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POOR LEGIBILITY
ONE OR MORE PAGES IN THIS DOCUMENT ARE DIFFICULT TO READDUE TO THE QUALITY OF THE ORIGINAL
NEL LABORATORIESReno • Las VegasPhoenix • Boise
Derek ReeveDumpco/Silverstate7900 Vegas Valley DriveLas Vegas, NV 89112
TEL: 702-431-3020
RE Project GH-3F-2631
Dear Derek Reeve:
2027897Las Vegas Division
4208 Arcata Way, Suite A • Las Vegas, Nevada 89030702-657-1010 • Fax: 702-657-1577
RECEIVED'02 MAR 18 P« 1=30
Order No.. L0203115
NEL Laboratories, Las Vegas received 1 sample on 3/11/02 for the analyses presented in thefollowing report.
There were no problems with the analyses and all data for associated QC met EPA or laboratoryspecifications except where noted in the Case Narrative.
If you have any questions regarding these tests results, please feel free to call.
Stan Van WagenenLaboratory Manager
Certifications:ArizonaCaliforniaIdahoMontanaNevadaNew MexicoUS Army Corps of Engineers
RenoAZ05201707CertifiedCertifiedNV033Certified
Las VegasAZ05182002CertifiedCertifiedNV052CertifiedCertified
Date
P: ,r' 7
NEL LABORATORIES
rl FFN'T- Dnmpro/Silversrare
PROJECT ID: GH-3F-2631
"RO.TF.rT#: GH-3F-26?'
MATRIX: AQUBOUS
Parameter
\t Hnnt-
hrn/rne
Bromobenzene
Bromochloromclhane•lioim.1i hloforrv-Ih jn j -
Bromoform
Bromomethane
2 B.jijnuucn-Butylbenzene
sec-Butylben/ene
icd-Bul>lbcn?i;nc
Cjrbon disulfide
Carbon telrachloridc
Chlorobenzenc
Chloroc thane
2-Chloroeihyl vinyl ether
ChUirofwm
i 'hloromethanc
-'-Chlorololuene: • not • ' iM.t '
Dibromuchloromethanc
1 ,2-Dibromo-3-chloropropane1 7-Dibrornnclhane
Hihrornnnie thane
1 ,2-Dichlorobenzenc
1 ,3-nichloroben?enc1 ,4-Dichlorobenzene
Dichlorodifluoromethanc
1,1-Dichloroethane1,2 Oichloroethanc
l,l-Dichloroethen*e
v.is-1 ,2-Dn.hlnruclhenc
\rans-l ,2-Dichloroethene
1 ,2-Dichloropropane
1 ,3-Dichloropropane
T,J UiclikiMiprupjm.1 .1 -Dichloropropcnc
-. "M 1 Dichlornprupcnt:
irans-1 ,3-DichlorupropcneEthylbenzene
Hcxachlorobutadienc.. HcxjnuriL
lodomethane
Isopropvlhenzcne
Result Unit32 up/L
NO pg,L
ND ug/L
ND ug/L
N".i ue'L
ND ug^.
ND ug/L
ND gg.1
ND- ug/L
ND ng/L
ND i,6a.ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND Hg/L
ND Hg/L
ND MSI :ND ug/L
ND ug/L
ND MlVL
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/l.ND ug/L
ND ug/L
ND ug/L
ND jig/LND pg/L
ND ug/l-ND UK/L
ND ugn.
ND ug'L
ND (jg/L
ND US/L
ND fig/L
N!1 pg'L
ND ug/L
ND ug/L
ReportingLimit
25~j ',5.0
5.05050
5.0
2 S
5.05.050
5.0
5.0
50
5.0
5.050
5.0
5.0S A
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
50
5.0
5.0
5.05.05.0.
50
5.0
505.0
5.05.025
5.0
5.0
CLIENT ID: GH-3F-263'
DATE SAMPLED: 3 il "2
NEL SAMPLE ID: L0203115-001A
DF1i11111i1111II11111i1I1i11111I11111i11I11111
MethodSW8260B
b\V«3fiOR
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8760B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SWS760B
SW82608
SW8260BSW8260B
SW8200B
SW8260B
SW8260B
SW8260B
SW8260BSW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260BSW8260B
SW8260B
SVY8260B
SW8260BSW8260B
SW82COB
SW8260B
SW8360BSW8260B
SW8260B
Prep Date Analjzed03/11/02
OV11'0203/11/02
03/1 1/02
03/11/02
03/11/02
03/11/02
OH/ 11/02
03/11/02
03/11/0203/11/02
03/1 1/02
03/11/02
03/11/02
03/11/0203/11/02
03/1 1/02
03/1 1/02
03/11/02
03/11/02
03/11/0203/1 1/02
03/1 1/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02ovi i/n?03/11/02
03/11/02
03/11/02
03/1 1/02
03/11/0203/1 1/02
03/1 1/02
03/11/0203/1 1/02
03/1 1/02
03/11/02
03/1 1/02
03/11/02
03/1 1/02
Analyst
DRM-LV
DRM L\'DRM-LV
DRM-LVDRM-LV
DKM-LVDRM-LV
DRM-I V
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LVDRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LVDKM-LV
DRM-LV
DRM-LV
DRM-I VDRM-LV
DRM-LV
UKM-LV
DRM-LV
DRM-LV
DRM-I V
DRM-LV
DRM-LV
DRM-I V
DRM-LV
DRM-LVDRM-LV
DRM-LV
DRM-LV
DRM I VDRM-LV
DRM-LV
DRM-LV
DRM-LS'
DRM-LV
ND - Not Delected at the Reporting Limit
DF - Dilution Factor
Pate: ll-Wnr-M
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
F - Value above quantilalion range Page 1 of 5
, NEL LABORATORIES
H I M r-'.n.p . '?•:•.
PROJFCTID: GH-3F-263'
3'RorFrrs: cu IF.WMATRIX: AQUEOUS
ParameterK,r rvl.aM,en '
Mclhylene chloride4-Methyl-2-pemanonc
M TRF.
.Vaph'halcnc
•i-Propylbenzenc
<>,r~...
1 ,1 ,1 ,2-Tetrachloroethane
1 , 1 ,2,2-Tetrachloroetnane
I'eirachlorocthene1 o'ucni.
! ,2.J-Tnchlorobenzcne
' "J 4 Tr'rh'nrobrnvenr
1 1,1-Tnchloroethanc
1 ,1 ,2-Trichloroethanc
T richloroethcric
! , 1 .2-Tri(-hlororrif!uorocthane
I 2 3-Tnchloropropane
1 .2,4- 1 nmelhylbenzene
1 ,3.5-Trimethylbenzcnc
Vinyl acetate
\ i n v t h 'in It
o-Xylenc
m.p-Xvlcnc
Surr: Dibramuftuoromtthant:
Surr: Tolucne-d8
Surr: 4-Brnmofluorohenzene
rUFNTTD:
DATE SAMPLED:
NEL SAMPLE ID:
Result
N-n19
ND
NDNU
NDNDNDNDNDNDNDNDNDNDND
ND
NDNDND
NDNO
NDND9t>.6
93.7
78.4
Unit
, J ?-L
Ug/L
ue/t-up/L
f ig- l -
Ug/LI'g'L
Ug/L
ug/1-
ug/i-MS'"
Ug/L
UZ/I-
ug/L
MS/L
Ug/L
Mg/L
Ug/L
UB/Lug/L
J»g/L
U £ ^
M-S^L
Ug/L
%REC
%REC
%REC
ReportingLimit
50
50
25
50
50
5.0
5 0
5.0
5.05.0
5 05.0S.O5.05.05.0
s n5.05.05.05.05.0t o5.010
89-102
90-102
70-106
DFiili1
i1i1iiiIi11ii1i11ii1ii1
Method
SW8260B
SW8260B
SW82GOB
SW8260B
SWK26'>n
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SWR260R
SW8260B
SW8260B
SWX260B
SW8260B
SW8260B
SWS2fiOR
SW8260B
SW8260B
SW826UB
SW8260B
SW8260B
SW8260B
SW826UB
SW8260B
SW8260B
SW8260B
SW8260B
3/11/02
L0203115-001A
Prep Date Analyzed
03/11/02
03/11/02
03/11/02
03/11/02
nvn/n?03/11/02
03/1 1/02
OJ/ 11/02
03/1 1/02
03/1 1/02
03/1 1/02
03/1 1/02
03/1 1/02
OJ/ 11/02
03/1 1/02
03/11/02
03/1 I/O?
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
nvn/0203/11/02
03/1 1/02
ovn/0303/11/02
03/1 1/02
Analyst
DRM-LV
DRM-LV
DRM-LV
DRM-LV
HRM-I V
DRM-LV
DRM-LV
URM-; \DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
PRM I \
DRM-LV
DRM-LV
DRM-I V
DRM-LV
DRM-LV
DRM-I V
DRM-LV
DRM-LV
DRM-LV
URM-LV
DRM-LV
DRM-I.V
DRM-LV
DRM-LV
ND - Not Detected at the Reporting Limit
DF - Dilution Factor
Date: 13-Mur-02
B - Analytc detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
£ - Value above quuniiunon range Page 2 of S
NEL LABORATORY
i : r . \ l . IJui::p,.u ^hCtdl j Ic
I'KO.IKCTID: GH-3F-26"'
-•KOJi ( T . J . oii ;!-:<>?•
MATRIX: AQUEOUS
i'.irameter
i t . mi -n
Calcium
Iron
Mij l inps ium
i'lHassiutn
Sodium
^ .t iudium
Antimony
Arsenic
Hr r v l l i u m
Cadmium
C'lirnmium
I l > U . l l l
Copper
Indium
I l'3<1
Mrkt-1
Selenium
SiUtr
Thallium
Zinc
Meicurv
Result
2(1
noo200
640
110
11)00
u :&0.0028
0.23
nno7guimn0.13
n of,o0.20
ND
0.081
0.33
ND
ono?i0.0063
0.85
ND
Unit
,.«•!
mii/J.
niR/L
mp/l.
"'ft/Imc/L
nig I
171 g/L
mg/L
me/L
iHR/1
mg/L
m!('l
mg/L
mg/LrnB/1-
mg/L
mg/L
nig/'
mg/L
mg/L
mg/L
ReportingLimit
OC2 '
?.5
0.50
2 510
2.5
<M>2S
00010
0.00100.0010
U.UOIO
oooion o n i o000100.001000010
O O O I O
O O O I O
OOOIO
000040
0.00100.00020
CLIENT m-
DATE SAMPLED:
NTI.S\M1'1E ID-
DP5
5
5
5
5
5s1I!
1
1
1
1
1
1
1
1
1
1
1
I
Method
WfiOlQB-To
SW6010B-TO
SW6010B-TO
SW60!OB-To
SW f.OKin 'Io
SW60IOB-To
SW6010B-To
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SV. 6020- Fc'U
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-TotaSW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 7470-Tola
CH-^F-263'
: vn/oi1 020^1 15-001B
PrepJDate
!' VI 2/02
03/12/02
03/12/02
03/12/02
i l « I2'02
03« 2/02
01 / 17/02
03/12/02
03/12/02
03/12/02
OVI2 '02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/13/02
Analyzed
OV12/02
03/12/02
03/12/02
03/12/02
OJ/ 17/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
ni'p'0203/12/02
03/12/02
03/12J02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/13/02
Analyst
JTY-Rcno
JlY-Reno
JTY-Rcno
JTY-Reno
JTY-Rcno
JTY-Reno
JTY-Reno
DHG-Renu
DHG-RenoDHG-RcnoDHG-Rcpo
DHG-KcnoDHG-Reno
UHO-R(.i,o
DHG-RcnoDHG-Reno
DHO-RcnoDHG-Rcno
DHG-Reno
DHO-Rrno
DHG-Reno
FIF-Reno
ND - Not Delected al the Reporting Limit
DF - Dilution Factor
Date: 13-Mar-02
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
b - Value above quannutiun range Page 3 of 5
'I'-
NEL LABORATORIES
( N K N l - l > i mpeo/S:h estate
PROJECTED- GH-3r-2(>:'I 'KOIKM H ti!l-*r--?r,- '
Mvrwix: \ourow
I'aramcterB-inum
CaUiuni
Im.i
M.nJufMUin
Poia*;*;hiin
Smhuin
Vji iddium
Anlimonv
Arsenic
H -.I ' l l T
i"«lmuim
^hromuirn
( !'(>., II
Copper
Lead
N ^ U l l
-Menium
Silver
'u hum
Zinc
Mercury
Result
onzy57»
ND1H0
509X0
ND0.0014
00020
N't>
ND
ND0.0012
0.0037
ND00019
00083
NDND
0.051
ND
Unit
me/Lmg/L
mg/I
•ii;> 1
mfi/I-nig/!.
mg/L
mg/L
mg/l
Ml 1
mg/L
mg/L
mg/L
nigA,
mg/L
inj» 1
mg/L
mg/L
mg/X
mg/L
mg/L
ReportingLimit
000502 5
0 10
2 510
2 SOOOSO0.0010
O O O I Oo 00 ' ( 1
O O O I O
0.001(1
000)0
0.0010
OOOIOC 0 0 1 0O O O I OO O O I O
U OUQ40
0.0010
0 00020
CLIENT ID: GH-3F-263'
DATE SAMPLED: 3/11 /07
NEL SAMPLE ID: L0203 1 1 5-001 C
DF Method Prep Date
1 SW6010B-Di
5 SW6010B-DI
i SW6010B-Die - w onion ui5 SW601QB-DI
5 S W 6 0 I O B D .
1 SWGOIOH-Di
1 SW 6020-Diss
1 SW 6020-DKs
1 S'A 6020-').^'.
1 SW 6020-Diss
1 SW 6020-Diss
1 SW 6020-Diss
1 SW 6020-Diss
1 SW 6020-Diss
1 SW OWO-Di^S
1 SW 6020-Diss
1 SW 6020-Diss
1 SW 6020-Diss
1 SW 6020-Diss
1 SW7470-Diss 03/13/02
Analyzed
03/12/02
03/12/02
03/12/02
03' 12/02
03/12/02
03/1 2'Q2
03/12/02
03/12/02
03/12/02
i t J / 1 2 / t J
03/12/02
0^/17/02
03/12/02
03/12/02
03/12/02
Ul/ 12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/13/02
Analyst
JTY-Rcno
.JTY-Reno
JTY-Rcnu
JTY Reno
JTY-Reno
)TY-Rcnn
JTY-Reno
DHG-Reno
DHG-Rcno
Uhlj-Renu
DHG-Reno
DHO-Rrnn
DHG-Reno
DHG-Reno
DHG-Renn
DHG-Rcno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
FIF-Reno
ND - Not Detected at the Reporting Limit
Of- - Dilution l-aunr
Date: I3-Mar-02
B - Analyte delected in the associated Method Blank
S - Spike Recovery outside accepted recovery lirruti
E - Value above quan illation range Page 4 of 5
. NOL LABORATORIES
'RO.TF< 1 ID: OH "1 ?6V
: OH-3F-26.V
DATE SAMPLED: 3-11702
NK1, SANfVLF, ID: T.0703115-00) D
•M XTHIX: AQUEOUS
Parameter
fhlori,!.-
^iT'i'r, a'. N
N-it V ,; V
. t •:.-.•Mki ' in i ty . Bicarhfin»tc (As CaCfW
\i^j l -n i !v . Carhonaic (A? l"3CCH)
1 lydroxidc (As CnC03)
Alkalinity, Total (As CnCO3)
fhf in ica l Oxygen Demand
^"mon.i a..v
';..!f,dc
1 olal Dissolved Solids
Result
noni.T.
ND
260U
f,«0
Nl)
ND
680
64
ND
ND
6130
Unit
•"K'Lrr,»'l.
nsj'L
mr/l.m?.1'mg/L
mg/i.
mi-A,
mc/l.
mjc'Lmg/L
mg/I
KeportingLimit
iO
2.52 5
Ml
250
250
750
250
10
0 30
0.030
«).0
DF
500
2S
25
500
H)
10
10
10
I1
14
Method Prep Date
EPA 300 0
EPA 300 0
f PA 300.0
B'A 300 ';
SM2320 B
SM2320B
SM7370B
SM2320 B
SM5520 D
SNW500-NH3
SM4500-S D
SM2540C
Analyzed
03/11/02
03/1 1/02
03/1 1/02
OV11/D2
03/11/02
01/1 I/O?
03/11/02
03/11/02
03/12/02
0V 12/02
03/12/02
03/11/02
Analyst
PJJ-LV
PJJ-LVPJJ-LV
P J I - l V
RDA-LV
KDA-l.VRDA-LV
RDA-LV
RDA-LV
RDA-l V
RWW-LV
PJI-LV
ND - Not Detected at the Reporting Limit
HF - Dilution Factor
Date: 13-Mar-02
B - Analyte detected in the associated Method Blank
S • Spike Recovery uubide accepted recovery limits
E - Value above quantiution range Page 5 of 5
NEL Laboratories, Las Vegas
CLIENT: Dumpco Silvcrstate\VorkOrder: 1.0203115Project: C.H-3F- '63'
ANALYTICAL QC S U> IM A IT> R K1 i ' JRT
TcstCcdc: 303 ',Vi IT:
Sample ID MB-R884
Client ID- ZZZZZ
Analyte
Chloride
Nitrate, as N
Nitrite, as N
.Sulfate
Samplypc: NiHLK
Batch ID. HS84
Result
ND
ND
ND
ND
TeitCode 300 W Units: me/1. PTCTJ Date "u" ID i. '.''-I f ^C ' ! ' . "i CJ r 'O '7
TenNo E300 Analy< i Oat: 3/11/02 'M.N.. 5" '6 '33 -ni*~ |"
PQL SPK value yp< RefVal 4 R J - C LowLmit ' . i^hLimil ?:P:') Rs-' Va i /Kl ' ! ' IM'HI. - "JLJ| ^ 7{ *!*->
010 d9
o.io J7,1 Z^o.io H!010 r
Qualifiers: ND - Noi '^elected at III? Reporting Limit
Anal>'e delected h t lnw quarinot ion lirnils
S Spike Kecovcry uuuide accepted recovery ! mils
R RPD ouLsidc accepted rccovei, limits
8 \na t \ l e detected if '-,,• j,:e •'••><td Mot ' i ' i
CLIENT:
Work Order:Project:
Dumpco/Silverstale
1,0203115GH-3F-2631
ANALYTICAL QC SUMMARY REPORT
TestCode: 6010\V D
Sample ID. MB-R659
Client ID ZZZZZ
Analyte
Samp Type: MBI.K
B a U h l D : R_R659
Result
TestCode. 6010W_D Units me/1
TestNo. SW6010B
PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 3(12/02
%REC LowLimit Highl mil RPD Ref Val
Run ID SUB-659
SeqN > 6434
° RPD RPDLtmit Qual
m
DOOID
5OIDmCO
Barium
Calcium
Iron
Magnesium
Potassium
Sodium
Vanadium
ND
ND
ND
ND
ND
ND
ND
00050
0.50
O.IO
0.50
2.0
0.50
00050
Qualifiers: »D - Not Delected ai >he Reportina Limit
) - Analyte nclectcd b low quantiunon limit-.
S • Spike Recovery oul^ide accepted recovery limits
R - RPD outside accep'cd recovery I mils
B • Analyte detected in r o associated Method Blank
Page 2 of 14
CLIENT:Work Order:
Project:
Dumpco/Silversiate
L0203115(.H-3F-2631
ANALYTICAL QC SUMMARY REPORT
TesiCode: 6010VV t
Sample ID. MB-3SI
Client ID: 7.ZZZZ
Analyte
Samplype- MBLK
Batch ID: R_351
Result
TestCode 6010W_t Units. mg/L
TestNo SW6G10B
PQL SPK. value SPK Ref Val
Prep Date. 3/12/02
Analyse Date: 3/12/02
%REC LowLnnil HighLimit RPD RefVal
Run IU SUB-660
SrqNn 6438
%RPD RPni.imit Oual
m
ccO13
O
1 3,m
Barium
Calcium
Iron
Magnesium
Potassium
Sodium
Vanadium
ND
ND
ND
ND
ND
ND
ND
Qualifiers:
0.0050
0.50
010
0.50
2.0
0.50
0.0050
VD - Not Detected at the Reporting Limit
- Analyle delected below quantiui on limits
S • Spike Recovery outside accepted iccovery limits
R - RPD outside acceptc 1 recovery limits
B Analyte delected in tlir associated Method Ulank
Page 3 of 14
CLIENT: Dumpco/Siherstate
Work Order: L( 203 11 5
Project: GH-3F-2631
Sample ID: MB-R661 SampT pe:
Client ID: Z.ZZZZ Batch ID
Analyte
AntimonyArsenic
Beryllium
CadmiumChromiumCobaltCopperLead
NickelSelenium
Silverthallium
2mc
MBLK
R R66I
Result
NDNDNDNDNDND
ND
ND
ND
ND
ND
ND
ND
ANALYTIC AL QC SUMMARY REPORT
Test( ode: 6020\V_1)
TestCode 6Q20WJ) Unit* mg/L Prep Date: Run :i) SUB-SSI
TestNo. SW6020 Analyst' Date: 3/12,02 ScqNo 6445
PQL SPKvaliiL- SPK. Ref Val %REC LowLir l HighLitr.it RP! Ref Val 7,,X"D .W.V.. m.il Ou.il
J0010
0.0010
O O O I O
0.0010
0.0010
0.0010
0.0010
0.00100.00100.0010O O O I O
'.00040
0.0010
mr~r~•>CDOD">— 1ODm09
Qualifiers: ND - Not Detcaed at t h j Reporting Limit
I Analylede' jctedbcl w quantitai,on limits
S • Spike Recovery outside accepted iccovery l i tits
R RPD outsidf acceplen recovery limits
8 • \nalyte dctctied in ttv is>uciali.-d Mclliod Itbnk
Page •' •>! 14
CLIENT: Du npco/Silvt-rstate
Work Order: LOJ03115Project: GH-3F-263'
Sanple ID: MB-350 SampTy ie.
Cli.-nllD: ZZZZZ Batch i j
Anjlyte
An:imony
Aricnic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Thallium
Zinc
MBLK
R_350
Result
NDNDND
NDNDNDNDNDNDNDND
ND
ND
ANALYTIC \L QC SUMMARY JREFORT
FextCode: (,C-20W_T
TestCode 6020\V_T Units mg/L Prep )ate. 3/II/H2 l-'un ID S1'0-«5S
TestNo: SW6020 Nr.alysis )ale: 3/12,112 ^^qN'i- 64:<<
i'QL SPKvilue SPK Ref Val %R£C . / iwLim' HighLtm • RPD Ket Val %!< '0 -'.'.'Ol mt v - j l
/0010
zmr-f—03Osn
i' 0010 , 30
oOOio ! friO O O I O , ^°
000 10
u O O l O
' 0010
oooio.'lOOIO
-> 0010s iOOlO
0.0010
a.ooio
Qualifiers: ND • Not Detened at thi Reporting L.mil
J Analyte delnted belo v quanlttatitMi limits
S • Spike Recovc'y outside accepted re,every lii'.ifs
R - RPD outside icceptrd recovery limi'-s
B • Analyte dc'.ct'ci! ia l jcia'.os M-thr <i 'i j
CLIENT: Dun.pco/Silvci stateWoik Order: L02I3115Project: GH-'F-263'
Sample ID: MB R893 ''arnpTyp.
Client ID: ZZ?,ZZ Batch 11
Analytc
Acetnne
Bcnrcnc
Bromobenzcne
Bromochloro methaneBromodichloromcthane
Bromoform
Bromome thane
2-Butanone
n-Burylbenzenc
sec-Butylbenzenc
tcrt-Butylbenzcnc
Carbon disullide
Carbon tctrachlonde
Chliirobenzene
Chloroethane
2-Chloroethyl vinyl ether
ChloroformCriloromethane
2-Chlorotolucne
4-Chlorololucnc
Dibromochloromethane
1 .2 • Dibromo-3 -chloropropane
1,2 Dibromoelriane
Dihromomethanc
1,2 Dichlorobenzenc
1,3 Dichlorobcnzene
1,4 Dichlorobcnjene
Du hlorodifluorrmcthanc
1,1-Dichloroethane1,2 Dichloroethane
1,1 Dichlorocthene
MBLK
X893
Result
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
NDNDNDNDNDNDNDNDND
ANALYTICAL QC SUMMARY MTfPOKT
TcslCodc: i:f>()_W
eslCode: 8260_W Units. ug/L PrepU.le '• n, '!) t vo*MS-I 020." HI
TestNo: SW8260B A-.alysis Pile 3/11-02 S»oN.- 0048
i'QL SPK. value SPKRcfVjl %REC LowLimil l i ighLimit R.PD ^cf Val ' J'") 1,. I i i . i n . • Cujl
25505.05.05.05050255.05050505.050
5.05.0505.0505.0
5.05.0
5.0505.05.05.05.05.05.05.0
Qualifiers: ND Not Deleck.l at the H -porting Limit
J /5 nalyte dclci.! .-d beluv, juanl i ta t ion ' imi ts
S - S|> ke Recovers outside incepted reco\ery l imns
R • RPD outside a< tcpted r. iovcry limits
B - Ai .n l j t e detCi-Ioil ir Id ,>•»'<!' ,u\,j Vet i >J O.-II
CLIENT: Dumr<_rySi!veisuteWork Order: L020^i5Project: GH-M-263 '
Sample ID MB-R893 SompType
Client ID ZZZ7Z Ja t 'h ID
Analyte
cisO,? Dichloroethene
trans 1 ,2-Dichlorof thene
1 ,2-Dichloropropane
1 ,3-Dichloropropane
2,2-Dichloropropane
1,1 Dichloropropenc
cis-1 ,3-DichIoropropene
trans- 1,3-Dichloropropcne
Ethylbcnzene
Hexachlorobutadicne
2-Hexanone
lodomc thane
Isopropylbenzenc
p-lsopropyltoluenc
Methylene chloride
4-Mcthyl-2-pentanone
MTBE
Naphthalene
n-Propylbenzene
Styrcne
1,1,1 2-Tetrachloroethane
1 ,1 ,2 ,2-Tetrachloroethane
Tetrachloroethcne
Toluene
1,2,3 Tnchlorobenzene
1 ,2 ,4 -Tnchlorobenzene
1,1,1-Tnchloroethane
1,1,2-lnchlorocthane
Tnchloroethenc
Tnthlarofluoro me thane
1 ,1 .T-TnchlorotTifluoroelhane
MBLK
R893
Result
ND
ND
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
Qualifiers: ND Not Detected at the Renortmg Limn
J - Analyte detcckd below q tantilation li nils
ANALYTICAL Qt SUMM -* KY 1 1 '; POP i ,
TessCorfe: S260 W
1 >(Code 8260_\V Units, u -/I Piep Dit Hun .0 I _S O,,\'-? :_ i2f -1 ' A
festNo. SWK260B \mlys isDa ' 3/U/02 i^Nu / (Ms
"'QL SPK^alue SPKRefVal ',,AEC Lr- vLimit H ghLirin , tPr^,\al R. ") L ' 1 ,i- -,-_-u_ -— -- , .1. MI -r— _ _ _ —ii n __ -.--mi TJ [ - -.vn.i_i.- Li.r-j.murr-.. I-. -..-..!._-- -j rri-L., ._-. ---m_-. -",— it
NEL LABORATOR
•50 m5.0
505050
505050255050
5050255010
5050
50
505050
5050505050
5050
S - Spike Recovery utside t^ epted reco\ try limits B - An ji ,tt . delected i '*ie „ .. j' <*•> 1 M n
R - RP ) outside jit p i e d r * % cry limits ' > ., ~ r , i
_0
< i- N t Du.npcu ^ iht 'Matc
Pr [oct GK-1F-2f."
i -1: 1 > ••:4-K8 Simp Type MBLK TesiCode
f t I t ' H1.7L RMoh ID KS9T TestNo
*• . u R.sult PQL
1 2 " Tn h ' r op-r . ND 5 0
! :,- i n .c" iMi i t - ND 50
1 3 ' fnn i 1 i v ND 50
Vir, -c. 'H ND 50
Vn (.tin- ND 50
o-v cv ND 50n r % > ; r " ND 10
S ' " I ) 1 nfU"- -dun 4928 5 0
S IT ' . d< 45 64 50c i - i -'Vjf en j842 50
t l i f t i ' t . N j - N o t **'< < t\ t l I* i'*.p( r a(* Lirn
' AnVy ' i . ' c ' t i l Scv qunr ' ' ' I " , , ' H T I '
ANALY TLCAL QC SUMMARY REPORT
lestCode. 8260_W
8260_\V Units Mg/L Prep Date Run ID L_VOAMS-2_020311B
SW8260B AialysisDale 3/11/02 ScqNo: 6048
SP1- value S}'< R,ef Va1 %REC Li wLimit HighLimil R J ' D R e f X j l %RPD RPDLimn Qua!
50 0 98 6 89 102 0 0
50 0 91 3 90 102 0 0
50 0 768 70 106 0 0
S -Spike 1 -unery fMiside accep ' recav n- limits B - Analjte u^tected i the associau d Method Blank
R- Rl'D ov 3 Jc acc-ptsd recovc I nuli Paei'8ofl4
NEL LABORATOR
men
CLIENT: Dun.p o'SiKciitateWork Order: L020M15Project: GH-31-263'
AJs'Al/i TIC \L QC SCVMAK^ PX; OUT
TcstCodc:
SampU ID MB-R898
Client !D ZZZZ7.
Analyte
Alkalinity, Bicarbonate (A< ' )CO3)
Alkalinity, Carborutc (As Ot'CH)
Hydroxide (As CaCO3)
Alkalinity, Total (As CaC03)
Sarnpl\pe MBLK
Sat.h ID R898
Result
ND
ND
ND
ND
ic 'Code ALK_W Jmts T../L C ' cpD: " 1 > %ri"V \ ' 2 ' > > ! M
T :btNo MI3:0 B V i a l v ^ s J s ' 3, 1J 02 ^ . u N i
?QL S P K x a l u e -PK Ref Val jREC Lo\s!n t ,,SnL -ni' RJ'D - ' \ it jc,i ) 1 ' '
•>5
25
75
25
Qualifiers: ND - Not Dctccied at the Reporting Limit
J - Anjlyle de ecu d hclois q janlilation limits
S - Spike Recover) o-.tstde ai epled recovtry limits
R - Ri D outsue a u i id av >.ery limits
die
CLIENT:Work Order:Project:
Dumpto/Siherbtuc
L020V, 15
GH-21 263'
ANALYTICAL QC SUMM
' .e COD
Sample ID MB-R900
Client II) ZZZZ/
Analyte
SaripType MBLK
A tch ID .-OOO
Result
T(.«.{_id« COD
Irs lNo Mf iZ IOC
PQ' SPK. \ iluc
Units n r !
t - P K R e f V a l
i f tp Di'c
•\ra! i s D a t VI : n
RLC L o v Limit ni j ihl i ' - 1
•>„,.
3 (, -'o
l'i"* c > •)! If
Chemical Oxygen Demand ND 1 )
Zrni""r~en*->
m
QualiTieri: ND - Noi Detected at ihe Reporting Limn
J Anal> le delected bi low quj .Illation limiu
S Spike Recover)'
f RPD uuideacc ' () iJ '
out ide accoted recovery limits B Am!)'" dt. ected 'n ') e ass
N limits
bnk
CLIENT:
Work Order:
Project:
Dumpco/Silverslaie
L 0 2 0 3 I I 5
GH-3F-263'
ANALYTICALQCSU
TcstCcde: I
.\l:\ RLi'ORT
Sample ID MB-359
Client ID- ZZZZZ
Analytt
SanpTypc MBLK
Ba ch ID. K_3S9
Result
TesiOide: HG_"'470_T Units: mg/L
li-stNo: SW7470
PQL SPKvj fue SPK Ref Val
! icp Date 3/13/02 \ur, !D •,<".* 669
\ n a K s i s D a t f .V13/02 ..^No '.45(1
"/.SEC Lov,limit ri'ghLimit R P D - ' : f \ 3 l %RI J) O J
Mercury ND 0 00020
O
IV.'
Qualincrs: ND - Nut Detected at ihe Reporting Limit
J • Analyte delected bi low quan'iiation limiii
S - Spike Recovery outside accepted recovery limits
R - RPD .jutside accepied recovery limits
B • ".nalytc Detected in the associated Me'.nyi L<l,.nk
Page U o! .'-'
('LIENT: Dumpcu/StlverstatcWork Order: L0203115
ANALYTICAL QC SUMMARY Rf.iMRT
Project:
Sample ID
Client ID
Analyle
GH-3P-2631
MB-R901 Simp Type: MQLK
ZZZZZ BakhlD: K901
Hesult
TesU ode
Tc;.:No
PQL
NH3-N_W Ur.its: mg/!.
M4500-NH3C
SPK value .SPK Ref Val
Prop Dats
\nal \5 is Date
VR&C Lov.Lirr.it !
TcslCodc: NTH3-N_\V
'.•'.-..n r.i :._.'.! _O:J" :H
3/;2,'flZ ":,:Nf •;",.>•
igM.imit R ' ' D R - j f \ j | v iRl ' l ' !••['!.;.••' 0 u.
ffir~
o1 -71
l >
^mmonla, as N ND 0.30 IO
i rr.
Qualifien: ND - Not Detected at the Reporting Limit
i - Anahte delected below quantitation limits
S • Spike Recovery ouside accepted recover, limits
R - RPD outside accep'ed recovery limits
B - Anahl'- detected in '.ho assniuin) M-ahoil II ,-II'K !
.. , .> y . j"iJg«f / . "/ . • j
CLIENT: Dumpco/Siherstate
Work Order: L0203115Project: GH-3F-26V
Sample ID MH-R879
Client ID ZZZZZ
Analyte
SampTypi. MBLK lestCodi
Batch ID R879 Tes'N
Result PQL
ANAI Y PC AX OC Sl'WARv '• Fx>
TcsiCoJc. Sl'I "_nA
SULF_W 'jmts mg/L Prep 'ijte K r 0 1 s f :_(t
vldSDO-S D \njly»is Date 11212 " i S',60
SPKvalue S P K h i - f V a l V 1LC LowLirn i Hi^i ii.nt s^D ^c Mi M'U t ' M
\T
Sulfidc ND 0030
m- r~
D3O
O'5moo
Qualifiers ND • Not Delected at the Reporting Limit
J • Analyte detected belou quantisation limits
S - Spike Recovery outside accepted r-covery limits
R- RPD outside accepted recover) .nits
B - A r d l j t e dck.tcd in the a<>nr ja t» i Method J'j ^
t 2C . 1 ',<
CLIENT:Work Order:Project:
Dumpco/Siheistate
L0203115GPMF-26.V
ANALYTICAL QC SI MMAUY
: IDS V»'
Total DissoUcd Solids
Tl
Sample ID:
Client ID:
Analyte
MB-R307
/ZZZZ
SampTypc
Batch ID
MBLK
K907
Result
lestCodc
TestNo
PQL
TDS_W
E160.I
SPK. value
•JM
SPK Ft
• v mg/L
T Val %
Prep
Analys i s
R.EC LOV.LI.T
DJ'C K u r . i. V\.' _ ':o.l!!D
Dj'.c 3 /11 01 S-u >'„ s t ' ^ 0
, Hi^nit AO^fV.i ,-|) - ,U. . - ,,-.
ND
Qualifiers: ND • Not Di'ccled at the ^eportir,g .imit
J - Analyte detected belov. quantila'.on limits
S - Spike Recovery outside accepted iccovery limits
R - R?D outside accepted recover)' 'iruls
0 - AinlyU dc'i-lcd ir. ,! c •>MII.I.-' <* V.cihoJ .'mi A
"O A N A L Y T i C A LL A B O R A T O R I E S
Vanessa PadiiU> r.HM'.J.v,;, < ! :,
4208 AicaUt Way, Ste A
Certificate of AnalysisT'.LAV CertiDcare
05
USK Submission #• 2002030SKI
BSK Sample lOf^: \,l >'{<»>}
Submi.<3icn Connnrnb
Sarrvl-Tvp LiquidS-tniplt rviCiiptioir G i r.lF-Sample Comnient>
llojectDesc: Dumpco
Date Sampled- 03/11/2002
Time Sampled; 0851Date Received- 03/12/7002
Inorganics
AnaMe Method Result Units PQL DiluUoa DLRPrep AnalyiisDate Dale
Dissolved Organic Cutwn pOC) SMS^O-D mg/L 0 ? 5 10 03/13/200? 03/1V20C2
mg/L: Milligrams/Liter (ppm)mg/Kg: MiDigrams/Kilogiam (ppm)
>ig/L: Micrograms/Liter (ppb)Hg/Kg Micrograras/Kilogram (ppb)%Rec: Percent Recovered (surrogates)
PQL: Practical Quajititation LimitDLR; Detection Limit for Reporting
: PQL x Dilution
ND None Detected at DLR
H: Analyzed outside of hold tonePreliminary result
S: Suspect result. See Cover Letter for comments.E' Analysis performed by External laboratory.
See External Laboratory Report attachments
Pa«e2of21414 Staruskus Street Fresno, CA 93706-1 623 Phone 559-497-2888, In CA 800-877-8310 Fix 559-485-6935
?J£L LABORATORIES CHMNOF CUSTODY
^f£L f/i<£Z~
OW o inhng walai SOWW /asm Waiei AO01 C
Custody Seal ntact? Y
] Reimq jishefl by
;/^
13
Date/Time Dal; -£
•^-//~t?J.; ?1'";d
. ^
Thali»biHyo1NELUiboialofieslnc islmiiKjsIf ci,iolh«pnwolsdmple'i"aly5istortt-D_ei.amples'c~ oivedingocdcocidilonty '•JEL NELisicrticspor i 'e lor loss d^tr age itfi " p! rgcd'' =rrtci<; •> rut,«Unduding adequate sample vo/ums and nun-b«f c* i onlainers Customef ji3Ta!ure of this "cC const ILTICS a purchase order fcf NEL top*w*c rr> work and onsli Jss ucccpiaace -> 3)NGtS r i c a a l e s a ' J w i
31 NEL Slanbard List Puces lor all servi osofria/*^ lemon e^eij' those acec/fiedoihem e «a ar vfL Q.j<xa'ion 'or Testing Services 10 8*ieci JMria li"" Ql saTip'e ei-^ipl NE-'utraiGj o 'mss ace •" j 6j i3bo?atory»ri«i 1630 will b« eonsideieirecBivoi ".r.irie nexl i-t. vng day ;ommil/nerl o laboralci-) to ihe re^^iteo 'umafo-ndtirne'ftill rucontir/ti-a ia Sanip'aC^^f naii; ansmp^c Ij •> e '»• -^r cei p
ORIGINAL
/ * ' t fif o
NEL LABORATORIESReno • Las VegasPhoenix • Boise
Las Vegas Division4208 Arcata Way, Suite A • Las Vegas, Nevada 89030
702-657-1010 • Fax: 702-657-15771-888-368-3282
Ed CarltonDumpco/Silverstate7900 Vegas Valley DriveLas Vegas, NV 89112
TEL: (702)431-3020
RE Project: GH-3F-263'
Dear Ed Carlton:
RECEIVED
Order No.: L0203115
NEL Laboratories, Las Vegas received 1 sample on 3/11/02 for the analyses presented in thefollowing report.
There were no problems with the analyses and all data for associated QC met EPA or laboratoryspecifications unless noted in the Case Narrative.
If you have any questions regarding these tests results, please feel free to call.
