Wisconsin Department of Natural Resources Laboratory · PDF filea, i,. I e~ Wisconsin...
Transcript of Wisconsin Department of Natural Resources Laboratory · PDF filea, i,. I e~ Wisconsin...
a, i,. I e~
Wisconsin Department of Natural ResourcesLaboratory Report
08/08/2016 Lab: 113133790 Sample: 26Z$35001 P(lge I of 22
£&bor¢Jory.. Wisconsin state Laboratory of Hygiene2601 Agriculture DrMadisonP/zo7je.. 8004424618
Sample:
Fz.e/d #.' MW1010PCollection start: 06lz8/2016 07..50 aim
CoJ/ecfec7 6v`.' ZOE MCMANAMAD#., 03180
Cot/#ty.. Rusk
VI 53718Fcac p¢oj?e .. 608-224-6213
I)IVR JD 113133790
Scz7xpJe #.. 262935001
Collection End.. 06/Z8/2016 0]..50 a.inwaterbody/Ouif ell Id:
ID Point #:Ac.count #.. WAj063
Sc7#ip/€ £ocafz.o7z.. FLAMBEAu hHNES'c!7xp/e I)escr7Pfro72.. GROUNDWATER MONITORING WELL -SPLIT SAMPLE
Siimple soui`ce.. Mon±torin8Wch Sample Depth.. NI)czre jtepor/ed`. 08/08/2016 S'cifxp/e s'/cltrs.. COMPLETE
Project No: Sanple Reasorl:Comment:
Analyses and Resuits:
4nelysis Method Analysis Dale Lab Coniment
EPA 200.7 06/30/2016C:ode Deschption Re!sult Units LOD Report Limit LOQ
1005 BAREM DISS 0.0444 MGfu 0.00100 0-00300
915 cALcrolvI Dlss 47.0 MGth 0.100 0.300
1030 CHROMIUM I)ISS ND ugth 1.00 3.00
1040 COPPER DISS ND ugth 5.00 15.0
46570 HARDNESS, CA MG CALCULATEI) 171 MGth 0.660 2.00
(MGn As cAco3)
Wisconsin Department of Natural ResourcesLaboratory Report
08/08/2016 Lab: 1T3133790 Sample: 26Z935001 Page 2 Of 22
Code Description Resul[ Units LOD Raport Liinit LOQ1046 IRON DISS ND MGEL 0.loo 0.300
925 MAGNEslun¢ Dlss 13.0 MGth 0.loo 0.300
1056 MANGANESE DISS 63.2 ugEL 1.00 3.00
1145 SELENIUM DISS ND ugth 10.0 30.0
1075 SILVER DISS ND ugth 2.00 6.00
logo ZINC DISS 7.29 ugth 5.00 15.0
nalysis Me{liod Aiialysis Date Lab comment
SM2540C 07/05/2016Code Descrip{iorl Result Urlits LOD Report Liriiil LOQ70300 RESIDUE DISS 180C (TOTAL 208 MGth 50,0 50.0
DISSOLVED SOLIDS)
iialysis Method `drlalysis Date L{ib corirment
sM25 1 oBI]PAi 5o. 1 ,sM23 2oB o6rso/2 oi 6Code Description Res{ilt Units LOD Repon Linii[ LOQ410 ALKALINITy TOTAL CAc03 154 MGn, 2.55 2.55
95 CONDUCTIVITY, UMHOS/CM @ 360 uS/cm 10.0 10.025C
403 PHLAB 7.75 SU i.00 I.00
nalysis Method A}ralvsis Date Lab corrrmenl
SM3113B 07/08/2016Code Description Resttlt Units LOD Report Linrit LOQ1025 CADMIUMDISS NI) ugth 0.0500 0,150
rlalysis Method Analysis Dale Lab comment
EPA 245.I 06/29/2016:ode Description Result Units LOD Report Limit LOQ
71890 MERCURY DISS ND ugEL 0.030 0.080
08/08/2016
Wisconsin Department of Natural ResourcesLaboratory Report
Z4Z...113133790 5'c}mp/e.. 262935002 Pc/g€ 3 a/22
I,flbormfory.. Wisconsin state Laboratory of Hygiene2601 Agriculture DrMadisonP/!o«e.. 8004424618
Sample:
Field #: NIW10L3Collection start.. 06/Z81201610..1S z`m
Co/jcc/ec/ bv..' ZOE MCMANAMAID#.. 03180
Coit#ty.. Rusk
VI 53718Fc£[ P¢oF?e .. 608-224-6213
DNRJD 113133790
Sample #.. 262935002Collec`tion End.. 0612812016 lo..1S am
Waterbody/Outf all Id :ID Point #:Ac.count #.. WA;063
Scr#7p/e focafro7€.. FLAMBEAU NINES'c2mp/e Descr!Z}fro7z.. GROUNDWATER MONITORING WELL -SPLIT SAMPLE
San3ple source: Nloultorin8"ldi Sample Depth:Dczre Repor/ed.. 08/08/2016 5Ycwxp/e 6'z#/z4b'.. COMPLETE
Project No : Sample Reason :Coriiment:
Analyses and Results..nalysis Method Analysis Date Lab comment
EPA 200.7 06/30/2016Cede Description1005 BARIUMDISS
915 CALCIUM DISS
1030 CHROMIUMDISS
1040 COPPERDISS
