VISIT REPORT - Counterview.Org · VISIT REPORT Sub : Ground water contamination in Luna & Umaraya...

28
Pag 1 of 8 VISIT REPORT Sub : Ground water contamination in Luna & Umaraya – Regarding…. Date and time of Sampling : 26/12/2018 10:00AM Onwards In connection with the above mentioned subject, officials of GPCB Regional Office Vadodara and – Vigilance office, Vadodara has visited the area along with Shri Rohit Prajapati, Shri Ghanshyambhai Ramanbhai Patel, Vill. Luna and Shri Kirit Amin. During visit, Shri Rohitbhai Prajapati of Paryavaran Suraksha Samiti , Ghanshyambahi Patel and other complainer remained present throughout sampling. Total 21 borewell/Abstraction well water samples were collected during visit. Sampling Details : During visit, total 21 samples of ground water were collected as per the details given hereunder.

Transcript of VISIT REPORT - Counterview.Org · VISIT REPORT Sub : Ground water contamination in Luna & Umaraya...

Pag 1 of 8

VISIT REPORT Sub : Ground water contamination in Luna & Umaraya – Regarding…. Date and time of Sampling : 26/12/2018 10:00AM Onwards In connection with the above mentioned subject, officials of GPCB Regional Office Vadodara and – Vigilance office, Vadodara has visited the area along with Shri Rohit Prajapati, Shri Ghanshyambhai Ramanbhai Patel, Vill. Luna and Shri Kirit Amin. During visit, Shri Rohitbhai Prajapati of Paryavaran Suraksha Samiti , Ghanshyambahi Patel and other complainer remained present throughout sampling. Total 21 borewell/Abstraction well water samples were collected during visit.

Sampling Details :

During visit, total 21 samples of ground water were collected as per the details given hereunder.

Pag 2 of 8

Abstraction well water samples collected within premises of Huntsman International ( India) P Ltd , vill: Umaraya , Ta: Padra, Dist : Vadodara Sample

No Sample location Latitude Longitude Ownership Year of

Use Approx

Approx. Depth in

Present use Physical Appearance

Remark

01* Abstraction well no 01 (AW -1) 22 015 36.32"N 73 002 03.28"E

Huntsman International India ( P) Ltd

Started in 2012

35M

Industrial use after treatment in ground water treatment facility provided by the unit as part of ground water remediation

Reddish Brown

02* Abstraction well no 02 (AW -2) 22°15'37.81"N 73°02'07.61"E 35M Reddish Brown 03* Abstraction well no 04 (AW -4) 22°15'43.79"N 73° 02'14.15"E 50M Brownish 04* Abstraction well no 03 (AW -3) 22°15'43.37"N 73° 02'17.05"E 50M Brownish At the time of

pumping it has been observed that flow is intermittent.

05* Abstraction well no 06 (AW -6) 22 015 43.45"N 73 002 20.00"E 80M Reddish Tinge 06* Abstraction well no 07 (AW -7) 22 015 39.78"N 73 002 19.44"E 80M Reddish Tinge Flow is

intermittent. 07* Abstraction well no 05 (AW -5) 22 015 46.22"N 73 002 13.94"E 80M Reddish 08* Abstraction well no 02 (AW -2)

(11:10 hrs) 22°15'37.81"N 73° 2'7.61"E 35M Reddish Brown Same borewell

sample collected after @1 hr of continuous withdrawal

09* Abstraction well no 01 (AW -1) (11:20 hrs)

22 015 36.32"N 73 002 03.28"E 35M

Reddish Brown Same borewell sample collected after @1 hr of continuous withdrawal

Pag 3 of 8

Borewell water samples collected from vill: luna /Umayara and other industrial units premises located surrounding Huntsman International (India) P Ltd, Ta: Padra, Dist :Vadodara

Sr No Sample location Latitude Longitude Ownership Year of Use

Approx. Depth in

ft

Present use Remarks about Contamination Physical Appearance

10* Bore well at farm of Geetaben Patel (Himanshu Patel), Sr. No. 399, Vill. Luna, Ta. Padra, Dist. Vadodara OSW-8

22 º16 11.5"N 73 º02 19.3" E Geetaben Patel Himanshu Patel

1997 220ft 160ft water lifting

Irrigation Sicne last six year yellow shining water coming.

Dark yellow

11* Bore well of Kapilaben Ramanbhai Patel at Sr.No-353 Vill. Luna, Ta. Padra, Dist. Vadodara OSW-6

22 º15 50.7"N 73 º02 34.8"E Kapila Ben Ramanbhai Patel

Sept 2014

160 ft Cattle drinking and irrigation

Contamination Since beginning As informed by owner after some time of its withdrawal color change to reddish from dark yellow

Earlier Light Red Now dark yellow

12* Bore well at farm of Ghanshyambhai Ramanbhai Patel Sr.No-333 Vill. Luna, Ta. Padra, Dist. Vadodara OSW-11

22 º15 42.4"N 73 º02 28.1"E Ghanshyam bhai Ramanbhai Patel

May 2014

200ft Agriculture and cattle drinking

Yellowish water since beginning Yellowish

13* Bore well at farm of Gansyambhai Chandubhai Patel, Sr.No-426 Vill. Luna, Ta. Padra, Dist. Vadodara

22 º16 11.5"N 73 º02 19.3" E Patel Fuleshbhai Dhyabhai

Since 1990

250ft Agriculture Since last seven year Light yellow water

Yellowish

14* Bore well at farm of Rameshbhai Somabhai Padhiyar Sr.No-709, Vill. Umraya, Ta. Padra, Dist. Vadoara OSW-3

22 º16 13.72"N 73 º02 14.46" E Rameshbhai Somabhai Padhiyar

Since 2005

220ft Irrigation Since last thrteen years Reddish water

Pale yellow

15* Bore well at premises of M/s Prasad International Ltd, Sr. No- 378/A & 313/p, Vill.Luna, Ta. Padra, Dist. Vadodara OSW-12

22 º16 00.0"N 73 º02 16.1" E Prasad International

Since 2000

170ft Manufacturing Process

Since last six years Reddish water. Previously there was an industry namely Novena Chemicals engaged with production of dyes intermediate e.g. Gamma Acid.

Reddish tinge

16 Borewell of Bhailalbahi Padhiyar Opp: Prasad Int OSW-7(A)

22 º15 57.53"N 73 º02 21.95" E Bhailalbahi Padhiyar

2016 260ft Saling through tanker to surrounding uses

Colourless

17* Bore well at farm of Bhadreshbhai Bachubhai Sindha Sr.No-552a/b Vill.Umraya, Ta.Padra, Dist.Vadodara

22 º15 34.9"N 73 º02 10.9" E Bhadresh bhai Bachubhai Sindha

Since 2008

180ft Agriculture and cattle drinking

Since last ten years Reddish Water

Reddish

Pag 4 of 8

Sr No Sample location Latitude Longitude Ownership Year of Use

Approx. Depth in

ft

Present use Remarks about Contamination Physical Appearance

OSW-1

18 Borewell of Chemstar Organics , Umaraya Ta: Padra

22 0 15 42.36"N 73 001 56.04"E of Chemstar Organics

Since 1996

200ft Industrial purpose

Unit located adjacent to Huntsman international premises. This unit is not in operation @ since 1998 now planning for restart.

Colourless

19 Borewell of Umaraya Gram panchayat 22 0 15 39.97"N 73 001 49.79"E Grampanchayat Umaraya

2018 200ft Lifting from 160ft

Domestic purpose

Panchayat borewell newly started

Colourless

20 Borewell of Amoli Organics , Luna Ta: Padra

22 0 16 12.75"N 73 002 12.27"E Amoli Organics Ltd

2003 200ft Industrial purpose

-- Colourless

21 Bore well of Luna gram panchyat located at garden (bag) Vill. Luna, Ta. Padra, Dist.Vadodara. OSW-5

22 º15 38.0"N 73 º02 50.2"E of Luna gram panchyat

Since 2012

250 ft Domestic use Slight yellow Colourless

* Samples additionally coded and sent for HPLC/GC analysis to NABL approved laboratory of GPCB Gandhinagar. Samples of ground water collected as mentioned above were sent to NABL approved laboratory of GPCB – Vadodara for analysis purpose. Part of the some sample was additionally coded and also sent for HPLC/GC analysis to NABL approved laboratory of GPCB Gandhinagar for specific parameters vide this office letter bearing no. GPCB/VRD/LAB-Gen/24(7)/4059/2018 dt.27/12/2018. Google Map showing locations of groundwater sampling points and photographs taken during visit are enclosed herewith.

R P Rana M.V Soni M.U Patel Asst. Env. Engr. VO-Vadodara

Asst. Env. Engr. VO-Vadodara

Dy. Env. Engr. RO-Vadodara

Pag 5 of 8

Google Map showing Ground water sampling locations_Luna /Umaraya Ta: Padra, Dist : Vadodara

Pag 6 of 8

Photographs taken during visit dtd 26/12/2018 is enclosed herewith.

1) Abstraction well no 01– AW- 1 2) Abstraction well no 02- AW- 2

3) Abstraction well no 04 – AW- 4 4) Abstraction well no 03– AW- 3

5) Abstraction well no 06– AW- 6 6) Abstraction well no 07– AW- 7

Pag 7 of 8

7) Abstraction well no 05– AW- 5 8) B/W of Geetaben G. Patel, Luna (OSW - 8)

9) B/W of Kapilaben R. Patel, Sr. no. 353, Luna (OSW - 6)

10) B/W at farm of Ghanshyambhai R. Patel, Sr. no. 333, Luna (OSW - 11)

11)B/W of Ghansyambhai C. Patel Sr. no-426,

Luna 12) B/W of Rameshbhai S. Padhiyar, 709

Umaraya (OSW - 3)

Pag 8 of 8

13) B/W of Prasad Int. Ltd. (OSW - 12) 14) B/W of Bhailalbhai Padhiyar, Opp. Prasad Int. (OSW – 7(A))

15) B/W of Bhadreshbhai Sindha,Umaraya

(OSW - 1) 16) B/W of Chemstar Organics, Umaraya

17 B/W of Umaraya Gram Panchayt

18) B/W of Amoli Organics, Luna

19 B/W of Luna Gram Panchayat near garden (Bag) (OSW - 5)

Sample ID:249415 - Analysis Completion:22/01/2019

ANALYSIS REPORT FOR

WATER / WASTE WATER SAMPLE

Dyes and Dye- Intermediates / LAB Inward : 31944

Gujarat Pollution Control Board,

Vadodara

GERI Compound

Race Course Road

Vadodara - 390007

Accreditation Standards & NABL Certificate Details : Biology & Chemical / TC-5287 / Issue: 17/03/2017 / Validity: 16/03/2019

TEST REPORT

Test Report No. : 31944 Date: 22/01/2019

3. Nature of Sample

4. Sample Collected By

5. Quantity of Sample Received

6. Code No. of the Sample

7. Date & Time of Collection & Inwarding

8. Date of Start & Completion of Analysis

9. Sampling Point

10. Flow Details (Remarks)

11. Mode of Disposal

12. Ultimate Receiving Body

13. Temperature on Collection

14. Carboys Nos for

15. Water Consumption & W.W.G (KLPD)

1. Name of the Customer

2. Address

Range of TestingTest MethodSr ResultUnitParameter

Ambient oC - 60 oCIS: 3025 (Part – 9) – 1984(Reaffirmed 2006)CentigradeTemperature 1 25

1 – 14 pH value As on digital pH meter.4500 H+ B APHA Standard Methods 22nd edi.2012pH UnitspH 2 7.74

2 - to 99 Hazen & 1-500 hazen2120 B APHA Standard Methods 22nd edi. 2012Pt.Co.Sc.Colour 3 NA

10 – 200000 mg/LGravimetric method. (2540 C APHA Standard Methods 22nd edi.)2012mg/lTotal Dissolved Solids 4 10348

2 – 10000 mg/LGravimetric method. (2540 D APHA Standard Methods 22nd edi.)2012mg/lSuspended Solids 5 10

1 - 2000 mg/l.1).Titrimetric method (4500 NH3 B & C APHA Standard Methods 22nd edi.)-2012mg/lAmmonical Nitrogen 6 1.68

1 - 50000 mg/lArgentometric method. (4500 Cl? B APHA Standard Methods 22nd edi.)-2012mg/lChloride 7 2600

2-40mg/lAPHA(22nd edi)4500 SO4 Emg/lSulphate 8 4288

5.0- 50000 mg/lAPHA (22nd Edition)- 5220 B Open Reflux Method-2012mg/lChemical Oxygen Demand 9 2609

01 – 1000 mg/lLiquid – Liquid Partition Gravimetric method. (5520 B APHA Standard Methods 22nd edi.)-2012mg/lOil & Grease 10 BDL

0.1 – 50 mg/l4 Amino Antipyrene method without Chloroform Extraction (Direct Photometric method) (5530 D APHA Standard Methods 22nd edi.) -2012mg/lPhenolic Compounds 11 0.44

0.02-150mg/l(3111 B APHA Standard methods 21st edi)mg/lIron 12 1.00

05–50000 mg/l3 – Day BOD test. (IS 3025 (Part 44) 1993 Reaffirmed 1999)-2009mg/lB.O.D (3 Days 27oC) 13 71

: REP-Representative/Grab, (Insp Type : ROU-Routine Visit)

: M.U.PATEL,DEE

: 5 Lit.

