/21/18 08:06 MBEK 06/21/18 SO Soil F2-3
FA55261-7 06/21/18 08:16 MBEK 06/21/18 SO Soil F3-0.5
FA55261-8 06/21/18 08:20 MBEK 06/21/18 SO Soil F3-2
FA55261-9 06/21/18 08:24 MBEK 06/21/18 SO Soil F3-3
FA55261-10 06/21/18 08:29 MBEK 06/21/18 SO Soil F4-0.5
FA55261-11 06/21/18 08:31 MBEK 06/21/18 SO Soil F4-2
FA55261-12 06/21/18 08:34 MBEK 06/21/18 SO Soil F4-4
FA55261-13 06/21/18 08:40 MBEK 06/21/18 SO Soil F5-0.5
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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Sample Summary(continued)
Terracon ConsultingJob No: FA55261
San Mateo; Kissimmee, FLProject No: H1177166A
Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID
FA55261-14 06/21/18 08:42 MBEK 06/21/18 SO Soil F5-2
FA55261-15 06/21/18 08:45 MBEK 06/21/18 SO Soil F5-4
FA55261-16 06/21/18 09:25 MBEK 06/21/18 SO Soil F6-0.5
FA55261-17 06/21/18 09:27 MBEK 06/21/18 SO Soil F6-2
FA55261-18 06/21/18 09:36 MBEK 06/21/18 SO Soil F7-0.5
FA55261-19 06/21/18 09:40 MBEK 06/21/18 SO Soil F7-2
FA55261-20 06/21/18 09:51 MBEK 06/21/18 SO Soil F8-0.5
FA55261-21 06/21/18 09:54 MBEK 06/21/18 SO Soil F8-2
FA55261-22 06/21/18 10:08 MBEK 06/21/18 SO Soil F9-0.5
FA55261-23 06/21/18 10:14 MBEK 06/21/18 SO Soil F9-2'
FA55261-24 06/21/18 10:19 MBEK 06/21/18 SO Soil F10-0.5
FA55261-25 06/21/18 11:25 MBEK 06/21/18 SO Soil F11-0.5
FA55261-26 06/21/18 11:28 MBEK 06/21/18 SO Soil F11-2
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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Sample Summary(continued)
Terracon ConsultingJob No: FA55261
San Mateo; Kissimmee, FLProject No: H1177166A
Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID
FA55261-27 06/21/18 11:32 MBEK 06/21/18 SO Soil F12-0.5
FA55261-28 06/21/18 11:33 MBEK 06/21/18 SO Soil F12-2
FA55261-29 06/21/18 11:36 MBEK 06/21/18 SO Soil F13-0.5
FA55261-30 06/21/18 11:39 MBEK 06/21/18 SO Soil F13-2
FA55261-31 06/21/18 11:42 MBEK 06/21/18 SO Soil F14-0.5
FA55261-32 06/21/18 11:44 MBEK 06/21/18 SO Soil F14-2
FA55261-33 06/21/18 11:47 MBEK 06/21/18 SO Soil F15-0.5
FA55261-34 06/21/18 11:50 MBEK 06/21/18 SO Soil F15-2
FA55261-35 06/21/18 11:57 MBEK 06/21/18 SO Soil F16-0.5
FA55261-36 06/21/18 12:00 MBEK 06/21/18 SO Soil F16-2
FA55261-37 06/21/18 12:07 MBEK 06/21/18 SO Soil F17-0.5
FA55261-38 06/21/18 12:10 MBEK 06/21/18 SO Soil F17-2
FA55261-39 06/21/18 12:18 MBEK 06/21/18 SO Soil F18-0.5
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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Sample Summary(continued)
Terracon ConsultingJob No: FA55261
San Mateo; Kissimmee, FLProject No: H1177166A
Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID
FA55261-40 06/21/18 12:20 MBEK 06/21/18 SO Soil F18-2
FA55261-41 06/21/18 12:34 MBEK 06/21/18 SO Soil F19-0.5
FA55261-42 06/21/18 12:36 MBEK 06/21/18 SO Soil F19-2
FA55261-43 06/21/18 12:39 MBEK 06/21/18 SO Soil F20-0.5
FA55261-44 06/21/18 12:41 MBEK 06/21/18 SO Soil F20-2
FA55261-45 06/21/18 12:43 MBEK 06/21/18 SO Soil F21-0.5
FA55261-46 06/21/18 12:45 MBEK 06/21/18 SO Soil F21-2
FA55261-47 06/21/18 12:55 MBEK 06/21/18 SO Soil F22-0.5
FA55261-48 06/21/18 12:57 MBEK 06/21/18 SO Soil F22-2
FA55261-49 06/21/18 12:59 MBEK 06/21/18 SO Soil F23-0.5
FA55261-50 06/21/18 13:01 MBEK 06/21/18 SO Soil F23-2
FA55261-51 06/21/18 13:10 MBEK 06/21/18 SO Soil F24-0.5
FA55261-52 06/21/18 13:12 MBEK 06/21/18 SO Soil F24-2
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
7 of 102
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1
SGS North America Inc.
Sample Summary(continued)
Terracon ConsultingJob No: FA55261
San Mateo; Kissimmee, FLProject No: H1177166A
Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID
FA55261-53 06/21/18 13:16 MBEK 06/21/18 SO Soil F25-0.5
FA55261-54 06/21/18 13:17 MBEK 06/21/18 SO Soil F25-2
FA55261-55 06/21/18 13:19 MBEK 06/21/18 SO Soil F25-4
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
8 of 102
FA55261
1
Summary of Hits Page 1 of 5 Job Number: FA55261Account: Terracon ConsultingProject: San Mateo; Kissimmee, FLCollected: 06/21/18
Lab Sample ID Client Sample ID Result/Analyte Qual PQL MDL Units Method
FA55261-1 F1-0.5
Arsenic 0.31 I 0.44 0.089 mg/kg SW846 6010C
FA55261-2 F1-2
No hits reported in this sample.
FA55261-3 F1-3
No hits reported in this sample.
FA55261-4 F2-0.5
No hits reported in this sample.
FA55261-5 F2-2
No hits reported in this sample.
