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FINAL

WASTE EXCAVATION PLAN

FTB-014 (SWMU-25) ORO GRANDE LANDFILL

FORT BLISS, NEW MEXICO

Contract Number W91ZLK-13-0003 Task Order Number 0003

Prepared for:

DEPARTMENT OF THE ARMY

U.S. ARMY ENVIRONMENTAL COMMAND 2450 Connell Road

Fort Sam Houston, TX 78234

and DEPARTMENT OF THE ARMY

Headquarters, U.S. Army Garrison Command 1741 Marshall Road Ft. Bliss, TX 79916

Prepared by:

404 E. Ramsey, Suite 206 San Antonio, TX 78216

CAPE Project Number 21003.003

Revision Number: Rev 0

October 2018

Waste Excavation Plan CAPE Oro Grande Landfill i October 2018 Fort Bliss Texas/New Mexico

TABLE OF CONTENTS Section Page

LIST OF ABBREVIATIONS AND ACRONYMS ...................................................................... iii

1.0 INTRODUCTION ...............................................................................................................1

1.1 Corrective Measures Objectives and Scope .........................................................................1

1.2 Regulatory Requirements.....................................................................................................1

1.3 Site Description and Operational History ............................................................................2

1.4 Previous Investigations ........................................................................................................2

1.4.1 RFI Soil Sampling Results .......................................................................................4

2.0 SITE CONDITIONS ............................................................................................................7

2.1 Site Geology.........................................................................................................................7

2.2 Site Hydrology .....................................................................................................................7

2.3 Contaminants of Concern ....................................................................................................7

3.0 SITE ACTIVITIES/ METHODS .......................................................................................10

3.1 Excavation Layout .............................................................................................................10

3.2 Excavation..........................................................................................................................10

3.3 Transport and Disposal ......................................................................................................11

3.4 Backfill ...............................................................................................................................12

3.5 Site Security .......................................................................................................................12

3.6 Construction Safety ............................................................................................................12

4.0 SAMPLING AND ANALYSIS .........................................................................................15

4.1 Waste Characterization Sampling ......................................................................................15

4.2 Confirmation Sampling ......................................................................................................16

4.3 Backfill Sampling ..............................................................................................................17

5.0 REFERENCES ..................................................................................................................18

Waste Excavation Plan CAPE Oro Grande Landfill ii October 2018 Fort Bliss Texas/New Mexico

TABLE OF CONTENTS

Section

FIGURES

1 Fort Bliss Site Location Map

2 Landfill Site Location

3 Soil Boring and Trench Locations

4 Haul Route Map

5 Waste Characterization Sampling Locations

6 Confirmation Sampling Locations

APPENDICES

A NMED Approval Letters

B RFI Soil Bearing Logs

C RFI Analytical Results Summary

D Sampling and Analysis Plan Addendum

E Waste Characterization Sampling Analytical Results

F Project Schedule

G Waste Acceptance Letter from Otero-Greentree Landfill

H Emergency Contact List

I Emergency Hospital Route Map

J Transporter Approval Letter

Waste Excavation Plan CAPE Oro Grande Landfill iii October 2018 Fort Bliss Texas/New Mexico

LIST OF ABBREVIATIONS AND ACRONYMS

ACM asbestos containing materials bgs below ground surface CAPE Cape Environmental Management Inc COC Contaminant of Concern CSP Certified Safety Professional CY Cubic Yard USEPA U.S. Environmental Protection Agency FTBL Fort Bliss Site H&S Health and Safety IAW in accordance with NMAC New Mexico Administrative Code NMED ̀ New Mexico Environment Department NMAC New Mexico Administrative Code NORM Naturally Occurring Radioactive Material OSHA Occupational Safety and Health Administration PCBs poly-chlorinated biphenyls PPE personal protective equipment RCRA Resource Conservation and Recovery Act RFI RCRA Facility Investigation SAP Sampling and Analysis Plan SSHO Site Safety & Health Officer SSHP Site Safety and Health Plan SSL Soil Screening Level SVOCs Semivolatile Organic Compounds TO Task Order TPH Total Petroleum Hydrocarbons USAEC United States Army Environmental Command VOCs Volatile Organic Compounds WEP Waste Excavation Plan

Waste Excavation Plan CAPE Oro Grande Landfill 1 October 2018 Fort Bliss New Mexico

1.0 INTRODUCTION

This Waste Excavation Plan (WEP) describes the proposed waste management activities for the Oro Grande Landfill, also designated as Solid Waste Management Unit (SWMU) 25 and Fort Bliss Site 14 (FTBL-14). Cape Environmental Management Inc (CAPE) will perform this work for the United States Army Environmental Command (USAEC) under Contract Number W91ZLK-13-003.

1.1 Corrective Measures Objectives and Scope

The Final Letter Report for the Cover and Borrow Area Investigation of the Oro Grande Landfill dated November 21, 2011 (Malcolm Pirnie, 2011), concluded that the best remedial options for the site were removing and disposing of all of the waste from SWMU-25/FTBL-014 in a permitted municipal landfill, or covering the landfill with an evapotranspiration cap. The report was submitted to the New Mexico Environment Department (NMED) with a cover letter dated September 6, 2013, that recommended the waste removal alternative. NMED concurred with the waste removal alternative in a letter dated June 26, 2014. The letter is attached in Appendix A.

The scope of this corrective action is to remove all of the buried waste material from the site, dispose of the waste at a permitted landfill, confirm the absence of contamination from the waste, restore the landfill area to its previous grade, and re-vegetate the restored surface.

The scope of this WEP is to assure the proper management of the waste removal and disposition of the excavated waste, and protection of site personnel and the public. Waste characterization samples were collected in July 2017, as discussed in Section 4. NMED approved this WEP in a letter dated October 25, 2018, attached in Appendix A.

1.2 Regulatory Requirements

These activities will be performed in accordance with the requirements of the federal Resource Conservation and Recovery Act (RCRA), the solid and hazardous waste rules included in the New Mexico Administrative Code (NMAC), and RCRA Corrective Action Permit #NM4213720101-01, issued by the NMED Hazardous Waste Bureau.

Work will also be performed in accordance with the approved Corrective Action Work Plan for the Oro Grande Landfill (CAPE, 2015). The Work Plan was submitted to NMED in December 2015. NMED approved the Corrective Action Work Plan with modifications (additional confirmation samples requested) in a letter dated May 13, 2016 (NMED, 2016).


1.3 Site Description and Operational History

The landfill is located in a remote area of Fort Bliss at the southwest edge of Elephant Mountain in the Tularosa Basin of New Mexico, as seen on Figures 1 and 2. Placement of waste material in the landfill area spanned a 30-year period, from 1964 until 1994. The Oro Grande site is a trench-type landfill.

The Oro Grande Landfill is situated at an approximate elevation of 4,240 feet above mean sea level. The terrain around the landfill generally slopes to the southwest. Arroyos are located east and west of the landfill. The arroyos appear to have been naturally formed by the surface runoff from infrequent rainfall events.

The soil type at the landfill is designated Pendero fine sand. The Pendero series is described as a reddish-brown loamy fine sand and is eolian in origin. The soil is described as having 2 percent to 5 percent slopes. Pendero soils are excessively drained and have low water capacity. Pendero fine sand contains 5 percent calcium carbonate and is considered moderately alkaline. The soil is typically 80 inches thick. Pendero fine sand can support desert shrub type vegetation and is generally used for livestock grazing.

The land for the Oro Grande Range Camp was acquired sometime after 1938, due to the increased use of anti-aircraft weapons and training programs. In 1949, Oro Grande Range Camp facilities consisted of a salt water well and cistern, a septic tank for sewage with capacity for a population of 2,000 troops, an evaporation pool, 10 mess halls, 10 latrine buildings, 20 accessory buildings, and tents for troops. In 1950, the range camp added a post-exchange building, three range buildings, a caretaker’s quarters, two storehouses, and a classroom. In 1962, the original buildings were demolished and new semi-permanent masonry or sheet metal buildings were constructed to accommodate approximately 1,000 troops. Water for the newly constructed site was provided via pipeline from the White Sands Missile Range.

Operations at the Oro Grande Landfill began about 1964, and the landfill was closed in 1994. The contents of the landfill occasionally were burned. The landfill was excavated out of native soil, unlined, and capped with native soil. The landfill was described as consisting of a hard-packed clay caliche pit and rock walls with a hard-packed clay and sand floor. No hazardous wastes or unexploded ordnance (UXO) was reported to have been disposed of at the Oro Grande Landfill (Malcolm Pirnie, 2009).

1.4 Previous Investigations

The Thompson Professional Group (TPG) investigated the Oro Grande landfill (SWMU 25) in 1996. A geophysical survey was performed, using frequency-domain electromagnetic, magnetometry, and ground penetrating radar techniques followed by excavation of an exploratory trench. TPG identified the following contents at the Oro Grande Landfill based on trenching activities: field communications wire, construction


materials, plastic sheeting and garbage bags, plant debris, asphalt, tar paper, metal items, a toilet, and household refuse.

Three soil borings were installed, and seven soil samples were collected from each boring, from approximately one to 50 feet bgs. Samples were analyzed for volatile organic compounds (VOCs), semi-volatile organic compounds (SVOCs), poly-chlorinated biphenyls (PCBs), pesticides and metals. Metals arsenic, barium, chromium and lead were detected in multiple samples, while VOCs, SVOCs, PCBs, and pesticides were not detected. Arsenic, barium chromium and lead were detected as high as 4.81 milligram per kilogram (mg/kg), 176 mg/kg, 13.3 mg/kg and 5.9 mg/kg, respectively, all below background concentrations for the respective metals (TPG, 1997). Four soil gas probes were also installed, and field soil gas readings were collected. Photoionization detector (PID) readings ranged from 0.2 to 7.1 ppm.

A RCRA Facility Investigation (RFI) Report prepared for the landfill provides waste composition information, including chemical data. The landfill was previously described as consisting of a hard-packed clay caliche pit and rock walls with a hard-packed clay and sand floor (Wagner, 2000). Cover material observed in the exploratory trenches consists of poorly-graded sand with clay, silty sand, and clayey sand with a thickness ranging from 1 to 10 feet with an average thickness of approximately 4.6 feet.

During the RFI, the landfill extents were delineated with trenches, and 21 soil samples were collected. Wood, plastics, building materials, and glass were found in the trenches. Based on the RFI Report, the extent of the buried waste is approximately 345 feet by 37 feet (0.29 acres), and averages 2.8 feet thick but varies up to about 7 feet thick. The soil cover averages 4.6 feet thick and varies from 1 to 10 feet thick, and the bottom of the debris layer is approximately 12 to 14 feet below ground surface (bgs). The RFI Report estimates the quantity of debris as 2,300 cubic yards (CY). This quantity was further refined to 2,075 CY based upon findings from subsequent additional test pits, as documented in the Final Letter Report for the Cover and Borrow Area Investigation (Malcolm Pirnie, 2011).

The RFI Report noted that tar material was disposed of on the ground surface in an arroyo to the west of the landfill. Over time, the tar disintegrated into small pieces, which were dispersed in the arroyo during storm events. Fort Bliss conducted removal activities related to the dispersed tar in 2004 and disposed of the material in a permitted landfill (Malcolm Pirnie, 2009).

During the RFI investigation, eight soil borings were installed with a hollow-stem auger rig, following trenching activities, to identify the extent of buried waste. One deep soil boring (F14-SB-6) was installed to 115 feet bgs, and two borings were installed to 30 feet bgs. Three soil borings were installed at a 30- degree angle at locations 7.5 feet outside the extent of waste as defined by the exploratory trenching.


Two soil borings were installed to 10 feet bgs in the northern and southern portions of the former tar material area. Soil samples were collected in the 0 to 1 ft interval to determine if COCs in the surface soils exceeded SSLs-Residential. Small fragments of tar ranging from gravel to cobble size were observed scattered across the surface of the former tar material area. Tar fragments were not observed in the soil borings advanced in this area.

During hollow-stem auger drilling, soil coring was conducted continuously from ground surface to total depth using a 5-foot barrel split spoon sampler. Soil cores were inspected in the field for soil classification, color, texture, moisture content, and any other pertinent observations (e.g., evidence of staining). Each five-foot soil core was screened with a PID. A composite sample of each five-foot soil core was placed in separate plastic sealable bags and any volatile organic compounds (VOCs) were allowed to equilibrate for headspace screening. The RFI boring logs are presented in Appendix B. 21 soil samples were also collected.

1.4.1 RFI Soil Sampling Results

Soil borings for the RFI investigation observed wastes including concrete, glass, wiring, roofing materials, plastics, sandbags, paper, caulking tubes, trash bags, strapping material, glass bottles, wiring, a tire, household trash, spray can, oil absorbent rags, truck axle, metal, sheetrock, duct tape, Styrofoam, plastic netting, concrete and asphalt debris, concrete rubble, razor wire, and wood. Wastes were generally distributed across the former landfill.

The summary of analytical results from the RFI soil sampling is attached in Appendix C, and included:

Volatile Organic Compounds (VOCs)

• Dichloromethane (methylene chloride) was detected below the NMED SSL-Residential standard of 182 mg/kg in twelve soil samples, from 0.0038 mg/kg to 0.0062 mg/kg. No other VOCs were detected.

Semivolatile Organic Compounds (SVOCs)

• Benzo(k)fluoranthene was detected below the NMED SSL-Residential concentration of 62.1 mg/kg in one sample, at 0.0066 mg/kg.

• Bis (2-ethylhexyl) phthalate was detected below the NMED SSL-Residential standard of 347 mg/kg in 10 soil samples, from 0.0015 mg/kg to 0.019 mg/kg.

• Caprolactum was detected in three soil samples ranging from 0.015 mg/kg to 0.12 mg/kg. An NMED SSL-Residential concentration has not been established for caprolactum.

• Chrysene was detected below the NMED SSL-Residential standard of 615 mg/kg in one soil sample, at 0.0067 mg/kg.


• Di-butyl phthalate was detected below the NMED SSL-Residential level of 6,110 mg/kg in 10 soil samples, from 0.0012 mg/kg to 0.015 mg/kg.

• Organochlorine pesticides, chlorinated herbicides and PCBs were not detected.

Total Petroleum Hydrocarbons (TPH)

• Diesel range TPH was detected below the NMED SSL-Residential concentration of 200 mg/kg in three samples, including one detection at the former tar pit area outside the landfill limits, from 0.51 mg/kg to 1.6 mg/kg.

Inorganic Chemicals

• Arsenic was detected in soil sample F14-SB-5 at 4.01 mg/kg, just above the NMED SSL-Residential concentration of 3.9 mg/kg. Although above the U.S. Environmental Protection Agency (USEPA) Region 6 Residential SL level of 0.39 mg/kg, the arsenic detection was below the USEPA Region 6 background range for arsenic of 1.1 to 16.7 mg/kg. The sample was collected from 28-30 feet bgs, well below the observed wastes and well below the projected excavation depth. Arsenic was considered to be the result of naturally occurring conditions, and not due to a release from the landfill. Arsenic was detected in all other samples collected from the site, all at concentrations below the NMED SSL-Residential standard and the USEPA Region 6 background concentration.

• Antimony, iron, molybdenum, strontium, thallium, and tin were detected below NMED SSLs-Residential standards.

• Calcium, lithium, magnesium, phosphorus, potassium, silica, sodium, and titanium were detected; however, NMED SSLs-Residential concentrations have not been established for these chemicals.

The RFI conclusions included:

• Buried wastes observed at the Oro Grande Landfill consisted of concrete, glass, building materials, plastic, wiring, packaging materials, and demolition debris. The estimated volume of the buried waste is approximately 2,300 CY, based on the observed average thickness of 2.8 feet.

• No evidence was found of a release of contaminants of concern (COCs) from the buried wastes. The single detection of a COC above NMED soil screening level (SSL)-Residential values was arsenic at 4.01 mg/kg, below published USEPA Region 6 background concentrations.

• Native materials below the buried wastes consist of sand with gravel and layers of caliche to approximately 30 feet below ground surface (bgs), and silty sand to 116 feet bgs.


• No completed exposure pathways to potential human or ecological receptors were identified, because no releases of COCs were observed.

• The Army and NMED agreed that the best option for the wastes was removal and disposal at a permitted municipal solid waste landfill.


2.0 SITE CONDITIONS

The following subsections are presented to characterize the site.

2.1 Site Geology

Otero County, New Mexico is considered the easternmost edge of the Basin and Range province (O’Neill, 1998). Geologically, the Fort Bliss Military Reservation is located within the Tularosa Basin and Hueco Bolson of the New Mexico Highland section of the Basin and Range province. A groundwater divide separates the two basins hydrogeologically. The Sacramento and Hueco Mountains lie to the east of the basins and the San Andres-Organ-Franklin Mountain chain lies to the west. The Oro Grande Landfill is situated at the southwest edge of Elephant Mountain at an approximate elevation of 4,240 feet above mean sea level.

The terrain around the landfill generally slopes to the southwest. Arroyos are located east and west of the landfill. The soil type at the landfill is designated Pendero fine sand. The Pendero series is described as reddish brown loamy fine sand and is eolian in origin.

Subsurface soils in this portion of the basin are dry unconsolidated basin fill deposits of fine-grained sand, silt, caliches, and clays. Based on the RFI, the landfill area cross-section consists of about 20 feet (depth) of sandy/gravelly soil overlying a layer caliche about 2 feet thick. It appears that the landfill debris trench is completely contained in this upper layer of sandy soil above the caliche layer. Below the caliche is a layer of sand and gravel extending to a depth of about 30 feet bgs, where there is another layer of caliche. The second layer of caliche is approximately 4 feet thick. Below the second layer of caliche is silty sand to a considerable depth (Malcolm Pirnie, 2009).

2.2 Site Hydrology

Groundwater is estimated to be at a depth between 250 and 500 feet bgs at this site. The water column in Otero County varies from 20 to 500 feet thick, but averages less than 100 feet in thickness.

The groundwater quality in the regional aquifer is reported to be non-potable due to high total dissolved solids. Groundwater is not used at the Oro Grande Camp for drinking water, as drinking water is piped in from the White Sands Missile Range. No groundwater was encountered in any of the geotechnical borings made for the RFI, and no groundwater is expected to be encountered during waste removal.

2.3 Contaminants of Concern

Soil

Only one minor exceedances of arsenic above NMED SSL-Residential values was detected during the RFI. However, if suspected contamination is discovered during


excavation, the waste will be segregated and fully characterized in accordance with the procedures included in the Sampling and Analysis Plan (SAP), submitted as Appendix B of the Corrective Action Work Plan (CAPE, 2015), and approved by NMED (NMED, 2016).

Waste characterization samples were collected in accordance with Section 4, and the Sampling and Analysis Plan Addendum in Appendix D. Waste characterization sampling analytical results are attached in Appendix E.

Since the purpose of this task is to remove waste debris and replace that volume of waste with clean soil, no potential for exposure to hazardous substances will remain.

Groundwater

Groundwater is thought to be at a depth of more than 250 feet bgs (Malcolm Pirnie, 2009). Groundwater quality in the regional aquifer is reported to be non-potable, due to high total dissolved solids. Drinking water at the nearby Oro Grande Range Camp is piped in from the White Sands Missile Range Headquarters. No water sources are near the Oro Grande Landfill site (Malcolm Pirnie, 2009).

Surface Water

Surface water is not an issue at this site with the exception of the arroyos that flow intermittently as a result of heavy rainfall events. Due to the sandy nature of the site soils, rainwater tends to soak into the ground quickly and not pond. Stormwater will be diverted by silt logs or berms to prevent runoff from flowing into the excavation. Silt fencing will be installed downgradient of the excavation to prevent excavated soil from leaving the site. Any stormwater that enters the excavation will be collected and characterized for disposal.

Direct Contact

Based on site historical information and previous RI soil sampling results, soil characterization sampling and excavation during this project is not anticipated to present a human health occupational exposure inhalation risk. It is anticipated that there will be a minor potential for dermal exposure to low level contamination of soil during excavation and loading of soil into containers for waste transportation and disposal. Water spray will be used to control generation of airborne dust. Personnel will not be directly handling contaminated soil. Modified Level D protection will be used as a precautionary measure during these activities. Decontamination procedures will be implemented so there will be minimal potential for skin contact. No eating, drinking or smoking will be allowed in the exclusion zone and decontamination procedures will be implemented so the potential for ingestion of contaminated soil is minimal. There is no documented contamination of soil above regulatory industrial or residential human health risk criteria within the site excavation boundary.


Air and Subsurface Gas

There is a remote possibility that landfill gases (e.g., methane, hydrogen sulfide) may be encountered during excavation and loading of contaminated soil. Contaminant concentrations are anticipated to be very low and the likelihood of significant airborne contaminant exposure is unlikely. If there is a site condition or work scope change that has the potential to expose workers to harmful concentrations of airborne contaminants or dust, work activities will cease and exposure monitoring requirements will be re-evaluated. In addition, if unusual odors or respiratory irritation is noticed, the work will cease and site personnel will remove themselves from the area, and contact the PM and SSHO to evaluate.

PID monitoring for VOCs will be conducted for operations where the presence of VOCs is likely to occur. If VOCs are detected or suspected to be present in an area, sampling of the work area and breathing zone of workers is conducted periodically during work. VOC measurements that are below 5 parts per million (ppm) will be considered acceptable for Level D protection work. If VOCs exceed 5 ppm, but are less than 50 ppm, the SSHO will implement requirements for use of engineering controls, safe work practices, and respiratory protection. If VOC concentrations in the workers breathing zone are between 5 ppm and 50 ppm, sustained over a 15-minute period, the SSHO will require Level C protection to be used. If VOC concentrations in the workers breathing zone are greater than 50 ppm, work will be stopped and the SSHO will evaluate.

It is not expected that air monitoring will be necessary to determine personnel exposures to chemical contaminants and/or physical agents for the project scope of work. However, periodic air monitoring for combustible gases (i.e., methane), oxygen, hydrogen sulfide and volatile organic compounds will be conducted to document a negative exposure during project work. If suspected air contaminants are encountered, the PM, SSHO and SHM will be contacted for further instructions including establishing site action level concentrations. It is generally recognized that dust is visible in the 2 to 3 mg/m3 range, it is expected that use of a “no visible dust” action level and water spray for dust control should be sufficient to keep airborne particulate exposures to a minimum. Airborne dust monitoring will be conducted to document a negative exposure assessment.

The SSHO or designee completes air monitoring. Should action level concentrations be exceeded, response actions will be initiated to implement engineering controls, safe work practices, upgrade or downgrade in PPE, work stoppage, emergency evacuation, and notification and evaluation by the PM and SSHO. The SSHO is responsible for maintaining copies of applicable monitoring records at the site for the duration of the project. The SSHO notifies site personnel of air monitoring results through correspondence or posting of information. See the project Site Safety and Health Plan for additional information regarding project occupational exposure monitoring.


3.0 SITE ACTIVITIES/ METHODS

CAPE will mobilize to the Oro Grande landfill site after NMED approves the Waste Excavation Plan. Staging areas and stockpile areas will be delineated. CAPE will mobilize personnel, equipment (e.g. excavator, loader, dozer, trucking), and construction support facilities to the site. CAPE will also install erosion controls.

Approximately 15 working days are anticipated to complete the excavation of the Oro Grande Landfill, and transport the wastes for disposal. Excavation and soil loading activities will be halted if winds are in excess of 30 miles per hour. The project schedule is shown in Appendix F.

3.1 Excavation Layout

The landfill area is marked with stakes set by a surveyor in February 2017. Existing stakes will be used as starting points for the excavation.

3.2 Excavation

The landfill area will be cleared and grubbed as needed. Brush was cut and removed in early February 2017. Clean cover soil (overburden) will be visually segregated, excavated and stockpiled on site for reuse as backfill. Stockpiles will be covered with polyethylene sheeting. The excavation area will be wetted with the water truck to control dust.

All excavation will be performed in strict accordance with Occupational Safety and Health Administration (OSHA) excavation safety requirements. Excavation safety will be implemented as described in Section 3.6. Cover material (clean overburden) observed in the exploratory trenches consists of poorly-graded sand with clay, silty sand, and clayey sand with a thickness ranging from 1 to 10 feet with an average thickness of approximately 4.6 feet (Malcolm Pirnie, 2009). The sides of the excavation will be benched or sloped appropriately to ensure stability. The soil at this site is anticipated to be OSHA Type C. As debris removal continues, the sidewalls will be laid back to a maximum allowable slope of 1.5:1 (H:V) or flatter. Personnel will not enter an excavation that is not properly sloped or benched. Water will be applied for dust control as needed to minimize airborne dust during heavy equipment operation.

Heavy equipment used to complete the excavation/backfill activities will include a John Deere 220 excavator, a John Deere 650 dozer, and a John Deere 544 loader (or similar equipment). A water truck will be used to control dust and to moisture-condition the backfill material as necessary.

Soil borings observed various wastes generally distributed across the former landfill, as discussed in Section 1.4. Based on the results of the RFI investigation, CAPE plans on treating the waste volume as one decision unit and does not plan on segregating the waste.


Waste materials will be excavated using an excavator and/or a loader and directly loaded in dump trucks for disposal. The excavation area will be wetted with the water truck to control dust, which will be monitored visually. The landfill waste material is classified as non-hazardous waste, based on results of the waste characterization sampling. Wastes will be screened with a PID if needed; however, based on the results of the waste characterization sampling, volatile organic wastes are not anticipated. If any of the waste appears to be from a different source or is observed to have different waste characteristics, it will be segregated and characterized separately.

Analytical results for waste characterization samples T030GL-WC06 (508 mg/kg) and T030GL-WC20 (120 mg/kg) exceeded the disposal criteria of 100 mg/kg and are thus considered Petroleum Contaminated Soil (PCS), as discussed in Section 4.1. Soil from these two areas, shown on Figure 5, will be excavated separately and segregated for transport and disposal as discussed in Section 3.3.

3.3 Transport and Disposal

Loads will be covered with tarps prior to removal from the site. Gross soil, debris, etc., will be swept from external parts of the trucks before they are allowed to enter roadways. Excavated waste materials and any incidental investigation derived waste (IDW) will be disposed at the Otero-Greentree Regional Landfill. A waste acceptance letter from the Otero-Greentree Landfill is included in Attachment G.

All waste material is characterized as non-hazardous waste, based on the waste characterization sampling results presented herein. Henry Trujillo, Inc, of El Paso, Texas will be used to transport soil and waste material and to haul clean backfill into the excavation site. Henry Trujillo, Inc. is licensed to transport municipal solid waste, construction and demolition debris and petroleum contaminated soils. The NMED approval letter is provided in Attachment J.

The waste material will be hauled to the Otero-Greentree Regional Landfill for disposal. Site access will utilize the existing dirt road to minimize disturbance. The roadway to the site will be graded, filled and/or stabilized as needed to allow truck access. Truck traffic within the project area will be routed in a controlled manner in order to avoid confusion and potential accidents during the excavation activities (Figure 4). All waste material and debris will be removed. Confirmation samples will be collected to confirm that contaminants have been removed.

Soil from the areas around samples T030GL-WC06 (508 mg/kg) and T030GL-WC20 (120 mg/kg) will be excavated separately and segregated. This soil will be transported separately and disposed at the Otero Greentree Landfill or alternate disposal facility as PCS special waste. The landfill will be notified in advance when these wastes will be transported and the TPH concentrations.


If any excavated material is suspected to contain hazardous substances, it will be segregated, properly characterized in accordance with Title 40 of the Code of Federal Regulations (40 CFR), Part 261, Subpart C, and managed in accordance with its waste determination. If hazardous waste is identified, it will be properly contained and properly disposed at a hazardous waste facility meeting the requirements of 40 CFR Part 268, Land Disposal Restrictions. If asbestos containing materials (ACM) are encountered, CAPE will subcontract a licensed company to handle ACM in accordance with (IAW) appropriate guidelines, and will dispose of them at a licensed disposal facility.

Investigative Derived Waste (IDW), (i.e., used personal protective equipment, expendable sampling equipment, plastic used to cover any waste or stockpiled materials) will be bagged and disposed, pending disposal clearance. Any non-disposable sampling equipment and excavation tools used during site activities will be decontaminated using techniques that minimize the generation of IDW. The IDW will be free of loose soil, and CAPE will discuss the acceptance criteria with the landfill prior to sending them any IDW. Any decontamination water will be sampled and characterized, and disposed at the Fort Bliss Wastewater Treatment Plant.

3.4 Backfill

Backfill material will be obtained from a Fort Bliss borrow sources. One sample will be collected for every 500 CY of backfill material and analyzed in accordance with the SAP to ensure that free of contamination prior to excavation. When approved, the backfill materials will be excavated and transported to the Oro Grande Landfill site.

Backfill of sandy fill material will be placed in 8- to 12-inch lifts and will be compacted by tracked machinery until surface defection are less than 4 inches, achieving compaction of 80 – 90 percent. Backfill compaction will be overseen by the Site Superintendent and documented by a geotechnical field technician. Since the backfill material is generally sandy, it is anticipated that compaction can be achieved using the dozer and loader. If not, lift thickness will be reduced.

3.5 Site Security

While the excavation is open during operations, and pending confirmation analytical results, construction fencing will be placed around the excavation to keep people and animals out of the area and signage (e.g. Construction Area - Keep Out) will be attached to the fencing. Signage in both Spanish and English will be posted.

3.6 Construction Safety

All personnel working on site will adhere to construction safety procedures as specified in the separate Site Safety and Health Plan (SSHP), submitted as Appendix C of the Corrective Action Work Plan (CAPE, 2015). The SSHP presents the contractor Health


and Safety (H&S) procedures to be implemented by CAPE in the execution of this project. The SSHP has been prepared to meet the requirements of OSHA standards, 29 CFR Part 1910 and 29 CFR Part 1926; USACE Safety and Health Requirements Manual (EM 385-1-1). The SSHP will be kept on site during the execution of all project activities and will be readily available to all on-site personnel. The Emergency Contact list is attached in Appendix H and the hospital route is shown in Appendix I.

Level D and Modified-Level D personal protection will be used during site work activities. Personal protective equipment (PPE) will include disposable coveralls for dust exposure, polyethylene Tyvek® for incidental splash protection, steel-toed/shank boots, gloves, hard hat, safety glasses with side shields, goggles (for liquid splash hazards), face shields (polycarbonate for pressure washing), ear plugs, respirators, and high-visibility safety vests with reflective striping.

The Site Safety and Health Officer (SSHO) will inspect excavation benches and/or slopes daily to monitor slope stability. Instability may be noted by cracks in the ground surface within a few feet of the excavation wall, sloughing material into the excavation, or water seeping into the excavation from the wall. If potential slope instability is noted, the affected areas will be corrected by additional sloping or benching.

In the event of a construction emergency (e.g. fire, earthwork failure, etc.), the Army will be orally notified immediately, followed by notification in writing within 72 hours of the event. CAPE will support the Army, which will initiate any other notifications to OSHA, USEPA, or NMED, as appropriate, within 24 hours. Written notifications will specify what happened, what response action is being taken and/or is planned, and any potential impacts on human health and/or the environment. The CAPE incident response process and report forms are included in the SSHP.

Only experienced personnel will operate excavation equipment on site. Heavy equipment operation safety procedures and precautions include conduct daily operator inspections of heavy equipment for safe operating condition. Excavation work areas will be properly marked and guarded with barriers and/or caution tape to prevent unauthorized personnel entry and to prevent personnel from falling into open holes. Training will be provided to site personnel during the site safety orientation briefing and daily safety meetings on heavy equipment hazards and heavy equipment procedures.

Excavation and trenching activities must comply with OSHA excavation requirements. Compliance with these requirements must be maintained when installing trenches 4 feet or more in depth and/or excavations 5 feet or more in depth into which personnel are required to descend. Use of protective systems such as shoring, sloping, benching, or shielding, is required for personnel entry into trenches 4 feet or more in depth and/or excavations 5 feet or more in depth.


Miscellaneous physical hazards and safety procedures to be followed are reviewed with personnel in safety meetings and may include discussion of the following topics:

Poor housekeeping Sharp objects Uneven walking surfaces Slippery work surfaces Tripping hazards Fall hazards

Biological hazards that may potentially be encountered during site work include:

Poisonous plants Venomous spiders Poisonous snakes (rattlesnakes) Rodents Insects


4.0 SAMPLING AND ANALYSIS

The sampling and analysis associated with this task includes waste characterization, analysis of stockpiled overburden soil from the excavation that will be used as backfill, analysis of borrow source soil, and confirmation sampling from the sidewalls and floor of the excavation to verify that the site is cleaned up to NMED SSL-Residential screening levels prior to backfilling. Sampling and analysis will be performed in accordance with the separate SAP, submitted to NMED as Appendix B of the approved Corrective Action Work Plan (CAPE, 2015).

4.1 Waste Characterization Sampling

Waste characterization sampling was conducted from July 24 through July 26 2017, to properly characterize the wastes for disposal. Waste characterization samples were collected at the rate of one sample per 100 CY of waste, as requested by the Otero-Greentree Landfill. Twenty-three waste characterization samples were collected from in-situ wastes to evaluate the disposal requirements for the wastes, as shown on Figure 5. Samples were collected with a hollow-stem auger drilling rig, to 16 feet bgs or to the bottom of wastes.

CAPE collected 23 samples of debris and any potentially impacted soil and analyzed for Toxicity Characteristic Leaching Procedure (TCLP) analysis for VOCs, SVOCs, metals, pesticides and herbicides. Wastes were also analyzed for PCBs, TPH, asbestos, ignitability, corrosivity and reactivity. Three waste characterization samples were also analyzed for radioisotope assay for strontium, gross alpha and beta, as strontium was detected in the 2009 RFI sampling results. Waste characterization sampling was performed as detailed in the Sampling and Analysis Plan Addendum in Appendix D.

The summary of analytical results from the waste characterization sampling is attached in Appendix E. Results included:

TCLP VOCs

• Benzene was detected in 6 of 23 soil samples, from 0.0104 mg/L to 0.446 mg/L.

• Chlorobenzene was detected in 1 of 23 soil samples at 0.0020 mg/L.

• Chloroform was detected in 8 of 23 soil samples, from 0.0031 mg/L to 0.0053 mg/L.

• Tetrachloroethylene was detected in 2 of 23 soil samples, from 0.0299 mg/L to 0.0346 mg/L.

• Trichloroethylene was detected in 2 of 23 soil samples, from 0.0057 mg/L to 0.0066 mg/L.

TCLP SVOCs

• No SVOCs were detected.


Total Petroleum Hydrocarbons (TPH)

• TPH diesel range organics (TPH-DRO) was detected in all 23 soil samples, from 3.19 mg/Kg to 508 mg/Kg. Analytical results for samples T030GL-WC06 and T030GL-WC20 (508 mg/kg and 120 mg/kg respectively) exceeded the disposal criteria of 100 mg/kg and are thus considered Petroleum Contaminated Soil (PCS) as discussed in Section 3.3. All other analytical results for TPH-DRO were less than 100 mg/kg. Soil sampling locations are shown on Figure 5.

TCLP Herbicides and TCLP Pesticides

• No herbicides or pesticides were detected.

Polychlorinated Biphenyls (PCBs)

• PCBs were detected in 6 of 23 soil samples, from 9.5 microgram per kilogram (µg/kg) to 105 µg/kg.

TCLP Metals

• Barium was detected in 17 of 23 soil samples, from 0.28 mg/L to 0.81 mg/L.

• Cadmium was detected in 10 of 23 soil samples, from 0.0020 mg/L to 0.014 mg/L.

• Chromium was detected in 1 of 23 soil sample at 0.012 mg/L.

• Lead was detected in 4 of 23 soil samples, from 0.013 mg/L to 0.77 mg/L.

• Silver was detected in 3 of 23 soil samples, will all three detections at 0.0080 mg/L.

Radioisotope Assay

• Strontium was not detected in any of the three samples in which it was analyzed.

• Gross alpha was detected at all three soil samples, from 10.5 picocuries per gram (pCi/g) to 16.4 pCi/g. These levels are consistent with Naturally Occurring Radioactive Material (NORM) in site soil.

• Gross beta was detected at all three soil samples, from 21.3 pCi/g to 24.1 pCi/g. The highest gross alpha or beta value of 24 pCi/g is below the lowest regulated level of 30 pCi/g above background (NMAC 20.3.14). Thus, gross alpha and beta levels do not indicate this waste as regulated NORM waste.

4.2 Confirmation Sampling

Confirmation sampling will be performed to verify that all of the waste material has been removed from the site and no COCs are above NMED SSL-Residential screening levels.


16 samples will be collected from the sidewalls and six samples will be collected from the excavation bottom, as discussed in the SAP and shown on Figure 6.

4.3 Backfill Sampling

Samples will be collected from Fort Bliss backfill sources to ensure that backfill material is clean. Samples will be collected at a rate of one sample result per 500 CY, prior to excavation of waste material.