: 249415

: 26/12/2018 , (1120 to 1120) & 27/12/2018

: 28/12/2018 & 22/01/2019

: From Abstraction well AW-1 ~ (11:20 hrs)

: ---

: ---

: No generation of industrial wastewater

: 25 & pH Range on pH Strip :@ 7-8 on pH strip

: Barcode & Color & Appearance :Reddish brown

: Ind :1723.000 , Dom :88.000 & Ind :1149.000 , Dom :66.000

: Huntsman International (India) P. Ltd. (formerly Baroda Textile Effect Limited) - 22289

: -,VILL : UMRAYA,-

Umaraya-391440, Taluka : Padra, District : Vadodara, GIDC : Not In Gidc

Laboratory Remarks : Approved By:236-lab_236 Dt.: 22/01/2019

D. N. Vasadia, Lab Head

11/03/2019N I C

Note :

1. * - These parameters are NOT covered under the scope of NABL.

2. The results refer only to the tested samples and applicable parameters. Endorsement of products is neither inferred nor implied.

3. Samples will be destroyed after 10 days from the date of issue of test report unless otherwise specified.

4. This report is not to be reproduced wholly or in part or used in any advertising media without the permission of the Board in writing.

5. The Board is not responsible for the authenticity for the samples not collected by the Board’s officials.

6. Total liability of our laboratory is limited to the invoiced amount. Any dispute arising out of this report is subject to

Gujarat Jurisdiction only.

7. Permissible Limits: as per Schedule VI of EPA Rules, 1986 as ammended by Second and Third ammendment 1993 for Effluents

8. Physicochemical and microbiological parameters, Std.Methods for Water and Waste Water- 22nd Edition by APHA.

9. Bioassay test (for toxicity) -IS:6582:Part-2:2001; Reaffirmed 2007.

sample collected after @1 hr of pumping startedField Observation :

Sample ID:249414 - Analysis Completion:22/01/2019

ANALYSIS REPORT FOR

WATER / WASTE WATER SAMPLE

Dyes and Dye- Intermediates / LAB Inward : 31943

Gujarat Pollution Control Board,

Vadodara

GERI Compound

Race Course Road

Vadodara - 390007

Accreditation Standards & NABL Certificate Details : Biology & Chemical / TC-5287 / Issue: 17/03/2017 / Validity: 16/03/2019

TEST REPORT

Test Report No. : 31943 Date: 22/01/2019

3. Nature of Sample

4. Sample Collected By

5. Quantity of Sample Received

6. Code No. of the Sample

7. Date & Time of Collection & Inwarding

8. Date of Start & Completion of Analysis

9. Sampling Point

10. Flow Details (Remarks)

11. Mode of Disposal

12. Ultimate Receiving Body

13. Temperature on Collection

14. Carboys Nos for

15. Water Consumption & W.W.G (KLPD)

1. Name of the Customer

2. Address

Range of TestingTest MethodSr ResultUnitParameter

Ambient oC - 60 oCIS: 3025 (Part – 9) – 1984(Reaffirmed 2006)CentigradeTemperature 1 25

1 – 14 pH value As on digital pH meter.4500 H+ B APHA Standard Methods 22nd edi.2012pH UnitspH 2 7.87

2 - to 99 Hazen & 1-500 hazen2120 B APHA Standard Methods 22nd edi. 2012Pt.Co.Sc.Colour 3 1500

10 – 200000 mg/LGravimetric method. (2540 C APHA Standard Methods 22nd edi.)2012mg/lTotal Dissolved Solids 4 10294

2 – 10000 mg/LGravimetric method. (2540 D APHA Standard Methods 22nd edi.)2012mg/lSuspended Solids 5 20

1 - 2000 mg/l.1).Titrimetric method (4500 NH3 B & C APHA Standard Methods 22nd edi.)-2012mg/lAmmonical Nitrogen 6 2.24

1 - 50000 mg/lArgentometric method. (4500 Cl? B APHA Standard Methods 22nd edi.)-2012mg/lChloride 7 2600

2-40mg/lAPHA(22nd edi)4500 SO4 Emg/lSulphate 8 1401

5.0- 50000 mg/lAPHA (22nd Edition)- 5220 B Open Reflux Method-2012mg/lChemical Oxygen Demand 9 2592

01 – 1000 mg/lLiquid – Liquid Partition Gravimetric method. (5520 B APHA Standard Methods 22nd edi.)-2012mg/lOil & Grease 10 BDL

0.1 – 50 mg/l4 Amino Antipyrene method without Chloroform Extraction (Direct Photometric method) (5530 D APHA Standard Methods 22nd edi.) -2012mg/lPhenolic Compounds 11 0.46

0.02-150mg/l(3111 B APHA Standard methods 21st edi)mg/lIron 12 0.91

05–50000 mg/l3 – Day BOD test. (IS 3025 (Part 44) 1993 Reaffirmed 1999)-2009mg/lB.O.D (3 Days 27oC) 13 67

: REP-Representative/Grab, (Insp Type : ROU-Routine Visit)

: M.U.PATEL,DEE

: 5 Lit.

: 249414

: 26/12/2018 , (1110 to 1110) & 27/12/2018

: 28/12/2018 & 22/01/2019

: From Abstraction well AW-2 ~ (11:10 hrs)

: ---

: ---

: No generation of industrial wastewater

: 25 & pH Range on pH Strip :@ 7-8 on pH strip

: Barcode & Color & Appearance :Reddish brown

: Ind :1723.000 , Dom :88.000 & Ind :1149.000 , Dom :66.000

: Huntsman International (India) P. Ltd. (formerly Baroda Textile Effect Limited) - 22289

: -,VILL : UMRAYA,-

Umaraya-391440, Taluka : Padra, District : Vadodara, GIDC : Not In Gidc

Laboratory Remarks : Approved By:236-lab_236 Dt.: 22/01/2019

D. N. Vasadia, Lab Head

11/03/2019N I C

Note :

1. * - These parameters are NOT covered under the scope of NABL.

2. The results refer only to the tested samples and applicable parameters. Endorsement of products is neither inferred nor implied.

3. Samples will be destroyed after 10 days from the date of issue of test report unless otherwise specified.

4. This report is not to be reproduced wholly or in part or used in any advertising media without the permission of the Board in writing.

5. The Board is not responsible for the authenticity for the samples not collected by the Board’s officials.

6. Total liability of our laboratory is limited to the invoiced amount. Any dispute arising out of this report is subject to

Gujarat Jurisdiction only.

7. Permissible Limits: as per Schedule VI of EPA Rules, 1986 as ammended by Second and Third ammendment 1993 for Effluents

8. Physicochemical and microbiological parameters, Std.Methods for Water and Waste Water- 22nd Edition by APHA.

9. Bioassay test (for toxicity) -IS:6582:Part-2:2001; Reaffirmed 2007.

sample collected after @45min of pumping startedField Observation :

Sample ID:249410 - Analysis Completion:22/01/2019

ANALYSIS REPORT FOR

WATER / WASTE WATER SAMPLE

Dyes and Dye- Intermediates / LAB Inward : 31938

Gujarat Pollution Control Board,

Vadodara

GERI Compound

Race Course Road

Vadodara - 390007

Accreditation Standards & NABL Certificate Details : Biology & Chemical / TC-5287 / Issue: 17/03/2017 / Validity: 16/03/2019

TEST REPORT

Test Report No. : 31938 Date: 22/01/2019

3. Nature of Sample

4. Sample Collected By

5. Quantity of Sample Received

6. Code No. of the Sample

7. Date & Time of Collection & Inwarding

8. Date of Start & Completion of Analysis

9. Sampling Point

10. Flow Details (Remarks)

11. Mode of Disposal

12. Ultimate Receiving Body

13. Temperature on Collection

14. Carboys Nos for

15. Water Consumption & W.W.G (KLPD)

1. Name of the Customer

2. Address

Range of TestingTest MethodSr ResultUnitParameter

Ambient oC - 60 oCIS: 3025 (Part – 9) – 1984(Reaffirmed 2006)CentigradeTemperature 1 24

1 – 14 pH value As on digital pH meter.4500 H+ B APHA Standard Methods 22nd edi.2012pH UnitspH 2 7.92

2 - to 99 Hazen & 1-500 hazen2120 B APHA Standard Methods 22nd edi. 2012Pt.Co.Sc.Colour 3 250

10 – 200000 mg/LGravimetric method. (2540 C APHA Standard Methods 22nd edi.)2012mg/lTotal Dissolved Solids 4 4346

2 – 10000 mg/LGravimetric method. (2540 D APHA Standard Methods 22nd edi.)2012mg/lSuspended Solids 5 10

1 - 2000 mg/l.1).Titrimetric method (4500 NH3 B & C APHA Standard Methods 22nd edi.)-2012mg/lAmmonical Nitrogen 6 2.24

1 - 50000 mg/lArgentometric method. (4500 Cl? B APHA Standard Methods 22nd edi.)-2012mg/lChloride 7 1200

2-40mg/lAPHA(22nd edi)4500 SO4 Emg/lSulphate 8 700

5.0- 50000 mg/lAPHA (22nd Edition)- 5220 B Open Reflux Method-2012mg/lChemical Oxygen Demand 9 296

01 – 1000 mg/lLiquid – Liquid Partition Gravimetric method. (5520 B APHA Standard Methods 22nd edi.)-2012mg/lOil & Grease 10 BDL

0.1 – 50 mg/l4 Amino Antipyrene method without Chloroform Extraction (Direct Photometric method) (5530 D APHA Standard Methods 22nd edi.) -2012mg/lPhenolic Compounds 11 bdl

0.02-150mg/l(3111 B APHA Standard methods 21st edi)mg/lIron 12 0.48

05–50000 mg/l3 – Day BOD test. (IS 3025 (Part 44) 1993 Reaffirmed 1999)-2009mg/lB.O.D (3 Days 27oC) 13 21

: REP-Representative/Grab, (Insp Type : ROU-Routine Visit)

: M.U.PATEL,DEE

: 5 Lit.

: 249410

: 26/12/2018 , (1030 to 1030) & 27/12/2018

: 28/12/2018 & 22/01/2019

: From Abstraction well AW-4 ~ .

: ---

: ---

: No generation of industrial wastewater

: 24 & pH Range on pH Strip :@ 7-8 on pH strip

: Barcode & Color & Appearance :Brownish

: Ind :1723.000 , Dom :88.000 & Ind :1149.000 , Dom :66.000

: Huntsman International (India) P. Ltd. (formerly Baroda Textile Effect Limited) - 22289

: -,VILL : UMRAYA,-

Umaraya-391440, Taluka : Padra, District : Vadodara, GIDC : Not In Gidc

Laboratory Remarks : Approved By:236-lab_236 Dt.: 22/01/2019

D. N. Vasadia, Lab Head

11/03/2019N I C

Note :

1. * - These parameters are NOT covered under the scope of NABL.

2. The results refer only to the tested samples and applicable parameters. Endorsement of products is neither inferred nor implied.

3. Samples will be destroyed after 10 days from the date of issue of test report unless otherwise specified.

4. This report is not to be reproduced wholly or in part or used in any advertising media without the permission of the Board in writing.

5. The Board is not responsible for the authenticity for the samples not collected by the Board’s officials.

6. Total liability of our laboratory is limited to the invoiced amount. Any dispute arising out of this report is subject to

Gujarat Jurisdiction only.

7. Permissible Limits: as per Schedule VI of EPA Rules, 1986 as ammended by Second and Third ammendment 1993 for Effluents

8. Physicochemical and microbiological parameters, Std.Methods for Water and Waste Water- 22nd Edition by APHA.

9. Bioassay test (for toxicity) -IS:6582:Part-2:2001; Reaffirmed 2007.

Field Observation :

Sample ID:249411 - Analysis Completion:10/01/2019

ANALYSIS REPORT FOR

WATER / WASTE WATER SAMPLE

Dyes and Dye- Intermediates / LAB Inward : 31939

Gujarat Pollution Control Board,

Vadodara

GERI Compound

Race Course Road

Vadodara - 390007

Accreditation Standards & NABL Certificate Details : Biology & Chemical / TC-5287 / Issue: 17/03/2017 / Validity: 16/03/2019

TEST REPORT

Test Report No. : 31939 Date: 11/01/2019

3. Nature of Sample

4. Sample Collected By

5. Quantity of Sample Received

6. Code No. of the Sample

7. Date & Time of Collection & Inwarding

8. Date of Start & Completion of Analysis

9. Sampling Point

10. Flow Details (Remarks)

11. Mode of Disposal

12. Ultimate Receiving Body

13. Temperature on Collection

14. Carboys Nos for

15. Water Consumption & W.W.G (KLPD)

1. Name of the Customer

2. Address

Range of TestingTest MethodSr ResultUnitParameter

Ambient oC - 60 oCIS: 3025 (Part – 9) – 1984(Reaffirmed 2006)CentigradeTemperature 1 24

1 – 14 pH value As on digital pH meter.4500 H+ B APHA Standard Methods 22nd edi.2012pH UnitspH 2 8.15

2 - to 99 Hazen & 1-500 hazen2120 B APHA Standard Methods 22nd edi. 2012Pt.Co.Sc.Colour 3 250

10 – 200000 mg/LGravimetric method. (2540 C APHA Standard Methods 22nd edi.)2012mg/lTotal Dissolved Solids 4 4964

2 – 10000 mg/LGravimetric method. (2540 D APHA Standard Methods 22nd edi.)2012mg/lSuspended Solids 5 06

1 - 2000 mg/l.1).Titrimetric method (4500 NH3 B & C APHA Standard Methods 22nd edi.)-2012mg/lAmmonical Nitrogen 6 1.12

1 - 50000 mg/lArgentometric method. (4500 Cl? B APHA Standard Methods 22nd edi.)-2012mg/lChloride 7 1220

2-40mg/lAPHA(22nd edi)4500 SO4 Emg/lSulphate 8 876

5.0- 50000 mg/lAPHA (22nd Edition)- 5220 B Open Reflux Method-2012mg/lChemical Oxygen Demand 9 204

01 – 1000 mg/lLiquid – Liquid Partition Gravimetric method. (5520 B APHA Standard Methods 22nd edi.)-2012mg/lOil & Grease 10 BDL

0.1 – 50 mg/l4 Amino Antipyrene method without Chloroform Extraction (Direct Photometric method) (5530 D APHA Standard Methods 22nd edi.) -2012mg/lPhenolic Compounds 11 bdl

0.02-150mg/l(3111 B APHA Standard methods 21st edi)mg/lIron 12 0.7

05–50000 mg/l3 – Day BOD test. (IS 3025 (Part 44) 1993 Reaffirmed 1999)-2009mg/lB.O.D (3 Days 27oC) 13 12

: REP-Representative/Grab, (Insp Type : ROU-Routine Visit)

: M.U.PATEL,DEE

: 5 Lit.