FA55261-6 F2-3
No hits reported in this sample.
FA55261-7 F3-0.5
Arsenic 0.42 I 0.48 0.096 mg/kg SW846 6010C
FA55261-8 F3-2
Arsenic 1.3 0.48 0.096 mg/kg SW846 6010C
FA55261-9 F3-3
Arsenic 0.81 0.47 0.094 mg/kg SW846 6010C
FA55261-10 F4-0.5
Arsenic 0.090 I 0.45 0.090 mg/kg SW846 6010C
FA55261-11 F4-2
No hits reported in this sample.
9 of 102
FA55261
2
Summary of Hits Page 2 of 5 Job Number: FA55261Account: Terracon ConsultingProject: San Mateo; Kissimmee, FLCollected: 06/21/18
Lab Sample ID Client Sample ID Result/Analyte Qual PQL MDL Units Method
FA55261-12 F4-4
No hits reported in this sample.
FA55261-13 F5-0.5
No hits reported in this sample.
FA55261-14 F5-2
No hits reported in this sample.
FA55261-15 F5-4
No hits reported in this sample.
FA55261-16 F6-0.5
No hits reported in this sample.
FA55261-17 F6-2
No hits reported in this sample.
FA55261-18 F7-0.5
Arsenic 0.30 I 0.52 0.10 mg/kg SW846 6010C
FA55261-19 F7-2
Arsenic 0.40 I 0.46 0.092 mg/kg SW846 6010C
FA55261-20 F8-0.5
Arsenic 0.46 I 0.52 0.10 mg/kg SW846 6010C
FA55261-21 F8-2
Arsenic 0.71 0.42 0.083 mg/kg SW846 6010C
FA55261-22 F9-0.5
No hits reported in this sample.
10 of 102
FA55261
2
Summary of Hits Page 3 of 5 Job Number: FA55261Account: Terracon ConsultingProject: San Mateo; Kissimmee, FLCollected: 06/21/18
Lab Sample ID Client Sample ID Result/Analyte Qual PQL MDL Units Method
FA55261-23 F9-2'
No hits reported in this sample.
FA55261-24 F10-0.5
No hits reported in this sample.
FA55261-25 F11-0.5
Arsenic 3.1 0.50 0.10 mg/kg SW846 6010C
FA55261-26 F11-2
No hits reported in this sample.
FA55261-27 F12-0.5
Arsenic 0.31 I 0.52 0.10 mg/kg SW846 6010C
FA55261-28 F12-2
No hits reported in this sample.
FA55261-29 F13-0.5
Arsenic 0.26 I 0.66 0.13 mg/kg SW846 6010C
FA55261-30 F13-2
No hits reported in this sample.
FA55261-31 F14-0.5
Arsenic 0.43 I 0.56 0.11 mg/kg SW846 6010C
FA55261-32 F14-2
Arsenic 0.11 I 0.52 0.10 mg/kg SW846 6010C
FA55261-33 F15-0.5
Arsenic 0.71 0.52 0.10 mg/kg SW846 6010C
11 of 102
FA55261
2
Summary of Hits Page 4 of 5 Job Number: FA55261Account: Terracon ConsultingProject: San Mateo; Kissimmee, FLCollected: 06/21/18
Lab Sample ID Client Sample ID Result/Analyte Qual PQL MDL Units Method
FA55261-34 F15-2
Arsenic 0.29 I 0.53 0.11 mg/kg SW846 6010C
FA55261-35 F16-0.5
Arsenic 0.57 0.52 0.10 mg/kg SW846 6010C
FA55261-36 F16-2
Arsenic 0.43 0.41 0.082 mg/kg SW846 6010C
FA55261-37 F17-0.5
Arsenic 0.27 I 0.52 0.10 mg/kg SW846 6010C
FA55261-38 F17-2
No hits reported in this sample.
FA55261-39 F18-0.5
Arsenic 0.48 I 0.54 0.11 mg/kg SW846 6010C
FA55261-40 F18-2
Arsenic 0.15 I 0.52 0.10 mg/kg SW846 6010C
FA55261-41 F19-0.5
Arsenic 0.19 I 0.41 0.082 mg/kg SW846 6010C
FA55261-42 F19-2
No hits reported in this sample.
FA55261-43 F20-0.5
Arsenic 0.14 I 0.58 0.12 mg/kg SW846 6010C
FA55261-44 F20-2
No hits reported in this sample.
12 of 102
FA55261
2
Summary of Hits Page 5 of 5 Job Number: FA55261Account: Terracon ConsultingProject: San Mateo; Kissimmee, FLCollected: 06/21/18
Lab Sample ID Client Sample ID Result/Analyte Qual PQL MDL Units Method
FA55261-45 F21-0.5
Arsenic 0.13 I 0.48 0.096 mg/kg SW846 6010C
FA55261-46 F21-2
Arsenic 0.24 I 0.44 0.088 mg/kg SW846 6010C
FA55261-47 F22-0.5
Arsenic 0.18 I 0.42 0.084 mg/kg SW846 6010C
FA55261-48 F22-2
Arsenic 0.087 I 0.40 0.079 mg/kg SW846 6010C
FA55261-49 F23-0.5
Arsenic 0.35 I 0.51 0.10 mg/kg SW846 6010C
FA55261-50 F23-2
No hits reported in this sample.