5.0 REFERENCES

CAPE, 2015. Corrective Action Work Plan, FTB-014 (SWMU-25) Oro Grande Landfill. December.

Malcolm Pirnie, 2009. RCRA Facility Investigation Report, Oro Grande Landfill (SWMU 25/FTBL-14). January.

Malcolm Pirnie, 2011. Final Letter Report for the Cover and Borrow Area Investigation of the Oro Grande Landfill. November.

NMED, 2014. Approval, Cover and Borrow Area Investigation of the Oro Grande Landfill. January.

NMED, 2016. Approval with Modifications, Corrective Action Work Plan, FTB-014 (SWMU-25) Oro Grande Landfill, Fort Bliss, New Mexico. May.

J. K. Wagner & Company, 2000. Landfill Usage Archives Search Report on Dona Ana, Oro Grande, and McGregor Range Complex. August.

Waste Excavation Plan CAPE Oro Grande Landfill October 2018 Fort Bliss Texas/New Mexico

FIGURES

Figure 1: Fort Bliss Site Location Map

Figure 2: Landfill Site Location

Figure 3: Soil Boring and Trench Locations

Figure 4: Truck Haul Route

Figure 5: Waste Characterization Sampling Locations

Figure 6: Conformation Sampling Locations

CONTRACT NO: SHEET NUMBER:

REVIEWED BY:

FILE NAME:

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DRAWN BY:

DateNo.

REVISIONS:

PROJECT NAME

SHEET TITLE

DATE:

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RemarksBy Chk

CORRECTIVE ACTION WORK PLAN

FTB-14 (SWMU-25)

OROGRANDE LANDFILL

W91ZLK-13-D0003 21003.003

N

LOCATION MAP

S.USNICK

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C.RIOS

SEPT. 2015

AS SHOWN OG Fig1_Loc Map

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CORRECTIVE ACTION WORK PLANFTB-14 (SWMU-25)

OROGRANDE LANDFILL

W91ZLK-13-D0003 21003.003

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CORRECTIVE ACTION WORK PLAN

FTB-14 (SWMU-25)

OROGRANDE LANDFILL

W91ZLK-13-D0003 21003.003

2790 ft

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Legend

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Waste Characterization

Sample Locations


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OROGRANDE LANDFILL - FTBL 14US DEPARTMENT OF THE ARMY

FORT BLISS, TX

W91ZLK-13-D0003 21003.003

WC14

WC16

WC15WC13

WC23

WC17

WC18

WC20

WC19WC22

WC11

WC9

WC10

WC8

WC6

WC7

WC5

WC2

WC3WC1

WC4

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Estimated Extent of PetroleumContaminated Soil (PCS)

AutoCAD SHX Text

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12037 Starcrest Drive

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US DEPARTMENT OF THE ARMY

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2008 Investigation

Legend

Confirmation Sample Locations

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APPENDIX A

NMED APPROVAL LETTERS

:iNEW MEXICO

ENVIRONMENT DEPARTMENT

Solid Waste BureauSUSANA MARTINEZ 1190 Saint Francis Drive, Room N-2150

Governor P.O. Box 5469

JOHN A. SANCHEZ Santa Fe, New Mexico 8 7502-5469 c BORREGOCt. Governor Telephone: (505) 827-0197 Facsimile: (505) 827-2902 Deputy Secretary

www.env.nm.gov/swb/

Certified Mail — Return Receipt Requested No. 7016 0600 0000 0905 1052

October25, 2018

Sylvia A. Waggoner, ChiefDirectorate of Public Works, Environmental DivisionDepartment of the ArmyUS Army Installation Management CommandHeadquarters, US Army Garrison, Fort Bliss1741 Marshall RoadFort Bliss, Texas 79916

Re: Approval of Waste Excavation Plan — Oro Grande Landfill, October 2018, Fort BlissSite No. 14 (FTBL-014) Solid Waste Management Unit 25 (SWMU-25) Oro GrandeLandfill, Fort Bliss, New Mexico

Dear Ms. Waggoner:

The Solid Waste Bureau (“SWB”), New Mexico Environment Department (“NMED”), hascompleted its review of the updated subject document and accepts the latest red-lined revisionreceived October 5, 2018 from Mr. Merle Miller, of CAPE Environmental Management. TheSWB has determined that the Waste Excavation Plan (“WEP”) meets the requirements of the NewMexico Solid Waste Rules (“SWR”), 20.9.2 — 20.9.10 NMAC, and is hereby approved with thefollowing conditions:

1. The petroleum contaminated soils (“PCS”) identified in the revised figure 5, SampleLocations, shall be managed as a special waste. This shall include segregating from solid wasteexcavated and hauled separately under a special waste manifest by Henry Trujillo Inc., a registeredhauler authorized to transport PC$, to a permitted facility.

2. The Otero/Greentree Regional Landfill is identified as the waste accepting landfillthroughout the WEP; however, they have deferred review and approval of a waste profile for thesubject waste pending the SWB’s approval of the WEP. It is ultimately the facility’s decision toaccept or deny the waste regardless of this WEP approval (the landfill contact, Mr. Lar,y Garner, CityofAlamogordo, has also been copied on this correspondence,).

3. The Otero/Greentree Regional Landfill has notified the SWB that they have suspendedtaking PCS, as of May 2018. The PCS proposed from the waste excavation may require disposal

BUTCH TONGA TECabinet Secretary

Sylvia A. WaggonerPage 2 of 2October 25, 2018

at another permitted facility, unless the Otero/Greentree Regional Landfill agrees to accept thewaste, including the PC$.

For your reference, as an alternative to the Otero/Greentree Regional Landfill, the nearestpermitted facilities to the Fort Bliss location that are authorized to accept PCS for disposal include:

• Corralitos Regional Landfill in Las Cmces [South Central Solid Waste Authority, phone:(575) 528-3800],

• Camino Real Landfill in Sunland Park [Camino Real Environmental Center Inc., phone:(575) 589-9440], or

• Valencia Regional Landfill and Recycling Facility west of Los Lunas [Waste Managementof New Mexico, phone: (505) 917-6232].

Whichever landfill is selected, a waste profile will need to be completed for the PCS. Pleaseinclude the estimated volume of PCS to dispose and the PCS analytical data for their review. Alsoinclude this WEP approval letter to the receiving facility(ies).

4. Please notify the SWB of the selected facility for disposal of the excavated PCS and solidwaste prior to transport.

5. Upon project completion, please send copies of all special waste manifests and disposaltickets to the SWB.

The SWMU permit and its closure requirements are managed by the NMED Hazardous WasteBureau (“HWB”). As a courtesy, Mr. Dave Cobrain, manager of the SWMU permit, has beencopied on this correspondence.

If you have any questions, please call me at (505) 383-2077 or you may reach me via electronicmail at teri.monaghanstate.nm.us.

Sincerely,

74t

Ten D. MonaghanEnforcement Coordinator

cc: Auralie Ashley-Marx, Chief, Solid Waste Bureau [via electronic mail]

Chuck Akeley, Manager, Enforcement Section, Solid Waste Bureau [via electronic mail]

Dave Cobrain, Manager, Hazardous Waste Bureau [via electronic mail]

Merle Miller, P.E., CAPE Environmental Management Inc. [via electronic mail to rnmitler(djcapeInc. corn]

Larry Garner, Public Works Director, Otero/Greentree Regional Landfill [via electronic mail to

lgarnerci. atarnogo rdo. Jun. usJ

Ryan McBee, Enforcement Officer, EA-III, Solid Waste Bureau [via electronic mailj


APPENDIX B

RFI SOIL BORING LOGS

Boring ID: F14-SB-1

BORING LOG

CLIENT USACE - Tulsa District PROJECT # 5285-027

PROJECT FB-14 Oro Grande Landfill DRILLING CONTRACTOR Enviro-Drill

LOCATION Oro Grande, NM DRILLER Mike Stone

START DATE 13-Feb-08 DRILLING METHOD HSA

FINISH DATE 13-Feb-08 HYDROGEOLOGIST C. Melson

DEPTH SAMPLE DESCRIPTION USCS PID NOTES

0-5' Sample F14-SB-1(0-2)

5

5'-30'

10

15 14'-15' - Dense layer of dry compact caliche.

20

25

30

Total Depth = 30.0 ft bgs

All depths are in feet below grade. SHEET 1 OF 1

0.0

0.0

Sample

F14-SB-1(13-15)

Sample

F14-SB-1(28-30)

0.6

0.0

SAND, fine grained, loosely packed, tan/reddish. Gravel sized chalky

caliche and gravel sized rock fragments.

SAND, fine grained tan/reddish, caliche gravel and rock throughout.

Firm, dense, and compact.

SW

0.0

0.0

P:\FORMS.HOU\LOGS\borelog.xls.xls (sb-1)

Boring ID: F14-SB-2

BORING LOG




START DATE 15-Feb-08 DRILLING METHOD HSA 30o

angle



0-5' Sample F14-SB-2(0-2)

5

5'-10'

10

10'-15' SAND, light reddish-tan, fine grained and loosely packed.

15

15'-30'

20

25

30



SAND, light tan, coarse grained with gravel sized rock fragments.

SAND, fine grained, loosely packed, light tan. Gravel sized rock and

root fragments throughout.

SW

0.0

0.0

0.0

0.0

Sample

F14-SB-2(13-15)

Sample

F14-SB-2(28-30)

Note: Drilled 35 linear ft at 30o angle to reach a point approximately 17 ft

beneath the landfill material and approximately 30 ft bgs.

SAND, light reddish-tan, fine grained, with gravel sized chalky caliche

and gravel to cobble sized quartzite rock fragments. Firm, dense, and

compact. Dry.

0.6

0.0


Boring ID: F14-SB-3

BORING LOG





angle



0-5' Sample F14-SB-3(0-2)

5

5'-25'

10

15

17'-20' - Dense layer of compact caliche.

20

25

25'-30'

30



0.0

0.0

0.0



SAND, light reddish-tan, fine grained with gravel to cobble sized rock

fragments mixed throughout. Dry.

SAND, fine grained, loosely packed, tan/reddish. Gravel sized chalky

caliche and gravel sized rock fragments.

SAND, light reddish-tan, gravel sized chalky caliche and rock mixed

throughout. Firm, dense, and compact.

Sample

F14-SB-3(13-15)

Sample

F14-SB-3(28-30)

0.0

0.0

SW

0.0


Boring ID: F14-SB-4

BORING LOG







0-5' Sample F14-SB-4(0-2)

5

5'-10'

10

10'-15'

15

15'-20'

20

20'-25'

25

25'-30'

30



SAND, fine grained, loosely packed, tan/reddish. Chalky caliche and

coarse grained gravel.



SW

0.0

0.5

0.0

0.7



SAND, tan/reddish, loosely packed, with dense white chalky caliche

layer at 17'-20'.

SAND, tan/reddish, loosely packed with gravel sized rock and chalky

caliche gravel. Very dense at 28-30 ft.

SAND, tan/reddish, loosely packed with gravel sized rock and chalky

caliche gravel. Dry.

Sample

F14-SB-4(13-15)

Sample

F14-SB-4(28-30)

0.3

0.0


Boring ID: F14-SB-5

BORING LOG





angle



0-5' Sample F14-SB-5(0-2)

5

5'-15'

10

15

15'-20'

20

20'-30'

25

30



SAND, light tan with chalky white caliche and gravel sized rock

fragments. Compact and firm.

SAND, light reddish-tan with gravel to cobble sized rock fragments anc

chalky caliche fragments. Firm and dense. Dry.

Sample

F14-SB-5(13-15)

Sample

F14-SB-5(28-30)

0.0

1.2

0.0

1.2

0.6

1.2



SAND, coarse grained with gravel, loosely packed, tan/reddish.

SAND, reddish-tan, fine grained, with gravel sized rock. Compact and

firm.

SW


Boring ID: F14-SB-6

BORING LOG







0-5' Sample F14-SB-6(0-2)

5

5'-10'

10

10'-15'

15

15'-20'

20

20'-25'

25

25'-30' SAND, fine grained, light reddish/tan, loosely packed.

30

30'-35

35

35'-40'

40

Continued on next page.


1.6

SAND, fine grained, light brown/tan compact and dense with chalky

gravel sized caliche at 14-15 ft.

SAND, fine grained, light reddish/tan. Compact, dense, chalky caliche

abundant trhougout.

SAND, fine grained light tan. Compact, dense, chalky caliche

throughout.

Sample

F14-SB-6(13-15)

Sample

F14-SB-6(28-30)

1.3

1.5

1.7

SAND, fine grained, loosely packed, tan/light brown with coarse

grained gravel and chalky caliche.

SAND, fine grained, loosely packed, tan/light brown with coarse

grained gravel and chalky caliche. Dense and compact at 9-10 ft.

0.7

0.0

0.6

0.4

SW

SAND, fine grained light reddish/tan with layer of light tan sand and

chalky caliche between 31 and 34 ft.

SAND, fine grained, light reddish/tan. Dense layer of sand and caliche

between 37 and 39 ft. Mixture of silty-sand and gravel sized caliche

and quartzite rock fragments at 39-40 ft.

P:\FORMS.HOU\LOGS\borelog.xls.xls (sb-6 (a))

Boring ID: F14-SB-6

BORING LOG







40'-50'

45

50

50'-57'

55

57'-80' SILTY-SAND, fine grained, loosely packed,

60

65

70

Quartzite rock fragments encoutnered after 72 ft.

75

80

Continued on next page.


2.5

SW

n/a

Mixture of silty-sand, chalky caliche, and gravel to cobble sized

quartzite rock fragments. Firm and densely packed.

0.0

0.3

SILTY-SAND, fine grained, light tan to brown. Compact and dense

with quartzite gravel mixed throughout.

2.3

1.9

n/a

2.8

P:\FORMS.HOU\LOGS\borelog.xls.xls (sb-6 (b))

Boring ID: F14-SB-6

BORING LOG







80'-85' SILTY-SAND, tan with gravel sized quartzite rock.

85

85.5'-86' CLAY, red brown, lean, firm and dense. Contains caliche. CL

90

90'-115' 2.0

95

1.6

100

105

110

115

Total Depth = 116.5 ft bgs.

120


3.2

n/a

Note: Layer of rock between 86-87', could not push sample, drilled

to 90 ft for next sample push.

n/a

0.3Sample

F14-SB-6(113-115)

Geotech Sample

F14-SB-6(115-116.5)

SILTY-SAND, fine grained, tan/brown, and densely

packed. Dry.

SW

SM

2.4

n/a

1.6

n/a

0.9

n/a

n/a

n/a

P:\FORMS.HOU\LOGS\borelog.xls.xls (sb-6 (c))

Boring ID: F14-SB-7

BORING LOG







0-5' Sample F14-SB-7(0-1)

5

5'-10'

10


15

20

25

30


SAND, coarse grained with gravel mixed throughout, loosely packed,

red-orange.

SAND, fine grained tan. Gravel throughout and root fragments

present. Dry.

2.7

2.1

SW


Boring ID: F14-SB-8

BORING LOG







0-5' Sample F14-SB-8(0-1)

5

5'-10' SAND, fine grained, tan. Gravel mixed throughout. Dry.

10


15

20

25

30


SAND, fine grained, loosely packed, red-orange. Coarse grained

gravel mixed throughout.

2.7

2.1

SW



APPENDIX C

RFI ANALYTICAL RESULTS SUMMARY

F14-SB-7 F14-SB-8

NMED

SSLs

Parameters 0-2 ft 13-15 ft 28-30 ft 0-2 ft 13-15 ft 28-30 ft 0-2 ft 13-15 ft 28-30 ft 0-2 ft 13-15 ft 28-30 ft 0-2 ft 13-15 ft 28-30 ft 0-2 ft 13-15 ft 28-30 ft 113-115 ft 0-1 ft 0-1 ft Residential

Dichloromethane 0.0051 J 0.0054 J 0.0052 J < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 0.0057 J 0.0048 J 0.0062 J < 0.01 < 0.01 < 0.01 0.0059 J 0.0049 J 0.0054 J 0.0053 J 0.0038 J 0.0039 J ne

All Other Analytes ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND various

Benxo(k)fluoranthene na na < 0.0066 na na < 0.0066 na na < 0.0066 na na < 0.0066 na na 0.0066 J na < 0.0066 < 0.0066 < 0.0066 < 0.0066 < 0.0066 62.1

Bis (2-ethylhexyl)phthalate na na 0.014 na na 0.0091 na na 0.017 na na 0.015 na na 0.019 na 0.015 0.01 0.015 0.0079 0.015 347

Caprolactum na na 0.025 na na < 0.0066 na na < 0.0066 na na 0.12 na na < 0.0066 na 0.015 < 0.0066 < 0.0066 < 0.0066 < 0.0066 ne

Chrysene na na < 0.0066 na na < 0.0066 na na < 0.0066 na na < 0.0066 na na 0.0067 na < 0.0066 < 0.0066 < 0.0066 < 0.0066 < 0.0066 615

Di-butyl phthalate na na 0.011 na na 0.0069 na na 0.015 na na 0.013 na na 0.012 na 0.015 0.0078 0.0082 0.0083 0.011 6110

All Other Analytes na na ND na na ND na na ND na na ND na na ND na ND ND ND ND ND various

All Analytes na ND na na ND na na ND na na ND na na ND na na ND na na ND ND various

All Analytes na ND na na ND na na ND na na ND na na ND na na ND na na ND ND various

All Analytes ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND na ND ND various

Diesel Range Organics < 1.7 < 1.7 na 1.6 J < 1.7 na 0.51 J < 1.7 na < 1.7 < 1.7 na < 1.7 < 1.7 na < 1.7 < 1.7 na na < 1.7 0.51 J 200 **

Notes :

ND - No detection of chemicals. mg/kg - milligrams per kilogram

na - Not analyzed ne - Not Established. No SSL for listed chemical.

< - Not detected at listed concentration. Samples were collected on February 13 to 16, 2008.

J - Estimated concentration below reporting limit.

SSL - Soil Screening Levels from Table A-1, NMED Hazardous Waste Bureau, Technical Background Document for the Development of Soil Screening Levels, Version 4.0, June 2006.

** - Screening value for soil affected with unknown oil (Table 2a), NMED Total Petroluem Hydrocarbon Screening Guidelines (October 2006).

F14-SB-6

Polychlorinated Biphenyls (mg/kg)

Total Petroleum Hydrocarbons (mg/kg)

Volatile Organic Compounds (mg/kg)

Semivolatile Organic Compounds (mg/kg)

Organochlorine Pesticides (mg/kg)

Chlorinated Herbicides (mg/kg)

F14-SB-5

Fort Bliss, New Mexico

Table 3 - 2

Summary of Detections - Organic Compounds - Soil Samples - February 2008

Oro Grande Landfill - FTBL-14

F14-SB-1 F14-SB-4F14-SB-3F14-SB-2

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F14-SB-7 F14-SB-9

NMED

SSLs

Parameters 0-2 ft 13-15 ft 28-30 ft 0-2 ft 13-15 ft 28-30 ft 0-2 ft 13-15 ft 28-30 ft 0-2 ft 13-15 ft 28-30 ft 0-2 ft 13-15 ft 28-30 ft 0-2 ft 13-15 ft 28-30 ft 113-115 ft 0-1 ft 0-1 ft Residential

Residential

SL

Soil

Background

Inorganic Chemicals (mg/kg)

Aluminum 4280 2980 6000 3960 2340 4260 4340 2960 3020 5430 2740 4360 3770 2370 6420 4230 2320 5370 5470 2700 2970 77800 77000 45000

Antimony < 0.485 < 0.467 < 0.472 0.199 J < 0.481 0.193 J < 0.463 < 0.485 < 0.485 < 0.481 < 0.45 < 0.439 < 0.459 < 0.472 < 0.485 < 0.446 0.173 J < 0.472 < 0.476 < 0.439 < 0.467 31.3 31 ne

Arsenic 1.92 1.77 3.38 2.16 2.71 2.25 2.59 2.18 2.69 2.77 1.92 1.74 2.27 1.57 4.01 2.41 1.74 2.67 2.01 1.25 1.35 3.9 0.39 / 22 ** 1.1 - 16.7

Baruim 110 16.9 24.6 60 30 94.4 124 36.1 58.7 119 44.9 27.5 79.3 24.8 28.7 69.8 31.2 46.2 79.8 37.5 35.9 15600 16000 430

Beryllium 0.285 J 0.209 J 0.304 J 0.254 J 0.147 J 0.255 J 0.269 J 0.184 J 0.213 J 0.346 J 0.191 J 0.228 J 0.225 J 0.145 J 0.354 J 0.298 J 0.185 J 0.254 J 0.292 J 0.23 J 0.196 J 156 160 0.5 - 2

Boron 2.88 4.73 7.42 3.36 4.88 5.53 3.01 4.47 5.01 5.12 3.01 3.81 3.08 4.42 6.82 1.98 J 4.48 5.32 6.41 1.95 J 1.45 J 15600 16000 2 - 200

Cadmium 0.101 J 0.0723 J 0.0791 J 0.0519 J < 0.481 0.0637 J 0.0548 J < 0.029 0.038 J 0.0939 J 0.0601 J 0.0672 J 0.0415 J < 0.472 0.0637 J 0.0591 J 0.0391 J 0.0345 J 0.0309 J 0.058 J < 0.467 39 39 0.01 - 1

Calcium 49400 14800 32700 28500 11200 39400 61600 12900 43400 48400 8730 28300 38800 11900 49300 26100 15800 22200 7430 2810 7060 ne ne ne

Chromium 3.1 2.91 4.14 3.74 3.05 5.22 3.59 3.24 3.22 3.54 2.99 3.1 3.44 2.76 5.34 4.37 3.36 4.88 5.28 3.59 3.38 234 210 38

Cobalt 1.7 1.04 1.96 1.8 0.952 1.88 1.89 1.18 1.64 2.05 0.887 1.33 1.64 0.918 2.2 2.29 1.12 1.79 2.06 1.53 1.23 1520 900 8

Copper 1.95 0.961 1.87 2.1 0.911 2 2.15 1.26 1.64 2.37 1.08 1.3 1.8 0.913 2.38 3.52 1.17 2.79 3.65 1.69 1.72 3130 2900 20

Cyanide < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 1220 1200 ne

Iron 3600 2840 4640 4240 2790 4530 4660 3360 3890 4320 2710 3190 4030 2620 5640 4840 3130 4740 5140 4490 3690 23500 55000 ne

Lead 3.35 2.51 3.22 3.28 2.3 3.81 3.41 2.57 2.98 4.06 2.39 2.56 3.23 2.25 4.12 4.79 2.47 3.31 3.4 2.92 2.87 400 400 10-18

Lithium < 4.76 5.63 9.3 < 4.76 < 4.67 5.05 < 4.9 < 4.59 < 4.81 4.82 < 4.72 7.69 < 4.76 < 4.81 15.6 < 4.76 < 4.9 20.1 7.86 < 4.39 < 4.46 ne ne ne

Magnesium 2030 1820 3720 2040 1770 2940 2530 1790 2260 2320 1300 2350 2320 1460 5260 1610 1590 4920 2510 898 1050 ne ne ne

Manganese 69 43.7 72 73.3 32.9 85.8 74.6 52.3 79 90.5 32.1 50.6 75.1 36.2 84.1 100 47.3 88.2 83.1 67.7 59.2 3590 3500 389 - 850

Mercury 0.00945 J < 0.0133 < 0.0131 0.00356 J < 0.0131 0.00219 J 0.0078 J < 0.0133 < 0.132 0.00524 J < 0.0132 < 0.0128 0.00197 J < 0.0132 < 0.0132 0.01 J < 0.0129 < 0.0131 < 0.0132 < 0.0131 < 0.0128 6.11 * 23 0.1

Molybdenum 0.2 J 0.173 J 0.256 J 0.246 J 0.119 J 0.358 J 0.216 J 0.157 J 0.225 J 0.208 J 0.186 J 0.177 J 0.212 J 0.168 J 0.124 J 0.133 J 0.248 J 0.309 J 0.172 J 0.197 J 0.1 J 391 390 ne

Nickel 3.06 2.07 3.78 2.92 1.88 3.07 3.37 2.29 2.5 4.14 1.8 2.6 2.7 1.79 4.68 3.82 2.08 3.53 3.87 2.5 2.49 1560 1600 16

Phosphorus 88.8 17.2 50 71.2 13.8 117 140 19.8 28.2 128 19.4 41.2 61.2 17.6 123 96.8 14.2 37.5 17.1 62 19.4 ne ne ne

Potassium 928 744 1700 1060 809 1220 1160 914 1040 1290 713 1190 972 740 2510 1110 744 1600 1640 608 695 ne ne ne

Selenium 0.445 J 0.247 J 0.407 J 0.407 J 0.352 J 0.525 0.709 0.359 J 0.538 0.6 0.221 J 0.286 J 0.576 0.357 J 0.583 0.493 0.425 J 0.403 J 0.452 J 0.34 J 0.324 J 391 390 0.2

Silica 16.3 8.65 14 29.6 8.71 16.9 9.37 9.21 13.4 18.5 12.3 28.5 17.8 13 30.8 33.2 20.3 94.2 196 76 18.3 ne ne ne

Silver 0.0285 J 0.0281 J 0.0204 J 0.116 J 0.1 J 0.116 J 0.103 J 0.102 J 0.101 J 0.027 J 0.0189 J 0.0201 J 0.105 J 0.0999 J 0.103 J 0.107 J 0.11 J 0.101 J 0.101 J 0.12 J 0.105 J 391 390 0.01 - 5

Sodium 83.8 403 433 < 47.2 454 367 74.7 452 273 266 290 79.3 42.6 J 202 417 < 44.6 370 463 372 19.3 J < 46.7 ne ne ne

Strontium 90.1 56.9 80.4 68.8 43.7 91.8 130 59.1 107 101 24.7 96.4 91.1 26.6 110 49.7 47 103 43.4 11 20.8 4690 4700 ne

Thallium 0.0813 J 0.0591 J 0.0836 J 0.0651 J < 0.481 0.0921 J < 0.463 < 0.049 < 0.0485 0.0798 J 0.053 J 0.0522 J 0.0529 J < 0.472 0.0667 J 0.0537 J 0.0746 J 0.0517 J 0.0554 J 0.149 J 0.576J 5.16 5.5 ne

Tin 1.03 J 1.07 J 1.13 J 1.04 J 1.09 J 1.08 J 0.945 J 1.1 J 1.03 J 0.972 J 1.05 J 1.07 J 1.00 J 1.06 J 1.07 J 0.955 J 1.12 J 1.18 J 1.05 J 1.07 J 1.05 J ne 47000 122

Titanium 94 66.5 102 104 65.6 113 91.8 75 104 105 58.6 69.8 97.9 67.8 100 104 69.1 93.3 92.9 80.9 81.1 ne ne ne

Vanadium 10.1 10.9 17.8 12 12.3 12.3 11.9 13.8 13.7 12.1 13 9.53 12.1 7.98 18 10.3 10 14.5 15.2 9.97 7.26 78.2 390 66

Zinc 9.47 5.96 10.5 10 5.85 11.5 10.3 7.1 8.96 10.5 5.61 7.45 10.7 5.84 14 12.8 6.58 12.1 13.7 9.42 8.33 23500 23000 22 - 50

Notes :

< - Not detected at listed concentration. mg/kg - milligrams per kilogram Boldface indicates that the detected concentration exceeded NMED SSL-Residential value.

J - Estimated concentration below reporting limit. Samples were collected on February 13 to 16, 2008.

ne - not established Analysis conducted by e-Lab, Inc., Houston, TX

SSL - Soil Screening Levels from Table A-1, NMED Hazardous Waste Bureau, Technical Background Document for the Development of Soil Screening Levels, Version 4.0, June 2006.

* - Mercury (methyl)

F14-SB-3 (angled boring)F14-SB-2 (angled boring) F14-SB-6F14-SB-5 (angled boring) USEPA Region 6

USEPA Region 6 Screening Levels (SLs) and background concentrations from Region 6 Human Health Medium- SCREENING LEVELS Specific Screening Levels 2008

Fort Bliss, Oro Grande, New Mexico

Table 3-3

Summary of Analytical Results for Inorganic Compounds - Soil Samples - February 2008

Oro Grande Landfill - FTBL-14

F14-SB-1 F14-SB-4

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APPENDIX D

SAMPLING AND ANALYSIS PLAN ADDENDUM

FINAL

SAMPLING AND ANALYSIS PLAN

FTB-014 (SWMU-25) ORO GRANDE LANDFILL

FORT BLISS, NEW MEXICO

Contract Number W91ZLK-13-0003 Task Order Number 0003

Prepared for:

DEPARTMENT OF THE ARMY U.S. ARMY ENVIRONMENTAL COMMAND

2450 Connell Road Fort Sam Houston, TX 78234

and

DEPARTMENT OF THE ARMY Headquarters, U.S. Army Garrison Command

1741 Marshall Road Ft. Bliss, TX 79916

Prepared by:

404 E. Ramsey, Suite 206 San Antonio, TX 78216

CAPE Project Number 21003.003

Revision Number: Rev 2

October 2018

Sampling and Analysis Plan CAPE Oro Grande Landfill Corrective Action i October 2018 Fort Bliss, NM

TABLE OF CONTENTS

Section Page

LIST OF ABBREVIATIONS AND ACRONYMS ...................................................................... iii

1.0 INTRODUCTION ...............................................................................................................1

2.0 ORO GRANDE LANDFILL FIELD SAMPLING ACTIVITIES ......................................2

2.1 Contaminant Delineation .........................................................................................2

2.2 Excavation Confirmation Sampling .........................................................................2

2.3 Clean Backfill Certification .....................................................................................3

2.4 Decontamination Procedures ...................................................................................3

2.5 Waste Characterization ...........................................................................................4

3.0 GENERAL SAMPLING PROCEDURES ..........................................................................6

3.1 General Sampling Materials ....................................................................................6

3.2 Sampling for Chemical Analyses.............................................................................6

3.3 Sample Containers and Preservation .......................................................................7

4.0 REFERENCES ....................................................................................................................9

FIGURES

1 Confirmation Sample Locations

TABLES

2-1 Sample Summary Table

2-2 Analytical Summary Table

2-3 IDW Analytical Method and Sample Bottle Requirements

Sampling and Analysis Plan CAPE Oro Grande Landfill Corrective Action ii October 2018 Fort Bliss, NM

LIST OF ABBREVIATIONS AND ACRONYMS

BCY banked cubic yards

bgs below ground surface

CAPE Cape Environmental Management, Inc.

CFR Code of Federal Regulations

CoC chain-of-custody

COPC Contaminant of Potential Concern

CY Cubic Yard

EPA Environmental Protection Agency

FD Field Duplicate (sample)

ft foot (feet)

GWTP groundwater treatment plant

IAW in accordance with

IDW investigative derive waste

MD matrix spike duplicate (sample)

MICC Mission and Installation Contracting Command

MS matrix spike (sample)

NMAC New Mexico Administrative Code

NMED ̀ New Mexico Environment Department

oz ounce

PAH poly-nuclear aromatic hydrocarbons

PBA Performance Based Acquisition

PCB Polychlorinated biphenyls

PM Project Manager

PPE personal protective equipment

PWS Performance Work Statement

QC Quality Control

QAPP Quality Assurance Project Plan

RCRA Resource Conservation and Recovery Act

RFI RCRA Facility Investigation

Sampling and Analysis Plan CAPE Oro Grande Landfill Corrective Action iii October 2018 Fort Bliss, NM

SAP Sampling and Analysis Plan

SOP Standard Operating Procedure

SSHP Site Safety and Health Plan

SSL Soil Screening Level

SVOC semi-volatile organic compound

SW Solid Waste

TAL Target Analyte List

TCL Target Compound List

TCLP Toxicity Characteristic Leaching Procedure

T&D Transport & Disposal

TO Task Order

TPH-DRO Total Petroleum Hydrocarbon-Diesel Range Organics

VOC volatile organic compound

Sampling and Analysis Plan CAPE Oro Grande Landfill 1 October 2018 Fort Bliss NM

1.0 INTRODUCTION

Cape Environmental Management Inc. (CAPE) is submitting this Sampling and Analysis Plan (SAP) to the United States Army in accordance with (IAW) the Performance Work Statement (PWS), dated April 13, 2015, included in the Performance-Based Acquisition (PBA) Contract W91ZLK-13-D-0003, Task Order (TO) 0003, for firm fixed-price environmental remediation services at four sites at Fort Bliss, Texas. The TO was issued by the U.S. Army Mission and Installation Contracting Command (MICC), Fort Sam Houston, Texas, on July 1, 2015. This SAP only applies to the Oro Grande Landfill Corrective Measures Action.

The Oro Grande Landfill is located in Otero County, New Mexico within the Fort Bliss Military Reservation. The landfill is 0.8 miles south-southwest of the Oro Grande Range Camp at the southwest edge of Elephant Mountain in the Tularosa Basin of New Mexico. Placement of waste material in the landfill area spanned a 30-year period of time, from 1964 until 1994. The waste material comprising the landfill is reported to consist of concrete, glass, building materials, plastic, wiring, packaging materials, and demolition debris. The Oro Grande is a trench-type landfill. Based on findings obtained in a Resource Conservation and Recovery Act (RCRA) Facility Investigation (RFI) report, the extent of the buried waste is approximately 345 feet by 37 feet (0.29 acres) and averages 2.8 feet thick, but varies up to about 7 feet thick. The soil cover averages 4.6 feet thick but varies from 1 to 10 feet thick, and the bottom of the debris layer is approximately 12 to 14 feet below ground surface (bgs). It is estimated that there are 2,075 cubic yards of waste debris in the landfill (NMED, 2014).

This SAP has been prepared in reference to environmental remediation work IAW RCRA and New Mexico Administrative Code (NMAC) regulations and requirements of the PWS and Fort Bliss. It defines the approach to collection of confirmation samples and waste characterization, and borrow source characterization samples. This SAP will be submitted to the Army and the New Mexico Environmental Department (NMED) for approval.


2.0 ORO GRANDE LANDFILL FIELD SAMPLING ACTIVITIES

The RFI report from 2009 states that analytical results from samples collected at this site indicate that there were no contaminant concentrations exceeding the NMED Soil Screening Levels (SSLs) for Residential exposure with the exception of arsenic, which was detected at a level below the naturally-occurring background levels for native soils at this site. Consequently, the RFI did not identify any contaminants of potential concern (COPCs). This section provides details and guidance for performing the environmental sampling necessary to provide waste characterization, clean closure confirmation, and clean backfill confirmation. These samples are summarized in Tables 2-1 and 2-2, Sample Summary Table and Analytical Summary Table, and are further described in the following sections.

2.1 Contaminant Delineation

Contaminant delineation sampling and exploratory trench excavations were made as part of the RFI and the excavation area is currently marked. Further excavation delineation will be performed visually in the field by removing debris as it is encountered. When the excavation appears to be clear of debris, confirmation sampling will be conducted.

2.2 Excavation Confirmation Sampling

Since there were no COPCs identified in the RFI, there were no exceedances of COPCs above NMED SSL-Residential values found during the RFI. Subsequently, confirmation soil samples will, be analyzed for the same chemical groups: volatile organic compounds VOCs), by Environmental Protection Agency (EPA) Solid Waste (SW) 5035/8260, semi-volatile organic compounds (SVOCs), by EPA SW 3541/8270, metals (by EPA SW 6020/7000), pesticides (by EPA SW 3541/8081), herbicides (by EPA SW 3550/8151), polychlorinated biphenyls (PCBs) via Arochlor mixtures, by EPA SW 3541/8082, and total petroleum hydrocarbons-diesel range organics (TPH-DRO), by EPA SW 5000/8015C. The most recent NMED SSL list of contaminants for each analytical group, contained in the NMED Risk Assessment Guidance for Site Investigations and Remediation dated July 2015 will be reported. If suspect contamination is discovered, the material will be segregated and characterized. Additional analyses may be performed based on any evidence of contaminants other than the NMED SSL list. If no suspicious materials or substances are uncovered during excavation, 21 confirmation samples will be collected. Sixteen samples will be collected from the sidewalls of the excavation and five from the base of the excavation, as shown on Figure 1. One field duplicate (FD), one matrix spike (MS), and one matrix spike duplicate (MD) will also be collected during confirmation sampling for Quality Control (QC) purposes. If suspicious materials are encountered during excavation, the sampling scheme will be tailored to fit the situation. Sample collection procedures are discussed in Section 3. All samples will be sent to Accutest Laboratories for analysis. The analytical results will be compared to the NMED SSL-Residential screening values published July 2015, to confirm if cleanup levels have been met or if excavation limits need to be adjusted.


2.3 Clean Backfill Certification

Backfill from the Fort Bliss borrow source will be certified as clean before it is used to backfill the excavation. All backfill material will have laboratory results at a rate of one sample result per 500 cubic yards (CY) and a minimum of one representative discrete sample per source to confirm it is clean. The discrete sample will be collected from a depth interval of 0.5 to 1.0 feet (ft.).

