VSC R2Everything - indico.cern.ch€¦ · LSS - scaling with luminosity 11/28/2017 Pawel Krakowski...
Transcript of VSC R2Everything - indico.cern.ch€¦ · LSS - scaling with luminosity 11/28/2017 Pawel Krakowski...
Pawel Krakowski
TE-VSC-ICM
Vacuum, Surfaces & Coatings Group
Technology Department 28/11/2017
VSC R2Everything
Results of the irradiation test campaigns of materials and electronics
Future actions
Vacuum, Surfaces & Coatings Group
Technology Department
VSC R2E results of irradiation campaigns and future actions
“VSC R2E project focuses on identifying and addressing the risk of radiation
induced failures in the vacuum equipment of CERN machines. It proposes radiation
tests and adequate strategies and developments.” VSC R2E WP (EDMS 1726800)
1. Evolution of radiation environment in LHC
2. R2E (Radiation to Electronics)
Project overview
Components and modules test results
3. R2M (Radiation to Material)
Projects overview
Irradiation tests results
4. VSC R2Everything numbers & summary
11/28/2017 Pawel Krakowski 2
Vacuum, Surfaces & Coatings Group
Technology Department
Fluence [cm-2] – (HEH – High Energy Hadron)
total number of particles that intersect a unit area
Flux [cm-2 s-1] – ”Fluence rate”
Dose [Gy] [J∙kg-1] – the absorption of one joule
of radiation energy by one kilogram of matter
Sv [J∙kg-1] – the health effect of low levels
of ionizing radiation on human body.
Depends of the type of radiation
How many apples will
fall on this area?
In time?
The particleHits received by
the sleeper
Will the headache
be the same
regardless of the
size or weight of the
apple?
The source (like accelerator)
Charged particles
interact strongly
and ionize directly
Neutral particles
interact less,
ionize indirectly
and penetrate further
Radiation related units
3
Amigo
11/28/2017 Pawel Krakowski
Vacuum, Surfaces & Coatings Group
Technology Department
Where the radiation in LHC comes from?
Main doses contribution sources are:
• Burn-off -> (interactions in the experiments) -> Luminosity
scaling -> Dominating for all areas next to the experiments
and up to RR1s
• Collimation -> IR23/IR27, RRs included:
• Momentum cleaning2 (IR3): dominated by luminosity
• Betatron cleaning3 (IR7): with assumption that all is lost
in IR3 and IR7 and determining ratio with BLM5s.
• Beam -> residual gas interaction (vacuum quality).
Affects All areas downstream the RRs, scaling with circulating
intensity (beam current) and residual gas pressure.
• For scaling in time, the energy increase can be neglected.
LSS - scaling with luminosity
11/28/2017 Pawel Krakowski
ARCs - scaling with intensity
4
1. RR → Shielded Alcoves in LHC ARCs.
2. IR → Insertion Regions. Middle of Long Straight Sections (LSS)
3. For particles with large betatron amplitudes (or energy deviations).
4. Fro particles with off-momentum deviations.
5. Beam Loss Monitor. The standard monitors are ionization chambers with parallel aluminium electrode plates.
Vacuum, Surfaces & Coatings Group
Technology Department
Pirani threshold 500 Gy
Piezo threshold 200 Gy
24VDC 3kGy limit – from 350Gy linear drop of voltage 7-10%/1kGy
Penning threshold 12-15 Gy
Luminosity driven Intensity driven
Evolution of radiation levels of the LHC for VSC controls
Luminosity driven
Intensity
Localized Loss
TE-VSC-ICM controls, even Rad-tol electronics, have to be relocated
as far as possible from odd cells quadruples !
11/28/2017 Pawel Krakowski
Salvatore Danzeca - Evian Workshop 2016
5
Vacuum, Surfaces & Coatings Group
Technology Department
VSC R2E test results
& future actions
11/28/2017 Pawel Krakowski 6
Vacuum, Surfaces & Coatings Group
Technology Department
Mixed field
CHARM
500 Gy
is our goal
PSI4
Proscan COMET
P+ 200-250 MeV
15 components
TESTED
Defining radiation environment
Where in the machine the electronics is installed?
Tunnel? RE or RR?
What levels of radiation are expected?
TID2 (Gy)
>1-5 Gy/y
HEH2 (n/cm2)
>1E7 n/cm2/y
Rad-effects of concern
Test of COTS (Commercial Off-The-Shelf)Component
classification:
component type
based technology
available expertises
& reports
Effects and criticality:
TID limit ?
SET3 ?
Ex. LOG stage
Gamma
CC605
Mixed field
CHARM6
RHA1 guideline Rad-Tol design qualification in 5 easy steps
How does VSC-ICM manage such studies?
