The scientific platform at your service · 2021. 4. 21. · Pierre Lavedan Stéphane Massou...
25
The scientific platform at your service Scientific and technical platform of the Institut de Chimie de Toulouse- Université Paul Sabatier 1
Transcript of The scientific platform at your service · 2021. 4. 21. · Pierre Lavedan Stéphane Massou...
The scientific platform
at your service
Scientific and technical platform of the Institut de Chimie de Toulouse- Universiteacute Paul Sabatier
1
Welcome to the Institut de Chimie de Toulouse
The platform is a collection of communal services that are indispensable to yourresearch It exists to respond to your needs and help you in your research
Specialists in the characterisation and purification of molecules informationtechnology glass blowing electronics and documentation are waiting to adviseyou Follow our service guide
You can also find us on the web at ictcnrsfr and subscribe to our newsletter at comictictups-tlsefr
During this pandemic situation the services have set up specific rules to complywith for everyonersquos sake Check with the staffDonrsquot hesitate to contact us
2
Summary
1 - Characterisation amp purification 4bull X-Ray Diffraction 5bull Chromatography 6bull Nuclear Magnetic Resonance 7bull Mass spectrometry 8bull Infrared spectroscopy 9
2- Technopolym 10bull Technopolym Platform 11
3- Cross-Platform Services 12bull Documentation 13bull Electronics 14bull Information technology 15bull Scientific glassware 16
4- LCC Services 17bull Thermal analyses 18bull Library resource center 19bull Single-crystal and powder X-Ray Diffraction 20bull Electrochemistry 21bull Magnetic measurement and Moumlssbauer spectroscopy 22bull Elementar analyses CHNS 23bull Nuclear Magnetic Resonance 24bull Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) 25
3
Characterisation amp purification
4
Single Crystal X-Ray Diffraction
How to request an analysis
bull Beforehand
As soon as the crystals are obtained contact the staff of theservice so that they can evaluate the quality of the sample
If hte sample quality is judged to be sufficient to measure theX-ray diffraction an analysis request form should becomleted and submitted with the sample
bull For all analysis requests
Every sample must be accompanied by a completed analysisrequest form You will find this form on the ICT website
ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsdiffraction-des-rayons-x
Take care to specify the properties of the sample (sensitivityto air tempeacuterature lighthellip) the reagents used and theexpected crystal structure
Also specify the information that you hope to obtain from theanalysis (eg absolute configuration hellip)
While yoursquore waiting for the evaluation of the
crystal quality manipulate the
sample as little as possible and keep it
at the crystallizationtemperature until the
analysis
Who to contactNathalie Saffon (Mgr)Sonia Mallet-Ladeira
Tel 05 61 55 83 48 or 8173 Email rxictchimieups-tlsefr
Where can you find us Door 2053 2nd floor
Laboratory - Door 055 basement building 2R1
Universiteacute Paul Sabatier
When Monday Tuesday Thursday and
Friday
Some advice
5
How to request an analysis or a purification
bull For any request for analysis or purification (reverse or normal phaseionic or supercritical chromatography)
All samples must be accompanied by a fully completed form preferablydouble-sided which will be retained by the service
You will find this form on the ICT website
ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upshplc
Any sample not accompanied by this form will not be treated
bull Samples preparation
For your analysis you can prepare yourself your samples in 02 microm self-filtering vials (available on the platform) with a concentration of 1 mgmL
For your purifications you can bring the raw product
All services are provided after a validated appointment given by theplatform staff when depositing samples
bull Recovery of your results or purified samples
A generic analysis report is sent by email in PDF format
The platform staff listen to your needs for a more detailed report
Come and collect your purified products upon receipt of the results
Please note that saving the results is not guaranteed in the long term Takecare we do not guarantee the long-term storage of your results
bull Self-service devices
Any equipment can be made available after validation of the training onthe device concerned by the platform manager
To do this make an appointment one month before the desired use inorder to obtain validation of your training on time This validation is validfor a fixed period
Online booking httpglpi-ictgrr-hplc to use equipments
For the preparation of your samples
solid phase extraction cartridges
and self-filtering vials are available
Contact us in case of difficulties in filling
in the form or in defining the best
separation method suitable for your
product
Who to contactIsabelle FabingOffice 05 61 55 81 98
Lab 05 61 55 62 95email hplcictchimieups-tlsefr
Where can you find us Door 30793083 3rd floor
building 2R1 Universiteacute Paul Sabatier
When Monday to Friday
Reception
9h30-11h30 am
Some advice
6
Chromatography
copyFreacutedeacuteric MaligneICT
How to request an analysis
bull For all analysis requests on the 400 and 500 MHz NMR spectrometerssituated in the High Technology Module (MHT)Each sample must be accompanied by a fully completed laquo AnalysisRequest raquo form You can find this form on the ICT websiteictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsrmn oron the website of the NMR service (httprmn-webups-tlsefr)It is essential to make an appointment by email telephone or in personat the NMR service
bull For all analysis requests on the 300 MHz open access NMR spectrometerslocated in Building 2R1You must sign up to the NMR training before using the 300 MHz spectrometers (inscription form on the website of the NMR service httprmn-webups-tlsefr)
bull Follow the instructionsI ndash NMR Tubes
NMR tubes must meet a minimum standard of qualityBroken or damaged tubes and Economy tubes are forbidden from the service as they are too fragile
II ndash Cleaning tubes After the analysis the tubes must be washed as quickly as possible using the same solvent that was used to dissolve the analyte After several rinses the tube should be dried at room temperature or in an oven at less than 60degC
III ndash Filling the tubesFor an optimal measurement your tube should contain 600 microL of
solvent bull Results spectra can be recovered by
- downloading from the NMR server- USB stick- by email (only for 1 D analyses)
Once the analysis has been completed you must come to pick up yoursamples from the NMR service
The sensitivity of an NMR experiment depends on the
nucleus studied and the concentration of your product
If necessary during samplepreparation filter your solutions
in order to remove any suspendedsolids
The choice of solvent dependsprimarily on the solubility of your
product at room temperature
If there are several possibilities choose a solvent whose peaks do
not interfere with those of yourproduct
For more information please feelfree to contact the staff of the NMR
service
Who to contact
Marc Vedrenne (Msg)Pierre Lavedan
Steacutephane MassouCaroline ToppanClaude Andreu
Tel 05-61-55 ext 84-78 68-78Email rmnictchimieups-tlsefr
Where to find us Door 45 Ground floor High
Technology Module Universiteacute Paul Sabatier
When Monday to Friday
09h00-12h00 and 14h00-16h30
Some advice
NMR Service
copyFreacutedeacuteric MaligneICT
Mass spectrometry
How to request an analysis
bull For all analysis requests
Each sample must be accompanied by a fully completedanalysis request form You can find this form on the ICT website ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsspectrometrie-de-masse
You can also fill in all the administrative details one timeonly and save them for your future requests and you canarchive your forms
Bring the forms (preferably double-sided) and sample duringopening hours We will check with you the feasibility of theproposed analyses
bull For air-sensitive samples
Make an appointment
bull For LCMS and GCMS analyses
Make an appointment
bull How to collect your results
The results will be sent to you in pdf format Upon receivingour mail you can come and pick up your samples and formsduring opening hours