Stan Van Wagenen »^ 'Laboratory Manager ^"^
Certifications:ArizonaCaliforniaIdahoMontanaNevadaNew MexicoUS Army Corps of Engineers
Kv
Reno Las VegasAZ0520 AZ05181707 2002Certified CertifiedCertified CertifiedNV033 NV052Certified Certified
Certified
Date
NEL LABORATORIESV
CLIENT: Dumpco/Silverstate
PROJECTED: GH-3F-263'
PROJECT #: GH-3F-2631
MATRIX: AQUEOUS
ParameterAcetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetraohlonde
Chlorobenzene
Chloroethane
2-Chloroethyl vmyl efher
Chloroform
Chlnrnmpthane
2-CHorotoluene
4-Chlorotoluene
Dibromochloromethane
1 ,2-Dibromo-3-chloropropane
1 ,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1 ,2-Dichloroethane
1 , 1 -Dichloroethene
cis-1 ,2-Dichloroethene
trans-l,2-Dichloroethene
1,2-Dichloropropane
1 ,3-Dichloropropane
2 ,2-Dichloropropane
1 , 1 -Dichloropropene
cis-1 ,3-Dichloropropene
trans-l,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
2-Hexanone
lodome thane
Isopropylbenzene
ND - Not Detected at the Reporting Limit
DF - Dilution Factor
Date: l3~Mar-02
Result Unit
32 ng/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ReportingLimit
2550505050505025505050505050505050505050505050505050505050505050505050505050505050255050
CLIENT ED: GH-3F-263 '
DATE SAMPLED: 3/11/02
NEL SAMPLE ED: L0203115-001A
DF Method Prep Date
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
Analyzed
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
Analyst
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 1 off
NEL LABORATORIESV
CLIENT: Dumpco/Silverstate
PROJECTED: GH-3F-263'
PROJECTS: GH-3F-2631
MATRIX: AQUEOUS
Parameter
p-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone
MTBE
Naphthalene
n-Propylbenzene
Styrene
1,1,1 ,2-Tetrachloroethane
1 ,1 ,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1 ,2,3-Tnchlorobenzerie
1 ,2,4-Tnchlorobenzene
1,1,1 -Tnchloroethane
1 , 1 ,2-Tnchloroethane
Tnchloroethene
Tnchlorofluoromethane
1 , 1 ,2-Tnchlorotnfluoroethane
1 ,2,3-Tnchloropropane
1 ,2,4-Tnmethylbenzene
1,3,5-Tnmethylbenzene
Vinyl acetate
Vinyl chlonde
o-Xylene
m,p-Xylene
Surr: Dibromofluoromethane
Surr: Toluene-d8
Surr: 4-Bromofluorobenzene
Result
ND19
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND96.6
93.7
78.4
Unit
ug/L
ftg/L
ug/L
ug/L
"g/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
UR/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
ReportingLimit
50502550505050505050505050505050505050505050505010
89-102
90-102
70-106
CLIENT ED: GH-3F-263'
DATE SAMPLED: 3/11/02
NEL SAMPLE DO: L0203115-001A
DF Method
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
Prep Date Analyzed
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
Analyst
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
ND - Not Detected at the Reporting Limit
DF - Dilution Factor
Date: 13-Mar-02
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 2 of 5
NEL LABORATORIES
CLIENT: Dumpco/Silverstate
PROJECT ED: GH-3F-2631
PROJECTS: GH-3F-2631
MATRIX: AQUEOUS
Parameter
Barium
Calcium
IronMagnesium
Potassium
SodiumVanadiumAntimony
Arsenic
Beryllium
Cadmium
Chromium
CobaltCopper
Indium
LeadNickelSelenium
SilverThallium
Zinc
Mercury
Result
2.0
1300200640110
10000.26
0.0028
0.230.0078
0.0037
0.130.0690.20ND
0.0810.33ND
0.0053
0.0063
0.85ND
Unit
mg/Lmg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/Lmg/L
mg/L
mg/L
mg/L
ReportingLimit
0025
25050251025
0025
0.0010
O O O I O
0.0010
0.0010
0.0010
0.0010O O O I O
OOOIO0.0010
0.0010
OOOIO0.0010
0.000400.0010
0.00020
CLIENT ID:
DATE SAMPLED
NEL SAMPLE ED:
DF
5555555111111111111111
Method
SW 6010B-TO
SW6010B-TO
SW6010B-TO
SW 6010B-TO
SW 60108-ToSW6010B-To
SW6010B-ToSW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-TotaSW 6020-TotaSW 6020-Tota
SW 6020-TotaSW 6020-Tota
SW 6020-Tota
SW 6020-TotaSW 6020-Tota
SW 7470-Tota
GH-3F-263'
: 3/11/02
: L0203115-001B
Prep Date
03/12/02
03/12/02
03/12/0203/12/02
03/12/02
03/12/0203/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/0203/12/0203/12/0203/12/02
03/12/02
03/12/0203/12/02
03/12/02
03/13/02
Analyzed
03/12/02
03/12/02
03/12/02
03/12/0203/12/02
03/12/02
03/12/0203/12/02
03/12/0203/12/02
03/12/02
03/12/02
03/12/02
03/12/0203/12/0203/12/02
03/12/0203/12/02
03/12/0203/12/02
03/12/02
03/13/02
Analyst
JTY-Reno
JTY-Reno
JTY-RenoJTY-Reno
JTY-Reno
JTY-Reno
JTY-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-RenoDHG-Reno
DHG-RenoDHG-RenoDHG-RenoDHG-Reno
DHG-Reno
DHG-RenoDHG-RenoDHG-RenoFIF-Reno
ND - Not Detected at the Reporting Limit
DF - Dilution Factor
Date: 13-Mar-02
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 3 of5
NEL LABORATORIES1 — _
CLEENT: Dumpco/Silverstate
PROJECT LO: GH-3F-263'
PROJECT #: GH-3F-2631
MATRIX: AQUEOUS
Parameter
Barium
Calcium
Iron
Magnesium
Potassium
Sodium
Vanadium
Antimony
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Thallium
Zinc
Mercury
Result
0.029
570
ND18050980ND
0.0014
0.0020
ND
ND
ND0.0012
0.0037
ND
0.0019
0.0083
NDND
0.051
ND
Unit
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
ReportingLimit
0005025010251025
00050OOOIOOOOIOOOOIOOOOIOOOOIOOOOIOOOOIOOOOIOOOOIOOOOIOOOOIO0 00040OOOIO0 00020
CLIENT ED: GH-3F-263'
DATE SAMPLED: 3/11/02
NEL SAMPLE ID: L0203115-001C
DF
l51555111111111111111
Method Prep Date
SW 60108-Di
SW6010B-Di
SW6010B-D1
SW 6010B-D1
SW6010B-Di
SW6010B-D1
SW 6010B-Di
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW7470-Diss 03/13/02
Analyzed
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/13/02
Analyst
JTY-Reno
JTY-Reno
JTY-Reno
JTY-Reno
JTY-Reno
JTY-Reno
JTY-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
FIF-Reno
ND - Not Detected at the Reporting Limit
DF - Dilution Factor
Date: 13-Mar-02
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 4 of 5
NEL LABORATORIES
CLIENT: Dumpco/Silverstate
PROJECTED: GH-3F-263'
PROJECTS: GH-3F-2631
MATRIX: AQUEOUS
Parameter
Chloride
Nitrate, as N
Nitrite, as N
Sulfate
Alkalinity, Bicarbonate (As CaCO3)
Alkalinity, Carbonate (As CaC03)
Hydroxide (As CaC03)
Alkalinity, Total (As CaCO3)
Chemical Oxygen Demand
Ammonia, as N
Sulfide
Total Dissolved Solids
Result
1100
NDND2600
680NDND68064
NDND
6130
Unit
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
ReportingLimit
5025255025025025025010
0300030600
CLIENT ED: GH-3F-263'
DATE SAMPLED: 3/11/02
NEL SAMPLE ED: L0203115-001D
DF
5002525500101010101114
Method Prep Date
EPA 300 0
EPA 300 0
EPA 3000
EPA 300 0
SM2320 B
SM2320 B
SM2320 B
SM2320 B
SM5520 D
SM4500-NH3
SM4500-S D
SM2540 C
Analyzed
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/12/02
03/12/02
03/12/02
03/11/02
Analyst
PJJ-LV
PJJ-LV
PJJ-LV
PJJ-LV
RDA-LV
RDA-LV
RDA-LV
RDA-LV
RDA-LV
RDA-LV
RWW-LV
PJJ-LV
ND - Not Detected at the Reporting Limit
DF - Dilution Factor
Date: 13-Mar-02
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 5 of 5
NEL Laboratories, Las Vegas Date: 13-M,ar-Q2
CLIENT:Work Order:Project:
Dumpco/SilverstateL0203115GH-3F-2631
ANALYTICAL QC SUMMARY REPORTTestCode: 300 W
m
Sample ID MB-R884
Client ID ZZZZZ
Analyte
Chloride
Nitrate, as N
Nitrite, as N
Sulfate
SampType MBLK
Batch ID R884
Result
NDNDNDND
TestCode 300_W Units mg/L
TestNo E300
PQL SPK value SPK Ref Val
0 10
0 10
0 10
0 10
Prep Date Run ID L_IC-1_020311A
Analysis Date 3/11/02 SeqNo 5996
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qua!
03oJO
ODOmCD
Qualifiers: ND - Not Detected at the Reporting Limit
J Analyte detected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
B - Analyte detected in the associated Method Blank
Page 1 of 14
CLIENT:Work Order:Project:
Dumpco/SilverstateL0203115GH-3F-263'
ANALYTICAL QC SUMMARY REPORTTestCode: 6010W D
Sample ID MB-R659
Client ID ZZZZZ
Analyte
SampType MBLK
Batch ID R_R659
Result
TestCode 6010W_D Units mg/L
TestNo SW6010B
PQL SPK value SPK Ref Val
Prep Date
Analysis Date 3/12/02
%REC LowLimit HighLimit RPD Ref Val
Run ID SUB-659
SeqNo 6434
%RPD RPDLimit Qual
m
03ODO
IDrn
Barium
Calcium
Iron
Magnesium
PotassiumSodium
Vanadium
NDNDNDND
NDNDND
00050
0500 10050
2 0050
00050
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte detected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
B - Analyte detected in the associated Method Blank
Page 2 of 14
CLIENT:Work Order:Project:
Dumpco/SilverstateL0203115GH-3F-263'
ANALYTICAL QC SUMMARY REPORTTestCode: 6010W t
Sample ID MB-351
Client ID ZZZZZ
Analyte
SampType MBLK
Batch ID R_351
Result
TestCode 6010WJ Units mg/L
TestNo SW6010B
PQL SPK value SPK Ref Val
Prep Date 3/12/02
Analysis Date 3/12/02
%REC LowLimit HighLimit RPD Ref Val
Run ID STJB-660
SeqNo 6438
%RPD RPDLimit Qual
m
00ODO
ITJm
BanumCalciumIronMagnesiumPotassiumSodiumVanadium
NDNDNDNDNDNDND
000500500 1005020
05000050
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte detected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R RPD outside accepted recovery limits
B - Analyte detected in the associated Method Blank
Page 3 of 14
CLIENT: Dumpco/SilverstateWork Order: L0203115Project: GH-3F-263'
Sample ID MB-R661 SampType
Client ID ZZZZZ Batch ID
Analyte
Antimony
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Thallium
Zinc
MBLK
R_R661
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ANALYTICAL QC SUMMARY REPORT
TestCode: 6020W_D
TestCode 6020W_D Units mg'L Prep Date Run ID SUB-661
TestNo SW6020 Analysis Date 3/12/02 SeqNo 6445
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
OOOIO
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I OO O O I O
O O O I O0 00040
O O O I O
TJ
\BO
RA
TO
R
mCO
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte detected below quantitation limits
S - Spike Recovery outs ide accepted recovery limits
R - RPD outside accepted recovery limits
B - Analyte detected in the associated Method Blank
Page 4 of 14
•
CLIENT: Dumpco/SilverstateWork Order: L0203115Project: GH-3F-263'
Sample ID MB-350 SampType
Client ID ZZZZZ Batch ID
Analyte
Antimony
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
SilverThallium
Zinc
MBLK
R_3SO
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ANALYTICAL QC SUMMARY REPORTTestCode: 6020WJT
TestCode 6020W_T Units mgTL Prep Date 3/12/02 Run ID SUB-656
TestNo SW6020 Analysis Date 3/12/02 SeqNo 6424
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLirmt Qual
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I OO O O I O
OOOIOO O O I O
-••
Tj
*>»^\BO
RA
TO
RIE
S
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte detected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
B - Analyte detected in the associated Method Blank
Page 5 of 14
••
CLIENT: Dumpco/SilverstateWork Order: L0203115Project: GH-3F-263'
Sample ID MB-R893 SampType
Client ID ZZZZZ Batch ID
Analyte
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane2-Butanone
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachlondeChlorobenzene
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
2-Chlorotoluene
4-Chloro toluene
Dibromochloromethane
1 ,2-Dibromo-3-chloropropane
1 ,2-Dibromoethane
Dibromomethane
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1 ,2-Dichloroethane
1,1-Dichloroethene
MBLK
R893
Result
NDNDND
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
NDNDNDNDNDNDNDNDND
NDND
ANALYTICAL QC SUMMARY REPORTTestCode: 8260_W
TestCode 8260_W Units fig/L Prep Date Run ID L_VOAMS-2_020311B
TestNo SW8260B Analysis Date 3/11/02 SeqNo 6048
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
255050505050502550
50505050505050
]
50505050
505050505050505050
5050
—ysJEL LABORATOR
mCO
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte detected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
B - Analyte detected in the associated Method Blank
Page 6 of 14
1
CLIENT: Dumpco/SilverstateWork Order: L0203115Project: GH-3F-263'
Sample ID MB-R893 SampType
Client ID ZZZZZ Batch ID
Analyte
cis-l,2-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
1 ,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-l,3-Dichloropropene
trans-1 ,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
2-Hexanone
lodome thane
Isopropylbenzene
p-IsopropyltolueneMethylene chloride
4-Methyl-2-pentanoneMTBE
Naphthalene
n-Propylbenzene
Styrene
1,1,1 ,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroe thene
Toluene
1 ,2,3-Tnchlorobenzene
1 ,2,4-Tnchlorobenzene
1,1,1 -Trichloroethane
1 , 1 ,2-Tnchloroethane
Tnchloroe thene
Tnchlorofluoromethane
1 ,1 ,2-Tnchlorotrifluoroethane
MBLK
R893
Result
NDNDNDNDNDNDNDNDNDNDNDNDNDNDND
NDNDNDNDND
NDNDNDND
NDNDNDNDNDNDND
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte detected below quantitation limits
ANALYTICAL QC SUMMARY REPORT
TestCode: 8260_W
TestCode 8260_W Units ug/L Prep Date Run ID L_VOAMS-2_020311B
TestNo SW8260B Analysis Date 3/11/02 SeqNo 6048
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
50 150505050505050505025505050502550
105050
505050505050505050
5050
S - Spike Recovery outside accepted recovery limits B - Analyte detected in the associateijl Method Blank
R - RPD outside accepted recovery limits Page 7 of 1 4
' '
NEL LABORATOR
rnCO
wm
CLIENT:Work Order:Project:
Dumpco/SilverstateL0203115GH-3F-263'
ANALYTICAL QC SUMMARY REPORTTestCode: 8260 W
Sample ID MB-R893
Client ID ZZZZZ
Analyte
1 ,2,3-Tnchloropropane
1 ,2,4-Tnmethylbenzene
1 ,3,5-Tnmethylbenzene
Vinyl acetate
Vinyl chloride
o-Xylene
m,p-Xylene
Surr Dibromofluoromethane
Surr Toluene-d8
Surr 4-Bromofluorobenzene
SampType MBLK
Batch ID R893
Result
ND
ND
ND
NDNDNDND
4928
4564
3842
TestCode
TestNo
PQL
50
50
50
50
5050
1050
50
50
8260_W Units pg/L
SW8260B
SPK value SPK Ref Val
50 0
50 0
50 0
Prep Date
Analysis Date 3/11/02
%REC LowLimit HighLimit RPD Ref Val
98 6 89 102 0
91 3 90 102 0
768 70 106 0
Run ID L_VOAMS-2_0203 1 1 B
SeqNo 6048
%RPD RPDLimit Qual
0
0
0
—
O3ODO
§DOmCO
m
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte detected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R RPD outside accepted recovery limits
B - Analyte detected in the associated Method Blank
Page 8 of 14
CLIENT:Work Order:Project:
Dumpco/SilverstateL0203115GH-3F-263'
ANALYTICAL QC SUMMARY REPORTTestCode: ALK W
Sample ID MB-R898
Client ID ZZZZZ
Analyte
Alkalinity, Bicarbonate (As CaCO3)Alkalinity, Carbonate (As CaCO3)Hydroxide (As CaCO3)Alkalinity, Total (As CaCO3)
SampType MBLK
Batch ID R898
Result
NDNDNDND
TestCode ALK_W Units mg'L Prep Date Run ID L_ATJTR-I_020311A
TestNo M2320B Analysis Date 3/11/02 SeqNo 6076
PQL SPK value SPK Ref Val %REC LowLirmt HighLimit RPD Ref Val %RPD RPDLimit Qual
25252525
i
. LABORATORIES
m
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte detected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepte d recovery limits
B - Analyte detected in the associated Method Blank
Page 9 of 14
CLIENT: Dumpco/Sdverstate ANALYTICAL QC SUMMARY REPORTWork Order: L0203115 ^Project: GH-3F-263' TestCode: COD
Sample ID MB-R900 SampType MBLK TestCode COD Units mg/L Prep Date Run ID L_SPE;C-2_0203 1 2C
Client ID ZZZZZ Batch ID R900 TestNo M5220 C Analysis Date 3/12/02 SeqNo 6090
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Chemical Oxygen Demand ND 10
? NEL
LABORATORIES
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte detected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
B - Analyte detected in the associated Method Blank
Page 10 of 14
CLIENT: Dumpco/SilverstateWork Order: L0203115Project: GH-3F-263' TestCode: HG_7470_T
ANALYTICAL QC SUMMARY REPORTWork Order: L0203115 ^
mSample ID MB-359
Client ID ZZZZZ
Analyte
Mercury
SampType MBLK
Batch ID R_359
Result
ND
TestCode HG_7470_T Units mg/L Prep Date 3/13/02 Run ID SUB-669
TestNo SW7470 Analysis Date 3/13/02 SeqNo 6450
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qua!
0 00020
—03ODO
5mCO
Qualifiers: ND - Not Detected at the Reporting Limit S - Spike Recovery outside accepted recovery limits B - Analyte detected in the associatecl Method Blank
J - Analyte detected below quantitation limits R - RPD outside accepted recovery limits Page 11 of 14
iCLIENT: Dumpco/SilverstateWork Order: L0203115Project: GH-3F-263'
Sample ID. MB-R901 SatnpType: MBLK
Client ID: ZZZZZ Batch ID: R901
Analyte Result
Ammonia, as N ND
ANALYTICAL QC SUMMARY REPORTTestCode: NH3-N_W
TestCode NH3-NJW Units: mg/L Prep Date- Run ID' L_WC;_020312B
TestNo: M4500-NH3 C Analysis Date. 3/12/02 SeqNo. 6099
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
0.30
: * NEL LABORATORIES
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte detected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
B - Analyte detected in the associated Method Blank
<Page 12 of 14
1
CLIENT: Dumpco/SilverstateWork Order: L0203115Project: GH-3F-263'
Sample ID MB-R879 SampType MBLK
Client ID ZZZZZ Batch ID R879
Analyte Result
Sulfide ND
ANALYTICAL QC SUMMARY REPORT
TestCode: SULF_W
TestCode SULF_W Units mg'L Prep Date Run ID I,_SP$C-2_020312A
TestNo M4500-SD Analysis Date 3/12/02 SeqNo 5960
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
0030
NEL LABORATORIES
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte detected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
B - Analyte detected in the associate^) Method Blank
Page 13 of 14
1
CLIENT: Dumpco/SilverstateWork Order: L0203115Project: GH-3F-263'
Sample ID MB-R907 SampType MBLK
Client ID ZZZZZ Batch ID R907
Analyte Result
Total Dissolved Solids ND
ANALYTICAL QC SUMMARY REPORT
TestCode: TDS_W
TestCode TDS_W Units mg/L Prep Date Run ID L_WC,_020311D
TestNo E160.1 Analysis Date 3/11/02 SeqNo 6140
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
150
-.
TJ
03ODO
ODOmCO
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte detected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
B - Analyte detected in the associated Method Blank
'Page 14 of 14
03/15/2002 FRI 9:48 FAX 559 485 6935 BSK LABS §1002/002
BSK A N A L Y T I C A LLABORATORIES
Vanessa PadillaNEL Laboratories Las Vegas4208 Arcata Way, SteALas Vegas, NV 89030
BSK Submission #: 2002030581
BSK Sample ID #: 189800Project ID: L0203115
Submission Comments:
Sample Type: LiquidSample Description: GH-3F-263Sample Comments:
Certificate of AnalysisELAP Certificate #1180
Report Issue Date: 03/15/2002
Project Desc: Dumpco
Date Sampled: 03/11/2002Time Sampled: 0851Date Received: 03/12/2002
Inorganics
Analyte Method Result Units PQL Dilution DLRPrepDate
AnalysisDate
Dissolved Organic Carbon (DOC) SM5310-D 5.8 mg/L 0,2 1.0 03/13/2002 03/13/2002
PQL: Practical Quantitation LimitDLR: Detection Limit for Reporting
: PQL x Dilution
ND: None Detected at DLR
mg/L: Milligrams/Liter (ppm)rag/Kg: Milligrams/Kilogram (ppm)ug/L: Micrograms/Liter (ppb)ug/Kg: Micrograms/Kilogram (ppb)%Rec: Percent Recovered (surrogates)
Report AjfceD&ition Code: 1111119111111111111111111 ID ID II HI II
1414 Stanislaus Street Fresno, CA 93706-1623 Phone 559-497-2888, m CA 800-877-8310 Fax 559-485-6935
H: Analyzed outside of hold timePreliminary resultS: Suspect result See Cover Letter for comments.E: Analysis performed by External laboratory.
See External Laboratory Report attachments.
Page 2 of2
NEL LABORATORIES CHAIN OF CUSTODY NEL Work Order: LOWReno • Las Vegas • Boise
Phoenix * Sacramento
'urchase Order NumberLas Vegas Division • 4208 Arcata Way, Suite A • Las Vegas, Nevada 89030
702-657-1010 • Fax: 702-657-1577 • 888-368-3282
ExpectadJSujJ Date
Requested Turnaround:
Time/DateSampled
N.E.LIdentificationCustomer Sample Identification
DW - Drinking Water SD - SolidWW • Waste Water AQ • AqueousOL - Oil/Organic Liquid A - Air
A, HCIB HNO3
C, H2S04'
E Ice OnlyF OtherG Not Preserved
Custody Seal intact'Con'
Relinquished by (Print) (Sjgrfature) Date/Time F.eceived by (Print) (Signa^ire) Date/Tima
The liability of NEL Laboratories Inc. is limited strictly to the price of sample analysis for those samples received in good condition by NEL. NEL is not responsible for loss, damage, resampling costs and/or qualified data related to samples not received in good condition,Including adequate sample volume and number of containers. Customer signature of this CoC constitutes a purchase order for NEL to perform work and constitutes acceptance of all NEL Standard Terms and Conditions, Signature also constitutes acceptanced(NEL Standard (JSt Prices fot all services Oldered h6I8 on, exCBpt those specified otherwise via an NEL Quotation for Testing Servi ;es in effect at the time of sample receipt. NEL turnaround times are measured In regular vyorking days. Samples received at thelaboratory after 16:30 will be considered received on the next working day. Commitment of laboratory to the requested turnaround limp will be confirmed via Sample Confirmation transmitted to the fax number provided above,
ORIGINAL
AHORATORir.SWev Suite A • Lea Veqas Ni-va-'n {ft iO
7r>?.6.r>r-inio« r-w- -v- T -~
- . , . , . .-I <--uie•, - -\i- \* • i--y I
Las Vctv*s, N V '391
•RE Proiorr: IWH-3F-263'
Dear Derek "Reeve:
Order No.: L0203U6
NEL J^aboratories, Las Vegas received 1 sample on 3/11/02 far the analyses presented in thelnl\owingrepoti.
There were no problems with the analyses and all data for associated QC met EPA or laboratoryspecifications except where noted in the Case Narrative.
If you have any questions regarding these tests results, please feel free to call.
Lftborstorv Manager
Certifications.ArizonaCaliforniaIdahoMontanaNevadaNew MexicoUS Army Corps of Engineers
Reno Las VegasAZ0520 AZ05181707 2002Certified CertifiedCertified CeitifiedNV033 NVOS2Certified Certified
Certified
Date
Ciu:
NEL LABORATORIES CHAIN OF CUSTODY NEL Work OrderRano • Las Vegas • Boise
Phoenix • Sacramento
Purchase Ordei NunberLas Vegas DMsion • 4208 Arcala Way. Suite A- Las Vegas, Nevada 89030
702457-1010 • Fax: 7IK-65M 577 • BBB-369-3282
Requesl&d Turnaround:
Time/DateSampled
N.E.LIdentificationCustoiner Sample Identification
A.HCIB HNO,C H,60,D
C'jstody Seal intactConi
(Sigijfirffire} Date/Time (Signptura) Date/Tipn
c.
IX
Cr.tr
,inelua^a KHquat* umple volume and nurebw of eortamom. Cuttomgr signature at Ws DaC constitutes a purctmsu aider lor NEL to perfaiffl work and constitutes aooepumc* of nil NEL S'andaid Tefint a.td>Condrt!oni. Slgnalure eliooowt'duld NELSIirvdud Liit PACSI ft» all ssrv^u onte«d tww an, .except tho»« if«cltl«a »;hi(Wie v1» in NO. Quotation for Ttsting Survcei In efect a) r)w <me d sample ieoff.pl NEUIumMottrKl titia* »a measured in ngiflai \voiving Cays Srmplii nowed «l \ho
co^, »n.T 1E30 vail b« ooniidared receVad on Ihe ivisd tvoffeng d»y. CoanmHenartt or labordtory lo lh» raquesiBd turnaroirvJbm« wintua contnmet) vi» Sonip* Coflliimiuinn trorwrnced to th« lux nunrt* provided abe«».
roCO
rv>CO
Fpn;i: qi 170?47!130~'7
NEL LABORATORIESReno » las VegasPhoenix « Botes
Derek ReeveDumped/Silvers tate7900 Vegas Valley DriveLas Vegas, NV 89112
TEL: 702-431-3020
RE Project: DGH-3F-2631
Dear Derek Reeve:
Las Vegas Division4208 Arcata Way, Suite A • Laa Vegas, Nevada 89030
702-657-1010 • Fax- 702-657-15?71-888-368-3282
Order No.: L0203U6
NEL Laboratories, Las Vegas received 1 sample on 3/11/02 for the analyses presented in thefollowing report.
There were no problems with the analyses and all data for associated QC met EPA or laboratoryspecifications except where noted in the Case Narrative.
If you have any questions regarding these tests results, please feel free to call.
Stan Vgft Wagofien" .Laboratory Manager
Certifications:ArizonaCaliforniaIdahoMontanaNevadaNew MexicoUS Army Corps of Engineers
~~p
Reno Las VegasAZ0520 AZ05181707 2002Certified CertifiedCertified CertifiedNV033 NV052Certified Certified
Certified
Date
I;-, r ..1 ,- rFi.l'l:-.'INRV'F i HMOf-fi
MEL LABORATORIESDuropco/Sih erstate
T.l.FPn
CLIENT ID: DGH-3F-263'
HATE SAMPLED: 3-'U/02
NEI.SAMPIYEIP: Lfl2031l6-OOlC
MVTH1X: AQUEOUS
Parameterrh'.ou.'C
Nurate, as N
>, f t- M U
SMII»UAlkalinity, B Ic»rban4t« (A* CnCO3)
Alka.u<icy. C irboiwc (A< CaCOl)
Hydroxide (As C^aCCM)
AlkaliuItVjTattl (A« C«CO3)
rii*rnic»J Otygert n^nan.!
Arnrruiiu, >•• N
Sulfidc
Total Distolvcil Solidi
Result
1300
ND
NTi
7<)0fl
(40
wnNO
<vU)
€1NDNO5619
Unit
me/Imt/Lirtj.t.
mc/L
nitt/L
mft/Lmp/Lmerl.
mg/Lnift/L
mg/Lmg/L
ReportingLimit
NO
2 52 i50
2502W25025010
0.300.030
600
DF5002575
50010!010101114
Method Prep Date
tPA 300.0
UPA 300.0
EPA 3000
EPA 300.0
SM2320B
SM2320 B
SM2320B
SM2320 B
SM5520 D
SM4500-NH3
SM4500-S D
BfA 160.1
Analyzed
03/J1/02
• O.Vll/02
03/11/03
03/1 1/02
03/1 1/0203/1 1/02
03/1 1/02
03/11/02
03/12/0203/12/02
03/12/02
03/11/02
Analyst
PJJ-LV
PJJ-LV
PJJ-LV
PJM,V
HDA-LV
RDA-LV
HUA-LV
RDA-LV
RTJA-LVRDA-LV
R\VW-LV
PJJ-LV
NO -Noj Oetetttd n the Reporting Unrii
DF - Dilution Factor
Date: 12-Mar-Q2
B - Analyw delected in the wwciitcd Method Blink
S - Spfkc Recavoiy outside accepted recovery hmitiE • Value above quanriabon range Page 1 of3
FflX NO. 70<? 657 1577
NEL LABORATORIES
CLIENT: Dumpco/^ilvmtste
PROJECT 1 D: W rrf-3«-?& V
riJENT 10: DGH-3F-2631
BATE SAMPLED: 3.'J1'03
AT.L SAMPLE ID: L02 03 116-00 ID
MATRIX: AQUEOUS
'.'arametcrAtUPnu
BcrufriC
':rom« benzeneHrumocUlQro methanearomndif.hlofomtlhaner>rc.rToforn!
flronmrnrih ine2-tiuirmoiicn-Bi.rYlbcrizi.ncscc-Butylbsr,zenQim-SulvlbfriTcncCarbon disulluicCarbon ietra.:hlQridcChlorobennntChlorocthaji :.i-Chlorocrtv/l vinyl ethernilorrfarmCWorometbiins2-CWoro toluene4-CWOrotoliieni;Dibromoshbromctrmne1 ,2-DibK>nvi-3-chluroprop»pii1 ,2-D]bronv3«ihari«Dibrornomeihinci ,2-Dichlorobenzenc1 ,}-D!chlorobfln7enc1 ,4-DtCtllor:ibert2ene
Dich'.orndifloarometharie1 ,1 -DichlorotiMne1,2-Dichlotciettanc! .\-l3iohlofncthEnf....s-l 2-Dic ,|.>roethencIrarH'l ,2-Dif hlorocrthcns1.2-Dichloioprnp»ne1 ,3-Dichlo)xjprop»tic2,2-DichIwoprop«ne1,1-Dicbioiopropcn:cii-l j-Dicftloropropencitians-1 .S-KchloropropencEthylbenrencHwichloiibutadiene2-Hexatxveloctometharie[sopropylbcnzene
R«iul
••<!
MDNDNr>NDKDNDNONT)NDNI3
NDNDrVDNDNDNDNDNDNDNDNDNDNDNONDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
\t IJn!t
IIC/J.
MS'LHS/LMF/LjiJ^LU?/LH8/L
Hg'LMS/t^6/LMg/L
MB/LK8/LMB/L
H6/LM8/I-HS^-H8/L1 8 .
fg'LHfrT-HBrt-Mg/Ll^S/L
US"-H^LMg/l-
tLg/L
Hg'LHB/l-MS^-H'S-''-HE/t-JiS/LHB/L
K6/LMg/I.Ht/LHfi/LH«^HS'LM8«-JIE/LUg/L
RoportinuI'"*
?*
;.o50505.0505,025505.05.05.05.05.05.05.05.05.0SO505.05.0505.05,05.05.0505.05.05.0s.o5.0505.05.05.0505.05.050
255-05.0
DF
11i11111111111111111J111111111111111111I1I11
Method PregJSW8560BSW8260BSW8260BSW8260RSW8250BSW8260BSW8260B .SW&260DSW82606SW82SOBSV/8260BSWS260BSW8260BSW8260BSW8260BSWS260BSWR2«OflSW8260BSWS2608SW826QBSW8260ESW8260BSW82SOBSW8260BSW85SOBSW8260BSW8260BSWS260BSWS160BSW8260ESW8260BSWS2fiftBSW8260BSW8260SSW8260BSW82608S NV8260SSW8260BSWS260BSW8260BSW8260BSW82606SW8260BSW8260B
Oate AnalH^,03/11/0203/11/02OV1 1/0203/1 1/0203/11/0203/11/02Q3/1 1/02
03/1 1/0203/11/0203/11/0203/11/0203/11/0203/1 1/0203/11/0203/11/0203/11/0203/11/0203/11/0203/11/0203/1 1/0203/1 1/0203/1 1/0203/11/0203/1 1/0203/11/0203/11/0203/1 1/0203/11/0203/11/0203/11/0203/1 1/0203/1 1/0203/11/0203/1 1/0203/11/0203/11/0203/1 1/0203/11/0203/1 1/0203/1 W0203/11/0203/1 1/0203/1 1/0203/11/02
AnalystDRM-t-VDRM-LVDRM-I vDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVUliM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDKM-LVDRM-LYDRM-LVPRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LV
NO - Not Detected at the Reporting Limit
DF - Dilution Kactor
Date: 12-Mar-02
B - Armlyw detected (n the auociafed Method Blank
S - Spika Recovery outride iwcepted recovery limits
£ - Value above quwuitation range Page 2 of 3
I! ;;.»:'i J ' i i .N'H FAX NO. 70? 657 1577
NEL LABORATORIES
CLIENT: D .-nr>~n. '; .'.v^fav
PROJECT ID: 1XHI-31?-2<S,V
MATRIX: AQilfOUS
Paraineter
?-l.-opTOpy»tcluenc
M«thyl«ne cUldrirfeS-Mctliyl-Henuninw
MT«rNaphthalene
:i sv.pylfccn-m,;
Slyrens
t,l,1,a-TctrjehIarMlr,»ju:'. ,1 ,2,2-Tctrtcliloroot!ian«
TeTrachlorotiheneToluefio
1 ,2,3-TricWr.irobenmiM1 ,2,4-Yrichlijroticnzdnc
J,l.l-Tri<;hliirt>eth»n«
I,l,2-Tri«hli>roe!hurt8
Trichlorocthune
Tricrilorofluoromeirmnii
1 ,1 ,2-Tnd)l-3rotrifiuorocthiirte
1 ?.1-Trirhl5ronropanc
! ,2,4-Trimetbylbsnuenc1,3,5-Trirnsir.ylberuencVinyl accuse
Yinyl chlorde
0-Xylene
m.p-XyletwSurr: DitirtmtinuorDmrthaneSurr: Tclucnc-d8Surr: J-'.iromcfluorobcnMnc
Result
-•in1?
NDN'D
NOb?DNDNOMDNDNDNDNO
ND
NDND
ND
ND
NO
NPNDNDNDND
ND97.9
91.8
81.3
Unit»'g.'l.Iv^'L
MfL[Ig/L
Pfrt.
i* s -pjpyijJitt/C
^p/Lut/L,JilC/I*
Mg/LUR/£-
pifi/X.
ue'Lcs^HC/LH8/LKB«.fg/LHg/LMS/LHg/I-HS/LMS/LV.KEC
V.RCC
%RF,C
Reportingl.lmjt
50SOJ5
5.05.0
50
5.0
5-05.05.0
S.O5.05.0
5.0
5.05.05.05.05.0 .5,05.05.05.05.010
89-10290-102•70-106
CLIENT ID: T>nH-3F-263'
ft.YTE SAMPLED: Vll-'Q?.
NTL SAMPLE in: T,(KW*I ifi-ooiD
BF1
Iill1]lll11l1lI1'Ill1lII1111
Method
SW82SOBSWBMOBSwa?.60BSVV8260B
sw82fionSWR260S
SW8260B
SW82f300
SW8260BSW82SOBSW8260BSV/8260BSW8260BSW8260BSW8260BSW8260BSW8J60BSWS2«OBSW8260HSW8260BSW&260BSW8260BSWS260BSW8260BSW8260BSWS2608S \V8260BSWS260B
PrcjjJDate Analyzftd
03/1 1/02
03/11/02
03/1 1/02
OVU/02
OV11/02
01/11/02
03/11/02
03/1 1/02
03/1 1/02
03/11/02
03/11/02
03/1 1/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/0203/11/0203/11/0203/11/0203/1 1/0203/11/0203/11/0203/U/0203/11/02
03/1 1/0203/1 1/02
AnalystDRM-LV
DRM-l.V
DRM-LV
DRM-LVDRM-LV
DRM-l-V
DRM-LV
PRM-LV
DRM-l.V
DRM-LV
DRM-LVDRM-LV
URM-LV
DRM-LVDRM-LV
DRM-LV
DRM-LV
DRM-LVDRM-LV
DRM-LV
DRM-LVDRM-LV
DRM-LV
DRM-LVDRM-LVDRM-LVDRM-LVDRM-LV
ND - Not Detected at the Reporting Limit
DF - Oiluiion Ficur
; 12-Mar-Q2
B • Anilyte detect^! in (he uuociited Method Blank
S • Spifcfl Recovery outride wcepied recovery lirniu
E • Value above quuitiutian rmge Page 3 Of 3
-13-20f>? !JF'
* *r"i "* 1 "V * "*>'j i - <r * ' i -
rn.v NO. /a? nsy is:AX NO, 7?S 348 254B r. o;
ATH
cuDATE SAMPLED:
NMUiSAMPIJK !»;****•
frisft Ito'ft
rail,
(MS
0*71
M«
ND
S3Q
wet
»{/L
S*lffllusSilver
Smtiuta
ND
ND
n«offlj•J*t.75
ng/Lmg/Lrki/1-tnfi'l.
n f W l f i
(M/L
O.WI"
S S
0,0010o.oo in0-00100.0010
O.M
00010M
aOOio10
o.ooia0.0010
25ODOMO0.033
0.0010
P.?f W fft7l>.Tlji>4
SW«0»-T^!
1W«)10S-Te>«»l
SW6020-TealSW6020-TTOI
SWWlOB'TtrtuI
SW 6030-Tou!SWWloa-Toul
OVI 7A)'.
OV12/0203/IW1rrt/lZ/02
03/17/0303/tWli
1 SW<020-Tow( OVI3/liZ
Din a/02M/lt/03
03/t?«2llVll'OZ
03/13AH
03/1 ZAJl
03/13*1 JTY-It«n>
CW12A32
DHO MCBO
QJ/17/W
OVIW32
OV15AB
os/cvniOStZ/ltt03/12/02
TTY-RoeoDHG-tMBO
DHO-RWO
v:> T^^ •- *. $ *V « "p I..7;..* ..'•: -s A • • > » •-' *. . ^». .«i' -lr» ?- •..-,.- ..- A. --•- j • ' •« ' •'•'- • - "" -" '*• '"'
I 1-.'".'.'• :. ' n i - ^ r ,v-J j i
CUKNT- NGt TJ* Vem
CT ID; /Vi'»
MATRfX; AQUEW"
Awtooor
8orlu-e
Chromium
()(W
Usri
NVle!
Xrftoiatn
Sodioro
IMJS
?**»*
Kft
HO
JM
»JM«
fcfW
ND
ND044*
mp'L
•OCA,
ms/U
l/lg/L
m^U
BOf/1*
CMHNT IDj
DATUSAKfPLEO: 3'11/OJ
N-'l^*MnJRlf>: M i**"
Reporting»4nrft REf/.oom i
unosno.ootoOOOIO
3.J
O.OOIQ
(l«»004010
O.IO
U.MlO
aj0.0010
too.noioo.ooio
250.00040
SW WUft-W*!
5W60lOft-Di»
I SWMI(W-Di»
I
j ft,
OVU'02
Kunm(W/I370S
AB&*
JTTHW10
OKO-feoo
DHO-JUftO
DKC-tutoJTY-Heno
»/l?/M03/13/02 iTY-ftMO
wnaw OHQ*B»JTY-IU(*oDHC-HW5
03/12ATI
03/12VB2 /TY-dnioOM2/02
ND - N« CMtswJ rt e» Reportfflg Uwrtt»P. \ t f i\f A 13? • v'
.i Li-'M 'f-j,.L.
SCS Engineers
To: Steve Wall From: Ed Carton
Fax: (415) 947-3530 Date: March 20, 2002
Phone: (41b) 972-3380 Pages: 23 (including cover sheet)
Re: Analytical Data - DGH-3F-263' CC: Sandra Doty, Brent Lewis
O Urgent 0 For Review Q Please Comment D Please Reply D Please Recycle
•Comments:
Duplicate sample for GH-3F-263' which was faxed previously
NEL LABORATORIESReno • Las VegasPhoenix • Boise
Derek Reeve
Vegas Valley DriveLas Vegas, NV 89112
TEL: 702-431-3020
RE Project. DGH-3F-263'
Dear Derek Rcc\c
Tt. .--r-H
Las Vegas Division4208 Arcata Way, Suite A • Las Vegas, Nevada 89030
702-657-1010 - P a x 702-057-'57?
RECEIVED'••§•:! HftR 18 PH 1=30
Order No.: L0203116
NEL Laboratories, Las Vegas received 1 sample on 3/11/02 for the analyses presented in thefb'lrnvnq report
There were no problems with the analyses and all data for associated QC met EPA or laboratoryspecifications except where noted in the Case Narrative.
If you have any questions regarding these tests results, please feel free to call
Stan Van Wagenen /1 ahoratorv Manaeer
Certifications-ArizonaCaliforniaIdahoMontanaNevadaisew MexicoUS Army Corps of Engineers
) cy^~~*^
RenoAZ05201707CertifiedCertifiedNV033Certified
Las VegasAZ05182002CertifiedCertifiedNV052CertifiedCertified
V/S:/QDate
.NEL.LABORATORIES
C L I K N l : Dumpco/Silverstate
I'RO IKCT 11): !>GH-*r-?.6V
J'KOJECT !#: PGr)-3F-;><W
MVTU1X: AQUEOUS
1' • r urn (IT
Barium
(Calcium
Iron
" '.tj'iiesMim
i'ot.iivium
v. i J i u n i
Y a n u U i u m
Antimony
Arsrnic
H c r v l l t u m
r'admium
f l i r u m i u m
Cobalt
Copper
Li-ad
-u-krl
Selenium
S.'-. tr
Thallium
Xinc
Mercury
Result
2.2
1400
220
(.90
no110(1
0.29
0.0016
0.73
0.0079
0.0018
o is0.070
0.19
O.ORO
n .wNU
ND
ND
0.75
ND
I'nil
niE/L
mg/L
me/1,
mii'i.
mg/1.
mtt !
mg/L
mg/L
mp/I.
m(j/L
mfi/L
niK/1
mg/L
mg/L
mg/1^
mjvL
mg/L
mg/I.
mg/L
rnR/L
mg/L
Reporting1. imit
0.025
2.5
050
2.5
10: s
0025
0.001Q
0.0010
O O O I O
0.0010
O O O I O
0.0010
0.0010
0.0010
G O O 10
0.00 10
O O O I O
0.00040
0.0010
0.00020
CLIENT ID;
D4.TK SAMPLED:
NEL SAMPLE U):
DF
5
5
55
5S
51il1111111II11
Method
SW6010B-To
SW 6010B-To
SW6(HOB-To
SW 60l')B-'lu
SW6010B-TO
s'A <.{)!{' '< To
SW 601 OB- To
SW 6020-Tota
SW 6020-Tota
SW f.020-Tiiu
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020 T.iu
SW 6020-Tota
SW 60?<>-Tota
SW 6020-Tota
SW 6020-Tota
SW 7470-Tota
DGH-3F-263'
.VU'O?
L0203116-001A
Prep Date
03/12/02
03/12/02
03/12/02
OJ/ 12/02
03/12/02
nvi;-o:03/12/02
03/12/02
03/17/02
01/1 2-02
03/12/02
OVP'O?
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/13/02
Analyzed
03/12/02
03/12/02
03/12/02
u i - 12/02
03/12/02nv.j'o?03/12/02
03/12/02
03/12/02
OJ/1J/02
03/12/02
03/12/0?
03/12/02
03/12/02
03/12/02
03' 12/02
03/12/02
OV12/02
03/12/02
03/12/02
03/13/02
Analyst
JTY-Reno
JTY-Reno
JTY-Rcno
J"! Y-Kcnn
JTY-Rcno
TY-Rcr.'
JTY-Rcnn
DHG-Rcno
DHG-Reno
DHG-Rcn.i
DHG-Reno
DHn-Rt-no
UHG-Reno
DHG-Reno
DHG-Reno
inr R mDHG-Reno
DHG-Rcno
DHG-Reno
DHG-Rcno
FFF-Reno
ND - Noi Detected ai the Reporting Limit
U!- - Dilution 1-acior
Date: 13-Mar-02
B - Analyte detected in the associated Method Blank
S - Spike Recovery ouliidc accepted recovery limib
E - Value above quantitation range Page 1 of 5
, - : U Y r.",. i f- i • ' _ . > . : : , _ • ' ! r - 4 • ± L
.NEL.LABORATORIES
l 1FNT:
J'KO.VKCTrf:
AQUiEOUS
e ' j lc ium
Magnesium
Sodium
Vanadium
A n t i m o n y
Beryllium
i hrcmmim
Cobalt
fm-kcl
Thallium
7ilK'
CLIENT!!): DGH-3F-263'
i)-UK SAMPLED: 3 i l ' n '
NKL SAMPLE JT>: 1,0203116-001B
Result
o.o?y57(1
NO
180
«:»
980
ND
00019
i) H)J8
ND
ND
ND
0.00130 0043
,\'O
0.0022
0.0078
ND
ND
0.046x *•
Unit
mj./L
ms/L:•"!','
me/1.
rr.K'lmR/L
mg/L
mg/L
mi} 1mg/L
mp./t
m|j,'Lmg/I^
niR/Lr,u; ,,
mg/L
mg/1,
mg/L
mg/L
mg/L, .; I
ReportingLimit
U 0050
2 5' 'if:
2 SHI
7 5
0.0050
O O O I O, , r .o ;oO O O I O
O O O I O
noo io0.0010
OOOIO
00010
O O O I O
O O O I O
0.0010
0 00040
0.0010
0 TT'»
DJb Method Prep Date
I SW6010B-D!
i SWC.OIOB-DI1 S\V f,0103 Oi
5 SW 60108-Di
i SWf,OinB-Di
5 SWoOIOB-Di1 SW6010B-Di
1 SW 6020-Diss
1 SW 6020 (•'isi
1 SW 6020-Diss
1 SW 60?0-Di«
1 SW 60?0-Diss
1 SW 6020-Diss
I SW 6020-Diss
! V.v f.0?0 Pi."