The backfill soil/sand will be analyzed for the following parameters:

Target Compound List (TCL) SVOCs, by EPA SW 3541/8270, including poly-nuclear aromatic hydrocarbons (PAH),

TCL VOCs, by EPA SW 5035/8260,

TCL Pesticides by EPA SW 3541/8081 and PCBs, by EPA SW 3541/8082,

Target Analyte List (TAL) Metals, by EPA SW 6020/7000.

Based on a total waste volume of approximately 2,075 CY that is estimated to be replaced with backfill borrow source material, three discrete samples from random locations within the borrow soil volume to be used for backfill will be submitted to Accutest to certify. In addition, all stockpiled overburden soil excavated to access the landfill waste material will also be sampled and analyzed at the same frequency of one sample per 500 CY. The results will be compared to the NMED SSL Residential values and to the United States Environmental Protection Agency Regional Screening Levels IAW the procedures contained in the NMED Risk Assessment Guidance for Site Investigations and Remediation dated July 2015 to approve the stockpiled overburden for reuse as backfill in the excavation.

2.4 Decontamination Procedures

For the limited sampling required for this excavation it is anticipated that disposable sampling equipment, e.g. food-grade disposable aluminum heating pans and stainless steel spoons for homogenization and bottling of samples will be used. Disposable sampling equipment will be used to collect one sample and then discarded or recycled. No decontamination will be needed for sampling equipment. All potentially contaminated materials will be handled with gloved hands and with the appropriate personal protective equipment (PPE) as determined by the Site Safety and Health Plan (SSHP).

Given the dry nature of this site and sandy soil, heavy equipment can likely be swept clean prior to removal from the site. No wet decontamination is anticipated; however, if COPCs are encountered during excavation and wet decontamination is required for heavy equipment, CAPE will decontaminate using a power washer. Any wastewater from a power washer will be captured on a plastic liner, drummed, sampled and appropriately disposed.


2.5 Waste Characterization

Excavation wastes will be characterized and classified in accordance with Title 40 Code of Federal Regulations (CFR) Part 261. All waste will be managed and disposed in accordance with the requirements of the USEPA, NMED, and Fort Bliss.

This project entails transport and disposal (T&D) of landfilled debris. CAPE will sample any portions of the debris necessary to provide the landfill proper waste characterization; however, it is not anticipated that waste characterization of the debris will be needed.

Any debris that appears to contain lead paint, fuels or solvents, industrial or sanitary waste, or any other solid waste not conforming to typical inert debris, will be stockpiled on-site and covered with plastic sheeting, or alternatively placed in drums. Liquid wastes will be placed in drums or poly tanks. Containers will be labeled to protect them from tampering and will be staged in a secured (fenced) area.

Waste characterization samples will be collected from in-situ wastes to evaluate the disposal requirements for the wastes. Samples will be collected with a Geoprobe or hollow-stem auger drill rig, to 16 feet bgs.

CAPE will collect samples of debris and any potentially impacted soil and analyze for Toxicity Characteristic Leaching Procedure (TCLP) analysis for VOCs, SVOCs, metals, pesticides and herbicides. Wastes will also be analyzed for PCBs, TPH, asbestos, radioisotope assay for strontium, ignitability, corrosivity and reactivity.

Analytical method and sample bottle requirement are provided in Table 2-2. Waste characterization results will be compared to the TCLP, ignitability, corrosivity and reactivity values listed in 40 CFR Part 261 Subpart C, values for PCBs listed in 40 CFR Part 761.61, radioisotope values in picocuries per gram and the TPH values for facility acceptance criteria.

The following waste streams could potentially be generated during T&D of landfilled debris:

Contaminated water from equipment decontamination

Contaminated solids from equipment decontamination

Contaminated debris, which include, but are not limited to, discarded materials used in decontamination, plastic sheeting, sampling materials, and personal protective clothing

General municipal waste.

Soil wastes, liquid waste, decontamination solids, decontamination liquid, and contaminated debris will be segregated from other solid waste generated during the proposed site activities. These wastes will be characterized to determine whether it must be managed and disposed of as special waste, hazardous waste, or non-hazardous waste.


Liquid wastes will be characterized to determine whether it can be transferred to the Fort Bliss groundwater treatment plant (GWTP) for disposal or disposed of as hazardous waste.

Investigative derive waste (IDW), such as used personal protective equipment, expendable sampling equipment, or plastic used to cover any waste or stockpiled materials, will be sampled as needed to characterize the IDW. CAPE will discuss the acceptance criteria with the landfill prior to sending them any IDW. Analytical methods are shown in Table 2-3.


3.0 GENERAL SAMPLING PROCEDURES

This section describes the general procedures to be used for soil contaminant delineation, confirmation and waste characterization sampling activities and provides checklists of the necessary equipment.

3.1 General Sampling Materials

The following general materials are required:

All data necessary to properly identify the scope of work. This should include items such as reports, historical field and lab data, and any special instructions (i.e., NMED guidelines, project specifications, etc.)

Chain-of-custody (CoC) forms

Field notebook/field forms

Custody seals

Sampling tool(s)

Laboratory-prepared sampling containers

Sample container labels

Waterproof marking pens

Laboratory-prepared travel blanks, if required

Preservatives (supplied by laboratory if required)

Insulated cooler & ice

Packing materials for shipping samples

PPE as specified in the SSHP (Appendix C of the Work Plan).

3.2 Sampling for Chemical Analyses

Sample containers (provided by the laboratory) will be pre-labeled prior to commencing the sampling activities. The sampling procedure for the confirmatory and waste characterization samples is summarized below (procedure modifications for grab sample collection are shown in parenthesis):

Prepare the work area around the sample location by placing plastic sheeting on the ground to avoid cross-contamination.

Verify that the sample containers for the current location are labeled correctly.

Collect the soil/sand sample with a disposable spoon.


Homogenize the sample material, place the soil aliquot in the sample containers and secure the caps tightly. Soil sampled for VOCs will not be homogenized. Soil samples to be analyzed for VOCs will be collected using a coring device (such as a modified syringe or Encore™ Sampler), and immediately capping the sample. New sample equipment (coring devices) will be used for each sample location. (Discrete samples: proceed to next step).

Check sample label. Be sure label is completed with all necessary information such as time, date and sampler initials.

Place filled sample containers on ice immediately.

Complete all required information on each sample collection log sheet prior to moving to the next sampling location.

Disposable non-latex gloves will be worn during sampling activities, and will be changed between sampling locations.

Complete COC documents and appropriate field log-book entries prior to leaving the sampling area for breaks, shift termination or for any other non-emergency reason.

Prior to any sample collection, if there are any unidentified odors in the air, or there is a reason to believe that potential hazardous or contaminant vapors are present, the Project Manager (PM) and Site Health and Safety Officer will be notified. Ventilation and/or other engineering controls will be implemented and the conditions will be noted on the field sampling form and the field logbook.

Some other products that may pose cross-contamination issues include: perfumes and cosmetics, skin-applied pharmaceuticals, suntan lotion, and automotive products (e.g., starting fluid, windshield de-icer, carburetor cleaners, upholstery cleaners, etc.). Use of these or other products constituting potential impact on sample integrity will be avoided before and while collecting/managing samples.

The PM will be consulted regarding significant departures from standard operating procedures (SOPs). The PM will document the modifications, then notify the Contracting Officer’s Representative to discuss any such variation from the SOP. Notes will be kept describing the sampling procedures and variations, and submitted to the PM for review. Any deviations from the SOPs or the SAP will be discussed in the Corrective Measures Completion Report.

3.3 Sample Containers and Preservation

Pre-preserved sample containers for soil samples will be provided by the contract laboratory. The containers will be shipped, along with labels and manufacturer’s quality control documentation, from the laboratory to CAPE via common carrier in clean coolers using custody seals. Coolers will be packed with ice, and will include a temperature blank. For all coolers containing samples for VOC analysis, a trip blank will also be


included. All samples will be collected and shipped such that the 24-hour hold time period for VOC sample preparation is not exceeded.


4.0 REFERENCES

CAPE, 2015. Corrective Action Work Plan, FTB-014 (SWMU-25) Oro Grande Landfill, Fort Bliss, New Mexico. September.

Malcolm Pirnie, 2009. RCRA Facility Investigation Report, Oro Grande Landfill (SWMU 25/FTBL-14). January.

Malcolm Pirnie, 2011. Final Letter Report for the Cover and Borrow Area Investigation of the Oro Grande Landfill (SWMU-25/FTBL-14). November.

NMED, 2015, Risk Assessment Guidance for Site Investigations and Remediation. July.

Sampling and Analysis Plan CAPE Oro Grande Landfill October 2018 Fort Bliss NM

FIGURES

Figure 1: Confirmation Sample Locations

CONFIRMATION SAMPLE LOCATIONS

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TABLES


Table 2-1 Sample Summary Table

Sampling and Analysis Plan Oro Grande Landfill Remedial Action Work Plan

Sampling Location Matrix Analytical Group Number of Samples

Rationale for Sampling Location

Excavation Base and Sidewalls Soil

Volatile organic compounds (VOCs), Semi-volatile organic compounds (SVOCs), metals, pesticides, herbicides,

polychlorinated biphenyls (PCBs), and total petroleum hydrocarbons-diesel range organics (TPH-DRO)

(reporting NMED SSL list of contaminants for each analytical group)

At least 21 (Additional 3 per

area of contamination, if

discovered)

Delineation and Confirmation

Excavated Contaminated Soil and/or Debris (if discovered) Soil / Debris

Toxicity Characteristic Leaching Procedure (TCLP) VOCs, TCLP SVOCs, TCLP Pesticides, TCLP Herbicides, PCBs, TPH-

DRO, Asbestos, Reactivity, Paint Filter test, selected as appropriate

To be calculated in accordance with

EPA SW-846, Chapter 9


Segregated Soil for Reuse Soil VOCs, SVOCs, metals, pesticides, herbicides, PCBs, and TPH-DRO (reporting NMED SSL list of contaminants for

each analytical group)

1 per 500 banked cubic yards (BCY)

Clean Soil Confirmation

Borrow Soil for Backfill Soil VOCs, SVOCs, metals, pesticides, herbicides, PCBs, and TPH-DRO (reporting NMED SSL list of contaminants for

each analytical group) 1 per 500 BCY Certification of Clean

Backfill


Table 2-2 Analytical Summary Table


Matrix Analytical Group

Analytical and Preparation Method/ SOP Reference Container Sample

Volume Preservation

Requirements Preparation

Holding Time Analytical

Holding Time

Solid VOCs SW-846 5030/8260B Encore or other sampling device - (3) 40-mL glass + (1) 2 oz glass jar

5 grams per 40 mL vial

Cool to 0-6°C, methanol and

sodium bisulfate 48 hours 48 hours

Solid SVOCs SW-846 3550C/8270D (1) 4 oz glass jar 30 grams Cool to 0-6°C 14 days 40 days Solid ICP Metals SW-846 3010A/6010C

(1) 8 oz glass jar 30 grams Cool to 0-6°C 180 days 180 days

Solid Mercury SW-846 3015A/7471B 30 grams Cool to 0-6°C 28 days 28 days Solid Pesticides SW-846 3550/8081B

(1) 8 oz glass jar 30 grams Cool to 4°C 14 days 40 days

Solid Herbicides SW-846 3550/8151A 30 grams Cool to 4°C 14 days 40 days

Solid Polychlorinated biphenyls SW-846 3550/8082A (1) 4 oz jar 30 grams Cool to 0-6°C 14 days 40 days

Solid

Total petroleum hydrocarbons – Gasoline range organics

SW-846 3550/8015 (1) 4 oz jar 30 grams Cool to 0-6°C 14 days 40 days

Solid

Total petroleum hydrocarbons – Diesel range organics


Waste

TCLP VOCs TCLP SVOCs TCLP Metals TCLP Pesticides TCLP Herbicides

SW-846 1311/8260B SW-846 1311/8270C SW-846 1311/6010C/7470A SW-846 1311/8081B SW-846 1311/8151A

16 oz glass jar

For full TCLP analyses - collect a TOTAL of

150 grams minimum

Cool to 0-6°C

VOC, SVOC, Pesticides,

Herbicides 14 Days Metals, Mercury

28 days else 6 months




Waste TPH SW-846 3550/8015 (1) 4 oz jar 30 grams Cool to 0-6°C 14 days 40 days Waste PCBs SW-846 3550/8082A (1) 4 oz jar 30 grams Cool to 0-6°C 14 days 40 days Waste Strontium EPA 905.0 Mod/DOE, RP501 Rev. 1 Mod (1) 4 oz jar 30 grams NA NA 28 Days Waste Reactivity Chapter 7, 9012B, 9034 (1) 4 oz jar 30 grams NA NA 28 Days Waste Corrosivity (1) 4 oz jar 30 grams NA NA 28 Days Waste Ignitability (1) 4 oz jar 30 grams NA NA 28 Days Waste Paint Filter SW-846 9095 NA NA 28 Days Waste Asbestos EPA-LIBBY-03 (TEM) (1) 4 oz glass jar 30 grams NA NA NA

VOCs – Volatile organic compounds SVOCs – Semivolatile organic compounds mL – milliliter oz – ounce


oC – degrees Celsius ICP – Inductively-coupled plasma TCLP – Toxicity Characteristic Leaching Procedure TEM – Transmission Electron Microscopy


Table 2-3

IDW Analytical Method and Sample Bottle Requirements

Parameter Analytical Method Bottle Requirement Preservative

TCLP VOCs SW1311/8260B (3) 40-milliliter glass vials Methanol (1) and NaHSO4 (2)

TCLP VOCs SW1311/8260B (1) 4-oz glass jar Ice

TCLP SVOCs SW1311/8270D (1) 8-oz glass jar Ice

TPH-DRO SW 3541/8015 (1) 8-oz glass jar Ice

TCLP Metals SW1311/6010C (1) 4-oz glass jar Ice

PCBs SW8082A (1) 4-oz glass jar Ice

Pesticides/ Herbicides SW8081B/SW8151A (1) 8-oz glass jar Ice

Ignitability SW1010/1020 (1) 4-oz glass jar None

Corrosivity SW9040/9045 (1) 4-oz glass jar None

Reactivity SW846 Chapter 7 (1) 4-oz glass jar None Notes: IDW = investigative-derived waste oz = ounce SVOC = semivolatile organic compound

TCLP = toxicity characteristic leaching procedure

TPH = total petroleum hydrocarbons

VOC = volatile organic compound

Sampling and Analysis Plan CAPE Oro Grande Landfill March 2017 Fort Bliss NM

TABLES


Table 2-1 Sample Summary Table


Sampling Location Matrix Analytical Group Number of Samples

Rationale for Sampling Location

Excavation Base and Sidewalls Soil

Volatile organic compounds (VOCs), Semi-volatile organic compounds (SVOCs), metals, pesticides, herbicides,

polychlorinated biphenyls (PCBs), and total petroleum hydrocarbons-diesel range organics (TPH-DRO)

(reporting NMED SSL list of contaminants for each analytical group)

At least 21 (Additional 3 per

area of contamination, if

discovered)

Delineation and Confirmation

Excavated Contaminated Soil and/or Debris (if discovered) Soil / Debris

Toxicity Characteristic Leaching Procedure (TCLP) VOCs, TCLP SVOCs, TCLP Pesticides, TCLP Herbicides, PCBs, TPH-

DRO, Asbestos, Reactivity, Paint Filter test, selected as appropriate

To be calculated in accordance with

EPA SW-846, Chapter 9


Segregated Soil for Reuse Soil VOCs, SVOCs, metals, pesticides, herbicides, PCBs, and TPH-DRO (reporting NMED SSL list of contaminants for

each analytical group)

1 per 500 banked cubic yards (BCY)

Clean Soil Confirmation

Borrow Soil for Backfill Soil VOCs, SVOCs, metals, pesticides, herbicides, PCBs, and TPH-DRO (reporting NMED SSL list of contaminants for

each analytical group) 1 per 500 BCY Certification of Clean

Backfill


Table 2-2 Analytical Summary Table


Matrix Analytical Group

Analytical and Preparation Method/ SOP Reference Container Sample

Volume Preservation

Requirements Preparation

Holding Time Analytical

Holding Time

Solid VOCs SW-846 5030/8260B Encore or other sampling device - (3) 40-mL glass + (1) 2 oz glass jar

5 grams per 40 mL vial

Cool to 0-6°C, methanol and

sodium bisulfate 48 hours 48 hours

Solid SVOCs SW-846 3550C/8270D (1) 4 oz glass jar 30 grams Cool to 0-6°C 14 days 40 days Solid ICP Metals SW-846 3010A/6010C

(1) 8 oz glass jar 30 grams Cool to 0-6°C 180 days 180 days

Solid Mercury SW-846 3015A/7471B 30 grams Cool to 0-6°C 28 days 28 days Solid Pesticides SW-846 3550/8081B

(1) 8 oz glass jar 30 grams Cool to 4°C 14 days 40 days

Solid Herbicides SW-846 3550/8151A 30 grams Cool to 4°C 14 days 40 days

Solid Polychlorinated biphenyls SW-846 3550/8082A (1) 4 oz jar 30 grams Cool to 0-6°C 14 days 40 days

Solid

Total petroleum hydrocarbons – Gasoline range organics


Solid

Total petroleum hydrocarbons – Diesel range organics


Waste

TCLP VOCs TCLP SVOCs TCLP Metals TCLP Pesticides TCLP Herbicides

SW-846 1311/8260B SW-846 1311/8270C SW-846 1311/6010C/7470A SW-846 1311/8081B SW-846 1311/8151A

16 oz glass jar

For full TCLP analyses - collect a TOTAL of

150 grams minimum

Cool to 0-6°C







Waste TPH SW-846 3550/8015 (1) 4 oz jar 30 grams Cool to 0-6°C 14 days 40 days Waste PCBs SW-846 3550/8082A (1) 4 oz jar 30 grams Cool to 0-6°C 14 days 40 days Waste Strontium EPA 905.0 Mod/DOE, RP501 Rev. 1 Mod (1) 4 oz jar 30 grams NA NA 28 Days Waste Reactivity Chapter 7, 9012B, 9034 (1) 4 oz jar 30 grams NA NA 28 Days Waste Corrosivity (1) 4 oz jar 30 grams NA NA 28 Days Waste Ignitability (1) 4 oz jar 30 grams NA NA 28 Days Waste Paint Filter SW-846 9095 NA NA 28 Days Waste Asbestos EPA-LIBBY-03 (TEM) (1) 4 oz glass jar 30 grams NA NA NA

VOCs – Volatile organic compounds SVOCs – Semivolatile organic compounds mL – milliliter oz – ounce


oC – degrees Celsius ICP – Inductively-coupled plasma TCLP – Toxicity Characteristic Leaching Procedure TEM – Transmission Electron Microscopy


Table 2-3

IDW Analytical Method and Sample Bottle Requirements

Parameter Analytical Method Bottle Requirement Preservative

TCLP VOCs SW1311/8260B (3) 40-milliliter glass vials Methanol (1) and NaHSO4 (2)

TCLP VOCs SW1311/8260B (1) 4-oz glass jar Ice

TCLP SVOCs SW1311/8270D (1) 8-oz glass jar Ice

TPH-DRO SW 3541/8015 (1) 8-oz glass jar Ice

TCLP Metals SW1311/6010C (1) 4-oz glass jar Ice

PCBs SW8082A (1) 4-oz glass jar Ice

Pesticides/ Herbicides SW8081B/SW8151A (1) 8-oz glass jar Ice

Ignitability SW1010/1020 (1) 4-oz glass jar None

Corrosivity SW9040/9045 (1) 4-oz glass jar None

Reactivity SW846 Chapter 7 (1) 4-oz glass jar None Notes: IDW = investigative-derived waste oz = ounce SVOC = semivolatile organic compound

TCLP = toxicity characteristic leaching procedure

TPH = total petroleum hydrocarbons

VOC = volatile organic compound


APPENDIX E

WASTE CHARACTERIZATION SAMPLING ANALYTICAL RESULTS

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DATA EVALUATION REPORT CHEMISTRY SERVICES

DATE: August 30, 2017

RECIPIENT: Krishna Nalavala ([email protected])

PREPARER: Albert Iannacone ([email protected])

COPY: [email protected]

PROJECT #: 21003.003.110

PROJECT NAME: Ft. Bliss Oro Grande Landfill

DESCRIPTION: Waste Characterization Samples

ITEMS SUBMITTED UNDER THIS TRANSMITTAL:

ITEM CLASSIFICATION ITEM DESCRIPTION # OF COPIES

Original Analytical Data (Hardcopy/CD) Lab Reports – Annotated Form 1s Twenty-three soil samples and three trip blank soils, 1 EDDs collected July 25, 2017 and analyzed by Quality Assurance Reports SGS Accutest Southeast, Orlando, FL and Planning Document GEL Laboratories, Charleston, SC (radiological only) Proposal Information Lab SOW and Pricing

ACTION CODE FOR RECIPIENT:

For Recipient Use

Revise and Resubmit to Preparer No exception taken Revise as noted PREPARER SIGNATURE

PREPARER COMMENTS:

This report covers four data packages, as follows:

Thirteen soil samples and one trip blank soil sample collected on July 25, 2017, and reported in SDG FA46136. Samples FA46136-02 through -14 correspond to field sample numbers T030GL-WC04 through -16.

Three soil samples and one trip blank soil sample collected on July 24, 2017, and reported in SDG FA46145.

Samples FA46145-02 through -04 correspond to field sample numbers T030GL-WC01 through -03.

Seven soil samples and one trip blank soil sample collected on July 26, 2017, and reported in SDG FA46163. Samples FA46163-02 through -08 correspond to field sample numbers T030GL-WC17 through -23.

Three soil samples collected on July 25, 2017, and reported in GEL SDG 428907. The samples 428907-001

through -003 correspond to SGS Accutest samples FA46136-2, -10 and -11 and to field sample numbers T030GL-WC04, -12 and -13, respectively.

The attached chain-of-custody forms present a summary of the CAPE identification numbers, data of collection, sample matrix, and the analyses requested.

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The samples were shipped to SGS Accutest Southeast, Orlando, FL for analysis. The radiological analyses were subcontracted to GEL Laboratories, LLC, Charleston, SC. The samples were analyzed for the following methods: Toxicity Characteristic Leaching Procedure (TCLP) Volatile Organic Compounds (VOCs) by SW-846 Method 8260B; TCLP Semivolatile Organic Compounds (SVOCs) by SW-846 Method 8270D; Organochlorine Pesticides by SW-846 Method 8081B; Polychlorinated Biphenyls (PCBs) by SW-846 Method 8082A; Chlorinated Herbicides by SW-846 Method 8151A; TCLP Metals/Mercury by SW-846 Methods 6010C/7470A; Total Petroleum Hydrocarbons (TPH) by SW-846 Method 8015C; Ignitability by EPA Method 1010; Corrosivity by SW-846 Chapter 7 (7.1); Reactive Cyanide/Sulfide by SW-846 Chapter 7 (7.2) Percent Solids by Standard Methods 2540G; Asbestos by EPA Method 600/R-93/116; Gross Alpha / Beta Activity by EPA Method 900.0 / SW-846 9310 / Standard Methods 7110B (modified); and Strontium 89 / 90 by EPA Method 905.0 (modified) / DOE RP 501 Revision 1 (modified). EPA Level IV data packages were provided for review. SGS Accutest Southeast Laboratories followed method SW-846 1311 to prepare the samples for TCLP analysis. The soil trip blank samples were analyses for total VOCs, but only the TCLP target list of compounds were reported.

Data Validation Comments

Data validation was performed in accordance with the U.S. Department of Defense (DoD) Quality Systems Manual (QSM) for Environmental Laboratories, Version 5.0, July 2013; and, a modified USEPA National Functional Guidelines (NFG) for Superfund Organic Methods Data Review, September 2016. When specific guidance was not available, the data was evaluated in a conservative manner consistent with USEPA standards using best professional judgement.

Results reported above the Detection Limits (DL) and below the Limit of Quantitation (LOQ) are qualified “J”. Non-detected results are reported at the Limit of Detection with a “U” qualifier. In cases of blank contamination at concentrations high enough to compromise the reliability of the sample data, a “B” qualifier is applied to the result. A “UJ” qualification indicates a nondetect result at an estimated detection limit.

Any aspect of the data not discussed in this report should be considered qualitatively and quantitatively valid, as reported, based on the deliverables reviewed.

Comments specific to each of the individual data packages follow: SDG FA46136 There were no problems that required qualification of data in the VOC trip blank soil sample. For soils FA46136-02 through -14, carbon tetrachloride was “UJ” qualified due to poor matrix spike/matrix spike duplicate (MS/MSD) recovery. Due to contamination in the associated laboratory (method) blank, the compound chloroform was qualified “B” in samples FA46136-12 through -14 (T030GL-WC14 through -16). For TCLP SVOCs, poor precision (excessive RPDs) were noted in the MS/MSD for 2-methylphenol and 3&4-methylphenol. As a result, “UJ” data qualification was required for these compounds in FA46136-02 through -14. Note that the laboratory was unable to separate 3-methylphenol and 4-methylphenol and reported the sum of the two as 3&4-

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methylphenol. Initial calibration verification criteria for 2,4,5- and 2,4,6-trichlorophenol and for pentachlorophenol were not met; “UJ” qualification was required for samples FA46136-02 through -14 as a result. For TCLP Pesticides, Lindane in sample FA46136-13 (T030GL-WC15) was qualified “J” due to poor agreement between GC columns (quantitative uncertainty of the concentration). For TCLP Herbicides, continuing calibration verifications indicated a change in instrument sensitivity for the compounds 2,4-D and 2,4,5-TP (Silvex), which were “UJ” qualified in samples FA46136-02 through -14 as a result. For TPH-GRO (C10-C28), the MSD analysis had unacceptably poor recovery, and a continuing calibration verification sample indicated a change in instrument sensitivity. As a result, samples FA46136-02 through -14 were qualified “J.” There were no problems in the remaining analyses that required any qualification of data. SDG FA46145 The VOC trip blank sample soil vials were not received at the laboratory within 48 hours of sample. As a result, there is a possibility of a low bias to the sample data for this sample. As all target compounds were nondetect, all results in this sample only (FA46145-01) are qualified “UJ.” There were no problems that required any qualification of data in the TCLP VOCs for the remaining soil samples. For TCLP SVOCs, the matrix spike/matrix spike duplicate (MS/MSD) analyses indicated poor precision (excessive RPDs) for 2-methylphenol and 3&4-methylphenol. As a result, “UJ” qualification of data was required for these compounds in samples FA46145-02 through -04. Note that the laboratory was unable to separate 3-methylphenol and 4-methylphenol and reported the sum of the two as 3&4-methylphenol. For TCLP SVOCs, an initial calibration verification (ICV) failed criteria for 2,4,5- and 2,4,6-trichlorophenol and for pentachlorophenol. “UJ” qualification of these compounds was required in samples FA46145-02 through -04. For TCLP Herbicides, continuing calibration verification indicated a change in instrument sensitivity for the compound 2,4-D. As a result, samples FA46145-02 through -04 were qualified “UJ” for this compound. For TPH-GRO (C10-C28), the MSD analysis had unacceptably poor recovery, and a continuing calibration verification sample indicated a change in instrument sensitivity. As a result, samples FA46145-02 through -04 were qualified “J.” There were no problems in the remaining analyses that required any qualification of data. SDG FA46163 There were no problems that required qualification of data in the VOC trip blank soil sample. Due to contamination in the associated laboratory (method) blank, the compound chloroform was qualified “B” in samples FA46163-02 through -06 (T030GL-WC17 through -21). In the same samples, benzene and tetrachloroethylene were “J” or “UJ” qualified (as appropriate) due to poor precision in the laboratory duplicate analysis. For TCLP SVOCs, the blank spike (laboratory control sample, LCS) and/or matrix spike/matrix spike duplicate (MS/MSD) analyses indicated poor precision (excessive RPDs) for 2,4,5- and 2,4,6-trichlorophenol, pyridine and hexachloroethane. As a result, “UJ” data qualification was required for these compounds in samples FA46163-02 through -08. The laboratory was unable to separate 3-methylphenol and 4-methylphenol and reported the sum of the two as 3&4-methylphenol. Due to failures in continuing calibration verification (CCV) criteria for hexachlorobutadiene and 2,4-dinitrotoluene, “UJ” qualification was required for these compounds in samples FA46163-02 through -08.

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For TPH-GRO (C10-C28), the MS/MSD analyses had unacceptably poor recovery, as did a surrogate recovery in sample FA46163-05 (T030GL-WC20). As a result, samples FA46163-02 through -08 were qualified “J.” The GC data indicated additional hydrocarbons heavier than C28; as a result, the concentrations may be lower estimates of the contamination present, which is an additional reason for “J” qualification of these data. There were no problems in the remaining analyses that required any qualification of data. SDG 428907 For all radiological methods, sample preservation and holding times were acceptable. Instruments were acceptable calibrated. The method blank samples were acceptably free of contamination, and spiked sample recoveries were acceptable. For the strontium isotope analyses, a false positive result was suspected for sample 428907-001 (T030GL-WC04), leading to a reanalysis of the sample. The results from the reanalysis are reported. There were no problems in the radiological analyses that required any qualification of data. Please see the attached data for your use and review. Note the data has undergone a data quality assessment and evaluation for the intended purpose of characterization for disposal only. Enclosed results are Approved for Quality Assurance Release by: Albert Iannacone, August 30, 2017.

Fort Bliss Waste Characterization Samples Collected July, 2017

Sample Identification T030GL-WC-TB01 T030GL-WC01 T030GL-WC02 T030GL-WC03 T030GL03-WC-TB02 T030GL-WC04 T030GL-WC05

Lab Identification FA46145-1 FA46145-2 FA46145-3 FA46145-4 FA46136-1 FA46136-2 FA46136-3Date 7/24/2017 7/24/2017 7/24/2017 7/24/2017 7/25/2017 7/25/2017 7/25/2017Matrix Trip Blank Soil Soil Soil Soil Trip Blank Soil Soil SoilPetroleum Hydrocarbons Method SW846 8015C mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/KgTPH-GRO (C6-C10) -- 2.5 U 2.2 U 2.7 U 2.9 U 2.5 U 2.3 U 2.6 UTPH (C10-C28) -- NA 12 J 14.2 J 5.81 J NA 3.19 J 71.6 JVolatiles Method SW846 8260B ug/Kg ug/Kg ug/KgBenzene 17,800 2.0 UJ NA NA NA 2.0 U NA NA2-Butanone (MEK) 37,400,000 15 UJ NA NA NA 15 U NA NACarbon Tetrachloride 10,700 2.0 UJ NA NA NA 2.0 U NA NAChlorobenzene 378,000 2.0 UJ NA NA NA 2.0 U NA NAChloroform 5,900 2.0 UJ NA NA NA 2.0 U NA NA1,4-Dichlorobenzene 32,800 2.0 UJ NA NA NA 2.0 U NA NA1,2-Dichloroethane 8,320 2.0 UJ NA NA NA 2.0 U NA NA1,1-Dichloroethylene 440,000 2.0 UJ NA NA NA 2.0 U NA NATetrachloroethylene 111,000 2.0 UJ NA NA NA 2.0 U NA NATrichloroethylene 6,770 2.0 UJ NA NA NA 2.0 U NA NAVinyl Chloride 742 2.0 UJ NA NA NA 2.0 U NA NATCLP Volatiles Method SW846 8260B mg/L mg/L mg/L mg/L mg/L mg/LBenzene 0.5 NA 0.0153 0.0050 U 0.0050 U NA 0.0050 U 0.01042-Butanone (MEK) 200.0 NA 0.035 U 0.035 U 0.035 U NA 0.035 U 0.035 UCarbon Tetrachloride 0.5 NA 0.0050 U 0.0050 U 0.0050 U NA 0.0050 UJ 0.0050 UJChlorobenzene 100.0 NA 0.0050 U 0.0050 U 0.0050 U NA 0.0050 U 0.0050 UChloroform 6.0 NA 0.0050 U 0.0050 U 0.0050 U NA 0.0050 U 0.0050 U1,4-Dichlorobenzene 7.5 NA 0.0050 U 0.0050 U 0.0050 U NA 0.0050 U 0.0050 U1,2-Dichloroethane 0.5 NA 0.0050 U 0.0050 U 0.0050 U NA 0.0050 U 0.0050 U1,1-Dichloroethylene 0.7 NA 0.0050 U 0.0050 U 0.0050 U NA 0.0050 U 0.0050 UTetrachloroethylene 0.7 NA 0.0050 U 0.0050 U 0.0346 NA 0.0050 U 0.0299Trichloroethylene 0.5 NA 0.0050 U 0.0050 U 0.0050 U NA 0.0050 U 0.0050 UVinyl Chloride 0.2 NA 0.0050 U 0.0050 U 0.0050 U NA 0.0050 U 0.0050 UTCLP Semivolatiles Method 8SW846 8270D mg/L mg/L mg/L mg/L mg/L mg/L2-Methylphenol 200 NA 0.010 UJ 0.010 UJ 0.010 UJ NA 0.010 UJ 0.010 UJ3&4-Methylphenol 200 NA 0.020 UJ 0.020 UJ 0.020 UJ NA 0.020 UJ 0.020 UJPentachlorophenol 100 NA 0.10 UJ 0.10 UJ 0.10 UJ NA 0.10 UJ 0.10 UJ2,4,5-Trichlorophenol 400 NA 0.020 UJ 0.020 UJ 0.020 UJ NA 0.020 UJ 0.020 UJ2,4,6-Trichlorophenol 2.0 NA 0.020 UJ 0.020 UJ 0.020 UJ NA 0.020 UJ 0.020 UJ1,4-Dichlorobenzene 7.5 NA 0.020 U 0.020 U 0.020 U NA 0.020 U 0.020 U2,4-Dinitrotoluene 0.13 NA 0.010 U 0.010 U 0.010 U NA 0.010 U 0.010 UHexachlorobenzene 0.13 NA 0.010 U 0.010 U 0.010 U NA 0.010 U 0.010 UHexachlorobutadiene 0.5 NA 0.010 U 0.010 U 0.010 U NA 0.010 U 0.010 UHexachloroethane 3.0 NA 0.020 U 0.020 U 0.020 U NA 0.020 U 0.020 UNitrobenzene 2.0 NA 0.020 U 0.020 U 0.020 U NA 0.020 U 0.020 UPyridine 5.0 NA 0.035 U 0.035 U 0.035 U NA 0.035 U 0.035 UTCLP Herbicides Method SW846 8151A mg/L mg/L mg/L mg/L mg/L mg/L2,4-D 10.0 NA 0.025 UJ 0.025 UJ 0.025 UJ NA 0.025 UJ 0.025 UJ2,4,5-TP (Silvex) 1.0 NA 0.0025 U 0.0025 U 0.0025 U NA 0.0025 UJ 0.0025 UJNotes1 New Mexico Environment Department (NMED) Residential Soil Screening Levels - July 2015TCLP Limits: Title 40 Code of Federal Regulations (40 CFR) Part 261 Subpart C U - Result is not detected UJ - Result is not detected at an estimated reporting limit

Bold results indicate positively detected valueHighlighted results exceed the Regulatory Limits

Regulatory Limits

mg/L: milligrams per liter; mg/Kg: milligrams per kilogramug/Kg: micrograms per kilogram


Sample Identification T030GL-WC-TB01 T030GL-WC01 T030GL-WC02 T030GL-WC03 T030GL03-WC-TB02 T030GL-WC04 T030GL-WC05

Lab Identification FA46145-1 FA46145-2 FA46145-3 FA46145-4 FA46136-1 FA46136-2 FA46136-3Date 7/24/2017 7/24/2017 7/24/2017 7/24/2017 7/25/2017 7/25/2017 7/25/2017Matrix Trip Blank Soil Soil Soil Soil Trip Blank Soil Soil Soil