We will assess the feasibility of the
analysis with you
If you donrsquot know which method of ionization is
better suited for your molecules then leave it
blank and we will choose together
Who to contactCatherine Claparols ( Mgr)
Valeacuterie BourdonEric Leroy
Nathalie Martins-FromentTel 33 5 61 55 64 69Fax 33 5 61 55 81 16
Email spectromasseictups-tlsefr
Where to find us
Door 157 groundfloor building 2R1 Universiteacute Paul Sabatier
When
Monday-Friday 10h30-12h and 13h30-15h00
Some advice
8
copyFreacutedeacuteric MaligneICT
INFRARED Spectroscopy
How to request an analysis
bull For each analysis request
Each sample must be accompanied by a fully completedanalysis request form You can find this form on the ICT website ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsspectroscopies-infrarouge and on the door of the service
Required sample quantity 05 to 2 mg for powders 1drop for liquids 1ml for solutions (in this case you will alsoneed to supply 10-20 ml of pure solvent)
bull For infrared microscopy kinetics
Please make an appointment
bull For other analyses transmission ATR DRIFT far-IR NIR
Leave your sample at the service If unattended a box isavailable on the door to drop off your samples
bull Open access equipment for ATR analyses only
It can be used after completion of a 1h training course Makean appointment
All kinds of samples can beanalyzed solids liquids solutions blocks grains of
wheathellipyou just needto choose the right
method depending on your sample and your
study
Come and discuss with us
Extensive infrared and Raman tables and
spectral data bases are available at the
service60 000 data base spectra
are available
Who to contactCorinne Routaboul
Tel 05 61 55 64 00Email routabouictchimieups-tlsefr
Where to find us Door 1025 1st floor building 2R1
Universiteacute Paul Sabatier
When Monday-Friday 9h00-17h00
If unattended leave the sample in the deposit box on the door If youhave more than 10 samples or if you need particular techniques please make an appointment
Some advice
9
copyFreacutedeacuteric MaligneICT
TECHNOPOLYM
10
Technopolym
How to request an analysis
bull Request an analysis via the central Technopolym emailtechnopolymictchimieups-tlsefr
Following this email we will inform you about the proposedtechniques of analyse costs time of delivery requiredquantity of sample conditioning sample deposit Dependingon your expected results an appointment to discuss yourproblem may be proposed before scheduling an analysis
bull For all analysis requestsEach sample must be accompanied by a fully completed
analysis request form You can find this form on the ICT website
ictcnrsfrplateforme-de-licttechnopolym or on the Technopolym website
httptechnopolymups-tlsefr
bull For more information
Visit our website to know about our skills equipment references
TechnopolymIs a virtual technological
platform dedicated to the characterization of polymeric
materials
We propose a range of analytical techniques
molecularcharacterization phase
transitions thermal stability behavior in
solution mechanicalproperties surface characterizationhellip
Come and talk to us
Who to contactPascale Saint-Aguet
Tel 05 61 55 68 08Tel (LCC) 05 61 33 31 34
Email technopolymictchimieups-tlsefr
Some advice
Where to find us
Door 30233rd floor building 2R1 Universiteacute Paul Sabatier
Door G064 ndashLCC 205 rte de Narbonne -
When
Monday-Friday 9h-12h and
14h-17h
11
Cross-Platform Services
12
Documentation
How to make a request
bull For all document requests
You can request your document by email telephone or inperson Donrsquot forget to indicate your full name and laboratorywith the references on your request
bull Consultation and loans
The catalogue of the chemistry library is available on theintranet
ictcnrsfrdocchimie
Borrowing is possible during office hours ndash outside thesehours please make an appointment
bull For bibliographic searches and training
Make an appointment
bull Open access
You can come and work at the library ndash computers and wifi are available Visit our website
ictcnrsfrplateforme-de-lictservices-transversesaccueil-de-la-documentation
Ask the documentation service for your intranet
password from
Feel free to call the service for any problems
relating to the use of bibliographic databases
Who to contactDanielle Brunet
Tel 05 61 55 85 69Email brunetictchimieups-tlsefr
Some advice
Where to find us
Door 0145 ground floor building 2R1
Universiteacute Paul Sabatier
When
Mon-Fri 9h-12h and 14h-17h If unattended make an
appointment
13
Electronics
How to make a request
Who to contactJean-Michel Martin
Tel 05 61 55 86 93Email scicassistanceictchimieups-tlsefr
Email martinjmictchimieups-tlsefr
Feel free to ask the service for
- Modification of existingelectronic devices and
proposals for improvement
- Troubleshooting and repair of electronic
devices
- Advice on purchase of new material
bull For all installation andor maintenance of equipment with astrong electronic component
Send an email phone or contact the service in person duringoffice hours
bull For all service requests
Send an email toscicassistanceictchimieups-tlsefrstating your name office number and a brief description of the problem
bull Loan of equipment
To address the needs of users specific equipment is availablein the electronics workshop (Oscilloscope component testerssoldering ironhellip) aswell as various tools
It is possible to borrow this equipment
Where to find usDoor 1015 1st floor building 2R1 Universiteacute Paul Sabatier
When Monday-Friday office hours
If unattended make an appointment
Some advice
14
Information Technology
How to make a request
bull For all requests for connection to the network andcreation of email accounts
First see the secretary of your laboratory
bull For all service requests
Write toscicassistanceictchimieups-tlsefr
stating your name office number and a brief description of the problem
The IT service manages developsand maintains the
network and associated services
Please contact us for more information on
the services provided (automatic
backup of data access to Cambridge CCDC data sharing
etc)
Who to contactPascal Puech
Edouard IvanovtchikTel 05 61 55 68 73
Email scicassistanceictchimieups-tlsefr
Some advice
Where to find usDoor 168 ground floor building 2R1
Universiteacute Paul Sabatier
WhenMonday-Friday office hours
If unattended make an appointment
15
Scientific Glassware
How to make a request
bull For all service requests
All glassware to repair or construct must be accompanied bya fully completed form You can find this form on the ICTwebsite ictcnrsfrVerrerie-scientifique
For obvious reasons of safety and hygiene glassware must beclean free of silicon grease and in a container identified withthe name of the research group
bull Do I need to go in person
In person contact is preferred if you are new to glasswork andif your request is complex
Photos et technical drawings sent by email are onlycomplementary information as in isolation they can lead tomisunderstandings and errors
For all glass repairs construction of new
equipment or prototyping
feel free to consult the glassware service
We can provide technicaladvice as well as contacts
in specialized domains
Who to contactSteacutephane Foulon
Tel 05 61 55 61 16Email foulonictchimieups-
tlsefr
Some advice
Where to find us
Door 0194 Ground Floor Building 2R1Universiteacute Paul
Sabatier
When
Monday-Friday during office hours We recommend that
external users make an appointment
16
copyFreacutedeacuteric MaligneICT
LCC Services
17
Thermal Analyses LCC
How to request an analysis
bull For any analysis request
DTATGA or DSC analyses each sample must be suppliedwith an analysis request form duly filled out To requestthese forms please contact the staff by e-mail
In the very first request please contact the staff fordetails about the process the sample amount requiredthe packaging of samples etc
In all other cases the analyses requests and the samplescan be deposited in the Thermal Analyses Departmentrsquosletter-box (within the LCC entrance hall)
bull Air-sensitive samples
Make an appointment with the staff
bull Results
Analyses results are emailed as a text file paper copy isavailable upon request
On completion of analyses remaining of samples must bepick up at LCC