Tests of modules
Test of the System
7
1. RHA → Radiation Hardness Assurance.
2. TID → Total Ionising Dose. HEH – High Energy Hadron
3. SET → Single Event Transient. → Traversing particles induced voltage pulses (i.e. glitches) that propagate through the circuit.
4. PSI → Paul Scherrer Institut - Villigen →200-250MeV proton beam from Proscan (Comet) cyclotron.
5. CC60 → facility located in CERN Prevessin with 60Co gamma source for the qualification of components against TID effects.
6. CHARM → The Cern High energy AcceleRator Mixed field facility located in the East Area, features a wide spectrum of radiation types and energies.
Pawel Krakowski11/28/2017
Vacuum, Surfaces & Coatings Group
Technology Department
Components tests at PSI
(Proton beam)
811/28/2017 Pawel Krakowski
Vacuum, Surfaces & Coatings Group
Technology Department
COTs (Commercial Off-The-Shelf) components tests at PSI
PIF- Proton Irradiation FacilityCOMET
PROSCAN
Proton beam
Emax= 250 Mev
Beam control and on-line monitoring DUTs (Device Under Test) local controls & supply & test station
Beamline and target
11/28/2017 Pawel Krakowski 9
1 Campaign = ~5 COTs = ~20 h and more! of test time
In total 15 components tested for Vacuum R2E project
Tests up to 500 Gy or 1kGy
ICM assists with the tests of other users and prepares its own test reports!
Vacuum, Surfaces & Coatings Group
Technology Department 10
PSI COTs – tests results examples
±5V Bandgap Reference
LT1029
PNP matched pair transistor
MAT03
2N3810
Op-amp + contitioning
OP2177
Electrometer grade
op-am
LMC6001
OPA128
Penning LOG stage components Tested REJECTED
0 100 200 300 400 500
1E-11
1E-10
1E-9
Fix
ed p
ressure
measure
ment [m
bar]
due
to r
adia
tion induced d
rop o
f V
_R
EF
DOSE (Gy)
REF 5.5E-10 mbar
F(dose): 5.5E-10 mbar
REF 1E-10 mbar
F(dose): 1E-10 mbar
REF 1E-11 mbar
F(dose): 1E-11 mbar
11/28/2017
Recommended by EN-STI-ECE Tested ACCEPTED
0 100 200 300 400 500
98
99
100
101
102
103
104
Matc
hin
g (
%)
Ib_1
to
Ib
_2
Dose (Gy)
2N3810_pair_1
2N3810_pair_2
2N3810_pair_3
2N3810_pair_REF
0 50 100 150 200
-5
-4
-3
-2
-1
0
1
V_o
ut [V
]
Dose (Gy)
LMC6001_3007
LMC6001_3003
LMC6001_3010
LMC6001_3005_REF
REJECTED
ACCEPTED
ACCEPTED
0 100 200 300 400 500
94
96
98
100
102
104
106
108
Matc
hin
g (
%)
Ib_1 to Ib_2
Dose [Gy]
MAT03_pair_1
MAT03_pair_2
MAT03_pair_3
MAT03_pair_REF
REJECTED
0 100 200 300 400 500
-30
-20
-10
0
10
20
30
OP
A1
28 r
ela
tive V
out
cha
ng
e [
mV
]
DOSE (Gy)
OPA128_3007
OPA128_3003
OPA128_3010
OPA128_3005_REF
ACCEPTED
Pawel Krakowski
Vacuum, Surfaces & Coatings Group
Technology Department
LOG stage test at CC60
(Gamma)
1111/28/2017 Pawel Krakowski
Vacuum, Surfaces & Coatings Group
Technology Department 12
CC60 test – cumulative TID effect
-5 V
V_REF
LT1029
V_out
±15V
Iin
DUT
DUT (Device Under Test) LOG OPA128 N.2 BOX at CC60.
Penning logarithmic stage contains 4 active
components:
1. OPA128 - Difet electrometer-grade operational amplifier.
2. LT1029 - 5V bandgap reference.
3. OP2177 - Low input bias current operational amplifier.
4. 2N3810 - PNP silicon dual matching transistor.
DUT (Device Under Test) LOG OPA128 N.2
LOG stage has been tested in two dose rates,
respectively HDR ~2.98 Gy/h and LDR ~0.36 Gy/h.
Iin =10pA sourced from SMU to the LOG trough Femto coax cable.
CC60 dose rates.