46570 HARDNESS, CA MG CALCULATED(MGEL AS CAC03)
1046 IRONDISS
925 MAGNESIUM DISS
1145 SELENIUMDISS
1075 sn.vERDlss
1090 ZINCDISS
Resulf Units LOD126 ug/L 1.00
150 MGth 0.100
ND ugth 1.00
21.9 ug/L 5.00
568 MGEL 0.660
1.73 MGth 0.loo
47.2 MGth 0.100
15.1 ug/L 10,0
2.79 ug/L 2.00
ND ugth 5-00
Report Lilnit I-OQ3.00
0-300
3.00
Analysis Method Analysis Date Lab commerit
EPA 245.I 06/29/2016`,ode I)esariptioii Result Units LOD Raport Limit LOQ
71890 MERCURY DISS ND ug/L 0.030 0.080
nalysis Method Alialysis Date Lch corrunen{
EPA 375.2 07/21/2016Code Description Rest{lt Units LOD Report Limit LOQ946 SULFATE DISS 29.4 MGth 4.70 15.0
Wisconsin Department of Natural ResourcesLaboratory Report
08/08/2016 Lab: 113133790 Sample: 26293S002 P(lge 4 Of 22
Code Descriptioii Resull Units LOD Report Limit LOQ
nalysis Method Analysis Date Lab cornnient
SM3113B 07/08/2016C:ode Description Result Units LOD Report I.imit LOQ1025 CADMIUMDISS ND ug/L 0.0500 0.150
nalvsis Method Aiialysis Dale Lab conimen{
SM2510B,EPA150.1,SM2320B 06/30/2016Code Deseripliori Result Units LOD Report Limi[ LOQ410 ALKALINITY TOTAL CAC03 608 MGth 0.255 0.255
95 CONDUCTIVITY, UMHOS/CM @ 1080 uS/cm i.00 1.0025C
403 PHLAB 6.30 SU 0.100 0.100
iialvsis Method Alralysis Date Lab corrmeri{
SM3113B 06/30/2016Code Desckp{ion Resiilt Uriits LOD Report Limit LOQ1049 LEADDISS ND ug/L 1.00 3.00
Analysis Method Analysi.s Date Lab comment
SM2540C 07/05/2016Code Descripfron Result Units LOD Report Liinit LOQ70300 RESIDUE I)ISS 180C (TOTAL 698 MGth 50.0 50.0
DISSOLVED SOLDS)
4naly,sis Method Analysis Date Lub comment
EPA 200.7 06/30/2016Code De.scription Result Uni,ts LOD Report Linit LOQ1056 MANGANESE DISS 27400 ugth 20.0 60.0
nalysis Method Analysis Date Lab comment
SM3113B 07/01/2016Code Description Result Units LOD Repott Linit LOQ1000 ARSENICDISS ND ug/L 2.00 6.00
Wisconsin Department of Natural ResourcesLaboratory Report
08/08/2016 Lab: 113133790 Sample: 26Z93sO03 Page 5 Of 22
I,flbor#fop?.. Wisconsin state Laboratory of Hygiene2601 Agriculture DrMadisonP/Io7!e I. 8004424618
Sample:
F7.a/d #.. MW1013ACollection start: 06lz81201610..2S aim
Co//eczec7 5v... ZOE MCMANAMAJD#.. 03180
Co!f#¢J.. Rusk
VI 53718Fas P¢o7}e .. 608-224-6213
z]rm+z] 113133790
Scz"p/e #.. 262935003Collection End: 06/2812016 10..2S ilm
Wtiterbody/Ouif ;all Id :
ID Point #:Ac.count #: WA063
^Scr#ip/c foca/I.o„.. FLAIVBEAu hflNES'a772p/e Descrzp/z-o7?.. GROUNDWATER MONITORING WELL -SPLIT SAMPLE
San€ple source: Mowitoringwch Sample Depth:Dc!!e j{epor/ed.. 08/08/2016 5'cz7#p/e sY/cj"ts`. COMPLETE
Project No.` Sample Reason:Comment:
Analyses and Results..4nalysis Method Analysis Date Lab comment
SM3113B 07/01/2016i:ediieiiFdriiii-Ji. Result Units LOD Report Limit LOQ1000 ARSENICDISS NI) ugth 2.00 6.00
1nalysis Method Ailalvsis D(ite Lab comment
EPA 245.1 06/29/2016Code Description Res.ilt Units LOD Report Linlit LOQ7i89o MERcuR¥ Dlss r`ro ugth o.o3o o.o8o
nalysis Method Analysis Dale Lab comment
SM2510B,EPA150.1,SM2320B 06/30/2016:ode Description Result Units LOD Report Linit LOQ410 ALKALINITY TOTAL CAC03 351 MGth 2.55 2.55
95 CONDUCTIVITY, UMHOS/CM @ 967 uS/cm 10.0 10.025C
403 PHLAB 6.88 SU 1.00 1.00
nalvsis Method Analysi.s Date Lab comment
EPA 375.2 07/21/2016I,,,`. ,,`..``.,.ipt- rl.-\!,.', I `,I,,` I.,-)1' R(p",., L,,,,,, I-1)(I)
946 SULFATEDISS 187 MGth 47.0 150
ralysis Method Analysis Dale Lab comment