Analytical Equipments
DTATGA for measuring the mass variation as a
function of temperature
DSC for detecting the phase changes without mass loss
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 1 0Email j-fmeunierlcc-toulousefr
Some advice
Where to find usLCC - Door CS12 basement level
205 route de Narbonne
When Opening hours 9h to 11h30 - 14h to 17hfrom Monday to Friday except on wednesday
18
Library Resource Center LCC
How to make a request
bull For any information request
- LCC research teams fill out the request form available onthe LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs contact the staff by e-mail
bull For bibliographical searches and access
Digital databases
- LCC research teams bibliographical searches databases areavailable on the LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs make an appointment with the staff
Paper print collections
Paperprint collections also are available and can be read in thelibrary premises
LCCrsquos Library access is free for LCC teams and subject to anappointment for outside labs
LCC teams Access to the LCC intranet is provided
with taking office
For further information feel free to contact us
Who to contact
Marie-Heacutelegravene Gullimarie-helenegullilcc-toulousefr
0561333217
Gilles Roujasgillesroujaslcc-toulousefr
0561333140
Gaeumltan Havetgaetanhavetlcc-toulousefr
0561333140
Some advice
Where to find usLCC 205 route de Narbonne
When Opening hours
9 h to 11h30 - 13h to 17h From Monday to Friday
19
Feel free to contact us for anyquestion about analyses
options or for anydiscussion about the
best strategy to meetyour specific issues
Single ndashcrystal and powder X-Ray Diffraction - LCC
How to request an analysis
bull Prior to any analysis
Contact the staff in charge of X-Ray Diffraction measurementsfor your team or your lab
bull Single-crystal X-ray diffraction
First the staff will evaluate the quality of the sample If quality isacceptable for a X-ray diffraction measurement an appointmentwill be set up for analysis
Following information must be provided expected compound used solvents any specific information concerning the sample(air-sensitive thermal-sensitive light-sensitivehellip) analysis and required data (absolute configuration hydride locationhellip)
bull Powder X-ray diffraction
Appointments are proposed in accordance with the type of measurement (reflection capillary measurements at variable temperatures x-ray grazing incidence on thin films)
Following information must be provided sample characteristics analytical conditions (scanning range of 2theta temperaturehellip) required data (phase identification crystallites sizehellip)
Useful tips Until getting staff opinion about the quality of yoursample particularly for a single-crystal handle it as little as possible
Who to contact Laure Vendier (Mgr)
Carine DuhayonSonia Mallet-Ladeira
Tel 05 61 33 31 18Email laurevendierlcc-toulousefr
carineduhayonlcc-toulousefrladeiraictchimieups-tlsefr
Some advice
Where to find us
LCC 205 route de NarbonneX-Ray Diffraction office ground floor door B017 X-Ray Diffraction Lab basement level door GS66
When
9h to 11h30 - 14h to 17hFrom Monday to Friday except on Wednesday afternoon
20
Electrochemistry - LCC
How to request an analysis
bull For any analysis request
Analyses are carried out by appointment onlyscheduled with the staff when requesting theanalysis
On the appointed date Bring the sample and the solvent Your presence is required during the analyses
bull Sample preparation
The sample(s) must be as pure as possible correspondingto a concentration of 10-3 molL-1 in 10 mL
For each sample bring 30 mL of purified solvent
bull Results
On completion of the analyses the mostrepresentative curves are provided in paper copy
Upon request the electronic files can be emailed
Who to contactAlix Sournia-Saquet (Mgr)
Alain MoreauTel 05 61 33 31 75
Email alixsaquetlcc-toulousefralainmoreaulcc-toulousefr
Some advice
Before any analysis feel free to contact us for any
discussion or question about feasibility and conditions of
analyses
The staff can help you
- to choose the best-suited technique to your needs
- for interpretation of your data
Where to find us LCC- door B015ndash ground floor-building B205 route de Narbonne
When 9h to 11h30 -14h to 17h
From Monday to Friday
21
Magnetic Measurement and Moumlssbauer spectroscopy - LCC
How to request an analysis
bull For any analysis request
For magnetic measurements SQUID andMoumlssbauer spectroscopy please contact Jean-Franccedilois Meunier by e-mail or phone
An appointment will be set up in order to studyyour analyses requests and to define theexperimental conditions
An analysis request form will be provided by thestaff
bull Results and samples
Results are emailed as text and excel files
On completion of the analyses samples must beretrieved at LCC
Further information on equipments
lcc-toulousefrServices Spectroscopie Moumlssbauer
Lcc-toulousefr
servicesMesures
Magneacutetiques
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 10Email Jf-meunierlcc-toulousefr
Where to find usLCC door CS012
205 route de Narbonne
When 9h to 12h - 14h to 17h30
From Monday to Friday
Some advice
22
Elemental Analysis C-H-NS - LCC
How to request an analysis
For any analysis request
Each sample must be supplied with an analysis request formavailable on LCC website
wwwlcc-toulousefr gt services gt services techniques ampscientifiques gt analyses chimiques gt Formulaire
Fill in electronically and send by mail (see framed who tocontact)
Samples
- Internal in my box DEPOT CHN in the mail locker analyseselementaires
- External ship by courrier to LCC service CHN or ask anappointment
Results
Results are sent by mail Samples are not returned
Analyses
Analyses are carried out every week
10 mg of compound areneeded for 2 essays andpackaged in a vial
Sensitive samples mustbe isolated in sealedampoule
For special analysisrequests please contactservice
Sulphur is analyzed oncea year if enoughdemand
Who to contact Isabelle BorgetTel 05 61 33 32 14
mail isabelleborgetlcc-toulousefr
Where to find service LCC door B038
205 route de Narbonne
When 9h to 11h30 - 14h to 16h30
From monday to friday
on appointment
Some advice
23
Nuclear Magnetic Resonance - LCC
How to request an analysis
bull For any analysis request (except self-service equipments)
For NMR equipments (400-solid and 600 MHz) analysisand appointment requests must be emailed to Y Coppelor C Bijani
The analysis request form can be loaded from the NMRfacility webpage on the LCC website (httplcc-toulousefr)
bull Self-service equipments
All the users have to follow a training conducted by NMRfacilityrsquos staff before any use of self-service spectrometers
- for LCC teams the training and NMR user accountrequests are provided with taking office
- for outside labs please contact the LCC personneldepartment
The requests when validated must be returned directlyto A Bonnet or D Paryl in order to plan the training
The users undertake to carefully respect the operatinginstructions and the LCC memos
All the data are automatically
- made available in the LCC teamsrsquo laquo Nuage raquo file
- emailed to the user from outside labs
Feel free to contact us for any question
about analysis capabilities or for
any discussion about the best strategy to
meet your specific issues
Who to contact
Yannick Coppel (Mgr)Christian BijaniTel 05 61 17 54 27
Antoine BonnetDavid Paryl
Tel 05 61 17 54 30Email yannickcoppellcc-
toulousefrchristianbijanilcc-toulousefrantoinebonnetlcc-toulousefr
davidparyllcc-toulousefr
Some advice
Where to find us
LCC RMN Building 205 route de Narbonne Toulouse
Door 030 (Y Coppel et C Bijani)
Door 033 (F Lacassin et D Paryl)
When8h30 to 11h30 -14h to 17h
From Monday to Friday
24
Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) - LCC
How to request an analysis
bull For any analysis request
Each sample must be supplied with an analysisrequest form To request this form please contact the staff
Sample amount depends on the concentration of chemical elements to be measured in the sampleanalyzed
In the very first request please contact the staff
bull Results
Results are delivered in the letter-box of the LCC team or for outside labs made available in the ICP departmentrsquos letter-box (within the LCC entrance hall)