2.98 Gy/h
0.36 Gy/h
11/28/2017 Pawel Krakowski
Vacuum, Surfaces & Coatings Group
Technology Department
0 100 200 300 400 500
-4.63
-4.62
-4.61
-4.60
-4.59
-4.58
-4.57
V_out of the LOG stage vs. Dose (CC60)
-4.579 V
V_
out
(V)
Dose (Gy)
LOG_CC60+20Gy
-4.596 V
475Gy in total
(including 20Gy
from previous run) 455Gy
CC60 LOG stage radiation test results LOG V_out (~-4.6V) for Iin of 10pA corresponding to 2.79E-11mbar
• LOG stage has received in total 475Gy (2 runs)
with negligable V_out degradation.
• Constant V_out offset of 200mV during irradiation(~3Gy/h) has been deducted from V_out measurement.
LOG stage CC60 radiation results. V_out compton offset of 200mV deducted.
11/28/2017 Pawel Krakowski
0 100 200 300 400 500 600
-4.60
-4.55
-4.50
-4.45
-4.40
V_out (V
)
Time (s)
V_out_10pA_LDR
V_out_10pA_HDR
130-140 mV
Offset dose rate
dependantSourceclosed
Source open
0 100 200 300 400 500
-5.00
-4.99
-4.98
-4.97
-4.96
-4.95
-4.94
-4.93
-4.92
-4.91
-4.90
-4.89
LT1029 ± 5V Bandgap Reference drift - different test facilities
V_R
EF
(V)
Dose (Gy)
V_ref_CC60
V_ref_PSI
V_ref_CHARM
Gamma (CC60)
200MeVProtons
PSI
Mixed field
CHARM
13
Vacuum, Surfaces & Coatings Group
Technology Department
LOG stage test at CHARM
(Mixed field)
1411/28/2017 Pawel Krakowski
Vacuum, Surfaces & Coatings Group
Technology Department
LOG stage CHARM
• 4 LOG stages in 3 runs (3 weeks in total)
• 10pA current sourced to each LOG trough TFA3 HV Triaxial cable
(CHARM VSC infrastructure)
• Monitoring of V_out, V_ref and PS in sampling rate of 1s.
11/28/2017 Pawel Krakowski 15
0 1x104
2x104
3x104
4x104
5x104
6x104
7x104
-4.60
-4.55
-4.50
-4.45
-4.40
-4.35
CHARM operation impact on 10pA measurement - Target IN/OUT
Value at 0Gy -4.63 V
NO Beam
V_
out
(V)
Sampling (number of samples)
LOG_Vout
~100Gy
Target
NO Target NO Beam
500 550 600 650 700 750 800
-4.64
-4.62
-4.60
-4.58
-4.56
-4.54
-4.52
-4.50
-4.48
-4.46
-4.44
-4.42
-4.40
Photocurrent impact on 10pA measurements - Target IN
Beam OFF
V_
out
(V)
Time (s)
LOG_180GyBeam ON TARGET IN
Total OFFSET
~150 mV
OFFSET_2 ~115mV
V_out -4.63 V at 0Gy 180Gy 30mV
-4.60V
0 1x103
2x103
3x103
4x103
5x103
6x103
7x103
-4.60
-4.55
-4.50
-4.45
-4.40
OF
FS
ET
~150m
V
CHARM operation impact on 10pA measurement - Beam ON/OFF
Beam on target
V_out
(V
)
Sampling (number od samples)
LOG_Vout
NO BEAM
Challenges of measuring low current under high fluxes of particles
Vacuum, Surfaces & Coatings Group
Technology Department
0 100 200 300 400 500
1E-11
2E-11
3E-11
4E-11
5E-11
6E-11
7E-11
8E-11
9E-111E-10
1 O
M
Fixed pressure readout change with absorbed dose
0Gy2.79E-11mbar
I(A) 10E-12A
Pre
ssure
(m
bar)
Dose (Gy)
500Gy 3.4E-11mbar
P=1.7-2I
0.8
in (mbar)
Iin(A)
LOG stage CHARM test resultsLOG V_out (~-4.603V) for Iin of 10pA corresponding to 2.79E-11mbar
• LOG_1 & LOG_2 have exceeded desired TID of 500Gy (RUN_1)
• LOG_3 & LOG_4 have accumulated ~495Gy (RUN_3).
• Slight differences in the drift of the V_outs of 4 DUTs is noticible.