: 249411

: 26/12/2018 , (1040 to 1040) & 27/12/2018

: 28/12/2018 & 10/01/2019

: From Abstraction well AW-3 ~ .

: ---

: ---

: No generation of industrial wastewater

: 24 & pH Range on pH Strip :@ 7-8 on pH strip

: Barcode & Color & Appearance :Brownish

: Ind :1723.000 , Dom :88.000 & Ind :1149.000 , Dom :66.000

: Huntsman International (India) P. Ltd. (formerly Baroda Textile Effect Limited) - 22289

: -,VILL : UMRAYA,-

Umaraya-391440, Taluka : Padra, District : Vadodara, GIDC : Not In Gidc

Laboratory Remarks : Approved By:236-lab_236 Dt.: 11/01/2019

D. N. Vasadia, Lab Head

11/03/2019N I C

Note :

1. * - These parameters are NOT covered under the scope of NABL.

2. The results refer only to the tested samples and applicable parameters. Endorsement of products is neither inferred nor implied.

3. Samples will be destroyed after 10 days from the date of issue of test report unless otherwise specified.

4. This report is not to be reproduced wholly or in part or used in any advertising media without the permission of the Board in writing.

5. The Board is not responsible for the authenticity for the samples not collected by the Board’s officials.

6. Total liability of our laboratory is limited to the invoiced amount. Any dispute arising out of this report is subject to

Gujarat Jurisdiction only.

7. Permissible Limits: as per Schedule VI of EPA Rules, 1986 as ammended by Second and Third ammendment 1993 for Effluents

8. Physicochemical and microbiological parameters, Std.Methods for Water and Waste Water- 22nd Edition by APHA.

9. Bioassay test (for toxicity) -IS:6582:Part-2:2001; Reaffirmed 2007.

flow of water is not continuous during pumping it is found intermittentField Observation :

Sample ID:249412 - Analysis Completion:10/01/2019

ANALYSIS REPORT FOR

WATER / WASTE WATER SAMPLE

Dyes and Dye- Intermediates / LAB Inward : 31940

Gujarat Pollution Control Board,

Vadodara

GERI Compound

Race Course Road

Vadodara - 390007

Accreditation Standards & NABL Certificate Details : Biology & Chemical / TC-5287 / Issue: 17/03/2017 / Validity: 16/03/2019

TEST REPORT

Test Report No. : 31940 Date: 14/01/2019

3. Nature of Sample

4. Sample Collected By

5. Quantity of Sample Received

6. Code No. of the Sample

7. Date & Time of Collection & Inwarding

8. Date of Start & Completion of Analysis

9. Sampling Point

10. Flow Details (Remarks)

11. Mode of Disposal

12. Ultimate Receiving Body

13. Temperature on Collection

14. Carboys Nos for

15. Water Consumption & W.W.G (KLPD)

1. Name of the Customer

2. Address

Range of TestingTest MethodSr ResultUnitParameter

Ambient oC - 60 oCIS: 3025 (Part – 9) – 1984(Reaffirmed 2006)CentigradeTemperature 1 24

1 – 14 pH value As on digital pH meter.4500 H+ B APHA Standard Methods 22nd edi.2012pH UnitspH 2 7.91

2 - to 99 Hazen & 1-500 hazen2120 B APHA Standard Methods 22nd edi. 2012Pt.Co.Sc.Colour 3 375

10 – 200000 mg/LGravimetric method. (2540 C APHA Standard Methods 22nd edi.)2012mg/lTotal Dissolved Solids 4 4708

2 – 10000 mg/LGravimetric method. (2540 D APHA Standard Methods 22nd edi.)2012mg/lSuspended Solids 5 04

1 - 2000 mg/l.1).Titrimetric method (4500 NH3 B & C APHA Standard Methods 22nd edi.)-2012mg/lAmmonical Nitrogen 6 19.6

1 - 50000 mg/lArgentometric method. (4500 Cl? B APHA Standard Methods 22nd edi.)-2012mg/lChloride 7 1280

2-40mg/lAPHA(22nd edi)4500 SO4 Emg/lSulphate 8 433

5.0- 50000 mg/lAPHA (22nd Edition)- 5220 B Open Reflux Method-2012mg/lChemical Oxygen Demand 9 209

01 – 1000 mg/lLiquid – Liquid Partition Gravimetric method. (5520 B APHA Standard Methods 22nd edi.)-2012mg/lOil & Grease 10 BDL

0.1 – 50 mg/l4 Amino Antipyrene method without Chloroform Extraction (Direct Photometric method) (5530 D APHA Standard Methods 22nd edi.) -2012mg/lPhenolic Compounds 11 0.14

0.02-150mg/l(3111 B APHA Standard methods 21st edi)mg/lIron 12 0.88

05–50000 mg/l3 – Day BOD test. (IS 3025 (Part 44) 1993 Reaffirmed 1999)-2009mg/lB.O.D (3 Days 27oC) 13 10

: REP-Representative/Grab, (Insp Type : ROU-Routine Visit)

: M.U.PATEL,DEE

: 5 Lit.

: 249412

: 26/12/2018 , (1045 to 1045) & 27/12/2018

: 28/12/2018 & 10/01/2019

: From Abstraction well AW-6 ~ .

: ---

: ---

: No generation of industrial wastewater

: 24 & pH Range on pH Strip :@ 7-8 on pH strip

: Barcode & Color & Appearance :Reddish tinge

: Ind :1723.000 , Dom :88.000 & Ind :1149.000 , Dom :66.000

: Huntsman International (India) P. Ltd. (formerly Baroda Textile Effect Limited) - 22289

: -,VILL : UMRAYA,-

Umaraya-391440, Taluka : Padra, District : Vadodara, GIDC : Not In Gidc

Laboratory Remarks : Approved By:236-lab_236 Dt.: 14/01/2019

D. N. Vasadia, Lab Head

11/03/2019N I C

Note :

1. * - These parameters are NOT covered under the scope of NABL.

2. The results refer only to the tested samples and applicable parameters. Endorsement of products is neither inferred nor implied.

3. Samples will be destroyed after 10 days from the date of issue of test report unless otherwise specified.

4. This report is not to be reproduced wholly or in part or used in any advertising media without the permission of the Board in writing.

5. The Board is not responsible for the authenticity for the samples not collected by the Board’s officials.

6. Total liability of our laboratory is limited to the invoiced amount. Any dispute arising out of this report is subject to

Gujarat Jurisdiction only.

7. Permissible Limits: as per Schedule VI of EPA Rules, 1986 as ammended by Second and Third ammendment 1993 for Effluents

8. Physicochemical and microbiological parameters, Std.Methods for Water and Waste Water- 22nd Edition by APHA.

9. Bioassay test (for toxicity) -IS:6582:Part-2:2001; Reaffirmed 2007.

Field Observation :

Sample ID:249409 - Analysis Completion:10/01/2019

ANALYSIS REPORT FOR

WATER / WASTE WATER SAMPLE

Dyes and Dye- Intermediates / LAB Inward : 31941

Gujarat Pollution Control Board,

Vadodara

GERI Compound

Race Course Road

Vadodara - 390007

Accreditation Standards & NABL Certificate Details : Biology & Chemical / TC-5287 / Issue: 17/03/2017 / Validity: 16/03/2019

TEST REPORT

Test Report No. : 31941 Date: 14/01/2019

3. Nature of Sample

4. Sample Collected By

5. Quantity of Sample Received

6. Code No. of the Sample

7. Date & Time of Collection & Inwarding

8. Date of Start & Completion of Analysis

9. Sampling Point

10. Flow Details (Remarks)

11. Mode of Disposal

12. Ultimate Receiving Body

13. Temperature on Collection

14. Carboys Nos for

15. Water Consumption & W.W.G (KLPD)

1. Name of the Customer

2. Address

Range of TestingTest MethodSr ResultUnitParameter

Ambient oC - 60 oCIS: 3025 (Part – 9) – 1984(Reaffirmed 2006)CentigradeTemperature 1 24

1 – 14 pH value As on digital pH meter.4500 H+ B APHA Standard Methods 22nd edi.2012pH UnitspH 2 8.05

2 - to 99 Hazen & 1-500 hazen2120 B APHA Standard Methods 22nd edi. 2012Pt.Co.Sc.Colour 3 37.5

10 – 200000 mg/LGravimetric method. (2540 C APHA Standard Methods 22nd edi.)2012mg/lTotal Dissolved Solids 4 3020

2 – 10000 mg/LGravimetric method. (2540 D APHA Standard Methods 22nd edi.)2012mg/lSuspended Solids 5 06

1 - 2000 mg/l.1).Titrimetric method (4500 NH3 B & C APHA Standard Methods 22nd edi.)-2012mg/lAmmonical Nitrogen 6 1.12

1 - 50000 mg/lArgentometric method. (4500 Cl? B APHA Standard Methods 22nd edi.)-2012mg/lChloride 7 820

2-40mg/lAPHA(22nd edi)4500 SO4 Emg/lSulphate 8 233

5.0- 50000 mg/lAPHA (22nd Edition)- 5220 B Open Reflux Method-2012mg/lChemical Oxygen Demand 9 78

01 – 1000 mg/lLiquid – Liquid Partition Gravimetric method. (5520 B APHA Standard Methods 22nd edi.)-2012mg/lOil & Grease 10 BDL

0.1 – 50 mg/l4 Amino Antipyrene method without Chloroform Extraction (Direct Photometric method) (5530 D APHA Standard Methods 22nd edi.) -2012mg/lPhenolic Compounds 11 bdl

0.02-150mg/l(3111 B APHA Standard methods 21st edi)mg/lIron 12 0.28

05–50000 mg/l3 – Day BOD test. (IS 3025 (Part 44) 1993 Reaffirmed 1999)-2009mg/lB.O.D (3 Days 27oC) 13 <5

: REP-Representative/Grab, (Insp Type : ROU-Routine Visit)

: M.U.PATEL,DEE

: 5 Lit.

: 249409

: 26/12/2018 , (1050 to 1050) & 27/12/2018

: 28/12/2018 & 10/01/2019

: From Abstraction well AW-7 ~ .

: -

: -

: No generation of industrial wastewater

: 24 & pH Range on pH Strip :@ 7-8 on pH strip

: Barcode & Color & Appearance :Reddish tinge

: Ind :1723.000 , Dom :88.000 & Ind :1149.000 , Dom :66.000

: Huntsman International (India) P. Ltd. (formerly Baroda Textile Effect Limited) - 22289

: -,VILL : UMRAYA,-

Umaraya-391440, Taluka : Padra, District : Vadodara, GIDC : Not In Gidc

Laboratory Remarks : Approved By:236-lab_236 Dt.: 14/01/2019

D. N. Vasadia, Lab Head

11/03/2019N I C

Note :

1. * - These parameters are NOT covered under the scope of NABL.

2. The results refer only to the tested samples and applicable parameters. Endorsement of products is neither inferred nor implied.

3. Samples will be destroyed after 10 days from the date of issue of test report unless otherwise specified.

4. This report is not to be reproduced wholly or in part or used in any advertising media without the permission of the Board in writing.

5. The Board is not responsible for the authenticity for the samples not collected by the Board’s officials.

6. Total liability of our laboratory is limited to the invoiced amount. Any dispute arising out of this report is subject to

Gujarat Jurisdiction only.