bull Analyses schedule
Analyses are carried out every 2 weeks
In general 10 mg per assay isneeded (provided that the
concentration is above 5 ww)
Chemical elements currentlyanalyzed (but not limited) Ag Al Au B Ba Be Bi Ca Cd Co Cr Cu Fe Ir K Li Mg Mn Na
Ni P Pb Pd Pt Ru Rh Sr Zn
Who to contact
Alain Moreau Tel 0561175850
E-mail alainmoreaulcc-toulousefr
Where to find usIPBS Bacirct A3
205 route de Narbonne
When 8h to 11h30 - 14h to 16h30From Monday to Friday (odd
week)
Some advice
25
Welcome to the Institut de Chimie de Toulouse
The platform is a collection of communal services that are indispensable to yourresearch It exists to respond to your needs and help you in your research
Specialists in the characterisation and purification of molecules informationtechnology glass blowing electronics and documentation are waiting to adviseyou Follow our service guide
You can also find us on the web at ictcnrsfr and subscribe to our newsletter at comictictups-tlsefr
During this pandemic situation the services have set up specific rules to complywith for everyonersquos sake Check with the staffDonrsquot hesitate to contact us
2
Summary
1 - Characterisation amp purification 4bull X-Ray Diffraction 5bull Chromatography 6bull Nuclear Magnetic Resonance 7bull Mass spectrometry 8bull Infrared spectroscopy 9
2- Technopolym 10bull Technopolym Platform 11
3- Cross-Platform Services 12bull Documentation 13bull Electronics 14bull Information technology 15bull Scientific glassware 16
4- LCC Services 17bull Thermal analyses 18bull Library resource center 19bull Single-crystal and powder X-Ray Diffraction 20bull Electrochemistry 21bull Magnetic measurement and Moumlssbauer spectroscopy 22bull Elementar analyses CHNS 23bull Nuclear Magnetic Resonance 24bull Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) 25
3
Characterisation amp purification
4
Single Crystal X-Ray Diffraction
How to request an analysis
bull Beforehand
As soon as the crystals are obtained contact the staff of theservice so that they can evaluate the quality of the sample
If hte sample quality is judged to be sufficient to measure theX-ray diffraction an analysis request form should becomleted and submitted with the sample
bull For all analysis requests
Every sample must be accompanied by a completed analysisrequest form You will find this form on the ICT website
ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsdiffraction-des-rayons-x
Take care to specify the properties of the sample (sensitivityto air tempeacuterature lighthellip) the reagents used and theexpected crystal structure
Also specify the information that you hope to obtain from theanalysis (eg absolute configuration hellip)
While yoursquore waiting for the evaluation of the
crystal quality manipulate the
sample as little as possible and keep it
at the crystallizationtemperature until the
analysis
Who to contactNathalie Saffon (Mgr)Sonia Mallet-Ladeira
Tel 05 61 55 83 48 or 8173 Email rxictchimieups-tlsefr
Where can you find us Door 2053 2nd floor
Laboratory - Door 055 basement building 2R1
Universiteacute Paul Sabatier
When Monday Tuesday Thursday and
Friday
Some advice
5
How to request an analysis or a purification
bull For any request for analysis or purification (reverse or normal phaseionic or supercritical chromatography)
All samples must be accompanied by a fully completed form preferablydouble-sided which will be retained by the service
You will find this form on the ICT website
ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upshplc
Any sample not accompanied by this form will not be treated
bull Samples preparation
For your analysis you can prepare yourself your samples in 02 microm self-filtering vials (available on the platform) with a concentration of 1 mgmL
For your purifications you can bring the raw product
All services are provided after a validated appointment given by theplatform staff when depositing samples
bull Recovery of your results or purified samples
A generic analysis report is sent by email in PDF format
The platform staff listen to your needs for a more detailed report
Come and collect your purified products upon receipt of the results
Please note that saving the results is not guaranteed in the long term Takecare we do not guarantee the long-term storage of your results
bull Self-service devices
Any equipment can be made available after validation of the training onthe device concerned by the platform manager
To do this make an appointment one month before the desired use inorder to obtain validation of your training on time This validation is validfor a fixed period
Online booking httpglpi-ictgrr-hplc to use equipments
For the preparation of your samples
solid phase extraction cartridges
and self-filtering vials are available
Contact us in case of difficulties in filling
in the form or in defining the best
separation method suitable for your
product
Who to contactIsabelle FabingOffice 05 61 55 81 98
Lab 05 61 55 62 95email hplcictchimieups-tlsefr
Where can you find us Door 30793083 3rd floor
building 2R1 Universiteacute Paul Sabatier
When Monday to Friday
Reception
9h30-11h30 am
Some advice
6
Chromatography
copyFreacutedeacuteric MaligneICT
How to request an analysis
bull For all analysis requests on the 400 and 500 MHz NMR spectrometerssituated in the High Technology Module (MHT)Each sample must be accompanied by a fully completed laquo AnalysisRequest raquo form You can find this form on the ICT websiteictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsrmn oron the website of the NMR service (httprmn-webups-tlsefr)It is essential to make an appointment by email telephone or in personat the NMR service
bull For all analysis requests on the 300 MHz open access NMR spectrometerslocated in Building 2R1You must sign up to the NMR training before using the 300 MHz spectrometers (inscription form on the website of the NMR service httprmn-webups-tlsefr)
bull Follow the instructionsI ndash NMR Tubes
NMR tubes must meet a minimum standard of qualityBroken or damaged tubes and Economy tubes are forbidden from the service as they are too fragile
II ndash Cleaning tubes After the analysis the tubes must be washed as quickly as possible using the same solvent that was used to dissolve the analyte After several rinses the tube should be dried at room temperature or in an oven at less than 60degC
III ndash Filling the tubesFor an optimal measurement your tube should contain 600 microL of
solvent bull Results spectra can be recovered by
- downloading from the NMR server- USB stick- by email (only for 1 D analyses)
Once the analysis has been completed you must come to pick up yoursamples from the NMR service
The sensitivity of an NMR experiment depends on the
nucleus studied and the concentration of your product
If necessary during samplepreparation filter your solutions
in order to remove any suspendedsolids
The choice of solvent dependsprimarily on the solubility of your
product at room temperature
If there are several possibilities choose a solvent whose peaks do
not interfere with those of yourproduct
For more information please feelfree to contact the staff of the NMR
service
Who to contact
Marc Vedrenne (Msg)Pierre Lavedan
Steacutephane MassouCaroline ToppanClaude Andreu
Tel 05-61-55 ext 84-78 68-78Email rmnictchimieups-tlsefr
Where to find us Door 45 Ground floor High
Technology Module Universiteacute Paul Sabatier
When Monday to Friday
09h00-12h00 and 14h00-16h30
Some advice
NMR Service
copyFreacutedeacuteric MaligneICT
Mass spectrometry
How to request an analysis
bull For all analysis requests
Each sample must be accompanied by a fully completedanalysis request form You can find this form on the ICT website ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsspectrometrie-de-masse
You can also fill in all the administrative details one timeonly and save them for your future requests and you canarchive your forms
Bring the forms (preferably double-sided) and sample duringopening hours We will check with you the feasibility of theproposed analyses
bull For air-sensitive samples
Make an appointment
bull For LCMS and GCMS analyses
Make an appointment
bull How to collect your results
The results will be sent to you in pdf format Upon receivingour mail you can come and pick up your samples and formsduring opening hours