1 SW 6020-Diss
1 SW 6020-D.ss
1 SW 6020-Diss1 SW 6020-Diss
1 SW 6020-Diss, c\y ^-"i f) oim/ni
Analyzed
03/12/02
03/17/02
(.?'i?'()203/12/02
OV12TO
03/12/02
03/12/02
03/12/02
o < 12 o;03/12/02
03/12/02
03/12/02
03/12/02
03/12/02pv-i'fn
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02OV] TO?
Analyst
JTY-Reno
JTY-Rcno
1 rY Km >
JTY-Reno
JTY-Rciu)J 1'Y-Reno
JTY-Reno
DHG-Reno
DUG Ken'
DHG-Reno
DHG-Renn
DHG-Reno
DHG-RenoDHG-Renor>HP, V,,r. ,
DHG-Reno
DHG-Reno
DHG-Rtno
DHG-RenoDHG-RenoKIF »<-pn
NO • Noi Delected ai the Reporting Limit
DF - Dilution Factor
Date: Il-Mur-02
B - Analyte delected in the aiiocntcd Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quiinnlalion range Page 2 of 5
.NEl.LABUHAIORitS
^ 1 Ib.M
PROJECT in:PROJECTS:H< \ i i-M V
PGH-?F-?6V
CI.IF.NT ID. DGH-3F-263'
DATE SAMPLED: 3/11 /O"!
NF( SAMPLE ID: 10203116-0010
Parameter
t I.U.riiirr l V - "v
Nitute. as N
Ukalinily, Bicarbonate (As CaCO3)
Alkalinity, Carbonate (As CaCO3)
I [ydroxuV (A< C iCOl)
VIk . , :n . lv !.,!.,! (As C j( CH)
Chi'miml Oxyjjcn Driniin'l
Ammonia ^ N
S i l l i d c
Tutal Dissolved Solids
Kesitll
1703
r,;NO
2900
640ND
ND640
61
ND
ND
5610
Unit
n^l.
• J i
ine/L
me/I.mfjl.mg/t .
mo/t
inj. 1
mK/L
mg/L
mg/L
mR/L
I irmt PF
YI 5(i;,.j * ~ *2 * 25
5v 500?SO !0
?SO 10
?10 10
2'0 .'J
10 1
030 1
0 030 1
60.0 4
Method PrcgJOale
hPA 300 0
U- \ } 0 ,
EPA JOO.O
f PA 300 0
SM2320 B
SM2320 B
SM7370 R
W.2i:'> !
SM5520 D
SM4500-NH3
SM4500-S D
SM2540 C
Analyzed
03/11/0?
( • . ; ••03/11/02
03/1 1'02
O U 11/02
03/1 1/02
01/11/02
01 i : 'n?03/12/02
03/12/02
03/12/02
03/1 1/02
Analyst
P1I-I V
!•)! : \PJJ-LV
PJJ-LV
RDA-LV
RDA-LV
RDA-I.V
Rll* I V
RDA-LV
RDA-LV
kww-i \PJJ-LV
ND - Not Delected at the Reporting Limit
DF • Dilution Factor
Date: 13-Mar-02
B - Analyle detected in the associated McLhitd Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quanttuuon range Page 3 of 5
f t . l l ' .ST-.
i'KO.IFCTf:: I 'CUJ-iF-.W
i~T..TKJVT ID: I)GH-3F-2<',y
j.) ATI! SAMPLED: 3 / ! 1 ••01
NrF.L SAMPLE 111: 1.020? 1 ! 6-001 0
'•'.irametcr•\.-ltl.M-
H: 'i/rru-
I'.rornohrn/erc
i-i'orr.ochlororriMhnne
HioinoiiichlflromiMh.inc
Bronofomi!'• : -."'.•-
J-Butanone
i.-F^lylben/cne
.,'.-L -Uulylhen^ene
icit-Burylbcnzcnc
C'irhon d'SuHidc•-, ' , . . , . > , ' , . . , ! ,
t..iiu)robenzcnc
H.loi. -ethane
.:-'. 'hlmc'.-'.l.yi v i n y l rllier
Chloroform
Chloro methane
?-rr,!rro'...:lu-v
— cltlnrnioluene
!.i:hromochloromcthanc
! ,2 l^ihromu-.S - th lurupropanc
1 ,2-Dibromoethane
Dihromo methane
1 7-nirhlon-.K-n--.-nr-
1 ,3-1 hchlornbenzrnc
1 ,4-Dichlorohenzene
I ' l -n l .m.d .Mu. i r . j iT ie ihane
1,1-Dichloroethane
1 ,2-Dichloroethane
1 .1 -Durhloroctbc-nc
v-::-l.2-D!cr. |or<)ethKne
trans-1 .2-Dichloroelhene
l .2-DiJi l . )n-pmpjr 'c
1 ,3-Dichloropropanc
2,2-Dichloropropane
1 , 1 -Dichloropropene
cii-i,3-Dicnloropropen?
trans-l,3-Dichloropropene
F'hvlhcn-/rni-
Hexachlorohutadiene
2-Hexanone
l lodomelhanc
!^piopvlr,ci,/ei,L
Hesult
Z'.'
r:nND
K'D
ND
ND
ND
ND
ND
ND
ND
ND
vnND
ND
ND
ND
ND
ND
NU
ND
N!)
ND
ND
Nf>
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NO
NDND
ND
NDNDND
Unit
w'l-•n-.'l.
1'll'f-I'C'L
I'!-/'L
Me/t,i;;'luo,'I^
Mfr'I-
Uj^/'I.
MK/Lug/L
i'".''.ug/'L
MS/LMJ-/L
MS/L-
(jg/L
MK'L
l»E'l-
Mg/L
Mf'L
Mg/LME/L
HP/I.
\i$j\.'
UK/L
M f r Lug/L
Mg/L
HK/L
jjg/'I,
ug/L
M&'Lup/L.
ug/L
"g/L
Mt'/L
Mg/L
•ie/I
ME/L
MS/L
Mg/L
H&L
ReportingLiuiii
:>5 0
50
50
5.0
50
< 0?s5.0
5.0
5.0
5.0C 0
5.0
5.0
5.0
5.0
5.0S O
5.0
5.0i 05.05.050
50
5.0
S t)
5.0
5.0
5.0•5.05.0
5.0
5,0
5.0
50
5.0
5.050
5.0
25
5.0
i o
DFi\i111!\
1
i
1
1
I
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
I
1
1
1
1
1
1
1
1
1
1
Method
:-\v---:v,(jH
swx;(.t>BSW$2t.GB
SW&760B
SWS260H
SVVX7.60U
SV.-«?f')P
SW8260B
SW82608
SVV8200H
SW8260D
SWS260B
swsroonSW826011
SW8?60R
SW87.60Q
SW8260B
SWS260B
SW8260R
SW82608
SW8260B
SW8260U
SW8260B
SW8260B
.SW8760R
SW8200H
SW8260B
SW8200B
SW8260B
SW8260B
SW8260B
SWS2(,OB
5>W8260B
SW8260B
SW8260B
SW8260B
SW82AOB
SWS^dOH
SW8260B
SW8260B
SW8260B
SWS260B
SW8260B
b'.VK2^0B
Prep Date Analyzed
r.viro203/11/0?
0.3.' !!'(!?
( U / l l / 0 2
03/1 1/0203/11/02
ni'!l'07
O.V 11/02
03/11/02
1)3/1 1/U2
03/11/02
03/11/02
m/i i 'o?03/1 1/02
03/11/02
03 /11 /02
03/1 1/02
03/1 1/02
03/11/0?
1)3/11/02
03/11/02
03/1 l ' 02
03/1 1/02
03/1 1/02
03/11/02
03/11/02
03/1 1/02
ft.TI I 'O?
03/1 1/02
03/1 1/02
03/11/02
03/11/02
03/11/02
03/11/02
03/1 1/02
03/11/02
03/1 1/02
OM1.02
03/11/02
t l i / l 1/02
03/1 1/02
03/1 1/02
03/11/02
'.;.i,' i I'D.'
Analyst
• )RM ! V
DRM-LV
DRM-LV
UKM-l-V
DRM-LV
DRM-LV
rm.M i vDRM-LV
DRM-LV
HKJ-.I-LV
DRM-LV
DRM-LV
DRM ! V
DRM-LV
DRM-l.V
DRM-I.V
DRM-LV
DRM-LV
DRM-l.V
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
HRM ! V
DRM-LV
DRM-LV
DRM-LV
IJKM-LV
DRM-LV
DRM-l.V
DRM-LV
DRM-LV
DRM-LV
DR,M-L\'
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
."iRAt 1 V
ND - Not Detected at the Reporting Limit
Ul- - Dilution t-aclor
Date: 13-Mar-Q2
B - Analyte delected in the associated Method Blank
S - Spike Recovery outside accepted recovery lunils
K - Value above quantitation range Page 4 of 5
. N i r L . L ' M S O R A I O H I i f i :
rnOJFfT ID: DGH-?F-?r.
M.\IK1\: / . V > : . » H H ; , >
Parameter
r t^-.-, ,>,il..wa^
i M f l h > l c n v cliloiiik-
-".-Mcthyl-2-pentanfne
M i n i :
N'jnmhHlcne
i.-Pr-ipylbei^rnr
. , .ci te
1.1,1,2- rctrachloroclhanc
i 1 ,? ?• i crr.K-hlarne(hane
Tcrrarrloroelhene
Toluene
} ,2."> Trichloruben/ene1 ! . , H V ".<.„..
1,1 ,1 -Tnchlorocthanc
1 1 2-rrict.lonx-thane
1 pchlnroethene
Tuchtorufluoronicihanc
1 .1 ,2-Trichlororrif!uorocthane
l J ' ' - t-hlon p i ' ip jnr
1 ,2,4- rnmelhylhenzem:
1 ,3.5-rrirrethylbenzene
Viny l acciatc
Vinyl chloride
'i-Xylene• , ,, V % ' . ,
Surr: DibromofluoromfthHnc
£urr: Toluene-d8
Surr: 4-Brumufluorobcnzene
3'
Result
M.'
1 1
NO
ND
ND
ND
N i J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NDND97.9
91 8
81 3
jjnit,ir j.M;;. 1.Mg'L
ui; 1
,'P-L
PiVL
MS: inS.iM g L
Mt','1-
W !
M;J/L,.,-T
ug/L
M6/L
ug/L
fg/L
|ig/L
M P ' L
MB/1-ng/1
JJ-^''i-
Mg/L
Mg/L
UP'!%REC%RFC%RFC
'{•'porliocf.iuiit
-^ u
-, •)25
i'G
5"
505 0S O
50
5.')
50
50
' 0
5.0
10
50
5.05.05 (1
5.0
5.050
5.0
5.0
!0
89-102
90-102
70-IOfi
DATKSAMPLFD:
NKI SAMPL.F ID-
DP Method
i ^ A s . ' r t - l
1 SW.S^.OU
1 SWh2( 00
1 S \W60H
i SWX2ci!)H
1 SW8260H_-,\\.-:(»IH
1 SW8760B
1 SWS260R
1 SW8760R
1 SW8260H
1 SW8260B
1 SV\'8?rOB
I SW8260B
! SW8260B
1 SW8260B
1 SW8260B
1 SW82COB
1 SWS7COB
1 SW8260B
1 SW8260B
1 iW»2t>OU
1 SW8260B
1 SW8260B
1 SW8260R
1 SW8260B
1 SW8260B
1 SW8260B
VI 1/02
1 ( • , ' ! > < ! 16-OlJ l f )
Prep Date Analyzed
u, . , _
03/1 1/02
cn/ii '0203/11/02
03/11/07
03/11/02
(, i . 1 .12
03/11/02
03/1 1/02
1)3/11/02
03/11/02
03/1 1/02
OJ/1 1/07
03/1 1/02
03/11/02
03/11/02
03/1 1/02
03/11/02
01/1 1'02
03/1 1/02
03/1 1/07
OJ/ 11/02
03/1 1/02
03/1 1/02
03/11/02
03/1 1/02
03/1 1/02
03/1 1/02
Analyst1 XX ' .
DRM-LV
DR.M-LV
DRM-LV
DRM-LV
DRM-LV
:)R.v vDRM-LV
DRM-l.V
DRM-LV
DRM-LVDRM-LV
PWM ! V
DRM-LV
DRM-LV
DRM-LV
DRM-LVDRM-LVDRM-1 V
DRM-LV
DRM-LV
DRM I.V
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
ND - Not Detected at Ihe Reporting Lirrut
DK - Dilution Factor
Date: 13-Mar-02
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 5 of5
NEL Laboratories, Las Vegas
CLIENT: Dumpco'SilveiMdteWork Order: L0203116Project: DGH-3?--263'
ANALYTICAL QC SUMMARY RI^'OR Y
TehiCvJ:: 3 , I \Vrn
Sample ID MB-H884
Client ID ZZZZZ
Analyte
Chloride
Nitrate, as N
Nitrite, as N
Sulfate
S.vnpTypc' .MHLK
i M t c h I D : R R X 4
Kisu l t
ND
ND
ND
ND
T
P
00
0
0
:stC ide: 300 W Units- m^/L Prop Date - i t . \l> :,J.',-)Ji: 1 . l \
Tcs'Nn E3QO \r. iy::s Dd'.e 3'11 02 ^Si-qNo £'.".>
3L SPK /alue SP.-^ Re fVa l ".RFC _•)•* l i m i t HighLirr.t PJ'D'.^i 'd1 rd. • K;'0 -/ , - '
10
10
10
10
• J>CO
' 21
i O
X
'
Qualifiers: ND - Not Delected ai the Reporting Limit
J - Analyte detected hi low quanti ' lion h'.
S - Spike Re. overy iii 5idc accepted recover limits
•i • RPD out uie acct; ted recovery irmts
Anaiy l i c! U 1 . ' td : 'he 2ij(^.'»\'it l,;v . ij Oh1)'-
•"« / i
CLIENT Dumpco/.Silvei.-'.jteWork Older: L0203116Project: DGH-3F-263'
4 r.1 < I -AAAL
r/::ovv i)
Sample ID ,MB-R6i9
Client ID ZZZZX
Analyle
Barium
Calcium
Iron
Magnesium
Potassium
Sodium
Vanadium
,p!ype. MULK
,'d. ID R_K659
R e s u l t
TestCeJL 601CSN_D t nils- wy/l.
TestNa: S\\
PQL SPK .3luc SPK At.f Val
! rep Dale
, ' ra l . i '« i - Date 3'12/"I
•7-,'ALC Lr^1. Tfiit I ipl iLirr . :
ND
ND
ND
ND
ND
ND
ND
0.0050
0.50
0.10
0.50
2.0
0.50
0.0050
-,rn
i'O!
-Aj
rncc
QualiFieri ND - Not Delected a' 'he Reporting Limit
J - Analyle .IcttcteiJ I-.-low quantit . lion l i nn
- Spike Ref overy r u ide accepted recover limits
• RPD ou'.sij<. acc,[ '-'d recovery innts
B Ar.i'ytc Jrscclt'1 m (hi a;?.1::.!!, i' M.
CLIENT: Dumpco/S.KerstafeWork Order: 1.0203116J'roject: DGH-3F-263'
Sample ID. MB-3S1 Sar.i;- Type. MBLK
Client ID: ZZZZZ B;,' h ID. R_35:
•\nalyle Rcsi.it
Barium NO
Calcium ND
Iron NJ
Magnesium ND
Potassium NO
Sodium NO
Vanadium NO
TestCode 6010W_t Unls irj'L
TestNo SW6010B
PQL S P K v j u e SPK Kef Val
0.0050
0.50
O.IO
0.50
2.0
0.50
J.0050
AN \LYT1CAL QC SI? MM ARY KEP- )RT
'IcstO.,,!?: 601t3%,V t |^
i -p D.I-.J- .312-01 i-'.'ir : >. ^..'.'.-,oD ; 1
An2 v is Dau: ^ '11/01 » " i N - > ^ ',! ' CD
; °%P.H> Lo\ v l u.til ^ I l ^ h c i i r i t K ^ ' n / ' , ,'r.l "i : \ l ' !> •'!', '!.i".' " Ci '•! ! -^
H0
mCO
li
i
lI
i
iiiii
i
Qualifiers: ND -Not Delated at the Reporting imit
J - Analyte directed bi )'iw quantitsti m lim
Spike Rcco' cry ou'.;"!e accepted fcovcry ii
RPD outFiC.- jcccp .-ii rcco-.'ery li.-'its
\ i i a ly t> : d ^ t v i i c d in I'v. -i-.sf.ijlj'j I
CLIENT: Jumpco/SiKerstale
Work Order: L0203116Project: X5H-3F-2631
Sample ID MB-R661 SarnpF^pc
ClienUD: /.ZZZZ i J . ' i n ' D -
Analyte
Antimony
Arsenic
Beryllium
Cadmium
Chromium
CobaltCopper
Lead
Nickel
Selenium
Silver
Thallium
Zinc
MHI K
K_R66I
Result
ND
NDND
NDNDNDNDNDNDNDNDNDND
TcslCfidr SOiO'A _D Units m f , < l
TestNi* S\V5li:o
PQL SPK -u.ue SPK Ril Val
00010
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I OO O O I O
00010
0.0010
0 00040
0 00)0
ANALYTICAL QC StMMAUY RE.'JRT ;
Test Co U': oO/ ,M-\ .D j^fj... „. r~
•• p Da'c ' r , i N ; •:- ,(,: , ]
JoI1S.IH L'v- 1 tmit Hs jh l i i r . i l RI'O ?..•'', ji ' !<! ' '> ' i 'Dl,. (,'- ' '] -^
i — 1
J O
m'COi
(
jiii1
Qualifiers: V «D - Not Detected at tl e Reporting Limit
' Analyle (jcfctcd (euu qua'itiwai limits
S Spike Recovery ouUhie accepted • covery I
•i RPD o'JtuV acccp'- i iecuvt'O' iu-i ib
CLIENT: 1 iumpco/Sil . muteWork Order: i 02031 16Project: r-OH-SF^oJ1
Sample ID: MB-350 Samp ; ype: MBLK
ClienUD: /ZZZZ Oauh ID R 350
Analyte R:su1'
Antimony ND
Arsenic NC
lltryllium N'D
Cadmium ND
Chromium ND
Cobalt ND
Copper Ni1
Lead NP
Nickel ND
Selenium NT)
Silver ND
1 hallium ND
Zinc ND
res'.Code 6020V\_r Ui.i ' i m;/L
PestNo S\\69:<>
i'QL S P K v a i e SPK Re, Val
O O O I O
O O O I O
O O O I O
0.0010
U0010
O O O I O
O O O I O0.0010
O O O I O
O O O I OO O O I O
O O O I OO O O I O
ANALYTICAL QC SUM^ARA MEI'.JRT
•i^irod.: h O - L VJ] Zjr—
/,.,, >„.- 3/j:,o2 ;<. , , :r. s: '.-".:. , r-V.-.: :i, Or.'. 3 / i iOZ ^ . • • N : <••:: ^
C%PJ£C L&> Liri i t ' i j'-.lj'rii! ,<l > - ' t-f '-j! ' t- !'T) .-'. l\ in yuj i ID
V
QDm•JO
Qualifiers: ND - No! DciCvted at thi Reporting L nut
I Ann!}'.;: rtjItUed txluw quantilaliuri
S - .Spike RcLOv.rv cu'i ' • scceptcd Tco-'er, I'mts
.-< VDo'jlitdi. jwccvt • rftovcr)' Irnii1^
3 Twilvl--c:.".'C'i'd ,r, ."c .•,', i . i Vn.'.!) iJ ^'lail
CLIENT: Uompco/SiUerstatcWork Order: I<i203116Project: DGH-3F-26/
SomplelD: MB-R893 .iarnpl-'pe:
CI.cntlD. ZZZZZ Bale', ID
Aialyte
Acetone
Ocnzcne
'.itomobcnzcnc
Diomochloro methane
Bromodichloromelhane
rtromoform3romome1hane
2-9ulanone
n-8ury]benzenc
sc-c-Butylbenzene
vu-Butylbenzcnc
Carbon disulfide
Carbon letrachloride
Chlorobenzene
Cnlorocthanc
?-Chloroethyl vinyl ethci
Chloroform
Chloromcthanc
2 Chlorotoluene
<t Chlorotoluene
Dibromochloromethant
'. 2-Dibromo-3-chloropii'pane
i 2-Dibromoeihane
Dibromomethane
1 2-Dichlorobenzcne
1 3-Dichlorobcnzcne
1 4-Dichlorobenzene
Dichlorodifluoromelhanc
1 1 -Dichloroeihane
! 2-Dichloroe\hane
1 l-Dichloroelhene
MBLK
R893
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
TcstCoJe. 1260_W Unib- jig/L
TesiNo SW8I60U
PQL ^PK value SPK Ref Val
25
5.0
5.0
5.0
5.0
5.0
5.0
25
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
ANALYTICAL QC SCMMA RY rJIPC :>T '
7e.,r<nK -60 W i : i
Prep Date: .\J.1 ,'"> l._ • ' • • < '(JS-:?_/. S I I H j , i' f>
\n'-iy; i ^ D:t: 3;:t-02 Scr'^o C O i r ! |; .jjI -^
%KTC towLim,. H';h;.;,™ '.?nici",V ' rPP •--:.„.! C ..i ' , X
Hg
IT.•
1
,
,;
r1
Qualifiers: ND - Not Dctrt'i'd at tin Reporting I imit
J Analyte riett 'ed bc'.n v qusntitation limits
S "-pike Recovery oiiwiJ.- accepted recovery li9. • -<?D outsicli' ...xcptcii recovery lirniLs
• A lalvu flc'.^ciic r. t'l.-1 j » r o v ) 3 ' • i Mt t luo '.dunk
CLFENT: Dtimpco/Silvsrstate
Work Order: L<.'2031]6Troject: DGH-3F-263'
Sample ID: MH-R893 Sam?1>,-c
Client ID: ZZZZZ Baler, n
Analyte
cis-1, 2-Dichluroi'thcnc
trans-l ,2-Dichloroelhcne
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1 Dichloropropcne
cis-l,3-Dichlompropcn:
trans-l ,3-Dichtnmpropenc
Elhylbenzene
Hexachlorobutadiene
2-Hexanone
lodomcthanc
Isopropylbenzene
p-lsopropyltoluene
Mcihylenc chloride
4-Methyl-2-pentanone
MTBE
Naphihalcnc
n-Propylbenzene
Styrcnc
1,1,1 ,2-Tetrachloroelhane
1 , 1 ,2,2-Tctrachlorocthanr
Tetrachloroethcne
Toluene
1,2,3-Trichlorobenzcne
1,2,4-Trichloro benzene
1,1,1-Trichloroethane
1, 1 ,2-Trichloroethane
Tnchlorocthenc
Trichlorofluoromelhanc
l,l,2-Trichlorotnfluoro(.''hane
MBLK
K893
RcciiU
ND
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
NDNDND
NDND
NDNDNDNDNDNDND
ND
ND
TcstCod;. !)260_W Units ag/L
TesiNo: SW8260B
POT O U I/ \ f« It t i CPV '7 ff \l i lrv^i- . j r lvVaiUO jrtS. ivEI X ' j j
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
25
5.0
5.05.0
5.0255.010
5.05.0
505.05.05.05.05.05.05.05.05.05.0
ANALYTICAL QC SYM MA K Y rvEPGHT ,' '"7
rest-Code: 5:2hO_V> -^
I'rcp )atc: R u n . : ) L_V().>\;Si-J_l!::.T: 1 i( " '
A-.a!;'Si» Dale- J.".l,()2 Scqs. •> f.'i48 • 'fn
i--
~3
:fjT!i/J
ii;i
I
Qualifiers: ND - Not Dctecl'-d at the <uponing Limit
J • \nalyte deleted belr>\ t|uan[itation li
v'pi^c H c i O i c r v outside ociep'.ed rt-cmcry 1-jniu
- kPD o''"iid; "i i cptjd K ;overy limits
CLIENT:Work Order:Project:
Dumpco/Sih asiateL02')3H6DGH-3F-263'
ANALYTICAL QC SUM>?,vR\ :'.1:POV.T
Sample ID: MB-R893
Client ID: ZZZZZ
Analyte
1,2,3-Tnchloropropanc
1,2,4-Trimcthylbcnzcnc
1 ,3,5-Tnmethytbcnzcnt
Vinyl acetate
Vinyl chloride
o-Xylene
m,p-Xylene
Surr. Dibromofluorometl.ane
Surr: Tolucne-d8
Surr 4-Bromofluorobsn?enc
:"3mpT>i - MBLK
Hatch 1!' R893
Result
NDNDNDNDNDNDND
49.28
45.64
38.42
icstCcide
IcstNo
I'QL
505.05.050
5 0
5.0
10
50
5.0
50
8260_W Ur.its. jig/L Prep Hate Xi;n :„ < _ \ i
SW8260B AnJ>^. . Hal- .Til 02 H'- t.O^A
SPK value S P K S c f V j l ",oR£C Lov.Lif.-i Hf^ .Lu t i i l R. ' l i Pcf \3'. : "',) -
50 0 986 3; 102 t. )
50 0 91 3 9'.i !02 ')
50 0 76.8 70 106 I, n
Qualifiers: ND - Not Delected ai the Reporting Limit
J - Analylc detected below viantitation linnls
S • SpKe Recover) outside accepted recovery l imits
R • RJ 1) outside L i '-p't-J r. ivcry limits
B - Am.ytc t^^vi.J i 'ht ,r '>t ; , t ! ' J ' ' . i hod lj'.i.
*' s'' *
CLIENT: Dumpio/SiiverstateWork Order: L0203I16Project: DGH-T-2631
ANALYTICAL QC SUMMAR\ R/' :OR
Tt-stC- k: M,K \V —i
Sample ID MB-R898
Client ID ZZZZZ
Analyte
Alkalinity, Bicarbonate (As C.CO3)
Alkalmi'y, Carbonate (As CaCO3)
Hydrox-de (As CaC03)
Alkal.mty, Total (As CaC03)
^an-pljpj MBLK Tc-it uiic \LK_W Uni's' mg/L Pfp Date '"'in If1 ' _ A l i . • 'IOV '
P./chlD ;<S98 ToiNo ^i:3208 % . lysis D v VSL02 i i,No r<-
Result ?Q1 -;?KNjlue "''K RefVal /-.libC LTV,!, rnit H.ghL i ! O'D i S a l "' R1 -v "
ND :^
ND 25
ND 2--
ND
Qualifiers: ND - No' Octet.ted at the Ropormg Limit
I • AnaK c dcUcH'd below qujrt i tat ion lim Is
S • SpiV ^ecovery ojlSKJea:c'-j-'cd reci< <~r 1 mils
K •IPu ts de 3c^,"e^ rs r > limits
Bu-
CLIENT: Dumpc. /SilvcrstateWork Order: L0203I16
Project: UGH-?r-263'
ANALYTICAL QC SUMMAVA RU OUT
Tcstf'o:;e: COD
Sample 1!) MB-R900
Client ID ZZZZZ
Analyle
Samp Type: MBLK
Bali h ID X900
Xcsult
TesK'oiie: COB
•H'-'.No: M5220 C
PQL SPK vf lue
Units: mg/L Pre-p 0:;?
A-.3V-SD.-:
3PK.RcfV.3l "IR£C -o'vl.i;nil :i.^
j ' .n ,D ;V.i-Ql '•'.-•-•N •. '•
iLiT, ' Ki'l'i '-'?: \ j! '.R?,
Chemical Onyjcn Dtr.-.aid
Qualifiers: ND -Not Selected al tt.c Report ng Limit
J - Analju iktcctcd be ow quari ' iiation limit.1'
S SoiVc K -cover/ oii '^i lc accept.-d recnvcr, l.mils
-i <PU uL-ide 3.:epte,: iccovt.! > limits
3 • -\na1yt. (ioicc;:1! r. 'Vic a-r." .ill ii \".' ' \' 9)jt >. I
CLIENT:Work Order:Project:
Sample ID: MB-359
Client ID: ZZZZZ
Analyte
Dumpco .SilverslatcL0203116DGH-3F-263'
Si inplype- MliLK Tc.nCf ie: HG_74-20_T Units: ni^i.
O u k h l D : R_:.59 TcitNo. SW7470
3 o MI It PQL SPK value SPK Ret'Vjl
ANALYTICAL
"« .1",
P.epDsti: 3/1 3/02
Aiu!j,i.-,nat." .Vi;,02
'•-.!»cC Low Lirr.il I'-:'nL!rr,i; X
QC SUM
Codk: KG
k
'!- -<','f'.'-ji
MARY
,.7-;70_T
•j i )lj SL.1^
,",\. «0 U H - 1 '
-:;,:<PD
REi'ORT ,i .j /^i «;~im
i! *~j!g
? i - n i . - • CM,, i i ^ D_;! >^
Mercury 0 00020
oo
Qualifiers: ND • Nol Dt'ected at the Rcportinp Limit
J • Analyte Ojtccted below quanti tot ion limits
S - Spike Ruin-cry oil-side accept1.! recovery Itrruis
R • K H D ou^icc accepted 'n.n-cr) i mils
B - Anaiyt': J . icc tcd i t t 'he ,iss. f.- . i1 ' .'. A'CI!'^' ' ".'.•jn'r
CLIENT:\VorkOrder:Project:
Sample ID MB-RSC
Client ID ZZZZZ
Analyte
Dumpco'3 IverslateL0203116DGH-3F-763'
1 Sun"pT>p<: MB! K Ics'Coa. \H3-N_W ' - , ( « , f-g/L
^ a ' c h i l ) R901 T -\" ^'I4"3G \V\ C
R"tjlt 'QL SPK . t'-je CIV J-f \ 'a l
AKAL\TICAL
'r< p Dote
V •> s % DJ'C Vl l /02
or s« ^ f * " \R>- '^FI.Cotlo NL'l 'MS
';> H- i M' ) i i
Ammonia, o"- N 030
Zm
1 OJ)
O5moo
Qualifiers ND • Not DcUcied at the Rcportmf ' imit
J • Analyte c.'ected bslo* juantital in limits
S - Spike R=u) cry ouNitk ^ctcpted r-coverj limits
R - RPD auU di' aLCCplcii rec i cry linuls
D - /
CLIENT: Dumpco/Sthei stateWork Order: L0203116Project: DGK-3F-7631
Sample ID MB-R879 SampT ype MBLK
Client ID: /.ZZZZ Batch 1 3 R879
Analyte P-csull
ANALV
TcstCo.i.' 3ULFJW I'.MIS ,i.g/L >>rcn '.j-i'.c
TcslN'u MJ500-S a A-Mly;-; DJ'C
!'QL SPK. value SPK. Ref Val ",tvt-X L<. ^Lim i -
riCAL QC SUMMARY UK;
T"-'Codc: SUi.rjtV
'/no: ^ '• <i')''.j
•"-t in it 'UR'. ' .W 1 J ! D ' l i l n .
^O^T
Sulfidc ND 0030
Zm
ccOID
OwU
rn00
Qualifiers: ND • Not DMrclcd at the Reporting Limit
J - Analyte detected below .juanlitauon limits
S - Sp kc Recovery ouliide accepted recovery limits
R - RI D outside- jtceplt-'d rfoscry Iirniis
8 - A'l.iKie dc:t, 'cc! in tnc S'.MIC • ' M?;!,o>, 'J .ink,
.;' : •.• ! <• f 14
CLIENT:Work Order:Project:
Dumpco/SilveistateL0203116DGH-3F-2631
ANALYTICAL QC S f M . M , V U \
'i: .-.Cut!?: H)S 'V
Sample ID
Client ID:
MB-R907
ZZZZZ
Sa-npTypc.
Bit.;. i f >
MBI K
R307
Resell
Tts tCoi-
Tcsu-'c
POL
TDSJW 'J",,tv n-:,!.
E 160.1
?P(C \ -'uc SP'< K - f Val
;-pI^e '-., ,V !._,.
Ana ' -^ ' sOo ie .Vll-02 s -, '-i 6:-:°.
'-( ' . . , ' - 1 1 H . - " - ir-it ""~)X-- ' i '•!'[)"
Total Dissolved Solids ND '.50
•m
O
HOXfTI
Qualifiers: ND - Not Due..ltd at ih: Kcponing I imit
J - Analyte deleted below qi iant i la tun hnnLs
S - S( ike Reco\er> oubide sctcpied fcoi'crj' l
R - Rl O outsins dtv.epud recovery In iti
13 -.'.rialy'i. o^ ' . ' n-J ir, '''.' J ^ • . c ^ . ^ ; • • '
1L>JU'V L A B O R A T O R I E S
Vanessa iV.diila:-'} ;f. I ;i'o( .r;»l. >;,-: } =- V4208 Aieali "Way, Ste Af /H Vtv;;--:. My ^
Certificate of Anals is
IISK Sut, minion fe: 2«K>2030578
ONK Pji.np'c m #!
Sampk'fyTf."v«np!c De^y.Sample rVirnnicTjls-
Oil>on
Date Sampled: 03/11/2002Tune Sampled.Date RecovcA- 03/12/2002
Mrfbod Hrndt Units5 1 ine'F,
J-?L_0?
Dilution DLRPrep AratyiUDate Date
OV1V7002 OVIV7007.
H: Analyzed outside of hold toneP. Preliminary resultS: Suspect result. See Cover Letter for comments.£: Analysis performed by External laboratory.
Sec External Laboratory Report attachments.
.-•bwowfr- \nm\UmHtmuntHmimmimmn Page 2 of 2
14J4 Stanislaus Street Fresno, CA 93706-1623 Phone 559-497-2888, In CA 800-877-8310 Fax 559-485-6935
mg/L: Mfflignims/Liter (ppm)mg/Kg: MJKgrams/KJlogrsan (ppm)
: Micrograras/Liter (ppb)g' MicTogrsms.'Kflograiri (ppb)
%Rec: Percent Recovered (surrogates)
PQL: Practical Qmntitation LimitDLR: Detection Limit for Reporting
•PQLxWutionND- None Detected at DLR
::EL LABOR-TORIES CHAIN OF C'JSTQG/ ? -L t'y
^'- 8 0 * o >/ jgss * Boise
rho NX » 5ac amento
las VegdS DIVISO i •-5203 Area a ". i " _ ' i . A - as </tgas Nevada 33030/02-6E-1 1010 • Per 7C" "~ 57- • a^ 253 3282
ocT?«n, / / L'-•£ tieie.
f-roio
I i
Rcquectod
Time/DateS-jmpled
-x? -jdrLjoCiia*^V. / l/i
7,f2 day 1 day _
Custom"1
Custody Seal mtact Y<
P ojs Nan e Sjr
P.
o
00
/•T
UA/ /
\>''/.*/
f FT
_L J I
i
rt« ft' OA CinVnjiVaie jl jjd
AVv .asiftWataf AC Aqjeov.5D_ ClOganc^ui ! ^ ~<
(Print) Signjrfijre)
_L_
Date/Tme J W (P' nt) D j " fie
i
ab / fyc^rS/EL La ra(o/'(«s (nc »s / r-/( dj H ' y (a*h 1 - c^of^Bmo" fltysis *or th" jsa-pi3l& ecpfved i goo^ rood 1 c-^ jy NEL Nh. isrciro^y-'1 sbe*o 'o=» c T\^q^caoqua'es? npevoiirT>eanGnvn-tr Mconure's Oustan"1 gnalu'oct^ii CoCco Muies apu ^.ssecrde Si -VEL to pe^am w t fo rons jn i ^ pi
dsfdUsIf icpsfor etlse^rpsoii dhye^n »> ^pt'h s t erjftodof-Tw se V T 2 ^Pl Qur^ Dr*-*r7's' c t"*vic*K in^-fiati*" aiecrfsa-i r ..-»»abora!o"> after 16 3C Ai!t be coneict'it-d rece t in Ihe r j' - v rh rg j Corrrn t/r n * la^ ry o 1"o fo t. Kd'v j ound tine v, i t>- cc r^a a 3 jr v. r<
ORIGir-'Al
-I 1 1
C
^3 L > " ^ 1
NEL LABORATORIESReno • Las VegasPhoenix • Boise
Las Vegas Division4208 Arcata Way, Suite A • Las Vegas, Nevada 89030
702-657-1010 • Fax: 702-657-15771-888-368-3282
Ed CarltonDumpco/Silverstate7900 Vegas Valley DriveLas Vegas, NV 89112
TEL: (702)431-3020
RE Project: DGH-3F-263'
Dear Ed Carlton:
RECEIVED ,
Order No.: L0203116
NEL Laboratories, Las Vegas received 1 sample on 3/11/02 for the analyses presented in thefollowing report.
There were no problems with the analyses and all data for associated QC met EPA or laboratoryspecifications unless noted in the Case Narrative.
If you have any questions regarding these tests results, please feel free to call.
$an Van Wagenen £H_ ,Laboratory Manager '
Certifications:ArizonaCaliforniaIdahoMontanaNevadaNew MexicoUS Army Corps of Engineers
WV
Reno Las VegasAZ0520 AZ05181707 2002Certified CertifiedCertified CertifiedNV033 NV052Certified Certified
Certified
Date
NEL LABORATORIES^
CLIENT: Dumpco/Silverstate
PROJECT ID: DGH-3F-263'
PROJECT*: DGH-3F-2631
MATRIX: AQUEOUS
Parameter
Barium
Calcium
Iron
Magnesium
Potassium
Sodium
Vanadium
Antimony
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Thallium
Zinc
Mercury
Result
2.2
1400
220690110
1100
0.29
0.0016
0.23
0.0079
0.0018
0.15
0.070
0.19
0.080
0.38
NDNDND0.75
ND
Unit
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
ReportingLimit
002525
050251025
0025OOOIOOOOIOO O O I OOOOIOOOOIOO O O I OO O O I OOOOIOO O O I OO O O I OOOOIO0 00040O O O I O
0 00020
CLIENT ID:
DATE SAMPLED
NEL SAMPLE ID:
DF
555555511111111111111
Method
SW6010B-To
SW6010B-TO
SW6010B-To
SW 6010B-To
SW6010B-To
SW6010B-To
SW6010B-To
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 7470-Tota
DGH-3F-263'
: 3/11/02
: L0203116-001A
Prep Date
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/13/02
Analyzed
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/13/02
Analyst
JTY-Reno
JTY-Reno
JTY-Reno
JTY-Reno
JTY-Reno
JTY-Reno
JTY-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
FIF-Reno
ND - Not Detected at the Reporting Limit
DF - Dilution Factor
Date: 13-Mar-02
B - Analyte detected m the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 1 of 5
NEL LABORATORIES•*
CLIENT: Dumpco/Silverstate
PROJECT ID: DGH-3F-2631
PROJECT #: DGH-3F-2631
MATRIX: AQUEOUS
Parameter
Barium
Calcium
Iron
Magnesium
Potassium
Sodium
Vanadium
Antimony
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Thallium
Zinc
Mercury
Result
0.029
570
ND18050
980
ND0.0019
0.0018
NDNDND
0.0013
0.0043
ND0.0022
0.0078
NDND
0.046
ND
Unit
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
ReportingLimit
0005025
0102 5
10
25
00050OOOIOO O O I OO O O I OO O O I OOOOIOOOOIOO O O I OOOOIOOOOIOOOOIOOOOIO0 00040OOOIO
0 00020
CLIENT ID: DGH-3F-2631 ^
DATE SAMPLED: 3/11/02
NEL SAMPLE ID: L0203116-001B
DF
l51
5
55111111111111111
Method Prep Date
SW6010B-D1
SW 60108-Di
SW6010B-Di
SW 6010B-Di
SW6010B-Di
SW 6010B-Di
SW 60108-Di
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW7470-Diss 03/13/02
Analyzed
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/12/02
03/13/02
Analyst
JTY-Reno
JTY-Reno
JTY-Reno
JTY-Reno
JTY-Reno
JTY-Reno
JTY-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
FIF-Reno
ND - Not Detecied at the Reporting Limit
DF - Dilution Factor
Date: 13-Mar-02
B - Analyte detected m the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 2 of5
NEL LABORATORIES
CLIENT:
PROJECT ID:
PROJECT*:
MATRIX:
Dumpco/Silverstate
DGH-3F-263'
DGH-3F-2631
AQUEOUS
CLIENT ID: DGH-3F-263'
DATE SAMPLED: 3/11/02
NEL SAMPLE ID: L0203116-001C
ReportingParameter Result Unit Limit DF Method
Chloride 1200 mg/L 50 500 EPA 300 0
Nitrate, as N ND mg/L 25 25 EPA 3000
Nitrite, asN ND mg/L 25 25 EPA 3000
Sulfate 2900 mg/L 50 500 EPA 3000
Alkalinity, Bicarbonate (As CaCO3) 640 mg/L 250 10 SM2320B
Alkalinity, Carbonate (As CaC03) ND mg/L 250 10 SM2320B
Hydroxide (As CaCO3) ND mg/L 250 10 SM2320 B
Alkalinity, Total (As CaCOS) 640 mg/L 250 10 SM2320 B
Chemical Oxygen Demand 61 mg/L 10 1 SM5520 D
Ammonia, as N ND mg/L 030 1 SM4500-NH3
Sulfide ND mg/L 0 030 1 SM4500-S D
Total Dissolved Solids 5610 mg/L 600 4 SM2540 C
Prep Date Analyzed
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/12/02
03/12/02
03/12/02
03/11/02
ND - Not Detected at the Reporting Limit
DF - Dilution Factor
Date: 13-Mar-02
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 3 of 5
NEL LABORATORIES«.