7. Permissible Limits: as per Schedule VI of EPA Rules, 1986 as ammended by Second and Third ammendment 1993 for Effluents

8. Physicochemical and microbiological parameters, Std.Methods for Water and Waste Water- 22nd Edition by APHA.

9. Bioassay test (for toxicity) -IS:6582:Part-2:2001; Reaffirmed 2007.

Field Observation :

Sample ID:249413 - Analysis Completion:22/01/2019

ANALYSIS REPORT FOR

WATER / WASTE WATER SAMPLE

Dyes and Dye- Intermediates / LAB Inward : 31942

Gujarat Pollution Control Board,

Vadodara

GERI Compound

Race Course Road

Vadodara - 390007

Accreditation Standards & NABL Certificate Details : Biology & Chemical / TC-5287 / Issue: 17/03/2017 / Validity: 16/03/2019

TEST REPORT

Test Report No. : 31942 Date: 22/01/2019

3. Nature of Sample

4. Sample Collected By

5. Quantity of Sample Received

6. Code No. of the Sample

7. Date & Time of Collection & Inwarding

8. Date of Start & Completion of Analysis

9. Sampling Point

10. Flow Details (Remarks)

11. Mode of Disposal

12. Ultimate Receiving Body

13. Temperature on Collection

14. Carboys Nos for

15. Water Consumption & W.W.G (KLPD)

1. Name of the Customer

2. Address

Range of TestingTest MethodSr ResultUnitParameter

Ambient oC - 60 oCIS: 3025 (Part – 9) – 1984(Reaffirmed 2006)CentigradeTemperature 1 25

1 – 14 pH value As on digital pH meter.4500 H+ B APHA Standard Methods 22nd edi.2012pH UnitspH 2 7.84

2 - to 99 Hazen & 1-500 hazen2120 B APHA Standard Methods 22nd edi. 2012Pt.Co.Sc.Colour 3 NA

10 – 200000 mg/LGravimetric method. (2540 C APHA Standard Methods 22nd edi.)2012mg/lTotal Dissolved Solids 4 3156

2 – 10000 mg/LGravimetric method. (2540 D APHA Standard Methods 22nd edi.)2012mg/lSuspended Solids 5 04

1 - 2000 mg/l.1).Titrimetric method (4500 NH3 B & C APHA Standard Methods 22nd edi.)-2012mg/lAmmonical Nitrogen 6 1.68

1 - 50000 mg/lArgentometric method. (4500 Cl? B APHA Standard Methods 22nd edi.)-2012mg/lChloride 7 640

2-40mg/lAPHA(22nd edi)4500 SO4 Emg/lSulphate 8 1039

5.0- 50000 mg/lAPHA (22nd Edition)- 5220 B Open Reflux Method-2012mg/lChemical Oxygen Demand 9 105

01 – 1000 mg/lLiquid – Liquid Partition Gravimetric method. (5520 B APHA Standard Methods 22nd edi.)-2012mg/lOil & Grease 10 BDL

0.1 – 50 mg/l4 Amino Antipyrene method without Chloroform Extraction (Direct Photometric method) (5530 D APHA Standard Methods 22nd edi.) -2012mg/lPhenolic Compounds 11 0.21

0.02-150mg/l(3111 B APHA Standard methods 21st edi)mg/lIron 12 0.48

05–50000 mg/l3 – Day BOD test. (IS 3025 (Part 44) 1993 Reaffirmed 1999)-2009mg/lB.O.D (3 Days 27oC) 13 8

: REP-Representative/Grab, (Insp Type : ROU-Routine Visit)

: M.U.PATEL,DEE

: 5 Lit.

: 249413

: 26/12/2018 , (1100 to 1100) & 27/12/2018

: 28/12/2018 & 22/01/2019

: From Abstraction well AW-5 ~ .

: ---

: ---

: No generation of industrial wastewater

: 25 & pH Range on pH Strip :@ 7-8 on pH strip

: Barcode & Color & Appearance :Reddish tinge

: Ind :1723.000 , Dom :88.000 & Ind :1149.000 , Dom :66.000

: Huntsman International (India) P. Ltd. (formerly Baroda Textile Effect Limited) - 22289

: -,VILL : UMRAYA,-

Umaraya-391440, Taluka : Padra, District : Vadodara, GIDC : Not In Gidc

Laboratory Remarks : Approved By:236-lab_236 Dt.: 22/01/2019

D. N. Vasadia, Lab Head

11/03/2019N I C

Note :

1. * - These parameters are NOT covered under the scope of NABL.

2. The results refer only to the tested samples and applicable parameters. Endorsement of products is neither inferred nor implied.

3. Samples will be destroyed after 10 days from the date of issue of test report unless otherwise specified.

4. This report is not to be reproduced wholly or in part or used in any advertising media without the permission of the Board in writing.

5. The Board is not responsible for the authenticity for the samples not collected by the Board’s officials.

6. Total liability of our laboratory is limited to the invoiced amount. Any dispute arising out of this report is subject to

Gujarat Jurisdiction only.

7. Permissible Limits: as per Schedule VI of EPA Rules, 1986 as ammended by Second and Third ammendment 1993 for Effluents

8. Physicochemical and microbiological parameters, Std.Methods for Water and Waste Water- 22nd Edition by APHA.

9. Bioassay test (for toxicity) -IS:6582:Part-2:2001; Reaffirmed 2007.

Field Observation :

Sample ID:249407 - Analysis Completion:22/01/2019

ANALYSIS REPORT FOR

WATER / WASTE WATER SAMPLE

Dyes and Dye- Intermediates / LAB Inward : 31937

Gujarat Pollution Control Board,

Vadodara

GERI Compound

Race Course Road

Vadodara - 390007

Accreditation Standards & NABL Certificate Details : Biology & Chemical / TC-5287 / Issue: 17/03/2017 / Validity: 16/03/2019

TEST REPORT

Test Report No. : 31937 Date: 22/01/2019

3. Nature of Sample

4. Sample Collected By

5. Quantity of Sample Received

6. Code No. of the Sample

7. Date & Time of Collection & Inwarding

8. Date of Start & Completion of Analysis

9. Sampling Point

10. Flow Details (Remarks)

11. Mode of Disposal

12. Ultimate Receiving Body

13. Temperature on Collection

14. Carboys Nos for

15. Water Consumption & W.W.G (KLPD)

1. Name of the Customer

2. Address

Range of TestingTest MethodSr ResultUnitParameter

Ambient oC - 60 oCIS: 3025 (Part – 9) – 1984(Reaffirmed 2006)CentigradeTemperature 1 24

1 – 14 pH value As on digital pH meter.4500 H+ B APHA Standard Methods 22nd edi.2012pH UnitspH 2 7.91

2 - to 99 Hazen & 1-500 hazen2120 B APHA Standard Methods 22nd edi. 2012Pt.Co.Sc.Colour 3 1500

10 – 200000 mg/LGravimetric method. (2540 C APHA Standard Methods 22nd edi.)2012mg/lTotal Dissolved Solids 4 11090

2 – 10000 mg/LGravimetric method. (2540 D APHA Standard Methods 22nd edi.)2012mg/lSuspended Solids 5 32

1 - 2000 mg/l.1).Titrimetric method (4500 NH3 B & C APHA Standard Methods 22nd edi.)-2012mg/lAmmonical Nitrogen 6 2.24

1 - 50000 mg/lArgentometric method. (4500 Cl? B APHA Standard Methods 22nd edi.)-2012mg/lChloride 7 2100

2-40mg/lAPHA(22nd edi)4500 SO4 Emg/lSulphate 8 1720

5.0- 50000 mg/lAPHA (22nd Edition)- 5220 B Open Reflux Method-2012mg/lChemical Oxygen Demand 9 2959

01 – 1000 mg/lLiquid – Liquid Partition Gravimetric method. (5520 B APHA Standard Methods 22nd edi.)-2012mg/lOil & Grease 10 BDL

0.1 – 50 mg/l4 Amino Antipyrene method without Chloroform Extraction (Direct Photometric method) (5530 D APHA Standard Methods 22nd edi.) -2012mg/lPhenolic Compounds 11 0.42

0.02-150mg/l(3111 B APHA Standard methods 21st edi)mg/lIron 12 1.10

05–50000 mg/l3 – Day BOD test. (IS 3025 (Part 44) 1993 Reaffirmed 1999)-2009mg/lB.O.D (3 Days 27oC) 13 81

: REP-Representative/Grab, (Insp Type : ROU-Routine Visit)

: M.U.PATEL,DEE

: 5 Lit.

: 249407

: 26/12/2018 , (1020 to 1020) & 27/12/2018

: 28/12/2018 & 22/01/2019

: From Abstraction well AW-2 ~ .

: ---

: ---

: No generation of industrial wastewater

: 24 & pH Range on pH Strip :@ 7-8 on pH strip

: Barcode & Color & Appearance :Reddish brown

: Ind :1723.000 , Dom :88.000 & Ind :1149.000 , Dom :66.000

: Huntsman International (India) P. Ltd. (formerly Baroda Textile Effect Limited) - 22289

: -,VILL : UMRAYA,-

Umaraya-391440, Taluka : Padra, District : Vadodara, GIDC : Not In Gidc

Laboratory Remarks : Approved By:236-lab_236 Dt.: 22/01/2019

D. N. Vasadia, Lab Head

11/03/2019N I C

Note :

1. * - These parameters are NOT covered under the scope of NABL.

2. The results refer only to the tested samples and applicable parameters. Endorsement of products is neither inferred nor implied.

3. Samples will be destroyed after 10 days from the date of issue of test report unless otherwise specified.

4. This report is not to be reproduced wholly or in part or used in any advertising media without the permission of the Board in writing.

5. The Board is not responsible for the authenticity for the samples not collected by the Board’s officials.

6. Total liability of our laboratory is limited to the invoiced amount. Any dispute arising out of this report is subject to

Gujarat Jurisdiction only.

7. Permissible Limits: as per Schedule VI of EPA Rules, 1986 as ammended by Second and Third ammendment 1993 for Effluents

8. Physicochemical and microbiological parameters, Std.Methods for Water and Waste Water- 22nd Edition by APHA.

9. Bioassay test (for toxicity) -IS:6582:Part-2:2001; Reaffirmed 2007.

Field Observation :

Sample ID:249406 - Analysis Completion:22/01/2019

ANALYSIS REPORT FOR

WATER / WASTE WATER SAMPLE

Dyes and Dye- Intermediates / LAB Inward : 31936

Gujarat Pollution Control Board,

Vadodara

GERI Compound

Race Course Road

Vadodara - 390007

Accreditation Standards & NABL Certificate Details : Biology & Chemical / TC-5287 / Issue: 17/03/2017 / Validity: 16/03/2019

TEST REPORT

Test Report No. : 31936 Date: 22/01/2019

3. Nature of Sample

4. Sample Collected By

5. Quantity of Sample Received

6. Code No. of the Sample

7. Date & Time of Collection & Inwarding

8. Date of Start & Completion of Analysis

9. Sampling Point

10. Flow Details (Remarks)

11. Mode of Disposal

12. Ultimate Receiving Body

13. Temperature on Collection

14. Carboys Nos for

15. Water Consumption & W.W.G (KLPD)

1. Name of the Customer

2. Address

Range of TestingTest MethodSr ResultUnitParameter

Ambient oC - 60 oCIS: 3025 (Part – 9) – 1984(Reaffirmed 2006)CentigradeTemperature 1 24

1 – 14 pH value As on digital pH meter.4500 H+ B APHA Standard Methods 22nd edi.2012pH UnitspH 2 8.06

2 - to 99 Hazen & 1-500 hazen2120 B APHA Standard Methods 22nd edi. 2012Pt.Co.Sc.Colour 3 NA

10 – 200000 mg/LGravimetric method. (2540 C APHA Standard Methods 22nd edi.)2012mg/lTotal Dissolved Solids 4 11188

2 – 10000 mg/LGravimetric method. (2540 D APHA Standard Methods 22nd edi.)2012mg/lSuspended Solids 5 22

1 - 2000 mg/l.1).Titrimetric method (4500 NH3 B & C APHA Standard Methods 22nd edi.)-2012mg/lAmmonical Nitrogen 6 1.68

1 - 50000 mg/lArgentometric method. (4500 Cl? B APHA Standard Methods 22nd edi.)-2012mg/lChloride 7 2200

2-40mg/lAPHA(22nd edi)4500 SO4 Emg/lSulphate 8 4133

5.0- 50000 mg/lAPHA (22nd Edition)- 5220 B Open Reflux Method-2012mg/lChemical Oxygen Demand 9 2722

01 – 1000 mg/lLiquid – Liquid Partition Gravimetric method. (5520 B APHA Standard Methods 22nd edi.)-2012mg/lOil & Grease 10 BDL

0.1 – 50 mg/l4 Amino Antipyrene method without Chloroform Extraction (Direct Photometric method) (5530 D APHA Standard Methods 22nd edi.) -2012mg/lPhenolic Compounds 11 0.46

0.02-150mg/l(3111 B APHA Standard methods 21st edi)mg/lIron 12 1.10

05–50000 mg/l3 – Day BOD test. (IS 3025 (Part 44) 1993 Reaffirmed 1999)-2009mg/lB.O.D (3 Days 27oC) 13 72

: REP-Representative/Grab, (Insp Type : ROU-Routine Visit)

: M.U.PATEL,DEE

: 5 Lit.

: 249406

: 26/12/2018 , (1015 to 1015) & 27/12/2018

: 28/12/2018 & 22/01/2019

: From Abstraction well AW-1 ~ .

: ---

: ---

: No generation of industrial wastewater

: 24 & pH Range on pH Strip :@ 7-8 on pH strip

: Barcode & Color & Appearance :Reddish brown

: Ind :1723.000 , Dom :88.000 & Ind :1149.000 , Dom :66.000

: Huntsman International (India) P. Ltd. (formerly Baroda Textile Effect Limited) - 22289

: -,VILL : UMRAYA,-

Umaraya-391440, Taluka : Padra, District : Vadodara, GIDC : Not In Gidc

Laboratory Remarks : Approved By:236-lab_236 Dt.: 22/01/2019

D. N. Vasadia, Lab Head

11/03/2019N I C

Note :

1. * - These parameters are NOT covered under the scope of NABL.