EPA 200.7 06/30/2016
Wisconsin Department of Natural ResourcesLaboratory Report
08/08/2016 Lch: 113133790 Sample: 26Z93S003 Page 6 Of 22
Description1005 BARIUMDISS
915 CALCIUM DISS
io3o clmoMluMDlss1040 COPPERDISS
46570 HARDNESS, CA MG CALCULATED(MGth AS CAC03)
1046 IRONDISS
925 MAGNE SIUM DISS
1056 MANGANESE DISS
1145 SELENIUMDISS
1075 SH.VERDISS
1090 ZINCDISS
Resull Units LOD77.4 ugth I.00
151 MGn, o.loo
ND ugth I.00
ND ugth 5-00
599 MGfr 0.660
0.285 MGth 0.loo
53.6 MGth 0.loo
4390 ug/L 1.00
NI) ugth 10.0
3.21 ug/L 2.00
ND ugth 5.00
rialysis Methc]d Analysis Dale Lab comment
SM3113B 07/08/2016i:iEET5e-:-Eii;ption Result Units LOD Report Limit LOQ
1025 CADMIUMI)ISS ND ug/L 0.0500 0.150
1nalvsis Metliod Amalvsis Date Lab co7mnent
•SM3113B 06/30/2 016
I-,;`i: ,\.,``.,.,.p,,"i, R`..`,,i,I !,,,` I,)I, il`:.."-, I,,:i,,I()(-,
1049 LEADDISS NI) ugH 1.00 3.00
nalysis Methoc] Analysis Date Lab corriment
SM2540C 07/05/2016:ode Description Result Units LOD Report Limit LOQ70300 RESIDUE DISS 180C (TOTAL 648 MGth 50.0 50.0
DISSOLVED SOLIDS)
Wisconsin Department of Natural ResourcesLaboratory Report
08/08/2016 Lab..1+3133790 Sample: 26&93sO04 Page 7 Of 22
I,&borflJory.. Wisconsin state Laboratory of Hygiene2601 Agriculture DrMadison VI 53 718P/jo7je.. 8004424618 Fan. P4oj7e.` 608-224-6213
Sample,
Fz.e/d #.. MW1013BCollection start.. 06/281201610..30 &m
Co//€cJec7 bv.. ZOE MCMANAMAJD#.. 03180
Co?/#fy.. Rusk
DNR ID 113133190
Sample #: 26293SO®4
Collection End.. 0612812016 10..30 zlm
wate].body/Outf all ld :ID Point #:Account #.. WAj063
Sc}#]p/e foca/I-o7!.. FLAMBEAU AflNES'c}#!pfe Descrzpfz.o7?.. GROUNDWATER MONITORING WELL -SPLIT SAMPLE
Sample source: Surf ]8Icewaller Sample Depth:Dc7fe Reporfed.. 08/08/2016 5Ycz;#p/e s'fo/!t6'.. COMPLETE
Proj ect No : Sample Reason :Comment:
Analyses ai.d Results..
r!alysis Method Analysis Date Lab commerit
EPA 200.7 06/30/2016Code Description Result Units LOD Report Limit LOQ
1056 MANGANESE DISS 32200 ug/L 20.0 60.0
}ialysis Method Analysis Date Lab comment
SM2540C 07/05/2016-`,-ode Description Re:suit Units LOD Report Limit LOQ
70300 RESIDUE DISS 180C (TOTAL 3100 MGA, 50.0 50.0DISSOLVED SOLIDS)
nalysis.Method Analysis Date Lab c,omment
SM3113B 07/01/2016I:&55fro&§EFi§T{6ir---- Re:sult Units LOD Report Limit LOQ
1000 ARSENIC DISS ND ug/L 2.00 6.00
08/08/2016
Wisconsin Department of Natural ResourcesLaboratory Report
Zc}b..113133790 6'o7#p/e.. 262935004 Pcrge 8 a/22
iialvsis Method A}ralvsis Date Lab corlunenl
EPA 200.7 06/30/2016Code Descriptionloos BARIUMDISS
915 CALCIUM DISS
1030 CHROMIUMDISS
1040 COPPERDISS
46570 IIARDNESS, CA MG CALCULATED(MGth AS CAC03)
1046 IRONDISS
925 MAGNESIUM DISS
1145 SELENIUMDISS
1075 SELVERDISS
1090 ZINCDISS
Res.ilt Units
10.5 ugth
609 MGth
1.13 ugEL
573 ugth
2130 MGth
LOD Reporl Limil LOQ1.00 3.00
0.loo 0.300
1.00 3.00
5.00 15.0
0.660 2.00
NI) MGEL 0.100
149 MGth 0.100
ND ugAJ 10-0
4.46 ug/L 2.00
130 ugth 5.00
nalvsis Method A]ralvsis Date Lab com}nenl
SM2510B,E PA150.1,SM23 20B 06/30/2016Code Desariptiori Result Units LOD Report Liniif LOQ410 ALKALINITY TOTAL CAC03 570 MGth 0.255 0,2.55
95 CONDUCTIVITY, UMHOS/CM @ 3070 uS/cm I.00 1.0025C
403 PHLAB 6.42 SU 0.100 0.100
iialvsis Method Aiialvsis Date Lab coriimen{
EPA 375.2 07/21/2016Code Description Result {jni{.s LOD Report Lini{ LOQ946 SULFATE Dlss isio MGn. 235 750
nalysis Method Analysis Date Lab comment
