' T McKesson Corporation One Post Street San Francisco, CA 94104 608.848.4134 Tel
Jean Mescher Director, Environmental Services
US I:PA RI-CORDSCKNTFR RKGION S
494726
MCKESSON Empowering Healthcare
Via Federal Express
December 8, 2005
Mr. Michael A. Gifford (RPM/OSC) Remedial Response Branch, Region 5 U.S. Environmental Protection Agency 77 W. Jackson Boulevard, SE-4J Chicago, IL 60604
Subject: Monthly Progress Report - November 2005 XXKem Site, Toledo, Ohio
Dear Mr. Gifford:
Pursuant to Section VI.2.6 of the Administrative Order by Consent in this matter, enclosed is Safety-Kleen Envirosystems Company's monthly progress report.
If you have any questions regarding this monthly progress report, please do not hesitate to contact me at (608) 848-4134.
/A. Mescher rbject Coordinator
Enclosure
Copy: Tim Christman, GEPA Sherry L. Estes, USEPA (via Federal Express) Paul Jayko, GEPA Jane Montgomery, Schiff, et. al. David Leffler, City of Toledo Frank Robinson, McKesson (w/o enclosure)
- • ' Cousins Waste Control Corporation - PSC
Memo Toe JeanMescher
Prom Michael Graf
12rt)5/2005
RK XXKEM 84*' Monthly Report >1
XXKEM 84tli Monthly Rsport - NovMnber 2005
Dear Jean,
DuringNovember2005, no LES operations have occurred at the XXKEM site in Toiedo, Ohio. Cousins Waste Corrtrol (CWCC) performed tasks to supplement the LES abandonment and well installation. Fluid samples collected from existing well PX-42 and new wells PX-58 and 59 were analyzed tiy Brighton Analytical of Brighton Michigan; the laboratory reports are attached. In addition, all wastes generated during October 2005 were taken off-site for dispr^; the Hazardous Waste Manifests will be included in next months report. Also, Mannik & Smith surveyed the new well casings and secondly containment discharge line near the southern boundary of the landfill; the results of the sun/ey are attached.
Plans for December 2005 include removal of the fiac tank.
If you have any questions, please call.
Sincerely.
Michael Graf
Attachments; Brighton Analytical Laboratory Reports Mannik & Smith Survey Results
1701 E. Matzinger Road Toledo. Ohio 43612 {419)726-1500
THg MANNIK & SMITH QROUF, INC. laOQ Indian Wood CIrola
Maumae. Ohio 43837-4088 (411)091-2322
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American Environmental Group Ltd.
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December 5,2005 ^ .
Cousins Waste Control, Inc. BBC/PSC ' ^ ; 1701 East Matzinger Road Toledo, OH 43612
Attn.: Mike Graf
SubJ.r Repair Work at Landfill Toledo, Ohio
Dear Mr. Graf,
Per our conversations concerning the r^r worit performed October 26"" and October 28"*, 2005 at the Cousins Landfill in Toledo, Ohio. AEGL certifies that all woric was performed to industry standards, AEGL further certifies that all seams made were made to industry standards and all seams were non-destructively tested and passed.
If you require further information, please contact me at 330-659-5930.
Sincerely, American Environmental Group, Ltd.
3600 Brecksville Rd, Suite 100. Richfield, OH 44286 • Pk 330-659-5930. Fx: 330-659-5931
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Brighton Analytical, L.L.C. 2105 Pless Drive
Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650
Sample Date: 10/28/2005 Submit Date: 10/28/2005 Report Date: 11/07/2005
To: Cousins Waste Control Corp. 1701 -1801 Matzinger Road Toledo, OH 43612
BA Report Number 83603 BA Sample ID: BK04764
Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number: P0#63602070
Sample ID: PX58 leachate
Parameters Results Units DL Method Reference Analyst Analysis
Date
[>CB/Pesticlde Analysis i-BHC Not detected ug/L 0.01 EPA 608 BY 11/02/2005
i-Chlordane Not detected ug/L 0.02 EPA 608 BY 11/02/2005
Kldrin Not detected ug/L 0.01 EPA 608 BY 11/02/2005
VRO 1016 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
^RO 1221 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
KRO 1232 Not detected ug/L 0.4 EPA 608 BY 11/02/2005
^R0 1242 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
^RO 1248 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
^RO 1254 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
IRQ 1260 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
^RO 1262 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
\R0 1268 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
)-BHC Not detected ug/L 0.01 EPA 608 BY 11/02/2005
3P-6(PBB) Not detected ug/L 0.01 EPA 608 BY 11/02/2005
1-BHC Not detected ug/L 0.01 EPA 608 BY 11/02/2005
1,4-DDD Not detected ug/L 0.02 EPA 608 BY 11/02/2005
1,4-DDE Not detected ug/L 0.02 EPA 608 BY 11/02/2005
1,4-DDT Not detected ug/L 0.02 EPA 608 BY 11/02/2005
^ieldrin Not detected ug/L 0.02 EPA 608 BY 11/02/2005
mdosulfan 1 Not detected ug/L 0.02 EPA 608 BY 11/02/2005
indosulfan 11 Not detected ug/L 0.03 EPA 608 BY 11/02/2005
Endosulfan sulfate Not detected ug/L 0.05 EPA 608 BY 11/02/2005
mdrin Not detected ug/L 0.02 EPA 608 BY 11/02/2005
mdrin aldehyde Not detected ug/L 0.02 EPA 608 BY 11/02/2005
mdrin ketone Not detected ug/L 0.02 EPA 608 BY 11/02/2005
5-BHC(Lindane) Not detected ug/L 0.01 EPA 608 BY 11/02/2005
5-Chlordane Not detected ug/L 0.02 EPA 608 BY 11/02/2005
leptachlor Not detected ug/L 0.01 EPA 608 BY 11/02/2005
3eptachlor epoxide Not detected ug/L 0.01 EPA 608 BY 11/02/2005
Pagel
Brighton Analytical, L.L.C. 2105 Pless Drive
Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650
Sample Date: 10/28/2005 Submit Date: 10/28/2005 Report Date: 11/07/2005
To: Cousins Waste Control Corp. 1701 -1801 Matzinger Road Toledo, OH 43612
BA Report Number: 83603 BA Sample ID: BK04764
Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number: P0#63602070
Sample ID: PX58 leachate
Parameters Results Units DL Method Reference Analyst Analysis
Date
texabromobenzene Not detected ug/L 0.02 EPA 608 BY 11/02/2005
vtethoxychlor Not detected ug/L 0.05 EPA 608 BY 11/02/2005
vtirex Not detected ug/L 0.02 EPA 608 BY 11/02/2005
Toxaphene Not detected ug/L 0.1 EPA 608 BY 11/02/2005
'CB/Pesticide liquid (extraction) Extracted 3510/3550 LS 11/01/2005
$eml-Volatile Analysis Dimethylaniline Not detected ug/L 10 EPA 625 RG 11/02/2005
JN A liquid (extraction) Extracted 3510/3550 LS 10/31/2005
Volatile Analysis \cetone Not detected ug/L 500 SW846 8260 JH 11/03/2005
\crylonitrile Not detected ug/L 20 SW846 8260 JH 11/03/2005
Jenzene 94 ug/L 20 SW846 8260 JH 11/03/2005
3romochloromethane Not detected ug/L 20 SW846 8260 JH 11/03/2005
Jromodichloromethane Not detected ug/L 20 SW846 8260 JH 11/03/2005
3romoform Not detected ug/L 20 SW846 8260 JH 11/03/2005
3romomethane(Methyl Bromide) Not detected ug/L 20 SW846 8260 JH 11/03/2005
l-Butanone (MEK.) Not detected ug/L 100 SW846 8260 JH 11/03/2005.