2. The results refer only to the tested samples and applicable parameters. Endorsement of products is neither inferred nor implied.

3. Samples will be destroyed after 10 days from the date of issue of test report unless otherwise specified.

4. This report is not to be reproduced wholly or in part or used in any advertising media without the permission of the Board in writing.

5. The Board is not responsible for the authenticity for the samples not collected by the Board’s officials.

6. Total liability of our laboratory is limited to the invoiced amount. Any dispute arising out of this report is subject to

Gujarat Jurisdiction only.

7. Permissible Limits: as per Schedule VI of EPA Rules, 1986 as ammended by Second and Third ammendment 1993 for Effluents

8. Physicochemical and microbiological parameters, Std.Methods for Water and Waste Water- 22nd Edition by APHA.

9. Bioassay test (for toxicity) -IS:6582:Part-2:2001; Reaffirmed 2007.

Field Observation :

Sample ID:249416 - Analysis Completion:10/01/2019

ANALYSIS REPORT FOR

WATER / WASTE WATER SAMPLE

/ LAB Inward : 31945

Gujarat Pollution Control Board,

Vadodara

GERI Compound

Race Course Road

Vadodara - 390007

Accreditation Standards & NABL Certificate Details : Biology & Chemical / TC-5287 / Issue: 17/03/2017 / Validity: 16/03/2019

TEST REPORT

Test Report No. : 31945 Date: 14/01/2019

3. Nature of Sample

4. Sample Collected By

5. Quantity of Sample Received

6. Code No. of the Sample

7. Date & Time of Collection & Inwarding

8. Date of Start & Completion of Analysis

9. Sampling Point

10. Flow Details (Remarks)

11. Mode of Disposal

12. Ultimate Receiving Body

13. Temperature on Collection

14. Carboys Nos for

15. Water Consumption & W.W.G (KLPD)

1. Name of the Customer

2. Address

Range of TestingTest MethodSr ResultUnitParameter

Ambient oC - 60 oCIS: 3025 (Part – 9) – 1984(Reaffirmed 2006)CentigradeTemperature 1 25

1 – 14 pH value As on digital pH meter.4500 H+ B APHA Standard Methods 22nd edi.2012pH UnitspH 2 7.91

2 - to 99 Hazen & 1-500 hazen2120 B APHA Standard Methods 22nd edi. 2012Pt.Co.Sc.Colour 3 50

10 – 200000 mg/LGravimetric method. (2540 C APHA Standard Methods 22nd edi.)2012mg/lTotal Dissolved Solids 4 2828

2 – 10000 mg/LGravimetric method. (2540 D APHA Standard Methods 22nd edi.)2012mg/lSuspended Solids 5 02

1 - 2000 mg/l.1).Titrimetric method (4500 NH3 B & C APHA Standard Methods 22nd edi.)-2012mg/lAmmonical Nitrogen 6 2.24

1 - 50000 mg/lArgentometric method. (4500 Cl? B APHA Standard Methods 22nd edi.)-2012mg/lChloride 7 720

2-40mg/lAPHA(22nd edi)4500 SO4 Emg/lSulphate 8 107

5.0- 50000 mg/lAPHA (22nd Edition)- 5220 B Open Reflux Method-2012mg/lChemical Oxygen Demand 9 82

01 – 1000 mg/lLiquid – Liquid Partition Gravimetric method. (5520 B APHA Standard Methods 22nd edi.)-2012mg/lOil & Grease 10 BDL

0.1 – 50 mg/l4 Amino Antipyrene method without Chloroform Extraction (Direct Photometric method) (5530 D APHA Standard Methods 22nd edi.) -2012mg/lPhenolic Compounds 11 0.27

05–50000 mg/l3 – Day BOD test. (IS 3025 (Part 44) 1993 Reaffirmed 1999)-2009mg/lB.O.D (3 Days 27oC) 12 7

: REP-Representative/Grab, (Insp Type : COM-On Complaint)

: M.U.PATEL,DEE

: 5 Lit.

: 249416

: 26/12/2018 , (1135 to 1135) & 27/12/2018

: 28/12/2018 & 10/01/2019

: Bore well of Geetaben Ghanshyambhai Patel, Vill. Luna, Ta. Padra, Dist. Vadodara (OSW - 8) ~

: ---

: ---

: 0

: 25 & pH Range on pH Strip :@ 7-8 on pH strip

: Barcode & Color & Appearance :Dark yellow

: Ind :10.000 , Dom :1.000 & Ind :9.000 , Dom :1.000

: Complaint - 32381

: Vadodara District,-,-

Vadodara Dist--, Taluka : Vadodara, District : Vadodara, GIDC : Not In Gidc

Laboratory Remarks : Approved By:236-lab_236 Dt.: 14/01/2019

D. N. Vasadia, Lab Head

06/03/2019N I C

Note :

1. * - These parameters are NOT covered under the scope of NABL.

2. The results refer only to the tested samples and applicable parameters. Endorsement of products is neither inferred nor implied.

3. Samples will be destroyed after 10 days from the date of issue of test report unless otherwise specified.

4. This report is not to be reproduced wholly or in part or used in any advertising media without the permission of the Board in writing.

5. The Board is not responsible for the authenticity for the samples not collected by the Board’s officials.

6. Total liability of our laboratory is limited to the invoiced amount. Any dispute arising out of this report is subject to

Gujarat Jurisdiction only.

7. Permissible Limits: as per Schedule VI of EPA Rules, 1986 as ammended by Second and Third ammendment 1993 for Effluents

8. Physicochemical and microbiological parameters, Std.Methods for Water and Waste Water- 22nd Edition by APHA.

9. Bioassay test (for toxicity) -IS:6582:Part-2:2001; Reaffirmed 2007.

Field Observation :

Sample ID:249417 - Analysis Completion:10/01/2019

ANALYSIS REPORT FOR

WATER / WASTE WATER SAMPLE

/ LAB Inward : 31946

Gujarat Pollution Control Board,

Vadodara

GERI Compound

Race Course Road

Vadodara - 390007

Accreditation Standards & NABL Certificate Details : Biology & Chemical / TC-5287 / Issue: 17/03/2017 / Validity: 16/03/2019

TEST REPORT

Test Report No. : 31946 Date: 14/01/2019

3. Nature of Sample

4. Sample Collected By

5. Quantity of Sample Received

6. Code No. of the Sample

7. Date & Time of Collection & Inwarding

8. Date of Start & Completion of Analysis

9. Sampling Point

10. Flow Details (Remarks)

11. Mode of Disposal

12. Ultimate Receiving Body

13. Temperature on Collection

14. Carboys Nos for

15. Water Consumption & W.W.G (KLPD)

1. Name of the Customer

2. Address

Range of TestingTest MethodSr ResultUnitParameter

Ambient oC - 60 oCIS: 3025 (Part – 9) – 1984(Reaffirmed 2006)CentigradeTemperature 1 25

1 – 14 pH value As on digital pH meter.4500 H+ B APHA Standard Methods 22nd edi.2012pH UnitspH 2 8.02

2 - to 99 Hazen & 1-500 hazen2120 B APHA Standard Methods 22nd edi. 2012Pt.Co.Sc.Colour 3 25

10 – 200000 mg/LGravimetric method. (2540 C APHA Standard Methods 22nd edi.)2012mg/lTotal Dissolved Solids 4 2268

2 – 10000 mg/LGravimetric method. (2540 D APHA Standard Methods 22nd edi.)2012mg/lSuspended Solids 5 08

1 - 2000 mg/l.1).Titrimetric method (4500 NH3 B & C APHA Standard Methods 22nd edi.)-2012mg/lAmmonical Nitrogen 6 5.6

1 - 50000 mg/lArgentometric method. (4500 Cl? B APHA Standard Methods 22nd edi.)-2012mg/lChloride 7 450

2-40mg/lAPHA(22nd edi)4500 SO4 Emg/lSulphate 8 129

5.0- 50000 mg/lAPHA (22nd Edition)- 5220 B Open Reflux Method-2012mg/lChemical Oxygen Demand 9 55

01 – 1000 mg/lLiquid – Liquid Partition Gravimetric method. (5520 B APHA Standard Methods 22nd edi.)-2012mg/lOil & Grease 10 BDL

0.1 – 50 mg/l4 Amino Antipyrene method without Chloroform Extraction (Direct Photometric method) (5530 D APHA Standard Methods 22nd edi.) -2012mg/lPhenolic Compounds 11 0.48

05–50000 mg/l3 – Day BOD test. (IS 3025 (Part 44) 1993 Reaffirmed 1999)-2009mg/lB.O.D (3 Days 27oC) 12 <5

: REP-Representative/Grab, (Insp Type : COM-On Complaint)

: M.U.PATEL,DEE

: 5 Lit.

: 249417

: 26/12/2018 , (1145 to 1145) & 27/12/2018

: 28/12/2018 & 10/01/2019

: Bore well of Kapila Ben Ramanbhai Patel survey no-353 vill.luna, Ta. Padra, Dist.vadodara ~ OSW - 6

: ---

: ---

: 0

: 25 & pH Range on pH Strip :@ 7-8 on pH strip

: Barcode & Color & Appearance :Dark yellow

: Ind :10.000 , Dom :1.000 & Ind :9.000 , Dom :1.000

: Complaint - 32381

: Vadodara District,-,-

Vadodara Dist--, Taluka : Vadodara, District : Vadodara, GIDC : Not In Gidc

Laboratory Remarks : Approved By:236-lab_236 Dt.: 14/01/2019

D. N. Vasadia, Lab Head

06/03/2019N I C

Note :

1. * - These parameters are NOT covered under the scope of NABL.

2. The results refer only to the tested samples and applicable parameters. Endorsement of products is neither inferred nor implied.

3. Samples will be destroyed after 10 days from the date of issue of test report unless otherwise specified.

4. This report is not to be reproduced wholly or in part or used in any advertising media without the permission of the Board in writing.

5. The Board is not responsible for the authenticity for the samples not collected by the Board’s officials.

6. Total liability of our laboratory is limited to the invoiced amount. Any dispute arising out of this report is subject to

Gujarat Jurisdiction only.

7. Permissible Limits: as per Schedule VI of EPA Rules, 1986 as ammended by Second and Third ammendment 1993 for Effluents

8. Physicochemical and microbiological parameters, Std.Methods for Water and Waste Water- 22nd Edition by APHA.

9. Bioassay test (for toxicity) -IS:6582:Part-2:2001; Reaffirmed 2007.

Field Observation :

Sample ID:249418 - Analysis Completion:10/01/2019

ANALYSIS REPORT FOR

WATER / WASTE WATER SAMPLE

/ LAB Inward : 31947

Gujarat Pollution Control Board,

Vadodara

GERI Compound

Race Course Road

Vadodara - 390007

Accreditation Standards & NABL Certificate Details : Biology & Chemical / TC-5287 / Issue: 17/03/2017 / Validity: 16/03/2019

TEST REPORT

Test Report No. : 31947 Date: 14/01/2019

3. Nature of Sample

4. Sample Collected By

5. Quantity of Sample Received

6. Code No. of the Sample

7. Date & Time of Collection & Inwarding

8. Date of Start & Completion of Analysis

9. Sampling Point

10. Flow Details (Remarks)

11. Mode of Disposal

12. Ultimate Receiving Body

13. Temperature on Collection

14. Carboys Nos for

15. Water Consumption & W.W.G (KLPD)

1. Name of the Customer

2. Address

Range of TestingTest MethodSr ResultUnitParameter

Ambient oC - 60 oCIS: 3025 (Part – 9) – 1984(Reaffirmed 2006)CentigradeTemperature 1 25

1 – 14 pH value As on digital pH meter.4500 H+ B APHA Standard Methods 22nd edi.2012pH UnitspH 2 8.25

2 - to 99 Hazen & 1-500 hazen2120 B APHA Standard Methods 22nd edi. 2012Pt.Co.Sc.Colour 3 10

10 – 200000 mg/LGravimetric method. (2540 C APHA Standard Methods 22nd edi.)2012mg/lTotal Dissolved Solids 4 1458

2 – 10000 mg/LGravimetric method. (2540 D APHA Standard Methods 22nd edi.)2012mg/lSuspended Solids 5 04

1 - 2000 mg/l.1).Titrimetric method (4500 NH3 B & C APHA Standard Methods 22nd edi.)-2012mg/lAmmonical Nitrogen 6 1.12

1 - 50000 mg/lArgentometric method. (4500 Cl? B APHA Standard Methods 22nd edi.)-2012mg/lChloride 7 380

2-40mg/lAPHA(22nd edi)4500 SO4 Emg/lSulphate 8 36

5.0- 50000 mg/lAPHA (22nd Edition)- 5220 B Open Reflux Method-2012mg/lChemical Oxygen Demand 9 27

01 – 1000 mg/lLiquid – Liquid Partition Gravimetric method. (5520 B APHA Standard Methods 22nd edi.)-2012mg/lOil & Grease 10 BDL

0.1 – 50 mg/l4 Amino Antipyrene method without Chloroform Extraction (Direct Photometric method) (5530 D APHA Standard Methods 22nd edi.) -2012mg/lPhenolic Compounds 11 0.30

05–50000 mg/l3 – Day BOD test. (IS 3025 (Part 44) 1993 Reaffirmed 1999)-2009mg/lB.O.D (3 Days 27oC) 12 <5

: REP-Representative/Grab, (Insp Type : COM-On Complaint)

: M.U.PATEL,DEE

: 5 Lit.