SM3113B 07/08/2016Code Description Result Units LOD Report Limit LOQ
1025 CADMIUMDISS 0.685 ugth 0.0500 0.150
08,/08/2016
Wisconsin Department of Natural ResourcesLaboratory Report
Zcrb..113133790 S'a7xp/e.. 262935005 Pcrge 9 a/22
I,¢bor¢fory.. Wisconsin state Laboratory of Hygiene2601 Agriculture DrMadisonP/!07je.. 800J424618
Sample,
Field #.. NIW1013CCo//ec/3.o7j s/¢rf.. 06/28/201610:10 am
Co//€c!ec/ dy... ZOE MCMANAMAJD#., 03180
Co!f#¢J.. Rusk
VI 53718FrtL-P¢o7!e .. 608-224-6213
DjvR /I) 113133790
Sample #: 26293S00SCollection End: 06/2812016 10..1® aim
Walerbody/Outf all Id :ID Point #:Account #.. WA:063
^S¢#!p/e foca/z.07!.. FLAIvmEAu hHhEAS'""p/e De,s'cj.I.p/z.a/2.. GROUNDWATER MONITORING WELL -SPLIT SAMPLE
Saniple source: Morirtorin8Wch Sample Depth.`Dc!re jzeporfed,. 08/08/2016 S'cz7xp/e s'rcj/zis`. COMPLETE
Proj ect No : Sanple Rea,son :Comment:
Analyses and Results:
rialysis Method Analysis Dare Lab comment
EPA 245.1 06/29/2016Code Description Result Units LOD Repo1.i Limit I.OQ71890 MERCURY DISS NI) ug/L 0.030 0.080
nulysis Method Analysis Date Lab comment
EPA 200.7 06/30/2016T6dFi- Description Re!sul{ Units LOD Report I.imit LOQ
1056 MANGANESEDISS 10700 ug/L 10.0 30.0
Analysis Method Analysi.s Date Lab comment
SM2510B ,EPA 150.1,SM232 0B 06/30/2 016f6dEiniiEFiFir6ir------- Result units LOD Report Lini{ LOQ410 ALKALINITYTOTAL CAC03 543 MGth 0.255 0.255
95 CONDUCTIVITY, UMHOS/CM @ 3050 uS/cm I.00 I.00
Wisconsin Department of Natural ResourcesLaboratory Report
08/08/2016 Lab: 1+3133190 Sample: 26Z93S005 Page lo of 22
fTJJ{froE§dr;F{{J;I---- Result units LOD Report Liinit LOQ25C
403 PHLAB 6.68 SU 0.loo 0.100
nalvsis Metliod Aiialysis Date Lab corlimenl
SM2540C 07/05/2 016i:[5J-fit;i;i;iJfr--- Res.lit units LOD Report Linii{ LOQ70300 RESIDUE DISS 180C (TOTAL 2940 MGth 50.0 50.0
DISSOLVED SOLIDS)
nalysis Method A]la[ysis Date Lab commerll
SM3113B 07/01/2016i=5iEIfE:Eifii6i-- Res.Ilt units LOD Report Linii[ LOQ
1000 ARSENICI}ISS 21.3 ug/L 2.00 6.00
4nalysis Method Analysis Dale Lab comment
EPA 200.7 06/30/2016Code Descriptionloos BARIUM DISS
915 CALCIUM DISS
1030 clmoMluMDlss1040 COPPERDISS
46570 HARDNESS, CA MG CALCULATED(MGEL AS CAC03)
1046 IRONDISS
925 MAGNESIUM DISS
1145 SELENIUM DISS
1075 SH.VERDISS
1090 ZINCDISS
Result Units LOD Report Limit LOQ15.5 ug/L 1.00 3.00
579 MGEL 0.100 0.300
ND ug/L i.00 3.00
ND ug/L 5.00 15.0
2050 MGEL 0.660 2.00
13.3 MGth
146 MGth
NI) ugfu
4.64 ugth
354 ugth
4ncllysis Method Analysis Date Lab comment
SM3113B 07/08/2016.`:-,h`.`. ,)"-`=;i,-,", ----- ` -__-` ` R`..`,,,, ,-,,,,` I-,)1\ R..r"i., I :,,,i, ((.)`']'
1025 CADMIUMDISS ND ug/L 0.0500 0.150
08/08/2016
Wisconsin Department of Natural ResourcesLaboratory Report
Lab: 113133]90 Sample: 262935006 Page I l of 22
I,&bor¢tory.. Wisconsin state Laboratory of Hygiene2601 Agriculture DrM adison lh71 53 718P/jo7je.. 8004424618 Fcrt p¢oj!e.. 608-224-6213
Sample,
F7.e/d #.. MW1014CCo//€c/z-o7! S/¢rJ.. 06/28/2016 08:30 am
Co/Jcc/ed Sv..' ZOE MCMANAMAJD#., 03180
Co?/7?fy.. Rusk
DIVRJD 113133790
Sample #.. 26293S006Collection End.. 06/28/2016 08..30 ilm
Waterbody/Outf all Id :ID Point #..Ac.count #: WA;063
^Sd#jp/e foccr/z.07i.. FLAIvmEAU NINES'c!xp/e Descrzpfz.07z.. GROUNDWATER MONITORING WELL -SPLIT SAMPLE
Sample source: NloHi:tor.\ngwch Sample Depthi`Dcf}e Rej7or/ed.. 08/08/2016 5'c"7jp/e s'J#/Its.. COMPLETE
Projec:i No : Sample Reason..