0 100 200 300 400 500
-4.650
-4.625
-4.600
-4.575
-4.550
-4.525
V_out of the Penning LOG amp vs. Dose
LOG_1_Vout LOG_2_Vout LOG_3_Vout LOG_4_Vout
V_out
(V)
Dose (Gy)
TEST GOAL 500 Gy
11/28/2017 Pawel Krakowski 16
0 100 200 300 400 500
0
2
4
6
8
10
12
14
16
18
20
V_out peak-to-peak, f(D)
V
_o
ut
(mV
)
Dose (Gy)
Average of 4 LOGs
~18mV of V_out noise at >500 Gy
Vacuum, Surfaces & Coatings Group
Technology Department
VSC R2E (Radiation to Electronics) Future actions
11/28/2017 Pawel Krakowski
Sub-WP1: R2E (Radiation to Electronics)Schedule Activity 2016 2017 2018 2019 2020 2021 2022 2023 2024 2025
• Task 1: Active gaugesin the Arcs (penning & pirani)
Study
DS+ARC Design & Proto
DS+ARC PSI & CC60 COTS rad testsDS+ARC CHARM modules rad testsDS+ARC CHARM final system test
DS series
DS rad test
DS installation
DS commissioning
ARC series
ARC rad test
ARC installation
ARC commissioning
• Task 1.2: Active piezo gauges in the ARCs & LSS
Preparation
Irradiation
Analysis
• Task 2: Active gauges in LSS
Study
Design & Proto & rad test
Series
Installation
Commissioning
• Task 3: 24 VDC local power supply for fixed pumpinggroups
Study
Design & Proto & rad test
Modification IT
Commissioning IT
Modification LSS
Commissioning LSS
17
Actions
Re-test
RadTol
re-design
Change to
Passive
Redesign &
relocation
VSC R2E - Sub-WP1: R2E : Task 1
• Tests of some of the modules and system moved to 2018
• DS commissioning moved to 2020
(NEW)VSC R2E - Sub-WP1: R2E : Task 1.2
Active piezo gauges in the ARCs & LSS
Vacuum, Surfaces & Coatings Group
Technology Department
VSC R2M test results
& future actions
11/28/2017 Pawel Krakowski 18
Vacuum, Surfaces & Coatings Group
Technology Department 11/28/2017 Pawel Krakowski
Consultations with
all VSC sections
Consolidation of VSC
sections requests
Defining test
procedures & safety
precautions !
Radiation levels feedback
MCWG1 & FLUKA2 team
1.MCWG- Monitoring and Calculation Working Group. 2. FLUKA is a fully integrated particle physics MonteCarlo simulation package.
3.Yellow book report CERN-98-01.Compilation of radiation damage test data http://cds.cern.ch/record/357576
Defining criticality
and impact on the
machines operation
Irradiation conditions &
SPECIFICATIONS
Crosscheck with R2M WG
& 3
Planning & consolidation
of tests in campaigns
+
Optimising steps
=
Significant reduction
of the cost!
Management of samples handling
& Irradiation
EDMS & R2E sharepoint
documentation, results analysis
& reports preparation
How does VSC manage such studies?
DOSE STEP (MGy) 0.05 0.25 0.5 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
0.05
0.05
5.1
15
0.25
0.5
1
5.2 5.3
1
5Task 4. Pumps
0.25
0.5
1
5
10
15
Kaptons
Task 2.2 New Bake-out
10
Task 1.2 O-rings
3 x 5 MGy
3
5
Task 8. Valves (also for BGS change)
0.5
1
5
15
0.5
10
0.5
1 (here I await for fluka team for confirmation)Task 7. Silicons
0.5
„Executed tests need to be properly documented
(preparation, execution, facilities report, PIE)
• Good example given by TE/VSC for R2M”
M. Calviani (EN/STI) R2E Cost & Schedule Review, 12-13 October 2017
„Long-term Material Radiation Damage”
19
Vacuum, Surfaces & Coatings Group
Technology Department
EPDM based F6 and F14 – chosen for functional test
Studies continuation
11/28/2017 Pawel Krakowski
0 50 250 500 1000 3000
0
5
10
15
20
25
30
35
Maxim
um
str
ess (
MP
a)
1st cycle
norm
alise
d to
orig
inal
Dose (kGy)
F6
F14
NBR
FKM
O-rings characterisation
Radiation conditions and samples
preparations
ResultsEDMS 1698871
NBR & FKM damage
in ~1 to 3MGy
Tests before irradiation
Assemblies test up to 10MGy
4 assemblies for 10 and 5 MGy
will be send this week
176 samples
20
2 types of assemblies for each formulation
O-rings elastomers formulation
Vacuum, Surfaces & Coatings Group
Technology Department
0 Gy
Radiation induced ageing example of Red Bake-out Jackets
11/28/2017 Pawel Krakowski
250 kGy 500 kGy 1 MGy 10 MGy
21
5 MGy
Radiation induced ageing example of White Bake-out Jackets and connectors
1 MGy
0 Gy
500 kGy
From 1 MGy
Sewing thread ok but glued
part fell apart with no force
needed!