: 249418

: 26/12/2018 , (1200 to 1200) & 27/12/2018

: 28/12/2018 & 10/01/2019

: Bore well at farm of Ghanshyambhai Ramanbhai Patel Survey no-333 Vill.Luna, Ta. Padra, Dist.Vadodar

: ---

: ---

: 0

: 25 & pH Range on pH Strip :@ 7-8 on pH strip

: Barcode & Color & Appearance :Yellowish

: Ind :10.000 , Dom :1.000 & Ind :9.000 , Dom :1.000

: Complaint - 32381

: Vadodara District,-,-

Vadodara Dist--, Taluka : Vadodara, District : Vadodara, GIDC : Not In Gidc

Laboratory Remarks : Approved By:236-lab_236 Dt.: 14/01/2019

D. N. Vasadia, Lab Head

06/03/2019N I C

Note :

1. * - These parameters are NOT covered under the scope of NABL.

2. The results refer only to the tested samples and applicable parameters. Endorsement of products is neither inferred nor implied.

3. Samples will be destroyed after 10 days from the date of issue of test report unless otherwise specified.

4. This report is not to be reproduced wholly or in part or used in any advertising media without the permission of the Board in writing.

5. The Board is not responsible for the authenticity for the samples not collected by the Board’s officials.

6. Total liability of our laboratory is limited to the invoiced amount. Any dispute arising out of this report is subject to

Gujarat Jurisdiction only.

7. Permissible Limits: as per Schedule VI of EPA Rules, 1986 as ammended by Second and Third ammendment 1993 for Effluents

8. Physicochemical and microbiological parameters, Std.Methods for Water and Waste Water- 22nd Edition by APHA.

9. Bioassay test (for toxicity) -IS:6582:Part-2:2001; Reaffirmed 2007.

Field Observation :

Sample ID:249419 - Analysis Completion:10/01/2019

ANALYSIS REPORT FOR

WATER / WASTE WATER SAMPLE

/ LAB Inward : 31948

Gujarat Pollution Control Board,

Vadodara

GERI Compound

Race Course Road

Vadodara - 390007

Accreditation Standards & NABL Certificate Details : Biology & Chemical / TC-5287 / Issue: 17/03/2017 / Validity: 16/03/2019

TEST REPORT

Test Report No. : 31948 Date: 14/01/2019

3. Nature of Sample

4. Sample Collected By

5. Quantity of Sample Received

6. Code No. of the Sample

7. Date & Time of Collection & Inwarding

8. Date of Start & Completion of Analysis

9. Sampling Point

10. Flow Details (Remarks)

11. Mode of Disposal

12. Ultimate Receiving Body

13. Temperature on Collection

14. Carboys Nos for

15. Water Consumption & W.W.G (KLPD)

1. Name of the Customer

2. Address

Range of TestingTest MethodSr ResultUnitParameter

Ambient oC - 60 oCIS: 3025 (Part – 9) – 1984(Reaffirmed 2006)CentigradeTemperature 1 25

1 – 14 pH value As on digital pH meter.4500 H+ B APHA Standard Methods 22nd edi.2012pH UnitspH 2 7.75

2 - to 99 Hazen & 1-500 hazen2120 B APHA Standard Methods 22nd edi. 2012Pt.Co.Sc.Colour 3 15

10 – 200000 mg/LGravimetric method. (2540 C APHA Standard Methods 22nd edi.)2012mg/lTotal Dissolved Solids 4 2674

2 – 10000 mg/LGravimetric method. (2540 D APHA Standard Methods 22nd edi.)2012mg/lSuspended Solids 5 02

1 - 2000 mg/l.1).Titrimetric method (4500 NH3 B & C APHA Standard Methods 22nd edi.)-2012mg/lAmmonical Nitrogen 6 4.48

1 - 50000 mg/lArgentometric method. (4500 Cl? B APHA Standard Methods 22nd edi.)-2012mg/lChloride 7 740

2-40mg/lAPHA(22nd edi)4500 SO4 Emg/lSulphate 8 65

5.0- 50000 mg/lAPHA (22nd Edition)- 5220 B Open Reflux Method-2012mg/lChemical Oxygen Demand 9 24

01 – 1000 mg/lLiquid – Liquid Partition Gravimetric method. (5520 B APHA Standard Methods 22nd edi.)-2012mg/lOil & Grease 10 BDL

0.1 – 50 mg/l4 Amino Antipyrene method without Chloroform Extraction (Direct Photometric method) (5530 D APHA Standard Methods 22nd edi.) -2012mg/lPhenolic Compounds 11 0.29

05–50000 mg/l3 – Day BOD test. (IS 3025 (Part 44) 1993 Reaffirmed 1999)-2009mg/lB.O.D (3 Days 27oC) 12 <5

: REP-Representative/Grab, (Insp Type : COM-On Complaint)

: M.U.PATEL,DEE

: 5 Lit.

: 249419

: 26/12/2018 , (1220 to 1220) & 27/12/2018

: 28/12/2018 & 10/01/2019

: Bore well of Gansyambhai Chandubhai Patel farm survey no-426 vill.luna, Ta.padra, Dist.vadodara ~ .

: ---

: ---

: 0

: 25 & pH Range on pH Strip :@ 7-8 on pH strip

: Barcode & Color & Appearance :Yellowish

: Ind :10.000 , Dom :1.000 & Ind :9.000 , Dom :1.000

: Complaint - 32381

: Vadodara District,-,-

Vadodara Dist--, Taluka : Vadodara, District : Vadodara, GIDC : Not In Gidc

Laboratory Remarks : Approved By:236-lab_236 Dt.: 14/01/2019

D. N. Vasadia, Lab Head

06/03/2019N I C

Note :

1. * - These parameters are NOT covered under the scope of NABL.

2. The results refer only to the tested samples and applicable parameters. Endorsement of products is neither inferred nor implied.

3. Samples will be destroyed after 10 days from the date of issue of test report unless otherwise specified.

4. This report is not to be reproduced wholly or in part or used in any advertising media without the permission of the Board in writing.

5. The Board is not responsible for the authenticity for the samples not collected by the Board’s officials.

6. Total liability of our laboratory is limited to the invoiced amount. Any dispute arising out of this report is subject to

Gujarat Jurisdiction only.

7. Permissible Limits: as per Schedule VI of EPA Rules, 1986 as ammended by Second and Third ammendment 1993 for Effluents

8. Physicochemical and microbiological parameters, Std.Methods for Water and Waste Water- 22nd Edition by APHA.

9. Bioassay test (for toxicity) -IS:6582:Part-2:2001; Reaffirmed 2007.

Field Observation :

Sample ID:249420 - Analysis Completion:10/01/2019

ANALYSIS REPORT FOR

WATER / WASTE WATER SAMPLE

/ LAB Inward : 31949

Gujarat Pollution Control Board,

Vadodara

GERI Compound

Race Course Road

Vadodara - 390007

Accreditation Standards & NABL Certificate Details : Biology & Chemical / TC-5287 / Issue: 17/03/2017 / Validity: 16/03/2019

TEST REPORT

Test Report No. : 31949 Date: 15/01/2019

3. Nature of Sample

4. Sample Collected By

5. Quantity of Sample Received

6. Code No. of the Sample

7. Date & Time of Collection & Inwarding

8. Date of Start & Completion of Analysis

9. Sampling Point

10. Flow Details (Remarks)

11. Mode of Disposal

12. Ultimate Receiving Body

13. Temperature on Collection

14. Carboys Nos for

15. Water Consumption & W.W.G (KLPD)

1. Name of the Customer

2. Address

Range of TestingTest MethodSr ResultUnitParameter

Ambient oC - 60 oCIS: 3025 (Part – 9) – 1984(Reaffirmed 2006)CentigradeTemperature 1 25

1 – 14 pH value As on digital pH meter.4500 H+ B APHA Standard Methods 22nd edi.2012pH UnitspH 2 7.92

2 - to 99 Hazen & 1-500 hazen2120 B APHA Standard Methods 22nd edi. 2012Pt.Co.Sc.Colour 3 5

10 – 200000 mg/LGravimetric method. (2540 C APHA Standard Methods 22nd edi.)2012mg/lTotal Dissolved Solids 4 2114

2 – 10000 mg/LGravimetric method. (2540 D APHA Standard Methods 22nd edi.)2012mg/lSuspended Solids 5 02

1 - 2000 mg/l.1).Titrimetric method (4500 NH3 B & C APHA Standard Methods 22nd edi.)-2012mg/lAmmonical Nitrogen 6 0.28

1 - 50000 mg/lArgentometric method. (4500 Cl? B APHA Standard Methods 22nd edi.)-2012mg/lChloride 7 610

2-40mg/lAPHA(22nd edi)4500 SO4 Emg/lSulphate 8 115

5.0- 50000 mg/lAPHA (22nd Edition)- 5220 B Open Reflux Method-2012mg/lChemical Oxygen Demand 9 4.6

01 – 1000 mg/lLiquid – Liquid Partition Gravimetric method. (5520 B APHA Standard Methods 22nd edi.)-2012mg/lOil & Grease 10 BDL

0.1 – 50 mg/l4 Amino Antipyrene method without Chloroform Extraction (Direct Photometric method) (5530 D APHA Standard Methods 22nd edi.) -2012mg/lPhenolic Compounds 11 bdl

05–50000 mg/l3 – Day BOD test. (IS 3025 (Part 44) 1993 Reaffirmed 1999)-2009mg/lB.O.D (3 Days 27oC) 12 <5

: REP-Representative/Grab, (Insp Type : COM-On Complaint)

: M.U.PATEL,DEE

: 5 Lit.

: 249420

: 26/12/2018 , (1235 to 1235) & 27/12/2018

: 28/12/2018 & 10/01/2019

: Bore well at farm of Rameshbhai Somabhai Padhiyar Sr.No-709 vill.umraya,ta. padra,Dist.vadoara ~ OS

: ---

: ---

: 0

: 25 & pH Range on pH Strip :@ 7-8 on pH strip

: Barcode & Color & Appearance :Pale yellow

: Ind :10.000 , Dom :1.000 & Ind :9.000 , Dom :1.000

: Complaint - 32381

: Vadodara District,-,-

Vadodara Dist--, Taluka : Vadodara, District : Vadodara, GIDC : Not In Gidc

Laboratory Remarks : Approved By:236-lab_236 Dt.: 15/01/2019

D. N. Vasadia, Lab Head

06/03/2019N I C

Note :

1. * - These parameters are NOT covered under the scope of NABL.

2. The results refer only to the tested samples and applicable parameters. Endorsement of products is neither inferred nor implied.

3. Samples will be destroyed after 10 days from the date of issue of test report unless otherwise specified.

4. This report is not to be reproduced wholly or in part or used in any advertising media without the permission of the Board in writing.

5. The Board is not responsible for the authenticity for the samples not collected by the Board’s officials.

6. Total liability of our laboratory is limited to the invoiced amount. Any dispute arising out of this report is subject to

Gujarat Jurisdiction only.

7. Permissible Limits: as per Schedule VI of EPA Rules, 1986 as ammended by Second and Third ammendment 1993 for Effluents

8. Physicochemical and microbiological parameters, Std.Methods for Water and Waste Water- 22nd Edition by APHA.

9. Bioassay test (for toxicity) -IS:6582:Part-2:2001; Reaffirmed 2007.

Field Observation :

Sample ID:249421 - Analysis Completion:10/01/2019

ANALYSIS REPORT FOR

WATER / WASTE WATER SAMPLE

/ LAB Inward : 31950

Gujarat Pollution Control Board,

Vadodara

GERI Compound

Race Course Road

Vadodara - 390007

Accreditation Standards & NABL Certificate Details : Biology & Chemical / TC-5287 / Issue: 17/03/2017 / Validity: 16/03/2019

TEST REPORT

Test Report No. : 31950 Date: 15/01/2019

3. Nature of Sample

4. Sample Collected By

5. Quantity of Sample Received

6. Code No. of the Sample

7. Date & Time of Collection & Inwarding

8. Date of Start & Completion of Analysis

9. Sampling Point

10. Flow Details (Remarks)

11. Mode of Disposal

12. Ultimate Receiving Body

13. Temperature on Collection

14. Carboys Nos for

15. Water Consumption & W.W.G (KLPD)

1. Name of the Customer

2. Address

Range of TestingTest MethodSr ResultUnitParameter

Ambient oC - 60 oCIS: 3025 (Part – 9) – 1984(Reaffirmed 2006)CentigradeTemperature 1 25

1 – 14 pH value As on digital pH meter.4500 H+ B APHA Standard Methods 22nd edi.2012pH UnitspH 2 7.89

2 - to 99 Hazen & 1-500 hazen2120 B APHA Standard Methods 22nd edi. 2012Pt.Co.Sc.Colour 3 75

10 – 200000 mg/LGravimetric method. (2540 C APHA Standard Methods 22nd edi.)2012mg/lTotal Dissolved Solids 4 3064

2 – 10000 mg/LGravimetric method. (2540 D APHA Standard Methods 22nd edi.)2012mg/lSuspended Solids 5 02

1 - 2000 mg/l.1).Titrimetric method (4500 NH3 B & C APHA Standard Methods 22nd edi.)-2012mg/lAmmonical Nitrogen 6 1.68

1 - 50000 mg/lArgentometric method. (4500 Cl? B APHA Standard Methods 22nd edi.)-2012mg/lChloride 7 640

2-40mg/lAPHA(22nd edi)4500 SO4 Emg/lSulphate 8 307

5.0- 50000 mg/lAPHA (22nd Edition)- 5220 B Open Reflux Method-2012mg/lChemical Oxygen Demand 9 142

01 – 1000 mg/lLiquid – Liquid Partition Gravimetric method. (5520 B APHA Standard Methods 22nd edi.)-2012mg/lOil & Grease 10 BDL

0.1 – 50 mg/l4 Amino Antipyrene method without Chloroform Extraction (Direct Photometric method) (5530 D APHA Standard Methods 22nd edi.) -2012mg/lPhenolic Compounds 11 0.24

05–50000 mg/l3 – Day BOD test. (IS 3025 (Part 44) 1993 Reaffirmed 1999)-2009mg/lB.O.D (3 Days 27oC) 12 12

: REP-Representative/Grab, (Insp Type : COM-On Complaint)

: M.U.PATEL,DEE

: 5 Lit.