We will assess the feasibility of the
analysis with you
If you donrsquot know which method of ionization is
better suited for your molecules then leave it
blank and we will choose together
Who to contactCatherine Claparols ( Mgr)
Valeacuterie BourdonEric Leroy
Nathalie Martins-FromentTel 33 5 61 55 64 69Fax 33 5 61 55 81 16
Email spectromasseictups-tlsefr
Where to find us
Door 157 groundfloor building 2R1 Universiteacute Paul Sabatier
When
Monday-Friday 10h30-12h and 13h30-15h00
Some advice
8
copyFreacutedeacuteric MaligneICT
INFRARED Spectroscopy
How to request an analysis
bull For each analysis request
Each sample must be accompanied by a fully completedanalysis request form You can find this form on the ICT website ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsspectroscopies-infrarouge and on the door of the service
Required sample quantity 05 to 2 mg for powders 1drop for liquids 1ml for solutions (in this case you will alsoneed to supply 10-20 ml of pure solvent)
bull For infrared microscopy kinetics
Please make an appointment
bull For other analyses transmission ATR DRIFT far-IR NIR
Leave your sample at the service If unattended a box isavailable on the door to drop off your samples
bull Open access equipment for ATR analyses only
It can be used after completion of a 1h training course Makean appointment
All kinds of samples can beanalyzed solids liquids solutions blocks grains of
wheathellipyou just needto choose the right
method depending on your sample and your
study
Come and discuss with us
Extensive infrared and Raman tables and
spectral data bases are available at the
service60 000 data base spectra
are available
Who to contactCorinne Routaboul
Tel 05 61 55 64 00Email routabouictchimieups-tlsefr
Where to find us Door 1025 1st floor building 2R1
Universiteacute Paul Sabatier
When Monday-Friday 9h00-17h00
If unattended leave the sample in the deposit box on the door If youhave more than 10 samples or if you need particular techniques please make an appointment
Some advice
9
copyFreacutedeacuteric MaligneICT
TECHNOPOLYM
10
Technopolym
How to request an analysis
bull Request an analysis via the central Technopolym emailtechnopolymictchimieups-tlsefr
Following this email we will inform you about the proposedtechniques of analyse costs time of delivery requiredquantity of sample conditioning sample deposit Dependingon your expected results an appointment to discuss yourproblem may be proposed before scheduling an analysis
bull For all analysis requestsEach sample must be accompanied by a fully completed
analysis request form You can find this form on the ICT website
ictcnrsfrplateforme-de-licttechnopolym or on the Technopolym website
httptechnopolymups-tlsefr
bull For more information
Visit our website to know about our skills equipment references
TechnopolymIs a virtual technological
platform dedicated to the characterization of polymeric
materials
We propose a range of analytical techniques
molecularcharacterization phase
transitions thermal stability behavior in
solution mechanicalproperties surface characterizationhellip
Come and talk to us
Who to contactPascale Saint-Aguet
Tel 05 61 55 68 08Tel (LCC) 05 61 33 31 34
Email technopolymictchimieups-tlsefr
Some advice
Where to find us
Door 30233rd floor building 2R1 Universiteacute Paul Sabatier
Door G064 ndashLCC 205 rte de Narbonne -
When
Monday-Friday 9h-12h and
14h-17h
11
Cross-Platform Services
12
Documentation
How to make a request
bull For all document requests
You can request your document by email telephone or inperson Donrsquot forget to indicate your full name and laboratorywith the references on your request
bull Consultation and loans
The catalogue of the chemistry library is available on theintranet
ictcnrsfrdocchimie
Borrowing is possible during office hours ndash outside thesehours please make an appointment
bull For bibliographic searches and training
Make an appointment
bull Open access
You can come and work at the library ndash computers and wifi are available Visit our website
ictcnrsfrplateforme-de-lictservices-transversesaccueil-de-la-documentation
Ask the documentation service for your intranet
password from
Feel free to call the service for any problems
relating to the use of bibliographic databases
Who to contactDanielle Brunet
Tel 05 61 55 85 69Email brunetictchimieups-tlsefr
Some advice
Where to find us
Door 0145 ground floor building 2R1
Universiteacute Paul Sabatier
When
Mon-Fri 9h-12h and 14h-17h If unattended make an
appointment
13
Electronics
How to make a request
Who to contactJean-Michel Martin
Tel 05 61 55 86 93Email scicassistanceictchimieups-tlsefr
Email martinjmictchimieups-tlsefr
Feel free to ask the service for
- Modification of existingelectronic devices and
proposals for improvement
- Troubleshooting and repair of electronic
devices
- Advice on purchase of new material
bull For all installation andor maintenance of equipment with astrong electronic component
Send an email phone or contact the service in person duringoffice hours
bull For all service requests
Send an email toscicassistanceictchimieups-tlsefrstating your name office number and a brief description of the problem
bull Loan of equipment
To address the needs of users specific equipment is availablein the electronics workshop (Oscilloscope component testerssoldering ironhellip) aswell as various tools
It is possible to borrow this equipment
Where to find usDoor 1015 1st floor building 2R1 Universiteacute Paul Sabatier
When Monday-Friday office hours
If unattended make an appointment
Some advice
14
Information Technology
How to make a request
bull For all requests for connection to the network andcreation of email accounts
First see the secretary of your laboratory
bull For all service requests
Write toscicassistanceictchimieups-tlsefr
stating your name office number and a brief description of the problem
The IT service manages developsand maintains the
network and associated services
Please contact us for more information on
the services provided (automatic
backup of data access to Cambridge CCDC data sharing
etc)
Who to contactPascal Puech
Edouard IvanovtchikTel 05 61 55 68 73
Email scicassistanceictchimieups-tlsefr
Some advice
Where to find usDoor 168 ground floor building 2R1
Universiteacute Paul Sabatier
WhenMonday-Friday office hours
If unattended make an appointment
15
Scientific Glassware
How to make a request
bull For all service requests
All glassware to repair or construct must be accompanied bya fully completed form You can find this form on the ICTwebsite ictcnrsfrVerrerie-scientifique
For obvious reasons of safety and hygiene glassware must beclean free of silicon grease and in a container identified withthe name of the research group
bull Do I need to go in person
In person contact is preferred if you are new to glasswork andif your request is complex
Photos et technical drawings sent by email are onlycomplementary information as in isolation they can lead tomisunderstandings and errors
For all glass repairs construction of new
equipment or prototyping
feel free to consult the glassware service
We can provide technicaladvice as well as contacts
in specialized domains
Who to contactSteacutephane Foulon
Tel 05 61 55 61 16Email foulonictchimieups-
tlsefr
Some advice
Where to find us
Door 0194 Ground Floor Building 2R1Universiteacute Paul
Sabatier
When
Monday-Friday during office hours We recommend that
external users make an appointment
16
copyFreacutedeacuteric MaligneICT
LCC Services
17
Thermal Analyses LCC
How to request an analysis
bull For any analysis request
DTATGA or DSC analyses each sample must be suppliedwith an analysis request form duly filled out To requestthese forms please contact the staff by e-mail
In the very first request please contact the staff fordetails about the process the sample amount requiredthe packaging of samples etc
In all other cases the analyses requests and the samplescan be deposited in the Thermal Analyses Departmentrsquosletter-box (within the LCC entrance hall)
bull Air-sensitive samples
Make an appointment with the staff
bull Results
Analyses results are emailed as a text file paper copy isavailable upon request
On completion of analyses remaining of samples must bepick up at LCC