From
1 MGy
NEW permanent bake-out for LHC bellows
Fabric Aerogel Sewing thread Connectors
Samples already at BGS
Permanent bake-out components (10y of HL-LHC operation)
Vacuum, Surfaces & Coatings Group
Technology Department 11/28/2017 Pawel Krakowski 22
Radiation induced material aging observed in the machine
1. Silicone rubber, Xiameter RTV-4136-M
2. Black PU, Axson RE 11501/1020
3. Grey PU, Axson UR 3440
Due to time constraints, more complete round of testing
of different polymers in different conditions will
be postponed to a later date. Batch 2, and it is still
to be defined.
Straight clamps in ATLAS after ~year of operation
and exposure to ~1MGy
Radiation test up to 1MGy and more if needed.
I. Bellow clamp in ATLAS
II. Short straight clamp in CMS.
1 2 3 2 3
I II
3 different material under test
Silicon rubbers & polyurethanes clamps
Vacuum, Surfaces & Coatings Group
Technology Department 23
CHARM
11/28/2017 Pawel Krakowski
Target dose 100kGy/y
CHARM TDC2
→CHARM
Biaxial Strain Gauges on-line
measurement (few months)
→Irrad
Uniaxial strain gauges on-line
measurement (1week, 1MGy with
24GeV/c proton beam)
→TDC2
4 set-ups with online pressure
monitoring and pumping (up LS2 and
beyond?)
Co
nc
lus
ion
?
Fu
ture
ac
tion
s
SMA (Shape Memory Alloy)
Vacuum, Surfaces & Coatings Group
Technology Department
Possible impact of radiation on the machine operation Passive penning gauges and its HV cable under high HEH
RUN_1 only penning
gauges
Immediate pressure change when
beam ONImmediate pressure change when
beam ON or OFF
When no beam pressure values
come back to previous states
No memory effect…
4 passive penning
connected to small
vacuum chambers
pumped down in
ranges from 10-10
up to 10-12 mbar
RUN_2 and 3 only 3 penning gauges
and 1 simulator
Gaugea2
disconnected
and replaced by
passive simulator
(11 TΩ)
BEAM OFF
BEAM ONBEAM ON
BEAM OFF BEAM OFF
BEAM ON
Test at CHARM facility at CERN in particles showers from 24GeV proton beam on copper target
The same behaviour was
observed with gauge and
passive vacuum simulator !
11/28/2017 Pawel Krakowski
4E-10 mbar
6E-11 mbar
~E-12 mbar
RUN_2 and 3 have confirmed that the TFA3 Triaxial cable is the source of “peaks”
24
Vacuum, Surfaces & Coatings Group
Technology Department
• Pressure measured byTPG300 controller LOG stagewith HV(3kV) on TFA3 cable.Current translated to thepressure.
• Pressure/current readout„Peaks” visible even withoutthe target. Beam passing tothe dump and dumpsbackscathered particles.
• Induced current observed also during LOG stage tests when no HV was applied to TFA3 cable.
• Is the HV TFA3 (triaxial) cable acting like ionisation chamber ?
TFA3 HV penning cables (different configurations) under E12 HEH
Possible impact of radiation on the machine operation
11/28/2017 Pawel Krakowski
200 400 600 800 1000 1200 1400
1E-11
1E-10
1E-9
1E-8
1E-7
1E-11mbar10pA
1E-9mbarnA
HV TFA3 penning cable response on E12 HEH -CHARM
Pre
ssure
(mbar)
Sampling (s)
TFA3_cable+connector
TFA3_cable
1E-10mbar100pA
25
BEAM ON
BEAM OFF
BEAM ONNo target
BEAM OFF
0 100 200 300 400
1E-11
1E-10
1E-9
1E-8
1E-7
HV (3kV)TFA3 penning cable response on E12 HEH - CHARM
Pre
ssure
(mbar)
Sampling (s)
TFA3_cable+connector+Vac sim
TFA3_cable+connector
TFA3_cable
Vac sim 4E-10mbar
With no beam Red and Blue open cable ur-11mbar
• Amplitude of the „peaks” depends on CHARM operation.• Peaks appearance below hundreds of pA level corresponding to ~E-10mbar
Vacuum, Surfaces & Coatings Group
Technology Department 11/28/2017 Pawel Krakowski
• Sub-WP2: R2M (Radiation to Material)Schedule Activity 2016 2017 2018 2019
• Task 1: O-ring sealsPreparation
Irradiation BGSAnalysis (LRCCP)