2arbon disulfide Not detected ug/L 100 SW846 8260 JH 11/03/2005
Tarbon t^rachloride Not detected ug/L 20 SW846 8260 JH 11/03/2005
2hlorobenzene 22 ug/L 20 SW846 8260 JH 11/03/2005
rhloroethanc 97 ug/L 20 SW846 8260 JH 11/03/2005
rhloroform Not detected ug/L 20 SW846 8260 JH 11/03/2005
rhloromethane(Methyl Chloride) Not detected ug/L 20 SW846 8260 JH 11/03/2005
;is-1,2-Dichloroethene Not detected ug/L 20 SW846 8260 JH 11/03/2005
:is-1,3-Dichloropropene Not detected ug/L 20 SW846 8260 JH 11/03/2005
1,2-Dibromo-3-Chloropropane Not detected ug/L 20 SW846 8260 JH 11/03/2005
3ibromochloromethane Not detected ug/L 20 SW846 8260 JH 11/03/2005
1,2-Dibromoethane Not detected ug/L 20 SW846 8260 JH 11/03/2005
3ibromomethane(Methylene Bromide) Not detected ug/L 20 SW846 8260 JH 11/03/2005
1,2-Dichlorobenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005
Page 2
Brighton Analytical, L.L.C. 2105 Pless Drive
Brighton, Michigan 48116 TM Phone; (810) 229-7575 FAX: (810) 229-8650
Sample Date: 10/28/2005 Submit Date: 10/28/2005 Rqx)rtDate: 11/07/2005
To: Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612
BA Report Number 83603 BA Sample ID: BK04764
Project Name: Cousins Waste ControI/XXKEM WV Abandonment Project Number: PO#63602D70
Sample ID: PX58 leachate
Parameters Results Units DL Method Reference Analyst Analysis
Date
l3-Dichlorobenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005
1,4-Dichlorobenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005
Qichlorodifluoromethane Not detected ug/L 20 SW846 8260 JH 11/03/2005
1,1-Dichloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005
1,2-Dichloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005
1,1-Dichloroethene Not detected ug/L 20 SW846 8260 JH 11/03/2005
1,2-Dichloropropane Not detected ug/L 20 SW846 8260 JH 11/03/2005
Diethyl ether Not detected ug/L 200 SW846 8260 JH 11/03/2005
Ethyl benzene 510 ug/L 20 SW846 8260 JH 11/03/2005
Hexachloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005
>-Hexanone(Methyl Butyl Ketone) Not detected ug/L 100 SW846 8260 JH 11/03/2005
isopropylbenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005
\tethyl iodide(Iodomethane) Not detected ug/L 20 SW846 8260 JH 11/03/2005
Vlethyl(tert)butyl ether(MTBE) Not detected ug/L 100 SW846 8260 JH 11/03/2005
t-Methyl-2-pentanonc(MIBK) Not detected ug/L 100 SW846 8260 JH 11/03/2005
vtethylene chloride Not detected ug/L 100 SW846 8260 JH 11/03/2005
1-Methylnaphthalene Not detected ug/L 100 SW846 8260 JH 11/03/2005
^Japhthalene Not detected ug/L 100 SW846 8260 JH 11/03/2005
i-Butylbenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005
1-Propylbenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005
styrene Not detected ug/L 20 SW846 8260 JH 11/03/2005
1,1,1,2-Tetrachloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005
1,1,2,2-Tetrachloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005
r etrachloroethene Not detected ug/L 20 SW846 8260 JH 11/03/2005
Toluene 46 ug/L 20 SW846 8260 JH 11/03/2005
rans-1,2-Dichloroethene Not detected ug/L 20 SW846 8260 JH 11/03/2005
rans-1,3-Dichloropropene Not detected ug/L 20 SW846 8260 JH 11/03/2005
rans-1,4-Dichloro-2-butene Not detected ug/L 20 SW846 8260 JH 11/03/2005
1,2,3-Trichlorobenzene Not detected ug/L 100 SW846 8260 JH 11/03/2005
1,2,4-Trichlorobenzene Not detected ug/L 100 SW846 8260 JH 11/03/2005
1,1,1-Trichloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005
1,1,2-T richloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005
Page 3
Brighton Analytical, L.L.C. 2105 Pless Drive
Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX; (810) 229-8650
Sample E>ate: 10/28/2005 Submit Date: 10/28/2005
Report Date: 11/07/2005
To: Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612
BA Report Number 83603 BA Sample ID: BK04764
Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number: P0#63602070
Sample ID: PX58 leachate
Parameters Results Units DL Method Reference Analyst Analysis
Date
rrichloroefliene Not detected ug/L 20 SW846 8260 JH 11/03/2005 rrichlorofluoromethane Not detected ug/L 20 SW846 8260 JH 11/03/2005 1,2,3-Trichloropropane Not detected ug/L 20 SW846 8260 JH 11/03/2005 1,2,3-Trimethylbenzene 44 ug/L 20 SW846 8260 JH 11/03/2005 1,2,4-Trimethylbenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005 1,3,5-Trimethylbenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005 Vinyl chloride 61 ug/L 20 SW846 8260 JH 11/03/2005
Xylenes(total) 1800 ug/L 60 SW846 8260 JH 11/03/2005
DL=Reported detection limit for analytical method requested. Some compounds Released by: require special analytical methods to achieve MDEQ designated target detection limits (TDL). Date:
Elevated volatile dl due to sample matrix.