CLIENT: Dumpco/Silverstate
PROJECT ID: DGH-3F-263'
PROJECT #: DGH-3F-2631
MATRIX: AQUEOUS
ParameterAcetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachlonde
Chlorobenzene
Chloroethane
2-CWoroethyl vinyl ether
Chloroform
Chlnrnmethane
2-Chlorotoluene
4-Chlorotoluene
Dibromocbloromethane
1 ,2-Dibromo-3-chloropropane
1 ,2-Dibromoethane
Dibromomethane
1 ,2-Di chlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifluoromethane
1 , 1 -Dichloroethane
1 ,2-Dichloroethane
1 ,1 -Dichloroethene
cis-1 ,2-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
1 ,3-Dichloropropane
2,2-Dichloropropane
1 , 1 -Dichloropropene
cis-l,3-Dichloropropene
trans-1 ,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
2-Hexanone
lodomethane
Isopropylbenzene
ND - Not Detected at the Reporting Limit
DF - Dilution Factor
Date: 13-Mar-02
Result Unit
29 fig/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ReportingLimit
2550505050505025505050505050505050505050505050505050505050505050505050505050505050255050
B - Analyte detected
CLIENT ID: DGH-3F-2631
DATE SAMPLED: 3/11/02
NEL SAMPLE ID: L0203116-001D
DF Method Prep Date Analyzed
lllllllllllll1llllllllllllllllllllllllllllll
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/1 1/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02--
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/02
Analyst
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 4 of 5
NEL LABORATORIES4
CLIENT: Dumpco/Silverstate
PROJECT ID: DGH-3F-263'
PROJECT #: DGH-3F-2631
MATRIX: AQUEOUS
Parameterp-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone
MTBENaphthalenen-Propylbenzene
Styrene1 ,1 ,1 ,2-Tetrachloroethane
1 ,1 ,2,2-Tetrachloroethane
Tetrachloroethene
Toluene1 ,2,3-Tnchlorobenzene
1 ,2,4-Tnchlorobenzene
1 ,1 ,1-Tnchloroethane
1,1,2-Tnchloroethane
TnchloroetheneTnchlorofluorome thane
1 1 2-Tnchlorotnfluoroethane
1,2,3-Tnchloropropane1 ,2,4-Tnmethylbenzene
1 ,3 ,5-Tnmethylbenzene
Vinyl acetateVinyl chloride
o-Xylene
m,p-XyleneSurr: Dibromofluoromethane
Surr: Toluene-d8
Surr: 4-Bromofluorobenzene
ResultND
17
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND97.9
91.8
81.3
Unit
Mg/Lug/L
Hg/L
ug/L
Mg/LMg/LUg/L
Mg/Lug/Lug/Lug/Lug/Lug/L
ug/Lug/Lug/L
Mg/Lug/L
Mg/Lug/LMg/Lug/L
Mg/LMg/LMg/L%REC%REC%KEC
ReportingLimit
50502550505050505050505050505050505050505050505010
89-102
90-102
70-106
CLIENT ID: DGH-3F-263'
DATE SAMPLED: 3/11/02
NEL SAMPLE ID: L0203116-001D
DF Method
1 SW8260B
1 SW8260B
1 SW8260B1 SW8260B
1 SW8260B1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B1 SW8260B
1 SW8260B1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B1 SW8260B
1 SW8260B1 SW8260B
1 SW8260B1 SW8260B1 SW8260B
1 SW8260B1 SW8260B
1 SW8260B
Prep Date Analyzed
03/11/0203/11/02
03/11/02
03/11/0203/11/02
03/11/0203/11/02
03/11/02
03/11/0203/11/02
03/11/02
03/11/0203/11/02
03/11/02
03/11/02
03/11/02
03/11/02
03/11/0203/11/02
03/11/0203/11/0203/11/02
03/11/0203/11/02
03/11/02
03/11/0203/11/02
03/11/02
AnalystDRM-LV
DRM-LVDRM-LV
DRM-LV
DRM-LVDRM-LV
DRM-LV
DRM-LVDRM-LV
DRM-LVDRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LVDRM-LV
DRM-LV
DRM-LVDRM-LV
DRM-LVDRM-LVDRM-LV
DRM-LVDRM-LV
DRM-LV
DRM-LVDRM-LV
DRM-LV
ND - Not Detected at the Reporting Limit
DF - Dilution Factor
Date: 13-Mar~02
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 5 of5
NEL Laboratories, Las Vegas Date: 13-hfar-02
CLIENT:Work Order:Project:
Dumpco/SilverstateL0203116DGH-3F-263'
ANALYTICAL QC SUMMARY REPORT
TestCode: 300 W
Sample ID MB-R884
Client ID ZZZZZ
Analyte
Chloride
Nitrate, as N
Nitrite, as NSulfate
SampType MBLK
Batch ID R884
Result
NDNDNDND
TestCode 300_W Units mgO.
TestNo E300
PQL SPK value SPK Ref Val
0 100 100 100 10
Prep Date Run ID LJC-1_02031 1A
Analysis Date 3/11/02 SeqNo 5996
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
1
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte detected below quantitation limits
S - Spike Recovery outs de accepted recovery limits
R - RPD outside accepted recovery limits
~TB - Analyte detected in the associated Method Blank
Page J of 14
— t -
CLIENT:Work Order:Project:
Dumpco/SilverstateL0203116DGH-3F-263'
ANALYTICAL QC SUMMARY REPORTi
TestCode: 6010W D
Sample ID MB-R659
Client ID ZZZZZ
Analyte
SampType MBLK
Batch ID R_R659
Result
TestCode 6010W_D Units mg'L
TestNo SW6010B
PQL SPK value SPK Ref Val
Prep Date
Analysis Date 3/12/02
%REC LowLimit HighLimit RPD Ref Val
Run ID SUB-659
SeqNo 6434
%RPD RPDLimit Qual
m
COO3D
§gomCO
Barium
Calcium
Iron
Magnesium
Potassium
SodiumVanadium
NDND
NDNDNDNDND
00050
0500 100502 0
05000050
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte detected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepts d recovery limits
B - Analyte detected in the associate^ Method Blank
Page 2 of 14
CLIENT: Dumpco/SilverstateWork Order: L0203116Project: DGH-3F-263'
Sample ID: MB-351 SampType:
Client ID: ZZZZZ Batch ID:
Analyte
Barium
Calcium
Iron
Magnesium
PotassiumSodium
Vanadium
MBLK
R_351
Result
NDNDNDNDNDNDND
*
ANALYTICAL QC SUMMARY REPORT
TestCode: 6010WJ
TestCode: 6010W_t Units: mg'L Prep Date: 3/12/02 Run ID: SUB-6^0
TestNo: SW6010B Analysis Date: 3/12/02 SeqNo: 6438 '1
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
0.0050
0.500.100.50
2.00.50
0.0050
T]
\BO
RA
TOR
mCO
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte detected below quantitation limits
S - Spike Recovery outsi de accepted recovery limits
R - RPD outside accepted recovery limits
B - Analyte detected in the associated Method Blank
! Page 3 of 14
11CLIENT: Dumpco/SilverstateWork Order: L0203116Project: DGII-3F-263'
Sample ID MB-R661 SampType
Client ID ZZZZZ Batch ID
Analyte
Antimony
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
CopperLead
Nickel
Selenium
Sliver
ThalliumZinc
MBLK
R_R661
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
NDNDNDND
ANALYTICAL QC SUMMARY REPORT
TestCode: 6020W_D
TestCode 6020WJO Units mg/L Prep Date Run ID SUB-661
TestNo SW6020 Analysis Date 3/12/02 SeqNo 6445
PQL SPK value SPK Ref Val %REC LowLirmt HighLimit RPD Ref Val %RPD RPDLimit Qual
O O O I O '
O O O I O
O O O I O
O O O I O j
O O O I O
OOOIO 1
O O O I O '
O O O I O
O O O I O 1
O O O I O
O O O I O
0 00040
O O O I O
JJ
—00oID
o2mCO
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte detected below quantitation limits
S - Spike Recovery outs de accepted recovery limits
R - RPD outside accepted recovery limits
B - Analyte detected in the associated Method Blank
1 Page 4 of 14
i ^
CLIENT: Dumpco/SilverstateWork Order: L0203116Project: DGH-3F-263'
Sample ID: MB-350 SampType.
Client ID: ZZZZZ Batch ID:
Analyte
Antimony
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Thallium
Zinc
MBLK
R_350
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ANALYTICAL QC SUMMARY JREPORT
TestCode: 6020WJT
TestCode: 6020W_T Units' mg/L Prep Date: 3/12/02 Run ID: SUB-6J56
TestNo: SW6020 Analysis Date: 3/12/02 SeqNo: 6424 i
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
0.0010 1
O O O I O
0.0010
0.0010
0.0010
0.0010 ,
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
0.0010
'
mr~r~\B
OR
ATC
IDmCO
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte detected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
B - Analyte detected in the associated Method Blank
Page 5 of 14
i
CLIENT: Dumpco/Silveistate
Work Order: L0203116Project: DGH-3F-263'
Sample ID MB-R893 SampType
Client ID ZZZZZ Batch ID
Analyte
Acetone
Benzene
Bromobenzene
BromochlofomethaneBromodichloromethane
Bromoform
Bromomethane
2-Butanone
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachlonde
Chlorobenzene
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochlorome thane
1 ,2-Dibromo-3-chloropropane
1 ,2-Dibromoethane
Dibromome thane
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-DichlorobenzeneDichlorodifluoromethane
1,1-Dichloroethane
1 ,2-Dichloroethane
1,1-Dichloroethene
MBLK
R893
Result
NDNDNDNDNDNDNDNDND
NDNDNDNDNDNDNDNDNDNDNDNDND
NDND
NDNDNDNDNDNDND
ANALYTICAL QC SUMMARY (REPORT
TestCode: 8260_W
TestCode 8260_W Units (ig/L Prep Date Run ID L_VOAMS-2_0203 11 B
TestNo SW8260B Analysis Date 3/11/02 SeqNo 6048
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
25 i5050505050502550
5050 ,505050 ,5050505050
505050
505050505050
505050
—7^JEL LABORATOR
mCO
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte detected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepte i recovery limits
B - Analyte detected in the associated Method Blank
Page 6 of 14
CLIENT: Dumpco/SilverstateWork Order: L0203116Project: DGH-3F-263'
Sample ID MB-R893 SampType
Client ID ZZZZZ Batch ID
Analyte
cis-l,2-Dichloroethenetrans-1 ,2 -Dichloroethene1 ,2-DichIoropropane1 ,3-Dichloropropane2,2-Dichloropropane1 , 1 -Dichloropropenecis-1 ,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzeneHexachlorobutadiene2-Hexanonelodome thaneIsopropylbenzenep-Isopropyltoluene
Methylene chloride4-Methyl-2-pentanoneMTBENaphthalenen-PropylbenzeneStyrene1,1,1 ,2-Tetrachloroethane
1,1 ,2,2-TetrachloroethaneTetrachloroe thene
Toluene
1 ,2,3-Tnchlorobenzene
1 ,2,4-Tnchlorobenzene1,1,1 -Tnchloroethane1 ,1 ,2-TnchloroethaneTnchloroe theneTnchlorofluoromethane1 ,1 ,2-Tnchlorotrifluoroethane
MBLK
R893
Result
NDNDNDND
NDNDNDNDND
NDNDNDNDND
NDNDNDNDNDNDNDND
NDND
ND
NDNDNDNDNDND
1 *
ANALYTICAL QC SUMMARY REPORTTestCode: 8260_W
TestCode 8260_W Units ug/L Prep Date Run ID L_VOAMS-2_020311B
TestNo SW8260B Analysis Date 3/11/02 SeqNo 6048
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD R|PDLimit Qual
50 '505050
50505050505025505050
50255010
505050
505050
50505050505050
— f^JEL LABORATOR
mCO
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyle detected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepts d recovery limits
B - Analyte detected in the associated Method Blank
Page 7 of 14
CLIENT:Work Order:Project:
Dumpco/Silverstate
L0203116
DGH-3F-263'
ANALYTICAL QC SUMMARY REPORT
TestCode: 8260 W
Sample ID MB-R893
Client ID ZZZZZ
Analyte
1 ,2,3-Tnchloropropane
1 ,2,4-Tnmethy Ibenzene
1 ,3,5-Tnmethylbenzene
Vinyl acetate
Vinyl chloride
o-Xylene
m,p-XyleneSurr Dibromofluoromethane
Surr Toluene-d8
Surr 4-Bromofluorobenzene
SampType MBLK
Batch ID R893
Result
ND
NDNDNDNDNDND
492845643842
TestCode
TestNo
PQL
50
505050505010
505050
8260_W Units ug/L
SW8260B
SPK value SPK Ref Val
50 0
50 050 0
Prep Date
Analysis Date 3/11/02
%REC LowLimit HighLimit RPD Ref Val
98 6 89 102 0
91 3 90 102 0768 70 106 0
Run ID L_VOAMS-2_020311B
SeqNo 6048
%RPD RPDLimit Qual
000
—00OIDH33mCO
m
Qualifiers: ND - Not Detected at the Repotting Limit
J - Analyie detected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
B - Analyte detected in the associated Method Blank
Page 8 of 14
CLIENT:Work Order:Project:
Dumpco/SilverstateL0203116DGH-3F-263'
ANALYTICAL QC SUMMARY REPORT
TestCode: ALK W m
00OID>
O
mCO
Sample ID MB-R898
Client ID ZZZZZ
Analyte
SampType MBLK
Batch ID R898
Result
TestCode ALK_W
TestNo M2320 B
Units mg/L
PQL SPK value SPK Ref Val
Prep Date
Analysis Date 3/11/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_ATITR-1_020311A
SeqNo 6076
%RPD RPDLimit Qual
Alkalinity, Bicarbonate (As CaCO3)
Alkalinity, Carbonate (As CaC03)
Hydroxide (As CaCO3)
Alkalinity, Total (As CaCO3)
NDNDNDND
25252525
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte detected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
B - Analyte detected in the associated Method Blank
Page 9 of 14
«
CLIENT: Dumpco/S.lverstate ANALYTICAL QC SUMMARY REPORTWork Order: L0203116 ^Project: DGII-3F-263' TestCode: COD
Sample ID MB-R900 SampType MBLK TestCode COD Units mg/L Prep Date Run ID L_SPEC-2_020312C
Client ID ZZZZZ Batch ID R900 TestNo M5220 C Analysis Date 3/12/02 SeqNo 6090
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Chemical Oxygen Demand ND 10
, * NEL LABORATORIES
Qualifiers: ND - Not Detected at the Reporting Limit
J - AnaJyle delected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
B - Analyte detected in the associated Method Blank
Page 10 of 14
1
CLIENT: Dumpco/SilverstateWork Order: L0203116Project: DGH-3F-263'
Sample ID MB-359 Samp Type MBLK
Client ID ZZZZZ Batch ID R_359
Analyte Result
Mercury ND
ANALYTICAL QC SUMMARY REPORTTestCode: HG_7470_T
TestCode HG_7470_T Units mg/L Prep Date 3/13/02 Run ID SUB-669
TestNo SW7470 Analysis Date 3/13/02 SeqNo 6450
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
0 00020
NEL LABORATORIES
B - Analyte detected in the associated Method Blank
Page 11 of 14
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte detected below quantitation limits
S Spike Recovery outside accepted recovery limits
R RPD outside accepted recovery limits
*
CLIENT:Work Order:Project:
Dumpco/SilverstateL0203116DGH-3F-263'
Sample ID MB-R901 SampType MBLK
Ghent ID ZZZZZ Batch ID R901
Analyte Result
ANALYTICAL QC
TestCode
SUMMARY REPORT
: NH3-N_W
TestCode NH3-N_W Units mg/L Prep Date Run ID L_WC_020312B
TestNo M4500-NH3 C Analysis Date 3/12/02 SeqNo 6099
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLmiit Qua!
Ammonia, as N ND 030
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte delected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside acceptc d recovery limits
B - Analyte detected in the associated Method Blank
Page 12 of 14
1 *
CLIENT: Dumpco/SilverstateWork Order: L0203116Project: DGH-3F-263'
Sample ID MB-R879 SampType MBLK
Client ID ZZZZZ Batch ID R879
Analyte Result
Sulfide ND
ANALYTICAL QC SUMMARY REPORT
TestCode: SULF_W
TestCode SULF_W Units mg'L Prep Date Run ID L_SP$C-2_020312A
TestNo M4500-SD Analysis Date 3/12/02 SeqNo 5960 '
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
0030
,. y
NEL LABORATORIES
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte detected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
B - Anatyte detected in the associated Method Blank
Page 1 3 o f l 4
1
CLIENT: Dumpco/SilverstateWork Order: L0203116Project: DGH-3F-263'
Sample ID MB-R907 SampType MBLK
Client ID ZZZZZ Batch ID R907
Analyte Result
Total Dissolved Solids ND
ANALYTICAL QC SUMMARY REPORT
TestCode: TDSJW
TestCode TDS_W Units mg/L Prep Date Run ID L_WC_020311D
TestNo E1601 Analysis Date 3/11/02 SeqNo 6140
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
150
c
v NEL LABORATORIES
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte detected below quantitation limits
S - Spike Recovery outs de accepted recovery limits
R - RPD outside accepted recovery limits
B - Analyte detected in the associated Method Blank
Page 14 of 14
03/15/2002 FRI 9:46 FAX 559 485 6935 BSK LABS ©002/002
BSK A N A L Y T I C A LLABORATORIES
Vanessa PadillaNEL Laboratories Las Vegas4208 Arcata Way, Ste ALas Vegas, NV 89030
BSK Submission #: 2002030578BSK Sample ID& 189784PiojectID: L0203116
Submission Comments:
Certificate of AnalysisELAP Certificate #1180
Report Issue Date: 03/15/2002
Project Desc: Dumpco
Sample Type: Liquid Date Sampled: 03/11/2002Sample Description: DGH-3F-263 Tune Sampled:Sample Comments: Date Received: 03/12/2002
Inorganics
AnalyteDissolved Organic Carbon (DOC)
Prep AnalysisMethod Result Units PQL Dilution DLR Date DateSM5310-D 5.3 mg/L 0.2 5 1.0 03/13/2002 03/13/2002
mg/L: Milligrams/Liter (ppm)mg/Kg: Milligrams/Kilogram (ppm)Ug/L: Micrograms/Liter (ppb)ug/Kg: Micrograms/Kilogram (ppb)%Rec: Percent Recovered (surrogates)
PQL: Practical Quantitation LimitDLR: Detection Limit for Reporting
: PQL x DilutionND: None Detected at DLR
H: Analyzed outside of hold timeP: Preliminary resultS: Suspect result See Cover Letter for comments.E: Analysis performed by External laboratory.
See External Laboratory Report attachments.
Page 2 of21414 Stanislaus Street Fresno, CA 93706-1623 Phone 559-497-2888, In CA 800-877-8310 Fax 559-485-6935
NEL LABORATORIES CHAIN OF CUSTODY NEL Work Order:Reno • Las Vegas • Boise
Phoenix • Sacramento
'urchase Order NumberLas Vegas Division • 4208 Arcata Way, Suite A • Las Vegas, Nevada 89030
702-657-1010 • Fax: 702-657-1577 • 888-368-3282
Requested Turnaround:
Time/DateSampled
N.E.LIdentificationCustomer Sample Identification
Custody Seal intactCon-
E Ice OnlyF OtherG Not Preserved
DW • Drinking WaterWW • Waste WaterOL - Oil/Organic Liquid
SD • SolidAQ • AqueousA-A i r
The liability of NEL Laboratories Ino is limited strictly to the price of sample analysis for those samples received in good condition by NEL NEL is not responsible for loss, damage, resampling costs and/or qualified data related to samples not received in good condition,including adequate sample volume and number of containers Customer signature of this CoC constitutes a purchase order for NEL to perform work and constitutes acceptance of all NEL Standard Terms and Conditions Signature also constitutes acceptanceof NEL Standard Ust Prices lor all services ordered here on, except those specified otherwise via an NEL Quotation for Testing Servic es in effect at the time of sample receipt NEL turnaround times are measured in regular working days Samples received a\ \helaboratory after 16 30 will be considered received on the next working day Commitment of laboratory to the requested turnaround time will be confirmed via Sample Confirmation transmitted to the fax number provided aboye
ORIfSINAI !
NEL LABORATORIESReno • Las VegasPhoenix • Boise
ILas Vegas Division
4208 Arcata Way, Suite A • Las Vegas, Nevada 89030702-657-1010 • Fax: 702-657-1577
1-888-368-3282
Ed CarltonDumpco/Silverstate7900 Vegas Valley DriveLas Vegas, NV 89112
TEL: (702)431-3020
RE Project: RGH-3F-2631
Dear Ed Carlton:
RECEIVED
Order No.: L0203117
NEL Laboratories, Las Vegas received 2 samples on 3/11/02 for the analyses presented in thefollowing report.
There were no problems with the analyses and all data for associated QC met EPA or laboratoryspecifications unless noted in the Case Narrative.
If you have any questions regarding these tests results, please feel free to call.
St^n Van Wagenen jf^- -*Laboratory Manager
Certifications:ArizonaCaliforniaIdahoMontanaNevadaNew MexicoUS Army Corps of Engineers
iW
Reno Las VegasAZ0520 AZ05181707 2002Certified CertifiedCertified CertifiedNV033 NV052Certified Certified
Certified
Date
NEL Laboratories, Las Vegas Date: 26-Mar-02
CLIENT: Dumpco/SilverstateProject: RGH-3F-263' CASE NARRATIVELab Order: L0203117
Attached are the analytical results for samples in support of the above referenced project.
The samples submitted for this project were not sampled by NEL. Should you have any questions orcomments, please feel free to contact our Client Services Department.
Analytical Comments:
EPA 8260: Samples were evaluated for the presence of Acrylonitrile and l,4-Dichloro-2-Butene.None of these analytes were present in the samples submitted in this work order at or above 5ppb.
Page 1 of 1
CLIENT: Dumpco/Silverstate
PROJECT ID: RGH-3F-2631
PROJECT #: RGH-3F-263'
MATRIX: AQUEOUS
ParameterBarium
Calcium
Iron
MagnesiumPotassiumSodiumVanadiumAntimonyArsenic
Beryllium
Cadmium
Chromium
Cobalt
CopperLead
Nickel
SeleniumSilverThalliumZincMercury
Result
NDNDNDNDND0.55NDNDNDNDNDNDNDNDND
0.0015NDNDND
0.0068ND
Unitmg/L
mg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L
ReportingLimit0005005001005020050
0.00500.00100.00100.0010O O O I O0.00100.00100.0010O O O I O0.00100.00100.0010
0.000400.00100.00020
CLIENT ID:
DATE SAMPLED:
NEL SAMPLE ID:
DF Method
1 SW6010B-To1 SW6010B-To1 SW6010B-To1 SW6010B-TO1 SW6010B-To1 SW6010B-TO1 SW6010B-TO1 SW 6020-Tota1 SW 6020-Tota1 SW 6020-Tota1 SW 6020-Tota1 SW 6020-Tota1 SW 6020-Tota1 SW 6020-Tota1 SW 6020-Tota1 SW 6020-Tota1 SW 6020-Tota1 SW 6020-Tota1 SW 6020-Tota1 SW 6020-Tota1 SW 7470-Tota
RGH-3F-263'-M
; 3/11/02
L0203117-001A
Prep Date03/12/0203/12/0203/12/0203/12/0203/12/0203/12/0203/12/0203/19/0203/19/0203/19/0203/19/0203/19/0203/19/0203/19/0203/19/0203/19/0203/19/0203/19/0203/19/0203/19/0203/19/02
Analyzed03/13/0203/13/0203/13/0203/13/0203/13/0203/13/0203/13/0203/20/0203/20/0203/20/0203/20/0203/20/0203/20/0203/20/0203/20/0203/20/0203/20/0203/20/0203/20/0203/20/0203/19/02
Analyst
FIF-RenoFIF-RenoFIF-RenoFIF-RenoFIF-RenoFIF-RenoFIF-RenoDHG-RenoDHG-RenoDHG-RenoDHG-RenoDHG-Reno
DHG-Reno
DHG-RenoDHG-RenoDHG-RenoDHG-RenoDHG-RenoDHG-RenoDHG-RenoJTY-Reno
ND - Not Detected at the Reporting Limit
DF - Dilution Factor
Date: 26-Mar-02
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 1 of 6
CLIENT: Dumpco/Silverstate
PROJECT ID: RGH-3F-2631
PROJECT*: RGH-3F-2631
MATRIX: AQUEOUS
Parameter Result Unit
\cetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
n-Butylbenzene
bec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachlonde
Chlorobenzene
Chloroe thane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1 ,2-Dibromo-3-chloropropane
1 ,2-Dibromoethane
Dibromomethane
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1 ,2-Dichloroe thane
1,1-Dichloroethene
cis-1 ,2-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
1 ,3-Dichloropropane
2,2-Dichloropropane
1 ,1 -DiUiloropropene
cib-1 ,3-Dichloropropene
tranb-1 ,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
2-Hexanone
lodome thane
Isopropylbenzene
ND - Not Detected at the Reporting Limit
DF - Dilution Factor
Date: 26-Mar-02
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ReportingLimit
255050505050502550505050505050505050505050505050505050505050505050505050505050505.0255050
CLLENTLD: RGH-3F-2631
DATE SAMPLED: 3/11/02
NEL SAMPLE ID: L02031 17-001B
DF Method Prep Date Analyzed
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
I SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
Analyst
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
B - Analyte detected m the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 2 of 6
CLIENT: Dumpco/Silverstate
PROJECT ID: RGH-3F-2631
PROJECT #: RGH-3F-263'
MATRIX: AQUEOUS
Parameter
p-lsopropyltoluene
Methylene chlonde
4-Methyl-2-pentanone
MTBE
Naphthalene
n-Propylbenzene
Styrene
1,1,1 ,2-Tetrachloroethane
1 , 1 ,2,2-Tetrachloroetnane
Tetrachloroethene
Toluene
1 ,2,3-Tnchlorobenzene
1 ,2,4-Tnchlorobenzene
1,1,1-Tnchloroethane
1 , 1 ,2-Tnchloroethane
Tnchloroethene
Tnchlorofluoromethane
1 , 1 ,2-Tnchlorotnfluoroethane
1 ,2,3-Tnchloropropane
1 ,2,4-Tnmethylbenzene
1 ,3 ,5-Tnmethylbenzene
Vmyl acetate
Vinyl chlonde
o-Xylene
m,p-Xylene
Surr: Dibromofluoromethane
Surr: Toluene-d8
Surr: 4-Bromofluorobenzene
Result
NDNDNDNDNDNDNDND
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND10298.0
95.7
Unit
ug/L
ug/L
ug/L
ug/L
ug/L
Ug/L
ug/L
ug/L
ug/L
ug/L
Ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
ReportingLimit
5050255050505.0505.050505050505.0505.05.05.0505.05.05.05010
808-119
848-102
562-139
CLIENT ID: RGH-3F-263'
DATE SAMPLED: 3/11/02
NEL SAMPLE LD: L02031 17-001B
DF Method
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
Prep Date Analyzed
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
Analyst
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
ND - Not Detected at the Reporting Limit
DF - Dilution Factor
Date: 26-Mar-02
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 3 of 6
CLIENT:
PROJECT ID:
PROJECT #:
MATRIX:
Dumpco/Silverstate
RGH-3F-2631
RGH-3F-2631
AQUEOUS
CLIENT LD: RGH-3F-263'
DATE SAMPLED: 3/11/02
NEL SAMPLE ID: L0203117-001C
ReportingParameter Result Unit Limit DF Method Prep Date Analyzed
Chloride ND mg/L 0.10 1 EPA 300.0 03/11/02
Nitrate, as N ND mg/L 0.10 1 EPA 300.0 03/11/02
Nitrite, as N ND mg/L 0.10 1 EPA 300.0 03/11/02
Sulfate ND mg/L 0.10 1 EPA 300.0 03/11/02
Alkalinity, Bicarbonate (As CaC03) ND mg/L 25 1 SM2320 B 03/11/02
Alkalinity, Carbonate (As CaC03) ND mg/L 25 1 SM2320 B 03/11/02
Hydroxide (As CaC03) ND mg/L 25 1 SM2320 B 03/11/02
Alkalinity, Total (As CaC03) ND mg/L 25 1 SM2320 B 03/11/02
Chemical Oxygen Demand 15 mg/L 10 1 SM5520D 03/12/02
Ammonia, as N ND mg/L 0.30 1 SM4500-NH3 03/12/02
Sulfide ND mg/L 0.030 1 SM4500-S D 03/12/02
Total Dissolved Solids 16.0 mg/L 15.0 1 SM2540 C 03/11/02
ND - Not Detected at the Reporting Limit
DF - Dilution Factor
Date: 26-Mar-02
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 4 of 6
FCLIENT: Dumpco/Silverstate
PROJECT ID: RGH-3F-263'
PROJECT #: RGH-3F-2631
MATRIX: AQUEOUS
ParameterAcetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachlonde
Chlorobenzene
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1 ,2-Dibromo-3-chloropropane
1 ,2-Dibromoethane
Dibromome thane
1 ,2-Dichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1 ,2-Dichloroethane
1,1-Dichloroethene
cis-1 ,2-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
1 ,3-Dichloropropane
2 ,2-Dichloropropane
1 ,1 -Dichloropropene
cii-1 ,3-Dichloropropene
trans- 1 ,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
2-Hexanone
lodomethane
Isopropylbenzene
ND - Not Detected at the Reporting
DF - Dilution Factor
Date: 26-Mar-02
Result
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
Limit
Unit
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Ug/L
Ug/L
Ug/L
Ug/L
ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
ReportingLimit
2550
5.0505.0505.0255.05.05.05.05.05.05.05.0505.0505.05.05.0505.05.0505.05.05.05.05.05.05.05.05.0505.05.05.05.05.0255.05.0
CLIENT ID: XGH-3F-2631
DATE SAMPLED: 3/11/02
NEL SAMPLE ID: L0203117-002A
DF
lll111111111l11111111111l1l11111111l11111111
Method Prep Date
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
Analyzed
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
Analyst
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 5 of 6
•ACLIENT: Dumpco/Silverstate
PROJECT ID: RGH-3F-2631
PROJECT #: RGH-3F-2631
MATRIX: AQUEOUS
Parameter
p-Isopropyltoluene
Methylene chlonde
4-Methyl-2-pentanone
MTBE
Naphthalene
n-Propylbenzene
Styrene
1,1,1 ,2-Tetrachloroethane
1,1,2 ,2-Tetrachloroethane
Tetrachloroethene
Toluene
1 ,2,3-Tnchlorobenzene
1 ,2,4-Tnchlorobenzene
1,1,1-Tnchloroethane
1,1,2-Tnchloroethane
Tnchloroethene
Tnchlorofluoromethane
1 , 1 ,2-Tnchlorotnfluoroethane
1 ,2,3-Tnchloropropane
1 ,2,4-Tnmethylbenzene
1 ,3,5-Tnmethylbenzene
Vinyl acetate
Vinyl chloride
o-Xylene
m,p-Xylene
Surr: Dibromofluoromethane
Surr: Toluene-d8
Surr: 4-Bromofluorobenzene
Result
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND10399.2
99.0
Unit
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L
Ug/L%REC
%REC
%REC
ReportingLimit
5.050255.05.05.0505.05.05.05.050505.05.05.05.05.05.05.05.05.05.05.010
808-119
84.8-102
562-139
CLIENT ID: XGH-3F-263'
DATE SAMPLED: 3/11/02
NEL SAMPLE ID: L02031 17-002A
DF Method
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
Prep Date Analyzed
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
03/23/02
Analyst
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
SKV-LV
ND - Not Detected at the Reporting Limit
DF - Dilution Factor
Date: 26-Mar-02
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 6 of 6
BSK A N A L Y T I C A LLABORATORIES
Vanessa Padilla Certificate of AnalysisNEL Laboratories Las Vegas ELAP Certificate #11804208 Arcata Way, Ste A Report issue Date: 03/15/2002Las Vegas, NV 89030
BSK Submission #: 2002030580BSK Sample ID #: 189799Project ID L0203117 Project Desc Dumpco
Submission Comments
Sample Type- Liquid
Sample Description. RGH-3F-263
Sample Comments.