FA55261-51 F24-0.5
Arsenic 0.19 I 0.53 0.11 mg/kg SW846 6010C
FA55261-52 F24-2
Arsenic 0.62 0.42 0.084 mg/kg SW846 6010C
FA55261-53 F25-0.5
Arsenic 0.29 I 0.43 0.086 mg/kg SW846 6010C
FA55261-54 F25-2
Arsenic 0.12 I 0.52 0.10 mg/kg SW846 6010C
FA55261-55 F25-4
Arsenic 0.089 I 0.41 0.081 mg/kg SW846 6010C
13 of 102
FA55261
2
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FLSection 3
14 of 102
FA55261
3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F1-0.5 Lab Sample ID: FA55261-1 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 88.8 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.31 I 0.44 0.089 mg/kg 1 06/23/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33930
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
15 of 102
FA55261
33.1
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F1-2 Lab Sample ID: FA55261-2 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 85.9 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.088 U 0.44 0.088 mg/kg 1 06/23/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33930
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
16 of 102
FA55261
33.2
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F1-3 Lab Sample ID: FA55261-3 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 83.2 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.082 U 0.41 0.082 mg/kg 1 06/23/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33930
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
17 of 102
FA55261
33.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F2-0.5 Lab Sample ID: FA55261-4 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 86.4 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.11 U 0.53 0.11 mg/kg 1 06/23/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33930
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
18 of 102
FA55261
33.4
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F2-2 Lab Sample ID: FA55261-5 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 81.9 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.088 U 0.44 0.088 mg/kg 1 06/23/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33930
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
19 of 102
FA55261
33.5
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F2-3 Lab Sample ID: FA55261-6 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 82.1 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.11 U 0.53 0.11 mg/kg 1 06/23/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33930
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
20 of 102
FA55261
33.6
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F3-0.5 Lab Sample ID: FA55261-7 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 84.2 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.42 I 0.48 0.096 mg/kg 1 06/23/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33930
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
21 of 102
FA55261
33.7
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F3-2 Lab Sample ID: FA55261-8 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 81.3 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 1.3 0.48 0.096 mg/kg 1 06/23/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33930
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
22 of 102
FA55261
33.8
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F3-3 Lab Sample ID: FA55261-9 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 82.9 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.81 0.47 0.094 mg/kg 1 06/23/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33930
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
23 of 102
FA55261
33.9
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F4-0.5 Lab Sample ID: FA55261-10 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 92.2 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.090 I 0.45 0.090 mg/kg 1 06/23/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33930
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
24 of 102
FA55261
33.10
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F4-2 Lab Sample ID: FA55261-11 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 87.3 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.080 U 0.40 0.080 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33933
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
25 of 102
FA55261
33.11
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F4-4 Lab Sample ID: FA55261-12 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 79.0 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.12 U 0.58 0.12 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33933
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
26 of 102
FA55261
33.12
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F5-0.5 Lab Sample ID: FA55261-13 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 92.5 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.099 U 0.50 0.099 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33933
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
27 of 102
FA55261
33.13
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F5-2 Lab Sample ID: FA55261-14 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 88.1 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.083 U 0.42 0.083 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33933
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
28 of 102
FA55261
33.14
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F5-4 Lab Sample ID: FA55261-15 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 81.4 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.087 U 0.44 0.087 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33933
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
29 of 102
FA55261
33.15
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F6-0.5 Lab Sample ID: FA55261-16 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 80.4 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.11 U 0.54 0.11 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33933
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
30 of 102
FA55261
33.16
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F6-2 Lab Sample ID: FA55261-17 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 82.5 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.11 U 0.56 0.11 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33933
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
31 of 102
FA55261
33.17
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F7-0.5 Lab Sample ID: FA55261-18 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 83.6 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.30 I 0.52 0.10 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33933
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
32 of 102
FA55261
33.18
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F7-2 Lab Sample ID: FA55261-19 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 82.0 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.40 I 0.46 0.092 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33933
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
33 of 102
FA55261
33.19
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F8-0.5 Lab Sample ID: FA55261-20 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 77.6 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.46 I 0.52 0.10 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33933
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
34 of 102
FA55261
33.20
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F8-2 Lab Sample ID: FA55261-21 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 81.1 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.71 0.42 0.083 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33933
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
35 of 102
FA55261
33.21
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F9-0.5 Lab Sample ID: FA55261-22 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 80.9 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.11 U 0.54 0.11 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33933
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
36 of 102
FA55261
33.22
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F9-2' Lab Sample ID: FA55261-23 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 81.9 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.11 U 0.57 0.11 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33933
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
37 of 102
FA55261
33.23
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F10-0.5 Lab Sample ID: FA55261-24 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 77.6 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.12 U 0.61 0.12 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33933
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
38 of 102
FA55261
33.24
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F11-0.5 Lab Sample ID: FA55261-25 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 78.3 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 3.1 0.50 0.10 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33933
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
39 of 102
FA55261
33.25
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F11-2 Lab Sample ID: FA55261-26 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 83.8 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.098 U 0.49 0.098 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33933
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
40 of 102
FA55261
33.26
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F12-0.5 Lab Sample ID: FA55261-27 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 80.3 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.31 I 0.52 0.10 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33933
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
41 of 102
FA55261
33.27
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F12-2 Lab Sample ID: FA55261-28 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 83.7 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.077 U 0.39 0.077 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33933
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
42 of 102
FA55261
33.28
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F13-0.5 Lab Sample ID: FA55261-29 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 75.9 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.26 I 0.66 0.13 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33933
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
43 of 102
FA55261
33.29
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F13-2 Lab Sample ID: FA55261-30 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 77.4 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.096 U 0.48 0.096 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA14998(2) Prep QC Batch: MP33933