Comment:
Analyses antl Results:
4nalysis Method Arialysis Date Lab comnient
SM3113B 07/01/2016Code Desaription Result Units LOD Repoi.i I.i}nit LOQ1000 ARSENIC DISS 27.2 ug/L 2.00 6.00
lralvsis Method Aiialvsis D(ite Lcib comment
SM2510B,EPA150.1,SM2320B 06/30/2016Code Desorip{ion Resillt Uiiits LOD Report Liniil LOQ410 ALKALINITY TOTAL CAC03 269 MGth 2.55 2.55
95 CONDUCTIVITY, UMHOS/CM @ 1000 uS/cm 10.0 10.025C
403 PHLAB 6.90 SU 1.00 I.00
rulysi.s Method Analysis Date Lab coriiment
EPA 200.7 06/30/2016Code Descriptiori Res.ilt Units LOD Report Linit{ LOQ
1005 BARIUM DISS 32.5 ug/L 1.00 3.00
915 CALCIUM DISS 150 MGth 0.loo 0.300
1030 cmoMluM Dlss NI) ug/L 1.oo 3.oo
Wisconsin Department of Natural ResourcesLaboratory Report
08,/08/2016 Lab: 1+3T33790 Sample: 26Z93S006 Page 1 2 Of 22
`:ode Description ResulJ Units LOD Repol.i himit LOQ
1040 COPPER DISS ND ugth 5.00 15.0
46570 HARDNESS, CA MG CALCULATED 523 MGEL 0.660 2.00
(MGEL AS CAC03)1046 IRON DISS 4.69 MGth 0.loo 0.300
925 MAGNEslln4 Dlss 36.4 MGth 0-loo 0.300
1056 MANGANESE DISS 1710 ugiv 1.00 3.00
1145 SELENIUM DISS ND ugth 10.0 30.0
1075 SH.VER DISS NI ugth 2.00 6.00
1090 ZINC DISS 266 ugth 5.00 15.0
mlysis Method Analysis Date Lab comment
EPA 245.1 06/29/2016i:5EEinEiE;S[{5ir---- Result units I.oD Report Limit I.OQ71890 MERCURY DISS ND ugth 0.030 0.080
nalvsis Method A]ralysis Date Lab comment
SM3113B 07/08/2016i:5diin[§CFSi{6ir---- Res.Ilt uiiits LOD Report Limit LOQ
1025 CADMIUMDISS ND ugfu 0.0500 0.150
4rialysis.Method Analysis Date Lab comment
EPA 375.2 07/21/2016T6ETir5EiiiFiT5T--- Result Units LOD Report Limit LOQ946 SULFATEDISS 211 MGth 47.0 150
iralvsis Method Anelvsis Date Lab c,oriiment
SM3113B 06/30/2016f55irifJEi;i;ipiion Resi{lt Units LOD Report Liniil LOQ1049 LEAD DISS ND ug/L 1.00 3.00
Wisconsin Department of Natural ResourcesLaboratory Report
08/08/2016 Lab: 1L3133790 Sample: Z62935008 Page I 3 Of 22
I,&bor¢fo]}j.. Wisconsin state Laboratory of Hygiene2601 Agriculture DrMadison lvI 53 718P;jo7€e.. 8004424618 Fff¥ P*o7?e.. 608-224-6213
Sample:
Field #:
Collection Start:
Collected bv:
JD #..Con,nty,
Sci"ple Location:
MW1014B06/28/2016 08:43 amZOE MCMANAMA03180RuskFLAIVBEAu nnNE
DNR ID 113133790
Sample #.. 262935008Collection End.. 06/2812016 08=43 gim
wate].body/Outf all Id :ID Point #:
Account #: WA063
^S'c}7#pze Descr!P/z.ojz.. GROUNDWATER MONITORING WELL -SPLIT SAMPLESample source: Morf uor.\ng"idi Sample Depth: INDc7fe Repor/ed.. 08/08/2016 S'c!7#p/e stcztets.. COMPLETE
Project No: Sample Reason :Comment:
Analyses and Results:
nalvsis Method A}ialysis Date Lab corirmen[
EPA 245.I 06/29/2016Code Description Res.Ilt Units LOD Report Limit LOQ71890 MERCURY DISS ND ug/L 0.030 0.080
Analysis Method Amalysi.s Date I.ab comment
EPA 200.7 06/30/2016Code Deseription Result Urii{s LOD Report Limit LOQ
1005 BARIUM DISS 21.7 ug/L 1.00 3.00
915 cALcluM Dlss 5ii MGfr 0.loo 0.300
1030 CHROMIUM I)ISS ND ug/L 1.00 3.00
Wisconsin Department of Natural ResourcesLaboratory Report
08/08/2016 Lab: 1T3133790 Sample: 26Z93S008 Page 14 Of 22
Code Descriptioii Result Units LOD Repoi.t Linit LOQ1040 COPPER DISS 455 ugth 5.00 15.0
46570 HARDNESS, CA MG CALCULATED 1770 MGth 0.660 2.00
(MGEL AS CAC03)1046 IRON DISS ND MGth 0.100 0.300
925 MAGNEslun4 Dlss 120 MGA 0.100 0.300
1145 SELENIUM DISS ND ugEL 10.0 30.0
1075 SILVER DISS 3.20 ugth 2.00 6.00
1090 ZINC DISS 1040 ugA- 5.00 15.0
4rlalysis Method Antilysis Dale Lab comnient
SM2540C 07/05/2016Code Desc'riptioil Result Units LOD Repol.i Limit LOQ70300 RESIDUE DISs l80C (TOTAL 2450 MGth 50.0 50.0
DISSOLVED SOLIDS)
4nalysis Method Analysis Date Lab comment
EPA 375.2 07/21/2016Code Descriptioii Result Uniis LOD Report I.imit LOQ946 SULFATE DISS 1210 MGEL 235 750
llalysis Method Aiialysis D(lie Lab comment