Regulatory Limits

TCLP Pesticides Method SW846 8081B mg/L mg/L mg/L mg/L mg/L mg/Lgamma-BHC (Lindane) 0.4 NA 0.000050 U 0.000050 U 0.000050 U NA 0.000050 U 0.000050 UChlordane 0.03 NA 0.00050 U 0.00050 U 0.00050 U NA 0.00050 U 0.00050 UEndrin 0.02 NA 0.000050 U 0.000050 U 0.000050 U NA 0.000050 U 0.000050 UHeptachlor 0.008 NA 0.000050 U 0.000050 U 0.000050 U NA 0.000050 U 0.000050 UHeptachlor epoxide 0.008 NA 0.000050 U 0.000050 U 0.000050 U NA 0.000050 U 0.000050 UMethoxychlor 10.0 NA 0.00010 U 0.00010 U 0.00010 U NA 0.00010 U 0.00010 UToxaphene 0.5 NA 0.0038 U 0.0038 U 0.0038 U NA 0.0038 U 0.0038 UPolychlorinated Biphenyls (PCBs ) Method SW846 8082A ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/KgAroclor 1016 3,980 NA 11 U 13 U 13 U NA 12 U 13 UAroclor 1221 1,810 NA 11 U 13 U 13 U NA 12 U 13 UAroclor 1232 1,860 NA 11 U 13 U 13 U NA 12 U 13 UAroclor 1242 2,430 NA 11 U 13 U 13 U NA 12 U 13 UAroclor 1248 2,430 NA 11 U 13 U 13 U NA 12 U 13 UAroclor 1254 1,140 NA 16 U 13 U 13 U NA 12 U 17.9 JAroclor 1260 2,430 NA 16 U 13 U 13 U NA 12 U 13 UTCLP Metals Method SW846 6010C mg/L mg/L mg/L mg/L mg/L mg/LArsenic 5.0 NA 0.050 U 0.050 U 0.050 U NA 0.050 U 0.050 UBarium 100 NA 0.57 J 0.40 J 0.63 J NA 0.53 J 0.52 JCadmium 1.0 NA 0.010 U 0.010 U 0.010 U NA 0.010 U 0.010 UChromium 5.0 NA 0.050 U 0.050 U 0.050 U NA 0.050 U 0.050 ULead 5.0 NA 0.016 J 0.77 0.020 U NA 0.020 U 0.020 USelenium 1.0 NA 0.050 U 0.050 U 0.050 U NA 0.050 U 0.050 USilver 5.0 NA 0.020 U 0.020 U 0.020 U NA 0.020 U 0.020 UTCLP Metals Method SW846 7470A mg/L mg/L mg/L mg/L mg/L mg/LMercury 0.2 NA 0.00056 J 0.00059 J 0.00055 J NA 0.00058 J 0.00062 JGeneral ChemistryCorrosivity as pH (su) <2, >12.5 NA 8.3 7.7 8.0 NA 8.4 8.0Cyanide Reactivity (mg/Kg) - NA 0.76 U 0.84 U 0.85 U NA 0.77 U 0.82 UIgnitability (Flashpoint) (Deg. F) <140 NA >200 >200 >200 NA >200 >200 Sulfide Reactivity (mg/Kg) - NA 51 U 56 U 57 U NA 52 U 54 UAsbestos Method EPA 600/R-93/116Asbestos -- NA ND ND ND NA ND NDLab Identification 428907001GFPC Gross A/B Method EPA 900.0/SW846 9310/SM 7110B Modified pCi/g

Alpha -- NA NA NA NA NA 10.5 NABeta -- NA NA NA NA NA 21.3 NAGFPC, Sr89&Sr90 Method EPA 905.0 Modified/DOE RP501 Rev 1 Modified pCi/g

Stronium-89 -- NA NA NA NA NA -0.0582U NAStronium-90 -- NA NA NA NA NA 0.239U NANotes1 New Mexico Environment Department (NMED) Residential Soil Screening Levels - July 2015TCLP Limits: Title 40 Code of Federal Regulations (40 CFR) Part 261 Subpart C ND: None Detected U - Result is not detected UJ - Result is not detected at an estimated reporting limit

pCi/g: picocuries per gramBold results indicate positively detected valueHighlighted results exceed the Regulatory Limits

ug/Kg: micrograms per kilogrammg/L: milligrams per liter; mg/Kg: milligrams per kilogram


Sample Identification

Lab IdentificationDateMatrixPetroleum Hydrocarbons Method SW846 8015CTPH-GRO (C6-C10) --TPH (C10-C28) --Volatiles Method SW846 8260B ug/KgBenzene 17,8002-Butanone (MEK) 37,400,000Carbon Tetrachloride 10,700Chlorobenzene 378,000Chloroform 5,9001,4-Dichlorobenzene 32,8001,2-Dichloroethane 8,3201,1-Dichloroethylene 440,000Tetrachloroethylene 111,000Trichloroethylene 6,770Vinyl Chloride 742TCLP Volatiles Method SW846 8260B mg/LBenzene 0.52-Butanone (MEK) 200.0Carbon Tetrachloride 0.5Chlorobenzene 100.0Chloroform 6.01,4-Dichlorobenzene 7.51,2-Dichloroethane 0.51,1-Dichloroethylene 0.7Tetrachloroethylene 0.7Trichloroethylene 0.5Vinyl Chloride 0.2TCLP Semivolatiles Method 8SW846 8270D mg/L2-Methylphenol 2003&4-Methylphenol 200Pentachlorophenol 1002,4,5-Trichlorophenol 4002,4,6-Trichlorophenol 2.01,4-Dichlorobenzene 7.52,4-Dinitrotoluene 0.13Hexachlorobenzene 0.13Hexachlorobutadiene 0.5Hexachloroethane 3.0Nitrobenzene 2.0Pyridine 5.0TCLP Herbicides Method SW846 8151A mg/L2,4-D 10.02,4,5-TP (Silvex) 1.0Notes1 New Mexico Environment Department (NMED) Residential Soil Screening Levels - July 2015TCLP Limits: Title 40 Code of Federal Regulations (40 CFR) Part 261 Subpart C U - Result is not detected UJ - Result is not detected at an estimated reporting limit


Regulatory Limits


T030GL-WC06 T030GL-WC07 T030GL-WC08 T030GL-WC09 T030GL-WC10 T030GL-WC11 T030GL-WC12

FA46136-4 FA46136-5 FA46136-6 FA46136-7 FA46136-8 FA46136-9 FA46136-107/25/2017 7/25/2017 7/25/2017 7/25/2017 7/25/2017 7/25/2017 7/25/2017

Soil Soil Soil Soil Soil Soil Soilmg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg2.6 U 2.5 U 2.5 U 3.3 U 2.3 U 2.9 U 2.3 U508 J 5.21 J 44.4 J 25.9 J 7.3 J 98.5 J 93 J

NA NA NA NA NA NA NANA NA NA NA NA NA NANA NA NA NA NA NA NANA NA NA NA NA NA NANA NA NA NA NA NA NANA NA NA NA NA NA NANA NA NA NA NA NA NANA NA NA NA NA NA NANA NA NA NA NA NA NANA NA NA NA NA NA NANA NA NA NA NA NA NA

mg/L mg/L mg/L mg/L mg/L mg/L mg/L0.0050 U 0.0050 U 0.0050 U 0.446 0.0050 U 0.0050 U 0.0050 U0.035 U 0.035 U 0.035 U 0.035 U 0.035 U 0.035 U 0.035 U

0.0050 UJ 0.0050 UJ 0.0050 UJ 0.0050 UJ 0.0050 UJ 0.0050 UJ 0.0050 UJ0.0020 J 0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U0.0050 U 0.0057 J 0.0066 J 0.0050 U 0.0050 U 0.0050 U 0.0050 U0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U

mg/L mg/L mg/L mg/L mg/L mg/L mg/L0.010 UJ 0.010 UJ 0.010 UJ 0.010 UJ 0.010 UJ 0.010 UJ 0.010 UJ0.020 UJ 0.020 UJ 0.020 UJ 0.020 UJ 0.020 UJ 0.020 UJ 0.020 UJ0.10 UJ 0.10 UJ 0.10 UJ 0.10 UJ 0.10 UJ 0.10 UJ 0.10 UJ

0.020 UJ 0.020 UJ 0.020 UJ 0.020 UJ 0.020 UJ 0.020 UJ 0.020 UJ0.020 UJ 0.020 UJ 0.020 UJ 0.020 UJ 0.020 UJ 0.020 UJ 0.020 UJ0.020 U 0.020 U 0.020 U 0.020 U 0.020 U 0.020 U 0.020 U0.010 U 0.010 U 0.010 U 0.010 U 0.010 U 0.010 U 0.010 U0.010 U 0.010 U 0.010 U 0.010 U 0.010 U 0.010 U 0.010 U0.010 U 0.010 U 0.010 U 0.010 U 0.010 U 0.010 U 0.010 U0.020 U 0.020 U 0.020 U 0.020 U 0.020 U 0.020 U 0.020 U0.020 U 0.020 U 0.020 U 0.020 U 0.020 U 0.020 U 0.020 U0.035 U 0.035 U 0.035 U 0.035 U 0.035 U 0.035 U 0.035 Umg/L mg/L mg/L mg/L mg/L mg/L mg/L

0.025 UJ 0.025 UJ 0.025 UJ 0.025 UJ 0.025 UJ 0.025 UJ 0.025 UJ0.0025 UJ 0.0025 UJ 0.0025 UJ 0.0025 UJ 0.0025 UJ 0.0025 UJ 0.0025 UJ



Lab IdentificationDateMatrix

Regulatory Limits

TCLP Pesticides Method SW846 8081B mg/Lgamma-BHC (Lindane) 0.4Chlordane 0.03Endrin 0.02Heptachlor 0.008Heptachlor epoxide 0.008Methoxychlor 10.0Toxaphene 0.5Polychlorinated Biphenyls (PCBs ) Method SW846 8082A ug/KgAroclor 1016 3,980Aroclor 1221 1,810Aroclor 1232 1,860Aroclor 1242 2,430Aroclor 1248 2,430Aroclor 1254 1,140Aroclor 1260 2,430TCLP Metals Method SW846 6010C mg/LArsenic 5.0Barium 100Cadmium 1.0Chromium 5.0Lead 5.0Selenium 1.0Silver 5.0TCLP Metals Method SW846 7470A mg/LMercury 0.2General ChemistryCorrosivity as pH (su) <2, >12.5Cyanide Reactivity (mg/Kg) -Ignitability (Flashpoint) (Deg. F) <140Sulfide Reactivity (mg/Kg) -Asbestos Method EPA 600/R-93/116Asbestos --Lab IdentificationGFPC Gross A/B Method EPA 900.0/SW846 9310/SM 7110B ModifiedAlpha --Beta --GFPC, Sr89&Sr90 Method EPA 905.0 Modified/DOE RP501 Rev 1 ModifiedStronium-89 --Stronium-90 --Notes1 New Mexico Environment Department (NMED) Residential Soil Screening Levels - July 2015TCLP Limits: Title 40 Code of Federal Regulations (40 CFR) Part 261 Subpart C ND: None Detected U - Result is not detected UJ - Result is not detected at an estimated reporting limit



T030GL-WC06 T030GL-WC07 T030GL-WC08 T030GL-WC09 T030GL-WC10 T030GL-WC11 T030GL-WC12

FA46136-4 FA46136-5 FA46136-6 FA46136-7 FA46136-8 FA46136-9 FA46136-107/25/2017 7/25/2017 7/25/2017 7/25/2017 7/25/2017 7/25/2017 7/25/2017

Soil Soil Soil Soil Soil Soil Soilmg/L mg/L mg/L mg/L mg/L mg/L mg/L

0.000050 U 0.000050 U 0.000050 U 0.000050 U 0.000050 U 0.000050 U 0.000050 U0.00050 U 0.00050 U 0.00050 U 0.00050 U 0.00050 U 0.00050 U 0.00050 U0.000050 U 0.000050 U 0.000050 U 0.000050 U 0.000050 U 0.000050 U 0.000050 U0.000050 U 0.000050 U 0.000050 U 0.000050 U 0.000050 U 0.000050 U 0.000050 U0.000050 U 0.000050 U 0.000050 U 0.000050 U 0.000050 U 0.000050 U 0.000050 U0.00010 U 0.00010 U 0.00010 U 0.00010 U 0.00010 U 0.00010 U 0.00010 U0.0038 U 0.0038 U 0.0038 U 0.0038 U 0.0038 U 0.0038 U 0.0038 U

ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg62 U 12 U 12 U 14 U 12 U 13 U 59 U62 U 12 U 12 U 14 U 12 U 13 U 59 U62 U 12 U 12 U 14 U 12 U 13 U 59 U62 U 12 U 12 U 14 U 12 U 13 U 59 U62 U 12 U 12 U 14 U 12 U 13 U 59 U105 J 22.7 12 U 12.5 J 12 U 9.5 J 59 U48.3 J 12 U 12 U 14 U 12 U 13 U 59 Umg/L mg/L mg/L mg/L mg/L mg/L mg/L

0.050 U 0.050 U 0.050 U 0.050 U 0.050 U 0.050 U 0.050 U0.61 J 0.45 J 0.56 J 0.28 J 0.52 J 0.81 J 0.57 J

0.010 U 0.010 U 0.0020 J 0.0030 J 0.0020 J 0.0020 J 0.0060 J0.012 J 0.050 U 0.050 U 0.050 U 0.050 U 0.050 U 0.050 U0.020 U 0.020 U 0.020 U 0.020 U 0.020 U 0.020 U 0.020 U0.050 U 0.050 U 0.050 U 0.050 U 0.050 U 0.050 U 0.050 U0.020 U 0.020 U 0.020 U 0.020 U 0.020 U 0.020 U 0.020 Umg/L mg/L mg/L mg/L mg/L mg/L mg/L

0.00065 J 0.00065 J 0.0010 U 0.0010 U 0.0010 U 0.0010 U 0.0010 U

8.1 7.9 8.2 8.1 8 7.1 8.00.81 U 0.79 U 0.77 U 0.92 U 0.78 U 0.86 U 0.77 U>200 >200 >200 >200 >200 >200 >200 54 U 53 U 51 U 62 U 52 U 57 U 51 U

ND ND ND ND ND ND ND428907002

pCi/g

NA NA NA NA NA NA 12.7NA NA NA NA NA NA 24.1

pCi/g

NA NA NA NA NA NA -1.32UNA NA NA NA NA NA -0.626U





Regulatory Limits


T030GL-WC13 T030GL-WC14 T030GL-WC15 T030GL-WC16 T030GL-WC-TB03 T030GL-WC17

FA46136-11 FA46136-12 FA46136-13 FA46136-14 FA46163-1 FA46163-27/25/2017 7/25/2017 7/25/2017 7/25/2017 7/26/2017 7/26/2017

Soil Soil Soil Soil Trip Blank Soil Soilmg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg2.3 U 2.6 U 2.3 U 2.2 U 2.5 U 2.4 U16.1 J 46.1 J 77.3 J 49.9 J NA 82.5 J

ug/KgNA NA NA NA 2.0 U NANA NA NA NA 15 U NANA NA NA NA 2.0 U NANA NA NA NA 2.0 U NANA NA NA NA 2.0 U NANA NA NA NA 2.0 U NANA NA NA NA 2.0 U NANA NA NA NA 2.0 U NANA NA NA NA 2.0 U NANA NA NA NA 2.0 U NANA NA NA NA 2.0 U NA

mg/L mg/L mg/L mg/L mg/L0.0050 U 0.0050 U 0.0050 U 0.298 NA 0.0050 UJ0.035 U 0.035 U 0.035 U 0.035 U NA 0.035 U

0.0050 UJ 0.0050 UJ 0.0050 UJ 0.0050 UJ NA 0.0050 U0.0050 U 0.0050 U 0.0050 U 0.0050 U NA 0.0050 U0.0050 U 0.0039 B 0.0032 B 0.0053 B NA 0.0039 B0.0050 U 0.0050 U 0.0050 U 0.0050 U NA 0.0050 U0.0050 U 0.0050 U 0.0050 U 0.0050 U NA 0.0050 U0.0050 U 0.0050 U 0.0050 U 0.0050 U NA 0.0050 U0.0050 U 0.0050 U 0.0050 U 0.0050 U NA 0.0050 UJ0.0050 U 0.0050 U 0.0050 U 0.0050 U NA 0.0050 U0.0050 U 0.0050 U 0.0050 U 0.0050 U NA 0.0050 U

mg/L mg/L mg/L mg/L mg/L0.010 UJ 0.010 UJ 0.010 UJ 0.010 UJ NA 0.010 U0.020 UJ 0.020 UJ 0.020 UJ 0.020 UJ NA 0.020 U0.10 UJ 0.10 UJ 0.10 UJ 0.10 UJ NA 0.10 U

0.020 UJ 0.020 UJ 0.020 UJ 0.020 UJ NA 0.020 UJ0.020 UJ 0.020 UJ 0.020 UJ 0.020 UJ NA 0.020 UJ0.020 U 0.020 U 0.020 U 0.020 U NA 0.020 U0.010 U 0.010 U 0.010 U 0.010 U NA 0.010 UJ0.010 U 0.010 U 0.010 U 0.010 U NA 0.010 U0.010 U 0.010 U 0.010 U 0.010 U NA 0.010 UJ0.020 U 0.020 U 0.020 U 0.020 U NA 0.020 UJ0.020 U 0.020 U 0.020 U 0.020 U NA 0.020 U0.035 U 0.035 U 0.035 U 0.035 U NA 0.035 UJmg/L mg/L mg/L mg/L mg/L

0.025 UJ 0.025 UJ 0.025 UJ 0.025 UJ NA 0.025 U0.0025 UJ 0.0025 UJ 0.0025 UJ 0.0025 UJ NA 0.0025 U




Regulatory Limits




T030GL-WC13 T030GL-WC14 T030GL-WC15 T030GL-WC16 T030GL-WC-TB03 T030GL-WC17

FA46136-11 FA46136-12 FA46136-13 FA46136-14 FA46163-1 FA46163-27/25/2017 7/25/2017 7/25/2017 7/25/2017 7/26/2017 7/26/2017

Soil Soil Soil Soil Trip Blank Soil Soilmg/L mg/L mg/L mg/L mg/L

0.000050 U 0.000050 U 0.000023 J 0.000050 U NA 0.000050 U0.00050 U 0.00050 U 0.00050 U 0.00050 U NA R0.000050 U 0.000050 U 0.000050 U 0.000050 U NA 0.000050 U0.000050 U 0.000050 U 0.000050 U 0.000050 U NA 0.000050 U0.000050 U 0.000050 U 0.000050 U 0.000050 U NA 0.000050 U0.00010 U 0.00010 U 0.00010 U 0.00010 U NA 0.00010 U 0.0038 U 0.0038 U 0.0038 U 0.0038 U NA R

ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg12 U 12 U 12 U 12 U NA 12 U12 U 12 U 12 U 12 U NA 12 U12 U 12 U 12 U 12 U NA 12 U12 U 12 U 12 U 12 U NA 12 U12 U 12 U 12 U 12 U NA 12 U54.8 12 U 12 U 12 U NA 12 U 12 U 12 U 12 U 12 U NA 12 U mg/L mg/L mg/L mg/L mg/L

0.050 U 0.050 U 0.050 U 0.050 U NA 0.050 U0.49 J 0.30 J 0.48 J 0.36 J NA 0.45 J

0.0090 J 0.0030 J 0.0060 J 0.014 J NA 0.010 U0.050 U 0.050 U 0.050 U 0.050 U NA 0.050 U0.020 U 0.020 U 0.020 U 0.020 U NA 0.500.050 U 0.050 U 0.050 U 0.050 U NA 0.050 U0.020 U 0.020 U 0.020 U 0.020 U NA 0.0080 Jmg/L mg/L mg/L mg/L mg/L

0.0010 U 0.0010 U 0.0010 U 0.0010 U NA 0.0010 U

8.0 8.5 7.9 8.0 NA 8.00.78 U 0.78 U 0.77 U 0.77 U NA 0.77 U>200 >200 >200 >200 NA >200 52 U 52 U 51 U 51 U NA 52 U

ND ND ND ND NA ND428907003

pCi/g

16.4 NA NA NA NA NA22.1 NA NA NA NA NA

pCi/g

-0.873U NA NA NA NA NA-0.655U NA NA NA NA NA





Regulatory Limits


T030GL-WC18 T030GL-WC19 T030GL-WC20 T030GL-WC21 T030GL-WC22 T030GL-WC23

FA46163-3 FA46163-4 FA46163-5 FA46163-6 FA46163-7 FA46163-87/26/2017 7/26/2017 7/26/2017 7/26/2017 7/26/2017 7/26/2017

Soil Soil Soil Soil Soil Soilmg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg2.4 U 2.4 U 2.7 U 2.2 U 2.6 U 2.4 U36.4 J 13.4 J 120 J 6.67 J 68.3 J 20.4 J

NA NA NA NA NA NANA NA NA NA NA NANA NA NA NA NA NANA NA NA NA NA NANA NA NA NA NA NANA NA NA NA NA NANA NA NA NA NA NANA NA NA NA NA NANA NA NA NA NA NANA NA NA NA NA NANA NA NA NA NA NA

mg/L mg/L mg/L mg/L mg/L mg/L0.0050 UJ 0.0050 UJ 0.0070 J 0.0050 UJ 0.231 0.0050 U0.035 U 0.035 U 0.035 U 0.035 U 0.035 U 0.035 U

0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U0.0033 B 0.0032 B 0.0031 B 0.0032 B 0.0050 U 0.0050 U0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U0.0050 UJ 0.0050 UJ 0.0050 UJ 0.0050 UJ 0.0050 U 0.0050 U0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U 0.0050 U

mg/L mg/L mg/L mg/L mg/L mg/L0.010 U 0.010 U 0.010 U 0.010 U 0.010 U 0.010 U0.020 U 0.020 U 0.020 U 0.020 U 0.020 U 0.020 U0.10 U 0.10 U 0.10 U 0.10 U 0.10 U 0.10 U

0.020 UJ 0.020 UJ 0.020 UJ 0.020 UJ 0.020 UJ 0.020 UJ0.020 UJ 0.020 UJ 0.020 UJ 0.020 UJ 0.020 UJ 0.020 UJ0.020 U 0.020 U 0.020 U 0.020 U 0.020 U 0.020 U0.010 UJ 0.010 UJ 0.010 UJ 0.010 UJ 0.010 UJ 0.010 UJ0.010 U 0.010 U 0.010 U 0.010 U 0.010 U 0.010 U0.010 UJ 0.010 UJ 0.010 UJ 0.010 UJ 0.010 UJ 0.010 UJ0.020 UJ 0.020 UJ 0.020 UJ 0.020 UJ 0.020 UJ 0.020 UJ0.020 U 0.020 U 0.020 U 0.020 U 0.020 U 0.020 U0.035 UJ 0.035 UJ 0.035 UJ 0.035 UJ 0.035 UJ 0.035 UJ

mg/L mg/L mg/L mg/L mg/L mg/L0.025 U 0.025 U 0.025 U 0.025 U 0.025 U 0.025 U

0.0025 U 0.0025 U 0.0025 U 0.0025 U 0.0025 U 0.0025 U




Regulatory Limits




T030GL-WC18 T030GL-WC19 T030GL-WC20 T030GL-WC21 T030GL-WC22 T030GL-WC23

FA46163-3 FA46163-4 FA46163-5 FA46163-6 FA46163-7 FA46163-87/26/2017 7/26/2017 7/26/2017 7/26/2017 7/26/2017 7/26/2017

Soil Soil Soil Soil Soil Soilmg/L mg/L mg/L mg/L mg/L mg/L

0.000050 U 0.000050 U 0.000050 U 0.000050 U 0.000050 U 0.000050 UR R R R R R

0.000050 U 0.000050 U 0.000050 U 0.000050 U 0.000050 U 0.000050 U0.000050 U 0.000050 U 0.000050 U 0.000050 U 0.000050 U 0.000050 U0.000050 U 0.000050 U 0.000050 U 0.000050 U 0.000050 U 0.000050 U0.00010 U 0.00010 U 0.00010 U 0.00010 U 0.00010 U 0.00010 U

R R R R R Rug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg12 U 12 U 52 U 12 U 12 U 50 U12 U 12 U 52 U 12 U 12 U 50 U12 U 12 U 52 U 12 U 12 U 50 U12 U 12 U 52 U 12 U 12 U 50 U12 U 12 U 52 U 12 U 12 U 50 U12 U 12 U 52 U 12 U 12 U 50 U 12 U 12 U 52 U 12 U 12 U 50 U mg/L mg/L mg/L mg/L mg/L mg/L

0.050 U 0.050 U 0.050 U 0.050 U 0.050 U 0.050 U0.050 U 0.58 J 0.45 J 0.050 U 0.42 J 0.39 J0.010 U 0.010 U 0.0030 J 0.010 U 0.010 U 0.010 U0.050 U 0.050 U 0.050 U 0.050 U 0.050 U 0.050 U0.020 U 0.020 U 0.020 U 0.020 U 0.020 U 0.013 J0.050 U 0.050 U 0.050 U 0.050 U 0.050 U 0.050 U0.020 U 0.020 U 0.020 U 0.0080 J 0.020 U 0.0080 Jmg/L mg/L mg/L mg/L mg/L mg/L

0.0010 U 0.0010 U 0.0020 J 0.0010 U 0.0010 U 0.0010 U

8.3 7.9 8.8 8.0 7.9 7.90.77 U 0.77 U 0.84 U 0.77 U 0.78 U 0.77 U>200 >200 >200 >200 >200 >200 52 U 51 U 56 U 52 U 52 U 52 U

ND ND ND ND ND ND

NA NA NA NA NA NANA NA NA NA NA NA

NA NA NA NA NA NANA NA NA NA NA NA

SDG FA46136

FA46136: Chain of CustodyPage 1 of 3

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FA46136

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FA46136

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Job Number: FA46136 Client: CAPE

Date / Time Received: 7/26/2017 9:15:00 AM Delivery Method: FX

Project: CORRECTIVE ACTION AT FORT BLISS

Airbill #'s: 811306952270

Cooler Information

1. Custody Seals Present

2. Custody Seals Intact

4. Cooler temp verification

3. Temp criteria achieved

5. Cooler media

IR Gun

Ice (Bag)

Trip Blank Information

1. Trip Blank present / cooler

2. Trip Blank listed on COC

2. Samples preserved properly

Sample Information

1. Sample labels present on bottles

5. Sample recvd within HT

4. Condition of sample

3. Sufficient volume/containers recvd for analysis:

Intact

Comments

SM001Rev. Date 05/24/17

SGS Accutest Sample Receipt Summary

Cooler Temps (Raw Measured) °C:

Cooler Temps (Corrected) °C:

Cooler 1: (1.8); Cooler 2: (3.4); Cooler 3: (1.7);

Cooler 1: (2.2); Cooler 2: (3.8); Cooler 3: (2.1);

3. Type Of TB Received

W or S N/A

6. Dates/Times/IDs on COC match Sample Label

7. VOCs have headspace

8. Bottles received for unspecified tests9. Compositing instructions clear

10. Voa Soil Kits/Jars received past 48hrs?

11. % Solids Jar received?

Misc. Information

25-Gram 5-GramNumber of Encores: Number of 5035 Field Kits: Number of Lab Filtered Metals:

Test Strip Lot #s: pH 0-3 230315 pH 10-12 219813A Other: (Specify)

Y or N N/A

Y or N

Therm ID: IR 1; Therm CF: 0.4; # of Coolers: 3

Y or N N/A

12. Residual Chlorine Present?

Residual Chlorine Test Strip Lot #:

Technician: Reviewer:PETERH Date:Date: 7/26/2017 9:15:00 AM


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FA46136

66.1

OrderID: 341706798

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SGS Accutest

Report of Analysis Page 1 of 1

Client Sample ID: T030GL03-WC-TB02

Lab Sample ID: FA46136-1 Date Sampled: 07/25/17

Matrix: SO - Trip Blank Soil Date Received: 07/26/17

Method: SW846 8260B Percent Solids: n/a

Project: Oro Grande, Fort Bliss, TX

File ID DF Analyzed By Prep Date Prep Batch Analytical Batch

Run #1 C0122994.D 1 07/27/17 11:55 EP n/a n/a VC4870

Run #2

Initial Weight Final Volume

Run #1 5.00 g 5.0 ml

Run #2

VOA TCLP List

CAS No. Compound Result LOQ LOD DL Units Q

71-43-2 Benzene 2.0 U 5.0 2.0 1.2 ug/kg

78-93-3 2-Butanone (MEK) 15 U 25 15 7.3 ug/kg

56-23-5 Carbon Tetrachloride 2.0 U 5.0 2.0 1.0 ug/kg

108-90-7 Chlorobenzene 2.0 U 5.0 2.0 1.0 ug/kg

67-66-3 Chloroform 2.0 U 5.0 2.0 1.3 ug/kg

106-46-7 1,4-Dichlorobenzene 2.0 U 5.0 2.0 1.2 ug/kg

107-06-2 1,2-Dichloroethane 2.0 U 5.0 2.0 1.0 ug/kg

75-35-4 1,1-Dichloroethylene 2.0 U 5.0 2.0 1.0 ug/kg

127-18-4 Tetrachloroethylene 2.0 U 5.0 2.0 1.3 ug/kg

79-01-6 Trichloroethylene 2.0 U 5.0 2.0 1.0 ug/kg

75-01-4 Vinyl Chloride 2.0 U 5.0 2.0 1.0 ug/kg

CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits

1868-53-7 Dibromofluoromethane 103% 75-124%

17060-07-0 1,2-Dichloroethane-D4 106% 72-135%

2037-26-5 Toluene-D8 94% 75-126%

460-00-4 4-Bromofluorobenzene 98% 71-133%

U = Not detected LOD = Limit of Detection J = Indicates an estimated value

LOQ = Limit of Quantitation DL = Detection Limit B = Indicates analyte found in associated method blank

E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound

Raw Data: C0122994.D

17 of 3028

FA46136

44.1

2.0U15U2.0U2.0U

2.0U2.0U2.0U2.0U2.0U2.0U2.0U

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Client Sample ID: T030GL03-WC-TB02



Method: SW846 8015C Percent Solids: n/a



Run #1 UV080582.D 1 08/03/17 17:33 AJC n/a n/a GUV4266

Run #2

Initial Weight Final Volume Methanol Aliquot

Run #1 5.00 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 2.5 U 5.0 2.5 2.5 mg/kg



98-08-8 aaa-Trifluorotoluene 92% 66-132%




Raw Data: UV080582.D

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FA46136

44.1

2.5U

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Client Sample ID: T030GL-WC04


Matrix: SO - Soil Date Received: 07/26/17

Method: SW846 8260B SW846 1311 Percent Solids: 96.5



Run #1 M97888.D 10 08/02/17 15:03 WV 07/31/17 12:30 OP66200 VM4200

Run #2

Purge Volume

Run #1 5.0 ml

Run #2

VOA TCLP List TCLP Leachate method SW846 1311

CAS No. Compound Result HW# MCL LOQ LOD DL Units Q

71-43-2 Benzene 0.0050 U D018 0.50 0.010 0.0050 0.0031 mg/l

78-93-3 2-Butanone (MEK) 0.035 U D035 200 0.050 0.035 0.020 mg/l

56-23-5 Carbon Tetrachloride 0.0050 U D019 0.50 0.010 0.0050 0.0036 mg/l

108-90-7 Chlorobenzene 0.0050 U D021 100 0.010 0.0050 0.0020 mg/l

67-66-3 Chloroform 0.0050 U D022 6.0 0.010 0.0050 0.0030 mg/l

106-46-7 1,4-Dichlorobenzene 0.0050 U D027 7.5 0.010 0.0050 0.0026 mg/l

107-06-2 1,2-Dichloroethane 0.0050 U D028 0.50 0.010 0.0050 0.0031 mg/l

75-35-4 1,1-Dichloroethylene 0.0050 U D029 0.70 0.010 0.0050 0.0032 mg/l

127-18-4 Tetrachloroethylene 0.0050 U D039 0.70 0.010 0.0050 0.0022 mg/l

79-01-6 Trichloroethylene 0.0050 U D040 0.50 0.010 0.0050 0.0035 mg/l

75-01-4 Vinyl Chloride 0.0050 U D043 0.20 0.010 0.0050 0.0041 mg/l




2037-26-5 Toluene-D8 101% 85-112%



MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank


Raw Data: M97888.D

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FA46136

44.2

0.0050U0.035U0.0050UJ

0.0050U0.0050U0.0050U

0.0050U0.0050U0.0050U

0.0050U0.0050U

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Method: SW846 8270D SW846 3510C Percent Solids: 96.5



Run #1 4D2071.D 1 08/04/17 20:18 NG 07/29/17 08:15 OP66197 S4D81

Run #2

Initial Volume Final Volume

Run #1 100 ml 1.0 ml

Run #2

ABN TCLP List TCLP Leachate method SW846 1311


95-48-7 2-Methylphenol 0.010 U D023 200 0.050 0.010 0.0056 mg/l

3&4-Methylphenol 0.020 U D024 200 0.050 0.020 0.0098 mg/l

87-86-5 Pentachlorophenol a 0.10 U D037 100 0.25 0.10 0.050 mg/l

95-95-4 2,4,5-Trichlorophenol 0.020 U D041 400 0.050 0.020 0.0074 mg/l

88-06-2 2,4,6-Trichlorophenol 0.020 U D042 2.0 0.050 0.020 0.0075 mg/l


121-14-2 2,4-Dinitrotoluene 0.010 U D030 0.13 0.050 0.010 0.0081 mg/l

118-74-1 Hexachlorobenzene 0.010 U D032 0.13 0.050 0.010 0.0069 mg/l

87-68-3 Hexachlorobutadiene 0.010 U D033 0.50 0.050 0.010 0.0050 mg/l

67-72-1 Hexachloroethane 0.020 U D034 3.0 0.050 0.020 0.016 mg/l

98-95-3 Nitrobenzene 0.020 U D036 2.0 0.050 0.020 0.0093 mg/l

110-86-1 Pyridine 0.035 U D038 5.0 0.10 0.035 0.020 mg/l


367-12-4 2-Fluorophenol 24% 14-67%

4165-62-2 Phenol-d5 14% 10-50%

118-79-6 2,4,6-Tribromophenol 74% 33-118%

4165-60-0 Nitrobenzene-d5 73% 42-108%

321-60-8 2-Fluorobiphenyl 76% 40-106%

1718-51-0 Terphenyl-d14 81% 39-121%

(a) Associated BS recovery outside control limits.