Analytical Equipments
DTATGA for measuring the mass variation as a
function of temperature
DSC for detecting the phase changes without mass loss
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 1 0Email j-fmeunierlcc-toulousefr
Some advice
Where to find usLCC - Door CS12 basement level
205 route de Narbonne
When Opening hours 9h to 11h30 - 14h to 17hfrom Monday to Friday except on wednesday
18
Library Resource Center LCC
How to make a request
bull For any information request
- LCC research teams fill out the request form available onthe LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs contact the staff by e-mail
bull For bibliographical searches and access
Digital databases
- LCC research teams bibliographical searches databases areavailable on the LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs make an appointment with the staff
Paper print collections
Paperprint collections also are available and can be read in thelibrary premises
LCCrsquos Library access is free for LCC teams and subject to anappointment for outside labs
LCC teams Access to the LCC intranet is provided
with taking office
For further information feel free to contact us
Who to contact
Marie-Heacutelegravene Gullimarie-helenegullilcc-toulousefr
0561333217
Gilles Roujasgillesroujaslcc-toulousefr
0561333140
Gaeumltan Havetgaetanhavetlcc-toulousefr
0561333140
Some advice
Where to find usLCC 205 route de Narbonne
When Opening hours
9 h to 11h30 - 13h to 17h From Monday to Friday
19
Feel free to contact us for anyquestion about analyses
options or for anydiscussion about the
best strategy to meetyour specific issues
Single ndashcrystal and powder X-Ray Diffraction - LCC
How to request an analysis
bull Prior to any analysis
Contact the staff in charge of X-Ray Diffraction measurementsfor your team or your lab
bull Single-crystal X-ray diffraction
First the staff will evaluate the quality of the sample If quality isacceptable for a X-ray diffraction measurement an appointmentwill be set up for analysis
Following information must be provided expected compound used solvents any specific information concerning the sample(air-sensitive thermal-sensitive light-sensitivehellip) analysis and required data (absolute configuration hydride locationhellip)
bull Powder X-ray diffraction
Appointments are proposed in accordance with the type of measurement (reflection capillary measurements at variable temperatures x-ray grazing incidence on thin films)
Following information must be provided sample characteristics analytical conditions (scanning range of 2theta temperaturehellip) required data (phase identification crystallites sizehellip)
Useful tips Until getting staff opinion about the quality of yoursample particularly for a single-crystal handle it as little as possible
Who to contact Laure Vendier (Mgr)
Carine DuhayonSonia Mallet-Ladeira
Tel 05 61 33 31 18Email laurevendierlcc-toulousefr
carineduhayonlcc-toulousefrladeiraictchimieups-tlsefr
Some advice
Where to find us
LCC 205 route de NarbonneX-Ray Diffraction office ground floor door B017 X-Ray Diffraction Lab basement level door GS66
When
9h to 11h30 - 14h to 17hFrom Monday to Friday except on Wednesday afternoon
20
Electrochemistry - LCC
How to request an analysis
bull For any analysis request
Analyses are carried out by appointment onlyscheduled with the staff when requesting theanalysis
On the appointed date Bring the sample and the solvent Your presence is required during the analyses
bull Sample preparation
The sample(s) must be as pure as possible correspondingto a concentration of 10-3 molL-1 in 10 mL
For each sample bring 30 mL of purified solvent
bull Results
On completion of the analyses the mostrepresentative curves are provided in paper copy
Upon request the electronic files can be emailed
Who to contactAlix Sournia-Saquet (Mgr)
Alain MoreauTel 05 61 33 31 75
Email alixsaquetlcc-toulousefralainmoreaulcc-toulousefr
Some advice
Before any analysis feel free to contact us for any
discussion or question about feasibility and conditions of
analyses
The staff can help you
- to choose the best-suited technique to your needs
- for interpretation of your data
Where to find us LCC- door B015ndash ground floor-building B205 route de Narbonne
When 9h to 11h30 -14h to 17h
From Monday to Friday
21
Magnetic Measurement and Moumlssbauer spectroscopy - LCC
How to request an analysis
bull For any analysis request
For magnetic measurements SQUID andMoumlssbauer spectroscopy please contact Jean-Franccedilois Meunier by e-mail or phone
An appointment will be set up in order to studyyour analyses requests and to define theexperimental conditions
An analysis request form will be provided by thestaff
bull Results and samples
Results are emailed as text and excel files
On completion of the analyses samples must beretrieved at LCC
Further information on equipments
lcc-toulousefrServices Spectroscopie Moumlssbauer
Lcc-toulousefr
servicesMesures
Magneacutetiques
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 10Email Jf-meunierlcc-toulousefr
Where to find usLCC door CS012
205 route de Narbonne
When 9h to 12h - 14h to 17h30
From Monday to Friday
Some advice
22
Elemental Analysis C-H-NS - LCC
How to request an analysis
For any analysis request
Each sample must be supplied with an analysis request formavailable on LCC website
wwwlcc-toulousefr gt services gt services techniques ampscientifiques gt analyses chimiques gt Formulaire
Fill in electronically and send by mail (see framed who tocontact)
Samples
- Internal in my box DEPOT CHN in the mail locker analyseselementaires
- External ship by courrier to LCC service CHN or ask anappointment
Results
Results are sent by mail Samples are not returned
Analyses
Analyses are carried out every week
10 mg of compound areneeded for 2 essays andpackaged in a vial
Sensitive samples mustbe isolated in sealedampoule
For special analysisrequests please contactservice
Sulphur is analyzed oncea year if enoughdemand
Who to contact Isabelle BorgetTel 05 61 33 32 14
mail isabelleborgetlcc-toulousefr
Where to find service LCC door B038
205 route de Narbonne
When 9h to 11h30 - 14h to 16h30
From monday to friday
on appointment
Some advice
23
Nuclear Magnetic Resonance - LCC
How to request an analysis
bull For any analysis request (except self-service equipments)
For NMR equipments (400-solid and 600 MHz) analysisand appointment requests must be emailed to Y Coppelor C Bijani
The analysis request form can be loaded from the NMRfacility webpage on the LCC website (httplcc-toulousefr)
bull Self-service equipments
All the users have to follow a training conducted by NMRfacilityrsquos staff before any use of self-service spectrometers
- for LCC teams the training and NMR user accountrequests are provided with taking office
- for outside labs please contact the LCC personneldepartment
The requests when validated must be returned directlyto A Bonnet or D Paryl in order to plan the training
The users undertake to carefully respect the operatinginstructions and the LCC memos
All the data are automatically
- made available in the LCC teamsrsquo laquo Nuage raquo file
- emailed to the user from outside labs
Feel free to contact us for any question
about analysis capabilities or for
any discussion about the best strategy to
meet your specific issues
Who to contact
Yannick Coppel (Mgr)Christian BijaniTel 05 61 17 54 27
Antoine BonnetDavid Paryl
Tel 05 61 17 54 30Email yannickcoppellcc-
toulousefrchristianbijanilcc-toulousefrantoinebonnetlcc-toulousefr
davidparyllcc-toulousefr
Some advice
Where to find us
LCC RMN Building 205 route de Narbonne Toulouse
Door 030 (Y Coppel et C Bijani)
Door 033 (F Lacassin et D Paryl)
When8h30 to 11h30 -14h to 17h
From Monday to Friday
24
Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) - LCC
How to request an analysis
bull For any analysis request
Each sample must be supplied with an analysisrequest form To request this form please contact the staff
Sample amount depends on the concentration of chemical elements to be measured in the sampleanalyzed
In the very first request please contact the staff
bull Results
Results are delivered in the letter-box of the LCC team or for outside labs made available in the ICP departmentrsquos letter-box (within the LCC entrance hall)