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
44 of 102
FA55261
33.30
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F14-0.5 Lab Sample ID: FA55261-31 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 81.8 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.43 I 0.56 0.11 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA15004(2) Prep QC Batch: MP33934
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
45 of 102
FA55261
33.31
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F14-2 Lab Sample ID: FA55261-32 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 81.7 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.11 I 0.52 0.10 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA15004(2) Prep QC Batch: MP33934
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
46 of 102
FA55261
33.32
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F15-0.5 Lab Sample ID: FA55261-33 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 82.3 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.71 0.52 0.10 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA15004(2) Prep QC Batch: MP33934
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
47 of 102
FA55261
33.33
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F15-2 Lab Sample ID: FA55261-34 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 81.6 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.29 I 0.53 0.11 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA15004(2) Prep QC Batch: MP33934
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
48 of 102
FA55261
33.34
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F16-0.5 Lab Sample ID: FA55261-35 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 90.1 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.57 0.52 0.10 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA15004(2) Prep QC Batch: MP33934
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
49 of 102
FA55261
33.35
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F16-2 Lab Sample ID: FA55261-36 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 88.3 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.43 0.41 0.082 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA15004(2) Prep QC Batch: MP33934
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
50 of 102
FA55261
33.36
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F17-0.5 Lab Sample ID: FA55261-37 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 86.3 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.27 I 0.52 0.10 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA15004(2) Prep QC Batch: MP33934
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
51 of 102
FA55261
33.37
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F17-2 Lab Sample ID: FA55261-38 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 82.5 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.11 U 0.57 0.11 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA15004(2) Prep QC Batch: MP33934
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
52 of 102
FA55261
33.38
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F18-0.5 Lab Sample ID: FA55261-39 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 84.8 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.48 I 0.54 0.11 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA15004(2) Prep QC Batch: MP33934
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
53 of 102
FA55261
33.39
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F18-2 Lab Sample ID: FA55261-40 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 85.6 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.15 I 0.52 0.10 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA15004(2) Prep QC Batch: MP33934
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
54 of 102
FA55261
33.40
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F19-0.5 Lab Sample ID: FA55261-41 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 83.7 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.19 I 0.41 0.082 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA15004(2) Prep QC Batch: MP33934
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
55 of 102
FA55261
33.41
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F19-2 Lab Sample ID: FA55261-42 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 84.4 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.10 U 0.50 0.10 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA15004(2) Prep QC Batch: MP33934
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
56 of 102
FA55261
33.42
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F20-0.5 Lab Sample ID: FA55261-43 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 81.1 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.14 I 0.58 0.12 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA15004(2) Prep QC Batch: MP33934
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
57 of 102
FA55261
33.43
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F20-2 Lab Sample ID: FA55261-44 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 83.8 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.099 U 0.50 0.099 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA15004(2) Prep QC Batch: MP33934
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
58 of 102
FA55261
33.44
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F21-0.5 Lab Sample ID: FA55261-45 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 87.9 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.13 I 0.48 0.096 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA15004(2) Prep QC Batch: MP33934
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
59 of 102
FA55261
33.45
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F21-2 Lab Sample ID: FA55261-46 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 83.9 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.24 I 0.44 0.088 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA15004(2) Prep QC Batch: MP33934
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
60 of 102
FA55261
33.46
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F22-0.5 Lab Sample ID: FA55261-47 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 92.1 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.18 I 0.42 0.084 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA15004(2) Prep QC Batch: MP33934
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
61 of 102
FA55261
33.47
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F22-2 Lab Sample ID: FA55261-48 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 83.9 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.087 I 0.40 0.079 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA15004(2) Prep QC Batch: MP33934
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
62 of 102
FA55261
33.48
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F23-0.5 Lab Sample ID: FA55261-49 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 83.5 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.35 I 0.51 0.10 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA15004(2) Prep QC Batch: MP33934
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
63 of 102
FA55261
33.49
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F23-2 Lab Sample ID: FA55261-50 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 83.3 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.10 U 0.52 0.10 mg/kg 1 06/25/18 06/25/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA15004(2) Prep QC Batch: MP33934
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
64 of 102
FA55261
33.50
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F24-0.5 Lab Sample ID: FA55261-51 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 85.7 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.19 I 0.53 0.11 mg/kg 1 06/26/18 06/26/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA15005(2) Prep QC Batch: MP33941
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
65 of 102
FA55261
33.51
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F24-2 Lab Sample ID: FA55261-52 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 82.7 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.62 0.42 0.084 mg/kg 1 06/26/18 06/26/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA15005(2) Prep QC Batch: MP33941
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
66 of 102
FA55261
33.52
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F25-0.5 Lab Sample ID: FA55261-53 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 92.0 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.29 I 0.43 0.086 mg/kg 1 06/26/18 06/26/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA15005(2) Prep QC Batch: MP33941
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
67 of 102
FA55261
33.53
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F25-2 Lab Sample ID: FA55261-54 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 87.8 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.12 I 0.52 0.10 mg/kg 1 06/26/18 06/26/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA15005(2) Prep QC Batch: MP33941
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
68 of 102
FA55261
33.54
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID: F25-4 Lab Sample ID: FA55261-55 Date Sampled: 06/21/18 Matrix: SO - Soil Date Received: 06/21/18
Percent Solids: 82.1 Project: San Mateo; Kissimmee, FL
Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 0.089 I 0.41 0.081 mg/kg 1 06/26/18 06/26/18 LM SW846 6010C 1 SW846 3050B 2
(1) Instrument QC Batch: MA15005(2) Prep QC Batch: MP33941
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
69 of 102
FA55261
33.55
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FLSection 4
70 of 102
FA55261
4
FA55261: Chain of CustodyPage 1 of 6
71 of 102
FA55261
44.1
FA55261: Chain of CustodyPage 2 of 6
72 of 102
FA55261
44.1
FA55261: Chain of CustodyPage 3 of 6
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FA55261
44.1
FA55261: Chain of CustodyPage 4 of 6
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FA55261
44.1
FA55261: Chain of CustodyPage 5 of 6
75 of 102
FA55261
44.1
Job Number: FA55261 Client: TERRACON
Date / Time Received: 6/21/2018 2:01:00 PM Delivery Method: DROP OFF
Project: LOT 22
Airbill #'s:
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments SAMPLE #9 THROUGH #12 NO ANALYSIS MARKED. SAMPLE #12 NO SAMPLE ID WRITTEN ON COC. BOTTLE LABEL READS F4-4.
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (3.9); Cooler 2: (4.3);
Cooler 1: (4.0); Cooler 2: (4.4);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores: Number of 5035 Field Kits: Number of Lab Filtered Metals:
Test Strip Lot #s: pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID: IR 1; Therm CF: 0.1; # of Coolers: 2
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician: Reviewer:PhilipD Date:Date: 6/21/2018 2:01:00 PM
FA55261: Chain of CustodyPage 6 of 6
76 of 102
FA55261
44.1
SGS North America Inc.