Inorganics
Analyte MethodDissolved Organic Carbon (DOC) SM 53 10-D
Date Sampled: 03/11/2002
Time Sampled 0700
Date Received: 03/12/2002
Prep AnalysisResult Units PQL Dilution DLR Date Date
0.50 mg/L 0.2 1 0.2 03/13/200203/13/2002
mg/L Milligrams/Liter (ppm) PQL: Practical Quantitation Limit H: Analyzed outside of hold timemg/Kg Milligrams/Kilogram (ppm) DLR: Detection Limit for Reporting P: Preliminary resultug/L Micrograms/Liter (ppb) : PQL x Dilution S: Suspect result. See Cover Letter for comments
ug/Kg Micrograms/Kilogram (ppb) ND: None Detected at DLR E: Analysis performed by External laboratory%Rec Percent Recovered (surrogates) See External Laboratory Report attachments
Report Authentication Code. I HUH Hill HI) [HIM 111 111 Page 1 of 1
1414 Stanislaus Street Fresno, CA 93706-1623 Phone 559-497-2888, In CA 800-877-8310 Fax 559-485-6935
CLIENT:Work Order:Project:
Dumpco/Silverstate
L0203117RGH-3F-263'
ANALYTICAL QC SUMMARY REPORTTestCode: 300 W
Sample ID L0203 11 7-001 CMS SampType MS TestCode 300_W Units mg/L Prep Date Run ID L_IC-1_020311 A
Client ID RGH-3F-263' Batch ID R884 TestNo E300 Analysis Date 3/11/02 SeqNo 5999
Analyte
Nitrite, as N
Sulfate
Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
0937 010 1 0 937 80 120 0 00855 010 1 0 855 80 120 0 0
Qualifiers: ND - Not Detected at the Reporting Limit
J Analyte detected be/ow quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
B - Analyte detected in the associated Method Blank
Page 2 of 16
NEL Laboratories, Las Vegas Date: 26-Mai-02
CLIENT: Dumpco/SilverstateWork Order: L0203117
ANALYTICAL QC SUMMARY REPORT
Project: RGH-3F-263'
Sample ID MB-R884
Client ID ZZZZZ
Analyte
Chlonde
Nitrate, as N
Nitrite, as N
Sulfate
Sample ID LCS-R884
Client ID ZZZZZ
Analyte
Chlonde
Nitrate, as N
Nitnte, as N
Sulfate
Sample ID LCSD-R884
Client ID ZZZZZ
Analyte
Chlonde
Nitrate, as N
Nitrite, as N
Sulfate
Sample ID L02031 1 7-001 CMS
Client ID RGH-3F-263'
Analyte
Chlonde
Nitrate, as N
SampType MBLK
Batch ID R884
Result
NDNDNDND
SampType LCS
Batch ID R884
Result
2054
09665
09612507
SampType LCSD
Batch ID R884
Result
2039
0953
0948
2494
SampType MS
Batch ID R884
Result
0974
0928
TestCode 300_W
TestNo E300
PQL SPK value
0 100100 100 10
TestCode 300JW
TestNo E300
PQL SPK value
0 10 20 10 10 10 10 10 25
TestCode 300_W
TestNo E300
PQL SPK value
010 2010 1
010 10 10 25
TestCode 300_\V
TestNo E300
PQL SPK value
0 10 10 10 1
Units mg/L
SPK Ref Val
Units mg/L
SPK Ref Val
0000
Units mg/L
SPK Ref Val
0000
Units mg/L
SPK Ref Val
00
Prep Date
Analysis Date
TestCode: 300_W
3/11/02
%REC LowLimit HighLimit RPD Ref Val
Prep Date
Analysis Date 3/11/02
%REC LowLimit HighLimit RPD Ref Val
103 80966 8096 1 80100 80
Prep Date
Analysis Date
120 0120 0120 0120 0
3/11/02
%REC LowLimit HighLimit RPD Ref Val
102 80953 80948 80998 80
Prep Date
Analysis Date
120 2054
120 09665
120 0961120 2 507
3/11/02
%RJ5C LowLimit HighLimit RPD Ref Val
974 8092 8 80
120 0120 0
Run ID LJC-1_020311A
SeqNo 5996
%RPD RPDLimit
Run ID L_IC-1_020311A
SeqNo 5995
%RPD RPDLimit
0000
Run ID L_IC-1_020311A
SeqNo 6000
%RPD RPDLimit
0733 25
1 41 251 36 25
0 520 25
Run ID L_IC-1_020311A
SeqNo 5999
%RPD RPDLimit
00
Qual
Qual
Qual
Qual
Qualifiers: ND - Not Detected at the Reporting I unit
S - Anafyle delected below quantilation limits
S - Spike Recovery outside accepted iccovery limits
R RPD outside accepted icco\cry limits
B - Analyte detected in the associated Method Blank
Page I of 16
CLIENT: Dumpco/SilverstateWork Order: L0203117
ANALYTICAL QC SUMMARY REPORT
Project: RGH-3F-263'
Sample ID MB-355
Client ID ZZZZZ
Analyte
Banum
Calcium
Iron
Magnesium
Potassium
Sodium
Vanadium
Sample ID LCS-355
Client ID ZZZZZ
Analyte
Banum
Calcium
Iron
MagnesiumPotassium
Sodium
Vanadium
Sample ID R0203046-001AMS
Client ID ZZZZZ
Analyte
Banum
Calcium
Iron
Magnesium
Potassium
Sodium
Vanadium
SampType MBLK
Batch ID R_355
Result
NDNDNDNDNDNDND
SampType LCS
Batch ID R_355
Result
1 0342079
10952062
2033
1980516
SampType MS
Batch ID R_355
Result
1 0414642
1 18466798056
338052
TestCode
TestNo
PQL
00050
0500 1005020
05000050
TestCode
TestNo
PQL
0005005001005020
05000050
TestCode
TestNo
PQL
00050
0500 1005020
05000050
6010W_T
SW6010B
SPK value
6010\V_T
SW6010B
SPK value
120
120202005
6010W_T
SW6010B
SPK value
120
120202005
Units mg/L
SPK Ref Val
Units mg/L
SPK Ref Val
0000000
Units mg/L
SPK Ref Val
0 03577
4385
0 1135
46146069
3200
%REC
%REC
103104
10910310299
103
%REC
101129107103
99490
104
Prep Date
Analysis Date
TestCode: 6010WJT
3/12/02
3/13/02
LowLimit HighLimit
Prep Date
Analysis Date
3/12/02
3/13/02
LowLimit HighLimit
85858585858585
Prep Date
Analysis Date
115115115115115115115
3/12/02
3/13/02
LowLimit HighLimit
75757575757575
125125125125125125125
RPD Ref Val
RPD Ref Val
0000000
RPD Ref Val
0000000
Run ID SDB-688
SeqNo 9779
%RPD RPDLimit Qual
Run ID SUB-688
SeqNo 8802
%RPD RPDLimit Qual
0000000
Run ID SUB-688
SeqNo 9132
%RPD RPDLimit Qual
00 C
00000
Qualifiers ND - Not Delected at the Reporting I imit
J Ana/ytc detected below quantitation limits
S Spike Recovery outside accepted recovery limits
R RPD outside accepted recovery limits
B Analyte detected in the associated Method Blank
Page 3 of } 6
CLIENT: Dumpco/SilverstateWork Order: L0203117Project: RGH-3F-263'
Sample ID R0203046-001AMSD
Client ID ZZZZZ
Analyte
BanumCalciumIronMagnesiumPotassiumSodiumVanadium
SampType MSD
Batch ID R_355
Result
1 04445791 18366628023
33705195
TestCode
TestNo
PQL
0005005001005020
05000050
6010W_T
SW6010B
SPK value
1
201
20202005
Units mg/L
SPK Ref Val
0 035774385
0 113546 146069
3200
%REC
10197
107102
97785
104
ANALYTICAL QC SUMMARY REPORT
TestCode: 6010W_T
Prep Date 3/12/02
Analysis Date 3/13/02
LowLimit HighLimit RPD Ref Val
0000000
Run ID SUB-688
SeqNo 9781
%RPD RPDLimit Qual
00000
00
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte detected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
B - Analyte1 detected in the- associated Method Blank
Page 4 of 16
CLIENT: Dumpco/SilveistateWork Order: L0203117
ANALYTICAL QC SUMMARY REPORT
Project: RGH-3F-263'
Sample ID MB-431
Client ID ZZZZZ
Analyte
AntimonyArsenicBerylliumCadmiumChromiumCobaltCopperLeadNickelSeleniumSilverThalliumZinc
Sample ID LCS-431
Client ID ZZZZZ
Analyte
AntimonyArsenicCadmiumChromiumCobaltCopperLeadNickelSeleniumSliverThalliumZinc
SampType MBLK
Batch ID R_431
Result
NDNDNDNDNDNDNDND
NDNDNDNDND
SampType LCS
Batch ID R_431
Result
004750 104400557005590 0555
0055150 052050056850 10680053
0 0546500568
TestCode
TestNo
PQL
00050000500005000050000500005000050000500005000050000500002000050
TestCode
TestNo
PQL
000500005000050000500005000050000500005000050000500005000050
6020WJT
SW6020
SPK value
6020WJT
SW6020
SPK value
00501
00500500500500500501
005005005
Units mg/L
SPK Ref Val
Units mg/L
SPK Ref Val
000000000000
%REC
%REC
95
104
111112111110104114107106109114
Prep Date
Analysis Date
TestCode: 6020WJT
3/19/02
3/20/02
LowLimit HighLimit RPD Ref Val
Prep Date
Analysis Date
3/19/02
3/20/02
LowLimit HighLimit RPD Ref Val
85
8585858585858585858585
115 0
115 0115 0115 0115 0115 0115 0115 0115 0115 0115 0115 0
Run ID SUB-807
SeqNo 9751
%RPD RPDLimit Qual
Run ID SUB-807
SeqNo 9789
%RPD RPDLimit Qual
00000000000
0
Qualifiers: ND - Not Detected at the Reporting I imit
J - Analyle delected below quanlitalion limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
B - Analyte detected in the associated Method Blank
Page 5 of 16
CLIENT: Dumpco/SilverstateWork Order: L0203117Project: RGH-3F-263'
Sample ID R0203179-001AMS
Client ID ZZZZZ
Analyte
AntimonyArsenicCadmiumChromiumCopperLeadNickelSeleniumSilverThalliumZinc
Sample ID R0203179-001AMSD
Client ID ZZZZZ
Analyte
AntimonyArsenicBerylliumCadmiumChromiumCobaltCopper
LeadNickelSeleniumSilverThalliumZinc
SampType MS
Batch ID R_431
Result
0052304244005450061903558
0 044350 102
022080181200476
0 08595
SampType MSD
Batch ID R_431
Result
0053904586
ND0 057750 065950668603906004590 109802356
0 19500502
009315
TestCode
TestNo
PQL
0005000050000500005000050000500005000050000500005000050
TestCode
TestNo
PQL
00050000500005000050000500005000050000500005000050000500005000050
6020WJT
SW6020
SPK value
00501
00500500500500501
005005005
6020W_T
SW6020
SPK value
0050101
0050050050050050050 1
005005005
Units mg/L
ANALYTICAL QC SUMMARY REPORTTestCode: 6020WJT
Prep Date 3/19/02
Analysis Date 3/20/02
SPK Ref Val
0033
000117503219
00 05395
012130 1406
000349
Units mg/L
%REC
105943109100
67788796199581 4952102
LowLimit
7575757575757575757575
HighLimit
125125125125125125125125125125125
RPD Ref Val
00000000000
Prep Date 3/19/02
Analysis Date 3/20/02
SPK Ref Val
0033
00
0011750595
032190
0 053950 12130 1406
000349
%REC
108129
0116108147137
91 8112114109100116
LowLimit HighLimit RPD Ref Val
0000000000000
Run ID SUB-807
SeqNo 9791
%RPD RPDLimit
00000000000
Run ID SUB-807
SeqNo 9792
%RPD RPDLimit
0000000000000
Qual
C
Qual
Jl
C
Qualifiers- ND - Not Detected at the Reporting Limit
J Anal>te detected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
B - Analyte detected in the associated Method Blank
Page 6 of 16
CLIENT: Dumpco/SilverstateWork Order: L0203117Project: RGH-3F-263'
Sample ID: MB-R1291 SampType:
Client ID: ZZZZZ Batch ID:
Analyte
AcetoneBenzeneBromobenzeneBromochloro methaneBromodichloromethaneBromoformBromomcthane2-Butanone
n-Butylbenzencsec-Butylbenzenetert-ButylbenzeneCarbon disulfideCarbon tetrachlorideChlorobenzeneChloroethane2-Chloroethyl vinyl etherChloroformChlorome thane2-Chloro toluene4-Chloro tolueneDibromochloromc thane1 ,2-Dibromo-3-chloropropane1 ,2-Dibromoe thaneDibromome thane1 ,2-Dichlorobenzene1 ,3-Dichlorobenzene1 ,4-DichlorobenzeneDichlorodifluoromcthane1,1-Dichloroe thane1 ,2-Dichloroe thane1 , 1 -Dichloroethene
MBLK
R1291
Result
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
NDNDNDNDNDNDND
ANALYTICAL QC SUMMARY REPORTTestCode: 8260_W
TestCode: 8260_W Units: ng/L Prep Date: Run ID: L_VOAMS-2_020323B
TestNo: SW8260B Analysis Date: 3/23/02 SeqNo: 8763
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
255.05.05.05.05.05.0255.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.0
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte dete-cted below quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
B - Analyte detected in the associated Method Blank
Page 7 of 16
CLIENT: Dumpco/SilverstateWork Order: L0203117Project: RGH-3F-263'
Sample ID. MB-R1291 SampType:
Client ID: ZZZZZ Batch ID'
Analyte
cis-1 ,2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropane1 ,3-Dichloropropane2,2-Dichloropropane1,1 -Dichloropropenecis-1 ,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzeneHexachlorobutadtene2-Hexanone
lodome thaneIsopropylbenzenep-Isopropyltoluene
Methylene chloride4-Methyl-2-pentanoneMTBENaphthalenen-PropylbenzeneStyrenc1,1,1 ,2-Tetrachloroethane1 ,1 ,2,2-TetrachloroethaneTetrachloroetheneToluene
1 ,2,3-Trichlorobenzene1 ,2,4-Trichlorobenzene1,1,1 -Trichloroethane1 , 1 ,2-TrichloroethaneTrichloroctheneTrichlorofluoro methane1 ,1 ,2-Trichlorotnfluoroethane
MBLK
R1291
Result
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
ANALYTICAL QC SUMMARY REPORTTestCode: 8260_W
TestCode: 8260_W Units: fig/L Prep Date: Run ID L_VOAMS-2_020323B
TestNo: SW8260B Analysis Date: 3/23/02 SeqNo: 8763
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
5.05.05.05.05.05.05.05.05.05.0255.05.05.05.0255.010
5.05.05.05.05.05.05.05.05.0
5.05.05.05.0
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte detected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
B - Analyte detected in the associated Method Blank
Page 8 of 16
CLIENT: Dumpco/SilverstateWork Order: L0203117Project: RGH-3F-263'
Sample ID MB-R1291
Client ID ZZZZZ
Analyte
1 ,2,3-Tnchloropropane
1 ,2,4-Tnmethylbenzene
1 ,3,5-Tnmethylbenzene
Vinyl acetate
Vinyl chlonde
o-Xylenem,p-Xylene
Surr Dibromofluoromethanc
Surr Toluene-d8
Surr 4-Bromofluorobenzene
Sample ID LCS-R1291
Client ID ZZZZZ
Analyte
Benzene
Bromome thane
ChlorobenzeneChloromethane
Dichlorodifluoromethane
1,1-Dichloroe theneToluene
Tnchloroe thene
Vinyl chlonde
Surr Dibromofluoromethane
Surr Toluene-d8
Surr 4-Bromofluorobenzene
SampType MBLK
Batch ID R1291
Result
ND
ND
ND
ND
ND
ND
ND
5053
5023
4803
SampType LCS
Batch ID R1291
Result
4994
5571
51 62
5057
5329
4963
5064
51 23
483
5065
5052
509
TestCode
TestNo
PQL
50
50
50
50
50
50
10
50
50
50
TestCode
TestNo
PQL
50
50
50
50
50
50
50
50
50
50
50
50
8260_W
SW8260B
SPK value
50
50
50
8260_W
SW8260B
SPK value
50
50
50
50
50
50
50
50
50
50
50
50
Units (ig/L
ANALYTICAL QC SUMMARY REPORT
TestCode: 8260_W
Prep Date
Analysis Date 3/23/02
SPK Ref Val
0
0
0
Units (ig/L
%REC
101
100
96 1
LowLimit
808
848
562
HighLimit
119
102
139
RPD Ref Val
0
0
0
Prep Date
Analysis Date 3/23/02
SPK Ref Val
0
0
0
0
0
0
0
0
0
0
0
0
%REC
999
111
103101107
993
101
102
966
101
101
102
LowLimit
70
70
70
70
70
80
80
70
80
8080
90
70
HighLimit
130
130
130
130
130
120
120
130
120
102
102
106
RPD Ref Val
0
0
0
0
0
0
0
0
0
0
0
0
Run ID L_VOAMS-2_020323B
SeqNo 8763
%RPD RPDLimit
0
0
0
Qual
Run ID L_VOAMS-2_020323B
SeqNo 8764
%RPD RPDLimit
0
0
0
0
0
0
0
00
0
0
0
Qual
S
Qualifiers: ND - Not Detected at the Reporting 1 milt
J - Analyte detected below quant i ta t ion l imits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits'
B - Analyte detected in the associated Method Blank
Page 9 of 16
CLIENT: Dumpco/SilverstateWork Order: L0203117Project: RGH-3F-263'
Sample ID L0203117-001BMS
Client ID RGH-3F-263'
Analyte
BenzeneBromo methaneChlorobenzeneChloromcthaneDichlorodifluoromethane1,1-DichloroetheneTolueneTnchloroe theneVinyl chlonde
Surr DibromofluoromcthaneSurr Toluene-d8Surr 4-Bromofluorobenzene
Sample ID L0203U7-001BMSD
Client ID RGH-3F-2631
Analyte
BenzeneBromomethaneChlorobenzeneChloromethaneDichlorodi fluoromethane1,1-DichloroetheneTolueneTnchloroetheneVinyl chlonde
Surr DibromofluoromethaneSurr Toluene-d8Surr 4-Bromofluorobenzenc
SampType MS
Batch ID R1291
Result
442541 535026428548 183924456845743367499348954852
SampType MSD
Batch ID R1291
Result
4256368448 19334
41 33362
436443 672908499448394869
TestCode
TestNo
PQL
505050505050505050
505050
TestCode
TestNo
PQL
505050505050505050505050
8260_W
SW8260B
SPK value
505050505050505050505050
8260_W
SW8260B
SPK value
505050505050
505050505050
Units ug/L
ANALYTICAL QC SUMMARY REPORTTestCode: 8260_W
Prep Date
Analysis Date 3/23/02
SPK Ref Val
000000000
000
Units ng/L
%REC
88583 1101
85796478591 491 5673
999979
97
LowLimit
70707070708080
7080899070
HighLimit
130130130130130120120130120102102106
RPD Ref Val
000000000000
Prep Date
Analysis Date 3/23/02
SPK Ref Val
000000000000
%REC
85 I737964668827724
87 3873582999968974
LowLimit
707070707080807080899070
HighLimit
130130130130130120120
130120102102106
RPD Ref Val
442541 535026428548 183924456845743367
000
Run ID L_VOAMS-2_020323B
SeqNo 8765
%RPD
000000000
000
Run ID L_
RPDLimit Qual
S
S
VOAMS-2_020323B
SeqNo 8766
%RPD
3891204 2 1248153806457463146
000
RPDLimit
252525252525252525000
Qual
S
S
S
Qualifiers: ND - Not Detected at the Reporting 1 imit
J Ana l> te detected below quantitation l imits
S - Spike Recovery outside accepted recovery limits
R RPD outside accepted recovery limits
B - Analyte detected in the associated Method Blank
Page 10 of 16
CLIENT:Work Order:Project:
Dumpco/Silvei state
L0203117
RGH-3F-263'
ANALYTICAL QC SUMMARY REPORT
TestCode: ALK W
Sample ID MB-R898
Client ID ZZZZZ
Analyte
SampType MBLK
Batch ID R898
Result
TestCode ALK_W Units mg/L
TestNo M2320 B
PQL SPK value SPK Ref Val
Prep Date
Analysis Date 3/11/02
%REC LowLimit HighLimit RPD Ref Val
Run 1 D L_ATITR-1 _0203 1 1 A
SeqNo 6076
%RPD RPDLimit Qual
Alkalinity, Bicarbonate (As CaCO3)
Alkalinity, Carbonate (As CaCO3)
Hydroxide (As CaCO3)
Alkalinity, Total (As CaCO3)
NDNDNDND
25252525
Sample ID LCS-R898
Client ID ZZZZZ
Analyte
SampType LCS
Batch ID R898
Result
TestCode ALKJW Units mg/L
TestNo M2320B
PQL SPK value SPK Ref Val
Prep Date
Analysis Date 3/11/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_ATITR-1_020311A
SeqNo 6075
%RPD RPDLirnit Qual
Alkalinity, Total (As CaCO3) 1255 25 125 100 80 120
Sample ID LCSD-R898
Client ID ZZZZZ
Analyte
SampType LCSD
Batch ID R898
Result
TestCode ALK_W Units mg/L
TestNo M2320 B
PQL SPK value SPK Ref Val
Prep Date
Analysis Date 3/11/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_ATITR-1 J)203 1 1 A
SeqNo 6077
%RPD RPDLimit Qual
Alkalinity, Total (As CaCO3) 1256 25 125 100 80 120 1255 00796 25
Sample ID L0203071-001ADUP SampType DUP
Client ID ZZZZZ Batch ID R898
Analyte
Alkalinity, Bicarbonate (As CaCO3)
Alkalinity, Carbonate (As CaCO3)
Hydroxide (As CaCO3)
Alkalinity, Total (As CaCO3)
Result
200NDND
200
TestCode ALK_W Units mg/L Prep Date
TestNo M2320B
PQL
252525
25
SPK value
0000
SPK Ref Val
20000
200
%REC
000
0
Analysis Date 3/11/02
LowLimit
000
0
HighLimit
000
0
RPD Ref Val
0000
Run ID L_ATITR-1_020311A
SeqNo 6078
%RPD RPDLimit
000
0
Qual
Qualifiers: ND - Not Detected at the Reporting Limit
J - Anal>te detected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted iccovery limits
B - Analyte detected in the associated Method Blank
Page 11 of 16
CLIENT:Work Order:Project:
Dumpco/Silverstate
L0203117RGH-3F-263'
ANALYTICAL QC SUMMARY REPORT
TestCode: COD
Sample ID
Client ID
Analyte
MB-R900
ZZZZZ
SampType
Batch ID
MBLK
R900
Result
TestCode
TestNo
PQL
COD
M5220 C
SPK value
Units mg/L
SPK Ref Val
Prep Date
Analysis Date 3/12/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_SPEC-2
SeqNo 6090
%RPD RPDI
_020312C
limit Qual
Chemical Oxygen Demand ND 10
Sample ID LCS-R900
Client ID ZZZZZ
Analyte
SampType LCS
Batch ID R900
Result
TestCode COD Units mg/L
TestNo M5220C
PQL SPK value SPK Ref Val
Prep Date
Analysis Date 3/12/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_SPEC-2_020312C
SeqNo 6089
%RPD RPDLimit Qual
Chemical Oxygen Demand 529 10 500 106 80 120
Sample ID LCSD-R900
Client ID ZZZZZ
Analyte
SampType LCSD
Batch ID R900
Result
TestCode
TestNo
PQL
COD Units mg/L
M5220 C
SPK value SPK Ref Val
Prep Date
Analysis Date
Run ID L_SPEC-2_020312C
3/12/02
%REC LowLimit HighLimit RPD Ref Val
SeqNo 6093
%RPD RPDLimit Qual
Chemical Oxygen Demand 519 10 500 104 80 120 529 1 91 15
Sample ID L0203 117-001 CMS
Client ID RGH-3F-263'
Analyte
SampType MS
Batch ID R900
Result
TestCode COD Units mg/L
TestNo M5220C
PQL SPK value SPK Ref Val
Prep Date
Analysis Date 3/12/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_SPEC-2_020312C
SeqNo 6091
%RPD RPDLimit Qual
Chemical Oxygen Demand 544 10 500 15 106 70 130
Sample ID
Client ID
Analyte
L0203117-001CMSD
RGH-3F-263'
SampType
Batch ID
MSD
R900
Result
TestCode
TestNo
PQL
COD
M5220 C
SPK value
Units mg/L
SPK Ref Val
Prep Date
Analysis Date
Run ID L_SPEC-2_020312C
3/12/02
%REC LowLimit HighLimit RPD Ref Val
SeqNo 6092
%RPD RPDLimit Qual
Chemical Oxygen Demand 535 10 500 15 104 70 130 544 1 67 25
Qualifiers: ND - Not Detected at the Reporting I innt
J - Anal>tc detected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted reco\cn, limits
B Analyte detected in the associated Method Blank
Page 12 of 16
CLIENT:Work Order:Project:
Dumpco/Silverstate
L0203117RGH-3F-263'
ANALYTICAL QC SUMMARY REPORT
TestCode: HG 7470 T
Sample ID
Client ID
Analyte
MB-419
ZZZZZ
SampType
Batch ID
MBLK
R_419
Result
TestCode
TestNo
PQL
HG_7470_T
SW7470
SPK value
Units mg/L
SPK Ref Val
Prep Date
Analysis Date
3/19/02
3/19/02
%REC LowLimit HighLimit RPD Ref Val
Run ID SUB-787
SeqNo 9785
%RPD RPDI imit Qual
Mercury ND 0 00020
Sample ID
Client ID
Analyte
LCS-419
ZZZZZ
SampType
Batch ID
LCS
R_419
Result
TestCode
TestNo
PQL
HG_7470_T
SW7470
SPK value
Units mg/L
SPKRefVai
Prep Date
Analysis Date
3/19/02
3/19/02
%REC LowLimit HighLimit RPD Ref Val
Run ID SUB-787
SeqNo 9408
%RPD RPDLimit Qual
Mercury 0 00474 0 00020 0005 948 85 115
Sample ID
Client ID
Analyte
L02031 17-001 A
RGH-3F-263'-M
SampType
Batch ID
MS
R_419
Result
TestCode
TestNo
PQL
HG_7470_T
SW7470
SPK value
Units mg/L
SPKRefVai
Prep Date
Analysis Date
3/19/02
3/19/02
%REC LowLimit HighLimit RPD Ref Val
Run ID SUB-787
SeqNo 9786
%RPD RPDLimit Qual
Mercury 00048 0 00020 0005 96 85 115
Sample ID
Client ID
Analyte
L02031 17-001 A
RGH-3F-263'-M
SampType
Batch ID
MSD
R_419
Result
TestCode
TestNo
PQL
HG_7470_T
SW7470
SPK value
Units mg/L
SPKRefVai
Prep Date
Analysis Date
3/19/02
3/19/02
%REC LowLimit HighLimit RPD Ref Val
Run ID SUB-787
SeqNo 9748
%RPD RPDLimit Qual
Mercury 0 00491 0 00020 0005 982
Sample ID
Client ID
Analyte
L0203117-001A
RGH-3F-263'-M
SampType
Batch ID
DUP
R_419
Result
TestCode
TestNo
PQL
HG_7470_T
SW7470
SPK value
Units mg/L
SPK Ref Val
Prep Date
Analysis Date
3/19/02
3/19/02
%REC LowLimit HighLimit RPD Ref Val
Run ID SUB-787
SeqNo 8594
%RPD RPDLimit Qual
Mercury ND 0 00020
Qualifiers: ND • Not Detected at the Reporting I miit
* J Analv te detected below quant i ta t ion l imits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery l imits
B Analyte detected in the associated Method Blank
Page 13 of 16
CLIENT:Work Order:Project:
Dumpco/SilverstateL0203117RGH-3F-263'
ANALYTICAL QC SUMMARY REPORTTestCode: NH3-N W
Sample ID MB-R901
Client ID ZZZZZ
Analyte
SampType MBLK
Batch ID R901
Result
TestCode NH3-N_W Units mg/L
TestNo M4500-NH3 C
PQL SPK value SPKRefVai
Prep Date
Analysis Date 3/12/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_WC_020312B
SeqNo 6099
%RPD RPDLimit Qual
Ammonia, as N ND 030
Sample ID LCS-R901
Client ID ZZZZZ
Analyte
SampType LCS
Batch ID R901
Result
TestCode NH3-N_W Units mg/L
TestNo M4500-NH3C
PQL SPK value SPKRefVai
Prep Date
Analysis Date 3/12/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_WC_020312B
SeqNo 6098
%RPD RPDLimit Qual
Ammonia, as N 1008 030 101 839 117
Sample ID LCSD-R901
Client ID ZZZZZ
Analyte
SampType LCSD
Batch ID R901
Result
TestCode NH3-N_W Units mg/L
TestNo M4500-NH3 C
PQL SPK value SPKRefVai
Prep Date
Analysis Date 3/12/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_WC_020312B
SeqNo 6100
%RPD RPDLimit Qual
Ammonia, as N 1 12 030 112 839 117
Qualifiers: ND - Not Detected at the Reporting Limit
f 3 - Anal>te detected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R RPD outside accepted recovery limits
B - Analyte detected in the associated Method Blank
Page 14 of 16
CLIENT:Work Order:Project:
Dumpco/SilverstateL0203117RGH-3F-263'
ANALYTICAL QC SUMMARY REPORT
TestCode: SULF W
Sample ID MB-R879
Client ID ZZZZZ
Analyte
SampType MBLK
Batch ID R879
Result
TestCode SULF_W Units mg/L
TestNo M4500-SD
PQL SPK value SPKRefVai
Prep Date
Analysis Date 3/12/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_SPEC-2_020312A
SeqNo 5960
%RPD RPDLimit Qual
Sulfide ND 0030
Sample ID LCS-R879
Client ID ZZZZZ
Analyte
SampType LCS
Batch ID R879
Result
TestCode SULF_W Units mg/L
TestNo M4500-SD
PQL SPK value SPKRefVai
Prep Date
Analysis Date 3/12/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_SPEC-2_020312A
SeqNo 5959
%RPD RPDLimit Qual
Sulfide 0 118 0030 0107 110 80 120
Sample ID LCSD-R879
Client ID ZZZZZ
Analyte
SampType LCSD
Batch ID R879
Result
TestCode SULF_W Units mg/L
TestNo M4500-SD
PQL SPK value SPKRefVai
Prep Date
Analysis Date 3/12/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_SPEC-2_020312A
SeqNo 5961
%RPD RPDLimit Qual
Sulfide O i l 0030 0107 103 80 120 0 118 702 25
Sample ID
Client ID
Analyte
L0203117-001CMSD
RGH-3F-263'
SampType
Batch ID
MSD
R879
Result
TestCode
TestNo
PQL
SULF_W
M4500-S D
SPK value
Units mg/L
SPKRefVai
Prep Date
Analysis Date
Run ID L_SPEC-2_020312A
3/12/02
%REC LowLimit HighLimit RPD Ref Val
SeqNo 5963
%RPD RPDLimit Qual
Sulfide 0 107 0030 0 107 100 70 130 25
Qualifiers: ND - Not Detected at the Reporting Limit
J - Anal^te detected below, quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recoveiy limits
B - Analyte detected in trie associated Method Blank
Page 15 of 16
CLIENT: Dumpco/SilverstateWork Order: L0203117Project: RGH-3F-263'
Sample ID MB-R907
Client ID ZZZZZ
Analyte
Total Dissolved Solids
Sample ID: LCS-R907
Client ID ZZZZZ
Analyte
Total Dissolved Solids
Sample ID: L02031 07-005 ADUP
Client ID: ZZZZZ
Analyte
SampType- MBLK
Batch ID: R907
Result
ND
SampType: LCS
Batch ID: R907
Result
997
SampType: DUP
Batch ID: R907
Result
TestCode: TDS_W Units: mg/L
TestNo: E160.1
PQL SPK value SPK Ref Val
15.0
TestCode: TDS_W Units: mg/L
TestNo: E160.1
PQL SPK value SPKRefVai
15.0 1000 0
TestCode: TDS_W Units: mg/L
TestNo: E160.1
PQL SPK value SPKRefVai
ANALYTICAL QC SUMMARY REPORTTestCode: TDS_W
Prep Date:
Analysis Date: 3/11/02
%REC LowLimit HighLimit RPD Ref Val
Prep Date:
Analysis Date: 3/11/02
%REC LowLimit HighLimit RPD Ref Val
99.7 80 120 0
Prep Date:
Analysis Date: 3/11/02
%REC LowLimit HighLimit RPD Ref Val
Run I D L_WC_0203 1 1 D
SeqNo 6140
%RPD RPDLimit
Run ID: L_WC_0203 1 1 D
SeqNo: 6139
%RPD RPDLimit
0
Run ID: L_WC_020311D
SeqNo: 6141
%RPD RPDLimit
Qual
Qual
Qual
Total Dissolved Solids 1133 15.0 2360 70.3 25
Qualifiers: ND - Not Detected at the Reporting Limit
J - Analyte detected below quantitation limits
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
B - Analyte detected in the associated Method Blank
Page 16 of 16
NEL LABORATORIESReno • Las Vegas • Boise
Phoenix • Sacramento
CHAIN OF CUSTODY NEL Work Order:
Las Vegas Division • 4208 Arcata Way, Suite A • Las Vegas, Nevada 89030702-657-1010 • Fax. 702-657-1577 • 888-368-3282
Company:,- Attentioi
Address:
Phone NumbSr
Billing Address:'*'•<" s?^)JLs»icr xvcjr
Requested Turnaround: jf 5-day 2-day 1-day
Time/Date N.E.L.Sampled Customer Sample Identification Identification
Project Name1
Purchase Order Number
Project Number
Sampled By
B3
Custody Seal intact?/ Y
CondTtttfn
Box#1 DW • Drinking WaterWW - Waste WaterOL - Oil/Organic Liquid
SO • SolidAQ • AqueousA • Air
Box #2 A HCIB HMO,C HjSO,,D NaOH
E Ice OnlyF OthwG Not Preserved
Relinquished by (Print) (Sigrgfure) Date/Time Received by (Print) (Signature)
Z^Date/Timee/Tirae
The liability of NEL Laboratories Inc is limited strictly to the price of sample analysis for those samples received m good condition by NEL NEL is not responsible for loss damage, resampling costs and/or qualified data related to samples not received in good condition,intruding adeQuate sample volume and number of containers Customer signature of this CoC constitutes a purchase order for NEL to perform work and constitutes acceptance of all NEL Standard Terms and Conditions Signature also constitutes acceptanceo1 M£\- Standard hsi Prices lot att services otdeted t\eie on, except those specilied otherwise via an NEL Quotation for Testing Services in effect at the time of sample receipt NEL turnaround times are measured in regular working days Samples received at thelaboratory after 16 30 will be considered received on the next working day Commitment of laboratory to the requested turnaround time will be confirmed via Sample Confirmation transmitted to the fax number provided above
ORIGINAL
NEL LABORATORIESReno • Las-Vegas- — -Phoenix • Burbank
Las Vegas Division4208 Arcata Way, Suite A • Las Vegas, NV 89030
(702)657-1010 -Fax: (702) 657-15771-888-368-3282
Nick SainesDumpco/Silverstate7900 Vegas Valley DriveLas Vegas, NV 89142
TEL: 702-431-3020
RE Project: GH-3F
Dear Nick Saines:
Order No.: L0204322
NEL Laboratories, Las Vegas received 5 samples on 4/22/02 for the analyses presented in thefollowing report.
There were no problems with the analyses and all data for associated QC met EPA or laboratoryspecifications unless noted in the Case Narrative.
If you have any questions regarding these tests results, please feel free to call.
<m^tA{MJ>o/Stan Van vagenea^ ALaboratory Manager
Certifications:ArizonaCaliforniaIdahoMontanaNevadaNew MexicoUS Army Corps of Engineers
'<(«<
RenoAZ05201707CertifiedCertifiedNV033Certified
Las VegasAZ05182002CertifiedCertifiedNV052CertifiedCertified
Corporate Office & Reno Division • 1030 Matley Lane • Reno, NV 89502 • (702) 348-2522
NEL LABORATORIES
NEL Laboratories, Las Vegas Date: 17-May-02
CLIENT:
Project:Lab Order:
RSSN
GH-3F
L0204322CASE NARRATIVE
Attached are the analytical results for samples in support of the above referenced project.
The samples submitted for this project were not sampled by NEL. Should you have any questions orcomments, please feel free to contact our Client Services Department.
Analytical Comments:
EPA 8260: Samples were evaluated for the presence of Acrylonitrile and trans-l,4-Dichloro-2-butene.Neither of these two compounds were present in the samples submitted in this work-order at or above5ppb.
Page 1 of 1
NEL LABORATORIESI
CLIENT: RSSN
PROJECT ID: GH-3F
PROJECTS: GH-3F
MATRIX: AQUEOUS
Parameter
Chloride
Nitrate, as N
Nitrite, as N
Sulfate
Alkalinity, Bicarbonate (As CaCOS)
Alkalinity, Carbonate (As CaC03)
Hydroxide (As CaC03)
Alkalinity, Total (As CaCO3)
Chemical Oxygen Demand
Ammonia, as N
Sulfide
Total Dissolved Solids
CLIENT ID: GH-3F
DATE SAMPLED: 4/22/02
NEL SAMPLE ID: L0204322-001B
Result
2200
ND
ND
3000
ND75
ND75
76
NDND
7220
Unit
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
ReportingLimit
200
2525200252525
25
10
0300030
150
DF
2000
2525
2000
1111111
10
Method Prep Date
EPA 300 0
EPA 300 0
EPA 300 0
EPA 300 0
SM2320 B
SM2320 B
SM2320 B
SM2320 B
SM5520 D
SM4500-NH3
SM4500-S D
SM2540 C
Analyzed
04/30/02
04/23/02
04/23/02
04/30/02
04/29/02
04/29/02
04/29/02
04/29/02
04/29/02
04/30/02
04/26/02
04/24/02
Analyst
PJJ-LV
PJJ-LV
PJJ-LV
PJJ-LV
RDA-LV
RDA-LV
RDA-LV
RDA-LV
RDA-LV
RDA-LV
RWW-LV
CRA-LV
ND -Not Detected at the Reporting Limit
DF - Dilution Factor
Date: 16-May-02
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 1 of 5
NEL LABORATORIES
CLIENT: RSSN
PROJECT ID: GH-3F
PROJECT #: GH-3F
MATRIX: AQUEOUS
Parameter
Aluminum
Barium
Calcium
IronMagnesium
Potassium
Sodium
Vanadium
Antimony
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Manganese
Nickel
Selenium
Silver
Thallium
Zinc
Mercury
Result
0.88
0.028
6200.78
19095
1600
NDND
0.021
ND
ND0.0081
0.0024
0.014
NDND
0.0065
NDNDND0.14
ND
Unit
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
ReportingLimit
0050000500200100202050
00050OOOIOOOOIOO O O I OOOOIOO O O I OOOOIOOOOIOOOOIOO O O I OO O O I OOOOIOOOOIO
0 00040O O O I O
0 00020
CLIENT ID:
DATE SAMPLED:
NEL SAMPLE ID:
DF
111111
1001111111111111111
Method
SW 6010B-To
SW6010B-To
SW 6010B-TO
SW6010B-TO
SW6010B-To
SW6010B-To
SW6010B-To
SW6010B-TO
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 7470-Tota
GH-3F-M
: 4/22/02
; L0204322-002A
Prep Date
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/24/02
Analyzed
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
Analyst
FIF-Reno
FIF-Reno
FIF-Reno
FIF-Reno
FIF-Reno
FIF-Reno
FIF-Reno
FIF-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
A
ND - Not Detected at the Reporting Limit
DF - Dilution Factor
Date: 16-May-02
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 2 of 5
NEL LABORATORIES
CLIENT: RSSN
PROJECT ID: GH-3F
PROJECT*: GH-3F
MATRIX: AQUEOUS
Parameter
Aluminum
Barium
Calcium
Iron
Magnesium
Potassium
Sodium
Vanadium
Antimony
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Manganese
Nickel
Selenium
Silver
Thallium
Zinc
Mercury
Result
0.099
0.020
620ND18088
1500
ND0.0011
0.019
NDND
0.0022
0.0014
0.0069
ND0.0024
0.0034
NDNDND
0.084
ND
Unit
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
ReportingLimit
0050
00050
0500100502050
00050
O O O I O
OOOIO
OOOIO
OOOIO
OOOIO
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
OOOIO
0 00040
OOOIO
0 00020
CLIENT ID: GH-3F-FFM
DATE SAMPLED: 4/22/02
NEL SAMPLE ID: L0204322-003A
DF Method Prep Date
1 SW 6010B-Di
1 SW 6010B-Di
1 SW 6010B-Di
1 SW 6010B-D1
1 SW 60108-Di
1 SW 6010B-D1
10 SW 6010B-D1
1 SW6010B-D1
1 SW 6020-Diss
1 SW 6020-Diss
1 SW 6020-Diss
1 SW 6020-Diss
1 SW 6020-Diss
1 SW 6020-Diss
1 SW 6020-Diss
1 SW 6020-Diss
1 SW 6020-Diss
1 SW 6020-Diss
1 SW 6020-Diss
1 SW 6020-Diss
1 SW 6020-Diss
1 SW 6020-Diss
1 SW 7470-Diss 04/24/02
Analyzed
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
Analyst
RAA-Reno
RAA-Reno
RAA-Reno
RAA-Reno
RAA-Reno
RAA-Reno
RAA-Reno
RAA-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
A
ND - Not Detected at the Repoitmg I unit
DF - Dilution Facun
Date: I6-Mav-02
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 3 of5
NEL LABORATORIES
CLIENT: RSSN
PROJECTED: GH-3F
PROJECTS: GH-3F
MATRIX: AQUEOUS
Parameter
1 ,1 ,1,2-Tetrachloroethane
• 1,1,1-Tncbloroethane1,1,2,2-Tetrachloroethane1,1,2-Tnchloroethane1 , 1 ,2-Tnchlorotrifluoi oethane1 , 1 -Dichloroethane1 1 -Dichloroethene
1 , 1 -Dichloropropene1 ,2,3-Tnchloroben7ene1 ,2,3-Tnchloropropane1 ,2,4-Tnchlorobenzene1 ,2,4-Tnmethylbenzene
1 ,2-Dibromo-3-chloropi opane
1 ,2-Dibromoethane1 ,2-Dichlorobenzene1,2-Dichloroethane1 ,2-Dichloropropane1 ,3,5-Tnmethylbenzene1 ,3-Dichlorobenzene1 ,3-Dichloropropane1 ,4-Dichlorobenzene2,2-Dichloropropane2-Butanone2-Chloroethyl vinyl ether
2-Chlorotoluene2-Hexanone4-Chlorotoluene
4-Methyl-2-pentanoneAcetoneBenzeneBromobenzeneBromochloromethaneBromodichloromethaneBromoformBromomethaneCarbon disulfideCarbon tetrachlondeChlorobenzeneChloroethaneChloroformChloromethanecis-1 ,2-Dichloroethenecis-1 ,3-DicliloropropeneDibromochloromethane
ND - Not Detected at the Reporting Limit
DF - Dilution Factor
Date: l6-May-02
CLIENT ED: FGH-3F (Field Blank)
DATE SAMPLED: 4/22/02
NEL SAMPLE ID: L0204322-004A
Result Unit
ND ug/LND ug/LND ug/LND ug/LND ng'LND ug/LND ug/L
ND ug/L
ND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/L
ND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/L
ND ug/L
ND ug'LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/L
ReportingLimit DF Method Prep Date Analyzed
50 150 150 150 150 150 150 150 150 150 150 150 150 150 150 150 150 150 150 150 150 150 125 150 150 125 150 125 125 150 150 150 150 150 150 150 150 150 150 150 150 150 150 150 1
SW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260B
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/0204/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/0204/23/02
Analyst
DRM-LVDRM-LVDRM-LVDRM-LV
DRM-LVDRM-LVDRM-LVDRM-LVDRM-LV
DRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LV
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 4 of 5
NEL LABORATORIES
CLIENT: RSSN
PROJECT ID: GH-3F
PROJECTS: GH-3F
MATRIX: AQUEOUS
Parameter
Dibromomethane
Dichlorodifluoromethane
Ethylbenzene
Hexachlorobutadiene
lodomethane
Isopropylbenzene
m,p-Xylene
Methylene chlonde
MTBEn-Butylbenzene
n-Propylbenzene
Naphthalene
o-Xylene
p-Isopropyltoluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1 ,2-Dichloroethene
trans-1 ,3-Dichloropropene
Tnchloroethene
Tnchlorofluoromethane
Vinyl acetate
Vinyl chlonde
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoi omethanc
Surr: Tolucne-d8
Result
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND90.8
96.3
109
Unit
ug/L
ug/L
ug/L
Ug/L
HS/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
ReportingLimit
50505050505010505050501050505050505050505050505050
85 3-104
92 6-108
957-112
CLIENT ID: FGH-3F (Field Blank)
DATE SAMPLED: 4/22/02
NEL SAMPLE ID: L0204322-004A
DF
llllllllllllllllllllllllllll
Method
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
SW8260B
Prep Date Analyzed
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
Analyst
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
ND - Not Detected at the Repotting Limit
DF - Dilution Factor
Date: 16-May-02
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 5 of 5
BSK A N A L Y T I C A L
Vanessa Padilla Certificate of AnalysisNEL Laboratories Las Vegas ELAP Certificate #11804208 AjCata Way, Ste A Report Issue Date: 05/01/2002
Las Vegas, NV 89030
BSK Submission #: 2002041149BSK Sample ID #: 201120Project ID L0204322 Project Desc Dumpco
Submission Comments
Sample Type:Sample Description:Sample Comments-
Inorganics
Analyte
LiquidGH-3F
Method
Date Sampled. 04/22/2002Time Sampled: 0940Date Received: 04/23/2002
Prep AnalysisResult Units PQL Dilution DLR Date Date
Dissolved Organic Carbon (DOC) SM5310-D 4.2 mg/L 02 5 10 04/29/200204/29/2002
mg/L: Milligrams/Liter (ppm) PQL: Practical Quantitation Limit H: Analyzed outside of hold timemg/Kg: Milligrams/Kilogram (ppm) DLR: Detection Limit for Reporting P: Preliminary resultUg/L: Micrograms/Liter (ppb) : PQL x Dilution S: Suspect result. See Cover Letter for commentsug/Kg: Micrograms/Kilogram (ppb) ND: None Detected at DLR E: Analysis performed by External laboratory.%Rec- Percent Recovered (surrogates) See External Laboratory Report attachments
Report Authentication Code: IllOIIIIIIiniilllllllllllllililliliiilllflllll page 1 uf [
1414 Stanislaus Street Fresno, CA 93706-1623 Phone 559-497-2888, In CA 800-877-8310 Fax 559-485-6935
BSICA N A L Y T I C A LLABOR-A-T-ORILS
QC Summary Report 05/01/2002
BSK Submission:Client:Date Submitted:Project ID :Project Desc:
2002041149NEL Laboratories Las Vegas04/23/2002L0204322Dumpco
BSK StarLims Run #: 36194Analyst Initials: DONNAHAnalyte Results MatrixAnalyte QCType Spike ID Result
Instrument ID:
Method Number: DOC%Rec Spike Spk Matrix
Units or RPD RPD Cone Cone UCL LCL Date
Dissolved Organic Carbon (DOC)
Dissolved Organic Carbon (DOC)
Dissolved Organic Carbon (DOC)
Dissolved Organic Carbon (DOC)
Dissolved Organic Carbon (DOC)
LCS
LCSD
MS
MSD
RBLK
N/A
N/A
201118
201118
N/A
1.03
1.01
23.87
23.78
0
mg/L
mg/L
mg/L
mg/L
mg/L
103
101
110
110
<0.2
1
2 1
10
0.37 10
ND
ND
12
12
130
130
130
130
0.2
70
70
70
70
N/A
04/29/02
04/29/02
04/29/02
04/29/02
04/29/02
Acceptable
Acceptable
Acceptable
Acceptable
Acceptable
Approved by:
%Rec: Percent Recovered
RPD: Relative Percent Difference
UCL: Upper Control Limit
LCL: Lower Control Limit
Parent Sample: Sample used as background matrix for MS/MSD
DOS-High: QC Result Above UCL
DOS-Low: QC Result Below LCL
Page 1 of 1
NEL LABORATORIES,^-:— 3JH|
i^•BK^^^•k-JOUHHBUI BIBBHIIIMh.