• Task 1.2: F14 Formulation O-Rings under compressionPreparation
Irradiation BGSAnalysis (LRCCP)
• Task 2: Permanent bake-out componentsPreparation
Irradiation BGSAnalysis
• Task 2.2: New bake out jackets for the LHC bellows close to the collimators
Preparation
Irradiation BGSAnalysis
• Task 3: NiTiNb SMA (shape memory alloy) connectorsPreparation
Irradiation CHARMAnalysis
• Task 3.2: SMA connectors set-up North Area (TDC2) long term exposure
Preparation
Irradiation TDC2 TDC2 Analysis
• Task 4: Primary and turbo pumpsPreparation
Irradiation BGSAnalysis
• Task 5: Micro switches and distributors for sector valvesPreparation
Irradiation IONISOS
Analysis
• Task 6: Passive penning gauges and its HV cable under radiation
Preparation
Irradiation CHARM
Analysis
• Task 6.2: Radiation induced current in coaxial/triaxial cablesPreparation
Irradiation 6.2 CHARM
• Task 6.3: Radiation induced cables aging impact on their electrical performance
Irradiation 6.3IONISOS
Analysis
• Task 7: Polymer, Silicon rubbers and polyurethanes clamps VacSeal and other epoxies
Preparation
Irradiation BGSAnalysis
• Task 8: Piezoelectric venting valvePreparation
Irradiation BGSAnalysis
• Task 9: Passive piezo resistive gauges in the LSS
Preparation
IrradiationCHARM
Analysis
DONE CONTINUATION
VSC R2M (Radiation to Material) Future actionsNEW TASKS
VSC groups in time irradiations of different projects
26
VSC R2M Planning
Vacuum, Surfaces & Coatings Group
Technology Department
VSC R2Everything
numbers
& summary
2711/28/2017 Pawel Krakowski
Vacuum, Surfaces & Coatings Group
Technology Department 11/28/2017 Pawel Krakowski
VSC R2M – 4+ facilities
BGS→(gamma, higher dose rate),
IONISOS→(gamma, lower dose rate)
CHARM→(R0, target proximity),
IRRAD → SMA small samples
TDC2 North Area – for long term SMA
set-up exposure
VSC R2E – 3 facilities
PSI→(proton beam), 500-1kGy
C60→(gamma), 500Gy
CHARM→(mixed field) >500Gy
„Radiation tests as a service, database and know-
how.” Alessandro Masi (EN/STI). From 2011 to now.
“R2E Cost & Schedule Review” 12 & 13 October
2017Chairmen : Marco Calviani, Elisa Guillermain.
Since 2012 up now.
VSC contribution in CERN R2E VSC contribution in CERN R2M
VSC basic gamma irradiation planDOSE STEP (MGy) 0.05 0.25 0.5 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
3 x 5 MGy
Task 1.2 O-rings
0.05
0.25
0.5
1
3
10
Task 2.2 New Bake-out
0.5
1
5
10
15
Kaptons
0.05
0.25
0.5
1
5
10
15
Task 4. Pumps 0.5
5
15
Task 7. Silicons0.5
1
Without combination
VSC OTHERS TOTAL
206 days 291 days 497 days
130.5k€ 130.5k€ 261 k€ !
VSC + others combination in 3 campaigns
228 days Reduction by factor 2
81.5 k€ Reduction by factor 3
28
VSC R2Everything
numbers & %
Vacuum, Surfaces & Coatings Group
Technology Department
VSC R2E&M projects mostly on schedule defined by VSC R2E WP
Vacuum Group successfuly identifies and addresses the risk of radiation
induced failures to various equipment types of CERN machines
by performing one of the most extensive radiation test campaign at CERN
VSC is active in R2E, R2M and MCWG fields:
induces side tasks, such as:
• RPLs dose rate response studies,
• Temperature control strips response under gamma radiation
• Support and consultations in other projects
• And many more
All presented projects are in respect of HL-LHC and are the part of VSC R2E WP
The Project is described in Vacuum R2E technical note – EDMS 1703323
All info is available on VSC group SharePoint –VSC R2E
SUMMARY
11/28/2017 Pawel Krakowski 29
Vacuum, Surfaces & Coatings Group
Technology Department
Sub-WP1: R2E (Radiation to Electronics)Gregory Pigny (TE-VSC-ICM); Nikolaos Chatzigeorgiou (TE-VSC-ICM); Salvatore Danzeca(EN-STI-ECE);
Gilles Foucard(EN-STI-ECE); Paul Peronnard (EN-STI-ECE).