Metals Analysis
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries• Matrix Spike and Duplicate Summaries• Blank Spike and Lab Control Sample Summaries• Serial Dilution Summaries
Orlando, FLSection 5
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FA55261
5
BLANK RESULTS SUMMARY Part 2 - Method Blanks
Login Number: FA55261 Account: TERCFLWP - Terracon Consulting
Project: San Mateo; Kissimmee, FL
QC Batch ID: MP33930 Methods: SW846 6010C Matrix Type: SOLID Units: mg/kg
Prep Date: 06/23/18
MB Metal RL IDL MDL raw final
Aluminum 10 .7 1.8
Antimony 1.0 .05 .065
Arsenic 0.50 .065 .1 -0.23 <0.50
Barium 10 .05 .05
Beryllium 0.25 .01 .025
Cadmium 0.20 .01 .025
Calcium 250 2.5 2.5
Chromium 0.50 .05 .05
Cobalt 2.5 .01 .025
Copper 1.3 .05 .05
Iron 15 .85 .85
Lead 1.0 .05 .05
Magnesium 250 1.8 1.8
Manganese 0.75 .025 .025
Molybdenum 2.5 .015 .025
Nickel 2.0 .02 .025
Potassium 500 10 10
Selenium 1.0 .12 .12
Silver 0.50 .035 .041
Sodium 500 25 25
Strontium 0.50 .025 .025
Thallium 0.50 .055 .055
Tin 2.5 .045 .045
Titanium 0.50 .025 .025
Vanadium 2.5 .025 .025
Zinc 1.0 .15 .15
Associated samples MP33930: FA55261-1, FA55261-2, FA55261-3, FA55261-4, FA55261-5, FA55261-6, FA55261-7,FA55261-8, FA55261-9, FA55261-10
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
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FA55261
55.1.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA55261 Account: TERCFLWP - Terracon Consulting
Project: San Mateo; Kissimmee, FL
QC Batch ID: MP33930 Methods: SW846 6010C Matrix Type: SOLID Units: mg/kg
Prep Date: 06/23/18 06/23/18
FA55117-1 QC FA55117-1 QC Metal Original DUP RPD Limits Original DUP RPD Limits
Aluminum anr
Antimony
Arsenic 2.8 3.4 (a) 19.4 0-20 2.8 3.0 (a) 6.9 0-20
Barium anr
Beryllium
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper
Iron
Lead anr
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium anr
Silver anr
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP33930: FA55261-1, FA55261-2, FA55261-3, FA55261-4, FA55261-5, FA55261-6, FA55261-7,FA55261-8, FA55261-9, FA55261-10
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested(a) Sample dilution required due to difficult matrix.
_________________________________________________________________________________________________________
Page 1
79 of 102
FA55261
55.1.2
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA55261 Account: TERCFLWP - Terracon Consulting
Project: San Mateo; Kissimmee, FL
QC Batch ID: MP33930 Methods: SW846 6010C Matrix Type: SOLID Units: mg/kg
Prep Date: 06/23/18
FA55117-1 Spikelot QC Metal Original MS MPFLICP2 % Rec Limits
Aluminum anr
Antimony
Arsenic 2.8 70.5 (a) 95.2 71.1N(b) 80-120
Barium anr
Beryllium
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper
Iron
Lead anr
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium anr
Silver anr
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP33930: FA55261-1, FA55261-2, FA55261-3, FA55261-4, FA55261-5, FA55261-6, FA55261-7,FA55261-8, FA55261-9, FA55261-10
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested(a) Sample dilution required due to difficult matrix.(b) Spike recovery indicates possible matrix interference and/or sample non-homogeneity.
_________________________________________________________________________________________________________
Page 2
80 of 102
FA55261
55.1.2
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA55261 Account: TERCFLWP - Terracon Consulting
Project: San Mateo; Kissimmee, FL
QC Batch ID: MP33930 Methods: SW846 6010C Matrix Type: SOLID Units: mg/kg
Prep Date: 06/23/18
FA55117-1 Spikelot MSD QC Metal Original MSD MPFLICP2 % Rec RPD Limit
Aluminum anr
Antimony
Arsenic 2.8 67.6 (a) 90.9 71.3N(b) 4.2 20
Barium anr
Beryllium
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper
Iron
Lead anr
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium anr
Silver anr
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP33930: FA55261-1, FA55261-2, FA55261-3, FA55261-4, FA55261-5, FA55261-6, FA55261-7,FA55261-8, FA55261-9, FA55261-10
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested(a) Sample dilution required due to difficult matrix.(b) Spike recovery indicates possible matrix interference and/or sample non-homogeneity.
