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Page 1: Assessing the Slaking Behavior of Clay-Bearing Rocks

Assessing the Slaking Behavior of Clay-Bearing Rocks

Abdul ShakoorTej P. Gautam

10th Annual Technical ForumGEOHAZARDS IMPACTING TRANSPORTATION IN

THE APPALACHIAN REGIONColumbus, OHIO

Department of Geology, Kent State University

Page 2: Assessing the Slaking Behavior of Clay-Bearing Rocks

CLAY-BEARING ROCKS

Because of their low durability, clay-bearing rocks result innumerous problems in engineering construction, especially slope stability

SHALES

CLAYSTONES

MUDSTONES

SILTSTONES

Comprise approximately two-thirds of the stratigraphic column

Cover one-third of the total land area

Deteriorate rapidly upon exposure to atmospheric processes (low

durability)

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A slope failure in Pittsburgh caused by low-durability claystone

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A slope failure in Ohio caused by low-durability claystone/mudstone

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Newly excavated rock mass

One year after excavation

FIELD BEHAVIOR OF CLAY-BEARING ROCKS

Because of extensive disintegration, it is hard to find an intact rock block

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RESEARCH OBJECTIVES

Assess the slaking behavior of clay-bearing rocks under natural atmospheric conditions and quantify the nature of slaked material in terms of grain size distribution.

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Twenty different clay-bearing rocks were selected for the study including:

5 shales5 claystones5 mudstones5 siltstones

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SAMPLE LOCATION AND CLASSIFICATION

Potter et al. (1980) classification was used to classify samples into shales, claystones, mudstones, and siltstones

Laboratory Tests:

Slake durability index (Id2, Id3, Id4, Id5)

Grain size distribution of the slaked material retained in 2 mm-mesh drum after the test

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Slake Durability Test Apparatus

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GSD of Slaked Material (Lab)Shale (2)

0

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110100Particle size (mm)

Perc

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Cycle 1

Cycle 2Cycle 3

Cycle 4Cycle 5

Claystone (1)

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Cycle 1Cycle 2Cycle 3Cycle 4Cycle 5

Siltstone (3)

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Cycle 1

Cycle 2Cycle 3

Cycle 4Cycle 5

Shale

Claystone Siltstone

Mudstone

Samples after 5th cycle

Mudstone (3)

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Cycle 1

Cycle 2Cycle 3Cycle 4Cycle 5

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Simulation of Field Slaking Behavior Twelve replicate samples of each of twenty clay-

bearing rocks were prepared. Each sample consisted of 10 pieces, weighing 40-60 g, with a total weight of 450 to 550 g. All sample pieces were retained on 1-inch sieve.

Each replicate sample was placed in a 9-inch diameter pan and exposed to natural climatic conditions for 1 year period, from September 2009 to September 2010.

After each month, one sample of each of four rock types was removed and its grain size distribution was determined.

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Samples Being Exposed to Natural Climatic Conditions

Picture: All samples on roof

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Initial Samples

Shale

ClaystoneSiltstone

Mudstone

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After 1 Month

Shale

Claystone Siltstone

Mudstone

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After 3 Months

Shale

Claystone Siltstone

Mudstone

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After 6 Months

Shale

Claystone Siltstone

Mudstone

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After 9 Months

Shale

Claystone Siltstone

Mudstone

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Observations of Slaking BehaviorSample Month-1 Month-3 Month-6 Month-9Shale-3 Highly

fractured; very few pieces remained intact

Most pieces crumbled into smaller particles

All pieces crumbled into smaller particles

All pieces crumbled into small particles (2-6.3 mm)

Claystone-1

Highly fractured; hardly any intact pieces left

Most pieces crumbled into smaller particles

All pieces crumbled into smaller particles

All pieces crumbled into approx. 2mm-size particles

Mudstone-3

Mostly intact pieces; some fractures developed

Numerous fractures developed; slightly-highly fragmented

Most pieces crumbled into smaller particles

All pieces crumbled into smaller, nearly uniform particle size (2-6.3 mm)

Siltstone-3

All pieces remained intact

All pieces remained intact

All pieces remained intact; a few small fractures developed

Some fractures appeared but all pieces remained intact

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GSD of Slaked Material (Field)After 1, 3, 6, 9 Months

Claystone (1)

0

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110100Particle size (mm)

Per

cent

reta

ined

by

wei

ght

Cycle 2

M1M3

M6M9

Mudstone (3)

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Cycle 2

M1M3

M6M9

Shale (3)

0

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40

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110100Particle size (mm)

Per

cent

reta

ined

by

wei

ght

Cycle 2

M1M3

M6M9

Siltstone (3)

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tCycle 2

M1M3

M6M9

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Second cycle slake durability test overestimates the durability for claystones and underestimates the durability for siltstones and shales. For mudstones, it appears to provide a more representative value.

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ASTM Description of Retained Material

Type I

Type II

Type III

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In order to represent a wide range of disintegration behavior of clay-bearing rocks, a new parameter called “disintegration ratio” was used (Erguler and Shakoor, 2009)

Grain Size Distribution

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tShale (3)Claystone (5)Mudstone (3)Siltstone (3)

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DISINTEGRATION RATIO

003.0)(

)()5( abcdAreabciAreaClaystoneD R

315.0)(

)()3( abcdAreabcgAreaMudstoneD R

926.0)()()3(

abcdAreafbceAreaSiltstoneD R

T

CR A

AD )( Ratiotion DisintegraAC = area under any grain size distribution curveAT = total area encompassing grain size distribution curves of all samples

DR = 1, Completely durable

DR = 0, Completely non-durable

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Disintegration Ratio vs. Slake Durability Index (2nd cycle) - Lab Results

y = 0.0001x2 - 0.004xR2 = 0.87

0

0.2

0.4

0.6

0.8

1

0 20 40 60 80 100

Slake durability index (Id2)

Dis

inte

grat

ion

ratio

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Disintegration Ratio (Field Samples) vs. Slake Durability Index (2nd cycle)

0.00.10.20.30.40.50.60.70.80.91.0

0 20 40 60 80 100

Slake durability index (Id2)

Dis

inte

grat

ion

ratio

(3 m

onth

s)

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CONCLUSIONS Slake durability test does not predict the field

behavior of clay-bearing rocks.

During the 9-months period of exposure, claystone and mudshale completely disintegrated during the first 3 months, whereas siltstone was found to be the most durable. Mudstone exhibited an average disintegration behavior.

A wide range of disintegration behavior, as indicated by the particle size distribution of slaked material, can be described using the disintegration ratio.

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