11/28/2017 Pawel Krakowski
Sub-WP2: R2M (Radiation to Materials)Markus Brugger (EN-EA); Elisa Guillermain (EN-STI-TCD); Ruben Garcia Alia (EN-STI-FDA);
Yacine Kadi(EN-EA); Angelo Infantino (EN-STI-FDA); Corinna Martinella (EN-EA); Robert Froeschl (HSE-
RP-AS); Helmut Vincke (HSE-RP-AS); Yann Pierre Pira (HSE-RP-AS); Mario Di Castro (EN-STI-ECE);
Giacomo Lunghi (EN-STI-ECE).
TE-VSC CollaborationPaulo Gomes (TE-VSC-ICM); Cedric Garion (TE-VSC-DLM); Mauro Taborelli (TE-VSC-SCC);
Giuseppe Bregliozzi (TE-VSC-BVO); Vincent Baglin (TE-VSC-VSM);
Germana Riddone (TE-VSC); Paul Cruikshank (TE-VSC); Paolo Chiggiato (TE-VSC).
Jose Antonio Ferreira Somoza (TE-VSC-BVO);Jaime Perez Espinos (TE-VSC-DLM); Willemjan Maan (TE-
VSC-DLM); Benoit Teissandier (TE-VSC-SCC); Josef Sestak (TE-VSC-BVO); Jorge Fraga (TE-VSC-ICM);
Hendrik Kos (TE-VSC-DLM); Lukasz Piotr Krzempek (TE-VSC-DLM); Caroline Guyenet (TE-VSC-DLM);
( Fabrizio Niccoli (TE-VSC-DLM); Yorick Maxence Delaup (TE-VSC-BVO); Jerome Gilles Chaure (TE-VSC-
BVO); Nicolas Zelko (TE-VSC-BVO); Jose Maria Ruiz (TE-VSC-BVO); Caroline Guyenet (TE-VSC-DLM);
VSC R2Everything
people
30
Vacuum, Surfaces & Coatings Group
Technology Department 11/28/2017 Pawel Krakowski 31
Thank you
for your attention
Vacuum, Surfaces & Coatings Group
Technology Department 11/28/2017 Pawel Krakowski 32
Spare slides
Vacuum, Surfaces & Coatings Group
Technology Department 11/28/2017 Pawel Krakowski 33
Motivation for Rad-tol penning design
IKR251 front-end electronics radiation test results
• Strong effects on electronics from 15 [Gy]!
• None survived designated dose
Vacuum, Surfaces & Coatings Group
Technology Department 11/28/2017 Pawel Krakowski 34
Motivation for FPG PS redesign and relocation
24VDC power supply for fixed vacuum pumping groups
• At 360 [Gy] voltage drop (92% linear correlation)
• At 1500 [Gy], 90%(255Ω) to 95%(1750Ω) of nominal voltage
Vacuum, Surfaces & Coatings Group
Technology Department
Material
Damage
R2E
Cumulative
damage
R2E
Single-Event
Effects
35Pawel Krakowski
LHC machine electronics Experiments
Protected
UJ
Shielded
RE/UA
Tunnel
ARCs/LSS
Commercial Hardened
RadTol
Custom Boards
+commercial
Damage
Experiment
caverns
Earth orbit deep spaceenvironment
Radiation levels in LHC
𝐇𝐄𝐇 [𝐜𝐦−𝟐 ∙ 𝐲−𝟏]
𝐓𝐈𝐃[𝐆𝐲 ∙ 𝐲−𝟏]
11/28/2017
Vacuum, Surfaces & Coatings Group
Technology Department 36Pawel Krakowski
Rad
iati
on
eff
ec
tsRadiation effects on electronics
Cumulativeaccumulating during the whole
LHC lifetime, due to the energy
deposited by radiation in the
electronics
Stochasticimmediate effects very
localized, event induced by a single particle
SEE (Single event effects)
TID(Total ionizing dose)
the dose is deposited by particles passing through the materials constituting the electronic devices.
DD(Displacement damage)
TransientSEU (Upset)
SET (Transient)
SEFI (Functional Interrupts
Destructive
SEL (Latchup) SEGR (Gate rupture)
SEB (Burnout)
11/28/2017
MOS
Bipolars
Optoel.