_________________________________________________________________________________________________________
Page 3
81 of 102
FA55261
55.1.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA55261 Account: TERCFLWP - Terracon Consulting
Project: San Mateo; Kissimmee, FL
QC Batch ID: MP33930 Methods: SW846 6010C Matrix Type: SOLID Units: mg/kg
Prep Date: 06/23/18
BSP Spikelot QC Metal Result MPFLICP2 % Rec Limits
Aluminum anr
Antimony
Arsenic 93.7 100 93.7 80-120
Barium anr
Beryllium
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper
Iron
Lead anr
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium anr
Silver anr
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP33930: FA55261-1, FA55261-2, FA55261-3, FA55261-4, FA55261-5, FA55261-6, FA55261-7,FA55261-8, FA55261-9, FA55261-10
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
82 of 102
FA55261
55.1.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: FA55261 Account: TERCFLWP - Terracon Consulting
Project: San Mateo; Kissimmee, FL
QC Batch ID: MP33930 Methods: SW846 6010C Matrix Type: SOLID Units: ug/l
Prep Date: 06/23/18
FA55117-1 QC Metal Original SDL 10:50%DIF Limits
Aluminum anr
Antimony
Arsenic 59.7 0.00 100.0(a) 0-10
Barium anr
Beryllium
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper
Iron
Lead anr
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium anr
Silver anr
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP33930: FA55261-1, FA55261-2, FA55261-3, FA55261-4, FA55261-5, FA55261-6, FA55261-7,FA55261-8, FA55261-9, FA55261-10
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
_________________________________________________________________________________________________________
Page 1
83 of 102
FA55261
55.1.4
POST DIGESTATE SPIKE SUMMARY
Login Number: FA55261 Account: TERCFLWP - Terracon Consulting
Project: San Mateo; Kissimmee, FL
QC Batch ID: MP33930 Methods: SW846 6010C Matrix Type: SOLID Units: ug/l
Prep Date: 06/23/18
Sample Final FA55117-1 PS Spike Spike Spike QC Metal ml ml Raw Corr.** ug/l ml ug/ml ug/l % Rec Limits
Aluminum
Antimony
Arsenic 9.8 10 59.7 58.506 164.9 0.2 5 100 106.4 80-120
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP33930: FA55261-1, FA55261-2, FA55261-3, FA55261-4, FA55261-5, FA55261-6, FA55261-7,FA55261-8, FA55261-9, FA55261-10
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(**) Corr. sample result = Raw * (sample volume / final volume)(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
84 of 102
FA55261
55.1.5
BLANK RESULTS SUMMARY Part 2 - Method Blanks
Login Number: FA55261 Account: TERCFLWP - Terracon Consulting
Project: San Mateo; Kissimmee, FL
QC Batch ID: MP33933 Methods: SW846 6010C Matrix Type: SOLID Units: mg/kg
Prep Date: 06/25/18
MB Metal RL IDL MDL raw final
Aluminum 10 .7 1.8
Antimony 1.0 .05 .065
Arsenic 0.50 .065 .1 -0.22 <0.50
Barium 10 .05 .05
Beryllium 0.25 .01 .025
Cadmium 0.20 .01 .025
Calcium 250 2.5 2.5
Chromium 0.50 .05 .05
Cobalt 2.5 .01 .025
Copper 1.3 .05 .05
Iron 15 .85 .85
Lead 1.0 .05 .05
Magnesium 250 1.8 1.8
Manganese 0.75 .025 .025
Molybdenum 2.5 .015 .025
Nickel 2.0 .02 .025
Potassium 500 10 10
Selenium 1.0 .12 .12
Silver 0.50 .035 .041
Sodium 500 25 25
Strontium 0.50 .025 .025
Thallium 0.50 .055 .055
Tin 2.5 .045 .045
Titanium 0.50 .025 .025
Vanadium 2.5 .025 .025
Zinc 1.0 .15 .15
Associated samples MP33933: FA55261-11, FA55261-12, FA55261-13, FA55261-14, FA55261-15, FA55261-16,FA55261-17, FA55261-18, FA55261-19, FA55261-20, FA55261-21, FA55261-22, FA55261-23, FA55261-24, FA55261-25, FA55261-26, FA55261-27, FA55261-28, FA55261-29, FA55261-30
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
85 of 102
FA55261
55.2.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA55261 Account: TERCFLWP - Terracon Consulting
Project: San Mateo; Kissimmee, FL
QC Batch ID: MP33933 Methods: SW846 6010C Matrix Type: SOLID Units: mg/kg
Prep Date: 06/25/18 06/25/18
FA55261-11 QC FA55261-11 Spikelot QC Metal Original DUP RPD Limits Original MS MPFLICP2 % Rec Limits
Aluminum
Antimony
Arsenic 0.0 0.0 NC 0-20 0.0 79.4 86.8 91.5 80-120
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP33933: FA55261-11, FA55261-12, FA55261-13, FA55261-14, FA55261-15, FA55261-16,FA55261-17, FA55261-18, FA55261-19, FA55261-20, FA55261-21, FA55261-22, FA55261-23, FA55261-24, FA55261-25, FA55261-26, FA55261-27, FA55261-28, FA55261-29, FA55261-30
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
86 of 102
FA55261
55.2.2
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA55261 Account: TERCFLWP - Terracon Consulting
Project: San Mateo; Kissimmee, FL
QC Batch ID: MP33933 Methods: SW846 6010C Matrix Type: SOLID Units: mg/kg
Prep Date: 06/25/18
FA55261-11 Spikelot MSD QC Metal Original MSD MPFLICP2 % Rec RPD Limit
Aluminum
Antimony
Arsenic 0.0 85.7 91.6 93.5 7.6 20
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP33933: FA55261-11, FA55261-12, FA55261-13, FA55261-14, FA55261-15, FA55261-16,FA55261-17, FA55261-18, FA55261-19, FA55261-20, FA55261-21, FA55261-22, FA55261-23, FA55261-24, FA55261-25, FA55261-26, FA55261-27, FA55261-28, FA55261-29, FA55261-30
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
87 of 102
FA55261
55.2.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA55261 Account: TERCFLWP - Terracon Consulting
Project: San Mateo; Kissimmee, FL
QC Batch ID: MP33933 Methods: SW846 6010C Matrix Type: SOLID Units: mg/kg
Prep Date: 06/25/18
BSP Spikelot QC Metal Result MPFLICP2 % Rec Limits
Aluminum
Antimony
Arsenic 93.4 100 93.4 80-120
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP33933: FA55261-11, FA55261-12, FA55261-13, FA55261-14, FA55261-15, FA55261-16,FA55261-17, FA55261-18, FA55261-19, FA55261-20, FA55261-21, FA55261-22, FA55261-23, FA55261-24, FA55261-25, FA55261-26, FA55261-27, FA55261-28, FA55261-29, FA55261-30