CLIENT: RSSNWork Order: L0204322Project: GII-3F
Sample ID MB-R2742
Analyte
Chlonde
Nitrate, as N
Nitnte.asNSulfate
Sample ID MB-R2993
Analyte
Chloride
Nitrate, as N
Nitrite, as N
Sulfate
Sample ID LCS-R2742
Analyte
Chloride
Nitrate, as N
Nitrite, as N
Sulfate
SampType MBLK
Batch ID R2742
Result
NDNDNDND
SampType MBLK
Batch ID R2993
Result
NDNDNDND
SampType LCS
Batch ID R2742
Result
2010994
096272
ANALYTICAL QC SUMMARY REPORT
300_W Test Method: EPA 300.0
TestCode 300_W Units mg/L Piep Date Run ID L_IC-I_020423A
TestNo E300 Analysis Date 4/23/02 SeqNo 20975
PQL SPK value SPKRefVai %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
0 100 100 100 10
TestCode 300_W Units mg/L Prep Date Run ID L_1C-1_020430A
TestNo E300 Analysis Date 4/30/02 SeqNo 23006
PQL SPK value SPKRefVai %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
0100 100 100 10
TestCode 300_W Units mg/L Prep Date Run ID L_IC-1_020423A
TestNo E300 Analysis Date 4/23/02 StqNo 20974
PQL SPK value SPKRefVai %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
010 2 0 101 80 120 0 0010 1 0 994 80 120 0 0010 1 0 96 80 120 0 0
010 25 0 109 80 120 0 0
Qualifiers: ND - Not Detected at the Repoitmg Limit C - Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted lecoveiy limits
j - This conccntiation is consideied an estimate due to LCS fa i lu ie
B - Analyte detected in the associated Method Blank
Page 1 of'26
Date: 16-May-02
CLIENT: RSSNWork Order: L0204322Project: GH-3F
Sample ID LCS-R2993
Analyte
Chloride
Nitrate, as N
Nitrite, as N
Sulfate
Sample ID LCSD-R2742
Analyte
Chloi ide
Nitiate, as N
Nitrite, as NSulfate
Sample ID LCSD-R2993
Analyte
Chlonde
NiUate, as N
Nitute, asN
Sulfate
Sample ID L0204322-001BMS
Analyte
Nitiate, as N
Nitrite, as N
ANALYTICAL QC SUMMARY REPORT
SampType LCS
Batch ID R2993
Result
20130986
1 0152547
SampType LCSD
Batch ID R2742
Result
2067
0994
0982719
SampType LCSD
Batch ID R2993
Result
2060972
1 022602
SampType MS
Batch ID R2742
Result
2463082
TestCode 300_W
TestNo E300
PQL SPK value
010 20 10 10 10 10 10 25
TestCode 300_W
TestNo E300
PQL SPK value
0 10 20 10 1
010 10 10 25
TestCode 300_W
TestNo E300
PQL SPK value
010 20 10 10 10 10 10 25
TestCode 300_W
TestNo E300
PQL SPK value
2 5 2525 25
300_W
Units mg/L
SPKRefVai
0000
Units mg/L
SPKRefVai
00
00
Units mg/L
SPKRefVai
0000
Units mg/L
SPKRefVai
00
Test Method: EPA 300.0 1
%REC
101986102102
%REC
103994
98109
%REC
103972102104
%R£C
984123
Piep Date
Analysis Date 4/30/02
LowLimit HighLimit RPD Ref Val
80808080
Pi ep Date
Analysis Date
120 0120 0120 0120 0
4/23/02
LowLimit HighLimit RPD Ref Val
80808080
Piep Date
Analysis Date
120 201120 0 994120 096120 272
4/30/02
LowLimit HighLimit RPD Ref Val
80808080
Piep Date
Analysis Date
120 2013120 0 986120 1 015120 2 547
4/23/02
LowLimit HighLimit RPD Ref Val
8080
120 0120 0
Run ID L_IC-1_020430A
SeqNo 23005
%RPD RPDLimit Qual
0000
Run ID L IC-1 020423A
SeqNo 20976
%RPD RPDLimit Qual
280 250 25
206 2500368 25
Run ID L_IC-1_020430A
SeqNo 23007
%RPD RPDLimit Qual '
231 25
1 43 250491 25
2 14 25 i
Run ID L_IC-1_020423A
SeqNo 20977
%RPD RPDLimit Qual
00 S i
Qualif icis- ND - Not Detected at the Repoitmg Limit C - Unspiked sample >5 times the amount spiked
Jl - MS or MSD outside accepance limits LCS acceptable R - RPD outside accepted lecoveiy limits
J This concentiation is consideied an estimate due to LCS failure
B - Analyte detected in the associated Method Blank
Page 2 of 26
Date: 16-May-02
CLIENT: RSSNWork Order: L0204322Project: GH-3F 300 W
ANALYTICAL QC SUMMARY REPORTTest Method: EPA 300.0
Sample ID L0204261-001 AMS
Analyte
Chlonde
Sulfate
Sample I D L0204323-00 1 BMS
Analyte
Chlonde
Sulfate
Sample ID L02042 1 7-00 1 AMS
Analyte
SampType MS
Batch ID R2742
Result
131 6
3659
SampType MS
Batch ID R2993
Result
3970
5130
SampType MS
Batch ID R2993
Result
TestCode 300_W
TestNo E300
PQL SPK value
10 100
10 100
TestCode 300_W
TestNo E300
PQL SPK value
200 2000
200 2000
TestCode 300_W
TestNo E300
PQL SPK value
Units mg/L
SPKRefVai
353
2592
Units mg/L
SPKRefVai
2200
3512
Units mg/L
SPKRefVai
Piep Date
Analysis Date 4/23/02
%REC LowLimit HighLimit RPD Ref Val
963 80 120 0
107 80 120 0
Prep Date
Analysis Date 4/30/02
%REC LowLimit HighLimit RPD Ref Val
88 5 80 120 0
809 80 120 0
Prep Date
Analysis Date 4/30/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_IC-1_020423A
SeqNo 20978
%RPD RPDLimit Qual
0
0
Run ID L_IC-1_020430A
SeqNo 23008
%RPD RPDLimit Qual
0
0
Run ID L_IC-I_020430A ,
SeqNo 23541
%RPD RPDLimit Qual
Nitrate, as N 2448 1 0 10 1422 103 80 120
Qualifiers: ND - Not Detected at the Repoitmg Limit C - Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted iccoveiy limits
J - This concentiation is consideied an estimate due to LCS failure
B - Analyte detected in the associated Method Blank
Page 3 of 26
Date: 16-May-02
CLIENT: RSSNWork Order: L0204322Project: GH-3F
Sample ID MB-R1591
Analyte
Aluminum
Barium
Calcium
Iron
Magnesium
Potassium
Sodium
Vanadium
Sample ID LCS-R1591
Analyte
Aluminum
Barium
Calcium
Iron
Magnesium
Potassium
Sodium
Vanadium
Sample ID L0204322-003A
Analyte
Aluminum
Barium
Calcium
Iron
ANALYTICAL QC SUMMARY REPORT
SampType MBLK
Batch ID RJU591
Result
NDNDNDNDND
NDNDND
SampType LCS
Batch ID R_R1591
Result
1 041 024
2059
1 1052033
2079
19405161
SampType MS
Batch ID R_R1591
Result
1 15
0969
6461 008
TestCode
TestNo
PQL
0050
00050
0500 1005020
05000050
TestCode
TestNo
PQL
0050
00050
0500 1005020
05000050
TestCode
TestNo
PQL
0050
00050
0500 10
6010WJD
SYV6010B
SPK value
6010W_D
SW6010B
SPK value
11
201
2020
2005
6010W_D
SW6010B
SPK value
11
201
6010W_D
Units mg/L
SPKRefVai
Units mg/L
SPKRefVai
00
0000
00
Units mg/L
SPKRefVai
0099
001958
6180
Test Method: SW 6010B-Diss
Pi cp Date
Analysis Date 4/23/02
%REC LowLimit HighLimit RPD Ref Val
Piep Date
Analysis Date 4/23/02
%REC LowLimit HighLimit RPD Ref Val
104 85102 85103 85110 85102 85104 85
97 85103 85
Piep Date
Analysis Date
115 0115 0115 0115 0
115 0115 0
115 0115 0
4/23/02
%REC LowLimit HighLnnit RPD Ref Val
105 75949 75140 75101 75
125 0125 0125 0125 0
Run ID SUB-1591
SeqNo 29920
%RPD RPDLimit
Run ID SUB-1591
SeqNo 29919
%RPD RPDLimit
00000000
Run ID SUB-1591
SeqNo 29996
%RPD RPDLimit
0000
Qual
Qual
Qual
C
Qualifiers: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted iccoveiy limits
J - This concentiation is consideied an estimate due to LCS fai luie
B - Analyte detected in the associated Method Blank
Page 4 of 26
Date: 16-May-02
CLIENT: RSSNWork Order: L0204322Project: GH-3F
Sample ID L0204322-003A
Analyte
Magnesium
Potassium
Vanadium
Sample ID L0204322-003A
Analyte
Aluminum
Banum
Calcium
Iron
Magnesium
Potassium
Vanadium
Sampl ype MS
Batch ID R_R1591
Result
19341057
05005
SampType MSD
Batch ID R_R1591
Result
1 110951
6491 014192310320497
TestCode
TestNo
PQL
0502 0
00050
TestCode
TestNo
PQL
0050
00050
0500 1005020
00050
6010W_D
SW6010B
SPK value
202005
6010W_D
SW6010B
SPK value
1
1
201
202005
6010W_D
Units mg/L
ANALYTICAL QC SUMMARY REPORT
Test Method: SW 6010B-Diss
Prep Date
Analysis Date 4/23/02
SPKRefVai
178875
0
Units mg/L
%REC
7791
100
LowLimit
757575
HighLimit
125125125
RPD Ref Val
000
Prep Date
Analysis Date 4/23/02
SPKRefVai
0099
001958
6180
178875
0
%REC
10193 1155101
71 5785994
LowLimit
75757575757575
HighLimit
125
125125125125125125
RPD Ref Val
0
000000
Run ID SUB-1591
SeqNo 29996
%RPD RPDLimit
000
Run ID SUB-1591
SeqNo 29923
%RPD RPDLimit
0
000000
Qual
Qual
C
C
Qualifiers: ND - Not Detected at the Repoitmg Limit C - Unspiked sample >5 times the amount spiked
Jl - MS or MSD outside accepance limits LCS acceptable R - RPD outside accepted recoveiy limits
J - This concentiation is consideied an estimate due to LCS f a i l u i e
B - Analyte detected in the associated Method Blank
Page 5 of 26
Date: 16-May-02
CLIENT: RSSNWork Order: L0204322Project: GH-3F
Sample ID MB-793
Analyte
Aluminum
Barium
Calcium
Iron
Magnesium
Potassium
Sodium
Vanadium
Sample ID LCS-793
Analyte
Aluminum
Barium
Calcium
Iron
Magnesium
Potassium
Sodium
Vanadium
Sample ID R02Q4220-001BMS
Analyte
Barium
Sodium
ANALYTICAL QC SUMMARY REPORT
SampType MBLK
Batch ID R_793
Result
NDNDNDNDNDNDNDND
SampType LCS
Batch ID R_793
Result
1 071 081209
1 11621 1921 26
197
05509
SampType MS
Batch ID R_793
Result
1 461520
TestCode
TestNo
PQL
0050
00050
0500 1005020
05000050
TestCode
TestNo
PQL
0050
00050
0500 100502 0
050
00050
TestCode
TestNo
PQL
00050
050
6010WJT
6010WJT Units mg/L
SW6010B
SPK value SPKRefVai
6010W_T Units mg/L
SW6010B
SPK value SPKRefVai
1 01 0
20 01 0
20 020 0
20 0
05 0
6010\V_T Units mg/L
SW6010B
SPK value SPKRefVai
1 0446
20 1490
Test Method: SW 6010B-Total
Prep Date
Analysis Date
4/23/02
4/24/02
%REC LowLimit HighLimit RPD Ref Val
Piep Date
Analysis Date
4/23/02
4/24/02
%REC LowLimit HighLimit RPD Ref Val
107 85108 85104 85112 85106 85106 85
98 5 85
110 85
Piep Date
Analysis Date
115 0115 0115 0115 0115 0115 0115 0
115 0
4/23/02
4/24/02
%REC LowLimit HighLimit RPD Ref Val
101 75150 75
125 0125 0
Run ID SUB-1616
SeqNo 29974
%RPD RPDLimit Qual
Run ID SUB-1616
SeqNo 29973
%RPD RPDLimit Qual
00000000
Run ID SUB-1616
SeqNo 29975
%RPD RPDLimit Qual
00 C
Qualifiers: ND - Not Detected at the Repotting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R RPD outside accepted iccovery limits
J - This concenliation is consideied an estimate due to LCS fai luie
B - Analyte detected in the associated Method Blank
Page 6 of 26
Date; 16-May-02
CLIENT: RSSNWork Order: L0204322Project: GH-3F
Sample ID R0204220-001BMSD
Analyte
Barium
Sodium
Sample ID R0204220-001BDUP
Analyte
Aluminum
Barium
Calcium
Iron
Magnesium
Potassium
Sodium
Vanadium
ANALYTICAL QC SUMMARY REPORT
SampType MSD
Batch ID R_793
Result
1 452
1490
SampType DUP
Batch ID R_793
Result
NDNDND
NDNDNDNDND
TestCode
TestNo
PQL
00050
050
TestCode
TestNo
PQL
0050
00050
050
0 100502 0
05000050
6010WJT
SW6010B
SPK value
1
20
6010WJT
SW6010B
SPK value
000
00000
6010WJT
Units mg/L
SPKRefVai
0446
1490
Units mg/L
SPKRefVai
000
00000
Test Method: SW 6010B-Total
%REC
101
0
%REC
00000000
Piep Date
Analysis Date
4/23/02
4/24/02
LowLimit HighLimit
Piep Date
Analysis Date
4/23/02
4/24/02
LowLimit HighLimit
00000000
00000000
RPD Ref Val
00
RPD Rei Val
00
000000
Run ID SUB-1616
SeqNo 29976
%RPD RPDLimit Qual
0
0
Run ID SUB-1616
SeqNo 29972
%RPD RPDLimit Qual
00000000
Quahfiei s: ND - Not Detected at the Repoiting Limit C - Unspiked sample >5 times the amount spiked
II - MS 01 MSD outside acccpance limits LCS acceptable R - RPD outside accepted recovery limits
] - This concentiation is consideied an estimate due to LCS failure
B - Analytt detected in the associated Method Blank
Page 7 of 26
Date: l6-May-02
CLIENT: RSSNWork Order: L0204322Project: GII-3F
Sample ID MB-R1615
Analyte
Antimony
Arsenic
Beryllium
Cadmium
Chiomium
Cobalt
Copper
Lead
Manganese
Nickel
Selenium
Silver
Thallium
Zinc
Sample ID LCS-R1615
Analyte
Antimony
Arsenic
Beiyllium
Cadmium
Chromium
Cobalt
Coppei
Lead
Manganese
Nickel
Selenium
Quahficis: ND -
SampType MBLK
Batch ID R_R1615
Result
NDNDNDNDND
NDNDNDNDNDNDNDNDND
SampType LCS
Batch ID R_R1615
Result
0 056280 09946
009871
0 05657
005339
005418
005261
0 05243
005574
0 05439
0 1082
Not Detected at the Repoiting Limit
ANALYTICAL QC SUMMARY REPORT
6020W_D Test Method: SW 6020-Diss I
TestCode 6020 W_D Units mg/L Piep Date
TestNo SW6020 Analysis Date 4/24/02
PQL SPK value SPKRefVai %REC LowLimit HighLimit
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
OOOIO
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
0 00040
O O O I O
TestCode 6020W_D Units mg/L Piep Date
TestNo SW6020 Analysis Date 4/24/02
PQL SPK value SPKRefVai %REC LowLimit HighLimit
O O O I O 005 0 113 85 115
O O O I O 01 0 995 85 115
O O O I O 01 0 987 85 115
O O O I O 005 0 113 85 115
O O O I O 005 0 107 85 115
O O O I O 005 0 108 85 115
O O O I O 005 0 105 85 115
OOOIO 005 0 105 85 115
O O O I O 005 0 111 85 115
O O O I O 005 0 109 85 115
O O O I O 01 0 108 85 115
C - Unspiked sample >5 times the amount spiked
Run ID SUB-1615
SeqNo 29928
RPD Ref Val %RPD RPDLimit Qual
<
Run ID SUB-1615
SeqNo 29927
RPD Ref Val %RPD RPDLimit Qual
0 00 00 00 00 0
0 0
0 0
0 00 0
0 0
0 0
B - Analyte detected in the associated Method Blank
Jl - MS or MSD outside acccpance limits LCS acceptable R - RPD outside accepted recovery limits
J - This concentialion is consideied an estimate due to LCS fa i lu ie
Page 8 of 26
Date: 16-May-02
CLIENT: RSSNWork Order: L0204322
Project: GII-3F
Sample ID LCS-R1615
Analyte
Silver
Thallium
Zinc
Sample ID L0204310-003A
Analyte
Antimony
Arsenic
Beiylhum
Cadmium
Chromium
Cobalt
Copper
Lead
Manganese
Nickel
Selenium
Silvci
Thal l ium
Zinc
Sample ID L0204310-003A
Analyte
Antimony
Arsenic
Beiylhum
SampType LCS
Batch ID R_R1615
Result
0 111
0 05628
005417
SampType MS
Batch ID R_R1615
Result
0 04629
0 1462
0 1402
00442
00634
005759
006179
004691
3573
0 06069
0 1298
0 1021
005421
0223
Samp I ype MSD
Batch ID R_R1615
Result
0 05058
0 1459
0 1423
TestCode
TestNo
PQL
O O O I O
0 00040
O O O I O
TestCode
TestNo
PQL
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I OO O O I O
O O O I OO O O I O
O O O I O
0 00040
O O O I O
TestCode
TestNo
PQL
O O O I O
O O O I O
O O O I O
6020W_D
SW6020
SPK value
0 1
005
005
6020W_D
SW6020
SPK value
005
0 1
0 1
005
005
005
005
005
005
005
0 1
0 1
005
005
6020\V_D
SW6020
SPK value
005
0 1
0 1
6020W_D
Units mg/L
SPKRefVai
0
0
0
Units mg/L
SPKRefVai
000135
00376
0
00 00384
0 00277
000489
0
4014
0 00706
0 00596
0
0
0 104
Units mg/L
SPKRefVai
000135
00376
0
ANALYTICAL QC SUMMARY REPORTTest Method: SW 6020-Diss
%REC
111113
108
%REC
899
109
140
884
119
110
114
93 8
-882
107
124
102
108
238
%REC
985
108
142
Piep Date
Analysis Date 4/24/02
LowLimit HighLimit
85
85
85
Pi ep Date
Analysis Date
115
115
115
4/24/02
LowLimit HighLimit
75
75
75
75
75
75
75
75
75
75
75
75
75
75
Piep Date
Analysis Date
125
125
125
125
125
125
125
125
125
125
125
125
125
125
4/24/02
LowLimit HighLimit
RPD Ref Val
0
0
0
RPD Ref Val
0
0
0
0
0000000000
RPD Ref Val
000
Run ID SUB-1615
SeqNo 29927
%RPD RPDLimit
0
0
0
Run ID SUB-1615
SeqNo 29929
%RPD RPDI unit
0
0
0
00
0
0
0
0
0
0
0
0
0
Run ID SUB-1615
SeqNo 29930
%RPD RPDLimit
0
0
0
Qual
Qual
Jl
C
Jl
Qual
Jl
Qualifiers: ND - Not Detected at the Repotting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS or MSD outside accepance l imits LCS acceptable R- RPD outside accepted lecovery limits
J - I his conccnlialion is consideied an estimate due to LCS failure
B - Analyte detected in the associated Method Blank
Page 9 of 26
Date: !6-May-02
CLIENT: RSSN
Work Order: L0204322Project: GH-3F
Sample ID L0204310-003A
Analyte
Cadmium
Cluomium
Cobalt
Copper
Lead
Manganese
Nickel
Selenium
Silver
Thallium
Zinc
Sample ID L0204310-003A
Analyte
Antimony
Arsenic
Beiylhum
Cadmium
Chiomium
Cobalt
Copper
Lead
Manganese
Nickel
Selenium
Silver
Thall ium
Zinc
ANALYTICAL QC SUMMARY REPORT
SampType MSD
Batch ID R_R1615
Result
00441
0 06237
00572
005881
004616
3581
006051
0 1274
0 101
0 05398
01804
SampType DUP
Batch ID R_R1615
Result
ND0 03632
NDND
0 00466
0 00294
0 00568
ND407
0 00724
NDNDND
0 108
TestCode
TestNo
PQL
O O O I O
O O O I O
O O O I O
O O O I OO O O I O
O O O I O
O O O I OOOOIOO O O I O
0 00040
O O O I O
TestCode
TestNo
PQL
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I OO O O I O
O O O I O
O O O I O
O O O I O
O O O I O
0 00040
O O O I O
6020W_D
SW6020
SPK value
0050050050050050050050 1
0 1
005005
6020W_D
SW6020
SPK value
00000000000000
6020W_D
Units mg/L
SPKRefVai
00 00384
0 00277
0 00489
04014
0 00706
0 00596
00
0 104
Units mg/L
SPKRefVai
0000
0
000000000
Test Method: SW 6020-Diss
%REC
88 2
117109
108923
-866
107121101108153
%REC
00000
0000000
00
Prep Date
Analysis Date 4/24/02
LowLimit HighLimit
Piep Date
Analysis Date 4/24/02
LowLimit HighLimit
00000
0000000
00
00000
000000000
RPD Ref Val
00000000000
RPD Ref Val
000000000
00000
Run ID SUB-1615
SeqNo 29930
%RPD RPDLimit Qual
0
00000 C
00000 Jl
Run ID SUB-1615
SeqNo 29926
%RPD RPDLimit Qual
00000000000000
— rQualifiers: ND - Not Detected at the Repotting Limit C Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R RPD outside accepted lecoveiy limits
J - This concentration is consideied an estimate due to LCS fai luie
B - Analyte detected in the associated Method Blank
Page 10 of 26
Date: 16-May-02
r
CLIENT: RSSNWork Order: L0204322Project: GH-3F
Sample ID MB-795
Analyte
AntimonyArsenic
BerylliumCadmiumChromiumCobaltCopperLeadManganeseNickel
SeleniumSilverThalliumZinc
Sample ID LCS-795
Analyte
AntimonyArsenicBeiyl l iumCadmium
Chromium
CobaltCopperLeadManganeseNickelSelenium
SampType MBLK
Batch ID R_795
Result
NDNDNDNDNDNDNDNDNDND
NDNDNDND
SampType LCS
Batch ID R_795
Result
0 056950 094 1 5
0 1524
0051900537
005475005670054500494
0055400956
6020WJT
TestCode 6020WJT Units mg/L
TestNo SW6020
PQL SPK value SPKRefVai
0005000050000500005000050000500005000050000500005000050000500005000050
TestCode 6020WJT Units mg/L
TestNo SW6020
PQL SPK value SPKRefVai
0 0050 0 05 00 0050 0 1 00 0050 0 1 00 0050 0 05 0
0 0050 0 05 00 0050 0 05 00 0050 0 05 00 0050 0 05 00 0050 0 05 00 0050 0 05 00 0050 0 1 0
ANALYTICAL QC SUMMARY REPORT
Pi ep Date
Analysis Date
Test Method: SW 6020-Total
4/23/02 Run ID SUB-1627
4/24/02 SeqNo 29953
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Piep Date
Analysis Date
4/23/02 Run ID SUB-1627
4/24/02 SeqNo 29952
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
114 85942 85152 85
104 85107 85
110 85113 85109 85
988 85
111 8595 6 85
115 0 0115 0 0115 0 0
115 0 0115 0 0115 0 0115 0 0115 0 0115 0 0115 0 0115 0 0
Qualifiers: ND - Not Detected at the Repotting Limit C - Unspiked sample >5 times the amount spiked
Jl MS 01 MSD outside accepance limits LCS acceptable R RPD outside accepted lecoveiy limits
} - This concentiation is consideied an estimate due to LCS fa i lu ie
B Analyte detected in the associated Method Blank
Page 11 of 26
Date: 16-May-D2
CLIENT: RSSNWork Order: L0204322Project: GH-3F
Sample ID LCS-795
Analyte
Silver
Thallium
Zinc
Sample ID R0204208-001BMS
Analyte
Antimony
Arsenic
Beiyllium
Cadmium
Chromium
Cobalt
Copper
Lead
Manganese
Nickel
Selenium
Silvei
Thallium
Zinc
Sample ID R0204208-001BMSD
Analyte
Antimony
Aisemc
Beiylhum
ANALYTICAL QC SUMMARY REPORT
SampType LCS
Batch ID R_795
Result
0 1364
00547
0 04785
SampType MS
Batch ID R_795
Result
00629
0 1046
0 1637
0 05525
0 05645
0059
006515
005685
00643
0 06255
0 1049
0 1384
0 06405
0 1304
SampType MSD
Batch ID R_795
Result
0 05965
0 0966
0 1534
TestCode
TestNo
6020WJT
SW6020
PQL SPK value
00050
00050
00050
TestCode
TestNo
PQL
00050
00050
00050
00050
00050
00050
00050
00050
00050
00050
00050
00050
00050
00050
TestCode
TestNo
PQL
00050
00050
00050
0 1
005
005
6020WJT
SW6020
SPK value
005
0 1
0 1
005
005
005
005
005
005
005
0 1
01
005
005
6020W_T
SVV6020
SPK value
005
0 1
0 1
6020W_T
Units mg/L
SPKRefVai
0
0
0
Units mg/L
SPKRefVai
0
0
0
0
00055
0
0 00675
0
00105
0
0
0
0
008105
Units mg/L
SPKRefVai
0
0
0
Test Method: SW 6020-TotaI
%REC
136
109
957
%REC
126
105
164
110
102
118
117
114
108
125
105
138
128
987
%REC
119
966
153
Piep Date
Analysis Date
4/23/02
4/24/02
LowLimit HighLimit
85
85
85
Piep Date
Analysis Date
115
115
115
4/23/02
4/24/02
LowLimit HighLimit
75
75
75
75
75
75
75
75
75
75
75
75
75
75
Pi ep Date
Analysis Date
125
125
125
125
125
125
125
125
125
125
125
125
125
125
4/23/02
4/24/02
LowLimit HighLimit
RPD Ref Val
0
0
0
RPD Ref Val
0
0
0
0
0
0
0
0
0
0
0
0
0
0
RPD Ref Val
0
0
0
Run ID SUB-1627
SeqNo 29952
%RPD RPDLimit Qual '
0
0
0
Run ID SUB-1627
SeqNo 29954
%RPD RPDLimit Qual
0
0
0 Jl
0
0
0
0
0
0
0
0
0 II
0 Jl
0
Run ID SUB-1627
SeqNo 29955
%RPD RPDLimit Qual
000 Jl
Qualifiers: ND - Not Detected at the Repotting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted lecoveiy limits
J - This concentiation is consideied an estimate due to LCS failuie
B - Analyte detected in the associated Method Blank
Page 12 of 26
Date: 16-May-02
CLIENT: RSSNWork Order: L0204322Project: GH-3F
Sample ID R0204208-001BMSD
Analyte
Cadmium
Chiomium
Cobalt
Copper
Lead
Manganese
Nickel
Selenium
Silver
Thallium
Zinc
Sample ID R0204208-001BDUP
Analyte
Antimony
Arsenic
BeiyHium
Cadmium
Chromium
Cobalt
Copper
Lead
Manganese
Nickel
Selenium
Silver
Thallium
Zinc
ANALYTICAL QC SUMMARY REPORT
SampType MSD
Batch ID R_795
Result
00516
005325
0 05525
0 06085
00528
0 05925
0 05675
0 1026
0 1308
005930 1252
SampType DUP
Batch ID R_795
Result
ND
ND
ND
NDNDND
00061ND
00094NDNDNDND
0 07405
TestCode
TestNo
PQL
00050
00050
00050
00050
00050
00050
00050
00050
00050
00050
00050
TestCode
TestNo
PQL
00050
00050
00050
00050
00050
00050
0005000050
000500005000050
00050
00050
00050
6020WJT
SW6020
SPK value
005
005
005
005
005
005
005
0 1
01
005
005
6020W_T
SW6020
SPK value
0
0
0
0
0
0
0
0
0
0
0
0
0
0
6020WJT
Units mg/L
SPKRefVai
0
00055
0
0 00675
0
00105
0
0
0
0
008105
Units mg/L
SPKRefVai
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Test Method: SW 6020-Total
%REC
103
955
110
108
106
975
114
103
131
119
884
%REC
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Pi ep Date
Analysis Date
4/23/02
4/24/02
LowLimit HighLimit
Piep Date
Analysis Date
4/23/02
4/24/02
LowLimit HighLimit
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
RPD Ref Val
0
0
0
0
0
0
0
0
0
0
0
RPD Ref Val
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Run ID SUB-1627
SeqNo 29955
%RPD RPDLimit Qual
0000000
o0 Jl
00
Run ID SUB-1627
SeqNo 29951
%RPD RPDLimit Qual
0
0
0
0
0
0|
00000000
Qualifiers: ND - Not Detected at the Repoitmg Limit C - Unspiked sample >5 times the amount spiked
Jl - MS or MSD oukidc accepance limits LCS acceptable R - RPD outside accepted iccoveiy limits
J - This concentiation is consideied an estimate due to LCS failure
B - Analyte detected in the assouated Method Blank
Page 13 of 26
Date: 16-May-02
CLIENT: RSSNWork Order: L0204322Project: GH-3F
Sample ID Method Blank 02
Analyte
1 ,1 ,2-Ti ichloroti ifluoroethane
MTBE
Acetone
Benzene
Bi omobenzene
Biomochlotomethane
Bi omodichloromethane
Biomoform
Bromomethane
2-Butanone
n-Butylbcnzene
sec-Butylbenzene
tei t-Butylbenzene
Carbon disulfide
Carbon tetrachlonde
ChlorobenzeneChloroethane
2-Chloioethyl vinyl etheiChloioform
Chloiome thane
2-Chloiotoluene
4-Chloiotolucne
Dibi omochloi omcthane
1 ,2-Dibi omo-3-chloropi opane
1 ,2-Dibiomoethane
Dibi omome thane
1 ,2-Dichloi obenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichloiodifluoiomethane
Qualifiers: N D - N o t
SampType MBLK
Batch ID R2684
Result
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
NDNDND
ND
NDNDND
Detected at the Reporting Limit
ANALYTICAL QC SUMMARY REPORT
8260_W Test Method: SW8260B
TestCode 8260_W Units ng/L Piep Date Run ID L_VOAMS-2_020423A
TestNo SW8260B Analysis Date 4/23/02 SeqNo 20642
PQL SPK value SPKRefVai %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
505025505050505050255050505050
50505050505050
505050
50
50505050
C - Unspiked sample >5 times the amount spiked B - Analyte detected in the associated Method Blank
Jl - MS or MSD outside accepance limits LCS acceptable R - RPD outside accepted lecovery limits
J - This concentiation is consideied an estimate due to LCS fa i lu ie
Page 14 of 26
Date: 16-May-02
CLIENT: RSSNWork Order: L0204322Project: GH-3F
ANALYTICAL QC SUMMARY REPORT8260 W Test Method: SW8260B
Sample ID Method Blank 02 SampType MBLK
Analyte
Batch ID R2684
Result
TestCode 8260_W Units ug/L
TestNo SW8260B
PQL SPK value SPKRefVai
Prep Date
Analysis Date 4/23/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_VOAMS-2_020423A '
SeqNo 20642
%RPD RPDLimit Qual
1,1-Dichloioethane1,2-Dichloi oethane1,1-Dichloioethene
cis-1,2-Dichloroetheneti ans-1,2-Dichloi oethene1,2-Dichloropropane1,3-Dichloropropane2,2-Dichloropropane1,1-Dichloropropenecis-l,3-Dichloropropene
trans-1,3-DichloiopropcneEthylbcnzeneHexachloi obutadiene2-HexanonelodomethaneIsopropylbenzenep-IsopiopyltolueneMethylene chlonde4-Methyl-2-pentanoneNaphthalene
n-PiopylbenzeneStyiene
1,1,2,2-Teti achloi oethaneTetiachloi oetheneToluene
1,2,3-Ti ichloiobenzcne1,2,4-Tnchloiobenzene
1,1,2-Tnchloi oethaneTnchloroctheneTiichlorofluoiomethane
NDND
NDNDNDNDNDNDNDND
NDNDND
NDNDNDNDNDNDND
NDND
NDNDNDNDNDNDNDND
5050
505050
5050
505050505050255050505025105050
5050
505050505050
Qualifiers: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times the amount spiked
11 - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted lecoveiy limits
J - This concentiation is consideied an estimate due to LCS failuie
B - Analyte detected in the associated Method Blank
Page 15 of 26
Date: !6-May-02
CLIENT: RSSNWork Order: L0204322Project: GII-3F
Sample ID Method Blank 02
Analyte
1 ,2,3-Tnchloropropane
1 ,2,4-Tnmethylbenzene
1 ,3,5-Tnmethylbenzeiie
Vinyl acetate
Vinyl chlonde
o-Xylene
m,p-Xylene
Surr Dibromofluoromethane
Surr Toluene-d8
Surr 4-Biomofluorobenzene
Sample ID Vstd050CCV02042
Analyte
Acetone
Benzene
Bi omoform
Biomomethane
Chlorobenzene
Chlorofoim
Chloiomethane
Dichloiodifluoiornethane
1,1-Dichloi oethane
1,1-Dichloroethene
1,2-Dichloropiopane
Clhylbcnzene
1 , 1 ,2 ,2 -Teti achloi oethane
Toluene
Tnchloi oethene
SampType MBLK
Batch ID R2684
Result
NDNDNDNDNDNDND
4804
5357
4476
SampType LCS
Batch ID R2684
Result
37814857
3986
78 3451 774996
6859
6665249
4887
49 165039
5234
4647
47 15
TestCode
TestNo
PQL
5 050505050
5010
505050
TestCode
TestNo
PQL
2550505050505050505 05050
505050
8260_W
SW8260B
SPK value
505050
8260_W
SW8260B
SPK value
505050505050505050
505050505050
8260_W
Units ug/L
SPKRefVai
000
Units ug/L
SPK Ref Val
000000000000
000
ANALYTICAL QC SUMMARY REPORT
Test Method: SW8260B
%REC
96 1107
895
%REC
75697 1
797157104
999137133105
97798 3
101105
929943
Prep Date
Analysis Date 4/23/02
LowLimit HighLimit
80808562
Piep Date
Analysis Date
120119139
4/23/02
LowLimit HighLimit
7070707070807070708080
80708070
130130130130130120130130130
120120120
130120130
RPD Ref Val
000
RPD Ref Val
000000000000000
Run ID L_VOAMS-2_020423A
SeqNo 20642
%RPD RPDLimit Qual
i
000
Run ID L_VOAMS-2_020423A
SeqNo 20645
%RPD RPDLimit Qual
00
00 S
000 S
0 S
0000000
Qualifiers: ND - Not Detected at the Repoiting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted lecoveiy limits
J - This concentiatlon is consideied an estimate due to LCS fai luie
B - Analyte detected in the associated Method Blank
Page 16 of 26
Date: 16-May-02
CLIENT: RSSNWork Order: L0204322Project: GH-3F
Sample ID Vstd050CCV02042
Analyte
Vinyl chlonde
Sun Dibiomofluoiomethanc
Sun Toluene-d8
SUIT 4-Bromofluorobcnzene
Sample ID L0204322-001A MS
Analyte
Acetone
BenzeneBromomethane
Chlorobenzene
Chloiome thane
Dichloiodifluoiomethane
1,1-Dichloroethene
Toluene
Trichloioethene
Vinyl chlonde
Sun Dibiomofluoiomethane
Sun Toluene-d8
Sun 4-Biomofluorobcnzene
Sample ID L0204322-001 A MSD
Analyte
Acetone
Benzene
Bromomethane
ANALYTICAL QC SUMMARY REPORT
SampType LCS
Batch ID R2684
Result
58 1744955268
42 1
SampType MS
Batch ID R2684
Result
51 335436
75.95366
8647
8365
58 155299
52 186921
46695546
4873
SampType MSD
Batch ID R2684
Result
4805
4938
67 13
Qualifiers: ND - Not Detected at the Repoiting Limit
TestCode 8260_W
TestNo SW8260B
PQL SPK value
50 5050 5050 5050 50
TestCode 8260_W
TestNo SW8260B
PQL SPK value
25 5050 505.0 5050 5050 5050 5050 5050 5050 5050 5050 5050 50
50 50
TestCode 8260_W
TestNo SW8260B
PQL SPK value
25 5050 5050 50
8260_W
Units ng/L
SPKRefVai
0000
Units ug/L
SPKRefVai
0000000000000
Units ug/L
SPKRefVai
00
0
C - Unspiked sample >5 times
Test Method: SW8260B
Piep Date
Analysis Date 4/23/02
%REC LowLimit HighLimit
116 80 120899 80 120105 808 119
842 562 139
Piep Date
Analysis Date 4/23/02
%REC LowLimit HighLimit
103 70 130109 70 130152 70 130107 70 130173 70 130167 70 130116 80 120106 80 120104 70 130138 80 120
93 4 92 6 108111 957 112
97 5 85 3 104
Pi ep Date
Analysis Date 4/23/02
%REC LowLimit HighLimit
96 1 70 130988 70 130
134 70 130
the amount spiked
RPD Ref Val
0000
RPD Ref Val
0000000000000
RPD Ref Val
51 3354 36
759
Run ID L_VOAMS-2_020423A
SeqNo 20645
%RPD RPDLimit Qual
0000
Run ID L_VOAMS-2_020423A
SeqNo 20643
%RPD RPDLimit Qual
000 S00 S
0 S
0000 S
00
o
Run ID L_VOAMS-2_020423A
SeqNo 20644
%RPD RPDLimit Qual
660 25960 25123 25 S
B - Analyte detected in the associated Method Blank
Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted recovery limits
J - This concentiation is consideied an estimate due to LCS failuie
Page 17 of 26
Date: !6-May-02
CLIENT: RSSNWork Order: L0204322Project: GH-3F 8260 W
ANALYTICAL QC SUMMARY REPORTTest Method: SW8260B
Sample ID L0204322-001A MSD SampType MSD
Batch ID R2684
Analyte
Chlorobenzene
ChloiomethaneDichlorodifluoiomethane
1 , 1 -Dichloi oethene
Toluene
Tnchloi oethene
Vinyl chlorideSurr Dibiomofluoiomethane
Surr Toluene-d8Sun 4-Bromofluorobenzene
Result
4966
6853
7924
5277
47 214778
5748
4707
5357
4505
TestCode 8260_W Units ug/L Prep Date
TestNo SW8260B
PQL
50505050505050505050
SPK value
5050505050
5050505050
SPKRefVai
0000000000
%REC
993137158106
944956115
94 1
10790 1
Analysis Date 4/23/02
LowLimit
70707080807080
92 6
957853
HighLimit
130130130120120130
120108112104
RPD Ref Val
53 668647
8365
581552 9952 186921
000
Run ID L_VOAMS-2_020423A
SeqNo 20644
%RPD
77423 154197011 5880185
0
00
RPDLimit Qual ,
2525 S25 S
2525
2525000
Qualifiers: ND - Not Detected at the Repoiting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS or MSD outside accepance l imits LCS acceptable R - RPD outside accepted lecoveiy limits
J - This concentiation is consideied an estimate due to LCS failuie
B - Analyte detected in the associated Method Blank
Page 18 of 26
Date: 16-May-02
CLIENT: RSSNWork Order: L0204322Project: GII-3F ALK W
ANALYTICAL QC SUMMARY REPORTTest Method: SM2320 B
Sample ID MB-R2983
Analyte
Alkalinity, Bicaibonate (As CaCO3)
Alkalinity, Caibonate (As CaCO3)Hydioxide(AsCaCO3)
Alkalinity, Total (As CaCO3)
Sample ID LCS-R2983
Analyte
Alkalinity, Total (As CaCO3)
Sample ID LCSD-R2983
Analyte
Alkalinity, Total (As CaCO3)
Sample ID L0204322-001BDUP
Analyte
Alkalinity, Bicaibonate (As CaCO3)
Alkalinity, Caibonate (As CaCO3)
Hydioxide(AsCaCO3)
Alkalinity, Total (As CaCO3)
SampType MBLK
Batch ID R2983
Result
NDNDNDND
SampType LCS
Batch ID R2983
Result
144
SampType LCSD
Batch ID R2983
Result
122
SampType DUP
Batch ID R2983
Result
ND
74ND
74
TestCode
TestNo
PQL
25252525
TestCode
TestNo
PQL
25
TestCode
TestNo
PQL
25
TestCode
TestNo
PQL
252525
25
ALK_W
M2320 B
SPK value
ALK_W
M2320 B
SPK value
125
ALK_W
M2320 B
SPK value
125
ALK_W
M2320 B
SPK value
000
0
Units mg/L
SPKRefVai
Units mg/L
SPKRefVai
0
Units mg/L
SPKRefVai
0
Units mg/L
SPKRefVai
0
00
0
Prep Date
Analysis Date 4/29/02
%REC LowLimit HighLimit RPD Ref Val
Prep Date
Analysis Date 4/29/02
%REC LowLimit HighLimit RPD Ref Val
115 80
Pi ep Date
Analysis Date
120 0
4/29/02
%REC LowLimit HighLimit RPD Ref Val
976 80
Prep Date
Analysis Date
120 144
4/29/02
%RBC LowLimit HighLimit RPD Rei Val
0 0
0 00 0
0 0
0 00 750 0
0 75
Run ID L_AT1TR-1_020429A '
SeqNo 22904
%RPD RPDLimit Qual j
Run ID L_ATJTR-1_020429A
SeqNo 22903
%RPD RPDLimit Qual
0
Run ID L_ATITR-1_020429A
SeqNo 22906
%RPD RPDLimit Qual
165 25
Run ID L_A1 ITR-1_020429A
SeqNo 22905
%RPD RPDLimit Qual
0 101 34 10
0 .10
1 34 10
Qualifiers: ND - Not Detected at the Repoiting Limit C - Unspiked sample >5 times the amount spiked
II - MS or MSD outside accepance limits LCS acceptable R - RPD outside accepted lecovery limits
I - This concentiation is consideied an estimate due to LCS failuie
B - Analyte detected in the associated Method Blank
Page 19 of 2 6
Date: 16-May-02
CLIENT: RSSN
Work Order: L0204322Project: GH-3F COD
ANALYTICAL QC SUMMARY REPORTTest Method: SM5520 D
Sample ID MB-R2949
Analyte
Chemical Oxygen Demand
SampType MBLK
Batch ID R2949
Result
ND
TestCode COD Units mg/L
TestNo M5220C
PQL SPK value SPKRefVai
10
Piep Date Run ID L_WC_020429C
Analysis Date 4/29/02 SeqNo 22627
%R£C LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Sample ID LCS-R2949
Analyte
Chemical Oxygen Demand
Sample ID LCSD-R2949
Analyte
SampType
Batch ID
SampType
Batch ID
LCS
R2949
Result
533
LCSD
R2949
Result
TestCode
TestNo
PQL
10
TestCode
TestNo
PQL
COD
M5220 C
SPK value
500
COD
M5220 C
SPK value
Units mg/L
SPKRefVai
0
Units mg/L
SPKRefVai
Pi ep Date
Analysis Date 4/29/02
%REC LowLimit HighLimit RPD Ref Val
107 80
Prep Date
Analysis Date
120 0
4/29/02
%REC LowLimit HighLimit RPD Ref Val
Run ID
SeqNo
L_WC_020429C
22626
%RPD
Run ID
SeqNo
0
L_
RPDLimit
\VC_020429C
Qual
22630
%RPD RPDLimit Qual
Chemical Oxygen Demand 503 10 500 101 120 533 579 15
Sample ID L0204310-001BMS SampType MS
Analyte
Batch ID R2949
Result
TestCode COD Units mg/L
TestNo M5220C
PQL SPK value SPKRefVai
Prep Date
Analysis Date 4/29/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L WC 020429C
SeqNo 22628
%RPD RPDLimit Qual
Chemical Oxygen Demand 554 10 4625 75 104 70 130
Sample ID L0204310-001BMSD SampType MSD TestCode COD Units mg/L Piep Date Run ID L_WC_020429C '
Analyte
Batch ID R2949 TestNo M5220 C Analysis Date 4/29/02 SeqNo 22629
Result PQL SPK value SPKRefVai %R£C LowLimit HighLimit RPD Ref Val %RPD RPDI.imit Qual
Chemical Oxygen Demand 546 10 462 5 75 102 70 130 546 25
Qualifieis: ND - Not Detected at the Repotting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted iccoveiy limits
1 - This concentiation is consideied an estimate due to LCS fa i l u i e
B - Analyte detected in the associated Method Blank
Page 20 of 26
Date: 16-May-02
T
CLIENT: RSSN
Work Order: L0204322Project: GH-3F HG 7470 D
ANALYTICAL QC SUMMARY REPORTTest Method: SW 7470-Diss
Sample ID MB-799
Analyte
SampType
Batch ID
MBLK
R_799
Result
TestCode
TestNo
PQL
HG_7470_D
SW7470
SPK value
Units mg/L
SPKRefVai
Piep Date
Analysis Date
%REC LowLimit Hi
4/24/02
4/24/02
ghLimit RPD Ref Val
Run ID
SeqNo
SUB-1625
29941
%RPD RPDLimit Qual
Meicuiy ND 0 00020
Sample ID LCS-799
Analyte
Meicury
Sample ID L0204310-003A
Analyte
Mercury
SampType LCS
Batch ID R_799
Result
0 00499
SampType MS
Batch ID R_799
Result
000521
TestCode HG_7470_D
TestNo S\\7470
PQL SPK value
0 00020 0 005
TestCode HG_7470_D
TestNo SW7470
PQL SPK value
0 00020 0 005
Units mg/L
SPKRefVai
0
Units mg/L
SPKRefVai
0
Prep Date
Analysis Date
4/24/02
4/24/02
%REC LowLimit HighLimit RPD Ref Val
998 85
Pi ep Date
Analysis Date
115 0
4/24/02
4/24/02
%REC LowLimit HighLimit RPD Ref Val
104 85 115 0
Run ID SUB-1625
SeqNo 29940
%RPD RPDLimit
0
Run ID SUB-1625
SeqNo 29942
%RPD RPDLimit
0
Qual
Qual
Sample ID R0204242-003AMS
Analyte
SampType
Batch ID
MS
R_799
Result
TestCode
TestNo
PQL
HG_7470.
SW7470
SPK value
_D Units mg/L
SPKRefVai
Piep Date
Analysis Date
4/24/02
4/24/02
%REC LowLimit HighLimit RPD Ref Val
Run ID
SeqNo
SUB-1625
30020
%RPD RPDLimit
]
Qual
Meicuty 000521 0 00020 0005 104 85 115
Sample ID L02043IO-003A
Analyte
SampType
Batch ID
MSD
R_799
Result
TestCode
TestNo
PQL
HG_7470_D
SW7470
SPK value
Units mg/L
SPKRefVai
Piep Date
Analysis Date
4/24/02
4/24/02
%R£C LowLimit HighLimit RPD Ref Val
Run ID
SeqNo
%RJ
SUB-1625
29943
JD RPDLimit Qual
Meicuiy 00051 0 00020 0005 102
Qualifiers: ND - Not Detected at the Repoitmg Limit C - Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R- RPD outside accepted lecoveiy limits
J - This concent!ation is consideied an estimate due to LCS failure
B - Analyte detected in the associated Method Blank
Page 21 of 26
Date: 16-May-02
CLIENT: RSSNWork Order: L0204322Project: GH-3F HG 7470 D
ANALYTICAL QC SUMMARY REPORTTest Method: SW 7470-Diss
Sample ID. R0204242-003AMSD SampType. MSD TestCode: HG_7470_D Units: mg/L Prep Date: 4/24/02 Run ID: SUB-1625
Analyte
Batch ID: R_799 TestNo: SW7470 Analysis Date. 4/24/02 SeqNo: 30021
Result PQL SPK value SPKRefVai %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Mercury 0.0051 0.00020 0.005 102
Qualifiers: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS or MSD outside accepance limits. LCS acceptable. R - RPD outside accepted recovery limits
J - This concentration is considered an estimate due to LCS failure.
B - Analyte detected in the associated Method Blank
Page 22 of 26
Date: I6-May-02
CLIENT: RSSNWork Order: L0204322Project: GH-3F HG 7470 T
ANALYTICAL QC SUMMARY REPORTTest Method: SW 7470-Total
Sample ID MB-800
Analyte
SampType
Batch ID
MBLK
R_800
Result
TestCode
TestNo
PQL
HG_7470_T
SW7470
SPK value
Units mg/L
SPKRefVai
Prep Date
Analysis Date
4/24/02
4/24/02
%REC LowLimit HighLimit RPD Ref Val
Run ID
SeqNo
SUB-1626
29947
%RPD RPDLimit Qual
Meicury ND 0 00020
Sample ID LCS-800
Analyte
Mercury
Samp Type LCS TestCode HG_7470_T Units mg/L Prep Date 4/24/02 Run ID SUB-1626
Batch ID R_800 TestNo SW7470 Analysis Date 4/24/02 SeqNo 29946
Result PQL SPK value SPKRefVai %R£C LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
000518 000020 0005 0 104 85 115 0 0
Sample ID L0204310-002A
Analyte
SampType
Batch ID
MS
R_800
Result
TestCode
TestNo
PQL
HG_7470_T
SW7470
SPK value
Units mg/L
SPKRefVai
Prep Date
Analysis Date
4/24/02
4/24/02
%REC LowLimit HighLimit RPD Ref Val
Run ID
SeqNo
SUB-1626
29948
%RPD RPDLimit Qual
Mercury 000541 0 00020 0005 108 85 115
Sample ID L0204310-002A
Analyte
SampType
Batch ID
MSD
R_800
Result
TestCode
TestNo
PQL
HG_7470_T
SW7470
SPK value
Units mg/L
SPKRefVai
Prep Date
Analysis Date
4/24/02
4/24/02
%REC LowLimit HighLimit RPD Ref Val
Run ID
SeqNo
%RJ
SUB-1626
29949
'D RPDLimit
!