: 249421

: 26/12/2018 , (1250 to 1250) & 27/12/2018

: 28/12/2018 & 10/01/2019

: Bore well at premises of M/s Prasad Int. Ltd., Sr. no. 378/a & 313/p, Vill. Luna, Padra, Vadodara ~

: ---

: ---

: 0

: 25 & pH Range on pH Strip :@ 7-8 on pH strip

: Barcode & Color & Appearance :Reddish tinge

: Ind :10.000 , Dom :1.000 & Ind :9.000 , Dom :1.000

: Complaint - 32381

: Vadodara District,-,-

Vadodara Dist--, Taluka : Vadodara, District : Vadodara, GIDC : Not In Gidc

Laboratory Remarks : Approved By:236-lab_236 Dt.: 15/01/2019

D. N. Vasadia, Lab Head

06/03/2019N I C

Note :

1. * - These parameters are NOT covered under the scope of NABL.

2. The results refer only to the tested samples and applicable parameters. Endorsement of products is neither inferred nor implied.

3. Samples will be destroyed after 10 days from the date of issue of test report unless otherwise specified.

4. This report is not to be reproduced wholly or in part or used in any advertising media without the permission of the Board in writing.

5. The Board is not responsible for the authenticity for the samples not collected by the Board’s officials.

6. Total liability of our laboratory is limited to the invoiced amount. Any dispute arising out of this report is subject to

Gujarat Jurisdiction only.

7. Permissible Limits: as per Schedule VI of EPA Rules, 1986 as ammended by Second and Third ammendment 1993 for Effluents

8. Physicochemical and microbiological parameters, Std.Methods for Water and Waste Water- 22nd Edition by APHA.

9. Bioassay test (for toxicity) -IS:6582:Part-2:2001; Reaffirmed 2007.

Field Observation :

Sample ID:249422 - Analysis Completion:11/01/2019

ANALYSIS REPORT FOR

WATER / WASTE WATER SAMPLE

/ LAB Inward : 31951

Gujarat Pollution Control Board,

Vadodara

GERI Compound

Race Course Road

Vadodara - 390007

Accreditation Standards & NABL Certificate Details : Biology & Chemical / TC-5287 / Issue: 17/03/2017 / Validity: 16/03/2019

TEST REPORT

Test Report No. : 31951 Date: 14/01/2019

3. Nature of Sample

4. Sample Collected By

5. Quantity of Sample Received

6. Code No. of the Sample

7. Date & Time of Collection & Inwarding

8. Date of Start & Completion of Analysis

9. Sampling Point

10. Flow Details (Remarks)

11. Mode of Disposal

12. Ultimate Receiving Body

13. Temperature on Collection

14. Carboys Nos for

15. Water Consumption & W.W.G (KLPD)

1. Name of the Customer

2. Address

Range of TestingTest MethodSr ResultUnitParameter

Ambient oC - 60 oCIS: 3025 (Part – 9) – 1984(Reaffirmed 2006)CentigradeTemperature 1 25

1 – 14 pH value As on digital pH meter.4500 H+ B APHA Standard Methods 22nd edi.2012pH UnitspH 2 7.95

2 - to 99 Hazen & 1-500 hazen2120 B APHA Standard Methods 22nd edi. 2012Pt.Co.Sc.Colour 3 7.5

10 – 200000 mg/LGravimetric method. (2540 C APHA Standard Methods 22nd edi.)2012mg/lTotal Dissolved Solids 4 1342

2 – 10000 mg/LGravimetric method. (2540 D APHA Standard Methods 22nd edi.)2012mg/lSuspended Solids 5 04

1 - 2000 mg/l.1).Titrimetric method (4500 NH3 B & C APHA Standard Methods 22nd edi.)-2012mg/lAmmonical Nitrogen 6 0.28

1 - 50000 mg/lArgentometric method. (4500 Cl? B APHA Standard Methods 22nd edi.)-2012mg/lChloride 7 410

2-40mg/lAPHA(22nd edi)4500 SO4 Emg/lSulphate 8 20

5.0- 50000 mg/lAPHA (22nd Edition)- 5220 B Open Reflux Method-2012mg/lChemical Oxygen Demand 9 4.6

01 – 1000 mg/lLiquid – Liquid Partition Gravimetric method. (5520 B APHA Standard Methods 22nd edi.)-2012mg/lOil & Grease 10 BDL

0.1 – 50 mg/l4 Amino Antipyrene method without Chloroform Extraction (Direct Photometric method) (5530 D APHA Standard Methods 22nd edi.) -2012mg/lPhenolic Compounds 11 0.34

05–50000 mg/l3 – Day BOD test. (IS 3025 (Part 44) 1993 Reaffirmed 1999)-2009mg/lB.O.D (3 Days 27oC) 12 <5

: REP-Representative/Grab, (Insp Type : COM-On Complaint)

: M.U.PATEL,DEE

: 5 Lit.

: 249422

: 26/12/2018 , (1300 to 1300) & 27/12/2018

: 28/12/2018 & 11/01/2019

: Bore well of Bhailalbhai Dhahya bhai Padhiyar(Opposite Prasad International Ltd) Vill.Luna,Ta.Padr

: ---

: ---

: 0

: 25 & pH Range on pH Strip :@ 7-8 on pH strip

: Barcode & Color & Appearance :Colorless

: Ind :10.000 , Dom :1.000 & Ind :9.000 , Dom :1.000

: Complaint - 32381

: Vadodara District,-,-

Vadodara Dist--, Taluka : Vadodara, District : Vadodara, GIDC : Not In Gidc

Laboratory Remarks : Approved By:236-lab_236 Dt.: 14/01/2019

D. N. Vasadia, Lab Head

06/03/2019N I C

Note :

1. * - These parameters are NOT covered under the scope of NABL.

2. The results refer only to the tested samples and applicable parameters. Endorsement of products is neither inferred nor implied.

3. Samples will be destroyed after 10 days from the date of issue of test report unless otherwise specified.

4. This report is not to be reproduced wholly or in part or used in any advertising media without the permission of the Board in writing.

5. The Board is not responsible for the authenticity for the samples not collected by the Board’s officials.

6. Total liability of our laboratory is limited to the invoiced amount. Any dispute arising out of this report is subject to

Gujarat Jurisdiction only.

7. Permissible Limits: as per Schedule VI of EPA Rules, 1986 as ammended by Second and Third ammendment 1993 for Effluents

8. Physicochemical and microbiological parameters, Std.Methods for Water and Waste Water- 22nd Edition by APHA.

9. Bioassay test (for toxicity) -IS:6582:Part-2:2001; Reaffirmed 2007.

Field Observation :

Sample ID:249424 - Analysis Completion:10/01/2019

ANALYSIS REPORT FOR

WATER / WASTE WATER SAMPLE

/ LAB Inward : 31953

Gujarat Pollution Control Board,

Vadodara

GERI Compound

Race Course Road

Vadodara - 390007

Accreditation Standards & NABL Certificate Details : Biology & Chemical / TC-5287 / Issue: 17/03/2017 / Validity: 16/03/2019

TEST REPORT

Test Report No. : 31953 Date: 15/01/2019

3. Nature of Sample

4. Sample Collected By

5. Quantity of Sample Received

6. Code No. of the Sample

7. Date & Time of Collection & Inwarding

8. Date of Start & Completion of Analysis

9. Sampling Point

10. Flow Details (Remarks)

11. Mode of Disposal

12. Ultimate Receiving Body

13. Temperature on Collection

14. Carboys Nos for

15. Water Consumption & W.W.G (KLPD)

1. Name of the Customer

2. Address

Range of TestingTest MethodSr ResultUnitParameter

Ambient oC - 60 oCIS: 3025 (Part – 9) – 1984(Reaffirmed 2006)CentigradeTemperature 1 26

1 – 14 pH value As on digital pH meter.4500 H+ B APHA Standard Methods 22nd edi.2012pH UnitspH 2 7.80

2 - to 99 Hazen & 1-500 hazen2120 B APHA Standard Methods 22nd edi. 2012Pt.Co.Sc.Colour 3 5

10 – 200000 mg/LGravimetric method. (2540 C APHA Standard Methods 22nd edi.)2012mg/lTotal Dissolved Solids 4 4370

2 – 10000 mg/LGravimetric method. (2540 D APHA Standard Methods 22nd edi.)2012mg/lSuspended Solids 5 12

1 - 2000 mg/l.1).Titrimetric method (4500 NH3 B & C APHA Standard Methods 22nd edi.)-2012mg/lAmmonical Nitrogen 6 0.28

1 - 50000 mg/lArgentometric method. (4500 Cl? B APHA Standard Methods 22nd edi.)-2012mg/lChloride 7 1380

2-40mg/lAPHA(22nd edi)4500 SO4 Emg/lSulphate 8 165

5.0- 50000 mg/lAPHA (22nd Edition)- 5220 B Open Reflux Method-2012mg/lChemical Oxygen Demand 9 6.1

01 – 1000 mg/lLiquid – Liquid Partition Gravimetric method. (5520 B APHA Standard Methods 22nd edi.)-2012mg/lOil & Grease 10 BDL

0.1 – 50 mg/l4 Amino Antipyrene method without Chloroform Extraction (Direct Photometric method) (5530 D APHA Standard Methods 22nd edi.) -2012mg/lPhenolic Compounds 11 bdl

05–50000 mg/l3 – Day BOD test. (IS 3025 (Part 44) 1993 Reaffirmed 1999)-2009mg/lB.O.D (3 Days 27oC) 12 <5

: REP-Representative/Grab, (Insp Type : COM-On Complaint)

: M.U.PATEL,DEE

: 5 Lit.

: 249424

: 26/12/2018 , (1355 to 1355) & 27/12/2018

: 28/12/2018 & 10/01/2019

: Bore well within premises of M/s Chemstar Organics, Vill. Umaraya, Ta. Padra, Dist. Vadodara ~

: ---

: ---

: 0

: 26 & pH Range on pH Strip :@ 7-8 on pH strip

: Barcode & Color & Appearance :Colorless and slight turbid

: Ind :10.000 , Dom :1.000 & Ind :9.000 , Dom :1.000

: Complaint - 32381

: Vadodara District,-,-

Vadodara Dist--, Taluka : Vadodara, District : Vadodara, GIDC : Not In Gidc

Laboratory Remarks : Approved By:236-lab_236 Dt.: 15/01/2019

D. N. Vasadia, Lab Head

11/03/2019N I C

Note :

1. * - These parameters are NOT covered under the scope of NABL.

2. The results refer only to the tested samples and applicable parameters. Endorsement of products is neither inferred nor implied.

3. Samples will be destroyed after 10 days from the date of issue of test report unless otherwise specified.

4. This report is not to be reproduced wholly or in part or used in any advertising media without the permission of the Board in writing.

5. The Board is not responsible for the authenticity for the samples not collected by the Board’s officials.

6. Total liability of our laboratory is limited to the invoiced amount. Any dispute arising out of this report is subject to

Gujarat Jurisdiction only.