Raw Data: 4D2071.D

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FA46136

44.2

0.010 UJ0.020 UJ0.10 UJ

0.020 UJ0.020 UJ0.020 U

0.020 U0.020 U0.035 U

0.010 U0.010U0.010U

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Method: SW846 8015C Percent Solids: 96.5




Run #2


Run #1 5.87 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 2.3 U 4.6 2.3 2.3 mg/kg








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44.2

2.3 U

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Method: SW846 8151A SW846 3510C Percent Solids: 96.5



Run #1 CC055209.D 1 08/03/17 14:05 MG 07/29/17 12:30 OP66199 GCC1169

Run #2


Run #1 10.0 ml 5.0 ml

Run #2

Herbicide TCLP Leachate TCLP Leachate method SW846 1311


94-75-7 2,4-D 0.025 U D016 10 0.050 0.025 0.017 mg/l

93-72-1 2,4,5-TP (Silvex) 0.0025 U D017 1.0 0.0050 0.0025 0.0013 mg/l


19719-28-9 2,4-DCAA 50% 39-135%




Raw Data: CC055209.D

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44.2

0.025UJ0.0025UJ

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Method: SW846 8081B SW846 3510C Percent Solids: 96.5



Run #1 KK85100.D 1 08/02/17 19:14 KL 07/29/17 10:00 OP66198 GKK2709

Run #2


Run #1 100 ml 5.0 ml

Run #2

Pesticide TCLP Leachate TCLP Leachate method SW846 1311


58-89-9 gamma-BHC (Lindane) 0.000050 U D013 0.40 0.00010 0.0000500.000022mg/l

12789-03-6 Chlordane 0.00050 U D020 0.030 0.0010 0.00050 0.00038 mg/l

72-20-8 Endrin 0.000050 U D012 0.020 0.00020 0.0000500.000021mg/l

76-44-8 Heptachlor 0.000050 U D031 0.0080 0.00010 0.0000500.000026mg/l

1024-57-3 Heptachlor epoxide 0.000050 U D031 0.0080 0.00010 0.0000500.000020mg/l

72-43-5 Methoxychlor 0.00010 U D014 10 0.00020 0.00010 0.000050mg/l

8001-35-2 Toxaphene 0.0038 U D015 0.50 0.0050 0.0038 0.0021 mg/l


877-09-8 Tetrachloro-m-xylene 94% 42-127%

2051-24-3 Decachlorobiphenyl 108% 27-127%




Raw Data: KK85100.D

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FA46136

44.2

0.00005U

0.00005U0.00005U0.00005U

0.0005U

0.00010U0.0038U

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Method: SW846 8082A SW846 3546 Percent Solids: 96.5



Run #1 MM43926.D 1 07/27/17 15:35 NJ 07/27/17 07:30 OP66167 GMM840

Run #2


Run #1 15.6 g 5.0 ml

Run #2

PCB List


12674-11-2 Aroclor 1016 12 U 17 12 6.6 ug/kg

11104-28-2 Aroclor 1221 12 U 17 12 8.3 ug/kg

11141-16-5 Aroclor 1232 12 U 17 12 8.3 ug/kg

53469-21-9 Aroclor 1242 12 U 17 12 6.6 ug/kg

12672-29-6 Aroclor 1248 12 U 17 12 6.6 ug/kg

11097-69-1 Aroclor 1254 12 U 17 12 6.6 ug/kg

11096-82-5 Aroclor 1260 12 U 17 12 6.6 ug/kg







Raw Data: MM43926.D

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FA46136

44.2

12 U12 U12 U

12 U12 U

12 U12 U

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Method: SW846 8015C SW846 3546 Percent Solids: 96.5



Run #1 JJ016047.D 1 08/05/17 14:20 SJL 07/27/17 08:00 OP66168 GJJ684

Run #2


Run #1 20.5 g 1.0 ml

Run #2


TPH (C10-C28) 3.19 5.1 3.8 2.5 mg/kg J


84-15-1 o-Terphenyl 85% 56-122%




Raw Data: JJ016047.D

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FA46136

44.2

3.19 J

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Percent Solids: 96.5


Metals Analysis, TCLP Leachate SW846 1311

Analyte Result HW# MCL LOQ LOD DL Units DF Prep Analyzed By Method

Arsenic 0.050 U D004 5.0 0.10 0.050 0.013 mg/l 1 07/28/17 07/28/17 LM SW846 6010C 1

Barium 0.53 J D005 100 2.0 0.050 0.050 mg/l 1 07/28/17 07/28/17 LM SW846 6010C 1

Cadmium 0.010 U D006 1.0 0.050 0.010 0.0020 mg/l 1 07/28/17 07/28/17 LM SW846 6010C 1

Chromium 0.050 U D007 5.0 0.10 0.050 0.010 mg/l 1 07/28/17 07/28/17 LM SW846 6010C 1

Lead 0.020 U D008 5.0 0.050 0.020 0.011 mg/l 1 07/28/17 07/28/17 LM SW846 6010C 1

Mercury 0.00058 J D009 0.20 0.0050 0.0010 0.00050 mg/l 1 07/31/17 07/31/17 JL SW846 7470A 2

Selenium 0.050 U D010 1.0 0.10 0.050 0.029 mg/l 1 07/28/17 07/28/17 LM SW846 6010C 1

Silver 0.020 U D011 5.0 0.10 0.020 0.0070 mg/l 1 07/28/17 07/28/17 LM SW846 6010C 1

(1) Instrument QC Batch: MA14256


(3) Prep QC Batch: MP32514


LOQ = Limit of Quantitation DL = Detection Limit U = Indicates a result < LOD

LOD = Limit of Detection B = Analyte found in associated blank J = Indicates a result >= DL (MDL) but < LOQ

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44.2

0.050 U

0.050 U0.050 U

0.050 U

0.020 U

0.050 U

0.53 J

0.00058 J

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General Chemistry

Analyte Result LOQ LOD DL Units DF Analyzed By Method

Corrosivity as pH 8.4 su 1 08/04/17 19:30 ZC SW846 CHAP7

Cyanide Reactivity 0.77 U 1.6 0.77 a 0.77 mg/kg 1 08/02/17 16:05 KH SW846 CHAP7

Ignitability (Flashpoint) b >200 Deg. F 1 07/27/17 12:30 KH SW846 1010

Solids, Percent 96.5 % 1 07/26/17 22:47 ZC SM19 2540G

Sulfide Reactivity 52 U 52 52 a 52 mg/kg 1 07/28/17 10:52 CH SW846 CHAP7

(a) Value reported is laboratory DL (MDL).

(b) Not ignitable.



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44.2

>200

96.5

52 U

0.77 U

8.4

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Run #1 M97890.D 10 08/02/17 15:53 WV 07/31/17 12:30 OP66200 VM4200

Run #2

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Run #2



71-43-2 Benzene 0.0104 D018 0.50 0.010 0.0050 0.0031 mg/l








127-18-4 Tetrachloroethylene 0.0299 D039 0.70 0.010 0.0050 0.0022 mg/l






2037-26-5 Toluene-D8 100% 85-112%





Raw Data: M97890.D

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44.3

0.0050 UJ0.0050 U0.0050 U

0.0050 U0.0050 U

0.0050 U0.02990.0050 U0.0050 U

0.01040.035 U

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Run #1 4D2073.D 1 08/04/17 21:15 NG 07/29/17 08:15 OP66197 S4D81

Run #2


Run #1 100 ml 1.0 ml

Run #2



95-48-7 2-Methylphenol 0.010 U D023 200 0.050 0.010 0.0056 mg/l3&4-Methylphenol 0.020 U D024 200 0.050 0.020 0.0098 mg/l










110-86-1 Pyridine 0.035 U D038 5.0 0.10 0.035 0.020 mg/l


367-12-4 2-Fluorophenol 25% 14-67%

4165-62-2 Phenol-d5 16% 10-50%

118-79-6 2,4,6-Tribromophenol 71% 33-118%

4165-60-0 Nitrobenzene-d5 67% 42-108%

321-60-8 2-Fluorobiphenyl 69% 40-106%

1718-51-0 Terphenyl-d14 83% 39-121%





Raw Data: 4D2073.D

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44.3

0.010 UJ

0.10 UJ

0.010 U

0.010 U0.010 U

0.020 UJ

0.020 U

0.020 U

0.020 U

0.020 UJ0.020 UJ

0.035 U

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Run #2


Run #1 5.68 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 2.6 U 5.2 2.6 2.6 mg/kg








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44.3

2.6 U

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Run #1 CC055211.D 1 08/03/17 14:37 MG 07/29/17 12:30 OP66199 GCC1169

Run #2


Run #1 10.0 ml 5.0 ml

Run #2



94-75-7 2,4-D 0.025 U D016 10 0.050 0.025 0.017 mg/l

93-72-1 2,4,5-TP (Silvex) 0.0025 U D017 1.0 0.0050 0.0025 0.0013 mg/l


19719-28-9 2,4-DCAA 77% 39-135%





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FA46136

44.3

0.025UJ

0.0025UJ

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Run #1 KK85102.D 1 08/02/17 19:49 KL 07/29/17 10:00 OP66198 GKK2709

Run #2


Run #1 100 ml 5.0 ml

Run #2




12789-03-6 Chlordane 0.00050 U D020 0.030 0.0010 0.00050 0.00038 mg/l

72-20-8 Endrin 0.000050 U D012 0.020 0.00020 0.0000500.000021mg/l




8001-35-2 Toxaphene 0.0038 U D015 0.50 0.0050 0.0038 0.0021 mg/l







Raw Data: KK85102.D

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FA46136

44.3

0.00005U

0.00005U

0.00005U0.00005U

0.0005U

0.00010U0.0038U

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Run #1 a MM43927.D 1 07/27/17 15:47 NJ 07/27/17 07:30 OP66167 GMM840

Run #2


Run #1 15.1 g 5.0 ml

Run #2

PCB List


12674-11-2 Aroclor 1016 13 U 18 13 7.2 ug/kg

11104-28-2 Aroclor 1221 13 U 18 13 9.0 ug/kg

11141-16-5 Aroclor 1232 13 U 18 13 9.0 ug/kg

53469-21-9 Aroclor 1242 13 U 18 13 7.2 ug/kg

12672-29-6 Aroclor 1248 13 U 18 13 7.2 ug/kg

11097-69-1 Aroclor 1254 17.9 18 13 7.2 ug/kg J

11096-82-5 Aroclor 1260 13 U 18 13 7.2 ug/kg




(a) All hits confirmed by dual column analysis.




Raw Data: MM43927.D

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FA46136

44.3

13 U13 U

13 U

13 U13 U13 U17.9J

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Run #1 JJ016048.D 5 08/05/17 14:49 SJL 07/27/17 08:00 OP66168 GJJ684

Run #2


Run #1 20.1 g 1.0 ml

Run #2


TPH (C10-C28) 71.6 27 20 14 mg/kg


84-15-1 o-Terphenyl 93% 56-122%





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FA46136

44.3

71.6 J

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Lead 0.020 U D008 5.0 0.050 0.020 0.011 mg/l 1 07/28/17 07/28/17 LM SW846 6010C 1










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44.3

0.050 U

0.050 U

0.050 U

0.020 U

0.020 U

0.010 U

0.00062 J

0.52 J

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General Chemistry


Corrosivity as pH 8.0 su 1 08/04/17 19:30 ZC SW846 CHAP7Cyanide Reactivity 0.82 U 1.6 0.82 a 0.82 mg/kg 1 08/02/17 16:05 KH SW846 CHAP7Ignitability (Flashpoint) b >200 Deg. F 1 07/27/17 12:30 KH SW846 1010Solids, Percent 91.9 % 1 07/26/17 22:47 ZC SM19 2540GSulfide Reactivity 54 U 54 54 a 54 mg/kg 1 07/28/17 10:52 CH SW846 CHAP7


(b) Not ignitable.



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44.3

>200

91.9

54 U

0.82 U

8.0

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Run #1 M97891.D 10 08/02/17 16:17 WV 07/31/17 12:30 OP66200 VM4200

Run #2

Purge Volume

Run #1 5.0 ml

Run #2



71-43-2 Benzene 0.0050 U D018 0.50 0.010 0.0050 0.0031 mg/l



108-90-7 Chlorobenzene 0.0020 D021 100 0.010 0.0050 0.0020 mg/l J











2037-26-5 Toluene-D8 100% 85-112%





Raw Data: M97891.D

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FA46136

44.4

0.0050 U0.035

0.0050 UJ0.0020 J0.0050 U0.0050 U

0.0050 U0.0050 U

0.0050 U0.0050 U0.0050 U

aiannacone

Stamp

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

SGS Accutest








Run #1 4D2074.D 1 08/04/17 21:43 NG 07/29/17 08:15 OP66197 S4D81

Run #2


Run #1 100 ml 1.0 ml

Run #2














110-86-1 Pyridine 0.035 U D038 5.0 0.10 0.035 0.020 mg/l


367-12-4 2-Fluorophenol 26% 14-67%

4165-62-2 Phenol-d5 17% 10-50%

118-79-6 2,4,6-Tribromophenol 75% 33-118%

4165-60-0 Nitrobenzene-d5 69% 42-108%

321-60-8 2-Fluorobiphenyl 75% 40-106%

1718-51-0 Terphenyl-d14 84% 39-121%





Raw Data: 4D2074.D

38 of 3028

FA46136

44.4

0.010 UJ

0.020 U

0.020 U

0.020 U0.035 U

0.10 UJ

0.010 U0.010 U0.010 U

0.020 UJ

0.020 UJ0.020 UJ

aiannacone

Stamp

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

SGS Accutest









Run #2


Run #1 5.85 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 2.6 U 5.1 2.6 2.6 mg/kg








39 of 3028

FA46136

44.4

2.6 U

aiannacone

Stamp

aiannacone

Cross-Out

SGS Accutest








Run #1 CC055212.D 1 08/03/17 14:53 MG 07/29/17 12:30 OP66199 GCC1169

Run #2


Run #1 10.0 ml 5.0 ml

Run #2



94-75-7 2,4-D 0.025 U D016 10 0.050 0.025 0.017 mg/l

93-72-1 2,4,5-TP (Silvex) 0.0025 U D017 1.0 0.0050 0.0025 0.0013 mg/l


19719-28-9 2,4-DCAA 64% 39-135%





40 of 3028

FA46136

44.4

0.025UJ0.0025UJ

aiannacone

Stamp

aiannacone

Cross-Out

aiannacone

Cross-Out

SGS Accutest








Run #1 KK85103.D 1 08/02/17 20:06 KL 07/29/17 10:00 OP66198 GKK2709

Run #2


Run #1 100 ml 5.0 ml

Run #2




12789-03-6 Chlordane 0.00050 U D020 0.030 0.0010 0.00050 0.00038 mg/l

72-20-8 Endrin 0.000050 U D012 0.020 0.00020 0.0000500.000021mg/l




8001-35-2 Toxaphene 0.0038 U D015 0.50 0.0050 0.0038 0.0021 mg/l







Raw Data: KK85103.D

41 of 3028

FA46136

44.4

0.00005U

0.00005U0.00005U0.00005U0.00010U0.0038U

0.00050U

aiannacone

Stamp

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

SGS Accutest








Run #1 a MM43928.D 5 07/27/17 15:58 NJ 07/27/17 07:30 OP66167 GMM840

Run #2


Run #1 15.3 g 5.0 ml

Run #2

PCB List


12674-11-2 Aroclor 1016 62 U 89 62 36 ug/kg

11104-28-2 Aroclor 1221 62 U 89 62 44 ug/kg

11141-16-5 Aroclor 1232 62 U 89 62 44 ug/kg

53469-21-9 Aroclor 1242 62 U 89 62 36 ug/kg

12672-29-6 Aroclor 1248 62 U 89 62 36 ug/kg

11097-69-1 Aroclor 1254 b 105 89 62 36 ug/kg J

11096-82-5 Aroclor 1260 b 48.3 89 62 36 ug/kg J




(a) All hits confirmed by dual column analysis. Dilution required due to matrix interference.

(b) Estimated value due to the presence of multiple overlapping Aroclor patterns.




Raw Data: MM43928.D

42 of 3028

FA46136

44.4

62 U

62 U62 U

62 U

62 U

105 J48.3 J

aiannacone

Stamp

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

SGS Accutest








Run #1 JJ016049.D 20 08/05/17 15:18 SJL 07/27/17 08:00 OP66168 GJJ684

Run #2


Run #1 20.2 g 1.0 ml

Run #2


TPH (C10-C28) 508 110 81 54 mg/kg


84-15-1 o-Terphenyl 0% a 56-122%

(a) Outside control limits due to dilution.





43 of 3028

FA46136

44.4

508 J

aiannacone

Stamp

aiannacone

Cross-Out

SGS Accutest












Chromium 0.012 J D007 5.0 0.10 0.050 0.010 mg/l 1 07/28/17 07/28/17 LM SW846 6010C 1

Lead 0.020 U D008 5.0 0.050 0.020 0.011 mg/l 1 07/28/17 07/28/17 LM SW846 6010C 1










44 of 3028

FA46136

44.4

0.050 U

0.050 U0.020 U

0.61 J0.010 U0.012 J

0.020 U0.00065J

aiannacone

Stamp

aiannacone

Line

aiannacone

Line

SGS Accutest







General Chemistry








(b) Not ignitable.



45 of 3028

FA46136

44.4

>200

91.8

54 U

0.81 U

8.1

aiannacone

Stamp

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 M97892.D 10 08/02/17 16:42 WV 07/31/17 12:30 OP66200 VM4200

Run #2

Purge Volume

Run #1 5.0 ml

Run #2



71-43-2 Benzene 0.0050 U D018 0.50 0.010 0.0050 0.0031 mg/l









79-01-6 Trichloroethylene 0.0057 D040 0.50 0.010 0.0050 0.0035 mg/l J





2037-26-5 Toluene-D8 100% 85-112%





Raw Data: M97892.D

46 of 3028

FA46136

44.5

0.0050 U0.035 U0.0050 UJ

0.0050 U0.0050 U0.0050 U

0.0050 U

0.0050 U0.0050 U0.0050 U0.0057 J

aiannacone

Stamp

aiannacone

Line

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 4D2075.D 1 08/04/17 22:11 NG 07/29/17 08:15 OP66197 S4D81

Run #2


Run #1 100 ml 1.0 ml

Run #2














110-86-1 Pyridine 0.035 U D038 5.0 0.10 0.035 0.020 mg/l


367-12-4 2-Fluorophenol 27% 14-67%

4165-62-2 Phenol-d5 18% 10-50%

118-79-6 2,4,6-Tribromophenol 81% 33-118%

4165-60-0 Nitrobenzene-d5 80% 42-108%

321-60-8 2-Fluorobiphenyl 82% 40-106%

1718-51-0 Terphenyl-d14 92% 39-121%





Raw Data: 4D2075.D

47 of 3028

FA46136

44.5

0.010 UJ0.020 UJ0.10 UJ

0.020 UJ0.020 UJ0.020 U0.010 U0.010 U0.010 U

0.020 U0.020 U0.035 U

aiannacone

Stamp

aiannacone

Line

aiannacone

Line

SGS Accutest









Run #2


Run #1 5.76 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 2.5 U 4.9 2.5 2.5 mg/kg








48 of 3028

FA46136

44.5

2.5 U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 CC055213.D 1 08/03/17 15:09 MG 07/29/17 12:30 OP66199 GCC1169

Run #2


Run #1 10.0 ml 5.0 ml

Run #2



94-75-7 2,4-D 0.025 U D016 10 0.050 0.025 0.017 mg/l

93-72-1 2,4,5-TP (Silvex) 0.0025 U D017 1.0 0.0050 0.0025 0.0013 mg/l


19719-28-9 2,4-DCAA 47% 39-135%





49 of 3028

FA46136

44.5

0.025UJ0.0025UJ

aiannacone

Stamp

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 KK85104.D 1 08/02/17 20:23 KL 07/29/17 10:00 OP66198 GKK2709

Run #2


Run #1 100 ml 5.0 ml

Run #2




12789-03-6 Chlordane 0.00050 U D020 0.030 0.0010 0.00050 0.00038 mg/l

72-20-8 Endrin 0.000050 U D012 0.020 0.00020 0.0000500.000021mg/l




8001-35-2 Toxaphene 0.0038 U D015 0.50 0.0050 0.0038 0.0021 mg/l







Raw Data: KK85104.D

50 of 3028

FA46136

44.5

0.00005 U

0.0005 U0.00005 U0.00005 U0.00005 U

0.00010 U0.0038 U

aiannacone

Stamp

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 a MM43929.D 1 07/27/17 16:10 NJ 07/27/17 07:30 OP66167 GMM840

Run #2


Run #1 15.2 g 5.0 ml

Run #2

PCB List


12674-11-2 Aroclor 1016 12 U 17 12 7.0 ug/kg

11104-28-2 Aroclor 1221 12 U 17 12 8.7 ug/kg

11141-16-5 Aroclor 1232 12 U 17 12 8.7 ug/kg

53469-21-9 Aroclor 1242 12 U 17 12 7.0 ug/kg

12672-29-6 Aroclor 1248 12 U 17 12 7.0 ug/kg

11097-69-1 Aroclor 1254 22.7 17 12 7.0 ug/kg

11096-82-5 Aroclor 1260 12 U 17 12 7.0 ug/kg








Raw Data: MM43929.D

51 of 3028

FA46136

44.5

12 U12 U12 U12 U12 U22.712 U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 WW11628.D 1 08/09/17 11:05 SJL 07/27/17 08:00 OP66168 GWW495

Run #2


Run #1 20.1 g 1.0 ml

Run #2


TPH (C10-C28) 5.21 5.3 4.0 2.6 mg/kg J


84-15-1 o-Terphenyl 107% 56-122%




Raw Data: WW11628.D

52 of 3028

FA46136

44.5

5.21 J

aiannacone

Stamp

aiannacone

Line

aiannacone

Line

SGS Accutest













Lead 0.020 U D008 5.0 0.050 0.020 0.011 mg/l 1 07/28/17 07/28/17 LM SW846 6010C 1










53 of 3028

FA46136

44.5

0.050 U0.45 J0.010 U0.050 U0.020 U0.00065J0.050 U0.020 U

aiannacone

Stamp

aiannacone

Line

aiannacone

Line

aiannacone

Cross-Out

SGS Accutest







General Chemistry




(b) Not ignitable.



54 of 3028

FA46136

44.5

>200

94.2

53 U

7.90.79 U

aiannacone

Stamp

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 M97893.D 10 08/02/17 17:06 WV 07/31/17 12:30 OP66200 VM4200

Run #2

Purge Volume

Run #1 5.0 ml

Run #2



71-43-2 Benzene 0.0050 U D018 0.50 0.010 0.0050 0.0031 mg/l









79-01-6 Trichloroethylene 0.0066 D040 0.50 0.010 0.0050 0.0035 mg/l J





2037-26-5 Toluene-D8 99% 85-112%





Raw Data: M97893.D

55 of 3028

FA46136

44.6

0.0050 U0.035 U

0.0050UJ

0.0050 U0.0050 U 0.0050 U0.0050 U 0.0050 U

0.0050 U0.0066 J0.0050 U

aiannacone

Stamp

aiannacone

Line

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 7G00156.D 1 08/08/17 20:05 NG 08/01/17 13:00 OP66232 S7G11

Run #2


Run #1 100 ml 1.0 ml

Run #2



95-48-7 2-Methylphenol 0.010 U D023 200 0.050 0.010 0.0056 mg/l3&4-Methylphenol 0.020 U D024 200 0.050 0.020 0.0098 mg/l

87-86-5 Pentachlorophenol 0.10 U D037 100 0.25 0.10 0.050 mg/l









110-86-1 Pyridine 0.035 U D038 5.0 0.10 0.035 0.020 mg/l


367-12-4 2-Fluorophenol 23% 14-67%

4165-62-2 Phenol-d5 12% 10-50%

118-79-6 2,4,6-Tribromophenol 105% 33-118%

4165-60-0 Nitrobenzene-d5 84% 42-108%

321-60-8 2-Fluorobiphenyl 90% 40-106%

1718-51-0 Terphenyl-d14 99% 39-121%




Raw Data: 7G00156.D

56 of 3028

FA46136

44.6

0.010 UJ0.020 UJ0.10 UJ

0.020 UJ0.020 UJ0.020 U

0.010 U0.010 U0.010 U0.020 U0.020 U0.035 U

aiannacone

Stamp

aiannacone

Line

SGS Accutest









Run #2


Run #1 5.15 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 2.5 U 5.1 2.5 2.5 mg/kg








57 of 3028

FA46136

44.6

2.5 U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 CC055224.D 1 08/03/17 18:05 MG 08/01/17 15:20 OP66234 GCC1169Run #2


Run #1 10.0 ml 5.0 ml

Run #2



94-75-7 2,4-D 0.025 U D016 10 0.050 0.025 0.017 mg/l

93-72-1 2,4,5-TP (Silvex) 0.0025 U D017 1.0 0.0050 0.0025 0.0013 mg/l


19719-28-9 2,4-DCAA 52% 39-135%





58 of 3028

FA46136

44.6

0.025 UJ0.0025 UJ

aiannacone

Stamp

aiannacone

Cross-Out

aiannacone

Cross-Out

SGS Accutest








Run #1 KK85181.D 1 08/08/17 14:53 KL 08/01/17 12:30 OP66233 GKK2713

Run #2


Run #1 100 ml 5.0 ml

Run #2




12789-03-6 Chlordane 0.00050 U D020 0.030 0.0010 0.00050 0.00038 mg/l

72-20-8 Endrin 0.000050 U D012 0.020 0.00020 0.0000500.000021mg/l




8001-35-2 Toxaphene 0.0038 U D015 0.50 0.0050 0.0038 0.0021 mg/l







Raw Data: KK85181.D

59 of 3028

FA46136

44.6

0.000050 U

0.00050 U0.000050 U

0.000050 U 0.000050U0.00010 U0.0038 U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 MM43930.D 1 07/27/17 16:22 NJ 07/27/17 07:30 OP66167 GMM840

Run #2


Run #1 15.1 g 5.0 ml

Run #2

PCB List


12674-11-2 Aroclor 1016 12 U 17 12 6.8 ug/kg

11104-28-2 Aroclor 1221 12 U 17 12 8.5 ug/kg

11141-16-5 Aroclor 1232 12 U 17 12 8.5 ug/kg

53469-21-9 Aroclor 1242 12 U 17 12 6.8 ug/kg

12672-29-6 Aroclor 1248 12 U 17 12 6.8 ug/kg

11097-69-1 Aroclor 1254 12 U 17 12 6.8 ug/kg

11096-82-5 Aroclor 1260 12 U 17 12 6.8 ug/kg







Raw Data: MM43930.D

60 of 3028

FA46136

44.6

12 U12 U12 U12 U12 U12 U12 U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 WW11629.D 1 08/09/17 11:34 SJL 07/27/17 08:00 OP66168 GWW495

Run #2


Run #1 20.2 g 1.0 ml

Run #2


TPH (C10-C28) a 44.4 5.1 3.8 2.5 mg/kg


84-15-1 o-Terphenyl 88% 56-122%

(a) Petroleum hydrocarbon pattern extends beyond C28.




Raw Data: WW11629.D

61 of 3028

FA46136

44.6

aiannacone

Stamp

aiannacone

Typewritten Text

44.4 J

aiannacone

Line

SGS Accutest











Cadmium 0.0020 J D006 1.0 0.050 0.010 0.0020 mg/l 1 08/01/17 08/01/17 LM SW846 6010C 2


Lead 0.020 U D008 5.0 0.050 0.020 0.011 mg/l 1 08/01/17 08/01/17 LM SW846 6010C 2

Mercury 0.0010 U D009 0.20 0.0050 0.0010 0.00050 mg/l 1 08/01/17 08/01/17 JL SW846 7470A 1









62 of 3028

FA46136

44.6

aiannacone

Stamp

aiannacone

Typewritten Text

0.050U 0.56J

aiannacone

Typewritten Text

0.0020J

aiannacone

Typewritten Text

0.050U

aiannacone

Typewritten Text

0.050 U

aiannacone

Typewritten Text

0.020 U

aiannacone

Typewritten Text

0.0010 U

aiannacone

Typewritten Text

0.020 U

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

SGS Accutest







General Chemistry








(b) Not ignitable.



63 of 3028

FA46136

44.6

>200

97.7

51 U

0.77 U

8.2

aiannacone

Stamp

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 M97894.D 10 08/02/17 17:29 WV 07/31/17 12:30 OP66200 VM4200

Run #2

Purge Volume

Run #1 5.0 ml

Run #2



71-43-2 Benzene 0.446 D018 0.50 0.010 0.0050 0.0031 mg/l














2037-26-5 Toluene-D8 97% 85-112%





Raw Data: M97894.D

64 of 3028

FA46136

44.7

aiannacone

Stamp

aiannacone

Typewritten Text

0.446

aiannacone

Typewritten Text

0.035 U

aiannacone

Typewritten Text

0.0050 UJ

aiannacone

Typewritten Text

0.0050 U

aiannacone

Line

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 7G00159.D 1 08/08/17 22:04 NG 08/01/17 13:00 OP66232 S7G11

Run #2


Run #1 100 ml 1.0 ml

Run #2














110-86-1 Pyridine 0.035 U D038 5.0 0.10 0.035 0.020 mg/l


367-12-4 2-Fluorophenol 21% 14-67%

4165-62-2 Phenol-d5 12% 10-50%

118-79-6 2,4,6-Tribromophenol 93% 33-118%

4165-60-0 Nitrobenzene-d5 76% 42-108%

321-60-8 2-Fluorobiphenyl 80% 40-106%

1718-51-0 Terphenyl-d14 90% 39-121%




Raw Data: 7G00159.D

65 of 3028

FA46136

44.7

aiannacone

Stamp

aiannacone

Typewritten Text

0.010 UJ 0.020 UJ 0.10 UJ

aiannacone

Typewritten Text

0.020UJ 0.020UJ 0.020U

aiannacone

Typewritten Text

0.010U 0.010U 0.010U

aiannacone

Typewritten Text

0.020U 0.020U 0.035U

aiannacone

Line

SGS Accutest









Run #2


Run #1 5.74 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 3.3 U 6.6 3.3 3.3 mg/kg








66 of 3028

FA46136

44.7

aiannacone

Stamp

aiannacone

Line

aiannacone

Typewritten Text

3.3 U

SGS Accutest








Run #1 CC055229.D 1 08/03/17 19:24 MG 08/01/17 15:20 OP66234 GCC1169

Run #2


Run #1 10.0 ml 5.0 ml

Run #2



94-75-7 2,4-D 0.025 U D016 10 0.050 0.025 0.017 mg/l

93-72-1 2,4,5-TP (Silvex) 0.0025 U D017 1.0 0.0050 0.0025 0.0013 mg/l


19719-28-9 2,4-DCAA 42% 39-135%





67 of 3028

FA46136

44.7

0.025 UJ0.0025 UJ

aiannacone

Stamp

aiannacone

Cross-Out

aiannacone

Cross-Out

SGS Accutest








Run #1 KK85184.D 1 08/08/17 15:45 KL 08/01/17 12:30 OP66233 GKK2713

Run #2


Run #1 100 ml 5.0 ml

Run #2




12789-03-6 Chlordane 0.00050 U D020 0.030 0.0010 0.00050 0.00038 mg/l

72-20-8 Endrin 0.000050 U D012 0.020 0.00020 0.0000500.000021mg/l




8001-35-2 Toxaphene 0.0038 U D015 0.50 0.0050 0.0038 0.0021 mg/l







Raw Data: KK85184.D

68 of 3028

FA46136

44.7

aiannacone

Stamp

aiannacone

Typewritten Text

0.000050 U

aiannacone

Typewritten Text

0.00050 U

aiannacone

Typewritten Text

0.000050 U

aiannacone

Typewritten Text

0.00010 U

aiannacone

Typewritten Text

0.0038 U

aiannacone

Line

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 a MM43937.D 1 07/27/17 17:43 NJ 07/27/17 07:30 OP66167 GMM840

Run #2


Run #1 15.4 g 5.0 ml

Run #2

PCB List


12674-11-2 Aroclor 1016 14 U 20 14 8.1 ug/kg

11104-28-2 Aroclor 1221 14 U 20 14 10 ug/kg

11141-16-5 Aroclor 1232 14 U 20 14 10 ug/kg

53469-21-9 Aroclor 1242 14 U 20 14 8.1 ug/kg

12672-29-6 Aroclor 1248 14 U 20 14 8.1 ug/kg

11097-69-1 Aroclor 1254 12.5 20 14 8.1 ug/kg J

11096-82-5 Aroclor 1260 14 U 20 14 8.1 ug/kg








Raw Data: MM43937.D

69 of 3028

FA46136

44.7

14 U14 U14 U14 U14 U12.5 J14 U

aiannacone

Stamp

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 WW11630.D 1 08/09/17 12:02 SJL 07/27/17 08:00 OP66168 GWW495

Run #2


Run #1 20.7 g 1.0 ml

Run #2


TPH (C10-C28) a 25.9 6.0 4.5 3.0 mg/kg


84-15-1 o-Terphenyl 120% 56-122%





Raw Data: WW11630.D

70 of 3028

FA46136

44.7

25.9 J

aiannacone

Stamp

aiannacone

Line

SGS Accutest













Lead 0.020 U D008 5.0 0.050 0.020 0.011 mg/l 1 08/01/17 08/01/17 LM SW846 6010C 2










71 of 3028

FA46136

44.7

aiannacone

Stamp

aiannacone

Typewritten Text

0.050 U

aiannacone

Typewritten Text

0.28 J

aiannacone

Typewritten Text

0.0030 J

aiannacone

Typewritten Text

0.050 U

aiannacone

Typewritten Text

0.020 U

aiannacone

Typewritten Text

0.0010 U

aiannacone

Typewritten Text

0.050 U

aiannacone

Typewritten Text

0.020 U

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

SGS Accutest







General Chemistry




(b) Not ignitable.



72 of 3028

FA46136

44.7

>200

80.6

62 U

8.10.92 U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 M97895.D 10 08/02/17 17:54 WV 07/31/17 12:30 OP66200 VM4200

Run #2

Purge Volume

Run #1 5.0 ml

Run #2



71-43-2 Benzene 0.0050 U D018 0.50 0.010 0.0050 0.0031 mg/l














2037-26-5 Toluene-D8 100% 85-112%





Raw Data: M97895.D

73 of 3028

FA46136

44.8

aiannacone

Stamp

aiannacone

Typewritten Text

0.0050 U

aiannacone

Typewritten Text

0.035 U

aiannacone

Typewritten Text

0.0050 UJ

aiannacone

Typewritten Text

0.0050 U

aiannacone

Line

SGS Accutest








Run #1 7G00160.D 1 08/08/17 22:43 NG 08/01/17 13:00 OP66232 S7G11

Run #2


Run #1 100 ml 1.0 ml

Run #2














110-86-1 Pyridine 0.035 U D038 5.0 0.10 0.035 0.020 mg/l


367-12-4 2-Fluorophenol 23% 14-67%

4165-62-2 Phenol-d5 13% 10-50%

118-79-6 2,4,6-Tribromophenol 98% 33-118%

4165-60-0 Nitrobenzene-d5 80% 42-108%

321-60-8 2-Fluorobiphenyl 86% 40-106%

1718-51-0 Terphenyl-d14 93% 39-121%




Raw Data: 7G00160.D

74 of 3028

FA46136

44.8

0.010UJ0.020UJ0.10UJ0.020UJ0.020UJ0.020 U0.010 U0.010 U0.010 U0.020 U0.020 U0.035 U

aiannacone

Stamp

aiannacone

Line

aiannacone

Line

SGS Accutest









Run #2


Run #1 5.97 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 2.3 U 4.6 2.3 2.3 mg/kg








75 of 3028

FA46136

44.8

2.3 U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 CC055230.D 1 08/03/17 19:40 MG 08/01/17 15:20 OP66234 GCC1169

Run #2


Run #1 10.0 ml 5.0 ml

Run #2



94-75-7 2,4-D 0.025 U D016 10 0.050 0.025 0.017 mg/l

93-72-1 2,4,5-TP (Silvex) 0.0025 U D017 1.0 0.0050 0.0025 0.0013 mg/l


19719-28-9 2,4-DCAA 50% 39-135%





76 of 3028

FA46136

44.8

0.025 UJ0.0025 UJ

aiannacone

Stamp

aiannacone

Cross-Out

aiannacone

Cross-Out

SGS Accutest








Run #1 KK85185.D 1 08/08/17 16:03 KL 08/01/17 12:30 OP66233 GKK2713

Run #2


Run #1 100 ml 5.0 ml

Run #2




12789-03-6 Chlordane 0.00050 U D020 0.030 0.0010 0.00050 0.00038 mg/l

72-20-8 Endrin 0.000050 U D012 0.020 0.00020 0.0000500.000021mg/l




8001-35-2 Toxaphene 0.0038 U D015 0.50 0.0050 0.0038 0.0021 mg/l







Raw Data: KK85185.D

77 of 3028

FA46136

44.8

aiannacone

Stamp

aiannacone

Typewritten Text

0.000050 U

aiannacone

Typewritten Text

0.00050 U

aiannacone

Typewritten Text

0.000050 U

aiannacone

Typewritten Text

0.000050 U

aiannacone

Typewritten Text

0.000050 U

aiannacone

Typewritten Text

0.00010 U

aiannacone

Typewritten Text

0.0038 U

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 MM43938.D 1 07/27/17 17:55 NJ 07/27/17 07:30 OP66167 GMM840

Run #2


Run #1 15.6 g 5.0 ml

Run #2

PCB List


12674-11-2 Aroclor 1016 12 U 17 12 6.7 ug/kg

11104-28-2 Aroclor 1221 12 U 17 12 8.4 ug/kg

11141-16-5 Aroclor 1232 12 U 17 12 8.4 ug/kg

53469-21-9 Aroclor 1242 12 U 17 12 6.7 ug/kg

12672-29-6 Aroclor 1248 12 U 17 12 6.7 ug/kg

11097-69-1 Aroclor 1254 12 U 17 12 6.7 ug/kg

11096-82-5 Aroclor 1260 12 U 17 12 6.7 ug/kg







Raw Data: MM43938.D

78 of 3028

FA46136

44.8

12 U12 U12 U12 U12 U12 U12 U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 WW11631.D 1 08/09/17 12:31 SJL 07/27/17 08:00 OP66168 GWW495

Run #2


Run #1 20.5 g 1.0 ml

Run #2


TPH (C10-C28) a 7.30 5.1 3.8 2.5 mg/kg


84-15-1 o-Terphenyl 100% 56-122%





Raw Data: WW11631.D

79 of 3028

FA46136

44.8

7.30 J

aiannacone

Stamp

aiannacone

Line

SGS Accutest













Lead 0.020 U D008 5.0 0.050 0.020 0.011 mg/l 1 08/01/17 08/01/17 LM SW846 6010C 2










80 of 3028

FA46136

44.8

aiannacone

Stamp

aiannacone

Typewritten Text

0.050 U

aiannacone

Typewritten Text

0.52 J

aiannacone

Typewritten Text

0.0020 J

aiannacone

Typewritten Text

0.050 U

aiannacone

Typewritten Text

0.020 U

aiannacone

Typewritten Text

0.0010 U

aiannacone

Typewritten Text

0.050 U

aiannacone

Typewritten Text

0.020 U

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

SGS Accutest







General Chemistry








(b) Not ignitable.