1
Page 4
Brighton Analytical, L.L.C. 2105 Pless Drive
Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650
Sample Date: 10/28/2005 Submit Date: 10/28/2005 Report Date: 11/07/2005
To: Cousins Waste Control Corp. 1701-1801 Matzlnger Road Toledo, OH 43612
BA Report Number: 83603 BA Sample ID: BK04765
Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number: P0#63602070
Sample ID: PX59 leachate
Parameters Results Units DL Method Reference Analyst Analysis
Date
PCB/Pesticide Analysis
i-BHC Not detected ug/L 0.01 EPA 608 BY 11/02/2005
i-Chlordane Not detected ug/L 0.02 EPA 608 BY 11/02/2005
\ldrin Not detected ug/L 0.01 EPA 608 BY 11/02/2005
\RO 1016 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
\RO 1221 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
\R0 1232 Not detected ug/L 0.4 EPA 608 BY 11/02/2005
\RO 1242 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
\RO 1248 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
\RO 1254 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
\RO 1260 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
\RO 1262 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
\R0 1268 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
)-BHC Not detected ug/L 0.01 EPA 608 BY 11/02/2005
3P-6(PBB) Not detected ug/L 0.01 EPA 608 BY 11/02/2005
1-BHC Not detected ug/L 0.01 EPA 608 BY 11/02/2005
1,4-DDD Not detected ug/L 0.02 EPA 608 BY 11/02/2005
1,4-DDE Not detected ug/L 0.02 EPA 608 BY 11/02/2005
1,4-DDT Not detected ug/L 0.02 EPA 608 BY 11/02/2005
Dieldrin Not detected ug/L 0.02 EPA 608 BY 11/02/2005
Endosulfan 1 Not detected ug/L 0.02 EPA 608 BY 11/02/2005
3ndosulfan 11 Not detected ug/L 0.03 EPA 608 BY 11/02/2005
3ndosulfan sulfate Not detected ug/L 0.05 EPA 608 BY 11/02/2005
3ndrin Not detected ug/L 0.02 EPA 608 BY 11/02/2005
Bndrin aldehyde Not detected ug/L 0.02 EPA 608 BY 11/02/2005
Sndrin ketone Not detected ug/L 0.02 EPA 608 BY 11/02/2005
j-BHC(Lindane) Not detected ug/L 0.01 EPA 608 BY 11/02/2005
;-Chlordane Not detected ug/L 0.02 EPA 608 BY 11/02/2005
rleptachlor Not detected ug/L 0.01 EPA 608 BY 11/02/2005
rleptachlor epoxide Not detected ug/L 0.01 EPA 608 BY 11/02/2005
-lexabromobenzene Not detected ug/L 0.02 EPA 608 BY 11/02/2005
Page 1
Brighton Analytical, L.L.C. 2105 Pless Drive
Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650
Sample Date: 10/28/2005 Submit Date: 10/28/2005 Report Date: 11/07/2005
To; Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612
BA Report Number. 83603 BA Sample ID: BK0476S
Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number: P0#63602070
Sample ID: PX59 leachate
Parameters Results Units DL Method Reference Analyst Analysis
Date
y4eflioxychlor Not detected ug/L 0.05 EPA 608 BY 11/02/2005
ttirex Not detected ug/L 0.02 EPA 608 BY 11/02/2005
Poxt^ene Not detected ug/L 0.1 EPA 608 BY 11/02/2005
X!B/Pesticide liquid (extraction) Extracted 3510/3550 LS 11/01/2005
Semi-Volatile Analysis
Dimethylaniline Not detected ug/L 10 EPA 625 RG 11/02/2005
3NA liquid (extraction) Extracted 3510/3550 LS 10/31/2005
i/olatile Analysis
\cetone Not detected ug/L 500 SW846 8260 JH 11/03/2005
\ctylonitrile Not detected ug/L 20 SW846 8260 JH 11/03/2005
Benzene 92 ug/L 20 SW846 8260 JH 11/03/2005
Bromochloromethane Not detected ug/L 20 SW846 8260 JH 11/03/2005
Bromodichloromethane Not detected ug/L 20 SW846 8260 JH 11/03/2005
Bromoform Not detected ug/L 20 SW846 8260 JH 11/03/2005
Bromomethane(Methyl Bromide) Not detected ug/L 20 SW846 8260 JH 11/03/2005
t-Butanone (MEK) Not detected ug/L 100 SW846 8260 JH 11/03/2005
2arbon disulfide Not detected ug/L 100 SW846 8260 JH 11/03/2005
2arbon tetrachloride Not detected ug/L 20 SW846 8260 JH 11/03/2005
Dhlorobenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005
Dhloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005
Chloroform Not detected ug/L 20 SW846 8260 JH 11/03/2005
Chloromethane(Methyl Chloride) Not detected ug/L 20 SW846 8260 JH 11/03/2005
:is-1,2-Dichloroethene Not detected ug/L 20 SW846 8260 JH 11/03/2005
:is-1,3-Dichloropropene Not detected ug/L 20 SW846 8260 JH 11/03/2005
1,2-Dibromo-3-Chloropropane Not detected ug/L 20 SW846 8260 JH 11/03/2005
Oibromochloromethane Not detected ug/L 20 SW846 8260 JH 11/03/2005
1,2-Dibromoethane Not detected ug/L 20 SW846 8260 JH 11/03/2005
[)ibromomethane(Methylene Bromide) Not detected ug/L 20 SW846 8260 JH 11/03/2005
1,2-Dichlorobenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005
1,3-Dichlorobenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005
Page 2
Brighton Analytical, L.L.C. 2105 Pless Drive
Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650
Sample Date; 10/28/2005 Submit Date: 10/28/2005 Report Date: 11/07/2005
To: Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612
BA Report Number 83603 BA Sample ID: BK04765
Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number; P0#63602070
Sample ID: PXS9 leachate
Parameters Results Units DL Method Reference Analyst Analysis
Date
1,4-Dichlorobenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005
Dichlorodifluoromethane Not detected ug/L 20 SW846 8260 JH 11/03/2005
1,1 -Dich loroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005
1,2-Dichloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005
1,1-Dichloroethene Not detected ug/L 20 SW846 8260 JH 11/03/2005
1,2-Dichloropropane Not detected ug/L 20 SW846 8260 JH 11/03/2005
diethyl ether Not detected ug/L 200 SW846 8260 JH 11/03/2005
ithyl benzene Not detected ug/L 20 SW846 8260 JH 11/03/2005
^exachloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005
l-Hexanonc(Methyl Butyl Ketone) Not detected ug/L 100 SW846 8260 JH 11/03/2005
sopropylbenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005
Methyl iodide(Iodomethane) Not detected ug/L 20 SW846 8260 JH 11/03/2005
Vlethyl(tert)butyl ether(MTBE) Not detected ug/L 100 SW846 8260 JH 11/03/2005
t-Methyl-2-pentanone(MlBK) Not detected ug/L 100 SW846 8260 JH 11/03/2005
\4ethylene chloride Not detected ug/L 100 SW846 8260 JH 11/03/2005
1-Methylnaphthalene Not detected ug/L 100 SW846 8260 JH 11/03/2005
*4aphthalene Not detected ug/L 100 SW846 8260 JH 11/03/2005
i-Butylbenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005
i-Propylbcnzene Not detected ug/L 20 SW846 8260 JH 11/03/2005
Styrene Not detected ug/L 20 SW846 8260 JH 11/03/2005
1,1,1,2-T etrachloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005
1,1,2,2-Tetrachloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005
relrachloroethene Not detected ug/L 20 SW846 8260 JH 11/03/2005
Toluoie 30 ug/L 20 SW846 8260 JH 11/03/2005
Tans-1,2-Dichloroethene Not detected ug/L 20 SW846 8260 JH 11/03/2005
rans-1,3-Dichloropropene Not detected ug/L 20 SW846 8260 JH 11/03/2005
xans-l ,4-Dichloro-2-butene Not detected ug/L 20 SW846 8260 JH 11/03/2005
1,2,3-T richloro benzene Not detected ug/L 100 SW846 8260 JH 11/03/2005
1,2,4-T rich lorobenzene Not detected ug/L 100 SW846 8260 JH 11/03/2005
1,1,1-Trich loroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005
1,1,2-T richloroethane Not detected ug/L 20 SW846 8260 JH 11/03/2005
rrichloroethene Not detected ug/L 20 SW846 8260 JH 11/03/2005
Page 3
Brighton Analytical, L.L.C. 2105 Pless Drive
Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650
Sample Date: 10/28/2005
Submit Date: 10/28/2005
Report Date: 11/07/2005
To: Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612
BA Report Number: 83603
BA Sample ID: BK04765
Project Name: Cousins Waste Control/XXKEM WV Abandonment
Project Number: P0#63602070 Sample ID: PXS91eachate
Parameters Results Units DL Method Reference Analyst Analysis
Date
Trichlorofluoromethane Not detected ug/L 20 SW846 8260 JH 11/03/2005 1,2,3-Trichloropropane Not detected ug/L 20 SW846 8260 JH 11/03/2005 1,2,3-T rimethylbenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005 1,2,4-Trimethylbenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005 1,3,5-T rimethylbenzene Not detected ug/L 20 SW846 8260 JH 11/03/2005 Vinyl chloride Not detected ug/L 20 SW846 8260 JH 11/03/2005 Xylenes(total) Not detected ug/L 60 SW846 8260 JH 11/03/2005
DL=Reported detection limit for analytical method requested. Some compounds Released by: require special analytical methods to achieve MDEQ designated target detection limits (TDL). Date:
Elevated volatile dl due to sample matrix.
Page 4 •4
Brighton Analytical, L.L.C. 2105 Pless Drive
Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650
Sample Date: 10/28/2005 Submit Date: 10/28/2005 Report Date: 11/07/2005
To: Cousins Waste Control Corp. 1701 -1801 Matzinger Road Toledo, OH 43612
BA Report Number: 83603 BA Sample ID: BK04766
Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number: P0«63602070
Sample ID: PX42 leachate & LNAPL
Parameters Results Units DL Method Reference Analyst Analysis
Date
PCB/Pesticide Analysis
i-BHC Not detected ug/L 0.04 EPA 608 BY 11/02/2005
i-Chlordane Not detected ug/L 0.08 EPA 608 BY 11/02/2005
\Idrin Not detected ug/L 0.04 EPA 608 BY 11/02/2005
\RO 1016 Not detected ug/L 0.80 EPA 608 BY 11/02/2005
\RO 1221 Not detected ug/L 0.80 EPA 608 BY 11/02/2005
ytO 1232 Not detected ug/L 1.6 EPA 608 BY 11/02/2005
\RO 1242 Not detected ug/L 0.80 EPA 608 BY 11/02/2005
\RO 1248 Not detected ug/L 0.80 EPA 608 BY 11/02/2005
\R0 1254 11 ug/L 0.80 EPA 608 BY 11/02/2005
\RO 1260 Not detected ug/L 0.80 EPA 608 BY 11/02/2005
\RO 1262 Not detected ug/L 0.80 EPA 608 BY 11/02/2005
\RO 1268 Not detected ug/L 0.80 EPA 608 BY 11/02/2005
5-BHC Not detected ug/L 0.04 EPA 608 BY 11/02/2005
3P-6(PBB) Not detected ug/L 0.04 EPA 608 BY 11/02/2005
1-BHC Not detected ug/L 0.04 EPA 608 BY 11/02/2005
1,4-DDD Not detected ug/L 0.08 EPA 608 BY 11/02/2005
1,4-DDE Not detected ug/L 0.08 EPA 608 BY 11/02/2005
1,4-DDT Not detected ug/L 0.08 EPA 608 BY 11/02/2005
Dieldrin Not detected ug/L 0.08 EPA 608 BY 11/02/2005
Endosulfan I Not detected ug/L 0.08 EPA 608 BY 11/02/2005
Endosulfan II Not detected ug/L 0.12 EPA 608 BY 11/02/2005
Endosulfan sulfate Not detected ug/L 0.20 EPA 608 BY 11/02/2005
indrin Not detected ug/L 0.08 EPA 608 BY 11/02/2005
Endrin aldehyde Not detected ug/L 0.08 EPA 608 BY 11/02/2005
Endrin ketone Not detected ug/L 0.08 EPA 608 BY 11/02/2005
j-BHC(Lindane) Not detected ug/L 0.04 EPA 608 BY 11/02/2005
;-Chlordane Not detected ug/L 0.08 EPA 608 BY 11/02/2005
Hleptachlor Not detected ug/L 0.04 EPA 608 BY 11/02/2005
Heptachlor epoxide Not detected ug/L 0.04 EPA 608 BY 11/02/2005
hiexabromobenzene Not detected ug/L 0.08 EPA 608 BY 11/02/2005
Page I
Brighton Analytical, L.L.C. 2105 Pless Drive
Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650
Sample Date: 10/28/2005 Submit Date: 10/28/2005 Report Date: 11/07/2005
To: Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612
BA Report Number 83603 BA Sample ID: BK04766
Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number: P0#63602070
Sample ID: PX42 leachate & LNAPL
Parameters Results Units DL Method Reference Analyst Analysis
Date
Methoxychlor Not detected ug/L 0.20 EPA 608 BY 11/02/2005
Mirex Not detected ug/L 0.08 EPA 608 BY 11/02/2005
