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Page 1: 1S¿ XÇG xÿ ¤ x { z ¥ ~ £ X M a X ¥ X¸Ê < e [ ChemTHEATRE T · 1S¿ XÇG xÿ ¤ x { z ¥ ~ £ X M a X ¥ X¸Ê < e [ChemTHEATRE TAIST-MeRAM Xå:'Ê \w1 ¨ l/2 ¨Ö 6k3 ¨T

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Chemicals in the THEATRE (Tractable and Heuristic E-Archive for Traceability and Responsible-care Engagement)

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ProjectID āiňŨƑƢſŲŸƈŘID Ę>�œ�+ PRA000020

ChemicalID $�Yċ1:¿ÚŘID Ę>�œ�+ CH0000277

ChemicalName $�Yċ1:¿; Ę>�œ�+ Diclofenac

OfficialMethod �V· �V·ľĸŨF:řƨŌŘ;ÙŔID No

Extraction �#· Solvent, LLE, SPE/SPME, Soxhlet, PSE/ASE SPE

Extraction_details �#·ŘĂã Solvent, Cartridge, Gel, Shaking, Homogenization, Sonication, etc. Cartridge

Cleanup ŸƟƥƣŮƄƑ· LLE, Deproteination, Alkali saponific, Filteration/ultrafiltration, Chromatography

Filtration

Cleanup_details ŸƟƥƣŮƄƑ·ŘĂã Solvent, Acid, Alkali, Filter, Cartridge, Gel, etc. Filter

Derivatization Ą[�1 Ą[�1Āíƨ�ÊņŖĹF:řNone None

Chromatography ŸƢƕƈŹƞƏůƥ GC, LC, IC, TLC, Other, or None LC

Detector ¥#? HRMS, Q-MS, MS-MS, IT-MS, Tof-MS, Tof/tof, Q-tof, FID, ECD, or Other MS-MS

Ionization Űŵƣ1 EI, NCI, PCI, FI, ESI, APCI, APPI, MALDI, or Other ESI

Standard ©º= Āí;Ù Diclofenac sodium

Recovery_correction @7Ãó® @7Ãó®Ř�½Yes or No Yes

Calibration ŷƚƟƐơƥžƝƣ 1. External calibration, 2. Internal calibration (isotope dilution method),3. Matrix-matched external calibration, 4. Standard additions

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Intra-day precision �"H0 �� 0.83%

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Recovery_spike_relative "ĝ©ºœó®ņōoŘ©Ï¿ďŘ@7à �� 90 ± 0.81%

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Recovery_IS "ĝ©ºŘæY@7à �� 80 ± 6.8%

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