81 of 3028

FA46136

44.8

>200

95.9

52 U

8.00.78U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 M97896.D 10 08/02/17 18:18 WV 07/31/17 12:30 OP66200 VM4200

Run #2

Purge Volume

Run #1 5.0 ml

Run #2



71-43-2 Benzene 0.0050 U D018 0.50 0.010 0.0050 0.0031 mg/l














2037-26-5 Toluene-D8 100% 85-112%





Raw Data: M97896.D

82 of 3028

FA46136

44.9

aiannacone

Stamp

aiannacone

Typewritten Text

0.0050 U

aiannacone

Typewritten Text

0.035 U

aiannacone

Typewritten Text

0.0050 UJ

aiannacone

Typewritten Text

0.0050 U

aiannacone

Line

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 7G00161.D 1 08/08/17 23:22 NG 08/01/17 13:00 OP66232 S7G11

Run #2


Run #1 100 ml 1.0 ml

Run #2














110-86-1 Pyridine 0.035 U D038 5.0 0.10 0.035 0.020 mg/l


367-12-4 2-Fluorophenol 20% 14-67%

4165-62-2 Phenol-d5 11% 10-50%

118-79-6 2,4,6-Tribromophenol 101% 33-118%

4165-60-0 Nitrobenzene-d5 80% 42-108%

321-60-8 2-Fluorobiphenyl 85% 40-106%

1718-51-0 Terphenyl-d14 99% 39-121%




Raw Data: 7G00161.D

83 of 3028

FA46136

44.9

0.020U

aiannacone

Stamp

aiannacone

Typewritten Text

0.010UJ

aiannacone

Typewritten Text

0.020UJ

aiannacone

Typewritten Text

0.10UJ

aiannacone

Typewritten Text

0.020UJ 0.020UJ

aiannacone

Typewritten Text

0.010 U

aiannacone

Typewritten Text

0.020 U

aiannacone

Typewritten Text

0.035 U

aiannacone

Line

aiannacone

Line

aiannacone

Line

SGS Accutest









Run #2


Run #1 5.75 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 2.9 U 5.7 2.9 2.9 mg/kg








84 of 3028

FA46136

44.9

2.9 U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 CC055231.D 1 08/03/17 19:56 MG 08/01/17 15:20 OP66234 GCC1169

Run #2


Run #1 10.0 ml 5.0 ml

Run #2



94-75-7 2,4-D 0.025 U D016 10 0.050 0.025 0.017 mg/l

93-72-1 2,4,5-TP (Silvex) 0.0025 U D017 1.0 0.0050 0.0025 0.0013 mg/l


19719-28-9 2,4-DCAA 45% 39-135%





85 of 3028

FA46136

44.9

0.025 UJ0.0025 UJ

aiannacone

Stamp

aiannacone

Cross-Out

aiannacone

Cross-Out

SGS Accutest








Run #1 KK85186.D 1 08/08/17 16:20 KL 08/01/17 12:30 OP66233 GKK2713

Run #2


Run #1 100 ml 5.0 ml

Run #2




12789-03-6 Chlordane 0.00050 U D020 0.030 0.0010 0.00050 0.00038 mg/l

72-20-8 Endrin 0.000050 U D012 0.020 0.00020 0.0000500.000021mg/l




8001-35-2 Toxaphene 0.0038 U D015 0.50 0.0050 0.0038 0.0021 mg/l







Raw Data: KK85186.D

86 of 3028

FA46136

44.9

aiannacone

Stamp

aiannacone

Typewritten Text

0.000050 U

aiannacone

Typewritten Text

0.00050 U

aiannacone

Typewritten Text

0.000050 U

aiannacone

Typewritten Text

0.00010 U

aiannacone

Typewritten Text

0.0038 U

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 a MM43970.D 1 07/31/17 12:00 NJ 07/27/17 07:30 OP66167 GMM841

Run #2


Run #1 15.7 g 5.0 ml

Run #2

PCB List


12674-11-2 Aroclor 1016 13 U 18 13 7.3 ug/kg

11104-28-2 Aroclor 1221 13 U 18 13 9.1 ug/kg

11141-16-5 Aroclor 1232 13 U 18 13 9.1 ug/kg

53469-21-9 Aroclor 1242 13 U 18 13 7.3 ug/kg

12672-29-6 Aroclor 1248 13 U 18 13 7.3 ug/kg

11097-69-1 Aroclor 1254 9.5 18 13 7.3 ug/kg J

11096-82-5 Aroclor 1260 13 U 18 13 7.3 ug/kg








Raw Data: MM43970.D

87 of 3028

FA46136

44.9

13 U13 U13 U13 U13 U9.5 J13 U

aiannacone

Stamp

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 WW11632.D 4 08/09/17 13:00 SJL 07/27/17 08:00 OP66168 GWW495

Run #2


Run #1 20.3 g 1.0 ml

Run #2


TPH (C10-C28) a 98.5 23 17 11 mg/kg


84-15-1 o-Terphenyl 108% 56-122%





Raw Data: WW11632.D

88 of 3028

FA46136

44.9

9.85 J

aiannacone

Stamp

aiannacone

Line

SGS Accutest













Lead 0.020 U D008 5.0 0.050 0.020 0.011 mg/l 1 08/01/17 08/01/17 LM SW846 6010C 2










89 of 3028

FA46136

44.9

aiannacone

Stamp

aiannacone

Typewritten Text

0.050 U

aiannacone

Typewritten Text

0.81 J

aiannacone

Typewritten Text

0.0020J

aiannacone

Typewritten Text

0.050U

aiannacone

Typewritten Text

0.020 U

aiannacone

Typewritten Text

0.0010U

aiannacone

Typewritten Text

0.050 U

aiannacone

Typewritten Text

0.020 U

aiannacone

Line

aiannacone

Line

SGS Accutest







General Chemistry








(b) Not ignitable.



90 of 3028

FA46136

44.9

>200

87.1

57 U

7.10.86U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 M97897.D 10 08/02/17 18:42 WV 07/31/17 12:30 OP66200 VM4200

Run #2

Purge Volume

Run #1 5.0 ml

Run #2



71-43-2 Benzene 0.0050 U D018 0.50 0.010 0.0050 0.0031 mg/l














2037-26-5 Toluene-D8 102% 85-112%





Raw Data: M97897.D

91 of 3028

FA46136

44.10

aiannacone

Stamp

aiannacone

Typewritten Text

0.0050 U

aiannacone

Typewritten Text

0.035 U

aiannacone

Typewritten Text

0.0050UJ

aiannacone

Typewritten Text

0.0050 U

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 7G00162.D 1 08/09/17 00:00 NG 08/01/17 13:00 OP66232 S7G11

Run #2


Run #1 100 ml 1.0 ml

Run #2














110-86-1 Pyridine 0.035 U D038 5.0 0.10 0.035 0.020 mg/l


367-12-4 2-Fluorophenol 24% 14-67%

4165-62-2 Phenol-d5 13% 10-50%

118-79-6 2,4,6-Tribromophenol 106% 33-118%

4165-60-0 Nitrobenzene-d5 87% 42-108%

321-60-8 2-Fluorobiphenyl 91% 40-106%

1718-51-0 Terphenyl-d14 100% 39-121%




Raw Data: 7G00162.D

92 of 3028

FA46136

44.10

0.020U

aiannacone

Stamp

aiannacone

Typewritten Text

0.010UJ

aiannacone

Typewritten Text

0.020UJ

aiannacone

Typewritten Text

0.10UJ

aiannacone

Typewritten Text

0.020UJ 0.020UJ

aiannacone

Typewritten Text

0.010 U

aiannacone

Typewritten Text

0.020 U

aiannacone

Typewritten Text

0.035 U

aiannacone

Line

aiannacone

Line

aiannacone

Line

SGS Accutest









Run #2


Run #1 5.79 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 2.3 U 4.5 2.3 2.3 mg/kg








93 of 3028

FA46136

44.10

2.3 U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 CC055232.D 1 08/03/17 20:12 MG 08/01/17 15:20 OP66234 GCC1169

Run #2


Run #1 10.0 ml 5.0 ml

Run #2



94-75-7 2,4-D 0.025 U D016 10 0.050 0.025 0.017 mg/l

93-72-1 2,4,5-TP (Silvex) 0.0025 U D017 1.0 0.0050 0.0025 0.0013 mg/l


19719-28-9 2,4-DCAA 41% 39-135%





94 of 3028

FA46136

44.10

0.025 UJ0.0025 UJ

aiannacone

Stamp

aiannacone

Cross-Out

aiannacone

Cross-Out

SGS Accutest








Run #1 KK85187.D 1 08/08/17 16:37 KL 08/01/17 12:30 OP66233 GKK2713

Run #2


Run #1 100 ml 5.0 ml

Run #2




12789-03-6 Chlordane 0.00050 U D020 0.030 0.0010 0.00050 0.00038 mg/l

72-20-8 Endrin 0.000050 U D012 0.020 0.00020 0.0000500.000021mg/l




8001-35-2 Toxaphene 0.0038 U D015 0.50 0.0050 0.0038 0.0021 mg/l







Raw Data: KK85187.D

95 of 3028

FA46136

44.10

aiannacone

Stamp

aiannacone

Typewritten Text

0.000050 U

aiannacone

Typewritten Text

0.00050 U

aiannacone

Typewritten Text

0.000050 U

aiannacone

Typewritten Text

0.00010 U

aiannacone

Typewritten Text

0.0038 U

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 a MM43940.D 5 07/27/17 18:18 NJ 07/27/17 07:30 OP66167 GMM840

Run #2


Run #1 15.1 g 5.0 ml

Run #2

PCB List


12674-11-2 Aroclor 1016 59 U 85 59 34 ug/kg

11104-28-2 Aroclor 1221 59 U 85 59 42 ug/kg

11141-16-5 Aroclor 1232 59 U 85 59 42 ug/kg

53469-21-9 Aroclor 1242 59 U 85 59 34 ug/kg

12672-29-6 Aroclor 1248 59 U 85 59 34 ug/kg

11097-69-1 Aroclor 1254 59 U 85 59 34 ug/kg

11096-82-5 Aroclor 1260 59 U 85 59 34 ug/kg




(a) Dilution required due to matrix interference.




Raw Data: MM43940.D

96 of 3028

FA46136

44.10

59 U59 U59 U59 U59 U59 U59 U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 WW11633.D 4 08/09/17 13:29 SJL 07/27/17 08:00 OP66168 GWW495

Run #2


Run #1 20.6 g 1.0 ml

Run #2


TPH (C10-C28) a 93.0 20 15 9.9 mg/kg


84-15-1 o-Terphenyl 99% 56-122%





Raw Data: WW11633.D

97 of 3028

FA46136

44.10

93.0 J

aiannacone

Stamp

aiannacone

Line

SGS Accutest













Lead 0.020 U D008 5.0 0.050 0.020 0.011 mg/l 1 08/01/17 08/01/17 LM SW846 6010C 2










98 of 3028

FA46136

44.10

aiannacone

Stamp

aiannacone

Typewritten Text

0.050 U

aiannacone

Typewritten Text

0.57 J

aiannacone

Typewritten Text

0.0060 J

aiannacone

Typewritten Text

0.050 U

aiannacone

Typewritten Text

0.020 U

aiannacone

Typewritten Text

0.0010 U

aiannacone

Typewritten Text

0.050 U

aiannacone

Typewritten Text

0.020 U

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

SGS Accutest







General Chemistry








(b) Not ignitable.



99 of 3028

FA46136

44.10

>200

97.6

51 U

8.00.77U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 M97898.D 10 08/02/17 19:05 WV 07/31/17 12:30 OP66200 VM4200

Run #2

Purge Volume

Run #1 5.0 ml

Run #2



71-43-2 Benzene 0.0050 U D018 0.50 0.010 0.0050 0.0031 mg/l














2037-26-5 Toluene-D8 100% 85-112%





Raw Data: M97898.D

100 of 3028

FA46136

44.11

aiannacone

Stamp

aiannacone

Typewritten Text

0.0050 U

aiannacone

Typewritten Text

0.035 U

aiannacone

Typewritten Text

0.0050UJ

aiannacone

Typewritten Text

0.0050 U

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 7G00163.D 1 08/09/17 00:38 NG 08/01/17 13:00 OP66232 S7G11

Run #2


Run #1 100 ml 1.0 ml

Run #2














110-86-1 Pyridine 0.035 U D038 5.0 0.10 0.035 0.020 mg/l


367-12-4 2-Fluorophenol 21% 14-67%

4165-62-2 Phenol-d5 12% 10-50%

118-79-6 2,4,6-Tribromophenol 97% 33-118%

4165-60-0 Nitrobenzene-d5 80% 42-108%

321-60-8 2-Fluorobiphenyl 85% 40-106%

1718-51-0 Terphenyl-d14 92% 39-121%




Raw Data: 7G00163.D

101 of 3028

FA46136

44.11

0.020U

aiannacone

Stamp

aiannacone

Typewritten Text

0.010UJ

aiannacone

Typewritten Text

0.020UJ

aiannacone

Typewritten Text

0.10UJ

aiannacone

Typewritten Text

0.020UJ 0.020UJ

aiannacone

Typewritten Text

0.010 U

aiannacone

Typewritten Text

0.020 U

aiannacone

Typewritten Text

0.035 U

aiannacone

Line

aiannacone

Line

aiannacone

Line

SGS Accutest









Run #2


Run #1 6.05 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 2.3 U 4.6 2.3 2.3 mg/kg








102 of 3028

FA46136

44.11

2.3 U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 CC055233.D 1 08/03/17 20:27 MG 08/01/17 15:20 OP66234 GCC1169

Run #2


Run #1 10.0 ml 5.0 ml

Run #2



94-75-7 2,4-D 0.025 U D016 10 0.050 0.025 0.017 mg/l

93-72-1 2,4,5-TP (Silvex) 0.0025 U D017 1.0 0.0050 0.0025 0.0013 mg/l


19719-28-9 2,4-DCAA 42% 39-135%





103 of 3028

FA46136

44.11

0.025 UJ0.0025 UJ

aiannacone

Stamp

aiannacone

Cross-Out

aiannacone

Cross-Out

SGS Accutest








Run #1 KK85190.D 1 08/08/17 17:30 KL 08/01/17 12:30 OP66233 GKK2713

Run #2


Run #1 100 ml 5.0 ml

Run #2




12789-03-6 Chlordane 0.00050 U D020 0.030 0.0010 0.00050 0.00038 mg/l

72-20-8 Endrin 0.000050 U D012 0.020 0.00020 0.0000500.000021mg/l




8001-35-2 Toxaphene 0.0038 U D015 0.50 0.0050 0.0038 0.0021 mg/l







Raw Data: KK85190.D

104 of 3028

FA46136

44.11

aiannacone

Stamp

aiannacone

Typewritten Text

0.000050 U

aiannacone

Typewritten Text

0.00050 U

aiannacone

Typewritten Text

0.000050 U

aiannacone

Typewritten Text

0.00010 U

aiannacone

Typewritten Text

0.0038 U

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 a MM43943.D 1 07/27/17 18:54 NJ 07/27/17 07:30 OP66167 GMM840

Run #2


Run #1 15.2 g 5.0 ml

Run #2

PCB List


12674-11-2 Aroclor 1016 12 U 17 12 6.9 ug/kg

11104-28-2 Aroclor 1221 12 U 17 12 8.6 ug/kg

11141-16-5 Aroclor 1232 12 U 17 12 8.6 ug/kg

53469-21-9 Aroclor 1242 12 U 17 12 6.9 ug/kg

12672-29-6 Aroclor 1248 12 U 17 12 6.9 ug/kg

11097-69-1 Aroclor 1254 54.8 17 12 6.9 ug/kg

11096-82-5 Aroclor 1260 12 U 17 12 6.9 ug/kg








Raw Data: MM43943.D

105 of 3028

FA46136

44.11

12 U12 U12 U12 U12 U54.812 U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 JJ016058.D 1 08/05/17 19:39 SJL 07/27/17 08:00 OP66168 GJJ684

Run #2


Run #1 20.4 g 1.0 ml

Run #2


TPH (C10-C28) 16.1 5.1 3.9 2.6 mg/kg


84-15-1 o-Terphenyl 95% 56-122%





106 of 3028

FA46136

44.11

16.1 J

aiannacone

Stamp

aiannacone

Line

SGS Accutest













Lead 0.020 U D008 5.0 0.050 0.020 0.011 mg/l 1 08/01/17 08/01/17 LM SW846 6010C 2










107 of 3028

FA46136

44.11

aiannacone

Stamp

aiannacone

Typewritten Text

0.050U

aiannacone

Typewritten Text

0.49 J

aiannacone

Typewritten Text

0.0090J

aiannacone

Typewritten Text

0.050U

aiannacone

Typewritten Text

0.020U

aiannacone

Typewritten Text

0.0010U

aiannacone

Typewritten Text

0.050U

aiannacone

Typewritten Text

0.020U

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

SGS Accutest







General Chemistry








(b) Not ignitable.



108 of 3028

FA46136

44.11

>200

95.3

52 U

8.00.78U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 J0985836.D 10 08/04/17 13:51 DP 08/02/17 14:00 OP66240 VJ5682

Run #2

Purge Volume

Run #1 5.0 ml

Run #2



71-43-2 Benzene 0.0050 U D018 0.50 0.010 0.0050 0.0031 mg/l




67-66-3 Chloroform 0.0039 D022 6.0 0.010 0.0050 0.0030 mg/l JB










2037-26-5 Toluene-D8 99% 85-112%





Raw Data: J0985836.D

109 of 3028

FA46136

44.12

aiannacone

Stamp

aiannacone

Typewritten Text

0.0050 U

aiannacone

Typewritten Text

0.035 U

aiannacone

Typewritten Text

0.0050UJ

aiannacone

Typewritten Text

0.0050 U

aiannacone

Typewritten Text

0.0039 B

aiannacone

Typewritten Text

0.0050 U

aiannacone

Line

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 7G00164.D 1 08/09/17 01:16 NG 08/01/17 13:00 OP66232 S7G11

Run #2


Run #1 100 ml 1.0 ml

Run #2














110-86-1 Pyridine 0.035 U D038 5.0 0.10 0.035 0.020 mg/l


367-12-4 2-Fluorophenol 23% 14-67%

4165-62-2 Phenol-d5 13% 10-50%

118-79-6 2,4,6-Tribromophenol 92% 33-118%

4165-60-0 Nitrobenzene-d5 78% 42-108%

321-60-8 2-Fluorobiphenyl 81% 40-106%

1718-51-0 Terphenyl-d14 88% 39-121%




Raw Data: 7G00164.D

110 of 3028

FA46136

44.12

0.020U

aiannacone

Stamp

aiannacone

Typewritten Text

0.010UJ

aiannacone

Typewritten Text

0.020UJ

aiannacone

Typewritten Text

0.10UJ

aiannacone

Typewritten Text

0.020UJ 0.020UJ

aiannacone

Typewritten Text

0.010 U

aiannacone

Typewritten Text

0.020 U

aiannacone

Typewritten Text

0.035 U

aiannacone

Line

aiannacone

Line

aiannacone

Line

SGS Accutest









Run #2


Run #1 5.31 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 2.6 U 5.1 2.6 2.6 mg/kg








111 of 3028

FA46136

44.12

2.6 U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 CC055234.D 1 08/03/17 20:43 MG 08/01/17 15:20 OP66234 GCC1169

Run #2


Run #1 10.0 ml 5.0 ml

Run #2



94-75-7 2,4-D 0.025 U D016 10 0.050 0.025 0.017 mg/l

93-72-1 2,4,5-TP (Silvex) 0.0025 U D017 1.0 0.0050 0.0025 0.0013 mg/l


19719-28-9 2,4-DCAA 46% 39-135%





112 of 3028

FA46136

44.12

0.025 UJ0.0025 UJ

aiannacone

Stamp

aiannacone

Cross-Out

aiannacone

Cross-Out

SGS Accutest








Run #1 KK85191.D 1 08/08/17 17:47 KL 08/01/17 12:30 OP66233 GKK2713

Run #2


Run #1 100 ml 5.0 ml

Run #2




12789-03-6 Chlordane 0.00050 U D020 0.030 0.0010 0.00050 0.00038 mg/l

72-20-8 Endrin 0.000050 U D012 0.020 0.00020 0.0000500.000021mg/l




8001-35-2 Toxaphene 0.0038 U D015 0.50 0.0050 0.0038 0.0021 mg/l







Raw Data: KK85191.D

113 of 3028

FA46136

44.12

aiannacone

Stamp

aiannacone

Typewritten Text

0.000050 U

aiannacone

Typewritten Text

0.00050 U

aiannacone

Typewritten Text

0.000050 U

aiannacone

Typewritten Text

0.00010 U

aiannacone

Typewritten Text

0.0030 U

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 MM43944.D 1 07/27/17 19:05 NJ 07/27/17 07:30 OP66167 GMM840

Run #2


Run #1 15.4 g 5.0 ml

Run #2

PCB List


12674-11-2 Aroclor 1016 12 U 17 12 6.8 ug/kg

11104-28-2 Aroclor 1221 12 U 17 12 8.4 ug/kg

11141-16-5 Aroclor 1232 12 U 17 12 8.4 ug/kg

53469-21-9 Aroclor 1242 12 U 17 12 6.8 ug/kg

12672-29-6 Aroclor 1248 12 U 17 12 6.8 ug/kg

11097-69-1 Aroclor 1254 12 U 17 12 6.8 ug/kg

11096-82-5 Aroclor 1260 12 U 17 12 6.8 ug/kg







Raw Data: MM43944.D

114 of 3028

FA46136

44.12

12 U12 U12 U12 U12 U12 U12 U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 JJ016059.D 1 08/05/17 20:07 SJL 07/27/17 08:00 OP66168 GJJ684

Run #2


Run #1 20.1 g 1.0 ml

Run #2


TPH (C10-C28) 46.1 5.2 3.9 2.6 mg/kg


84-15-1 o-Terphenyl 120% 56-122%





115 of 3028

FA46136

44.12

46.1 J

aiannacone

Stamp

aiannacone

Line

SGS Accutest













Lead 0.020 U D008 5.0 0.050 0.020 0.011 mg/l 1 08/01/17 08/01/17 LM SW846 6010C 2










116 of 3028

FA46136

44.12

aiannacone

Stamp

aiannacone

Line

aiannacone

Typewritten Text

0.050U

aiannacone

Typewritten Text

0.30J

aiannacone

Typewritten Text

0.0030J

aiannacone

Typewritten Text

0.050U

aiannacone

Typewritten Text

0.020U

aiannacone

Typewritten Text

0.0010U

aiannacone

Typewritten Text

0.050U

aiannacone

Typewritten Text

0/020U

SGS Accutest







General Chemistry








(b) Not ignitable.



117 of 3028

FA46136

44.12

>200

96.1

52 U

8.50.78U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 J0985838.D 10 08/04/17 14:38 DP 08/02/17 14:00 OP66240 VJ5682

Run #2

Purge Volume

Run #1 5.0 ml

Run #2



71-43-2 Benzene 0.0050 U D018 0.50 0.010 0.0050 0.0031 mg/l














2037-26-5 Toluene-D8 99% 85-112%






118 of 3028

FA46136

44.13

aiannacone

Stamp

aiannacone

Typewritten Text

0.0050 U

aiannacone

Typewritten Text

0.035 U

aiannacone

Typewritten Text

0.0050UJ

aiannacone

Typewritten Text

0.0050 U

aiannacone

Typewritten Text

0.0032 B

aiannacone

Typewritten Text

0.0050 U

aiannacone

Line

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 7G00165.D 1 08/09/17 01:53 NG 08/01/17 13:00 OP66232 S7G11

Run #2


Run #1 100 ml 1.0 ml

Run #2














110-86-1 Pyridine 0.035 U D038 5.0 0.10 0.035 0.020 mg/l


367-12-4 2-Fluorophenol 22% 14-67%

4165-62-2 Phenol-d5 12% 10-50%

118-79-6 2,4,6-Tribromophenol 100% 33-118%

4165-60-0 Nitrobenzene-d5 82% 42-108%

321-60-8 2-Fluorobiphenyl 90% 40-106%

1718-51-0 Terphenyl-d14 90% 39-121%




Raw Data: 7G00165.D

119 of 3028

FA46136

44.13

0.020U

aiannacone

Stamp

aiannacone

Typewritten Text

0.010UJ

aiannacone

Typewritten Text

0.020UJ

aiannacone

Typewritten Text

0.10UJ

aiannacone

Typewritten Text

0.020UJ 0.020UJ

aiannacone

Typewritten Text

0.010 U

aiannacone

Typewritten Text

0.020 U

aiannacone

Typewritten Text

0.035 U

aiannacone

Line

aiannacone

Line

aiannacone

Line

SGS Accutest









Run #2


Run #1 5.73 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 2.3 U 4.7 2.3 2.3 mg/kg








120 of 3028

FA46136

44.13

2.3 U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 CC055235.D 1 08/03/17 20:59 MG 08/01/17 15:20 OP66234 GCC1169

Run #2


Run #1 10.0 ml 5.0 ml

Run #2



94-75-7 2,4-D 0.025 U D016 10 0.050 0.025 0.017 mg/l

93-72-1 2,4,5-TP (Silvex) 0.0025 U D017 1.0 0.0050 0.0025 0.0013 mg/l


19719-28-9 2,4-DCAA 40% 39-135%





121 of 3028

FA46136

44.13

0.025 UJ0.0025 UJ

aiannacone

Stamp

aiannacone

Cross-Out

aiannacone

Cross-Out

SGS Accutest








Run #1 a KK85192.D 1 08/08/17 18:04 KL 08/01/17 12:30 OP66233 GKK2713

Run #2


Run #1 100 ml 5.0 ml

Run #2



58-89-9 gamma-BHC (Lindane) b 0.000023 D013 0.40 0.00010 0.0000500.000022mg/l J

12789-03-6 Chlordane 0.00050 U D020 0.030 0.0010 0.00050 0.00038 mg/l

72-20-8 Endrin 0.000050 U D012 0.020 0.00020 0.0000500.000021mg/l




8001-35-2 Toxaphene 0.0038 U D015 0.50 0.0050 0.0038 0.0021 mg/l





(b) Primary and confirmation results differ by more than 40%. Lower value reported due to possible coelution.




Raw Data: KK85192.D

122 of 3028

FA46136

44.13

aiannacone

Stamp

aiannacone

Typewritten Text

0.000023 J

aiannacone

Typewritten Text

0.00050 U

aiannacone

Typewritten Text

0.000050 U

aiannacone

Typewritten Text

0.00010 U

aiannacone

Typewritten Text

0.0038 U

aiannacone

Line

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 MM43945.D 1 07/27/17 19:17 NJ 07/27/17 07:30 OP66167 GMM840

Run #2


Run #1 15.2 g 5.0 ml

Run #2

PCB List


12674-11-2 Aroclor 1016 12 U 17 12 6.8 ug/kg

11104-28-2 Aroclor 1221 12 U 17 12 8.5 ug/kg

11141-16-5 Aroclor 1232 12 U 17 12 8.5 ug/kg

53469-21-9 Aroclor 1242 12 U 17 12 6.8 ug/kg

12672-29-6 Aroclor 1248 12 U 17 12 6.8 ug/kg

11097-69-1 Aroclor 1254 12 U 17 12 6.8 ug/kg

11096-82-5 Aroclor 1260 12 U 17 12 6.8 ug/kg







Raw Data: MM43945.D

123 of 3028

FA46136

44.13

12 U12 U12 U12 U12 U12 U12 U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 JJ016060.D 1 08/05/17 20:36 SJL 07/27/17 08:00 OP66168 GJJ684

Run #2


Run #1 20.8 g 1.0 ml

Run #2


TPH (C10-C28) 77.3 5.0 3.7 2.5 mg/kg


84-15-1 o-Terphenyl 110% 56-122%





124 of 3028

FA46136

44.13

77.3 J

aiannacone

Stamp

aiannacone

Line

SGS Accutest













Lead 0.020 U D008 5.0 0.050 0.020 0.011 mg/l 1 08/01/17 08/01/17 LM SW846 6010C 2










125 of 3028

FA46136

44.13

aiannacone

Stamp

aiannacone

Typewritten Text

0.050 U

aiannacone

Typewritten Text

0.48 J

aiannacone

Typewritten Text

0.0060J

aiannacone

Typewritten Text

0.050U

aiannacone

Typewritten Text

0.020U

aiannacone

Typewritten Text

0.0010U

aiannacone

Typewritten Text

0.050U

aiannacone

Typewritten Text

0.020U

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

aiannacone

Cross-Out

SGS Accutest







General Chemistry








(b) Not ignitable.



126 of 3028

FA46136

44.13

>200

96.7

51 U

7.90.77U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 J0985839.D 10 08/04/17 15:02 DP 08/02/17 14:00 OP66240 VJ5682

Run #2

Purge Volume

Run #1 5.0 ml

Run #2



71-43-2 Benzene 0.298 D018 0.50 0.010 0.0050 0.0031 mg/l














2037-26-5 Toluene-D8 98% 85-112%






127 of 3028

FA46136

44.14

aiannacone

Stamp

aiannacone

Typewritten Text

0.298

aiannacone

Typewritten Text

0.035 U

aiannacone

Typewritten Text

0.0050UJ

aiannacone

Typewritten Text

0.0050 U

aiannacone

Typewritten Text

0.0053 B

aiannacone

Typewritten Text

0.0050 U

aiannacone

Line

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 7G00167.D 1 08/09/17 03:07 NG 08/01/17 13:00 OP66232 S7G11

Run #2


Run #1 100 ml 1.0 ml

Run #2














110-86-1 Pyridine 0.035 U D038 5.0 0.10 0.035 0.020 mg/l


367-12-4 2-Fluorophenol 23% 14-67%

4165-62-2 Phenol-d5 13% 10-50%

118-79-6 2,4,6-Tribromophenol 96% 33-118%

4165-60-0 Nitrobenzene-d5 81% 42-108%

321-60-8 2-Fluorobiphenyl 87% 40-106%

1718-51-0 Terphenyl-d14 92% 39-121%




Raw Data: 7G00167.D

128 of 3028

FA46136

44.14

0.020U

aiannacone

Stamp

aiannacone

Typewritten Text

0.010UJ

aiannacone

Typewritten Text

0.020UJ

aiannacone

Typewritten Text

0.10UJ

aiannacone

Typewritten Text

0.020UJ 0.020UJ

aiannacone

Typewritten Text

0.010 U

aiannacone

Typewritten Text

0.020 U

aiannacone

Typewritten Text

0.035 U

aiannacone

Line

aiannacone

Line

aiannacone

Line

SGS Accutest









Run #2


Run #1 6.14 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 2.2 U 4.3 2.2 2.2 mg/kg








129 of 3028

FA46136

44.14

2.2 U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 CC055237.D 1 08/03/17 21:31 MG 08/01/17 15:20 OP66234 GCC1169

Run #2


Run #1 10.0 ml 5.0 ml

Run #2



94-75-7 2,4-D 0.025 U D016 10 0.050 0.025 0.017 mg/l

93-72-1 2,4,5-TP (Silvex) 0.0025 U D017 1.0 0.0050 0.0025 0.0013 mg/l


19719-28-9 2,4-DCAA 39% 39-135%





130 of 3028

FA46136

44.14

0.025 UJ0.0025 UJ

aiannacone

Stamp

aiannacone

Cross-Out

aiannacone

Cross-Out

SGS Accutest








Run #1 KK85194.D 1 08/08/17 18:39 KL 08/01/17 12:30 OP66233 GKK2713

Run #2


Run #1 100 ml 5.0 ml

Run #2




12789-03-6 Chlordane 0.00050 U D020 0.030 0.0010 0.00050 0.00038 mg/l

72-20-8 Endrin 0.000050 U D012 0.020 0.00020 0.0000500.000021mg/l




8001-35-2 Toxaphene 0.0038 U D015 0.50 0.0050 0.0038 0.0021 mg/l







Raw Data: KK85194.D

131 of 3028

FA46136

44.14

aiannacone

Stamp

aiannacone

Typewritten Text

0.000050 U

aiannacone

Typewritten Text

0.00050 U

aiannacone

Typewritten Text

0.000050 U

aiannacone

Typewritten Text

0.00010 U

aiannacone

Typewritten Text

0.0038 U

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 MM43946.D 1 07/27/17 19:29 NJ 07/27/17 07:30 OP66167 GMM840

Run #2


Run #1 15.3 g 5.0 ml

Run #2

PCB List


12674-11-2 Aroclor 1016 12 U 17 12 6.7 ug/kg

11104-28-2 Aroclor 1221 12 U 17 12 8.4 ug/kg

11141-16-5 Aroclor 1232 12 U 17 12 8.4 ug/kg

53469-21-9 Aroclor 1242 12 U 17 12 6.7 ug/kg

12672-29-6 Aroclor 1248 12 U 17 12 6.7 ug/kg

11097-69-1 Aroclor 1254 12 U 17 12 6.7 ug/kg

11096-82-5 Aroclor 1260 12 U 17 12 6.7 ug/kg







Raw Data: MM43946.D

132 of 3028

FA46136

44.14

12 U12 U12 U12 U12 U12 U12 U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 JJ016061.D 1 08/05/17 21:05 SJL 07/27/17 08:00 OP66168 GJJ684

Run #2


Run #1 20.3 g 1.0 ml

Run #2


TPH (C10-C28) a 49.9 5.1 3.8 2.5 mg/kg


84-15-1 o-Terphenyl 101% 56-122%

(a) Associated MS/MSD outside of control limits.





133 of 3028

FA46136

44.14

49.9 J

aiannacone

Stamp

aiannacone

Line

SGS Accutest













Lead 0.020 U D008 5.0 0.050 0.020 0.011 mg/l 1 08/01/17 08/01/17 LM SW846 6010C 2










134 of 3028

FA46136

44.14

aiannacone

Stamp

aiannacone

Typewritten Text

0.050U

aiannacone

Typewritten Text

0.36J

aiannacone

Typewritten Text

0.014J

aiannacone

Typewritten Text

0.050U

aiannacone

Typewritten Text

0.020U

aiannacone

Typewritten Text

0.0010U

aiannacone

Typewritten Text

0.050U

aiannacone

Typewritten Text

0.020U

aiannacone

Line

SGS Accutest







General Chemistry




(b) Not ignitable.