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
88 of 102
FA55261
55.2.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: FA55261 Account: TERCFLWP - Terracon Consulting
Project: San Mateo; Kissimmee, FL
QC Batch ID: MP33933 Methods: SW846 6010C Matrix Type: SOLID Units: ug/l
Prep Date: 06/25/18
FA55261-11 QC Metal Original SDL 1:5 %DIF Limits
Aluminum
Antimony
Arsenic 0.00 0.00 NC 0-10
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP33933: FA55261-11, FA55261-12, FA55261-13, FA55261-14, FA55261-15, FA55261-16,FA55261-17, FA55261-18, FA55261-19, FA55261-20, FA55261-21, FA55261-22, FA55261-23, FA55261-24, FA55261-25, FA55261-26, FA55261-27, FA55261-28, FA55261-29, FA55261-30
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
89 of 102
FA55261
55.2.4
POST DIGESTATE SPIKE SUMMARY
Login Number: FA55261 Account: TERCFLWP - Terracon Consulting
Project: San Mateo; Kissimmee, FL
QC Batch ID: MP33933 Methods: SW846 6010C Matrix Type: SOLID Units: ug/l
Prep Date: 06/25/18
Sample Final FA55261-11 PS Spike Spike Spike QC Metal ml ml Raw Corr.** ug/l ml ug/ml ug/l % Rec Limits
Aluminum
Antimony
Arsenic 9.8 10 96.1 0.2 5 100 96.1 80-120
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP33933: FA55261-11, FA55261-12, FA55261-13, FA55261-14, FA55261-15, FA55261-16,FA55261-17, FA55261-18, FA55261-19, FA55261-20, FA55261-21, FA55261-22, FA55261-23, FA55261-24, FA55261-25, FA55261-26, FA55261-27, FA55261-28, FA55261-29, FA55261-30
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(**) Corr. sample result = Raw * (sample volume / final volume)(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
90 of 102
FA55261
55.2.5
BLANK RESULTS SUMMARY Part 2 - Method Blanks
Login Number: FA55261 Account: TERCFLWP - Terracon Consulting
Project: San Mateo; Kissimmee, FL
QC Batch ID: MP33934 Methods: SW846 6010C Matrix Type: SOLID Units: mg/kg
Prep Date: 06/25/18
MB Metal RL IDL MDL raw final
Aluminum 10 .7 1.8
Antimony 1.0 .05 .065
Arsenic 0.50 .065 .1 -0.030 <0.50
Barium 10 .05 .05
Beryllium 0.25 .01 .025
Cadmium 0.20 .01 .025
Calcium 250 2.5 2.5
Chromium 0.50 .05 .05
Cobalt 2.5 .01 .025
Copper 1.3 .05 .05
Iron 15 .85 .85
Lead 1.0 .05 .05
Magnesium 250 1.8 1.8
Manganese 0.75 .025 .025
Molybdenum 2.5 .015 .025
Nickel 2.0 .02 .025
Potassium 500 10 10
Selenium 1.0 .12 .12
Silver 0.50 .035 .041
Sodium 500 25 25
Strontium 0.50 .025 .025
Thallium 0.50 .055 .055
Tin 2.5 .045 .045
Titanium 0.50 .025 .025
Vanadium 2.5 .025 .025
Zinc 1.0 .15 .15
Associated samples MP33934: FA55261-31, FA55261-32, FA55261-33, FA55261-34, FA55261-35, FA55261-36,FA55261-37, FA55261-38, FA55261-39, FA55261-40, FA55261-41, FA55261-42, FA55261-43, FA55261-44, FA55261-45, FA55261-46, FA55261-47, FA55261-48, FA55261-49, FA55261-50
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
91 of 102
FA55261
55.3.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA55261 Account: TERCFLWP - Terracon Consulting
Project: San Mateo; Kissimmee, FL
QC Batch ID: MP33934 Methods: SW846 6010C Matrix Type: SOLID Units: mg/kg
Prep Date: 06/25/18 06/25/18
FA55261-31 QC FA55261-31 Spikelot QC Metal Original DUP RPD Limits Original MS MPFLICP2 % Rec Limits
Aluminum
Antimony
Arsenic 0.43 0.43 0.0 0-20 0.43 95.7 98.6 96.6 80-120
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP33934: FA55261-31, FA55261-32, FA55261-33, FA55261-34, FA55261-35, FA55261-36,FA55261-37, FA55261-38, FA55261-39, FA55261-40, FA55261-41, FA55261-42, FA55261-43, FA55261-44, FA55261-45, FA55261-46, FA55261-47, FA55261-48, FA55261-49, FA55261-50
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
92 of 102
FA55261
55.3.2
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA55261 Account: TERCFLWP - Terracon Consulting
Project: San Mateo; Kissimmee, FL
QC Batch ID: MP33934 Methods: SW846 6010C Matrix Type: SOLID Units: mg/kg
Prep Date: 06/25/18
FA55261-31 Spikelot MSD QC Metal Original MSD MPFLICP2 % Rec RPD Limit
Aluminum
Antimony
Arsenic 0.43 111 116 95.0 14.8 20
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP33934: FA55261-31, FA55261-32, FA55261-33, FA55261-34, FA55261-35, FA55261-36,FA55261-37, FA55261-38, FA55261-39, FA55261-40, FA55261-41, FA55261-42, FA55261-43, FA55261-44, FA55261-45, FA55261-46, FA55261-47, FA55261-48, FA55261-49, FA55261-50
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
93 of 102
FA55261
55.3.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA55261 Account: TERCFLWP - Terracon Consulting
Project: San Mateo; Kissimmee, FL
QC Batch ID: MP33934 Methods: SW846 6010C Matrix Type: SOLID Units: mg/kg
Prep Date: 06/25/18
BSP Spikelot QC Metal Result MPFLICP2 % Rec Limits
Aluminum
Antimony
Arsenic 94.4 100 94.4 80-120
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP33934: FA55261-31, FA55261-32, FA55261-33, FA55261-34, FA55261-35, FA55261-36,FA55261-37, FA55261-38, FA55261-39, FA55261-40, FA55261-41, FA55261-42, FA55261-43, FA55261-44, FA55261-45, FA55261-46, FA55261-47, FA55261-48, FA55261-49, FA55261-50
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
94 of 102
FA55261
55.3.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: FA55261 Account: TERCFLWP - Terracon Consulting
Project: San Mateo; Kissimmee, FL
QC Batch ID: MP33934 Methods: SW846 6010C Matrix Type: SOLID Units: ug/l
Prep Date: 06/25/18
FA55261-31 QC Metal Original SDL 1:5 %DIF Limits
Aluminum
Antimony
Arsenic 7.70 8.00 3.9 0-10
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP33934: FA55261-31, FA55261-32, FA55261-33, FA55261-34, FA55261-35, FA55261-36,FA55261-37, FA55261-38, FA55261-39, FA55261-40, FA55261-41, FA55261-42, FA55261-43, FA55261-44, FA55261-45, FA55261-46, FA55261-47, FA55261-48, FA55261-49, FA55261-50