7. Permissible Limits: as per Schedule VI of EPA Rules, 1986 as ammended by Second and Third ammendment 1993 for Effluents

8. Physicochemical and microbiological parameters, Std.Methods for Water and Waste Water- 22nd Edition by APHA.

9. Bioassay test (for toxicity) -IS:6582:Part-2:2001; Reaffirmed 2007.

Field Observation :

Sample ID:249425 - Analysis Completion:10/01/2019

ANALYSIS REPORT FOR

WATER / WASTE WATER SAMPLE

/ LAB Inward : 31954

Gujarat Pollution Control Board,

Vadodara

GERI Compound

Race Course Road

Vadodara - 390007

Accreditation Standards & NABL Certificate Details : Biology & Chemical / TC-5287 / Issue: 17/03/2017 / Validity: 16/03/2019

TEST REPORT

Test Report No. : 31954 Date: 15/01/2019

3. Nature of Sample

4. Sample Collected By

5. Quantity of Sample Received

6. Code No. of the Sample

7. Date & Time of Collection & Inwarding

8. Date of Start & Completion of Analysis

9. Sampling Point

10. Flow Details (Remarks)

11. Mode of Disposal

12. Ultimate Receiving Body

13. Temperature on Collection

14. Carboys Nos for

15. Water Consumption & W.W.G (KLPD)

1. Name of the Customer

2. Address

Range of TestingTest MethodSr ResultUnitParameter

Ambient oC - 60 oCIS: 3025 (Part – 9) – 1984(Reaffirmed 2006)CentigradeTemperature 1 26

1 – 14 pH value As on digital pH meter.4500 H+ B APHA Standard Methods 22nd edi.2012pH UnitspH 2 8.36

2 - to 99 Hazen & 1-500 hazen2120 B APHA Standard Methods 22nd edi. 2012Pt.Co.Sc.Colour 3 5

10 – 200000 mg/LGravimetric method. (2540 C APHA Standard Methods 22nd edi.)2012mg/lTotal Dissolved Solids 4 558

2 – 10000 mg/LGravimetric method. (2540 D APHA Standard Methods 22nd edi.)2012mg/lSuspended Solids 5 32

1 - 2000 mg/l.1).Titrimetric method (4500 NH3 B & C APHA Standard Methods 22nd edi.)-2012mg/lAmmonical Nitrogen 6 0.28

1 - 50000 mg/lArgentometric method. (4500 Cl? B APHA Standard Methods 22nd edi.)-2012mg/lChloride 7 180

2-40mg/lAPHA(22nd edi)4500 SO4 Emg/lSulphate 8 26

5.0- 50000 mg/lAPHA (22nd Edition)- 5220 B Open Reflux Method-2012mg/lChemical Oxygen Demand 9 4.6

01 – 1000 mg/lLiquid – Liquid Partition Gravimetric method. (5520 B APHA Standard Methods 22nd edi.)-2012mg/lOil & Grease 10 BDL

0.1 – 50 mg/l4 Amino Antipyrene method without Chloroform Extraction (Direct Photometric method) (5530 D APHA Standard Methods 22nd edi.) -2012mg/lPhenolic Compounds 11 bdl

05–50000 mg/l3 – Day BOD test. (IS 3025 (Part 44) 1993 Reaffirmed 1999)-2009mg/lB.O.D (3 Days 27oC) 12 <5

: REP-Representative/Grab, (Insp Type : COM-On Complaint)

: M.U.PATEL,DEE

: 5 Lit.

: 249425

: 26/12/2018 , (1420 to 1420) & 27/12/2018

: 28/12/2018 & 10/01/2019

: Bore well of Umaraya Gram Panchayat (Lupin Foundation), Vill. Umaraya, Ta. Padra, Dist. Vadodara ~

: ---

: ---

: 0

: 26 & pH Range on pH Strip :@ 7-8 on pH strip

: Barcode & Color & Appearance :Colourless and slight turbid

: Ind :10.000 , Dom :1.000 & Ind :9.000 , Dom :1.000

: Complaint - 32381

: Vadodara District,-,-

Vadodara Dist--, Taluka : Vadodara, District : Vadodara, GIDC : Not In Gidc

Laboratory Remarks : Approved By:236-lab_236 Dt.: 15/01/2019

D. N. Vasadia, Lab Head

11/03/2019N I C

Note :

1. * - These parameters are NOT covered under the scope of NABL.

2. The results refer only to the tested samples and applicable parameters. Endorsement of products is neither inferred nor implied.

3. Samples will be destroyed after 10 days from the date of issue of test report unless otherwise specified.

4. This report is not to be reproduced wholly or in part or used in any advertising media without the permission of the Board in writing.

5. The Board is not responsible for the authenticity for the samples not collected by the Board’s officials.

6. Total liability of our laboratory is limited to the invoiced amount. Any dispute arising out of this report is subject to

Gujarat Jurisdiction only.

7. Permissible Limits: as per Schedule VI of EPA Rules, 1986 as ammended by Second and Third ammendment 1993 for Effluents

8. Physicochemical and microbiological parameters, Std.Methods for Water and Waste Water- 22nd Edition by APHA.

9. Bioassay test (for toxicity) -IS:6582:Part-2:2001; Reaffirmed 2007.

Field Observation :

Sample ID:249426 - Analysis Completion:10/01/2019

ANALYSIS REPORT FOR

WATER / WASTE WATER SAMPLE

/ LAB Inward : 31955

Gujarat Pollution Control Board,

Vadodara

GERI Compound

Race Course Road

Vadodara - 390007

Accreditation Standards & NABL Certificate Details : Biology & Chemical / TC-5287 / Issue: 17/03/2017 / Validity: 16/03/2019

TEST REPORT

Test Report No. : 31955 Date: 14/01/2019

3. Nature of Sample

4. Sample Collected By

5. Quantity of Sample Received

6. Code No. of the Sample

7. Date & Time of Collection & Inwarding

8. Date of Start & Completion of Analysis

9. Sampling Point

10. Flow Details (Remarks)

11. Mode of Disposal

12. Ultimate Receiving Body

13. Temperature on Collection

14. Carboys Nos for

15. Water Consumption & W.W.G (KLPD)

1. Name of the Customer

2. Address

Range of TestingTest MethodSr ResultUnitParameter

Ambient oC - 60 oCIS: 3025 (Part – 9) – 1984(Reaffirmed 2006)CentigradeTemperature 1 26

1 – 14 pH value As on digital pH meter.4500 H+ B APHA Standard Methods 22nd edi.2012pH UnitspH 2 8.01

2 - to 99 Hazen & 1-500 hazen2120 B APHA Standard Methods 22nd edi. 2012Pt.Co.Sc.Colour 3 5

10 – 200000 mg/LGravimetric method. (2540 C APHA Standard Methods 22nd edi.)2012mg/lTotal Dissolved Solids 4 2264

2 – 10000 mg/LGravimetric method. (2540 D APHA Standard Methods 22nd edi.)2012mg/lSuspended Solids 5 34

1 - 2000 mg/l.1).Titrimetric method (4500 NH3 B & C APHA Standard Methods 22nd edi.)-2012mg/lAmmonical Nitrogen 6 0.28

1 - 50000 mg/lArgentometric method. (4500 Cl? B APHA Standard Methods 22nd edi.)-2012mg/lChloride 7 710

2-40mg/lAPHA(22nd edi)4500 SO4 Emg/lSulphate 8 84

5.0- 50000 mg/lAPHA (22nd Edition)- 5220 B Open Reflux Method-2012mg/lChemical Oxygen Demand 9 4.6

01 – 1000 mg/lLiquid – Liquid Partition Gravimetric method. (5520 B APHA Standard Methods 22nd edi.)-2012mg/lOil & Grease 10 BDL

0.1 – 50 mg/l4 Amino Antipyrene method without Chloroform Extraction (Direct Photometric method) (5530 D APHA Standard Methods 22nd edi.) -2012mg/lPhenolic Compounds 11 bdl

05–50000 mg/l3 – Day BOD test. (IS 3025 (Part 44) 1993 Reaffirmed 1999)-2009mg/lB.O.D (3 Days 27oC) 12 <5

: REP-Representative/Grab, (Insp Type : COM-On Complaint)

: M.U.PATEL,DEE

: 5 Lit.

: 249426

: 26/12/2018 , (1535 to 1535) & 27/12/2018

: 28/12/2018 & 10/01/2019

: Bore well within premises of Amoli Organics Pvt. Ltd, Vill. Luna, Ta. Padra, Dist. Vadodara. ~

: ---

: ---

: 0

: 26 & pH Range on pH Strip :@ 7-8 on pH strip

: Barcode & Color & Appearance :Colorless

: Ind :10.000 , Dom :1.000 & Ind :9.000 , Dom :1.000

: Complaint - 32381

: Vadodara District,-,-

Vadodara Dist--, Taluka : Vadodara, District : Vadodara, GIDC : Not In Gidc

Laboratory Remarks : Approved By:236-lab_236 Dt.: 14/01/2019

D. N. Vasadia, Lab Head

11/03/2019N I C

Note :

1. * - These parameters are NOT covered under the scope of NABL.

2. The results refer only to the tested samples and applicable parameters. Endorsement of products is neither inferred nor implied.

3. Samples will be destroyed after 10 days from the date of issue of test report unless otherwise specified.

4. This report is not to be reproduced wholly or in part or used in any advertising media without the permission of the Board in writing.

5. The Board is not responsible for the authenticity for the samples not collected by the Board’s officials.

6. Total liability of our laboratory is limited to the invoiced amount. Any dispute arising out of this report is subject to

Gujarat Jurisdiction only.

7. Permissible Limits: as per Schedule VI of EPA Rules, 1986 as ammended by Second and Third ammendment 1993 for Effluents

8. Physicochemical and microbiological parameters, Std.Methods for Water and Waste Water- 22nd Edition by APHA.

9. Bioassay test (for toxicity) -IS:6582:Part-2:2001; Reaffirmed 2007.

Field Observation :

Sample ID:249428 - Analysis Completion:10/01/2019

ANALYSIS REPORT FOR

WATER / WASTE WATER SAMPLE

/ LAB Inward : 31956

Gujarat Pollution Control Board,

Vadodara

GERI Compound

Race Course Road

Vadodara - 390007

Accreditation Standards & NABL Certificate Details : Biology & Chemical / TC-5287 / Issue: 17/03/2017 / Validity: 16/03/2019

TEST REPORT

Test Report No. : 31956 Date: 15/01/2019

3. Nature of Sample

4. Sample Collected By

5. Quantity of Sample Received

6. Code No. of the Sample

7. Date & Time of Collection & Inwarding

8. Date of Start & Completion of Analysis

9. Sampling Point

10. Flow Details (Remarks)

11. Mode of Disposal

12. Ultimate Receiving Body

13. Temperature on Collection

14. Carboys Nos for

15. Water Consumption & W.W.G (KLPD)

1. Name of the Customer

2. Address

Range of TestingTest MethodSr ResultUnitParameter

Ambient oC - 60 oCIS: 3025 (Part – 9) – 1984(Reaffirmed 2006)CentigradeTemperature 1 26

1 – 14 pH value As on digital pH meter.4500 H+ B APHA Standard Methods 22nd edi.2012pH UnitspH 2 8.05

2 - to 99 Hazen & 1-500 hazen2120 B APHA Standard Methods 22nd edi. 2012Pt.Co.Sc.Colour 3 5

10 – 200000 mg/LGravimetric method. (2540 C APHA Standard Methods 22nd edi.)2012mg/lTotal Dissolved Solids 4 932

2 – 10000 mg/LGravimetric method. (2540 D APHA Standard Methods 22nd edi.)2012mg/lSuspended Solids 5 02

1 - 2000 mg/l.1).Titrimetric method (4500 NH3 B & C APHA Standard Methods 22nd edi.)-2012mg/lAmmonical Nitrogen 6 0.28

1 - 50000 mg/lArgentometric method. (4500 Cl? B APHA Standard Methods 22nd edi.)-2012mg/lChloride 7 210

2-40mg/lAPHA(22nd edi)4500 SO4 Emg/lSulphate 8 31

5.0- 50000 mg/lAPHA (22nd Edition)- 5220 B Open Reflux Method-2012mg/lChemical Oxygen Demand 9 4.6

01 – 1000 mg/lLiquid – Liquid Partition Gravimetric method. (5520 B APHA Standard Methods 22nd edi.)-2012mg/lOil & Grease 10 BDL

0.1 – 50 mg/l4 Amino Antipyrene method without Chloroform Extraction (Direct Photometric method) (5530 D APHA Standard Methods 22nd edi.) -2012mg/lPhenolic Compounds 11 bdl

05–50000 mg/l3 – Day BOD test. (IS 3025 (Part 44) 1993 Reaffirmed 1999)-2009mg/lB.O.D (3 Days 27oC) 12 <5

: REP-Representative/Grab, (Insp Type : COM-On Complaint)

: M.U.PATEL,DEE

: 5 Lit.

: 249428

: 26/12/2018 , (1605 to 1605) & 27/12/2018

: 28/12/2018 & 10/01/2019

: Bore well of Luna Gram Panchyat at garden (bag) Vill. Luna, Ta.Padra, Dist.Vadodara. ~ OSW - 5

: ---

: ---

: 0

: 26 & pH Range on pH Strip :@ 7-8 on pH strip

: Barcode & Color & Appearance :Colorless

: Ind :10.000 , Dom :1.000 & Ind :9.000 , Dom :1.000

: Complaint - 32381

: Vadodara District,-,-

Vadodara Dist--, Taluka : Vadodara, District : Vadodara, GIDC : Not In Gidc

Laboratory Remarks : Approved By:236-lab_236 Dt.: 15/01/2019

D. N. Vasadia, Lab Head

11/03/2019N I C

Note :

1. * - These parameters are NOT covered under the scope of NABL.

2. The results refer only to the tested samples and applicable parameters. Endorsement of products is neither inferred nor implied.

3. Samples will be destroyed after 10 days from the date of issue of test report unless otherwise specified.

4. This report is not to be reproduced wholly or in part or used in any advertising media without the permission of the Board in writing.

5. The Board is not responsible for the authenticity for the samples not collected by the Board’s officials.

6. Total liability of our laboratory is limited to the invoiced amount. Any dispute arising out of this report is subject to

Gujarat Jurisdiction only.

7. Permissible Limits: as per Schedule VI of EPA Rules, 1986 as ammended by Second and Third ammendment 1993 for Effluents

8. Physicochemical and microbiological parameters, Std.Methods for Water and Waste Water- 22nd Edition by APHA.

9. Bioassay test (for toxicity) -IS:6582:Part-2:2001; Reaffirmed 2007.

Field Observation :