Total PCB 11 ug/L 0.80 EPA 608 BY 11/02/2005
Toxaphene Not detected ug/L 0.40 EPA 608 BY 11/02/2005
PCB/Pesticide liquid (extraction) Extracted 3510/3550 LS 11/01/2005
Semi-Volatile Analysis Dimethylaniline Not detected ug/L 10 EPA 625 RG 11/02/2005
BNA liquid (extraction) Extracted 3510/3550 LS 10/31/2005
Volatile Analysis Acetone Not detected ug/L 50 SW846 8260 JH 11/03/2005
Acrylonitrile Not detected ug/L 2 SW846 8260 JH 11/03/2005
Benzene Not detected ug/L 2 SW846 8260 JH 11/03/2005
Bromochioromethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
Bromodichloromethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
Bromoform Not detected ug/L 2 SW846 8260 JH 11/03/2005
Bromomethane(Methyl Bromide) Not detected ug/L 2 SW846 8260 JH 11/03/2005
2-Butanone (MEK) Not detected ug/L 10 SW846 8260 JH 11/03/2005
Carbon disulfide Not detected ug/L 10 SW846 8260 JH 11/03/2005
Carbon tetrachloride Not detected ug/L 2 SW846 8260 JH 11/03/2005
Chlorobenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005
Chloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
Chloroform Not detected ug/L 2 SW846 8260 JH 11/03/2005
Chloromethane(Methyl Chloride) Not detected ug/L 2 SW846 8260 JH 11/03/2005
cis-1,2-Dichloroethene Not detected ug/L 2 SW846 8260 JH 11/03/2005
:is-1,3-Dichloropropene Not detected ug/L 2 SW846 8260 JH 11/03/2005
l,2-Dibromo-3-Chloropropane Not detected ug/L 2 SW846 8260 JH 11/03/2005
Dibromochloromethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
1,2-Dibromoethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
Dibromomethane(Methylene Bromide) Not detected ug/L 2 SW846 8260 JH 11/03/2005
1,2-Dichlorobenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005
Page 2
1 4
Brighton Analytical, L.L.C. 2105 Pless Drive
Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650
Sample Date: 10/28/2005 Submit Date: 10/28/2005 Report Date: 11/07/2005
To: Cousins Waste Control Corp. 1701 -1801 Matzinger Road Toledo, OH 43612
BA Report Number 83603 BA Sample ID: BK04766
Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number: P0#63602070
Sample ID: PX42 leachate & LNAPL
Parameters Results Units DL Method Reference Analyst Analysis
Date
1,3-Dichlorobenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005
1,4-Dichlorobenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005
Dichlorodifluoromethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
1,1-Dichloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
1,2-Dichloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
1,1-Dichioroethene Not detected ug/L 2 SW846 8260 JH 11/03/2005
1,2-Dichloropropane Not detected ug/L 2 SW846 8260 JH 11/03/2005
Diethyl ether Not detected ug/L 20 SW846 8260 JH 11/03/2005
Ethyl benzene 180 ug/L 2 SW846 8260 JH 11/03/2005
Hexachloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
Z-Hexanone(Methyl Butyl Ketone) Not detected ug/L 10 SW846 8260 JH 11/03/2005
Isopropyibenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005
Methyl iodide(Iodomethane) Not detected ug/L 2 SW846 8260 JH 11/03/2005
Methyl(tert)butyl ether(MTBE) Not detected ug/L 10 SW846 8260 JH 11/03/2005
t-Methyl-2-pentanone(MIBK) Not detected ug/L 10 SW846 8260 JH 11/03/2005
Methylene chloride Not detected ug/L 10 SW846 8260 JH 11/03/2005
Z-Methylnaphthalene Not detected ug/L 10 SW846 8260 JH 11/03/2005
Naphthalene Not detected ug/L 10 SW846 8260 JH 11/03/2005
ri-Butylbenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005
i-Propylbenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005
Styrene Not detected ug/L 2 SW846 8260 JH 11/03/2005
1,1,1,2-T etrachloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
1,1,2,2-Tetrachloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
Tetrachloroethene Not detected ug/L 2 SW846 8260 JH 11/03/2005
Toluene 30 ug/L 2 SW846 8260 JH 11/03/2005
xans-1,2-Dichloroethene Not detected ug/L 2 SW846 8260 JH 11/03/2005
xans-l ,3-Dichloropropene Not detected ug/L 2 SW846 8260 JH 11/03/2005
;rans-1,4-Dichloro-2-butene Not detected ug/L 2 SW846 8260 JH 11/03/2005
1,2,3-Trichlorobenzene Not detected ug/L 10 SW846 8260 JH 11/03/2005
1,2,4-T richlorobenzaie Not detected ug/L 10 SW846 8260 JH 11/03/2005
1,1,1-Trichloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
1,1,2-Trichloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
Page 3
Brighton Analytical, L.L.C. 2105 Pless Drive
Brighton, Michigan 48116 TM Phone; (810) 229-7575 FAX: (810) 229-8650
Sample Date: 10/28/2005 Submit Date: 10/28/2005
Report Date: 11/07/2005
To; Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612
BA Report Number: 83603
BA Sample ID: BK04766
Project Name: Cousins Waste Control/XXKEM WV Abandonment
Project Number: P0#63602070
Sample ID: PX42 leachate & LNAPL
Parameters Results Units DL Method Reference Analyst Analysis
Date
Trichloroethene Not detected ug/L 2 SW846 8260 JH 11/03/2005 Trichlorofluoromethane Not detected ug/L 2 SW846 8260 JH 11/03/2005 1,2,3-Trichloropropane Not detected ug/L 2 SW846 8260 JH 11/03/2005 1,2,3-Trimethylbenzene 65 ug/L 2 SW846 8260 JH 11/03/2005 1,2,4-T rimethy Ibenzene 70 ug/L 2 SW846 8260 JH 11/03/2005 1,3,5-T rimethy Ibenzene 24 ug/L 2 SW846 8260 JH 11/03/2005 Vinyl chloride Not detected ug/L 2 SW846 8260 JH 11/03/2005 Xylenes(total) 1400 ug/L 6 SW846 8260 JH 11/03/2005
DL=Reported detection limit for analytical method requested. Some compounds require special analytical methods to achieve MDEQ designated target detection limits (TDL).
Elevated PCB/pesticide dl due to sample matrix. Elevated volatile dl due to sample matrix.
