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Underpinning the credibility ofmeasurement results :
How to combine skills of both OIV and international measurement infrastructure
“Oenology - Nutrition & Health - Methods of analysis” UnitJ. Claude Ruf, Ph.D. - OIV
“Oenology - Nutrition & Health - Methods of analysis” UnitJ. Claude Ruf, Ph.D. - OIV
IntergovernmentalOrganisation
Workshop on Comparability and traceability in food analysis18-19 November 2003 - Sevres (France)
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Overview
The wine sector : its economic value
The OIV : background information
Two examples
Collaborating with a metrology institute : how OIV profited
Future outlook
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the wine sector : its economic value Les échanges internationaux en 2002
(en parts de marché)
65%
21%
14% 10%
71%75%79%76%
15%
0%
25%
50%
75%
100%
moy 81-85 moy 86-90 moy 91-95 moy 96-00 2002 prev.
« Hémisphère Sud »(Arg, ChiIi, AFS, Aust, NZ)
et USA
PECO et Maghreb
• France : 1er exportateurmondial (env. 15,4 Mio hl)• Italie (15 Mio hl ; - 3 %)• Espagne (9,5 Mio hl ; - 4,5 %)
Note O.I.V. de conjoncture mondiale (Patrick AIGRAIN - mars 2003)
en 2002
5 premiers paysexportateurs de l ’UE
(F, I, Sp, D, P)
Note O.I.V. de conjoncture mondiale
70,5%
17,8%
4,9%
4,0%2,9%
20012001266,1 10 6 hl
Europe
AmericaAfrica
AsiaOceania
0
2
4
6
8
10
12
Wine, must Olive oil wheat Total cereals
% of different products in the UE final agriculture production
Wine production
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OIV - IRMM structuresOIV : Intergovernmental organisation 47 member states Missions: - to assist other international organisations especially those which carry out standardisation
activities; - to contribute to international harmonisation of
existing practices and standards and, as necessary, to the preparation of new international standards
OIV : Intergovernmental organisation 47 member states Missions: - to assist other international organisations especially those which carry out standardisation
activities; - to contribute to international harmonisation of
existing practices and standards and, as necessary, to the preparation of new international standardsIRMM : is part of the Directorate General - Joint Research Centre of the European Commission Missions: - The mission of the IRMM is to promote a common European measurement system in support of EU policies, especially health and consumer protection, environment, agriculture, internal market and industrial standards
IRMM : is part of the Directorate General - Joint Research Centre of the European Commission Missions: - The mission of the IRMM is to promote a common European measurement system in support of EU policies, especially health and consumer protection, environment, agriculture, internal market and industrial standards
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A partnership based on strength ofOIV IRMM
• Expert in wine matters and wine methods
• links to wine sector institutes
• knowledgeable on those issues that are key to quality & safety
• Experts in reference measurements & materials
• links to metrology, accreditation, standardisation bodies
• knowledgeable on best practice in measurements across sectors
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Common interest : Reliable measurement results
Measurements are used to make decisions- in trade - consumer protection
OIV goal : result from Chilean lab equivalent to that from France …
Creating confidence in measurements :- by showing that best practice is followed- by having a transparent system
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OIV : long tradition in measurements
Sub-commission on Analysis (since 1935 mod.1954)
OIV produces standardised methods (compendium)
OIV members perform validation of these methods on interlaboratory tests
Strong link with networks of field laboratories, national regulation systems, and with international organisation (e.g. Codex Alimentarius, CEN, ISO, AOAC, IAM )
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Measurement result quality : some key issues
Quality of a result : responsibility of individual laboratories in member states
Laboratory competence assessment : OIV stimulates use of accreditation
How equivalent is measurement capability across the world ? Diffic ult to assess for OIV
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Example 1 :The European project REFMAT
OBJECTIVES:
Establishing field reference materials for the authentication of food and beverages by isotopic analysesD and 18O of water13C of sugar and ethanol
Certification of 5 Reference Materials suitable for isotopic analysis of wine, alcohol, fruit juices and sugars.
Improve the comparison of isotopic determinations in enforcement laboratories
funded by the DG Research of the European Commission (SMT3 - CT96 – 2086).
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Example 2 :IMEP-16
41st Meeting of the OIV sub-
commission of methods of analysis
Presentation of the International measurement Evaluation Programme (IMEP-16) concerning lead in wine
- 160 laboratories, 40 countries - Lead concentration: 27 0.33 µg/l see http//www.irmm.jrc.be/imep
aim : global assessment measurement capability
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Assessing the quality of results of measurements : IMEP-16
13.59
16.31
19.03
21.74
24.46
27.18
29.90
32.62
35.33
38.05
40.77
-50
-40
-30
-20
-10
0
10
20
30
40
50
Use of an official method
No use of an official method
No information
Pb
Results from all participants in relation to the use of an official analytical method
IMEP- 16: Pb in wine
Certified value : 27.18 ± 0.33 µg·L-1
[U=k·uc (k =2)]
Use of an official method 3
No use of an official method 7
No info 1
Values below -50%
No use of an official method 5
'Less than' value
Values above 50%
Use of an official method 6
No use of an official method 20
No info 1
official method 2676/90
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Assessing the quality of results of measurements : IMEP-16
13.6
16.3
19.0
21.7
24.5
27.2
29.9
32.6
35.3
38.1
40.8
-50
-40
-30
-20
-10
0
10
20
30
40
50
Pb amount content
Results from all participants with indication of the results of the OIVV members
IMEP- 16: Pb in wineCertified value : 27.18 ± 0. 33 µg·L
-1 [U =k ·u c (k =2)]
5 'less than' values11 values
below -50%
28 valuesabove 50%
OIVV members
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BIPM-CCQM pilot study 12
0.066
0.088
0.110
0.132
0.154
0.176
0.198
c
1
0-9
mo
l·g
-1
CCQM-P12 : Pb in wine
IRMM certified value(corresponds to IMEP-16 certified value)
Results from BAM, Germany; CENAM, Mexico; CSIR-NML, South-Africa; EMPA, Switzerland; IRMM, European Commission; KRISS, Korea; LGC, United Kingdom; LNE, France; NARL, Australia; NIMC, Japan; NIST, United States of America; NRCCRM, China; PTB, Germany; VNIIM, Russian Federation
±50%
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Conclusions :how did OIV profit ?
Link with a community previously unknown, opportunities for symbiosis
Reference Measurements and Materials is not OIV core business : profit from core business of others
Exposed to best practice : designation of laboratories (e.g. control, inspection, reference laboratories) should ideally be backed up by demonstrated competence
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Conclusion : further prospects
Scope for further strengthening link with metrology infrastructure via appropriate projects– interlaboratory comparisons– appropriate wine CRMs– appropriate training of laboratories and
end-users (e.g. enforcers, regulators)
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