Qual
Meicuiy 000539 0 00020 0005 108
Sample ID L0204310-002A
Analyte
SampType
Batch ID
DUP
R_800
Result
TestCode
TestNo
PQL
HG_7470_T
SW7470
SPK value
Units mg/L
SPKRefVai
Pi ep Date
Analysis Date
4/24/02
4/24/02
%REC LowLimit HighLimit RPD Ref Val
Run ID
SeqNo
SUB-1626
29945
%RPD RPDLimit Qual
Meicuiy ND 0 00020
Qualifiers: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R- RPD outside accepted lecoveiy limits
J - This concentiation is considcicd an estimate due to LCS failure
B - Analyte detected in the associated Method Blank
Page 23 of 26
Date: 16-May-02
CLIENT: RSSNWork Order: L0204322Project: GH-3F NH3-N W
ANALYTICAL QC SUMMARY REPORTTest Method: SM4500-NII3 C
Sample ID MB-R2996
Analyte
Ammonia, as N
SampType MBLK
Batch ID R2996
Result
ND
TestCode NH3-N_W Units mg/L
TestNo M4500-NH3 C
PQL SPK value SPKRefVai
030
Prep Date Run ID L_\VC_020430A
Analysis Date 4/30/02 SeqNo 23035
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Sample ID LCS-R2996
Analyte
Ammonia, as N
Sample ID LCSD-R2996
Analyte
SampType
Batch ID
SampType
Batch ID
LCS
R2996
Result
1 008
LCSD
R2996
Result
TestCode
TestNo
PQL
030
TestCode
TestNo
PQL
NH3-NJW
M4500-NH3
SPK value
1
NH3-N_W
M4500-NH3
SPK value
Units mg/L
C
SPKRefVai
0
Units mg/L
C
SPKRefVai
Piep
Analysis
Date
Date 4/30/02
%REC LowLimit HighLimit RPD Ref Val
101 83
Piep
Analysis
9
Date
Date
117 0
4/30/02
%REC LowLimit HighLimit RPD Ref Val
Run ID
SeqNo
L_WC_020430A
23034
%RPD RPDLimit
Run ID
SeqNo
0
L_WC_020430A
23037
%RPD RPDLimit
Qual
Qual
Ammonia, as N 101 030 101 839 117 1 008 0 198 25
Sample ID L0204322-001BMS
Analyte
Ammonia, as N
SampType MS TestCode NH3-NJVY Units mg/L Prep Date Run ID L_WC_020430A
Batch ID R2996 TestNo M4500-NH3 C Analysis Date 4/30/02 SeqNo 23036 ,
Result PQL SPK value SPKRefVai %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
1 12 030 1 0 112 764 124 0 0
Qualifiers: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted lecoveiy limits
j - This concentiation is consideied an estimate due to LCS fa i lu ie
B - Analyte detected in the associated Method Blank
Page 24 of 26
Date: 16-May-02
CLIENT: RSSNWork Order: L0204322Project: GH-3F SULF W
ANALYTICAL QC SUMMARY REPORT
Test Method: SM4500-S D
Sample ID MB-R2855 SampType MBLK
Analyte
Batch ID R2855
Result
TestCode SULF_W Units mg/L
TestNo M4500-S D
PQL SPK value SPKRefVai
Piep
Analysis
Date
Date 4/26/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_SPEC-2_020426A
SeqNo 21795
%RPD RPDLimit Qual
Sulfide ND 0030
Sample ID LCS-R2855
Analyte
Sulfide
Sample ID LCSD-R2855
Analyte
SampType
Batch ID
SampType
Batch ID
LCS
R2855
Result
0 107
LCSD
R2855
Result
TestCode
TestNo
PQL
0030
TestCode
TestNo
PQL
SULF_W
M4500-S D
SPK value
0 107
SULF_W
M4500-S D
SPK value
Units mg/L
SPKRefVai
0
Units mg/L
SPKRefVai
Piep Date
Analysis Date 4/26/02
%REC LowLimit HighLimit RPD Ref Val
100 80
Prep Date
Analysis Date
120 0
4/26/02
%REC LowLimit HighLimit RPD Ref Val
Run ID
SeqNo
L_SPEC-2_020426A
21794
%RPD RPDLimit
Run ID
SeqNo
%R
0
Qual
L_SPEC-2_020426A '
21796
>D RPDLimit Qual
Sulfide 0 111 0030 0 107 104 80 120 0 107 367 25
Sample ID L0204310-001BMS SampType MS TestCode SULF_W Units mg/L Prep Date Run ID L_SPEC-2_020426A
Analyte
Sulfide
Batch ID R2855 TestNo M4500-S D Analysis Date 4/26/02 SeqNo 21797
Result PQL SPK value SPKRefVai %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
O H 4 0030 0107 0 107 70 130 0 0
Sample ID L0204310-
Analyte
001BMSD SampType MSD
Batch ID R2855
Result
TestCode SULFJW Units mg/L
TestNo M4500-SD
PQL SPK value SPKRefVai
Piep
Analysis
Date
Date 4/26/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_SI'EC-2_020426A
SeqNo 21798
%R1'D RPDLimit Qual }
Sulfide 0 109 0030 0 107 102 70 130 0 114 4 48 25
Qualifiers: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted iccoveiy limits
J - This concent!ation is consideied an estimate due to LCS failuie
B - Analyte detected in the associated Method Blank
Page 25 of 26
Date: 16-May-02
CLIENT: RSSN
Work Order: L0204322Project: GII-3F TDS W
ANALYTICAL QC SUMMARY REPORTTest Method: SM2540 C
Sample ID MB-R2814
Analyte
SampType MBLK
Batch ID R2814
Result
TestCode TDS_W Units mg/L
TestNo E160.1
PQL SPK value SPKRefVai
Prep Date
Analysis Date 4/24/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_WC_020424I
SeqNo 21508
%RPD RPDLimit Qual
Total Dissolved Solids ND 150
Sample ID LCS-R2814
Analyte
SampType
Batch ID
LCS
R2814
Result
TestCode
TestNo
PQL
TDS_W
E160.1
SPK value
Units mg/L
SPKRefVai
Piep Date
Analysis Date 4/24/02
%REC LowLimit HighLimit RPD Ref Val
Run ID
SeqNo
L_WC_020424I
21507
%RPD RPDLimit Qual
Total Dissolved Solids 967 150 1000 967 80 120
Sample ID L0204356-003EDUP SampType DUP
Analyte
Batch ID R2814
Result
TestCode TDS_W Units mg/L
TestNo E160.1
PQL SPK value SPKRefVai
Prep Date
Analysis Date 4/24/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_\VC_020424I
SeqNo 21509
%RPD RPDLimit
1
Qual
Total Dissolved Solids 346 150 367 589 25
Qualifiers: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted iccovery limits
J - This concentration is consideied an estimate due to LCS f a i l u i e
B - Analyte detected in the associated Method Blank
Page 26 of 26
Date: 16-May-02
NEL LABORATORIESReno • Las Vegas • Boise
Phoenix • Sacramento
CHAIN OF CUSTODY NEL Work Order: LQ L& *f
Project Name
Phoenix Division • 3201 So. 35th Street, Suite B6 • Phoenix, Arizona 85034602-437-0099 • Fax. 602-437-2225 • 888-238-2514
Attention
Address.
Requested Turnaround:
Time/DateSampled Customer Sample Identification
N.E.LIdentification
'urchase Order Number
Project Number
Sampled By
Remarks
/-J2-03.
Y
oV
Custody Seal intact? YCondition
Box#1 DW - Drinking Water SD - SolidWW - Waste Water AQ - AqueousOL • Oil/Organic Liquid A - Air
Box #2 A HCIB HNO3
C HjSO,D NaOH
E Ice Only IF Other IG Not PreserVW
Relinquished by (Print) Date/Time Received by (Print) Date/Time/
The liability of NEL Laboratories Inc is limited strictly to the price of sample analysis for those samples received in good condition by NEL NEL is not responsible for loss, damage, resampling costs and/or qualified data related to samples not received In good condition,including adequate sample volume and number of containers Customer signature of this CoC constitutes a purchase order for NEL to perform work and constitutes acceptance of all NEL Standard Terms and Conditions Signature also constitutes acceptance<jfNEL Standard List Pnce5 for all services ordered here on, except those specified otherwise via an NEL Quotation for Testing Services in effect at the time of sample receipt NEL turnaround times are measured in regular working days Samples received at thelaboratory after 16 30 will be considered received on the next working day Commitment of laboratory to the requested turnaround time will be confirmed via Sample Confirmation transmitted to the fax number provided above
ORIGINAL
NEL LABORATORIESReno • Las VegasPhoenix • Burbank
Las Vegas Division4208 Arcata Way, Suite A • Las Vegas, NV 89030
(702) 657-1010 • Fax: (702) 657-15771-888-368-3282
Nick SainesRSSN7900 Vegas Valley DriveLas Vegas. NV 89142
TEL: 702-431-3020
RE Project: DGH-3F
Dear Nick Saines:
Order No.: L0204323
NEL Laboratories, Las Vegas received 3 samples on 4/22/02 for the analyses presented in thefollowing report.
There were no problems with the analyses and all data for associated QC met EPA or laboratoryspecifications unless noted in the Case Narrative.
If you have any questions regarding these tests results, please feel free to call.
?/Uu--a^-vy// .r-'-v y :Stan VaiiWagefien JLaboratory Manager
Certifications:ArizonaCaliforniaIdahoMontanaNevadaNew MexicoUS Army Corps of Engineers
"V
Reno Las VegasAZ0520 AZ05181707 2002Certified CertifiedCertified CertifiedNV033 NV052Certified Certified
Certified
Date
Corporate Office & Reno Division • 1030 Matley Lane • Reno, NV 89502 • (702) 348-2522
NEL LABORATORIES
NEL Laboratories, Las Vegas Date:
CLIENT: RSSN
Project: DGH-3F CASE NARRATIVELab Order: L0204323
Attached are the analytical results for samples in support of the above referenced project.
The samples submitted for this project were not sampled by NEL. Should you have any questions orcomments, please feel free to contact our Client Services Department.
Analytical Comments:
EPA 8260: Samples were evaluated for the presence of Acrylonitrile and trans-l,4-Dichloro-2-butene.Neither of these two compounds were present in the samples submitted in this work-order at or above5ppb.
Page 1 of 1
NEL LABORATORIES
CLIENT: RSSN
PROJECTED: DGH-3F
PROJECT #: DGH-3F
MATRLX: AQUEOUS
Parameter
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloiomethane
Bromoform
Bromomethane
2-Butanone
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Caibon disulfide
Carbon tetrachlonde
Chloiobenzene
Chloroethane
2-Chloroethyl vinyl ethei
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1 ,2-Dibromo-3-chloropropane
1 ,2-Dibromoethane
Dibromomethane
1 ,2-Oichlorobenzene
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethaiie
1 ,2-Dichloroethane
1,1-Dichloroethene
cis-l,2-Dichloroethene
trans-1 ,2-Dichloroethene
1 ,2-Dichloropropane
1 ,3-Dichloropropane
2,2-Dichloropropane
1 , 1 -Dichloropropene
cis-l,3-Dichloropropene
trans-l,3-Dichloropropene
Ethylbenzene
Hexachlorobutadiene
2-Hexanone
lodomethane
Isopropylbenzene
ND - Not Detected at the Reporting I imit
DF - Dilution Factor
Date: 16-May~02
Result Unit
ND ug/L
ND ug/L
ND ng/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND p.g/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND (ig/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND (ig/L
ND Mg/L
ND ug/L
ND ug/L
ND (ig/L
ND ug/L
ND ug/L
ND ng/L
ND ug/L
ND (ig/L
ND ug/L
ReportingLimit
2550505050505025505050505050505050505050505050505050505050505050505050505050505050255050
CLIENT ED: DGH-3F
DATE SAMPLED: 4/22/02
NEL SAMPLE ID: L0204323
DF Method Prep Date
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
-001A
Analyzed
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04'23/02
04/23/02
04/23/02
04/23/02
04/23/02
04'23'02
04/23/02
04/23/02
Analyst
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-I V
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted reco\ ery limits
E - Value above quantitation range Page 1 of 5
NEL LABORATORIES
CLIENT: RSSN
PROJECTED: DGH-3F
PROJECTS: DGH-3F
MATRIX: AQUEOUS
Parameter
p-Isopropyltoluene
Methylene chlonde
4-Methyl-2-pentanone
MTBE
Naphthalene
n-Propylbenzene
Styrene
1 ,1 ,1 ,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene1 ,2,3-Tnchlorobenzene
1 ,2,4-Tnchloi obenzene
1 ,1 ,1-Tnchloroethane
1 ,1 ,2-Tnchloroethane
Tnchloroethene
1 nchlorofluoromethane
1 ,1 ,2-Tnchlorotnfluoroethane
1 ,2 ,3 -Tuchl oropropane
1 ,2,4-Tnmethylbenzene
1 ,3 ,5-Tnmethylbenzen e
Vinyl acetate
Vinyl chlonde
o-Xylene
m,p-Xylene
Surr: Dibromofluoromethane
Surr: Toluene-d8
Surr: 4-Bromofluorobenzene
Result
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND93.7
10989.3
Unit
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%REC
%REC
%REC
ReportingLimit
50502550505050505050505050505050505050505050505010
92 6-108
957-112
85 3-104
CLIENT ED: DGH-3F
DATE SAMPLED: 4/22/02
NEL SAMPLE ID: L0204323-001A
DF Method
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
1 SW8260B
Prep Date Analyzed
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
Analyst
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
DRM-LV
ND - Not Detected at the Reporting Limit
DF - Dilution Factor
Date: 16-May-02
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 2 of 5
NEL LABORATORIES
CLIENT:
PROJECT ID:
PROJECTS:
MATRIX:
RSSN
DGH-3F
DGH-3F
AQUEOUS
CLEENTD3: DGH-3F
DATE SAMPLED: 4/22/02
NEL SAMPLE ID: L0204323-001B
ReportingParameter Result Unit Limit DF Method
Chloride 2200 mg/L 200 2000 EPA 3000
Nitrate, as N ND mg/L 25 25 EPA 3000
Nitrite, as N ND mg/L 25 25 EPA 300 0
Sulfate 3500 mg/L 200 2000 EPA 300 0
Alkalinity, Bicarbonate (As CaC03) ND mg/L 25 1 SM2320B
Alkalinity, Carbonate (As CaC03) 75 mg/L 25 1 SM2320 B
Hydroxide (As CaC03) ND mg/L 25 1 SM2320B
Alkalinity, Total (As CaCO3) 75 mg/L 25 1 SM2320B
Chemical Ox> gen Demand 78 mg/L 10 1 SM5520 D
Ammonia, as N ND mg/L 030 1 SM4500-NH3
Sulfide ND mg/L 0030 1 SM4500-S D
Total Dissolved Solids 6990 mg/L 150 10 SM2540 C
Prep Date Analyzed
04/30/02
04/23/02
04/23/02
04/30/02
04/29/02
04/29/02
04/29/02
04/29/02
04/29/02
04/30/02
04/26/02
04/24/02
ND - Not Detected at the Reporting I imit
DF - Dilution Factor
Date: 16-May-02
B - Analyte detected m the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 3 of 5
NEL LABORATORIES
CLIENT: RSSN
PROJECT ID: DGH-3F
PROJECT #: DGH-3F
MATRIX: AQUEOUS
Parameter
Aluminum
Barium
Calcium
Iron
Magnesium
Potassium
Sodium
Vanadium
Antimony
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Manganese
Nickel
Selenium
Silver
Thallium
Zinc
Mercury
Result
3.2
0.047
6902.2
210
110
1800
0.0088
ND0.021
ND
ND0.011
0.0025
0.014
00011
0.049
00088
NDNDND0.14
ND
Unit
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
ReportingLimit
0050
00050
0200 100202050
00050
O O O I O
O O O I O
OOOIO
OOOIO
O O O I O
O O O I O
OOOIO
OOOIO
OOOIO
OOOIO
OOOIO
OOOIO
0 00040
OOOIO
0 00020
CLIENT ED:
DATE SAMPLED:
NEL SAMPLE ID:
DF
lll111
1001111111111111111
Method
SW6010B-To
SW 6010B-To
SW6010B-To
SW 6010B-TO
SW6010B-To
SW6010B-To
SW6010B-To
SW6010B-To
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 6020-Tota
SW 7470-Tota
DGH-3F-M
: 4/22/02
: L0204323-002A
Prep Date
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/24/02
Analyzed
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
Analyst
FIF-Reno
FIF-Reno
FIF-Reno
FIF-Reno
FIF-Reno
FIF-Reno
FIF-Reno
FIF-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
A
ND - Not Detected at the Reporting Limit
DF - Dilution Factor
Date: 16-May-02
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 4 of 5
NEL LABORATORIES
CLIENT: RSSN
PROJECTED: DGH-3F
PROJECTS: DGH-3F
MATRIX: AQUEOUS
ParameterAluminum
Barium
Calcium
Iron
Magnesium
Potassium
Sodium
Vanadium
Antimony
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Manganese
Nickel
Selenium
Silver
Thallium
Zinc
Mercury
Result
0.0810.016
680ND
180
881500
ND0.0010
0.019
NDND
0.0016
0.0013
0.0063
ND0.0012
0.0032
NDNDND
0.075
ND
Unit
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
ReportingLimit
0050
00050
0200100202050
00050
OOOIO
OOOIO
O O O I O
OOOIO
OOOIO
O O O I O
O O O I O
OOOIO
O O O I O
O O O I O
O O O I O
O O O I O
0 00040
O O O I O
0 00020
CLIENT ED: DGH-3F-FFM
DATE SAMPLED: 4/22/02
NEL SAMPLE ID: L0204323-003A
DF
111l1l
101111111111111111
Method Prep Date
SW6010B-Di
SW 6010B-Di
SW6010B-Di
SW6010B-Di
SW6010B-Di
SW 6010B-Di
SW6010B-Di
SW6010B-Di
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 6020-Diss
SW 7470-Diss 04/24/02
Analyzed
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/23/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
04/24/02
Analyst
RAA-Reno
RAA-Reno
RAA-Reno
RAA-Reno
RAA-Reno
RAA-Reno
RAA-Reno
RAA-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
DHG-Reno
A
ND - Not Detected at the Reporting Limit
DF - Dilution Factor
Date: 16-Mav-02
B - Analyte detected m the associated Method Blank
S - Spike Recovery outside accepted recovery limits
E - Value above quantitation range Page 5 of 5
A N A L Y T I C A LLABORATORIES
Vanessa PadillaNEL Laboratories Las Vegas4208 Arcata Way, SteXLas Vegas, NV 89030
BSK Submission #: 2002041150BSK Sample ID #: 201121Project ID: L0204323
Submission Comments:
Certificate of AnalysisELAP Certificate #1180
Report Issue Date: 05/01/2002
Project Desc: Dumpco
Sample Type: LiquidSample Description: DGH-3FSample Comments:
Inorganics
Analyte MethodDissolved Organic Carbon (DOC) SM 5310-D
Date Sampled: 04/22/2002Time Sampled: 0940Date Received: 04/23/2002
Prep AnalysisResult Units PQL Dilution DLR Date Date
4.0 mg/L 0.2 5 1.0 04/29/200204/29/2002
mg/L: Milligrams/Liter (ppm)mg/Kg: Milligrams/Kilogram (ppm)Ug/L: Micrograms/Liter (ppb)Hg/Kg: Micrograms/Kilogram (ppb)%Rec: Percent Recovered (surrogates)
Report Authentication Code:
1414 Stanislaus Street Fresno, CA 93706-1623
PQL: Practical Quantitation LimitDLR: Detection Limit for Reporting
: PQL x Dilution
ND: None Detected at DLR
H: Analyzed outside of hold timeP: Preliminary resultS: Suspect result. See Cover Letter for comments.E: Analysis performed by External laboratory.
See External Laboratory Report attachments.
Page 1 of 1
Phone 559-497-2888, In CA 800-877-8310 Fax 559-485-6935
BSK A N A L Y T I C A LLABORATORIES
QC Summary Report 05/01/2002
BSK Submission
Client
Date Submitted
Project ID
Project Desc
2002041150NEL Laboratories Las Vegas04/23/2002L0204323Dumpco
BSK StarLims Run #: 36194
Analyst Initials DONNAHAnalyte Results MatrixAnalyte QCType Spike ID Result
Instrument ID
Method Number DOC
%Rec Spike Spk Matrix
Units or RPD RPD Cone Cone UCL LCL Date
Dissolved Organic Carbon (DOC)
Dissolved Organic Carbon (DOC)
Dissolved Organic Carbon (DOC)
Dissolved Organic Carbon (DOC)
Dissolved Organic Carbon (DOC)
LCS
LCSD
MS
MSD
RBLK
N/A
N/A
201118
201118
N/A
103
101
2387
2378
0
mg/L
mg/L
mg/L
mg/L
mg/L
103
101
110
110
<02
1
2 1
10
037 10
ND
ND
12
12
130
130
130
130
02
70
70
70
70
N/A
04/29/02
04/29/02
04/29/02
04/29/02
04/29/02
Acceptable
Acceptable
Acceptable
Acceptable
Acceptable
Approved by
%Rec Percent Recovered
RPD Relative Percent Difference
UCL Upper Control Limit
LCL Lower Control Limit
Parent Sample Sample used as background matrix for MS/MSD
OOS-High QC Result Above UCL
DOS-Low QC Result Below LCL
Page 1 ofl
NEL LABORATORIES
ffBrmi^ff ffliniiiTfiBli '
CLIENT: RSSNWork Order: L0204323Project: DGH-3F
Sample ID MB-R2742
Analyte
Chlonde
Nitiate, as N
Nitrite, as N
Sulfate
Sample ID MB-R2993
Analyte
Chlonde
Nitrate, as N
Nitrite, as N
Sulfate
Sample ID LCS-R2742
Analyte
Chlonde
Nitiate, as NNitrite, as N
Sullate
SampType MBLK
Batch ID R2742
Result
NDNDNDND
SampType MBLK
Batch ID R2993
Result
NDNDNDND
SampType LCS
Batch ID R2742
Result
201
0994
096272
ANALYTICAL QC SUMMARY REPORT
300_W Test Method: EPA 300.0
TestCode 300_W Units mg/L Prep Date Run ID L_IC-1_020423A
TestNo E300 Analysis Date 4/23/02 SeqNo 20975
PQL SPK value SPKRefVai %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
0 10
0 100 100 10
TestCode 300_W Units mg/L Piep Date Run ID L_IC-1_020430A
TestNo E300 Analysis Date 4/30/02 SeqNo 23006
PQL SPK value SPKRefVai %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
0 100 100 100 10
TestCode 300_W Units mg/L Piep Date Run ID l,_IC-l_020423A
TestNo E300 Analysis Date 4/23/02 SeqNo 20974
PQL SPK value SPKRefVai %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
0 10 2 0 101 80 120 0 0
010 1 0 994 80 120 0 0
010 1 0 96 80 120 0 0010 25 0 109 80 120 0 0
Qualifici s: ND - Not Detected at the Repotting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance l imits LCS acceptable R - RPD outside accepted recoveiy limits
J - This concentiation is consideied an estimate due to LCS failure
B - Analyte detected in the associated Method Blank
Page 1 of 28
Date: 16-May-02
CLIENT: RSSNWork Order: L0204323Project: DGH-3F
Sample ID LCS-R2993 SampType LCS
Batch ID R2993
Analyte
ChlondeNitiate, as NNitnte.asNSulfate
Sample ID
Analyte
ChlondeNitrate, as NNitrite, as NSulfate
Sample ID
Analyte
ChlondeNitrate, as NNitrite, as NSulfate
Sample ID
Analyte
Result
201309861 0152547
LCSD-R2742 SampType LCSD
Batch ID R2742
Result
20670994
0982719
LCSD-R2993 SampType LCSD
Batch ID R2993
Result
2060972
1 022602
L0204322-001BMS SampType MS
Batch ID R2742
Result
Nitiate, as N 246Nitute, asN 3082
Qualiflcis: ND - Not Detected at the Repoitmg Limit
11 - MS 01 MSD outside accepance limits
TestCode
1 eslNo
300_W
300_W Units mg/L
E300
PQL SPK value SPKRefVai
0 100 100 100 10
TestCode
1 estNo
PQL
0 100 100 100 10
TestCode
TestNo
PQL
0 100 100 100 10
TestCode
TestNo
PQL
2 525
LCS acceptable
J - Th i s concentiation is consideied an estimate due to LCS
2 01 01 0
2 5 0
300_W Units mg/L
E300
SPK value SPKRefVai
2 01 01 0
25 0
300_W Units mg/L
E300
SPK value SPKRefVai
2 0
1 01 0
25 0
300_W Units mg/L
E300
SPK value SPKRefVai
25 025 0
ANALYTICAL QC SUMMARY REPORT
Test Method: EPA 300.0
%REC
101986102102
%REC
103994
98109
%REC
103972102104
%REC
984123
Piep Date
Analysis Date 4/30/02
LowLimit HighLimit
80808080
Piep Date
Analysis Date
120120120120
4/23/02
LowLimit HighLimit
80808080
Piep Date
Analysis Date
120120120120
4/30/02
LowLimit HighLimit
80808080
Piep Date
Analysis Date
120120120120
4/23/02
LowLimit HighLimit
8080
120120
C - Unspiked sample >5 times the amount spiked
R - RPD outside accepted recoveiy limits
failuie
Run ID L_IC-1_
SeqNo 23005
020430A
RPD Ret Val %RPD RPDLimit Qual 1
0 00 00 00 0
Run ID L_IC-1_
SeqNo 20976
RPD Ref Val %RPD RP
201 2800994 0
0 96 2 062 72 0 0368
Run ID LJC-I.
SeqNo 23007
i
.020423A
DLimit Qual
25252525
_020430A
RPD Ref Val %RPD RPDLimit Qual
2013 2310 986 1 431 015 04912547 2 1 4
Run ID LJC-1
SeqNo 20977
RPD Ref Val %RPD RI
0 00 0
B - Analyte detected in the associated
252525 i25
_020423A
'DLimit Qual
S
Method Blank
Page 2 of 28
Date: l6-May-02
CLIENT: RSSNWork Order: L0204323Project: DGH-3F 300 W
ANALYTICAL QC SUMMARY REPORTTest Method: EPA 300.0
Sample ID L0204261-001AMS
Analyte
Chloi ide
Sulfate
Sample ID L0204323-001BMS
Analyte
ChlondeSulfate
Sample ID L0204217-001AMS
Analyte
SampType MS
Batch ID R2742
Result
131 63659
SampType MS
Batch ID R2993
Result
3970
5130
SampType MS
Batch ID R2993
Result
TestCode 300_W
TestNo E300
PQL SPK value
10 10010 100
TestCode 300_\V
TestNo E300
PQL SPK value
200 2000
200 2000
TestCode 300_W
TestNo E300
PQL SPK value
Units mg/L
SPKRefVai
3532592
Units mg/L
SPKRefVai
22003512
Units mg/L
SPKRefVai
Piep Date
Analysis Date 4/23/02
%REC LowLimit HighLimit RPD Ref Val
963 80 120 0107 80 120 0
Piep Date
Analysis Date 4/30/02
%REC LowLimit HighLimit RPD Ref Val
885 80 120 0809 80 120 0
Prep Date
Analysis Date 4/30/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_IC-1_020423A
SeqNo 20978
%RPD RPDLimit Qual
00
Run ID L_IC-1_020430A 1
SeqNo 23008
%RPD RPDLimil Qual
00
Run ID L_IC-1_020430A
SeqNo 23541
%RPD RPDLimit Qual
Nitrate, as N 2448 1 0 10 1422 103 80 120
Qualifiers: ND - Not Detected at the Repoiting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted recoveiy limits
J - Tins concentiation is consideied an estimate due to LCS fai luie
B - Analyte detected in the associated Method Blank
Page 3 of 28
Date: 16-May-02
CLIENT: RSSNWork Order: L0204323Project: DGH-3F
Sample ID MB-R1591
Analyte
AluminumBarium
Calcium
Iron
Magnesium
Potassium
Sodium
Vanadium
Sample iD LCS-R1591
Analyte
Aluminum
Barium
Calcium
Iron
Magnesium
Potassium
Sodium
Vanadium
Sample ID L0204322-003A
Analyte
Aluminum
Banum
Calcium
Iron
ANALYTICAL QC SUMMARY REPORT
SampType MBLK
Batch ID R_R1591
Result
NDNDNDNDND
NDNDND
SampType LCS
Batch ID R_R1591
Result
1 041 02420591 1052033
2079194
05161
SampType MS
Batch ID R_R1591
Result
1 150969
6461 008
TestCode
TestNo
PQL
0050
00050
0500 10050
20050
00050
TestCode
TestNo
PQL
0050
00050
0500 100502 0
05000050
TestCode
TestNo
PQL
0050
00050
0500 10
6010\V_D
SW6010B
SPK value
6010W_D
SW6010B
SPK value
11
201
20202005
6010W_D
SW6010B
SPK value
11
201
6010W_D
Units mg/L
SPKRefVai
Units mg/L
SPKRefVai
0000
0000
Units mg/L
SPKRefVai
0099
001958
6180
Test Method: SW 6010B-Diss
Piep Date
Analysis Date 4/23/02
%REC LowLimit HighLimit RPD Ref Val
Piep Date
Analysis Date 4/23/02
%REC LowLimit HighLimit RPD Ref Val
104 85102 85103 85110 85102 85104 8597 85
103 85
Piep Date
Analysis Date
115 0115 0115 0115 0115 0115 0115 0115 0
4/23/02
%REC LowLimit HighLimit RPD Ref Val
105 75949 75140 75101 75
125 0125 0125 0
125 0
Run ID SUB-1591
SeqNo 30037
%RPD RPDLimit Qual
Run ID SUB-1591
SeqNo 30036
%RPD RPDLimit Qual
000 i00000
Run ID SDB-1591
SeqNo 29996
%R!'D RPDLimit Qual
000 C '
0
Qualifiers: ND - Not Detected at the Repoitmg Limit C - Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted lecovery limits
J - This concenuation is consideied an estimate due to LCS f a t l u i e
B - Analyte detected m the associated Method Blank
Page 4 of 28
Date: 16-May-02
CLIENT: RSSNWork Order: L0204323Project: DGH-3F 6010W D
ANALYTICAL QC SUMMARY REPORTTest Method: SW 6010B-Diss
Sample ID L0204322-003A
Analyte
Magnesium
Potassium
Vanadium
Sample ID R0204258-003AMS
Analyte
Sodium
Sampl ype MS
Batch ID R_R1591
Result
1934
1057
05005
SampType MS
Batch ID R_R1591
Result
1750
TestCode
TestNo
PQL
0502 0
00050
TestCode
TestNo
PQL
50
6010W_D
SYV6010B
SPK value
202005
6010W_D
SW6010B
SPK value
200
Units mg/L Pi ep Date
Analysis Date 4/23/02
SPKRefVai
178875
0
Units mg/L
%RJCC
7791
100
LowLimit
757575
HighLimit
125125125
RPD Rei Val
000
Prep Date
Analysis Date 4/23/02
SPKRefVai
1520
%REC
115
LowLimit
75
HighLimit
125
RPD Ref Val
0
Run ID SUB-1591
SeqNo 29996
%RPD RPDLimit
000
Run ID SUB-1591
SeqNo 30039
%RPD RPDLimit
0
Qual
Qual
Sample ID L0204322-003A
Analyte
Aluminum
Barium
Calcium
lion
Magnesium
Potassium
Vanadium
Sample ID R0204258-003AMSD
Analyte
Sodium
SampType MSD
Batch ID R_R1591
Result
1 11
0951
6491 014
192 3
1032
0497
SampType MSD
Batch ID R_R1591
Result
1760
TestCode
TestNo
PQL
0050
00050
0500 10
05020
00050
TestCode
TestNo
PQL
50
6010W_D
SW6010B
SPK value
1
120
12020
05
6010W_D
SW6010B
SPK value
200
Units mg/L
SPKRefVai
0099
001958
6180
178875
0
Units mg/L
SPKRefVai
1520
%REC
10193 1
155101
71 5
785
994
%REC
120
Prep Date
Analysis Date 4/23/02
LowLimit HighLimit
757575757575
75
Pi ep Date
Analysis Date
125125125125125125
125
4/23/02
LowLimit HighLimit
75 125
RPD Ref Val
000000
0
RPD Ref Val
0
Run ID SUB-1591
SeqNo 29923
%RPD RPDLimit Qual
000 C
00 C
0
0
Run ID SUB-1591
SeqNo 30041
%RPD RPDLimit Qual
0
Qualifiers: ND - Not Detected at the Repotting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted lecoveiy limits
J - Tins conccntialioii is consideied an estimate due lo LCS failuie
B - Analyte detected in the associated Method Blank
Page 5 of 28
Date: 16-May-02
CLIENT: RSSNWork Oi dor: L0204323Project: DGH-3F
Sample ID MB-793
Analyte
Aluminum
Bai mmCalcium
Iron
Magnesium
Potassium
Sodium
Vanadium
Sample ID LCS-793
Analyte
Aluminum
Barium
Calcium
lion
Magnesium
Potassium
Sodium
Vanadium
Sample ID R0204220-001BMS
Analyte
Banum
Sodium
ANALYTICAL QC SUMMARY REPORT i
SampType IMBLK
Batch ID R_793
Result
NDNDNDNDNDNDNDND
SampType LCS
Batch ID R_793
Result
1 07
1081209
1 11621 1921 26
197
05509
SampType MS
Batch ID R_793
Result
1 46
1520
TestCode
TestNo
PQL
0050
00050
050
0 1005020
05000050
TestCode
TestNo
PQL
0050
00050
0500 1005020
05000050
TestCode
TestNo
PQL
00050
050
6010WJT
6010W_T Units mg/L
SW60IOB
SPK value SPKRefVai
6010\V_T Units mg/L
SW6010B
SPK value SPKRefVai
1 01 0
20 01 0
20 0
20 020 005 0
6010W_T Units mg/L
SW6010B
SPK value SPK Ref Val
1 0446
20 1490
Test Method: SW 6010B-Total 'l
Pi ep Date
Analysis Date
4/23/02
4/24/02
%REC LowLimit HighLimit RPD Ref Val
Piep Date
Analysis Date
4/23/02
4/24/02
%REC LowLimit HighLimit RPD Ref Val
107 85108 85104 85112 85106 85106 85
985 85110 85
Piep Date
Analysis Date
115 0115 0115 0115 0115 0115 0115 0115 0
4/23/02
4/24/02
%R£C LowLimit HighLimit RPD Ref Val
101 75150 75
125 0125 0
Run ID SUB-1616
SeqNo 29974
%RPD RPDLimit Qual
1
Run ID SUB-1616
SeqNo 29973
%RPD RPDLimit Qual
000
100000
Run ID SUB-1616
SeqNo 29975
%RPD RPDLimit Qual
00 C
4Qualifiers: ND - Not Detected at the Repoiting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted lecovety limits
J - T his (.onceilliation is consideied an estimate due to LCS failuie
B - Analyte detected in the associated Method Blank
Page 6 of 28
Date: 16-May-02
CLIENT: RSSNWork Order: L0204323Project: DGH-3F
Sample ID R0204220-001BMSD
Analyte
Bai mm
Sodium
Sample ID R0204220-001BDUP
Analyte
Aluminum
Barium
Calcium
Iron
Magnesium
Potassium
Sodium
Vanadium
ANALYTICAL QC SUMMARY REPORT
SampType MSU
Batch ID R_793
Result
1 4521490
Samp I ype DUP
Batch ID R_793
Result
NDNDNDNDNDNDNDND
I estCode
TestNo
PQL
00050
050
TestCode
TestNo
PQL
0050
00050
0 500 1005020
05000050
fioiowjrSW6010B
SPK value
120
6010W_T
SW6010B
SPK value
00000000
6010W_T
Units mg/L
SPK Ref Val
0446
1490
Units mg/L
SPKRefVai
000
00000
Test Method : S W 60 1 OB-Total
%REC
1010
%REC
000
00000
Piep Date
Analysis Date
4/23/02
4/24/02
LowLimit HighLimit
Piep Date
Analysis Date
4/23/02
4/24/02
LowLimit HighLimit
00000000
00000000
RPD Ref Val
00
RPD Ref Val
00000000
Run ID SUB-1616
SeqNo 29976
%RPD RPDLimit Qual
00
Run ID SUB-1616
SeqNo 29972
%RPD RPDLimit Qual
00000000
Qualifici s: ND - Not Detected at the Repoiting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted iccoveiy limits
J - This concentialion is consideied an estimate due to LCS fa i lu ie
B - Analyte detected in the associated Method Blank '
Page 7 of 28
Date: 16-May-02
CLIENT: RSSNWork Order: L0204323Project: DGH-3F
Sample ID MB-R1615
Analyte
Antimony
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Coppei
Lead
Manganese
Nickel
Selenium
Silvei
Thallium
Zinc
Sample ID LCS-R1615
Analyte
Antimony
Aisenic
Beiylhum
Cadmium
Chiomium
Cobalt
Coppei
Lead
Manganese
Nickel
Selenium
ANALYTICAL QC SUMMARY REPORT
SampType MBLK
Batch ID R_R1615
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SampType LCS
Batch ID R_R1615
Result
0 05628
0 09946
009871
005657
0053390054180052610 05243005574005439
0 1082
6020W_D
TestCode 6020W_D Units mg/L
TestNo SW6020
PQL SPK value SPKRefVai
OOOIO
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I OO O O I OO O O I O
0 00040
O O O I O
TestCode 6020W_D Units mg/L
TestNo SW6020
PQL SPK value SPKRefVai
O O O I O 005 0
O O O I O 01 0
O O O I O 01 0
O O O I O 005 0
O O O I O 005 0
O O O I O 005 0
O O O I O 005 0
O O O I O 005 0
O O O I O 005 0
O O O I O 005 0
O O O I O 01 0
Test Method: SW 6020-Diss
Prep Date
Analysis Date 4/24/02
%REC LowLimit HighLimit RPD Ref Val
Prep Date
Analysis Date 4/24/02
%REC LowLimit HighLimit RPD Ref Val
113 85 115 0
995 85 115 0
987 85 115 0
113 85 115 0
107 85 115 0
108 85 115 0
105 85 115 0
105 85 115 0
111 85 115 0
109 85 115 0
108 85 115 0
Run ID SUB-1615
SeqNo 29928
%RPD RPDLimit Qual
i
,
1
Run ID SUB-1615
SeqNo 29927
%RPD RPDLimit Qual
0
0
0
0000000
o
Qualifiers: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS or MSD outside accepance limits LCS acceptable R - RPD outside accepted iccoveiy limits
J - This concentiation is consideied an estimate due to LCS fa i lu ie
B - Analyte detected in the associated Method Blank
Page 8 of 28
Date: 16-May-02
CLIENT: RSSNWork Order: L0204323Project:
Sample ID
Analyte
Silver
Thallium
Zinc
Sample ID
Analyte
Antimony
Arsenic
Beiylhum
Cadmium
Chromium
Cobalt
Coppei
LeadManganese
Nickel
Selenium
Silvei
Thal l ium
Zinc
Sample ID
Analyte
AntimonyAisenic
Beryllium
Qualifiers
DGH-3F
LCS-R1615 SampType LCS
Batch ID R_R1615
Result
0 111005628
005417
L02043 10-003 A SampType MS
Batch ID R_R1615
Result
0 04629
0 14620 140200442
00634
0 05759
006179
0046913 573
0 06069
0 12980 1021
005421
0223
R0204242-003AMS SampType MS
Batch ID R_R1615
Result
0 046290 1462
0 1402
: ND - Not Detected at the Repoitmg Limit
Jl - MS 01 MSD outside accepance l imi ts
TestCode
TestNo
PQL
O O O I O
0 00040
OOOIO
TestCode
TestNo
PQL
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O0 00040
O O O I O
lestCode
TestNo
PQL
O O O I O
O O O I O
O O O I O
6020W_D
SW6020
SPK value
01005005
6020W_D
SW6020
SPK value
005
0 10 1
0050050050050050050050 10 1
005005
6020W_D
SW6020
SPK value
0050 10 1
6020W_D
Units mg/L
SPKRefVai
0
00
Units mg/L
SPKRefVai
000135
00376
00
0 00384
0 00277
0 00489
04014
0 00706
0 0059600
0 104
Units mg/L
SPKRefVai
000135
00376
0
ANALYTICAL QC SUMMARY REPORT!