bull Analyses schedule
Analyses are carried out every 2 weeks
In general 10 mg per assay isneeded (provided that the
concentration is above 5 ww)
Chemical elements currentlyanalyzed (but not limited) Ag Al Au B Ba Be Bi Ca Cd Co Cr Cu Fe Ir K Li Mg Mn Na
Ni P Pb Pd Pt Ru Rh Sr Zn
Who to contact
Alain Moreau Tel 0561175850
E-mail alainmoreaulcc-toulousefr
Where to find usIPBS Bacirct A3
205 route de Narbonne
When 8h to 11h30 - 14h to 16h30From Monday to Friday (odd
week)
Some advice
25
Summary
1 - Characterisation amp purification 4bull X-Ray Diffraction 5bull Chromatography 6bull Nuclear Magnetic Resonance 7bull Mass spectrometry 8bull Infrared spectroscopy 9
2- Technopolym 10bull Technopolym Platform 11
3- Cross-Platform Services 12bull Documentation 13bull Electronics 14bull Information technology 15bull Scientific glassware 16
4- LCC Services 17bull Thermal analyses 18bull Library resource center 19bull Single-crystal and powder X-Ray Diffraction 20bull Electrochemistry 21bull Magnetic measurement and Moumlssbauer spectroscopy 22bull Elementar analyses CHNS 23bull Nuclear Magnetic Resonance 24bull Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) 25
3
Characterisation amp purification
4
Single Crystal X-Ray Diffraction
How to request an analysis
bull Beforehand
As soon as the crystals are obtained contact the staff of theservice so that they can evaluate the quality of the sample
If hte sample quality is judged to be sufficient to measure theX-ray diffraction an analysis request form should becomleted and submitted with the sample
bull For all analysis requests
Every sample must be accompanied by a completed analysisrequest form You will find this form on the ICT website
ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsdiffraction-des-rayons-x
Take care to specify the properties of the sample (sensitivityto air tempeacuterature lighthellip) the reagents used and theexpected crystal structure
Also specify the information that you hope to obtain from theanalysis (eg absolute configuration hellip)
While yoursquore waiting for the evaluation of the
crystal quality manipulate the
sample as little as possible and keep it
at the crystallizationtemperature until the
analysis
Who to contactNathalie Saffon (Mgr)Sonia Mallet-Ladeira
Tel 05 61 55 83 48 or 8173 Email rxictchimieups-tlsefr
Where can you find us Door 2053 2nd floor
Laboratory - Door 055 basement building 2R1
Universiteacute Paul Sabatier
When Monday Tuesday Thursday and
Friday
Some advice
5
How to request an analysis or a purification
bull For any request for analysis or purification (reverse or normal phaseionic or supercritical chromatography)
All samples must be accompanied by a fully completed form preferablydouble-sided which will be retained by the service
You will find this form on the ICT website
ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upshplc
Any sample not accompanied by this form will not be treated
bull Samples preparation
For your analysis you can prepare yourself your samples in 02 microm self-filtering vials (available on the platform) with a concentration of 1 mgmL
For your purifications you can bring the raw product
All services are provided after a validated appointment given by theplatform staff when depositing samples
bull Recovery of your results or purified samples
A generic analysis report is sent by email in PDF format
The platform staff listen to your needs for a more detailed report
Come and collect your purified products upon receipt of the results
Please note that saving the results is not guaranteed in the long term Takecare we do not guarantee the long-term storage of your results
bull Self-service devices
Any equipment can be made available after validation of the training onthe device concerned by the platform manager
To do this make an appointment one month before the desired use inorder to obtain validation of your training on time This validation is validfor a fixed period
Online booking httpglpi-ictgrr-hplc to use equipments
For the preparation of your samples
solid phase extraction cartridges
and self-filtering vials are available
Contact us in case of difficulties in filling
in the form or in defining the best
separation method suitable for your
product
Who to contactIsabelle FabingOffice 05 61 55 81 98
Lab 05 61 55 62 95email hplcictchimieups-tlsefr
Where can you find us Door 30793083 3rd floor
building 2R1 Universiteacute Paul Sabatier
When Monday to Friday
Reception
9h30-11h30 am
Some advice
6
Chromatography
copyFreacutedeacuteric MaligneICT
How to request an analysis
bull For all analysis requests on the 400 and 500 MHz NMR spectrometerssituated in the High Technology Module (MHT)Each sample must be accompanied by a fully completed laquo AnalysisRequest raquo form You can find this form on the ICT websiteictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsrmn oron the website of the NMR service (httprmn-webups-tlsefr)It is essential to make an appointment by email telephone or in personat the NMR service
bull For all analysis requests on the 300 MHz open access NMR spectrometerslocated in Building 2R1You must sign up to the NMR training before using the 300 MHz spectrometers (inscription form on the website of the NMR service httprmn-webups-tlsefr)
bull Follow the instructionsI ndash NMR Tubes
NMR tubes must meet a minimum standard of qualityBroken or damaged tubes and Economy tubes are forbidden from the service as they are too fragile
II ndash Cleaning tubes After the analysis the tubes must be washed as quickly as possible using the same solvent that was used to dissolve the analyte After several rinses the tube should be dried at room temperature or in an oven at less than 60degC
III ndash Filling the tubesFor an optimal measurement your tube should contain 600 microL of
solvent bull Results spectra can be recovered by
- downloading from the NMR server- USB stick- by email (only for 1 D analyses)
Once the analysis has been completed you must come to pick up yoursamples from the NMR service
The sensitivity of an NMR experiment depends on the
nucleus studied and the concentration of your product
If necessary during samplepreparation filter your solutions
in order to remove any suspendedsolids
The choice of solvent dependsprimarily on the solubility of your
product at room temperature
If there are several possibilities choose a solvent whose peaks do
not interfere with those of yourproduct
For more information please feelfree to contact the staff of the NMR
service
Who to contact
Marc Vedrenne (Msg)Pierre Lavedan
Steacutephane MassouCaroline ToppanClaude Andreu
Tel 05-61-55 ext 84-78 68-78Email rmnictchimieups-tlsefr
Where to find us Door 45 Ground floor High
Technology Module Universiteacute Paul Sabatier
When Monday to Friday
09h00-12h00 and 14h00-16h30
Some advice
NMR Service
copyFreacutedeacuteric MaligneICT
Mass spectrometry
How to request an analysis
bull For all analysis requests
Each sample must be accompanied by a fully completedanalysis request form You can find this form on the ICT website ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsspectrometrie-de-masse
You can also fill in all the administrative details one timeonly and save them for your future requests and you canarchive your forms
Bring the forms (preferably double-sided) and sample duringopening hours We will check with you the feasibility of theproposed analyses
bull For air-sensitive samples
Make an appointment
bull For LCMS and GCMS analyses
Make an appointment
bull How to collect your results
The results will be sent to you in pdf format Upon receivingour mail you can come and pick up your samples and formsduring opening hours
We will assess the feasibility of the
analysis with you
If you donrsquot know which method of ionization is
better suited for your molecules then leave it
blank and we will choose together
Who to contactCatherine Claparols ( Mgr)
Valeacuterie BourdonEric Leroy
Nathalie Martins-FromentTel 33 5 61 55 64 69Fax 33 5 61 55 81 16
Email spectromasseictups-tlsefr
Where to find us
Door 157 groundfloor building 2R1 Universiteacute Paul Sabatier
When
Monday-Friday 10h30-12h and 13h30-15h00
Some advice
8
copyFreacutedeacuteric MaligneICT
INFRARED Spectroscopy
How to request an analysis
bull For each analysis request