SM3113B 07/01/2016Code Description Resillt Ullits LOD Report Limit LOQ
1000 ARSENICDISS ND ugth 2`00 6.00
nalysis Method Analysis Date Lab comment
SM3113B 06/30/2016`.ode Desci-iption Resul[ Units LOD Report Limit LOQ
1049 LEADDISS ND ug/L 1.00 3.00
Analysis.Method Analysis Date Lab comment
EPA 200.7 06/30/2016Code Description Result Uiiits LOD Report Linit LOQ1056 MANGANESE DISS 10800 ugth 10.0 30.0
Wisconsin Department of Natural ResourcesLaboratory Report
08/08/2016 Lab: 1T3T3379® Sanple: 26E93S009 Page I 5 Of 22
£¢bormtory.. Wisconsin state Laboratory of Hygiene2601 Agriculture DrMadison VI 53 718P/jo7je.. 8004424618 Ffrt. P¢077e.. 608-224-6213
Sample,
F7.e/d #.. MW1014ACollection start.. 0612612016 08..S0 z\m
Co//ecJec7 bv.' ZOE MCMANAMAJD#.. 03180
Co!f#ty.. Rusk
DNRJD 113133790
Sc}7#p/e #.. 262935009
Collec`tion End: 06/26/2016 08..S0 iimWaterbody/Ouif all ld :
ID Point #:Ac.count #: WA\063
^Scr#Ip/e foca/z.o73.. FLAMBEAU NINESYaxp!e Dt?sc/.zP/i.07z.. GROUNDWATER MONITORING WELL -SPLIT SAMPLE
Sample source`. Surt3ueewatf3r Sample Dapth:Da/e Raporjed.. 08/08/2016 S'¢7xp/e 6?c!/!tb'.. COMPIJETE
Project No : Sample Reason :Comment:
Analyses and Resuits..n{ilysis Method Analysis Date Lab comment
SM3113B 07/01/2016fina6- Description Result Units LOD Report Liinit LOQ
1000 ARSENIC DISS ND ug/L 2.00 6.00
iialysis Method Analysis Date Lab comment
EPA 200.7 06/30/2016Code Description1005 BARIUMDISS
915 CALCIUM DISS
1030 CHROMIUMDISS
1040 COPPERDISS
46570 HARDNESS, CA MG CALCULATED(MGn As cAco3)
1046 IRONDISS
925 MAGNESIUM DISS
1056 MANGANESE DISS
1145 SELENIUMDISS
1075 SHjvERDISS
1090 ZINCDISS
Res{Ilt Units LOD
13.6 ugth I.00
335 MGth 0.100
ND u8rfu 1.00
ND ugth 5.00
1330 MGEL 0.660
ND MGEL 0.100
120 MGth 0.100
98.2 ug/L 1.00
ND ugth 10.0
ND ugth 2.00
8.40 ug/L 5.00
1nalvsis Method Analysis Date Lab corirmenr
SM3113B 07/08/2016
Wisconsin Department of Natural ResourcesLaboratory Report
08/08/2016 Lab: 1+3T33790 Sample: 2629350Ow Page l 6 Of 22
Code Descriptioii Result Units LOD Repol.i Li]nit LOQ1025 CADMIUMDISS ND ug/L 0.0500 0.150
nalysis Method Aiialysis Date Lab coryrmeii[
EPA 245.1 06/29/2016-Code Description Result Units LOD Report Limit I,OQ
71890 MERCURY DISS NI) ug/L 0.030 0.080
n{ilysis Method Analysis Date I~ab comment
EPA 375.2 07/21/2016T6d{iniiFFii{{5Tr----- Result units LOD Re|ioi.t Linit LOQ946 SULFATEDISS 855 MGEL 235 750
nalysis Me{hcid Analysis Date Lab coriimerit
SM2510BF PA150.1,SM232 0B 06/30/2 016Code i5Z;I;STidfr-- Result units LOD Report Liniil LOQ410 ALKALINITY TOTAL CAC03 486 MGth 0.255 0.255
95 CONDUCTIVITY, UMHOS/CM @ 2090 uS/cm I.00 1.0025C
403 PHLAB 6.75 SU 0.100 0.100
nalysis Method Aunlysis Dale Lab comment
SM2540C 07/01 /2 016-i:ode Description Result Units LOD Report Linijl LOQ
70300 RESIDUE DISS 180C (TOTAL 1850 MGth 50.0 50.0DISSOLVED SOLIDS)
nalysis Method Analysis Date Lab corlrment
SM3113B 07/05/2016i:JdT--5e:s-chp{ion Result Units LOD Rapor{ Lirliit LOQ
1049 LEADI)ISS ND ug/L I.00 3.00
Wisconsin Department of Natural ResourcesLaboratory Report
08/08/2016 Lab: 113T33]9® Sample: 26293S010 Page 1 7 Of 22
£&bor¢fory.. Wisconsin state Laboratory of Hygiene2601 Agricu]tuFe DrMadison lh71 53 718P/jo7!e.. 8004424618 Fcur p¢oj7e.. 608-224-6213
Sam.plc:
Field#: 4®14
Collection start.. 06lz812016 09..00 i."Co//€cfec7 bv.. ZOE MCMANAMA
JD#.. 03180Cot/#O;.. Rusk
DjvR/D 113133790
Sci7#j7/e #.. 262935010
Collection End.. 06/2812016 09..00 aim
Waterbody/Ouifall Id:ID Point #:Account #.. V`lA;063
^Scr777p/e focafz.o7!.. FLAMBEAu nflNEAS'c}fflpze I)escr7Pfz-o7?.. GROUNDWATER MONITORING WELL -SPLIT SAMPLE
Sample source: Mohitorin8Vwdi Sample Depth: RII)aire I?ej7or/ed`. 08/08/2016 6Yc#7qp/e s'£"/w,}`.. COMPLETE
Project No: Sanple Reason :Comment:
Analyses and Results:.