Released by:
Date:
Page 4
;i
Brighton Analytical, L.L.C. 2105 Pless Drive
Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650
Sample Date: 10/28/2005 Submit Date: 10/28/2005 RqjortDate: 11/07/2005
To: Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612
BA Report Number 83603 BA Sample ID: BK04767
Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number: P(M63602070
Sample ID: Dupl leachate
Parameters Results Units DL Mediod Reference Analyst Analysis
Date
PCB/Pesticide Analysis i-BHC Not detected ug/L 0.01 EPA 608 BY 11/02/2005
a-Chlordane Not detected ug/L 0.02 EPA 608 BY 11/02/2005
4ldrin Not detected ug/L 0.01 EPA 608 BY 11/02/2005
4RO 1016 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
4RO 1221 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
4RO 1232 Not detected ug/L 0.4 EPA 608 BY 11/02/2005
\RO 1242 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
ARO 1248 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
4RO 1254 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
4RO 1260 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
4RO 1262 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
4RO 1268 Not detected ug/L 0.2 EPA 608 BY 11/02/2005 b-BHC Not detected ug/L 0.01 EPA 608 BY 11/02/2005
BP-6(PBB) Not detected ug/L 0.01 EPA 608 BY 11/02/2005
i-BHC Not detected ug/L 0.01 EPA 608 BY 11/02/2005
t,4-DDD Not detected ug/L 0.02 EPA 608 BY 11/02/2005
t,4-DDE Not detected ug/L 0.02 EPA 608 BY 11/02/2005
t,4-DDT Not detected ug/L 0.02 EPA 608 BY 11/02/2005
Dieldrin Not detected ug/L 0.02 EPA 608 BY 11/02/2005
Endosulfan I Not detected ug/L 0.02 EPA 608 BY 11/02/2005
Bndosul&n II Not detected ug/L 0.03 EPA 608 BY 11/02/2005
Bndosulfan sulfate Not detected ug/L 0.05 EPA 608 BY 11/02/2005
Endrin Not detected ug/L 0.02 EPA 608 BY 11/02/2005
Bndrin aldehyde Not detected ug/L 0.02 EPA 608 BY 11/02/2005
Endrin ketone Not detected ug/L 0.02 EPA 608 BY 11/02/2005
;-BHC(Lindane) Not detected ug/L 0.01 EPA 608 BY 11/02/2005
j-Chlordane Not detected ug/L 0.02 EPA 608 BY 11/02/2005
Heptachlor Not detected ug/L 0.01 EPA 608 BY 11/02/2005
Heptachlor epoxide Not detected ug/L 0.01 EPA 608 BY 11/02/2005
Flexabromobenzene Not detected ug/L 0.02 EPA 608 BY 11/02/2005
Page 1
Brighton Analytical, L.L.C. 2105 Pless Drive
Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650
Sample Date: 10/28/2005
Submit Date: 10/28/2005
Report Date: 11/07/2005
To: Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612
BA Report Number 83603 BA Sample ID: BK04767
Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number: PO#636D2070
Sample ID: Dnpl leachate
Parameters Results Units DL Method Reference Analyst Analysis
Date
VIettioxychlor Not detected ug/L 0.05 EPA 608 BY 11/02A2005
Mirex Not detected ug/L 0.02 EPA 608 BY 11/02/2005
Foxaphene Not detected ug/L 0.1 EPA 608 BY 11/02/2005
PCB/Pesticide liquid (extraction) Extracted 3510/3550 LS 11/01/2005
Senii-Volatik Analysis
Dimethylaniline Not detected ug/L 10 EPA 625 RG 11/02/2005
SNA liquid (extraction) Extracted 3510/3550 LS 10/31/2005
Volatile Analysis
\cetone Not detected ug/L 50 SW846 8260 JH 11/03/2005
4ctylonitrile Not detected ug/L 2 SW846 8260 JH 11/03/2005
Benzene 78 ug/L 2 SW846 8260 JH 11/03/2005
Bromochloromethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
Bromodichloromethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
Bromoform Not detected ug/L 2 SW846 8260 JH 11/03/2005
Bromomethane(Methyl Bromide) Not detected ug/L 2 SW846 8260 JH 11/03/2005
t-Butanone (MEK) Not detected ug/L 10 SW846 8260 JH 11/03/2005
Carbon disulfide Not detected ug/L 10 SW846 8260 JH 11/03/2005
Carbon tetrachloride Not detected ug/L 2 SW846 8260 JH 11/03/2005
Chlorobenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005
Chloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
Chloroform Not detected ug/L 2 SW846 8260 JH 11/03/2005
Chloromethane(MethyI Chloride) Not detected ug/L 2 SW846 8260 JH 11/03/2005
:is-1,2-Dichloroethene Not detected ug/L 2 SW846 8260 JH 11/03/2005
:is-1,3-Dichloropropene Not detected ug/L 2 SW846 8260 JH 11/03/2005
[ ,2-Dibromo-3-Chloropropane Not detected ug/L 2 SW846 8260 JH 11/03/2005
Dibromochloromethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
1,2-Dibromoethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
3ibromomethane(Methylene Bromide) Not detected ug/L 2 SW846 8260 JH 11/03/2005
1,2-Dichlorobenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005
1,3-Dichlorobenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005
Page 2
Brighton Analytical, L.L.C. 2105 Pless Drive
Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650
Sample Date: 10/28/2005 Submit Date: 10/28/2005 Report Date: 11/07/2005
To; Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612
BA Report Number; 83603 BA Sample ID: BK04767
Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number: P0#63602070
Sample ID: Dnpl ieacbate
Parameters Results Units DL Method Reference Analyst Analysis
Date
1,4-Dichlorobenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005
3ichlorodifluoromethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
1,1-Dichloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
1,2-Dichloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
1,1-Dichioroethene Not detected ug/L 2 SW846 8260 JH 11/03/2005
1,2-Dichloropropane Not detected ug/L 2 SW846 8260 JH 11/03/2005
diethyl ether Not detected ug/L 20 SW846 8260 JH 11/03/2005
ithyl benzene Not detected ug/L 2 SW846 8260 JH 11/03/2005
3exachloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
J-Hexanone(Methyl Butyl Ketone) Not detected ug/L 10 SW846 8260 JH 11/03/2005
sopropy 1 ben zene Not detected ug/L 2 SW846 8260 JH 11/03/2005
diethyl iodide(Iodomethane) Not detected ug/L 2 SW846 8260 JH 11/03/2005
Vlethyl(tert)butyl ether(MTBE) Not detected ug/L 10 SW846 8260 JH 11/03/2005
l-Methyl-2-pentanone{MlBK) Not detected ug/L 10 SW846 8260 JH 11/03/2005
Vlethylene chloride Not detected ug/L 10 SW846 8260 JH 11/03/2005
J-Methylnaphthalene Not detected ug/L 10 SW846 8260 JH 11/03/2005
Naphthalene Not detected ug/L 10 SW846 8260 JH 11/03/2005
i-Butylbenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005
i-Propylbenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005
Styrene Not detected ug/L 2 SW846 8260 JH 11/03/2005
1,1,1,2-T etrachioroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
[, 1,2,2-T etrachioroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
Tetrachloroethene Not detected ug/L 2 SW846 8260 JH 11/03/2005
Toluene 23 ug/L 2 SW846 8260 JH 11/03/2005
rans-1,2-Dichloroethene Not detected ug/L 2 SW846 8260 JH 11/03/2005
rans-1,3-Dichloropropene Not detected ug/L 2 SW846 8260 JH 11/03/2005
rans-1,4-Dichioro-2-butene Not detected ug/L 2 SW846 8260 JH 11/03/2005
1,2,3-T richlorobenzene Not detected ug/L 10 SW846 8260 JH 11/03/2005
1,2,4-T richlorobenzene Not detected ug/L 10 SW846 8260 JH 11/03/2005
1,1,1 -T richloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
1,1,2-T richloroethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
frichloroethene Not detected ug/L 2 SW846 8260 JH 11/03/2005
Page 3
Brighton Analytical, LX.C. 2105 Pless Drive
Brighton, Michigan 48116 TM Phone: (810)229-7575 FAX: (810) 229-8650
Sample Date: 10/28/2005
Submit Date: 10/28/2005 Report Date: 11/07/2005
To: Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612
BA Report Number 83603 BA Sample ID: BK04767
Project Name: Cousins Waste ControI/XXKEM WV Abandonment Project Number: P0#63602070
Sample ID: Dnpl leachate
Parameters Results Units DL Method Reference Analyst Analysis
Date
frichlorofluoromethane Not detected ug/L 2 SW846 8260 JH 11/03/2005
1,2,3-Trich loropropane Not detected ug/L 2 SW846 8260 JH 11/03/2005
1,2,3-T rimethy Ibenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005
1,2,4-T rimethy Ibenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005
1,3,5-Trimethylbenzene Not detected ug/L 2 SW846 8260 JH 11/03/2005
Vinyl chloride Not detected ug/L 2 SW846 8260 JH 11/03/2005
Xylcnes(total) Not detected ug/L 6 SW846 8260 JH 11/03/2005
[)L=Reported detection limit for analytical method requested. Some compounds Released by: •equire special analytical methods to achieve MDEQ designated target detection imits (TDL). Date:
alevated volatile dl due to sample matrix.