CMOS
Memories
Processors
Power MOSFET
Vacuum, Surfaces & Coatings Group
Technology Department 37Pawel Krakowski
Radiation effects on electronics
Total Ionising Dose vs. Single Events Effect
TID + DD
In time components degrade slowly
There are no unwanted “stops”
The final failure can be predicted Interventions can be planned
SEEElectronics can work without any signs
of malfunction
Gy ∙ y-1 Time
HEH [cm-1]
Expected life time
Fa
ilu
re p
rob
ab
ilit
y
Fa
ilu
re p
rob
ab
ilit
y
Failures can appear and rapidly increase
in frequency
Nonzero probability of a failure
Destructive failures possible
Immediate interventions needed
Threshold
11/28/2017
Vacuum, Surfaces & Coatings Group
Technology Department 11/28/2017 Pawel Krakowski 38
Consequences on systems and equipmentDamage to the material of a defined system might alter its functioning !
• Optical issues
• Loss of transmission
• Change of refractive Index
• Mechanical issues
• Strength, ductility, toughness modifications
• Cracks can appear
• Electrical issues
• Insulation properties
• Devices electrical properties modified
Metals
Lattice displacements
Voids, bubbles, clusters
Liquids
Radiolysis
Polymer
Radiolysis
Chain rupture
Recombination
Glass
Color centers,
Lattice displacement
CeramicsLattice displacements,
Color centers
Semiconductors
Lattice displacement
Radiation effects on materials
Vacuum, Surfaces & Coatings Group
Technology Department
0 50 250 500 1000 3000
0
5
10
15
20
25
Pre
ssure
[M
Pa]
Dose [kGy]
MPa
Each point is an average of 5 measurements
# SampleREF 50 kGy 250 kGy 500 kGy 1 MGy 3 MGy
Pressure[MPa]
Δ [MPa]
Pressure[MPa]
Δ [MPa]
Pressure[MPa]
Δ [MPa]
Pressure[MPa]
Δ [MPa]
Pressure[MPa]
Δ [MPa]Pressure
[MPa]Δ
[MPa]
1 23.6 -0.7 26.8 3.4 23.2 0.6 21.6 0.2 21.2 -0.3 24 1.2
2 24.8 0.5 24 0.6 22.4 -0.2 20 -1.4 21.2 -0.3 24 1.2
3 24 -0.3 22 -1.4 22 -0.6 21.6 0.2 21.6 0.1 23.8 1.0
4 25.2 0.9 22.4 -1.0 22.8 0.2 22.4 1.0 21.2 -0.3 22 -0.8
5 23.8 -0.5 22 -1.4 22.4 -0.2 21.6 0.2 22.4 0.9 20 -2.8
AV 24.28 0.6 23.44 1.8 22.56 0.4 21.44 0.8 21.52 0.5 22.76 1.6
39
VSC R2E - Sub-WP2: R2MGlued Kapton (polyimide) sheets for beam heaters
11/28/2017
Heaters characterisation and work conditions (ex. ATLAS chamber), samples preparation and irradiation
Original heater
25µm Polyimide
Adhesive layer
(epoxy resin)
25µm Polyimide
*
Sample attached to the
surface with another epoxy
The probe attached to the surface
of a sample with the same epoxy
as to the surface
Measurement of the force
needed to detach one layer
from another
Adhesive layer Known epoxy
Edges of the sample were
cut to the size of the probe*
Samples provided by Jerome Gilles Chaure (BVO).
Test developed and performed by SCC (B.Teissandier, P.Bole)
Force applied
Test samples
Next batch of samples from different manufacturer already
in BGS (up to 15MGy!)
10MGy samples irradiated, still to be measured
Pawel Krakowski
Vacuum, Surfaces & Coatings Group
Technology Department
64
6
0 500
0
10
20
30
40
50
60
70
OIT
in
da
ys
Dose [kGy]
Decrease of OIT by factor 10
646 days
40
VSC R2E - Sub-WP2: R2M
Permanent bake-out components in respect of 10 years operation
Example for NH25 cable studies on radiation induced degradation in high doses (example for 500 kGy)
0 Gy 500 kGy
0 500
0
20
40
60
80
100
120
104.2
The m
eltin
g tem
pera
ture
(non-isoth
erm
al)
[°C
]
Dose [kGy]
~110.4105.4
Repeatable measurements
Decrease in melting point after irradiation
Strong radiation induced degradation
• 9 White cables
• 10 Brown cables
• 1 Yellow/Green
• 5 Red cables
500
0.000
0.002
0.004
0.006
0.008
0.010
0.012
Dose [kGy]
0
0
2
4
6
8
10
Oxid
atio
n I
nd
uctio
n T
ime
(O
IT)
[h]
Dose [kGy]
Test performed by VSC-SCC
(B.Teissandier, P.Bole)
Transition from hours to less than minute !
Preparation Measurements Results
External
cable shield
Inner wires
insulation
Less than 1 minute of Oxidation Induction Time !
Cables are not protected in 105 Gy range
Pawel Krakowski11/28/2017