135 of 3028

FA46136

44.14

>200

97.1

51 U

8.00.77U

aiannacone

Stamp

aiannacone

Line

EMSL Analytical, Inc.3303 PARKWAY CENTER COURT Orlando, FL 32808

Tel/Fax: (407) 599-5887 / (407) 599-9063

http://www.EMSL.com / [email protected]

341706798EMSL Order:

Customer ID: ACCT51B

Customer PO:

Project ID:

Attention: Phone:Andrea Colby (407) 425-6700

Fax:Accutest (407) 425-0707

Received Date:4405 Vinland Road 07/25/2017 11:15 AM

Analysis Date:Orlando, FL 32811 08/08/2017

Collected Date: 07/25/2017


Test Report: Asbestos Analysis of Bulk Materials via EPA 600/R-93/116 Method using Polarized

Light Microscopy

Sample Description Appearance % Fibrous % Non-Fibrous

Non-Asbestos Asbestos

% Type

2X

341706798-0001

None DetectedQuartz

Ca Carbonate

Non-fibrous (Other)

35%

15%

50%

Red

Non-Fibrous

Homogeneous

T030GL-WC04

Soil is a problem matrix. Other analytical options are recommended such as EPA 600 PLM/TEM with milling prep

3X

341706798-0002

None DetectedQuartz

Ca Carbonate

Non-fibrous (Other)

35%

15%

50%

Red

Non-Fibrous

Homogeneous

T030GL-WC05


4X

341706798-0003

None DetectedQuartz

Ca Carbonate

Non-fibrous (Other)

35%

15%

50%

Brown

Non-Fibrous

Homogeneous

T030GL-WC06


5X

341706798-0004

None DetectedQuartz

Ca Carbonate

Non-fibrous (Other)

35%

15%

50%

Brown

Non-Fibrous

Homogeneous

T030GL-WC07


6X

341706798-0005

None DetectedQuartz

Ca Carbonate

Non-fibrous (Other)

35%

15%

50%

Brown

Non-Fibrous

Homogeneous

T030GL-WC08


7X

341706798-0006

None DetectedQuartz

Ca Carbonate

Non-fibrous (Other)

35%

15%

50%

Brown

Non-Fibrous

Homogeneous

T030GL-WC09


8X

341706798-0007

None DetectedQuartz

Ca Carbonate

Non-fibrous (Other)

35%

15%

50%

Red

Non-Fibrous

Homogeneous

T030GL-WC10


9X

341706798-0008

None DetectedQuartz

Ca Carbonate

Non-fibrous (Other)

35%

15%

50%

Brown

Non-Fibrous

Homogeneous

T030GL-WC11


10X

341706798-0009

None DetectedQuartz

Ca Carbonate

Non-fibrous (Other)

40%

5%

55%

Tan

Non-Fibrous

Homogeneous

T030GL-WC12


11X

341706798-0010

None DetectedQuartz

Ca Carbonate

Non-fibrous (Other)

40%

5%

55%

Tan

Non-Fibrous

Homogeneous

T030GL-WC13


12X

341706798-0011

None DetectedQuartz

Ca Carbonate

Non-fibrous (Other)

45%

5%

50%

Tan

Non-Fibrous

Homogeneous

T030GL-WC14


13X

341706798-0012

None DetectedQuartz

Ca Carbonate

Non-fibrous (Other)

40%

5%

51%

Cellulose4%Tan

Non-Fibrous

Homogeneous

T030GL-WC15


Initial report from: 08/08/2017 10:44:01

Page 1 of 2ASB_PLM_0008_0001 - 1.78 Printed: 8/8/2017 10:44 AM

137 of 3028

FA46136

5

aiannacone

Stamp


Tel/Fax: (407) 599-5887 / (407) 599-9063




Customer PO:

Project ID:


Light Microscopy



% Type

14X

341706798-0013

None DetectedQuartz

Ca Carbonate

Non-fibrous (Other)

55%

5%

37%

Cellulose3%Tan

Non-Fibrous

Heterogeneous

T030GL-WC16


Analyst(s)

Jessicka Lopez (8)

Timothy Kleehammer (5)

Carlos Rivadeneyra, Laboratory Director

or Other Approved Signatory

EMSL maintains liability limited to cost of analysis . This report relates only to the samples reported and may not be reproduced, except in full, without written approval by EMSL. EMSL bears no

responsibility for sample collection activities or analytical method limitations. Interpretation and use of test results are the responsibility of the client. This report must not be used by the client to claim

product certification, approval, or endorsement by NVLAP, NIST or any agency of the federal government . Non-friable organically bound materials present a problem matrix and therefore EMSL

recommends gravimetric reduction prior to analysis. Samples received in good condition unless otherwise noted. Estimated accuracy, precision and uncertainty data available upon request. Unless

requested by the client, building materials manufactured with multiple layers (i.e. linoleum, wallboard, etc.) are reported as a single sample. Reporting limit is 1%

Samples analyzed by EMSL Analytical, Inc. Orlando, FL NVLAP Lab Code 101151-0



138 of 3028

FA46136

5

aiannacone

Stamp

SDG FA46145


43 of 1825

FA46145

66.1



Project: CORRECTIVE ACTION

Airbill #'s: 811306952258

Cooler Information





5. Cooler media

IR Gun

Ice (Bag)





Sample Information





Intact

Comments

SM001Rev. Date 05/24/17




Cooler 1: (3.4);

Cooler 1: (3.8);


W or S N/A






Misc. Information

25-Gram 5-GramNumber of Encores: 4Number of 5035 Field Kits: Number of Lab Filtered Metals:


Y or N N/A

Y or N


Y or N N/A



Technician: Reviewer:JORGEC P.H Date: 7/26/2017Date: 7/26/2017 9:15:00 AM


44 of 1825

FA46145

66.1

SGS Accutest


Client Sample ID: T030GL-WC-TB01






Run #1 a C0123017.D 1 07/28/17 12:06 EP n/a n/a VC4871

Run #2


Run #1 5.00 g 5.0 ml

Run #2

VOA TCLP List


71-43-2 Benzene 2.0 U 5.0 2.0 1.2 ug/kg














2037-26-5 Toluene-D8 93% 75-126%


(a) Soil vials were not received within 48 hours of sampling; results are considered minimum values.





11 of 1825

FA46145

44.1

aiannacone

Stamp

aiannacone

Typewritten Text

2.0 UJ 15 UJ 2.0 UJ

aiannacone

Line

aiannacone

Line

SGS Accutest









Run #2


Run #1 5.00 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 2.5 U 5.0 2.5 2.5 mg/kg








12 of 1825

FA46145

44.1

aiannacone

Stamp

aiannacone

Line

aiannacone

Typewritten Text

2.5 U

SGS Accutest








Run #1 M97784.D 10 07/28/17 17:25 WV 07/27/17 09:30 OP66160 VM4196

Run #2

Purge Volume

Run #1 5.0 ml

Run #2



71-43-2 Benzene 0.0153 D018 0.50 0.010 0.0050 0.0031 mg/l














2037-26-5 Toluene-D8 101% 85-112%





Raw Data: M97784.D

13 of 1825

FA46145

44.2

aiannacone

Stamp

aiannacone

Typewritten Text

0.0153 0.035 U 0.0050U

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 4D2076.D 1 08/04/17 22:38 NG 07/29/17 08:15 OP66197 S4D81

Run #2


Run #1 100 ml 1.0 ml

Run #2



95-48-7 2-Methylphenol a 0.010 U D023 200 0.050 0.010 0.0056 mg/l

3&4-Methylphenol a 0.020 U D024 200 0.050 0.020 0.0098 mg/l

87-86-5 Pentachlorophenol b 0.10 U D037 100 0.25 0.10 0.050 mg/l









110-86-1 Pyridine 0.035 U D038 5.0 0.10 0.035 0.020 mg/l


367-12-4 2-Fluorophenol 25% 14-67%

4165-62-2 Phenol-d5 16% 10-50%

118-79-6 2,4,6-Tribromophenol 72% 33-118%

4165-60-0 Nitrobenzene-d5 63% 42-108%

321-60-8 2-Fluorobiphenyl 66% 40-106%

1718-51-0 Terphenyl-d14 82% 39-121%

(a) Associated MS/MSD recovery or RPD outside control limits.

(b) Associated BS recovery outside control limits.




Raw Data: 4D2076.D

14 of 1825

FA46145

44.2

aiannacone

Stamp

aiannacone

Typewritten Text

0.010UJ 0.020UJ 0.1UJ

aiannacone

Typewritten Text

0.020UJ 0.020UJ

aiannacone

Typewritten Text

0.020U 0.010U

aiannacone

Typewritten Text

0.020U 0.020U 0.035U

aiannacone

Line

aiannacone

Line

SGS Accutest









Run #2


Run #1 5.96 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 2.2 U 4.4 2.2 2.2 mg/kg








15 of 1825

FA46145

44.2

aiannacone

Stamp

aiannacone

Line

aiannacone

Typewritten Text

2.2 U

SGS Accutest








Run #1 CC055214.D 1 08/03/17 15:25 MG 07/29/17 12:30 OP66199 GCC1169

Run #2


Run #1 10.0 ml 5.0 ml

Run #2



94-75-7 2,4-D 0.025 U D016 10 0.050 0.025 0.017 mg/l

93-72-1 2,4,5-TP (Silvex) 0.0025 U D017 1.0 0.0050 0.0025 0.0013 mg/l


19719-28-9 2,4-DCAA 45% 39-135%





16 of 1825

FA46145

44.2

aiannacone

Stamp

aiannacone

Typewritten Text

0.025 UJ 0.0025 U

aiannacone

Line

SGS Accutest








Run #1 KK85107.D 1 08/02/17 21:15 KL 07/29/17 10:00 OP66198 GKK2709

Run #2


Run #1 100 ml 5.0 ml

Run #2




12789-03-6 Chlordane 0.00050 U D020 0.030 0.0010 0.00050 0.00038 mg/l

72-20-8 Endrin 0.000050 U D012 0.020 0.00020 0.0000500.000021mg/l




8001-35-2 Toxaphene 0.0038 U D015 0.50 0.0050 0.0038 0.0021 mg/l







Raw Data: KK85107.D

17 of 1825

FA46145

44.2

0.000050 U

0.00050 U0.000050 U

0.00010 U0.0038 U

aiannacone

Stamp

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 MM43953.D 1 07/27/17 20:51 NJ 07/27/17 07:30 OP66167 GMM840

Run #2


Run #1 15.8 g 5.0 ml

Run #2

PCB List


12674-11-2 Aroclor 1016 11 U 16 11 6.5 ug/kg

11104-28-2 Aroclor 1221 11 U 16 11 8.1 ug/kg

11141-16-5 Aroclor 1232 11 U 16 11 8.1 ug/kg

53469-21-9 Aroclor 1242 11 U 16 11 6.5 ug/kg

12672-29-6 Aroclor 1248 11 U 16 11 6.5 ug/kg

11097-69-1 Aroclor 1254 16 U 16 16 16 ug/kg

11096-82-5 Aroclor 1260 16 U 16 16 16 ug/kg







Raw Data: MM43953.D

18 of 1825

FA46145

44.2

aiannacone

Stamp

aiannacone

Typewritten Text

11 U 11 U 11 U 11 U 11 U 16 U 16 U

aiannacone

Line

SGS Accutest








Run #1 JJ016067.D 1 08/05/17 23:59 SJL 07/27/17 08:00 OP66168 GJJ684

Run #2


Run #1 20.4 g 1.0 ml

Run #2


TPH (C10-C28) 12.0 5.0 3.8 2.5 mg/kg


84-15-1 o-Terphenyl 98% 56-122%





19 of 1825

FA46145

44.2

aiannacone

Stamp

aiannacone

Line

aiannacone

Typewritten Text

12.0 J

SGS Accutest













Lead 0.016 J D008 5.0 0.050 0.020 0.011 mg/l 1 07/28/17 07/28/17 LM SW846 6010C 1










20 of 1825

FA46145

44.2

aiannacone

Stamp

aiannacone

Typewritten Text

0.050 U

aiannacone

Typewritten Text

0.057 J

aiannacone

Typewritten Text

0.010 U 0.050 U

aiannacone

Typewritten Text

0.016 J

aiannacone

Typewritten Text

0.00056 J

aiannacone

Typewritten Text

0.050 U

aiannacone

Typewritten Text

0.020 U

aiannacone

Line

SGS Accutest







General Chemistry





Solids, Percent 97.6 % 1 07/27/17 17:36 CH SM19 2540G



(b) Not ignitable.



21 of 1825

FA46145

44.2

>200

97.6

51 U

8.30.76 U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 M97785.D 10 07/28/17 17:50 WV 07/27/17 09:30 OP66160 VM4196

Run #2

Purge Volume

Run #1 5.0 ml

Run #2



71-43-2 Benzene 0.0050 U D018 0.50 0.010 0.0050 0.0031 mg/l














2037-26-5 Toluene-D8 100% 85-112%





Raw Data: M97785.D

22 of 1825

FA46145

44.3

aiannacone

Stamp

aiannacone

Typewritten Text

0.0050U 0.035U 0.0050U

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 4D2079.D 1 08/05/17 00:01 NG 07/29/17 08:15 OP66197 S4D81

Run #2


Run #1 100 ml 1.0 ml

Run #2














110-86-1 Pyridine 0.035 U D038 5.0 0.10 0.035 0.020 mg/l


367-12-4 2-Fluorophenol 24% 14-67%

4165-62-2 Phenol-d5 15% 10-50%

118-79-6 2,4,6-Tribromophenol 79% 33-118%

4165-60-0 Nitrobenzene-d5 72% 42-108%

321-60-8 2-Fluorobiphenyl 74% 40-106%

1718-51-0 Terphenyl-d14 83% 39-121%





Raw Data: 4D2079.D

23 of 1825

FA46145

44.3

aiannacone

Stamp

aiannacone

Typewritten Text

0.010UJ 0.020UJ 0.10UJ

aiannacone

Typewritten Text

0.020UJ 0.020UJ 0.020U

aiannacone

Typewritten Text

0.010U 0.010U 0.010U

aiannacone

Typewritten Text

0.020U 0.020U 0.035U

aiannacone

Line

SGS Accutest









Run #2


Run #1 5.76 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 2.7 U 5.5 2.7 2.7 mg/kg








24 of 1825

FA46145

44.3

aiannacone

Stamp

aiannacone

Line

aiannacone

Typewritten Text

2.7 U

SGS Accutest








Run #1 CC055219.D 1 08/03/17 16:45 MG 07/29/17 12:30 OP66199 GCC1169

Run #2


Run #1 10.0 ml 5.0 ml

Run #2



94-75-7 2,4-D 0.025 U D016 10 0.050 0.025 0.017 mg/l

93-72-1 2,4,5-TP (Silvex) 0.0025 U D017 1.0 0.0050 0.0025 0.0013 mg/l


19719-28-9 2,4-DCAA 48% 39-135%





25 of 1825

FA46145

44.3

aiannacone

Stamp

aiannacone

Typewritten Text

0.025 UJ 0.0025 U

aiannacone

Line

SGS Accutest








Run #1 KK85110.D 1 08/02/17 22:06 KL 07/29/17 10:00 OP66198 GKK2709

Run #2


Run #1 100 ml 5.0 ml

Run #2




12789-03-6 Chlordane 0.00050 U D020 0.030 0.0010 0.00050 0.00038 mg/l

72-20-8 Endrin 0.000050 U D012 0.020 0.00020 0.0000500.000021mg/l




8001-35-2 Toxaphene 0.0038 U D015 0.50 0.0050 0.0038 0.0021 mg/l







Raw Data: KK85110.D

26 of 1825

FA46145

44.3

0.000050 U

0.00050 U0.000050 U

0.00010 U0.0038 U

aiannacone

Stamp

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 MM43954.D 1 07/27/17 21:02 NJ 07/27/17 07:30 OP66167 GMM840

Run #2


Run #1 15.3 g 5.0 ml

Run #2

PCB List


12674-11-2 Aroclor 1016 13 U 18 13 7.3 ug/kg

11104-28-2 Aroclor 1221 13 U 18 13 9.2 ug/kg

11141-16-5 Aroclor 1232 13 U 18 13 9.2 ug/kg

53469-21-9 Aroclor 1242 13 U 18 13 7.3 ug/kg

12672-29-6 Aroclor 1248 13 U 18 13 7.3 ug/kg

11097-69-1 Aroclor 1254 13 U 18 13 7.3 ug/kg

11096-82-5 Aroclor 1260 13 U 18 13 7.3 ug/kg







Raw Data: MM43954.D

27 of 1825

FA46145

44.3

aiannacone

Stamp

aiannacone

Typewritten Text

13 U 13 U 13 U 13 U 13 U 13 U 13 U

aiannacone

Line

SGS Accutest








Run #1 JJ016068.D 1 08/06/17 00:27 SJL 07/27/17 08:00 OP66168 GJJ684

Run #2


Run #1 20.2 g 1.0 ml

Run #2


TPH (C10-C28) 14.2 5.6 4.2 2.8 mg/kg


84-15-1 o-Terphenyl 104% 56-122%





28 of 1825

FA46145

44.3

aiannacone

Stamp

aiannacone

Typewritten Text

14.2 J

aiannacone

Line

SGS Accutest













Lead 0.77 D008 5.0 0.050 0.020 0.011 mg/l 1 07/28/17 07/28/17 LM SW846 6010C 1










29 of 1825

FA46145

44.3

aiannacone

Stamp

aiannacone

Typewritten Text

0.050 U

aiannacone

Typewritten Text

0.40 J

aiannacone

Typewritten Text

0.010 U 0.050 U

aiannacone

Typewritten Text

0.77

aiannacone

Typewritten Text

0.00059J

aiannacone

Typewritten Text

0.050 U

aiannacone

Typewritten Text

0.020 U

aiannacone

Line

SGS Accutest







General Chemistry





Solids, Percent 89 % 1 07/27/17 17:36 CH SM19 2540G



(b) Not ignitable.



30 of 1825

FA46145

44.3

>200

89

56 U

0.84 U

7.7

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 M97786.D 10 07/28/17 18:13 WV 07/27/17 09:30 OP66160 VM4196

Run #2

Purge Volume

Run #1 5.0 ml

Run #2



71-43-2 Benzene 0.0050 U D018 0.50 0.010 0.0050 0.0031 mg/l








127-18-4 Tetrachloroethylene 0.0346 D039 0.70 0.010 0.0050 0.0022 mg/l






2037-26-5 Toluene-D8 101% 85-112%





Raw Data: M97786.D

31 of 1825

FA46145

44.4

0.0050 U0.035 U0.0050 U

0.03460.0050 U0.0050 U

aiannacone

Stamp

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 4D2080.D 1 08/05/17 00:28 NG 07/29/17 08:15 OP66197 S4D81

Run #2


Run #1 100 ml 1.0 ml

Run #2














110-86-1 Pyridine 0.035 U D038 5.0 0.10 0.035 0.020 mg/l


367-12-4 2-Fluorophenol 28% 14-67%

4165-62-2 Phenol-d5 19% 10-50%

118-79-6 2,4,6-Tribromophenol 86% 33-118%

4165-60-0 Nitrobenzene-d5 81% 42-108%

321-60-8 2-Fluorobiphenyl 84% 40-106%

1718-51-0 Terphenyl-d14 89% 39-121%





Raw Data: 4D2080.D

32 of 1825

FA46145

44.4

aiannacone

Stamp

aiannacone

Typewritten Text

0.010UJ 0.020UJ 0.10UJ

aiannacone

Typewritten Text

0.010U 0.010U 0.010U

aiannacone

Typewritten Text

0.020U 0.020U 0.035U

aiannacone

Typewritten Text

0.020UJ 0.020UJ 0.020U

aiannacone

Line

SGS Accutest









Run #2


Run #1 5.58 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 2.9 U 5.8 2.9 2.9 mg/kg








33 of 1825

FA46145

44.4

aiannacone

Stamp

aiannacone

Typewritten Text

2.9 U

aiannacone

Line

SGS Accutest








Run #1 CC055252.D 1 08/08/17 13:03 MG 07/29/17 12:30 OP66199 GCC1170

Run #2


Run #1 10.0 ml 5.0 ml

Run #2



94-75-7 2,4-D 0.025 U D016 10 0.050 0.025 0.017 mg/l

93-72-1 2,4,5-TP (Silvex) 0.0025 U D017 1.0 0.0050 0.0025 0.0013 mg/l


19719-28-9 2,4-DCAA 41% 39-135%





34 of 1825

FA46145

44.4

aiannacone

Stamp

aiannacone

Typewritten Text

0.025 UJ 0.0025 U

aiannacone

Line

SGS Accutest








Run #1 KK85111.D 1 08/02/17 22:24 KL 07/29/17 10:00 OP66198 GKK2709

Run #2


Run #1 100 ml 5.0 ml

Run #2




12789-03-6 Chlordane 0.00050 U D020 0.030 0.0010 0.00050 0.00038 mg/l

72-20-8 Endrin 0.000050 U D012 0.020 0.00020 0.0000500.000021mg/l




8001-35-2 Toxaphene 0.0038 U D015 0.50 0.0050 0.0038 0.0021 mg/l







Raw Data: KK85111.D

35 of 1825

FA46145

44.4

aiannacone

Stamp

aiannacone

Line

aiannacone

Typewritten Text

0.000050 U

aiannacone

Typewritten Text

0.00050 U 0.000050 U

aiannacone

Typewritten Text

0.00010 U 0.0038 U

aiannacone

Line

SGS Accutest








Run #1 MM43955.D 1 07/27/17 21:14 NJ 07/27/17 07:30 OP66167 GMM840

Run #2


Run #1 15.1 g 5.0 ml

Run #2

PCB List


12674-11-2 Aroclor 1016 13 U 19 13 7.6 ug/kg

11104-28-2 Aroclor 1221 13 U 19 13 9.5 ug/kg

11141-16-5 Aroclor 1232 13 U 19 13 9.5 ug/kg

53469-21-9 Aroclor 1242 13 U 19 13 7.6 ug/kg

12672-29-6 Aroclor 1248 13 U 19 13 7.6 ug/kg

11097-69-1 Aroclor 1254 13 U 19 13 7.6 ug/kg

11096-82-5 Aroclor 1260 13 U 19 13 7.6 ug/kg







Raw Data: MM43955.D

36 of 1825

FA46145

44.4

aiannacone

Stamp

aiannacone

Typewritten Text

13 U 13 U 13 U 13 U 13 U 13 U 13 U

aiannacone

Line

SGS Accutest








Run #1 JJ016069.D 1 08/06/17 00:56 SJL 07/27/17 08:00 OP66168 GJJ684

Run #2


Run #1 20.3 g 1.0 ml

Run #2


TPH (C10-C28) 5.81 5.6 4.2 2.8 mg/kg


84-15-1 o-Terphenyl 106% 56-122%





37 of 1825

FA46145

44.4

aiannacone

Stamp

aiannacone

Line

aiannacone

Typewritten Text

5.81 J

SGS Accutest













Lead 0.020 U D008 5.0 0.050 0.020 0.011 mg/l 1 07/28/17 07/28/17 LM SW846 6010C 1










38 of 1825

FA46145

44.4

aiannacone

Stamp

aiannacone

Typewritten Text

0.050 U

aiannacone

Typewritten Text

0.63 J

aiannacone

Typewritten Text

0.010U 0.050U

aiannacone

Typewritten Text

0.020 U 0.00055J

aiannacone

Typewritten Text

0.050U

aiannacone

Typewritten Text

0.020U

aiannacone

Line

SGS Accutest







General Chemistry








(b) Not ignitable.



39 of 1825

FA46145

44.4

>200

87.5

57 U

0.85 U

8.0

aiannacone

Stamp

aiannacone

Line


Tel/Fax: (407) 599-5887 / (407) 599-9063




Customer PO:

Project ID:



Received Date:4405 Vinland Road 07/27/2017 11:15 AM



Project: FA46145X


Light Microscopy



% Type

2X

341706797-0001

None DetectedQuartz

Ca Carbonate

Non-fibrous (Other)

20%

10%

70%

Red

Non-Fibrous

Homogeneous

T030GL-WC01

3X

341706797-0002

None DetectedQuartz

Ca Carbonate

Non-fibrous (Other)

25%

10%

65%

Brown

Non-Fibrous

Homogeneous

T030GL-WC02

4X

341706797-0003

None DetectedQuartz

Ca Carbonate

Non-fibrous (Other)

25%

10%

65%

Brown

Non-Fibrous

Homogeneous

T030GL-WC03

Analyst(s)

Jessicka Lopez (3) Carlos Rivadeneyra, Laboratory Director










41 of 1825

FA46145

5

aiannacone

Stamp

SDG FA46163

OrderID: 341706796

Page 1 Of 1

81 of 2611

FA46163

5


83 of 2611

FA46163

66.1



Project: CORRECTIVE ACTION AT FORT BLISS

Airbill #'s: 804726011232

Cooler Information





5. Cooler media

IR Gun

Ice (Bag)





Sample Information





Intact

Comments

SM001Rev. Date 05/24/17




Cooler 1: (1.8);

Cooler 1: (2.2);


W or S N/A






Misc. Information

25-Gram 5-GramNumber of Encores: Number of 5035 Field Kits: Number of Lab Filtered Metals:


Y or N N/A

Y or N


Y or N N/A



Technician: Reviewer:PETERH PDS Date: 7/27/2017Date: 7/27/2017 9:00:00 AM


84 of 2611

FA46163

66.1

SGS Accutest








Run #1 C0123018.D 1 07/28/17 12:29 EP n/a n/a VC4871

Run #2


Run #1 5.00 g 5.0 ml

Run #2

VOA TCLP List


71-43-2 Benzene 2.0 U 5.0 2.0 1.2 ug/kg














2037-26-5 Toluene-D8 96% 75-126%






14 of 2611

FA46163

44.1

2.0 U15 U2.0 U

aiannacone

Stamp

aiannacone

Line

aiannacone

Line

SGS Accutest









Run #2


Run #1 5.00 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 2.5 U 5.0 2.5 2.5 mg/kg








15 of 2611

FA46163

44.1

aiannacone

Stamp

aiannacone

Typewritten Text

2.5 U

aiannacone

Line

SGS Accutest








Run #1 J0985840.D 10 08/04/17 15:26 DP 08/02/17 14:00 OP66240 VJ5682

Run #2

Purge Volume

Run #1 5.0 ml

Run #2



71-43-2 Benzene 0.0050 U D018 0.50 0.010 0.0050 0.0031 mg/l














2037-26-5 Toluene-D8 100% 85-112%






16 of 2611

FA46163

44.2

aiannacone

Stamp

aiannacone

Typewritten Text

0.0050UJ 0.035 U

aiannacone

Typewritten Text

0.0050UJ 0.0050 U 0.0050 U

aiannacone

Typewritten Text

0.0050U 0.0050U 00039B

aiannacone

Typewritten Text

0.0050U

aiannacone

Line

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 L0692673.D 1 08/10/17 17:57 NJ 08/04/17 08:15 OP66301 SL4060

Run #2


Run #1 100 ml 1.0 ml

Run #2









121-14-2 2,4-Dinitrotoluene a 0.010 U D030 0.13 0.050 0.010 0.0081 mg/l


87-68-3 Hexachlorobutadiene b 0.010 U D033 0.50 0.050 0.010 0.0050 mg/l

67-72-1 Hexachloroethane c 0.020 U D034 3.0 0.050 0.020 0.016 mg/l


110-86-1 Pyridine 0.035 U D038 5.0 0.10 0.035 0.020 mg/l


367-12-4 2-Fluorophenol 21% 14-67%

4165-62-2 Phenol-d5 14% 10-50%

118-79-6 2,4,6-Tribromophenol 88% 33-118%

4165-60-0 Nitrobenzene-d5 81% 42-108%

321-60-8 2-Fluorobiphenyl 72% 40-106%

1718-51-0 Terphenyl-d14 76% 39-121%

(a) Associated CCV and BS outside control limits.

(b) Associated CCV outside control limits.

(c) Associated BS recovery outside control limits.




Raw Data: L0692673.D

17 of 2611

FA46163

44.2

aiannacone

Stamp

aiannacone

Typewritten Text

0.020UJ 0.020UJ

aiannacone

Typewritten Text

0.020U 0.010UJ

aiannacone

Typewritten Text

0.010U 0.020U 0.10U

aiannacone

Typewritten Text

0.010U 0.010UJ 0.010UJ

aiannacone

Typewritten Text

0.020U 0.035UJ

aiannacone

Line

SGS Accutest









Run #2


Run #1 5.65 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 2.4 U 4.7 2.4 2.4 mg/kg








18 of 2611

FA46163

44.2

aiannacone

Stamp

aiannacone

Typewritten Text

2.4 U

aiannacone

Line

SGS Accutest








Run #1 CC055263.D 1 08/09/17 14:39 MG 08/08/17 16:20 OP66350 GCC1171

Run #2


Run #1 10.0 ml 5.0 ml

Run #2



94-75-7 2,4-D a 0.025 U D016 10 0.050 0.025 0.017 mg/l

93-72-1 2,4,5-TP (Silvex) b 0.0025 U D017 1.0 0.0050 0.0025 0.0013 mg/l


19719-28-9 2,4-DCAA 55% 39-135%

(a) Associated CCV outside of control limits high, sample was ND.






19 of 2611

FA46163

44.2

aiannacone

Stamp

aiannacone

Typewritten Text

0.025U 0.0025U

aiannacone

Line

SGS Accutest








Run #1 KK85262.D 1 08/11/17 17:01 KL 08/04/17 08:15 OP66302 GKK2717

Run #2


Run #1 100 ml 5.0 ml

Run #2




12789-03-6 Chlordane 0.00050 U D020 0.030 0.0010 0.00050 0.00038 mg/l

72-20-8 Endrin 0.000050 U D012 0.020 0.00020 0.0000500.000021mg/l



72-43-5 Methoxychlor a 0.00010 U D014 10 0.00020 0.00010 0.000050mg/l

8001-35-2 Toxaphene 0.0038 U D015 0.50 0.0050 0.0038 0.0021 mg/l








Raw Data: KK85262.D

20 of 2611

FA46163

44.2

aiannacone

Stamp

aiannacone

Typewritten Text

0.000050U

aiannacone

Typewritten Text

R 0.000050U

aiannacone

Typewritten Text

0.000050U 0.000050U 0.00010U R

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 MM44158.D 1 08/02/17 06:44 NJ 07/28/17 07:40 OP66183 GMM842

Run #2


Run #1 15.5 g 5.0 ml

Run #2

PCB List


12674-11-2 Aroclor 1016 12 U 17 12 6.7 ug/kg

11104-28-2 Aroclor 1221 12 U 17 12 8.3 ug/kg

11141-16-5 Aroclor 1232 12 U 17 12 8.3 ug/kg

53469-21-9 Aroclor 1242 12 U 17 12 6.7 ug/kg

12672-29-6 Aroclor 1248 12 U 17 12 6.7 ug/kg

11097-69-1 Aroclor 1254 a 12 U 17 12 6.7 ug/kg

11096-82-5 Aroclor 1260 a 12 U 17 12 6.7 ug/kg








Raw Data: MM44158.D

21 of 2611

FA46163

44.2

aiannacone

Stamp

aiannacone

Typewritten Text

12 U

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 JJ015993.D 1 08/03/17 14:27 SJL 07/31/17 08:00 OP66208 GJJ682

Run #2


Run #1 19.6 g 1.0 ml

Run #2


TPH (C10-C28) a 82.5 5.3 4.0 2.6 mg/kg


84-15-1 o-Terphenyl 100% 56-122%






22 of 2611

FA46163

44.2

aiannacone

Stamp

aiannacone

Line

aiannacone

Typewritten Text

82.5 J

SGS Accutest













Lead 0.50 D008 5.0 0.050 0.020 0.011 mg/l 1 08/02/17 08/03/17 LM SW846 6010C 2



Silver 0.0080 J D011 5.0 0.10 0.020 0.0070 mg/l 1 08/02/17 08/03/17 LM SW846 6010C 2







23 of 2611

FA46163

44.2

0.050U0.045J

0.010U

0.050U0.050

0.0010U0.050U0.0080J

aiannacone

Stamp

aiannacone

Line

SGS Accutest







General Chemistry








(b) Not ignitable.



24 of 2611

FA46163

44.2

>200

96.8

52 U

8.00.77U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 J0985841.D 10 08/04/17 15:50 DP 08/02/17 14:00 OP66240 VJ5682

Run #2

Purge Volume

Run #1 5.0 ml

Run #2



71-43-2 Benzene 0.0050 U D018 0.50 0.010 0.0050 0.0031 mg/l














2037-26-5 Toluene-D8 99% 85-112%






25 of 2611

FA46163

44.3

aiannacone

Stamp

aiannacone

Typewritten Text

0.0050UJ 0.035U

aiannacone

Typewritten Text

0.0050U 0.0050U 0.0033B

aiannacone

Typewritten Text

0.0050U

aiannacone

Typewritten Text

0.0050UJ 0.0050U 0.0050U

aiannacone

Line

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 L0692676.D 1 08/10/17 19:23 NJ 08/04/17 08:15 OP66301 SL4060

Run #2


Run #1 100 ml 1.0 ml

Run #2














110-86-1 Pyridine 0.035 U D038 5.0 0.10 0.035 0.020 mg/l


367-12-4 2-Fluorophenol 24% 14-67%

4165-62-2 Phenol-d5 17% 10-50%

118-79-6 2,4,6-Tribromophenol 87% 33-118%

4165-60-0 Nitrobenzene-d5 85% 42-108%

321-60-8 2-Fluorobiphenyl 74% 40-106%

1718-51-0 Terphenyl-d14 78% 39-121%








26 of 2611

FA46163

44.3

aiannacone

Stamp

aiannacone

Typewritten Text

0.010U 0.020U 0.10U

aiannacone

Typewritten Text

0.020UJ 0.020UJ

aiannacone

Typewritten Text

0.020U 0.010UJ

aiannacone

Typewritten Text

0.010U 0.010UJ 0.010UJ

aiannacone

Typewritten Text

0.020U 0.035UJ

aiannacone

Line

SGS Accutest









Run #2


Run #1 5.64 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 2.4 U 4.8 2.4 2.4 mg/kg








27 of 2611

FA46163

44.3

aiannacone

Stamp

aiannacone

Line

aiannacone

Typewritten Text

2.4U

SGS Accutest








Run #1 CC055266.D 1 08/09/17 15:28 MG 08/08/17 16:20 OP66350 GCC1171

Run #2


Run #1 10.0 ml 5.0 ml

Run #2



94-75-7 2,4-D a 0.025 U D016 10 0.050 0.025 0.017 mg/l

93-72-1 2,4,5-TP (Silvex) b 0.0025 U D017 1.0 0.0050 0.0025 0.0013 mg/l


19719-28-9 2,4-DCAA 59% 39-135%







28 of 2611

FA46163

44.3

aiannacone

Stamp

aiannacone

Typewritten Text

0.025U 0.0025U

aiannacone

Line

SGS Accutest








Run #1 KK85265.D 1 08/11/17 17:52 KL 08/04/17 08:15 OP66302 GKK2717

Run #2


Run #1 100 ml 5.0 ml

Run #2




12789-03-6 Chlordane 0.00050 U D020 0.030 0.0010 0.00050 0.00038 mg/l

72-20-8 Endrin 0.000050 U D012 0.020 0.00020 0.0000500.000021mg/l




8001-35-2 Toxaphene 0.0038 U D015 0.50 0.0050 0.0038 0.0021 mg/l








Raw Data: KK85265.D

29 of 2611

FA46163

44.3

aiannacone

Stamp

aiannacone

Typewritten Text

0.000050U

aiannacone

Typewritten Text

R 0.000050U 0.000050U 0.000050U 0.00010U

aiannacone

Typewritten Text

R

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 MM44159.D 1 08/02/17 06:56 NJ 07/28/17 07:40 OP66183 GMM842

Run #2


Run #1 15.2 g 5.0 ml

Run #2

PCB List


12674-11-2 Aroclor 1016 12 U 17 12 6.8 ug/kg

11104-28-2 Aroclor 1221 12 U 17 12 8.5 ug/kg

11141-16-5 Aroclor 1232 12 U 17 12 8.5 ug/kg

53469-21-9 Aroclor 1242 12 U 17 12 6.8 ug/kg

12672-29-6 Aroclor 1248 12 U 17 12 6.8 ug/kg

11097-69-1 Aroclor 1254 a 12 U 17 12 6.8 ug/kg

11096-82-5 Aroclor 1260 a 12 U 17 12 6.8 ug/kg








Raw Data: MM44159.D

30 of 2611

FA46163

44.3

aiannacone

Stamp

aiannacone

Typewritten Text

12 U

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 JJ015996.D 1 08/03/17 15:54 SJL 07/31/17 08:00 OP66208 GJJ682

Run #2


Run #1 19.7 g 1.0 ml

Run #2


TPH (C10-C28) a 36.4 5.3 3.9 2.6 mg/kg


84-15-1 o-Terphenyl 96% 56-122%






31 of 2611

FA46163

44.3

aiannacone

Stamp

aiannacone

Line

aiannacone

Typewritten Text

36.4 J

SGS Accutest










Barium 0.050 U D005 100 2.0 0.050 0.050 mg/l 1 08/02/17 08/03/17 LM SW846 6010C 2



Lead 0.020 U D008 5.0 0.050 0.020 0.011 mg/l 1 08/02/17 08/03/17 LM SW846 6010C 2










32 of 2611

FA46163

44.3

0.050U0.050U0.010U0.050U

0.020U0.0010U

0.050U0.020U

aiannacone

Stamp

aiannacone

Line

SGS Accutest







General Chemistry




Ignitability (Flashpoint) b >200 Deg. F 1 08/10/17 16:10 LJ SW846 1010




(b) Not ignitable.