4nalysis Method Arialysis Date Lab comment
SM3113B 07/01/2016
Code Descriptioi. Result Units LOD Report himit LOQ1000 ARSENICDISS ND ug/L 2.00 6.00
rralvsis Method Alialvsis Date L{ib commeiit
SM3113B 07/05/2016Code Description Resiilt Units LOD Report Linit LOQ1049 LEAD Dlss run u8th i.00 3.00
Analysis Method Analysi.s Dtffe Lub cominen[
EPA 245.1 06/29/2016Code Deseription Result Units LOD Report Limit LOQ71890 MERCURY DISS ND ug/L 0.030 0.080
nalysis Method Analysis Dale Lab comment
SM3113B 07/08/2016
08/08/2016
Wisconsin Department of Natural ResourcesLaboratory Report
Lab: 113133790 Sample: 26293S010 Page 1 8 Of 22
Code Descriptioii Result Units LOD Report Limit LOQ1025 CADMIUMDISS 0.0778 ugth 0.0500 0.150
halvsis Method Analvsis Dcite Ijab commeni
SM2540C 07/05/2016Code Deseription Result Units LOD Report Linrif LOQ70300 RESIDUE DISs l80C (TOTAL 488 MGth 50.0 50.0
DISSOLVED SOLIDS)
1iralvsis Method A}.alvsis Date Lab conirmen[
EPA 375.2 07/21/2016Code Description Resillt Uiiits LOD Eel)or[ Lirrli{ LOQ
946 SULFATE DISS 116 MGth 23.5 75.0
nalysis Method Arlalysi.s Dc}{e Lab comment
EPA 200.7 06/30/2016Code Description1005 BARIUMDISS
915 CALCIUM DISS
1030 clmoMluMDlss1040 COPPERDISS
46570 HARDNESS, CA MG CALCULATED(MGEL AS CAC03)
1046 IRONDISS
925 MAGNESIUM DISS
1056 MANGANESE DISS
1145 SELENIUMDISS
io75 sn.vERDlss
1090 ZINCDISS
Result Units LOD Report Limit LOQ36.4 ug/L I-00
81.3 MGth 0.loo
ND ugth I.00
ND u8fr 5.00
316 MGft 0.660
ND MGth 0.loo
27.4 MGth
2030 ugth
ND ugfu
rlD ugth
6.04 ugAJ
08,/08/2016
Wisconsin Department of Natural ResourcesLaboratory Report
fcrb..113133790 6'c#7?p/e.. 262935011 Page J9 o/22
£q!borotory.. Wisconsin state Labol.atory of Hygiene2601 Agriculture DrMadison lh71 53 718P/!07je.. 8004424618 Fcur p#o7?e.. 608-224-6213
Sample,
F''€'d #.. MW|000PRCollection start.. 06lz812016 0]..3S am
Co/Jccfet7 bv.. ZOE MCMANAMAJD#.. 03180
Co{f#¢J.. Rusk
DNR ID 113133790
S:cz7xp/e #.. 262935011
Collec.{ion End:. 06lz812016 07..35 gim
Waterbody/Outf all Id :ID Point #:Account #: "A,063
Sc}#jp/€ £oca/z.o7z.. FLAMBEAu hflNES'cj/72p/e Deb`crrp#-07z.. GROUNDWATER MONITORING WELL -SPLIT SAMPLE
Sample source: Nhorirtoringwch Sample Depth.`Dcrfe Repor/ed.. 08/08/2016 STcgmp/e 6'zc2/zfb'`. COMPLETE
Project No: Sample Reason:coTiiTnent:
Analyses and Resuits..rialysis Method Analysis Date Lab comment
SM2 540C 07/05/2 016Code Description Result Units LOD Report Limit LOQ70300 RESIDUE DISS 180C (TOTAL 544 MGAij 50.0 50.0
DISSOLVED SOLIDS)
nalysis Method Arlalysis Date Lab comment
SM3113B 07/05/2016Code Desci.ipliori Result Unils LOD Report Limit LOQ1000 ARSENIC DISS 8.55 ugth 2.00 6.00
lialvsis Method A}.alvsis Date Lcib corlimeiil
EPA 200.7 06rso;2016Code Deseription1005 BARIUMDISS
915 CALCIUM DISS
1030 CHROMIUMDISS
1040 COPPERDISS
46570 HARDNESS, CA MG CALCULATED(MGEL AS CAC03)
1046 IRONDISS
925 MAGNESIUM DISS
1056 MANGANESE DISS
ii45 sELENruMDlss
Res{Ilt Units LOD Report hiriiit34.3 ugth 1.00
Ill MGEL 0.100
NI) ugth I.00
NI) ugth 5.00
394 MGth 0.660
0.507 MGn. 0.loo
28.6 MGft 0.100
2070 ug/L I.00
ND u8fr io.0
Wisconsin Department of Natural ResourcesLaboratory Report
08,/08/2016 Lab: 1L3T33790 Sample: 26293S011 Page 20 Of 22
`,ode Description Result Units LOD Repoi.t Limit LOQ
1075 SHjvERDISS ND ug/L 2.00 6.00
1090 ZINCDISS 302 ug/L 5.00 15.0
nalvsis Method Airalvsis Date Lab coriiinenf
SM3113B 07/05/2016Code Descrip{iori Result Units LOD R.epori Limit LOQ
1049 LEAD DISS NI) ugth 1.00 3.00
nalysis Method Analysis Date Lab comnient
EPA 245.I 06/29/2016:ode Description Result Units LOD Report Limit LOQ
71890 MERCURY DISS ND ug/L 0.030 0.080
nalysis Method Analysis Date Lab com]nenl
EPA 375.2 07/21/2016Code Description Result Units LOD Report Limit LOQ946 SULFATE DISS 196 MGth 47.0 150
Comj#e7jJ.. MATRIX SPIKE QC EXCEEI)£D.