Test Method: SW 6020-Diss
%REC
111113108
%REC
899109140
884119110114
93 8-882
107124102108238
%REC
899109
140
Piep Date
Analysis Date 4/24/02
LowLimit HighLimit
858585
Piep Date
Analysis Date
115
115115
4/24/02
LowLimit HighLimit
75
75757575757575757575757575
Piep Date
Analysis Date
125125125125125125125125125125125125125125
4/24/02
LowLimit HighLimit
757575
125125125
C - Unspiked sample >5 times the amount spiked
LCS acceptable
J - This cuncentiation is consideied an estimate due to LCS
R - RPD outside accepted
fai lu ie
RPD Ref Val
000
RPD Ref Val
0
0000000000000
RPD Ref Val
000
Run ID SUB-1615
SeqNo 29927
%RPD RPDLimit Qual
000
Run ID SUB-1615
SeqNo 29929
%RPD RPDLimit Qual
0
00 Jl000000 C00000 Jl
Run ID SUB-1615
SeqNo 30046
%RPD RPDLimil Qual
000 II
B - Analyte detected in the associated Method Blank
lecoveiy limits Page 9 of 28
Date: 16-May-02
CLIENT: RSSNWork Order: L0204323Project: DG1I-3F
Sample ID R0204242-003AMS
Analyte
Cadmium
Chiomium
Cobalt
Copper
Lead
Manganese
Nickel
Selenium
Silver
Thallium
Zinc
Sample ID L02043 10-003 A
Analyte
Antimony
Aisemc
Beryllium
Cadmium
Chiomium
Cobalt
Coppei
Lead
Manganese
Nickel
Selenium
Silver
Thallium
Zinc
SampType MS
Batch ID R_R1615
Result
00442
006340 05759
006179
004691
3573
0 06069
0 12980 1021
0 05421
0223
SampType MSD
Batch ID R_R1615
Result
0 05058
0 1459
0 142300441
0 0623700572
005881
004616
3 581
006051
0 12740 101
005398
0 1804
TestCode
TestNo
PQL
O O O I O
O O O I O
O O O I O
O O O I O
O O O I OO O O I O
OOOIO
O O O I O
O O O I O
0 00040
O O O I O
TestCode
TestNo
PQL
O O O I O
OOOIO
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
0 00040
O O O I O
6020W_D
SW6020
SPK value
005005005005005005005
0 10 1
005
005
6020W_D
SW6020
SPK value
0050 10 1
005005005005005005005
0 10 1
005005
6020W_D
Units mg/L
ANALYTICAL QC SUMMARY REPORT
Test Method: SW 6020-Diss
Pi ep Date
Analysis Date 4/24/02
SPK Ref Val
0000384
0 00277
0 00489
04014
0 00706
0 00596
00
0 104
Units mg/L
%REC
884
119110114
93 8-882107124102108238
LowLimit
757575757575
7575757575
HighLimit
125125125125125125125125125125125
RPD Ref Val
00000000000
Pi ep Date
Analysis Date 4/24/02
SPKRefVai
000135
00376
00
000384
0 00277
0 00489
04014
0 00706
0 00596
00
0 104
%REC
985
108142
882117109
108923866
107121101108153
LowLimit HighLimit RPD Ref Val
00000000000000
Run ID SUB-1615
SeqNo 30046
%RPD RPDLimit Qual
000000 C00000 Jl
Run ID SUB-1615
SeqNo 29930
%RPD RPDLimit Qual
000 Jl000000 C
00000 Jl
Qualifiers: ND - Not Detected at the Repoiting Limit C - Unspiked sample >5 times the amount spiked
II - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted iccoveiy limits
J - 1 his concentiation is consideied an estimate due to LCS failuie
B - Analyte detected in the associated Method Blank
Page 10 of 28
Date: 16-May-02
CLIENT: RSSNWork Order: L0204323Project: DGH-3F
Sample ID R0204242-003AMSD
Analyte
Antimony
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
CopperLead
Manganese
Nickel
SeleniumSilver
ThalliumZinc
Sample ID L02043 10-003 A
Analyte
Antimony
Aisemc
Beiylhum
Cadmium
Chiomium
Cobalt
Copper
Lead
Manganese
Nickel
Selenium
ANALYTICAL QC SUMMARY REPORT
Samplype MSD
Batch ID R_R1615
Result
0 05058
0 1459
0 142300441
0 06237
00572
005881
004616
3581006051
0 12740 101
0 053980 1804
SampType DUP
Batch ID R_R1615
Result
ND003632
NDND
0 00466
0 00294
0 00568
ND4 07
0 00724
ND
TestCode
TestNo
PQL
O O O I O
OOOIO
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
0 00040O O O I O
TestCode
TestNo
PQL
O O O I O
O O O I O
O O O I O
O O O I O
OOOIO
O O O I O
O O O I OO O O I O
O O O I O
O O O I O
O O O I O
6020\Y_D
SW6020
SPK value
005
0 10 1
005005005005005005005010 1
005005
6020W_D
SW6020
SPK value
0
000000000
0
6020W_D
Units mg/L
SPKRefVai
000135
00376
0
00 00384
0 00277
0 00489
04014
0 00706
0 00596
00
0 104
Units mg/L
SPKRefVai
00000
00000
0
Test Method: SW 6020-Diss
Pi ep Date
Analysis Date 4/24/02
%REC LowLimit HighLimit
985
108142
882117
109108
923-866107121101108153
Piep Date
Analysis Date 4/24/02
%REC LowLimit HighLimit
0 0 00 0 00 0 00 0 00 0 0
0 0 00 0 00 0 00 0 00 0 00 0 0
RPD Ref Val
0
0000000000000
RPD Ref Val
00000000000
Run ID SUB-1615
SeqNo 30047
%RPD RPDLimit Qual
000 Jl
000000 C
1
00000 Jl
Run ID SUB-1615 ]
SeqNo 29926
%RPD RPDLimit Qual
00
000000000
Qualifiers: ND - Not Detected at the Repoiting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS or MSD outside accepance limits LCS acceptable R - RPD outside accepted recoveiy limits
J - This concenUation is consideied an estimate due to LCS failuie
B - Analyte detected in the associated Method Blank i
Page 11 of 28
Date: 16-May-02
CLIENT: RSSNWork Order: L0204323Project: DGH-3F
Sample ID L02043 10-003 A
Analyte
Silver
Thallium
Zinc
Sample ID R0204242-003ADUP
Analyte
Antimony
Aisemc
Beiylhum
Cadmium
Chromium
Cobalt
Copper
Lead
Manganese
Nickel
Selenium
Silver
Thal l ium
Zinc
ANALYTICAL QC SUMMARY REPORT
SampType DUP
Batch ID R_R1615
Result
ND
ND
0 108
SampType DUP
Batch ID R_R1615
Result
ND
0 03632
ND
ND
0 00466
0 00294
0 00568
ND407
0 00724
ND
ND
ND
0 108
TestCode
TestNo
PQL
O O O I O
0 00040
O O O I O
TestCode
TestNo
PQL
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I O
O O O I OO O O I O
O O O I OO O O I O
O O O I O
0 00040
O O O I O
6020W_D
SW6020
SPK value
0
0
0
6020W_D
SW6020
SPK value
0
0
0
0
0
0
0
0
0
0
0
0
0
0
6020W_D
Units mg/L
SPKRefVai
0
0
0
Units mg/L
SPKRefVai
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Test Method: SW 6020-Diss
%REC
0
0
0
%REC
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Piep Date
Analysis Date 4/24/02
LowLimit HighLimit
0
0
0
Pi ep Date
Analysis Date
0
0
0
4/24/02
LowLimit HighLimit
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
RPD Ref Val
0
0
0
RPD Ref Val
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Run ID SUB-1615
SeqNo 29926
%RPU RPDLimit Qual
0
0
0
Run ID SUB-1615
SeqNo 30043
%RPD RPDLimit Qual
00000000000000
Qualifiers: ND - Not Detected at the Repotting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted lecoveiy limits
J - This concenuaijon is consideied an estimate due lo LCS failuie
B - Analyte detected in the associated Method Blank
Page 12 of 28
Date: 16-May-02
CLIENT: RSSNWork Order: L0204323Project:
Sample ID
Analyte
Antimony
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
LeadManganese
Nickel
Selenium
SilverThallium
Zinc
Sample ID
Analyte
Antimony
Arsenic
Beryllium
Cadmium
Chiomium
Cobalt
Coppei
Lead
Manganese
Nickel
Selenium
Qualif icis
DGH-3F
MB-795 SampType MBLK
Batch ID R_795
Result
NDNDNDNDNDNDNDNDNDNDNDNDNDND
LCS-795 SampType LCS
Batch ID R_795
Result
0 05695
009415
0 1524
00519
00537
0 05475
00567
00545
00494
00554
00956
ND - Not Detected at the Repoitmg Limit
Jl - MS 01 MSD outside accepance limits
TestCode
TestNo
PQL
00050
00050
00050
00050
00050
00050
00050
00050
00050
00050
00050
00050
00050
00050
TestCode
TestNo
PQL
00050
00050
00050
00050
00050
00050
00050
00050
00050
00050
00050
LCS acceptable
J - This coucentialion is cons,ideied an estimate due to LCS
ANALYTICAL QC SUMMARY REPORT6020W_T Test Method: SW 6020-Total
6020W_T Units mg/L Piep Date 4/23/02 Run ID SUB-1627
SW6020 Analysis Date 4/24/02 SeqNo 29953
SPK value SPKRefVai %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
1
6020WJT Units mg/L Piep Date 4/23/02 Run ID SUB-1627
SW6020 Analysis Date 4/24/02 SeqNo 29952
SPK value SPKRefVai %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
005 0 114 85 115 0 00 1 0 942 85 115 0 001 0 152 85 115 0 0
005 0 104 85 115 0 0
005 0 107 85 115 0 0005 0 110 85 115 0 0005 0 113 85 115 0 0005 0 109 85 115 0 0
005 0 988 85 115 0 0005 0 111 85 115 0 0
0 1 0 956 85 115 0 0
C - Unspiked sample >5 times the amount spiked B - Analyte detected in the associated Method Blank
R - RPD outside accepted recovery limits Page 13 of 28
failuie Date: 16-May-02
CLIENT: RSSNWork Order: L0204323Project: DGH-3F
Sample ID LCS-795
Analyte
Silver
Thall ium
Zinc
Sample ID R0204208-001BMS
Analyte
Antimony
Arsenic
Beiylhum
Cadmium
Chromium
Cobalt
Copper
Lead
Manganese
Nickel
Selenium
Silvei
Thall ium
Zinc
Sample ID R0204208-001BMSD
Analyte
Antimony
Arsenic
Beiylhum
ANALYTICAL QC SUMMARY REPORT
SampType LCS
Batch ID RJ795
Result
0 1364
00547
0 04785
SampType MS
Batch ID RJ795
Result
00629
0 1046
0 1637
0 05525
0 05645
0059
006515
0 05685
00643
0 062550 1049
0 1384
0 06405
0 1304
SampType MSD
Batch ID R_795
Result
0 05965
00966
0 1534
TestCode
TestNo
6020W_T
SW6020
PQL SPK value
00050
00050
00050
TestCode
TestNo
PQL
00050
00050
00050
00050
00050
00050
00050
00050
00050
0005000050
00050
00050
00050
TestCode
TestNo
PQL
00050
00050
00050
0 1
005
005
6020WJT
SW6020
SPK value
005
0 1
0 1
005
005
005
005
005
005
005
0 1
0 1
005
005
6020W_T
SW6020
SPK value
005
0 1
0 1
6020WJT
Units mg/L
SPKRefVai
000
Units mg/L
SPKRefVai
0
0
0
0
00055
0
0 00675
0
00105
00
0
0
008105
Units mg/L
SPK Ref Va!
0
0
0
Test Method: SW 6020-Total
%REC
136
109
957
%REC
126
105
164
110
102
118
117
114
108
125
105
138
128
987
%REC
119
966
153
Piep Date
Analysis Date
4/23/02
4/24/02
I owLimit HighLimit
85
85
85
Piep Date
Analysis Date
115
115
115
4/23/02
4/24/02
LowLimit HighLimit
75
75
75
75
75
75
75
75
75
75
75
75
75
75
Piep Date
Analysis Date
125
125
125
125
125
125
125
125
125
125
125
125
125
125
4/23/02
4/24/02
LowLimit HighLimit
RPD Ref Val
0
0
0
RPD Ref Val
0
0
0
0
0
0
0
0
0
0
0
0
0
0
RPD Ref Val
0
0
0
Run ID SUB-1627
SeqNo 29952
%RPD RPDLimit Qual
0
0
0
Run ID SUB-1627
SeqNo 29954
%RPD RPDLimit Qual
0
0
0 Jl
0
0
0
0
0
0
00
0 Jl
0 Jl
0
Run ID SUB-1627
SeqNo 29955
%RPD RPD! milt Qual
0
0
0 Jl i
Qualifiers: ND - Not Detected at the Repoitmg Limit C - Unspiked sample >5 times the amount spiked
Jl - MS or MSD outside accepance limits LCS acceptable R - RPD outside accepted recoveiy limits
J - This concentiation is consideied an estimate due to LCS i a i l u i e
B - Analyte detected in the associated Method Blank
Page 14 of 28
Date: 16-May-02
CLIENT: RSSNWork Order: L0204323Project: DGH-3F
Sample ID R0204208-001BMSD
Analyte
Cadmium
Chiomium
Cobalt
Copper
Lead
ManganeseNickel
Selenium
Silver
ThalliumZinc
Sample ID R0204208-001BDUP
Analyte
Antimony
Arsenic
Beiylhum
Cadmium
Chromium
Cobalt
Copper
Lead
ManganeseNickel
Selenium
Silver
ThalliumZinc
ANALYTICAL QC SUMMARY REPORT
SampType MSD
Batch ID R_795
Result
00516
0 05325
0 055250 06085
00528
0 05925
0 05675
0 10260 130800593
0 1252
SampType DUP
Batch ID RJ795
Result
NDNDND
NDND
ND00061
ND
00094
ND
NDNDND
0 07405
TestCode
TestNo
PQL
00050
00050
0005000050
00050
0005000050
00050
00050
00050
00050
TestCode
TestNo
PQL
00050
00050
00050
00050
00050
00050
00050
00050
00050
00050
00050
00050
00050
00050
6020WJT
SW6020
SPK value
005005
005005005005005
0 101
005005
6020W_T
SW6020
SPK value
000000
000
00000
6020WJT
Units mg/L
SPKRefVai
000055
00 00675
000105
0000
008105
Units mg/L
SPKRefVai
000000
00000000
Test Method: SW 6020-Total
Prep Date
Analysis Date
4/23/02
4/24/02
%REC LowLimit HighLimit
103955110108106
975114103131119
884
Piep Date
Analysis Date
4/23/02
4/24/02
%REC LowLimit HighLimit
0 00 00 0
0 00 0
0 00 00 00 00 00 0
0 00 00 0
000
00
0000000
00
RPD Ref Val
00000000000
RPD Ref Val
00000000000
0
00
Run ID SUB-1627
SeqNo 29955
%RPD RPDLimit Qual
000000000 Jl
00
Run ID SUB-1627
SeqNo 29951
%RPD RPDLimit Qual
000
00000000000
r»noi;r,o^c. Kin _ M^t riMprip/i M il-ip R^nmimo 1 irmt P - 1 IncmVprl camnle >S timps thp amnimi snikpri R - Analvte detected in the associated Method Blank
Jl - MS or MSD outside accepance limits LCS acceptable R - RPD outside accepted lecovery limits
J - Tins conccnuation is consideied an estimate due to LCS failuie
Page 15 of 28
Date: 16-May-02
CLIENT: RSSNWork Order: L0204323Project: DGH-3F
-J.-t
8260 W
ANALYTICAL QC SUMMARY REPORTTest Method: SW8260B
Sample ID Method Blank 02 SampType MBLK
Analyte
Batch ID R2684
Result
TestCode 8260_W Units ug/L
TestNo SW8260B
PQL SPK value SPKRefVai
Prep Date
Analysis Date 4/23/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_VOAMS-2_020423A
SeqNo 20642
%RPD RPDLimit Qual
1,1,2-Ti ichlorotnfluoioethaneMTBEAcetoneBenzeneBromobenzeneBromochloro methaneBiomodichloiomethaneBromofoi mBiomomethane2-Butanonen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneCarbon disulfideCarbon tctiachlondeChloiobenzeneChloioelhane2-Chloioethyl vinyl etheiChloioformChloiomethane2-Chloiotoluene4-ChloiotolueneDibi omochloromethane1,2-Dibi omo-3-chloi opi opane1,2-DibiomoethaneDibiomomethane1,2-Dichloiobcnzene1,3-Dichloiobenzcne1,4-Dichloi obenzene
Dichloi odi lluoi omethanc
ne NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
NDNDNDNDNDNDND
lane ND
NDNDND
NDND
ND
50502550505050505025505050505050
505050505050505050
50505050
50
Qualifiers: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS or MSD outbide accepance limits LCS acceptable R - RPD outside accepted lecoveiy l imits
J - 1 Ins concentiation is consideied an estimate due to LCS failuie
B - Analyte detected in the associated Method Blank
Page 16 of 28
Date: 16-May-Q2
CLIENT: RSSNWork Order: L0204323Project: DGH-3F
Sample ID Method Blank 02
Analyte
1,1-Dichloi oethane
1 ,2-Dichloroethane1,1-Dichloi oethene
cis-l,2-Dichloroetheneti ans- 1 ,2-Dichloroethene1 ,2-Dichloi opropane1 ,3-Dichloropropane
2,2-Dichloi opropane1 ,1 -Dichloi opropenecis-l,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzeneHexachlorobutadiene
2-HexanonelodomethaneIsopropylbenzenep-Isopiopyltoluene
Methylene chlonde4-Methyl-2-pentanoneNaphthalene
n-PiopylbenzeneStyiene1,1,1 ,2-Teti achloi oethane
1 , 1 ,2,2-Teti achloi oethaneTeti achloi oethene
Toluene1 ,2,3-Tnchloiobenzene1 ,2,4-Tnchloiobenzene1,1,1-Tnchloi oethane1 ,1 ,2-1 richloroethane
Samplype MBLK
Batch ID R2684
Result
NDNDND
NDNDNDNDNDNDNDNDNDNDNDND
NDNDNDNDND
NDNDND
NDNDNDNDNDNDND
ANALYTICAL QC SUMMARY REPORT )
8260_W Test Method: SW8260B
TestCode 8260_W Units ug/L Prep Date Run ID L_VOAMS-2_020423A
TestNo SW8260B Analysis Date 4/23/02 SeqNo 20642
PQL SPK value SPKRefVai %RLC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
505050
50505050
5050505050502550
5050502510
5050505050505050505 0
Qualifiets: ND - Not Detected at the Repoiting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS or MSD outside accepance limits LCS acceptable R - RPD outside accepted recoveiy limits
J - This concentiation is considered an estimate due to LCS fa i lu ie
B - Analyte detected in the associated Method Blank
Page 17 of 28
Date: 16-May-02
CLIENT: RSSNWork Order: L0204323Project: DGH-3F
Sample ID Method Blank 02
Analyte
Trichloroethene
Trichlorofluoi ome thane
1 ,2,3-Ti ichloropropane
1 ,2,4-Ti imethy Ibenzene
1 ,3,5-Ti imethylbenzene
Vinyl acetate
Vinyl chloride
o-Xylene
m,p-Xylene
Surr Dibiomofluoiomethane
Surr Foluene-dS
SUIT 4-Bromofluorobenzene
Sample ID Vstd050CCV02042
Analyte
Acetone
Benzene
Biomofoirn
Bromomethane
Chloiobcnzene
Chloiolorm
Chloiomethane
Dichloi odi fluoi omethane
1,1-Dichloi oethane
1,1-Dicliloi oethene
1,2-Dichloiopiopane
Ethylbeiizcne
1 ,1 ,2,2-Tetrachloioethane
SampType MBLK
Batch ID R2684
Result
NDNDNDNDND
NDNDNDND
4804
5357
4476
SampType LCS
Batch ID R2684
Result
37814857
3986
7834
51 774996
6859
6665249
4887
49 165039
5234
TestCode
TestNo
PQL
505050
5050
50505010
505050
TestCode
TestNo
PQL
25505050505050
5050505050
50
8260_W
SW8260B
SPK value
505050
8260_W
SW8260B
SPK value
50505050505050
5050505050
50
8260_W
Units u-g/L
ANALYTICAL QC SUMMARY REPORT
Test Method: SW8260B
Prep Date
Analysis Date 4/23/02
SPKRefVai
000
Units ug/L
%REC
96 1107
895
LowLimit
80808562
HighLimit
120119139
RPD Ref Val
0
00
Piep Date
Analysis Date 4/23/02
SPKRefVai
00000
00
000000
%REC
75697 1797157104
999137133105
977983
101105
LowLimit
70707070708070
707080808070
HighLimit
130130130130130
120130
130130120120120130
RPD Ref Val
00000
00
000000
Run ID L_VOAMS-2_020423A
SeqNo 20642
%RPD RPDLimit
000
Qual
Run ID L_VOAMS-2_020423A
SeqNo 20645
%RPD RPDLimit
000000
0
000000
Qual
S
SS
Qualifiers: ND - Not Detected at the Repoiting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS or MSD outside accepance limits LCS acceptable R - RPD outside accepted lecoveiy limits
J - This concent!ation is consideied an estimate due to LCS fai luie
B - Analyte detected m the associated Method Blank
Page 18 of 28
Date: 16-May-02
CLIENT: RSSNWork Order: L0204323Project: DGH-3F
Sample ID Vstd050CCV02042
Analyte
Toluene
TrichloioetheneVinyl chlonde
SUIT Dibiomofluoromethane
Suir Toluene-dS
Sun 4-Bromofluorobcnzene
Sample ID L0204322-001A MS
Analyte
Acetone
BenzeneBromomethane
Chloiobenzene
Chlorome thane
Dichloi odifluoi omethane
1,1-Dichloi oethene
Toluene
Trichloioethene
Vinyl chlonde
Surr Dibi omofluoi omethane
Sun 1oluene-d8Sun 4-Bi omofluoi obenzcne
Sample ID L0204322-001 A MSD
Analyte
Acetone
ANALYTICAL QC SUMMARY REPORT
SampType LCS
Batch ID R2684
Result
4647
47 1558 174495
5268
42 1
SampType MS
Batch ID R2684
Result
51 33
5436759
5366
8647
8365
58 15
5299
52 186921
4669
5546
4873
SampType MSD
Batch ID R2684
Result
4805
Quahfieis: ND - Not Detected at the Reporting Limit
Jl - MS 01 MSD outside accepance limits LCS
J - This cunccntiation is coiiiideied an estimate
TestCode 8260_W
TestNo SW8260B
PQL SPK value
50 5050 5050 5050 5050 5050 50
TestCode 8260_W
TestNo SW8260B
PQL SPK value
25 5050 5050 5050 5050 5050 5050 5050 5050 5050 5050 5050 5050 50
TestCode 8260_W
TestNo SW8260B
PQL SPK value
25 50
8260 W
Units u.g/L
SPKRefVai
00000
0
Units ug/L
SPK Ref Val
00000000
00000
Units ug/L
SPKRefVai
0
*
Test Method: SW8260B
Piep Date
Analysis Date 4/23/02
%RBC LowLimit HighLimit
92 9 80 12094 3 70 130116 80 120
89 9 80 120105 808 119
842 562 139
Piep Date
Analysis Date 4/23/02
%REC LowLimit HighLimit
103 70 130109 70 130152 70 130107 70 130173 70 130167 70 130116 80 120106 80 120104 70 130138 80 120
934 926 108111 957 112
975 853 104
Piep Date
Analysis Date 4/23/02
%REC LowLimit l l ighLimi t
96 1 70 130
C - Unspiked sample >5 times the amount spiked
acceptable R - RPD outside accepted
due to LCS fai luie
recoveiy limits
RPD Ref Val
000000
RPD Ref Val
0000000000000
RPD Ref Val
51 33
i
Run ID L_VOAMS-2_020423A
SeqNo 20645
%RPD RPDLimit Qual
000000 i
Run ID L_VOAMS-2_020423A
SeqNo 20643
%RPD RPDLimit Qual
000 S00 S0 S0
o00 S00o
Run ID L_VOAMS-2_020423A
SeqNo 20644
%RPD RPDLimit Qual
660 25
B - Analyte detected in the associated Method Blank '
Page 1 9 of 28
Date: 16-May-02\
CLIENT: RSSNWork Order: L0204323Project: DGH-3F
Sample ID L0204322-001A MSD
Analyte
Benzene
Bromomethane
Chloiobenzene
Chloi omethane
Dichloiodifluoi omethane
1,1-Dichloi oethene
Toluene
Trichloioethene
Vinyl chlorideSun Dibiomofluoromethane
Surr Toluene-d8
Sun 4-Biomofluoiobenzene
ANALYTICAL QC SUMMARY REPORT
SampType MSD
Batch ID R2684
Result
4938
67 13
4966
6853
7924
5277472147785748
4707
53 57
4505
TestCode
TestNo
PQL
50
50
50
50
50
50
50
50
50
50
50
50
8260_\Y
SW8260B
SPK value
50
50
50
50
50
50
50
50
50
50
50
50
8260_W
Units u.g/L
SPKRefVai
0
0
0
0
0
0
0
0
0
0
0
0
Test Method: SW8260B
%REC
988
134
99.3
137
158
106
944
956
115
94 1
107
90 1
Piep Date
Analysis Date 4/23/02
LowLimit HighLimit
70
70
70
70
70
80
80
70
80
926
957
853
130
130
130
130
130
120
120
130
120
108
112
104
Run ID L_VOAMS-2_020423A
SeqNo 20644
RPD Ref Val
5436
759
5366
8647
8365
58 15529952 18
6921
0
0
0
%RPD
960
123
774
231
5 4 1
97011 5
880
185
0
0
0
RPDLimit Qual
2525 S
25
25 S
25 S
2525
25
25
0
o0
Qualifiers: ND - Not Detected at the Repotting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS or MSD outside accepance limits LCS acceptable R - RPD outside accepted iccovery limits
J - This concentiation is consideied an estimate due to LCS fai lu ie
B - Analyte detected in the associated Method Blank
Page 20 of 28
Date: l6-May-02
CLIENT: RSSNWork Order: L0204323
DGI1-3F ALK W
ANALYTICAL QC SUMMARY REPORTTest Method: SM2320 B
Sample ID MB-R2983
Analyte
Alkalinity, Bicaibonate (As CaCO3)
Alkalinity, Caibonate (As CaCO3)
Hydroxide (As CaCO3)
Alkalinity, Total (As CaCO3)
Sample ID LCS-R2983
Analyte
SampType MBLK
Batch ID R2983
Result
NDNDNDND
SampType LCS
Batch ID R2983
Result
TestCode ALK_W Units mg/L
TestNo M2320 B
PQL SPK value SPKRefVai
25252525
TestCode ALK_W Units mg/L
TestNo M2320B
PQL SPK value SPKRefVai
Prep Date
Analysis Date 4/29/02
%REC LowLimit HighLimit RPD Ref Val
Piep Date
Analysis Date 4/29/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_APITR-1_020429A
SeqNo 22904
%RPD RPDLimit Qual
Run ID L_AT1TR-1_020429A
SeqNo 22903
%RPD RPDLimit Qual
Alkalinity, Total (As CaCO3) 144 25 125 115 80 120
Sample ID LCSD-R2983
Analyte
Alkalinity, Total (As CaCO3)
Sample ID L0204322-001BDUP
Analyte
Alkalinity, Bicaibonate (As CaCO3)
Alkalinity, Caibonate (As CaCO3)
Hydi oxide (As CaC03)
Alkal ini ty, Total (As CaCO3)
SampType LCSD
Batch ID R2983
Result
122
SampType DUP
Batch ID R2983
Result
ND74
ND74
TestCode
TestNo
PQL
25
TestCode
TestNo
PQL
25252525
ALK_W
M2320 B
SPK value
125
ALK_W
M2320 B
SPK value
0000
Units mg/L
SPKRefVai
0
Units mg/L
SPKRefVai
0000
%REC
976
%R£C
0
000
Prep Date
Analysis Date 4/29/02
LowLimit HighLimit
80
Piep Date
Analysis Date
120
4/29/02
LowLimit HighLimit
0000
0
000
RPD Ref Val
144
RPD Ref Val
0750
75
Run ID L_ATITR-1
SeqNo 22906
_020429A
%RPD RPDLimit
165
Run ID L.AT1TR-1
SeqNo 22905
25
Qual
_020429A
%RPD RPDLimit
01 34
01 34
10101010
Qual
Qualifiers: ND - Not Delected at the Repoitmg Limit C - Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R- RPD outside accepted lecoveiy limits
J - This conccniiation is consideied an estimate due to LCS fa i lu ie
B - Analyte detected in the associated Method Blank
Page 21 of 28
Date: l6-May-02
CLIENT: RSSNWork Order: L0204323
Project: DGH-3F COD
ANALYTICAL QC SUMMARY REPORTTest Method: SM5520 D
Sample ID MB-R2949
Analyte
Chemical Oxygen Demand
Sample ID LCS-R2949
Analyte
Chemical Oxygen Demand
Sample ID LCSD-R2949
Analyte
Chemical Oxygen Demand
Sample ID L0204310-001BMS
Analyte
Chemical Oxygen Demand
Sample ID L0204310-001 BMSD
Analyte
SampType MBLK
Batch ID R2949
Result
ND
SampType LCS
Batch ID R2949
Result
533
SampType LCSD
Batch ID R2949
Result
503
SampType MS
Batch ID R2949
Result
554
SampType MSD
Batch ID R2949
Result
TestCode
TestNo
PQL
10
TestCode
TestNo
PQL
10
TestCode
TestNo
PQL
10
TestCode
TestNo
PQL
10
TestCode
TestNo
PQL
COD
M5220 C
SPK value
COD
M5220 C
SPK value
500
COD
M5220 C
SPK value
500
COD
M5220 C
SPK value
4625
COD
M5220 C
SPK value
Units mg/L
SPK Ref Val
Units mg/L
SPKRefVai
0
Units mg/L
SPKRefVai
0
Units mg/L
SPKRefVai
75
Units mg/L
SPK Ret Val
Prep Date
Analysis Date 4/29/02
%REC LowLimit HighLimit RPD Ref Val
Piep Date
Analysis Date 4/29/02
%REC LowLimit HighLimit RPD Ref Val
107 80
Piep Date
Analysis Date
120 0
4/29/02
%REC LowLimit HighLimit RPD Ref Val
101 80
Piep Date
Analysis Date
%REC LowLimit Hi
104 70
Piep Date
Analysis Date
120 533
4/29/02
ghLimit RPD Ref Val
130 0
4/29/02
%REC LowLimit HighLimit RPD Ref Val
Run ID 1 _\VC_020429C
SeqNo 22627
%RPD RPDLimit
Run ID L_\VC_020429C
SeqNo 22626
%RPD RPDLimit
0
Run ID L_WC_020429C
SeqNo 22630
%RPD RPDLimit
579 15
Run ID I _WC_020429C
SeqNo 22628
%RPD RPDLimit
0
Run ID L_\VC_020429C
SeqNo 22629
%RPD RPDLimit
Qual ,
Qual
Qual
Qual
Qual
Chemical Oxygen Demand 546 10 4625 75 102 70 130 546 25
Qualifiers: ND - Not Detected at the Repotting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R-RPD outside accepted lecoveiy limits
/ - This concenUation is consideied an estimate due to LCS failuie
B - Analyte detected in the associated Method Blank
Page 22 of 28
Date: 16-May-02
CLIENT: RSSNWork Order: L0204323Project: DGH-3F HG 7470 D
ANALYTICAL QC SUMMARY REPORTTest Method: SW 7470-Diss
Sample ID MB-799
Analyte
Mercury
Samplype MBLK
Batch ID R_799
Result
ND
TestCode HG_7470_D Units mg/L
TestNo SW7470
PQL SPK value SPKRefVai
0 00020
Piep Date
Analysis Date
4/24/02
4/24/02
%REC LowLimit HighLimit RPD Ref Val
Run ID SUB-1625
SeqNo 29941
%RPD RPDLimit Qual
Sample ID LCS-799
Analyte
Meicury
Sample ID L0204310-003A
Analyte
Mercury
Sample ID R0204242-003AMS
Analyte
Mercury
Sample ID L0204310-003A
Analyte
SampType LCS
Batch ID R_799
Result
0 00499
SampType MS
Batch ID R_799
Result
000521
SampType MS
Batch ID R_799
Result
000521
SampType MSD
Batch ID R_799
Result
TestCode HG_7470_
TestNo SW7470
PQL SPK value
0 00020 0 005
TestCode HG_7470_
TestNo SW7470
PQL SPK value
0 00020 0 005
TestCode HG_7470_
TestNo SW7470
PQL SPK value
0 00020 0 005
TestCode HG_7470
TestNo SW7470
PQL SPK value
D Units mg/L
SPKRefVai
0
D Units mg/L
SPKRefVai
0
_D Units mg/L
SPKRefVai
0
_D Units mg/L
SPK Ref Val
Piep Date
Analysis Date
4/24/02
4/24/02
%REC LowLimit HighLimit RPD Ref Val
998 85
Prep Date
Analysis Date
115 0
4/24/02
4/24/02
%REC LowLimit HighLimit RPD Ref Val
104 85
Piep Date
Analysis Date
115 0
4/24/02
4/24/02
%REC LowLimit HighLimit RPD Ref Val
104 85
Piep Date
Analysis Date
115 0
4/24/02
4/24/02
%REC LowLimit HighLimit RPD Ref Val
Run ID SUB-1625
SeqNo 30057
%RPD RPDLimit
0
Run ID SUB-1625
SeqNo 29942
%RPD RPDLimit
0
Run ID SUB-1625
SeqNo 30059
%RPD RPDLimit
0
Run ID SUB-1625
SeqNo 29943
%RPD RPDLimit
Qual
Qual
Qual
Qual
Meicuiy 00051 0 00020 0005 102
Qualifiers: ND - Not Detected at the Repoitmg Limit C - Unspiked sample >5 tunes the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R- RPD outside accepted iccoveiy limits
J - Tins conctntiation is consideied an estimate due to LCS fai lu ie
B - Analyte detected in the associated Method Blank
Page 23 of 28
Date: 16-May-02
CLIENT: RSSN
Work Order: L0204323Project: DGH-3F HG 7470 D
ANALYTICAL QC SUMMARY REPORTTest Method: SW 7470-Diss
Sample ID R0204242-003AMSD
Analyte
SampType MSD
Batch ID R_799
Result
FestCode HGJ7470_D Units mg/L
FestNo SW7470
PQL SPK value SPKRefVai
Prep Date 4/24/02
Analysis Date 4/24/02
%REC LowLimit HighLimit RPD Ref Val
Run ID SUB-1625
SeqNo 30021
%RPD RPDLimit Qual
Mercuiy 00051 0 00020 0005 102
Qualifiers: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R- RPD outside accepted lecoveiy limits
J - This concentiation is consideied an estimate due to LCS fa i lu ie
B - Analyte detected in the associated Method Blank
Page 24 of 28
Date: 16 May-02
CLIENT: RSSNWork Order: L0204323Project: DGH-3F HG 7470 T
ANALYTICAL QC SUMMARY REPORT iTest Method: SW 7470-TotaI
Sample ID MB-800
Analyte
SampType
Batch ID
MBLK
R_800
Result
TestCode
TestNo
PQL
HG_7470_T
SW7470
SPK value
Units mg/L
SPKRefVai
Pi ep Date
Analysis Date
4/24/02
4/24/02
%REC LoviLmiit HighLimit RPD Ref Val
Run ID
SeqNo
SUB-1626
29947
%RPD RPDLimit Qual
Meicury ND 0 00020
Sample ID LCS-800
Analyte
Meicuiy
Sample ID L02043 10-002 A
Analyte
Samp Type LCS
Batch ID R_800
Result
000518
SampType MS
Batch ID R_800
Result
TestCode HG_7470_T
TestNo SW7470
PQL SPK value
0 00020 0 005
TestCode HG_7470_T
TestNo SW7470
PQL SPK value
Units mg/L
SPKRefVai
0
Units mg/L
SPKRefVai
Piep Date
Analysis Date
4/24/02
4/24/02
%REC LowLimit HighLimit RPD Ref Val
104 85
Prep Date
Analysis Date
115 0
4/24/02
4/24/02
%REC LowLimit HighLimit RPD Ref Val
Run ID SUB-1626
SeqNo 29946
%RPD RPDLimit
0
Run ID SUB-1626
SeqNo 29948
%RPD RPDLimit
Qual
Qual
Mercury 000541 0 00020 0005 108 85 115
Sample ID L0204310-002A
Analyte
SampType
Batch ID
MSD
R_800
Result
TestCode
TestNo
PQL
HG_7470_T
SW7470
SPK value
Units mg/L
SPKRefVai
Piep Date
Analysis Date
4/24/02
4/24/02
Run ID
SeqNo
%REC LowLimit HighLimit RPD Ref Val %R
SUB-1626
29949
PD RPDI imit Qual
Meicuiy 0 00539 0 00020 0005 108
Sample ID L0204310-002A
Analyte
SampType
Batch ID
DUP
R_800
Result
TestCode
TestNo
PQL
HG_7470_T
SW7470
SPK value
Units mg/L
SPKRefVai
Piep Date
Analysis Date
4/24/02
4/24/02
Run ID
SeqNo
%REC LowLimit HighLimit RPD Ret Val %R
SUB-1626
29945
PD RPDLimit Qual
Meicuiy ND 0 00020
Qualifiers: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted recoveiy limits
J - This concentiation is consideied an estimate due to LCS f a i l u i e
B - Analyte detected in the associated Method Blank
Page 25 of 28
Date: 16-May-02
CLIENT: RSSNWork Order: L0204323Project: DGH-3F NH3-N W
ANALYTICAL QC SUMMARY REPORT
Test Method: SM4500-NH3 C
Sample ID MB-R2996
Analyte
SampType MBLK
Batch ID R2996
Result
FestCode NH3-N_W Units mg/L
TestNo M4500-NH3 C
PQL SPK value SPKRefVai
Piep Date
Analysis Date 4/30/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_WC_020430A i
SeqNo 23035|
%RPD RPDLimit Qual 1
Ammonia, as N ND 030
Sample ID LCS-R2996
Analyte
SampType LCS
Batch ID R2996
Result
TestCode NH3-N_W Units mg/L
TestNo M4500-NH3 C
PQL SPK value SPKRefVai
Piep Date
Analysis Date 4/30/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L WC 020430Aj
SeqNo 23034
%RPD RPDLimit Qual
Ammonia, as N 1008 030 101 839 117
Sample ID LCSD-R2996 SampType LCSD
Analyte
Batch ID R2996
Result
TestCode NH3-N_W Units mg/L
TestNo M4500-NH3 C
PQL SPK value SPKRefVai
Piep Date
Analysis Date 4/30/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_WC_020430A
SeqNo 23037
%RPD RPDLunit
|
1
Qual
Ammonia, as N 1 01 030 101 839 117 1 008 0 198 25
Sample ID L0204322-001BMS
Analyte
SampType MS
Batch ID R2996
Result
TestCode NH3-N_W Units mg/L
TestNo M4500-NH3 C
PQL SPK value SPKRefVai
Piep Date
Analysis Date 4/30/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_WC_020430A 1
SeqNo 23036
%RPD RPDLimit Qual
Ammonia, as N 1 12 030 112 764 124
Qualifiers: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R RPD outside accepted lecoveiy limits
J -1 his conccntialion is consideied an estimate due to LCS failuie
B - Analyte detected m the associated Method Blank
Page 26 of 28
Date: !6-May-Q2
CLIENT: RSSNWork Order: L0204323Project: DGII-3F SULF W
ANALYTICAL QC SUMMARY REPORTTest Method: SM4500-S D
Sample ID MB-R2855 SampType MBLK
Analyte
Sulfide
Batch ID R2855
Result
ND
TestCode SULF_W Units mg/L
TestNo M4500-S D
PQL SPK value SPKRefVai
0030
Prep Date Run ID LjSPEC-2_020426A
Analysis Date 4/26/02 SeqNo 21795
%REC LowLimit HighLimit RPD Ret Val %RPD RPDLimit Qual
Sample ID LCS-R2855
Analyte
Sulfide
SampType LCS TestCode SULF_W Units mg/L Piep Date Run ID L_SPEC-2_020426A
Batch ID R2855 TestNo M4500-S D Analysis Date 4/26/02 SeqNo 21794
Result PQL SPK value SPKRefVai %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
0107 0030 0107 0 100 80 120 0 0
Sample ID LCSD-R2855
Analyte
Sulfide
Sample ID L0204310-001BMS
Analyte
SampType LCSD
Batch ID R2855
Result
0 111
SampType MS
Batch ID R2855
Result
TestCode
TestNo
PQL
0030
TestCode
TestNo
PQL
SULF_W Units mg/L
M4500-S D
SPK value SPKRefVai
0 107 0
SULF_W Units mg/L
M4500-S D
SPK value SPKRefVai
Piep Date
Analysis Date 4/26/02
%REC LowLimit HighLimit RPD Ref Val
104 80 120 0 107
Piep Date
Analysis Date 4/26/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_SPEC-2_020426A
SeqNo 21796
%RPD RPDLimit
367 25
Qual
Run ID L_SPEC-2_020426A
SeqNo 21797
%RPD RPDLimit Qual
Sulfide 0 114 0030 0107 0 107 70 130 0
Sample ID L0204310-001BMSD
Analyte
SampType MSD
Batch ID R2855
Result
TestCode SULF_W Units mg/L
TestNo M4500-SD
PQL SPK value SPKRefVai
Piep Date
Analysis Date 4/26/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_SPEC-2_020426A
SeqNo 21798
%RPD RPDLimit Qual
Sulfide 0 109 0030 0 107 102 70 130 0 114 4 4 8 25
Qualifiers: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted tecoveiy limits
J - 1 his concent!ation is consideied an estimate due to LCS failuie
B - Analyte detected in the associated Method Blank
Page 2 7 of 28
Date: 16-May-02
CLIENT: RSSNWork Order: L0204323Project: DGH-3F TDS W
ANALYTICAL QC SUMMARY REPORTTest Method: SM2540 C
Sample ID MB-R2814
Analyte
SampType
Batch ID
MBLK
R2814
Result
TestCode
TestNo
PQL
TDS_W
E160.1
SPK value
Units mg/L
SPKRefVai
Prep Date
Analysis Date
%REC LowLimit Hi
4/24/02
ghLimit RPD Ref Val
Run ID
SeqNo
L_\VC_0204241
21508i
%RPD RPDLimit Qual
Total Dissolved Solids ND 150
Sample ID LCS-R2814
Analyte
Total Dissolved Solids
SampType LCS TestCode TDS_W Units mg/L Prep Date Run ID L_\VC_020424I '
Batch ID R2814 TestNo E160.1 Analysis Date 4/24/02 SeqNo 21507
Result PQL SPK value SPKRefVai %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
967 150 1000 0 967 80 120 0 0
Sample ID L0204356-003EDUP SampType DUP
Analyte
Batch ID R2814
Result
TestCode TDS_W Units mg/L
TestNo E160.1
PQL SPK value SPKRefVai
Prep Date
Analysis Date 4/24/02
%REC LowLimit HighLimit RPD Ref Val
Run ID L_WC_020424I
SeqNo 21509
%RPD RPDLimit1
Qual '
Total Dissolved Solids 346 150 367 589 25
Qualifiei s: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times the amount spiked
Jl - MS or MSD outside accepance limits LCS acceptable R - RPD outside accepted lecoveiy limits
J - This concentiation is consideied an estimate due to LCS fa i lu ie
B - Analyte delected in the associated Method Blank
Page 28 of 28
Date: 16-May-02
NEL LABORATORIESReno • Las Vegas • Boise
Phoenix • Sacramento
CHAIN OF CUSTODY NEL Work Order: £-O'LO<~(
Project Name
Phoenix Division • 3201 So 35th Street, Suite B6 • Phoenix, Arizona 85034602-437-0099 • Fax 602-437-2225 • 888-238-2514
Company Attention
Address
Phone Numb ax Number
Billing Address Expected Due Date/v
Requested Turnaround1 5-day 2-day 1 -day Othe
Time/DateSampled Customer Sample Identification
NE.LIdentification
urchase Order Number
Project Number
Sampled By
Analysis
X
JLY 7%
Q( Y
D fflt£ X
Custody Seal intact? YCondition
Box#1 DW Drinking Water SD SolidWW Waste Water AQ AqueousOI_ Oil/Organic Uquid A Air
Box #2 A HC!B HNO3
C H2SO4
D NaOH
E Ice OnlyF Other_G Not Preserved
Relinquished by (Ppnt) Date/Time Received by (Print) (Signature) Date/Time \
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The liability of NEL Laboratories Inc is limited strictly to the price of sample analysis for those samples received in good condition by NEL NEL is not responsible for loss damage resampling costs and/or qualified data related to samples not received in good conditionIncluding adequate sample volume and number of containers Customer signature of this CoC constitutes a purchase order for NEL to perform work and constitutes acceptance of all NEL Standard Terms and Conditions Signature also constitutes acceptanceof NEL Standard List Prices for all services ordered here on, except those specified otherwise via an NEL Quotation for Testing Services in effect at the time of sample receipt NEL turnaround times are measured in regular working days Samples received at thelaboratory after 16 30 will be considered received on the next working day Commitment of laboratory to the requested turnaround time wilt be confirmed via Sample Confirmation transmitted to the fax number provided above
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