33 of 2611

FA46163

44.3

>200

96.5

52 U

8.30.77U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 J0985842.D 10 08/04/17 16:14 DP 08/02/17 14:00 OP66240 VJ5682

Run #2

Purge Volume

Run #1 5.0 ml

Run #2



71-43-2 Benzene 0.0050 U D018 0.50 0.010 0.0050 0.0031 mg/l














2037-26-5 Toluene-D8 100% 85-112%






34 of 2611

FA46163

44.4

aiannacone

Stamp

aiannacone

Typewritten Text

0.0050UJ 0.035U

aiannacone

Typewritten Text

0.0050U 0.0050U 0.0032B

aiannacone

Typewritten Text

0.0050U

aiannacone

Typewritten Text

0.0050UJ 0.0050U 0.0050U

aiannacone

Line

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 L0692677.D 1 08/10/17 19:53 NJ 08/04/17 08:15 OP66301 SL4060

Run #2


Run #1 100 ml 1.0 ml

Run #2














110-86-1 Pyridine 0.035 U D038 5.0 0.10 0.035 0.020 mg/l


367-12-4 2-Fluorophenol 23% 14-67%

4165-62-2 Phenol-d5 16% 10-50%

118-79-6 2,4,6-Tribromophenol 82% 33-118%

4165-60-0 Nitrobenzene-d5 80% 42-108%

321-60-8 2-Fluorobiphenyl 72% 40-106%

1718-51-0 Terphenyl-d14 80% 39-121%








35 of 2611

FA46163

44.4

aiannacone

Stamp

aiannacone

Typewritten Text

0.010U 0.020U 0.10U

aiannacone

Typewritten Text

0.020UJ 0.020UJ

aiannacone

Typewritten Text

0.020U 0.010UJ 0.010U

aiannacone

Typewritten Text

0.010UJ 0.020UJ

aiannacone

Typewritten Text

0.020U 0.035UJ

aiannacone

Line

SGS Accutest









Run #2


Run #1 5.54 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 2.4 U 4.8 2.4 2.4 mg/kg








36 of 2611

FA46163

44.4

aiannacone

Stamp

aiannacone

Line

aiannacone

Typewritten Text

2.4U

SGS Accutest








Run #1 CC055268.D 1 08/09/17 16:00 MG 08/08/17 16:20 OP66350 GCC1171

Run #2


Run #1 10.0 ml 5.0 ml

Run #2



94-75-7 2,4-D a 0.025 U D016 10 0.050 0.025 0.017 mg/l

93-72-1 2,4,5-TP (Silvex) b 0.0025 U D017 1.0 0.0050 0.0025 0.0013 mg/l


19719-28-9 2,4-DCAA 65% 39-135%







37 of 2611

FA46163

44.4

aiannacone

Stamp

aiannacone

Line

aiannacone

Typewritten Text

0.025U 0.0025U

SGS Accutest








Run #1 KK85266.D 1 08/11/17 18:08 KL 08/04/17 08:15 OP66302 GKK2717

Run #2


Run #1 100 ml 5.0 ml

Run #2




12789-03-6 Chlordane 0.00050 U D020 0.030 0.0010 0.00050 0.00038 mg/l

72-20-8 Endrin 0.000050 U D012 0.020 0.00020 0.0000500.000021mg/l




8001-35-2 Toxaphene 0.0038 U D015 0.50 0.0050 0.0038 0.0021 mg/l








Raw Data: KK85266.D

38 of 2611

FA46163

44.4

aiannacone

Stamp

aiannacone

Typewritten Text

0.000050U

aiannacone

Typewritten Text

R 0.000050U 0.000050U 0.000050U

aiannacone

Typewritten Text

0.00010U R

aiannacone

Line

SGS Accutest








Run #1 MM44160.D 1 08/02/17 07:08 NJ 07/28/17 07:40 OP66183 GMM842

Run #2


Run #1 14.7 g 5.0 ml

Run #2

PCB List


12674-11-2 Aroclor 1016 12 U 17 12 7.0 ug/kg

11104-28-2 Aroclor 1221 12 U 17 12 8.7 ug/kg

11141-16-5 Aroclor 1232 12 U 17 12 8.7 ug/kg

53469-21-9 Aroclor 1242 12 U 17 12 7.0 ug/kg

12672-29-6 Aroclor 1248 12 U 17 12 7.0 ug/kg

11097-69-1 Aroclor 1254 a 12 U 17 12 7.0 ug/kg

11096-82-5 Aroclor 1260 b 12 U 17 12 7.0 ug/kg





(b) Associated CCV outside of control limits high.




Raw Data: MM44160.D

39 of 2611

FA46163

44.4

aiannacone

Stamp

aiannacone

Line

aiannacone

Typewritten Text

12 U

aiannacone

Line

SGS Accutest








Run #1 JJ015997.D 1 08/03/17 16:23 SJL 07/31/17 08:00 OP66208 GJJ682

Run #2


Run #1 19.8 g 1.0 ml

Run #2


TPH (C10-C28) a 13.4 5.2 3.9 2.6 mg/kg


84-15-1 o-Terphenyl 104% 56-122%






40 of 2611

FA46163

44.4

aiannacone

Stamp

aiannacone

Typewritten Text

13.4 J

aiannacone

Line

SGS Accutest













Lead 0.020 U D008 5.0 0.050 0.020 0.011 mg/l 1 08/02/17 08/03/17 LM SW846 6010C 2










41 of 2611

FA46163

44.4

0.050U0.058J0.010U0.050U

0.020U0.0010U

0.050U0.020U

aiannacone

Stamp

aiannacone

Line

SGS Accutest







General Chemistry








(b) Not ignitable.



42 of 2611

FA46163

44.4

>200

97.2

51 U

7.90.77U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 J0985843.D 10 08/04/17 16:37 DP 08/02/17 14:00 OP66240 VJ5682

Run #2

Purge Volume

Run #1 5.0 ml

Run #2



71-43-2 Benzene 0.0070 D018 0.50 0.010 0.0050 0.0031 mg/l J














2037-26-5 Toluene-D8 100% 85-112%






43 of 2611

FA46163

44.5

aiannacone

Stamp

aiannacone

Line

aiannacone

Typewritten Text

0.0070J 0.035U

aiannacone

Typewritten Text

0.0050U 0.0050U 0.0031B

aiannacone

Typewritten Text

0.0050U

aiannacone

Typewritten Text

0.0050UJ 0.0050U 0.0050U

aiannacone

Line

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 L0692678.D 1 08/10/17 20:21 NJ 08/04/17 08:15 OP66301 SL4060

Run #2


Run #1 100 ml 1.0 ml

Run #2














110-86-1 Pyridine 0.035 U D038 5.0 0.10 0.035 0.020 mg/l


367-12-4 2-Fluorophenol 24% 14-67%

4165-62-2 Phenol-d5 15% 10-50%

118-79-6 2,4,6-Tribromophenol 84% 33-118%

4165-60-0 Nitrobenzene-d5 80% 42-108%

321-60-8 2-Fluorobiphenyl 70% 40-106%

1718-51-0 Terphenyl-d14 73% 39-121%








44 of 2611

FA46163

44.5

aiannacone

Stamp

aiannacone

Typewritten Text

0.010U 0.020U 0.10U

aiannacone

Typewritten Text

0.020UJ 0.020UJ

aiannacone

Typewritten Text

0.020U 0.010UJ 0.010U

aiannacone

Typewritten Text

0.010UJ 0.020UJ

aiannacone

Typewritten Text

0.020U 0.035UJ

aiannacone

Line

SGS Accutest









Run #2


Run #1 5.78 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 2.7 U 5.5 2.7 2.7 mg/kg








45 of 2611

FA46163

44.5

aiannacone

Stamp

aiannacone

Line

aiannacone

Typewritten Text

2.7 U

SGS Accutest








Run #1 CC055269.D 1 08/09/17 16:16 MG 08/08/17 16:20 OP66350 GCC1171

Run #2


Run #1 10.0 ml 5.0 ml

Run #2



94-75-7 2,4-D a 0.025 U D016 10 0.050 0.025 0.017 mg/l

93-72-1 2,4,5-TP (Silvex) b 0.0025 U D017 1.0 0.0050 0.0025 0.0013 mg/l


19719-28-9 2,4-DCAA 51% 39-135%







46 of 2611

FA46163

44.5

aiannacone

Stamp

aiannacone

Typewritten Text

0.025U 0.0025U

aiannacone

Line

SGS Accutest








Run #1 KK85267.D 1 08/11/17 18:25 KL 08/04/17 08:15 OP66302 GKK2717

Run #2


Run #1 100 ml 5.0 ml

Run #2




12789-03-6 Chlordane 0.00050 U D020 0.030 0.0010 0.00050 0.00038 mg/l

72-20-8 Endrin 0.000050 U D012 0.020 0.00020 0.0000500.000021mg/l




8001-35-2 Toxaphene 0.0038 U D015 0.50 0.0050 0.0038 0.0021 mg/l








Raw Data: KK85267.D

47 of 2611

FA46163

44.5

aiannacone

Stamp

aiannacone

Typewritten Text

0.000050U

aiannacone

Typewritten Text

R 0.000050U 0.000050U 0.000050U

aiannacone

Typewritten Text

0.00010U R

aiannacone

Line

SGS Accutest








Run #1 a MM44462.D 4 08/10/17 01:53 NJ 08/04/17 08:00 OP66287 GMM846

Run #2


Run #1 15.2 g 5.0 ml

Run #2

PCB List


12674-11-2 Aroclor 1016 52 U 74 52 30 ug/kg

11104-28-2 Aroclor 1221 52 U 74 52 37 ug/kg

11141-16-5 Aroclor 1232 52 U 74 52 37 ug/kg

53469-21-9 Aroclor 1242 52 U 74 52 30 ug/kg

12672-29-6 Aroclor 1248 52 U 74 52 30 ug/kg

11097-69-1 Aroclor 1254 52 U 74 52 30 ug/kg

11096-82-5 Aroclor 1260 52 U 74 52 30 ug/kg








Raw Data: MM44462.D

48 of 2611

FA46163

44.5

aiannacone

Stamp

aiannacone

Typewritten Text

52 U

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 a WW11662.D 2 08/10/17 16:02 SJL 08/01/17 09:00 OP66227 GWW496

Run #2 WW11681.D 5 08/11/17 15:22 SJL 08/11/17 09:00 OP66394 GWW497


Run #1 19.6 g 1.0 ml

Run #2 20.1 g 2.0 ml


TPH (C10-C28) b 120 c 56 42 28 mg/kg


84-15-1 o-Terphenyl 42% d 91% 56-122%

(a) Confirmation run.

(b) Re-extract results reported because they were significantly higher than original results. Sample re-extracted

beyond hold-time.

(c) Result is from Run# 2

(d) Outside control limits.




Raw Data: WW11662.D WW11681.D

49 of 2611

FA46163

44.5

aiannacone

Stamp

aiannacone

Line

aiannacone

Typewritten Text

120 J

SGS Accutest













Lead 0.020 U D008 5.0 0.050 0.020 0.011 mg/l 1 08/02/17 08/03/17 LM SW846 6010C 2










50 of 2611

FA46163

44.5

0.050U0.45J0.0030J 0.050U

0.020U0.0020J0.050U0.020U

aiannacone

Stamp

aiannacone

Line

SGS Accutest







General Chemistry





Solids, Percent 89 % 1 07/28/17 12:15 VK SM19 2540G



(b) Not ignitable.



51 of 2611

FA46163

44.5

>200

89

56 U

8.80.84U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 J0985844.D 10 08/04/17 17:01 DP 08/02/17 14:00 OP66240 VJ5682

Run #2

Purge Volume

Run #1 5.0 ml

Run #2



71-43-2 Benzene 0.0050 U D018 0.50 0.010 0.0050 0.0031 mg/l














2037-26-5 Toluene-D8 99% 85-112%






52 of 2611

FA46163

44.6

aiannacone

Stamp

aiannacone

Line

aiannacone

Typewritten Text

0.0050UJ 0.035U

aiannacone

Typewritten Text

0.0050U 0.0050U 0.0032B

aiannacone

Typewritten Text

0.0050U

aiannacone

Typewritten Text

0.0050UJ 0.0050U 0.0050U

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 L0692679.D 1 08/10/17 20:49 NJ 08/04/17 08:15 OP66301 SL4060

Run #2


Run #1 100 ml 1.0 ml

Run #2














110-86-1 Pyridine 0.035 U D038 5.0 0.10 0.035 0.020 mg/l


367-12-4 2-Fluorophenol 25% 14-67%

4165-62-2 Phenol-d5 17% 10-50%

118-79-6 2,4,6-Tribromophenol 85% 33-118%

4165-60-0 Nitrobenzene-d5 80% 42-108%

321-60-8 2-Fluorobiphenyl 69% 40-106%

1718-51-0 Terphenyl-d14 79% 39-121%








53 of 2611

FA46163

44.6

aiannacone

Stamp

aiannacone

Typewritten Text

0.010U 0.020U 0.010U

aiannacone

Typewritten Text

0.020UJ 0.020UJ

aiannacone

Typewritten Text

0.020U 0.010UJ

aiannacone

Typewritten Text

0.010U 0.010UJ 0.020UJ

aiannacone

Typewritten Text

0.020U 0.035UJ

aiannacone

Line

SGS Accutest









Run #2


Run #1 6.04 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 2.2 U 4.4 2.2 2.2 mg/kg








54 of 2611

FA46163

44.6

aiannacone

Stamp

aiannacone

Typewritten Text

2.2U

aiannacone

Line

SGS Accutest








Run #1 CC055272.D 1 08/09/17 17:05 MG 08/08/17 16:20 OP66350 GCC1171

Run #2


Run #1 10.0 ml 5.0 ml

Run #2



94-75-7 2,4-D a 0.025 U D016 10 0.050 0.025 0.017 mg/l

93-72-1 2,4,5-TP (Silvex) b 0.0025 U D017 1.0 0.0050 0.0025 0.0013 mg/l


19719-28-9 2,4-DCAA 50% 39-135%







55 of 2611

FA46163

44.6

aiannacone

Stamp

aiannacone

Line

aiannacone

Typewritten Text

0.025U 0.0025U

SGS Accutest








Run #1 KK85268.D 1 08/11/17 18:42 KL 08/04/17 08:15 OP66302 GKK2717

Run #2


Run #1 100 ml 5.0 ml

Run #2




12789-03-6 Chlordane 0.00050 U D020 0.030 0.0010 0.00050 0.00038 mg/l

72-20-8 Endrin 0.000050 U D012 0.020 0.00020 0.0000500.000021mg/l




8001-35-2 Toxaphene 0.0038 U D015 0.50 0.0050 0.0038 0.0021 mg/l








Raw Data: KK85268.D

56 of 2611

FA46163

44.6

aiannacone

Stamp

aiannacone

Typewritten Text

0.000050U

aiannacone

Typewritten Text

R 0.000050U 0.000050U

aiannacone

Typewritten Text

0.000050U

aiannacone

Typewritten Text

0.00010U R

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 MM44161.D 1 08/02/17 07:19 NJ 07/28/17 07:40 OP66183 GMM842

Run #2


Run #1 14.5 g 5.0 ml

Run #2

PCB List


12674-11-2 Aroclor 1016 12 U 18 12 7.1 ug/kg

11104-28-2 Aroclor 1221 12 U 18 12 8.9 ug/kg

11141-16-5 Aroclor 1232 12 U 18 12 8.9 ug/kg

53469-21-9 Aroclor 1242 12 U 18 12 7.1 ug/kg

12672-29-6 Aroclor 1248 12 U 18 12 7.1 ug/kg

11097-69-1 Aroclor 1254 a 12 U 18 12 7.1 ug/kg

11096-82-5 Aroclor 1260 a 12 U 18 12 7.1 ug/kg








Raw Data: MM44161.D

57 of 2611

FA46163

44.6

aiannacone

Stamp

aiannacone

Typewritten Text

12 U

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 WW11647.D 1 08/09/17 22:02 SJL 08/01/17 09:00 OP66227 GWW495

Run #2


Run #1 19.9 g 1.0 ml

Run #2


TPH (C10-C28) a 6.67 5.2 3.9 2.6 mg/kg


84-15-1 o-Terphenyl 104% 56-122%





Raw Data: WW11647.D

58 of 2611

FA46163

44.6

aiannacone

Stamp

aiannacone

Line

aiannacone

Typewritten Text

6.67J

SGS Accutest










Barium 0.050 U D005 100 2.0 0.050 0.050 mg/l 1 08/02/17 08/03/17 LM SW846 6010C 2



Lead 0.020 U D008 5.0 0.050 0.020 0.011 mg/l 1 08/02/17 08/03/17 LM SW846 6010C 2










59 of 2611

FA46163

44.6

0.050U0.050U0.010U0.050U

0.020U0.0010U0.050U0.0080J

aiannacone

Stamp

aiannacone

Line

SGS Accutest







General Chemistry





Solids, Percent 97.1 % 1 07/28/17 12:15 VK SM19 2540G



(b) Not ignitable.



60 of 2611

FA46163

44.6

>200

97.1

52 U

8.00.77U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 N0104823.D 10 08/09/17 12:21 WV 08/08/17 13:00 OP66330 VN4789

Run #2

Purge Volume

Run #1 5.0 ml

Run #2



71-43-2 Benzene 0.231 D018 0.50 0.010 0.0050 0.0031 mg/l














2037-26-5 Toluene-D8 97% 85-112%





Raw Data: N0104823.D

61 of 2611

FA46163

44.7

aiannacone

Stamp

aiannacone

Typewritten Text

0.231 0.035U

aiannacone

Typewritten Text

0.0050U

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 L0692680.D 1 08/10/17 21:18 NJ 08/04/17 08:15 OP66301 SL4060

Run #2


Run #1 100 ml 1.0 ml

Run #2














110-86-1 Pyridine 0.035 U D038 5.0 0.10 0.035 0.020 mg/l


367-12-4 2-Fluorophenol 22% 14-67%

4165-62-2 Phenol-d5 15% 10-50%

118-79-6 2,4,6-Tribromophenol 86% 33-118%

4165-60-0 Nitrobenzene-d5 80% 42-108%

321-60-8 2-Fluorobiphenyl 70% 40-106%

1718-51-0 Terphenyl-d14 80% 39-121%








62 of 2611

FA46163

44.7

aiannacone

Stamp

aiannacone

Typewritten Text

0.010U 0.020U 0.10U

aiannacone

Typewritten Text

0.020UJ 0.020UJ

aiannacone

Typewritten Text

0.020U 0.010UJ

aiannacone

Typewritten Text

0.010U 0.010UJ 0.020UJ

aiannacone

Typewritten Text

0.020U 0.035UJ

aiannacone

Line

SGS Accutest









Run #2


Run #1 5.18 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 2.6 U 5.2 2.6 2.6 mg/kg








63 of 2611

FA46163

44.7

aiannacone

Stamp

aiannacone

Typewritten Text

2.6 U

aiannacone

Line

SGS Accutest








Run #1 CC055273.D 1 08/09/17 17:21 MG 08/08/17 16:20 OP66350 GCC1171

Run #2


Run #1 10.0 ml 5.0 ml

Run #2



94-75-7 2,4-D a 0.025 U D016 10 0.050 0.025 0.017 mg/l

93-72-1 2,4,5-TP (Silvex) b 0.0025 U D017 1.0 0.0050 0.0025 0.0013 mg/l


19719-28-9 2,4-DCAA 57% 39-135%







64 of 2611

FA46163

44.7

aiannacone

Stamp

aiannacone

Line

aiannacone

Typewritten Text

0.025U 0.0025U

SGS Accutest








Run #1 KK85271.D 1 08/11/17 19:32 KL 08/04/17 08:15 OP66302 GKK2717

Run #2


Run #1 100 ml 5.0 ml

Run #2




12789-03-6 Chlordane 0.00050 U D020 0.030 0.0010 0.00050 0.00038 mg/l

72-20-8 Endrin 0.000050 U D012 0.020 0.00020 0.0000500.000021mg/l




8001-35-2 Toxaphene 0.0038 U D015 0.50 0.0050 0.0038 0.0021 mg/l








Raw Data: KK85271.D

65 of 2611

FA46163

44.7

aiannacone

Stamp

aiannacone

Typewritten Text

0.000050U

aiannacone

Typewritten Text

R

aiannacone

Typewritten Text

0.000050U

aiannacone

Typewritten Text

0.00010U R

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 MM44162.D 1 08/02/17 07:31 NJ 07/28/17 07:40 OP66183 GMM842

Run #2


Run #1 15.5 g 5.0 ml

Run #2

PCB List


12674-11-2 Aroclor 1016 12 U 17 12 6.7 ug/kg

11104-28-2 Aroclor 1221 12 U 17 12 8.4 ug/kg

11141-16-5 Aroclor 1232 12 U 17 12 8.4 ug/kg

53469-21-9 Aroclor 1242 12 U 17 12 6.7 ug/kg

12672-29-6 Aroclor 1248 12 U 17 12 6.7 ug/kg

11097-69-1 Aroclor 1254 a 12 U 17 12 6.7 ug/kg

11096-82-5 Aroclor 1260 a 12 U 17 12 6.7 ug/kg








Raw Data: MM44162.D

66 of 2611

FA46163

44.7

aiannacone

Stamp

aiannacone

Line

aiannacone

Typewritten Text

12 U

aiannacone

Line

SGS Accutest








Run #1 WW11648.D 1 08/09/17 22:30 SJL 08/01/17 09:00 OP66227 GWW495

Run #2


Run #1 20.3 g 1.0 ml

Run #2


TPH (C10-C28) a 68.3 5.1 3.8 2.6 mg/kg


84-15-1 o-Terphenyl 97% 56-122%





Raw Data: WW11648.D

67 of 2611

FA46163

44.7

aiannacone

Stamp

aiannacone

Typewritten Text

68.3 J

aiannacone

Line

SGS Accutest













Lead 0.020 U D008 5.0 0.050 0.020 0.011 mg/l 1 08/02/17 08/03/17 LM SW846 6010C 2










68 of 2611

FA46163

44.7

0.050U0.42J0.010U0.050U

0.020U0.0010U0.050U0.020U

aiannacone

Stamp

aiannacone

Line

SGS Accutest







General Chemistry








(b) Not ignitable.



69 of 2611

FA46163

44.7

>200

96.1

52 U

7.90.78U

aiannacone

Stamp

aiannacone

Line

SGS Accutest








Run #1 N0104824.D 10 08/09/17 12:45 WV 08/08/17 13:00 OP66330 VN4789

Run #2

Purge Volume

Run #1 5.0 ml

Run #2



71-43-2 Benzene 0.0050 U D018 0.50 0.010 0.0050 0.0031 mg/l














2037-26-5 Toluene-D8 97% 85-112%





Raw Data: N0104824.D

70 of 2611

FA46163

44.8

aiannacone

Stamp

aiannacone

Typewritten Text

0.0050U 0.035U 0.0050U

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 L0692681.D 1 08/10/17 21:47 NJ 08/04/17 08:15 OP66301 SL4060

Run #2


Run #1 100 ml 1.0 ml

Run #2














110-86-1 Pyridine 0.035 U D038 5.0 0.10 0.035 0.020 mg/l


367-12-4 2-Fluorophenol 20% 14-67%

4165-62-2 Phenol-d5 13% 10-50%

118-79-6 2,4,6-Tribromophenol 80% 33-118%

4165-60-0 Nitrobenzene-d5 71% 42-108%

321-60-8 2-Fluorobiphenyl 62% 40-106%

1718-51-0 Terphenyl-d14 82% 39-121%








71 of 2611

FA46163

44.8

aiannacone

Stamp

aiannacone

Typewritten Text

0.010U 0.020U 0.10U

aiannacone

Typewritten Text

0.020UJ 0.020UJ

aiannacone

Typewritten Text

0.020U 0.010UJ

aiannacone

Typewritten Text

0.010U 0.010UJ 0.020UJ

aiannacone

Typewritten Text

0.020U 0.035UJ

aiannacone

Line

SGS Accutest









Run #2


Run #1 5.64 g 5.0 ml 100 ul

Run #2


TPH-GRO (C6-C10) 2.4 U 4.8 2.4 2.4 mg/kg








72 of 2611

FA46163

44.8

aiannacone

Stamp

aiannacone

Typewritten Text

2.4 U

aiannacone

Line

SGS Accutest








Run #1 CC055274.D 1 08/09/17 17:37 MG 08/08/17 16:20 OP66350 GCC1171

Run #2


Run #1 10.0 ml 5.0 ml

Run #2



94-75-7 2,4-D a 0.025 U D016 10 0.050 0.025 0.017 mg/l

93-72-1 2,4,5-TP (Silvex) b 0.0025 U D017 1.0 0.0050 0.0025 0.0013 mg/l


19719-28-9 2,4-DCAA 50% 39-135%







73 of 2611

FA46163

44.8

aiannacone

Stamp

aiannacone

Typewritten Text

0.025 U 0.0025U

aiannacone

Line

SGS Accutest








Run #1 KK85272.D 1 08/11/17 19:49 KL 08/04/17 08:15 OP66302 GKK2717

Run #2


Run #1 100 ml 5.0 ml

Run #2




12789-03-6 Chlordane 0.00050 U D020 0.030 0.0010 0.00050 0.00038 mg/l

72-20-8 Endrin 0.000050 U D012 0.020 0.00020 0.0000500.000021mg/l




8001-35-2 Toxaphene 0.0038 U D015 0.50 0.0050 0.0038 0.0021 mg/l








Raw Data: KK85272.D

74 of 2611

FA46163

44.8

aiannacone

Stamp

aiannacone

Typewritten Text

0.000050U

aiannacone

Typewritten Text

R 0.000050U

aiannacone

Typewritten Text

0.00010U R

aiannacone

Line

aiannacone

Line

SGS Accutest








Run #1 a MM44157.D 4 08/02/17 06:33 NJ 07/28/17 07:40 OP66183 GMM842

Run #2


Run #1 14.5 g 5.0 ml

Run #2

PCB List


12674-11-2 Aroclor 1016 50 U 71 50 29 ug/kg

11104-28-2 Aroclor 1221 50 U 71 50 36 ug/kg

11141-16-5 Aroclor 1232 50 U 71 50 36 ug/kg

53469-21-9 Aroclor 1242 50 U 71 50 29 ug/kg

12672-29-6 Aroclor 1248 50 U 71 50 29 ug/kg

11097-69-1 Aroclor 1254 b 50 U 71 50 29 ug/kg

11096-82-5 Aroclor 1260 b 50 U 71 50 29 ug/kg





(b) Associated CCV outside of control limits high, sample was ND.




Raw Data: MM44157.D

75 of 2611

FA46163

44.8

aiannacone

Stamp

aiannacone

Line

aiannacone

Typewritten Text

50 U

aiannacone

Line

SGS Accutest








Run #1 a WW11649.D 4 08/09/17 22:59 SJL 08/01/17 09:00 OP66227 GWW495

Run #2


Run #1 20.4 g 1.0 ml

Run #2


TPH (C10-C28) b 20.4 20 15 10 mg/kg


84-15-1 o-Terphenyl 93% 56-122%


(b) Petroleum hydrocarbon pattern extends beyond C28.




Raw Data: WW11649.D

76 of 2611

FA46163

44.8

aiannacone

Stamp

aiannacone

Line

aiannacone

Typewritten Text

20.4 J

SGS Accutest













Lead 0.013 J D008 5.0 0.050 0.020 0.011 mg/l 1 08/02/17 08/03/17 LM SW846 6010C 2










77 of 2611

FA46163

44.8

0.050U0.39J0.010U0.050U

0.13J0.0010U

0.050U0.0080J

aiannacone

Stamp

aiannacone

Line

SGS Accutest







General Chemistry








(b) Not ignitable.



78 of 2611

FA46163

44.8

>200

96.5

52 U

7.90.77U

aiannacone

Stamp

aiannacone

Line


Tel/Fax: (407) 599-5887 / (407) 599-9063




Customer PO:

Project ID:



Received Date:4405 Vinland Road 07/27/2017 12:30 PM



Project: FA46163X


Light Microscopy



% Type

2X

341706796-0001

None DetectedQuartz

Ca Carbonate

Non-fibrous (Other)

35%

5%

60%

Brown

Non-Fibrous

Heterogeneous

T030GL-WC17

3X

341706796-0002

None DetectedQuartz

Ca Carbonate

Non-fibrous (Other)

45%

5%

50%

Brown

Non-Fibrous

Heterogeneous

T030GL-WC18

4X

341706796-0003

None DetectedQuartz

Ca Carbonate

Non-fibrous (Other)

50%

5%

45%

Brown

Non-Fibrous

Heterogeneous

T030GL-WC19

5X

341706796-0004

None DetectedQuartz

Ca Carbonate

Non-fibrous (Other)

50%

5%

45%

Tan

Non-Fibrous

Heterogeneous

T030GL-WC20

6X

341706796-0005

None DetectedQuartz

Ca Carbonate

Non-fibrous (Other)

50%

5%

45%

Tan

Non-Fibrous

Heterogeneous

T030GL-WC21

7X

341706796-0006

None DetectedQuartz

Ca Carbonate

Non-fibrous (Other)

50%

5%

45%

Tan

Non-Fibrous

Heterogeneous

T030GL-WC22

8X

341706796-0007

None DetectedQuartz

Ca Carbonate

Non-fibrous (Other)

50%

10%

40%

Tan

Non-Fibrous

Heterogeneous

T030GL-WC23

Analyst(s)

Timothy Kleehammer (7) Carlos Rivadeneyra, Laboratory Director










80 of 2611

FA46163

5

aiannacone

Stamp

SDG 428907

aiannacone

Stamp

aiannacone

Typewritten Text

10.5 21.3

aiannacone

Typewritten Text

-0.0582 U 0.239 U

aiannacone

Line

aiannacone

Line

aiannacone

Line

aiannacone

Stamp

aiannacone

Typewritten Text

12.7 24.1

aiannacone

Typewritten Text

-1.32 U -0.626 U

aiannacone

Line

aiannacone

Line

aiannacone

Line

aiannacone

Stamp

aiannacone

Typewritten Text

16.4 22.1

aiannacone

Typewritten Text

-0.873 U -0.655 U

aiannacone

Line

aiannacone

Line

aiannacone

Line

aiannacone

Line


APPENDIX F

PROJECT SCHEDULE

ID Task Mode

Task Name Duration Start Finish Predecessors

1 Contract Award 0 days Wed 7/1/15 Wed 7/1/15

2 OPSEC / iWatch / and Other Security Requirements 90 days Wed 7/1/15 Mon 9/28/15 1

3 POP Completion Date 0 days Tue 5/5/20 Tue 5/5/20

4 0010_Complete a CA Work Plan at Oro Grande Landfill ‐ POP 24 mont1217 days Wed 7/1/15 Mon 10/29/18

5 NTP for CLIN 0010 0 days Wed 7/1/15 Wed 7/1/15

6 CA Work Plan 401 days Wed 7/1/15 Fri 8/5/16

7 Prepare and Submit Draft 91 days Wed 7/1/15 Mon 9/28/15 5

8 Army Review of Draft 124 days Thu 10/1/15 Sun 1/31/16 7

9 Address Comments and Prepare Draft Final 15 days Tue 2/2/16 Tue 2/16/16 8

10 Army Review of Draft Final 7 days Wed 2/17/16 Tue 2/23/16 9

11 Army Approval of Draft Final CA Work Plan 0 days Tue 2/23/16 Tue 2/23/16 10

12 Prepare Final and Submit to NMED 8 days Wed 2/24/16 Wed 3/2/16 11

13 NMED Review of Final 72 days Thu 3/3/16 Fri 5/13/16 12

14 Receive Notice of Disapproval (NOD), Prepare RTCs and Submit 1 day Mon 5/16/16 Mon 5/16/16 13

15 NMED Review and Acceptance of RTCs (Revise and Submit Slip Pa66 days Tue 5/17/16 Wed 7/20/16 14

16 Prepare and Submit Revised Final CA Work Plan 14 days Sat 7/23/16 Thu 8/4/16 15

17 Army and NMED Approval of Revised Final CA Work Plan 0 days Fri 8/5/16 Fri 8/5/16 16

18 Waste Excavation Plan (WEP) 820 days Mon 8/1/16 Mon 10/29/18

19 Prepare and Submit Draft 30 days Mon 8/1/16 Tue 8/30/16

20 Army Review of Draft 30 days Wed 8/31/16 Thu 9/29/16 19

21 Address Comments and Prepare Draft Final 20 days Fri 9/30/16 Wed 10/19/16 20

22 Army Review of Draft Final 15 days Thu 10/20/16 Thu 11/3/16 21

23 Prepare Draft Final and Submit to NMED 20 days Fri 11/4/16 Wed 11/23/16 22

24 NMED Review of Draft Final 160 days Thu 11/24/16 Tue 5/2/17 23

25 Address Comments (Waste Charecterization) and Prepare Revised Draft Final

200 days Wed 5/3/17 Sat 11/18/17 24

26 NMED Review and Comments 178 days Sun 11/19/17 Tue 5/15/18 25

27 Address comments and submitt revised WEP, with RTC's 143 days Wed 5/16/18 Fri 10/5/18 26

28 Army and NMED Approval of Revised WEP 24 days Sat 10/6/18 Mon 10/29/18 27

29 0011_(OPTION)_Complete CA and Final Report at Oro Grande Landfill ‐ POP 24 months

1144 days Fri 10/21/16 Mon 12/9/19

30 NTP for CLIN 0011 0 days Fri 10/21/16 Fri 10/21/16

31 CA Implementation 18 days Mon 1/14/19 Thu 1/31/19 28

32 Pre‐Construction Meeting 1 day Mon 1/14/19 Mon 1/14/19 28FS+51 days

33 Mobilization 1 day Mon 1/14/19 Mon 1/14/19 32SS

34 Site Preparation 1 day Mon 1/14/19 Mon 1/14/19 33SS

35 Soil Excavation 6 days Tue 1/15/19 Wed 1/23/19 34

36 Backfilling 9 days Thu 1/17/19 Wed 1/30/19 35SS+2 days

7/1

7/1

2/23

8/5

10/21

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Project: Environmental RemediDate: Wed 10/31/18

ID Task Mode

Task Name Duration Start Finish Predecessors

37 Site Restoration & Demobilization Complete 1 day Thu 1/31/19 Thu 1/31/19 36

38 CA Report 703 days Fri 1/5/18 Mon 12/9/19

39 Prepare and Submit Draft 60 days Fri 1/5/18 Mon 3/5/18 37

40 Army Review of Draft 45 days Tue 3/6/18 Thu 4/19/18 39

41 Address Comments and Prepare Draft Final 30 days Fri 4/20/18 Sat 5/19/18 40

42 Army Review of Draft Final 30 days Sun 5/20/18 Mon 6/18/18 41

43 Army Approval of Draft Final CA Report 0 days Tue 6/19/18 Tue 6/19/18 42

44 Prepare Final and Submit to NMED 14 days Tue 6/19/18 Mon 7/2/18 43

45 NMED Review of Final 360 days Tue 7/3/18 Thu 6/27/19 44

46 Receive Notice of Disapproval (NOD), Prepare RTCs and Submit 30 days Fri 6/28/19 Sat 7/27/19 45

47 NMED Review and Acceptance of RTCs 120 days Sun 7/28/19 Sun 11/24/19 46

48 Prepare and Submit Revised Final CA Report 14 days Mon 11/25/19 Sun 12/8/19 47

49 Army and NMED Approval of Revised Final CA Report 0 days Mon 12/9/19 Mon 12/9/19 48

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Project: Environmental RemediDate: Wed 10/31/18


APPENDIX G

WASTE ACCEPTANCE LETTER FROM OTERO-GREENTREE LANDFILL


APPENDIX H

EMERGENCY CONTACT LIST


EMERGENCY CONTACT LIST

Ambulance/Paramedics/Fire/Police – Emergency 9-1-1

Emergency Hospital: University Medical Center of El Paso 4815 Alameda Avenue, El Paso, TX 79905

Telephone: (915) 544-1200 Website: umcelpaso.org

Base Security: TBD Base Security Dispatch Office

Telephone:

Fort Bliss POC Sylvia Waggoner.

Office: (915) 568-7031 Email: [email protected]

US Army Environmental Command Contracting POC: Mike Bowlby 2450 Connell Road., Fort Sam Houston, TX 78234


US Army Corps of Engineers COR: Frank Roepke


CAPE (Project Office – San Antonio, TX) 404 E. Ramsey, Suite 206, San Antonio, TX 78216

Office: (808) 791-6880 FAX: (808) 791-6888

CAPE (Corporate - Atlanta, GA) 500 Pinnacle Court, Suite 200, Norcross, GA 30071

Office: (770) 908-7200 FAX: (770) 908-7219

CAPE Project Manager Krishna Nalavala

Office: Mobile: (678) 287-1351 Email: [email protected]

CAPE Site Superintendent/SSHO John Karp

Mobile: (570) 665-1210 Email: [email protected]

CAPE Safety and Health Manager Frank Garrett

Office: (949) 236-3000 Mobile: (714) 401-9506 Email: [email protected]

CAPE SVPRM Corporate Risk Manager Chris Caviness, PE, JD


CAPE Corporate Human Resources Manager Elena Linnar

Office: (949) 236-3052 FAX: (949) 231-1346 Email: [email protected]

mailto:[email protected]




APPENDIX I

EMERGENCY HOSPITAL ROUTE MAP

EMERGENCY HOSPITAL ROUTE MAP

Emergency Hospital: University Medical Center of El Paso 4815 Alameda Avenue, El Paso, TX 79905 (915) 544-1200 Emergency Hospital Route: Estimated Time: 50 minutes; Starting from Oro Grande Landfill, NM. Head south on US-54 W toward El Paso, TX; Turn LEFT onto State Line Road (0.2 miles); Turn RIGHT onto Dyer Street (2.7 miles); Turn LEFT onto Railroad Drive (10.5 miles); Keep RIGHT to stay on Railroad Drive (1.2 miles); Merge onto Gateway S. Blvd (0.3 miles); Use the left 2 lanes to merge onto US-54 W towards Juarez (0.4 miles); Continue on US-54W; take exit 20A for US-62 toward Paisano Drive (2.9 miles); Turn LEFT onto US-62 E Paisano Drive (0.9 miles); Turn LEFT onto S. Val Verde Street (0.1 miles); Turn LEFT onto Alameda Avenue (0.1 miles); The hospital will be on the right at 4815 Alameda Avenue, El Paso, TX 79905. NOTE: SSHO must drive emergency hospital route before start of field work.


APPENDIX J

TRANSPORTER APPROVAL LETTER

WASTE EXCAVATION PLAN - hwbdocuments.env.nm.gov Bliss/2018-10... · Fort Bliss New Mexico 1.3 Site...

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