Page 4
Brighton Analytical, L.L.C. 2105 Pless Drive
Brighton, Michigan 48116 TM Phone: (810)229-7575 FAX: (810) 229-8650
Sample Date: 10/28/2005 Submit Date: 10/28/2005
RqaortDate: 11/07/2005
To: Cousins Waste Control Corp.
1701-1801 Matzinger Road
Toledo, OH 43612
BA Report Numben 83603 BA Sample ID: BK04768
Project Name: Cousins Waste Control/XXKEM WV Abandonment Project Number: P0#63602070
Sample ID: Trip Blank
Parameters Results Units DL Method Reference Analyst Analysis
Date
PCB/Pesticide Analysis i-BHC Not detected ug/L 0.01 EPA 608 BY 11/02/2005
j-Chlordane Not detected ug/L 0.02 EPA 608 BY 11/02/2005
Aldrin Not detected ug/L 0.01 EPA 608 BY 11/02/2005
ARO 1016 Not detected Ug/L 0.2 EPA 608 BY 11/02/2005
ARO 1221 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
ARO 1232 Not detected ug/L 0.4 EPA 608 BY 11/02/2005
ARO 1242 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
ARO 1248 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
ARO 1254 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
ARO 1260 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
ARO 1262 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
ARO 1268 Not detected ug/L 0.2 EPA 608 BY 11/02/2005
IvBHC Not detected ug/L 0.01 EPA 608 BY 11/02/2005
3P-6(PBB) Not detected ug/L 0.01 EPA 608 BY 11/02/2005
1-BHC Not detected ug/L 0.01 EPA 608 BY 11/02/2005
M-DDD Not detected ug/L 0.02 EPA 608 BY 11/02/2005
t,4-DDE Not detected ug/L 0.02 EPA 608 BY 11/02/2005
»,4-DDT Not detected ug/L 0.02 EPA 608 BY 11/02/2005
Oieldrin Not detected ug/L 0.02 EPA 608 BY 11/02/2005
Endosulfan 1 Not detected ug/L 0.02 EPA 608 BY 11/02/2005
Bndosulfan 11 Not detected ug/L 0.03 EPA 608 BY 11/02/2005
Bndosulfan sulfate Not detected ug/L 0.05 EPA 608 BY 11/02/2005
Bndrin Not detected ug/L 0.02 EPA 608 BY 11/02/2005
Endrin aldehyde Not detected ug/L 0.02 EPA 608 BY 11/02/2005
Endrin ketone Not detected ug/L 0.02 EPA 608 BY 11/02/2005
;-BHC(Lindane) Not detected ug/L 0.01 EPA 608 BY 11/02/2005
{-Chlordane Not detected ug/L 0.02 EPA 608 BY 11/02/2005
deptachlor Not detected ug/L 0.01 EPA 608 BY 11/02/2005
deptachlor epoxide Not detected ug/L 0.01 EPA 608 BY 11/02/2005
dexabromobenzene Not detected ug/L 0.02 EPA 608 BY 11/02/2005
Page 1
Brighton Analytical, L.L.C. 2105 Pless Drive
Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650
Sample Date; 10/28/2005 Submit Date: 10/28/2005 Report Date: 11/07/2005
To: Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612
BA Report Number 83603 BA Sample ID: BK04768
Project Name: Consins Waste Control/XXKEM WV Abandonment Project Number: P0#63602070
Sample ID: Trip Blank
Parameters Results Units DL Method Reference Analyst Analysis
Date
Vlethoxychlor Not detected ug/L 0.05 EPA 608 BY 11/02/2005
^irex Not detected ug/L 0.02 EPA 608 BY 11/02/2005
Foxaphene Not detected ug/L 0.1 EPA 608 BY 11/02/2005
iHTB/Pesticide liquid (extraction) Extracted 3510/3550 LS 11/01/2005
Semi-Volatile Analysis
Dimethylaniiine Not detected ug/L 10 EPA 625 RG 11/02/2005
3NA liquid (extraction) Extracted 3510/3550 LS 10/31/2005
i^olatile Analysis
\cetone Not detected ug/L 25 SW846 8260 JH 11/03/2005
\crylonitrile Not detected ug/L 1 SW846 8260 JH 11/03/2005
Benzene Not detected ug/L 1 SW846 8260 JH 11/03/2005
Bromochloromethane Not detected ug/L 1 SW846 8260 JH 11/03/2005
3romodichloromethane Not detected ug/L 1 SW846 8260 JH 11/03/2005
Jromoform Not detected ug/L 1 SW846 8260 JH 11/03/2005
3romomethane(Methyl Bromide) Not detected ug/L 1 SW846 8260 JH 11/03/2005
1-Butanone (MEK) Not detected ug/L SW846 8260 JH 11/03/2005
Zlarbon disulfide Not detected ug/L SW846 8260 JH 11/03/2005
Darbon tetrachloride Not detected ug/L 1 SW846 8260 JH 11/03/2005
Dhlorobenzene Not detected ug/L 1 SW846 8260 JH 11/03/2005
"hloroethane Not detected ug/L 1 SW846 8260 JH 11/03/2005
Chloroform Not detected ug/L 1 SW846 8260 JH 11/03/2005
Chloromethane(Methyl Chloride) Not detected ug/L 1 SW846 8260 JH 11/03/2005
:is-1,2-Dichloroethene Not detected ug/L 1 SW846 8260 JH 11/03/2005
:is- 1,3-Dichloropropene Not detected ug/L 1 SW846 8260 JH 11/03/2005
1,2-Dibromo-3-Chloropropane Not detected ug/L 1 SW846 8260 JH 11/03/2005
Dibromochloromethane Not detected ug/L 1 SW846 8260 JH 11/03/2005
1,2-Dibromoethane Not detected ug/L 1 SW846 8260 JH 11/03/2005
Z)ibromomethane(Methylene Bromide) Not detected ug/L 1 SW846 8260 JH 11/03/2005