Analysis Method Analysis Date Lub comment
SM2510B,EPA150.1,SM2320B 06/30/2016Code Description Result Uwifs LOD Report Lini{ LOQ410 ALKALINITY TOTAL CAC03 211 MGth 2.55 2.55
95 CONDUCTIVITY, UMHOS/CM @ 779 uS/cm 10.0 10.025C
403 PHLAB 6.78 SU 1.00 I.00
inalysis Method Analysis Date Lab comment
SM3113B 07/08/2016Code Description Result Uni}s LOD Report Linit LOQ)
1025 CADMIUMDISS 0.107 ugivL 0.0500 0.150
Wisconsin Department of Natural ResourcesLaboratory Report
08/08/2016 Lab: T13133]90 Sample: 26Z93SOL2 Page 2 I of 22
I,&4ordrfory.. Wisconsin state Laboratory of Hygiene2601 Agriculture DrMadison Wrl 53 7 1 8P/!o7je.. 8004424618 Fur p#oj7e.. 608-224-6213
Sample,
F7.e/d #.I MW1000RCollection start: 06/2812016 01..20 am
Co/JecJec7 6v... ZOE MCMANAMAJD#., 03180
Co!f#ty.. Rusk
DNJZJD 113133790
Sample #.. 26Z93S012Collection End: ®6/28/2016 07..20 aim
wate].body/Outf all Id:ID Point #:Account #: WAL063
Scr#}p/€ £occ}/z.of!.. FLAMBEAU NINES'amp/e Descrrpfz.o77.. GROUNDWATER MONITORING WELL -SPLIT SAMPLE
Sample source: Pillonftorin8Wch Sample Depth:Dczfe Jtepor/ed.. 08/08/2016 5'c[7xp/e s/czr€is.. COMPLETE
Project No: Sanple Retlsan :Commerlt:
Ai.alyses and Resuits:nalysis Method Analysis Date I.ab comment
EPA 245.1 06/29/2016ffJile Description Resuli Units LOD Report I.ilnit I.OQ71890 MERCURY DISS ND ug/L 0.030 0.080
llalysis Method Aiialysis Date Lab comment
EPA 200.7 06/30/2016-Code Description Res{Ilt Units LOD Report Limit LOQ
1056 MANGANESE DISS 10200 ug/L 10.0 30.0
4rialysis Method Analysis Date Lab comment
SM3113B 07/05/2016:ode Desci.iption Resuh Units LOB Report Linit LOQ1000 ARSENIC DISS NI) ug/L 2.00 6.00
4ralysis Method Analvsis Date Lab Comment
EPA 200.7 06/30/2016
Code Description Result Units LOD Rapori Limit LOQ
1005 BARIUIVI DISS 28.3 ugth 1.00 3.00
915 CALCIUM DISS 69.0 MGfr 0.loo 0.300
1030 CHROMIUM DISS NI) ugth 1.00 3.00
1040 COPPER DISS 65.4 ugth 5.00 15.0
46570 IIARDNESS, CA MG CALCULATED 259 MGth 0.660 2.00
(MGEL AS CAC03)
08/08/2016
Wisconsin Department of Natural ResourcesLaboratory Report
Lab: 113133790 Sample: 262935012 Page 22 Of 22
Code Descriptioi. Result Units LOB Report Li]nit LOQ1046 IRON DISS ND MGEL 0.100 0.300
925 MAGNEslun¢ Dlss 21.0 MGEL 0.100 0.300
1145 SELENIUM DISS ND ugEL 10.0 30.0
1075 SILVER DISS ND ugEL 2.00 6.00
1090 ZINC DISS ND ugEL 5.00 15.0
iialvsis Method Analvsis Date Lab comment
SM2510BJIPA150.1,SM2320B 06/30/2016Code Descripliori Res{Ilt Units LOD Report Linli[ LOQ410 ALKALINITY TOTAL CAC03 145 MGth 2.55 2.55
95 CONDUCTIVITY, UMHOS/CM @ 559 uS/cm 10.0 10,025C
403 PHLAB 6.53 SU I.00 I.00
nalysis Method f roalysis Date Lab comment
SM3113B 07/08/2016Code Description Restilt Units LOD Report Lirliil LOQ1025 CADMIUMDISS 0.0711 ugth 0.0500 0.150
4nalysis Method Analysis Date Lab comment
SM3113B 07/05/2016:ode Description Resull Units LOD Report Liinit LOQ1049 LEADDISS ND ug/L 1.00 3.00
nalysis Method Analysis Date Lab coriiment
SM2540C 07/05/2016Code Description Resiilt Units LOD Report Liniit LOQ70300 RESIDUE DISs l80C (TOTAL 380 MGth 50.0 50.0
DISSOLVED SOLDS)
Analysis Method Analysis Date Lab comment
EPA 375.2 07/21/2016Code Description Result Units LOD Report Linlil LOQ946 SULFATE DISS 107 MGth 23.5 75.0
Co7#/tge7!f.. MATRIX SPIKE QC EXCEEDED.