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
95 of 102
FA55261
55.3.4
POST DIGESTATE SPIKE SUMMARY
Login Number: FA55261 Account: TERCFLWP - Terracon Consulting
Project: San Mateo; Kissimmee, FL
QC Batch ID: MP33934 Methods: SW846 6010C Matrix Type: SOLID Units: ug/l
Prep Date: 06/25/18
Sample Final FA55261-31 PS Spike Spike Spike QC Metal ml ml Raw Corr.** ug/l ml ug/ml ug/l % Rec Limits
Aluminum
Antimony
Arsenic 9.8 10 7.7 7.546 106 0.2 5 100 98.5 80-120
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP33934: FA55261-31, FA55261-32, FA55261-33, FA55261-34, FA55261-35, FA55261-36,FA55261-37, FA55261-38, FA55261-39, FA55261-40, FA55261-41, FA55261-42, FA55261-43, FA55261-44, FA55261-45, FA55261-46, FA55261-47, FA55261-48, FA55261-49, FA55261-50
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(**) Corr. sample result = Raw * (sample volume / final volume)(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
96 of 102
FA55261
55.3.5
BLANK RESULTS SUMMARY Part 2 - Method Blanks
Login Number: FA55261 Account: TERCFLWP - Terracon Consulting
Project: San Mateo; Kissimmee, FL
QC Batch ID: MP33941 Methods: SW846 6010C Matrix Type: SOLID Units: mg/kg
Prep Date: 06/26/18
MB Metal RL IDL MDL raw final
Aluminum 10 .7 1.8
Antimony 1.0 .05 .065
Arsenic 0.50 .065 .1 -0.040 <0.50
Barium 10 .05 .05
Beryllium 0.25 .01 .025
Cadmium 0.20 .01 .025
Calcium 250 2.5 2.5
Chromium 0.50 .05 .05
Cobalt 2.5 .01 .025
Copper 1.3 .05 .05
Iron 15 .85 .85
Lead 1.0 .05 .05
Magnesium 250 1.8 1.8
Manganese 0.75 .025 .025
Molybdenum 2.5 .015 .025
Nickel 2.0 .02 .025
Potassium 500 10 10
Selenium 1.0 .12 .12
Silver 0.50 .035 .041
Sodium 500 25 25
Strontium 0.50 .025 .025
Thallium 0.50 .055 .055
Tin 2.5 .045 .045
Titanium 0.50 .025 .025
Vanadium 2.5 .025 .025
Zinc 1.0 .15 .15
Associated samples MP33941: FA55261-51, FA55261-52, FA55261-53, FA55261-54, FA55261-55
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
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FA55261
55.4.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA55261 Account: TERCFLWP - Terracon Consulting
Project: San Mateo; Kissimmee, FL
QC Batch ID: MP33941 Methods: SW846 6010C Matrix Type: SOLID Units: mg/kg
Prep Date: 06/26/18 06/26/18
FA55261-51 QC FA55261-51 Spikelot QC Metal Original DUP RPD Limits Original MS MPFLICP2 % Rec Limits
Aluminum
Antimony
Arsenic 0.19 0.23 19.0 0-20 0.19 86.5 87.1 99.1 80-120
Barium
Beryllium
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper
Iron
Lead anr
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP33941: FA55261-51, FA55261-52, FA55261-53, FA55261-54, FA55261-55
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
98 of 102
FA55261
55.4.2
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA55261 Account: TERCFLWP - Terracon Consulting
Project: San Mateo; Kissimmee, FL
QC Batch ID: MP33941 Methods: SW846 6010C Matrix Type: SOLID Units: mg/kg
Prep Date: 06/26/18
FA55261-51 Spikelot MSD QC Metal Original MSD MPFLICP2 % Rec RPD Limit
Aluminum
Antimony
Arsenic 0.19 86.9 78.3 110.7 0.5 20
Barium
Beryllium
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper
Iron
Lead anr
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP33941: FA55261-51, FA55261-52, FA55261-53, FA55261-54, FA55261-55
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
99 of 102
FA55261
55.4.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA55261 Account: TERCFLWP - Terracon Consulting
Project: San Mateo; Kissimmee, FL
QC Batch ID: MP33941 Methods: SW846 6010C Matrix Type: SOLID Units: mg/kg
Prep Date: 06/26/18
BSP Spikelot QC Metal Result MPFLICP2 % Rec Limits
Aluminum
Antimony
Arsenic 99.7 100 99.7 80-120
Barium
Beryllium
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper
Iron
Lead anr
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP33941: FA55261-51, FA55261-52, FA55261-53, FA55261-54, FA55261-55
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
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100 of 102
FA55261
55.4.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: FA55261 Account: TERCFLWP - Terracon Consulting
Project: San Mateo; Kissimmee, FL
QC Batch ID: MP33941 Methods: SW846 6010C Matrix Type: SOLID Units: ug/l
Prep Date: 06/26/18
FA55261-51 QC Metal Original SDL 1:5 %DIF Limits
Aluminum
Antimony
Arsenic 3.60 0.00 100.0(a) 0-10
Barium
Beryllium
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper
Iron
Lead anr
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP33941: FA55261-51, FA55261-52, FA55261-53, FA55261-54, FA55261-55
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
_________________________________________________________________________________________________________
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FA55261
55.4.4
POST DIGESTATE SPIKE SUMMARY
Login Number: FA55261 Account: TERCFLWP - Terracon Consulting
Project: San Mateo; Kissimmee, FL
QC Batch ID: MP33941 Methods: SW846 6010C Matrix Type: SOLID Units: ug/l
Prep Date: 06/26/18
Sample Final FA55261-51 PS Spike Spike Spike QC Metal ml ml Raw Corr.** ug/l ml ug/ml ug/l % Rec Limits
Aluminum
Antimony
Arsenic 9.8 10 3.6 3.528 107.8 0.2 5 100 104.3 80-120
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP33941: FA55261-51, FA55261-52, FA55261-53, FA55261-54, FA55261-55
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(**) Corr. sample result = Raw * (sample volume / final volume)(anr) Analyte not requested
_________________________________________________________________________________________________________
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102 of 102
FA55261
55.4.5
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