1,2-Dichlorobenzene Not detected ug/L 1 SW846 8260 JH 11/03/2005
1,3-Dichlorobenzene Not detected ug/L 1 SW846 8260 JH 11/03/2005
Page 2
Brighton Analytical, L.L.C. 2105 Pless Drive
Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650
Sample Date: 10/28/2005 Submit Date: 10/28/2005 Report Date: 11/07/2005
To: Cousins Waste Control Corp. 1701-1801 Matzinger Road Toledo, OH 43612
BA Report Number. 83603 BA Sample ID: BK04768
Project Name: Consins Waste ControI/XXKEM WV Abandonment Project Number: P0#63602070
Parameters Results
Sample ID: Trip Blank
Units DL Method Reference Aruilyst Analysis
Date
1,4-Dichlorobenzene Not detected ug/L 1 SW846 8260 JH 11/03/2005
Dichlorodlfluoromethane Not detected ug/L 1 SW846 8260 JH 11/03/2005
1,1-Dichloroethane Not detected ug/L 1 SW846 8260 JH 11/03/2005
1,2-Dichloroethane Not detected ug/L 1 SW846 8260 JH 11/03/2005
1,1-Dichloroethene Not detected ug/L 1 SW846 8260 JH 11/03/2005
1,2-Dichloropropane Not detected ug/L 1 SW846 8260 JH 11/03/2005
Diethyl ether Not detected ug/L 10 SW846 8260 JH 11/03/2005
Ethyl benzene Not detected ug/L 1 SW846 8260 JH 11/03/2005
Hexachioroethane Not detected ug/L 1 SW846 8260 JH 11/03/2005
2-Hexanone(Methyl Butyl Ketone) Not detected ug/L 5 SW846 8260 JH 11/03/2005
Isopropylbenzene Not detected ug/L 1 SW846 8260 JH 11/03/2005
Methyl iodide(Iodomethane) Not detected ug/L 1 SW846 8260 JH 11/03/2005
Methyl(tert)butyl ether(MTBE) Not detected ug/L 5 SW846 8260 JH 11/03/2005
4-Methyl-2-pentanone(MIBK) Not detected ug/L SW846 8260 JH 11/03/2005
Methylene chloride Not detected ug/L SW846 8260 JH 11/03/2005
2-Methylnaphthalene Not detected ug/L 5 SW846 8260 JH 11/03/2005
Naphthalene Not detected ug/L 5 SW846 8260 JH 11/03/2005
n-Butylbenzene Not detected ug/L 1 SW846 8260 JH 11/03/2005
n-Propylbenzene Not detected ug/L 1 SW846 8260 JH 11/03/2005
Styrene Not detected ug/L 1 SW846 8260 JH 11/03/2005
1,1,1,2-T etrachloroethan e Not detected ug/L 1 SW846 8260 JH 11/03/2005
1,1,2,2-Tetrachloroethane Not detected ug/L 1 SW846 8260 JH 11/03/2005
FeU^hloroethene Not detected ug/L 1 SW846 8260 JH 11/03/2005
Toluene Not detected ug/L 1 SW846 8260 JH 11/03/2005
rans-1,2-Dichloroethene Not detected ug/L 1 SW846 8260 JH 11/03/2005
trans-1,3-Dichloropropene Not detected ug/L 1 SW846 8260 JH 11/03/2005
trans-1,4-Dichloro-2-butene Not detected ug/L 1 SW846 8260 JH 11/03/2005
1,2,3-Trichlorobenzene Not detected ug/L 5 SW846 8260 JH 11/03/2005
1,2,4-T rich lorobenzene Not detected ug/L SW846 8260 JH 11/03/2005
1,1,1 -T richloroethane Not detected ug/L 1 SW846 8260 JH 11/03/2005
1,1,2-T richloroethane Not detected ug/L 1 SW846 8260 JH 11/03/2005
Trichloroethene Not detected ug/L 1 SW846 8260 JH 11/03/2005
Pages
Brighton Analytical, L.L.C. 2105 Pless Drive
Brighton, Michigan 48116 TM Phone: (810) 229-7575 FAX: (810) 229-8650
Sample Date: 10/28/200S Submit Date: 10/28/2005 Report Date: 11/07/2005
To: Cousins Waste Control Corp. 1701 -1801 Matzinger Road Toledo, OH 43612
BA Report Number; 83603 BA Sample ID: BK04768
Project Name: Cousins Waste ControI/XXKEM WV Abandonment Project Number: P0#63602070
Sample ID: Trip Blank
Parameters Results Units DL Method Reference Analyst Analysis
Date
rrichlorofluoromcthane Not detected ug/L 1 SW846 8260 JH 11/03/2005 1,2,3-Trichloropropane Not detected ug/L 1 SW846 8260 JH 11/03/2005 1,2,3-T rimethy Ibenzene Not detected ug/L 1 SW846 8260 JH 11/03/2005 1,2,4-Trimethylbenzene Not detected ug/L 1 SW846 8260 JH 11/03/2005 1,3,5-T rimethy Ibenzene Not detected ug/L 1 SW846 8260 JH 11/03/2005 ^inyl chloride Not detected ug/L 1 SW846 8260 JH 11/03/2005 Xylcnes(total) Not detected ug/L 3 SW846 8260 JH 11/03/2005
DL=Reported detection limit for analytical method requested. Some compounds Released by: 'equire special analytical methods to achieve MDEQ designated target detection imits (TDL). Date:
Page 4
-u . : I
Brighton Analytical, L.L.C. | 2105 Pless Drive
Brighton, Michigan 48116 I jM Phone: (810) 229-7575 FAX: (810) 229-8650 |
To: Cousins Waste Control Corp. Sample Date: 10/28/2005 1701-1801 Matzinger Road Submit Date: 10/28/2005 Toledo, OH 43612 Report Date: 11/07/2005
BA Report Numben 83603 Project Name: Cousins Waste ControI/XXKEM WV Abandonment BA Sample ID: BK04768 Project Number: P0#63602070
Sample ID: Trip Blank
Analysis Parameters Results Units DL Method Reference Analyst D^te
Page 5