Each sample must be accompanied by a fully completedanalysis request form You can find this form on the ICT website ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsspectroscopies-infrarouge and on the door of the service
Required sample quantity 05 to 2 mg for powders 1drop for liquids 1ml for solutions (in this case you will alsoneed to supply 10-20 ml of pure solvent)
bull For infrared microscopy kinetics
Please make an appointment
bull For other analyses transmission ATR DRIFT far-IR NIR
Leave your sample at the service If unattended a box isavailable on the door to drop off your samples
bull Open access equipment for ATR analyses only
It can be used after completion of a 1h training course Makean appointment
All kinds of samples can beanalyzed solids liquids solutions blocks grains of
wheathellipyou just needto choose the right
method depending on your sample and your
study
Come and discuss with us
Extensive infrared and Raman tables and
spectral data bases are available at the
service60 000 data base spectra
are available
Who to contactCorinne Routaboul
Tel 05 61 55 64 00Email routabouictchimieups-tlsefr
Where to find us Door 1025 1st floor building 2R1
Universiteacute Paul Sabatier
When Monday-Friday 9h00-17h00
If unattended leave the sample in the deposit box on the door If youhave more than 10 samples or if you need particular techniques please make an appointment
Some advice
9
copyFreacutedeacuteric MaligneICT
TECHNOPOLYM
10
Technopolym
How to request an analysis
bull Request an analysis via the central Technopolym emailtechnopolymictchimieups-tlsefr
Following this email we will inform you about the proposedtechniques of analyse costs time of delivery requiredquantity of sample conditioning sample deposit Dependingon your expected results an appointment to discuss yourproblem may be proposed before scheduling an analysis
bull For all analysis requestsEach sample must be accompanied by a fully completed
analysis request form You can find this form on the ICT website
ictcnrsfrplateforme-de-licttechnopolym or on the Technopolym website
httptechnopolymups-tlsefr
bull For more information
Visit our website to know about our skills equipment references
TechnopolymIs a virtual technological
platform dedicated to the characterization of polymeric
materials
We propose a range of analytical techniques
molecularcharacterization phase
transitions thermal stability behavior in
solution mechanicalproperties surface characterizationhellip
Come and talk to us
Who to contactPascale Saint-Aguet
Tel 05 61 55 68 08Tel (LCC) 05 61 33 31 34
Email technopolymictchimieups-tlsefr
Some advice
Where to find us
Door 30233rd floor building 2R1 Universiteacute Paul Sabatier
Door G064 ndashLCC 205 rte de Narbonne -
When
Monday-Friday 9h-12h and
14h-17h
11
Cross-Platform Services
12
Documentation
How to make a request
bull For all document requests
You can request your document by email telephone or inperson Donrsquot forget to indicate your full name and laboratorywith the references on your request
bull Consultation and loans
The catalogue of the chemistry library is available on theintranet
ictcnrsfrdocchimie
Borrowing is possible during office hours ndash outside thesehours please make an appointment
bull For bibliographic searches and training
Make an appointment
bull Open access
You can come and work at the library ndash computers and wifi are available Visit our website
ictcnrsfrplateforme-de-lictservices-transversesaccueil-de-la-documentation
Ask the documentation service for your intranet
password from
Feel free to call the service for any problems
relating to the use of bibliographic databases
Who to contactDanielle Brunet
Tel 05 61 55 85 69Email brunetictchimieups-tlsefr
Some advice
Where to find us
Door 0145 ground floor building 2R1
Universiteacute Paul Sabatier
When
Mon-Fri 9h-12h and 14h-17h If unattended make an
appointment
13
Electronics
How to make a request
Who to contactJean-Michel Martin
Tel 05 61 55 86 93Email scicassistanceictchimieups-tlsefr
Email martinjmictchimieups-tlsefr
Feel free to ask the service for
- Modification of existingelectronic devices and
proposals for improvement
- Troubleshooting and repair of electronic
devices
- Advice on purchase of new material
bull For all installation andor maintenance of equipment with astrong electronic component
Send an email phone or contact the service in person duringoffice hours
bull For all service requests
Send an email toscicassistanceictchimieups-tlsefrstating your name office number and a brief description of the problem
bull Loan of equipment
To address the needs of users specific equipment is availablein the electronics workshop (Oscilloscope component testerssoldering ironhellip) aswell as various tools
It is possible to borrow this equipment
Where to find usDoor 1015 1st floor building 2R1 Universiteacute Paul Sabatier
When Monday-Friday office hours
If unattended make an appointment
Some advice
14
Information Technology
How to make a request
bull For all requests for connection to the network andcreation of email accounts
First see the secretary of your laboratory
bull For all service requests
Write toscicassistanceictchimieups-tlsefr
stating your name office number and a brief description of the problem
The IT service manages developsand maintains the
network and associated services
Please contact us for more information on
the services provided (automatic
backup of data access to Cambridge CCDC data sharing
etc)
Who to contactPascal Puech
Edouard IvanovtchikTel 05 61 55 68 73
Email scicassistanceictchimieups-tlsefr
Some advice
Where to find usDoor 168 ground floor building 2R1
Universiteacute Paul Sabatier
WhenMonday-Friday office hours
If unattended make an appointment
15
Scientific Glassware
How to make a request
bull For all service requests
All glassware to repair or construct must be accompanied bya fully completed form You can find this form on the ICTwebsite ictcnrsfrVerrerie-scientifique
For obvious reasons of safety and hygiene glassware must beclean free of silicon grease and in a container identified withthe name of the research group
bull Do I need to go in person
In person contact is preferred if you are new to glasswork andif your request is complex
Photos et technical drawings sent by email are onlycomplementary information as in isolation they can lead tomisunderstandings and errors
For all glass repairs construction of new
equipment or prototyping
feel free to consult the glassware service
We can provide technicaladvice as well as contacts
in specialized domains
Who to contactSteacutephane Foulon
Tel 05 61 55 61 16Email foulonictchimieups-
tlsefr
Some advice
Where to find us
Door 0194 Ground Floor Building 2R1Universiteacute Paul
Sabatier
When
Monday-Friday during office hours We recommend that
external users make an appointment
16
copyFreacutedeacuteric MaligneICT
LCC Services
17
Thermal Analyses LCC
How to request an analysis
bull For any analysis request
DTATGA or DSC analyses each sample must be suppliedwith an analysis request form duly filled out To requestthese forms please contact the staff by e-mail
In the very first request please contact the staff fordetails about the process the sample amount requiredthe packaging of samples etc
In all other cases the analyses requests and the samplescan be deposited in the Thermal Analyses Departmentrsquosletter-box (within the LCC entrance hall)
bull Air-sensitive samples
Make an appointment with the staff
bull Results
Analyses results are emailed as a text file paper copy isavailable upon request
On completion of analyses remaining of samples must bepick up at LCC
Analytical Equipments
DTATGA for measuring the mass variation as a
function of temperature
DSC for detecting the phase changes without mass loss
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 1 0Email j-fmeunierlcc-toulousefr
Some advice
Where to find usLCC - Door CS12 basement level
205 route de Narbonne
When Opening hours 9h to 11h30 - 14h to 17hfrom Monday to Friday except on wednesday
18
Library Resource Center LCC
How to make a request
bull For any information request
- LCC research teams fill out the request form available onthe LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs contact the staff by e-mail
bull For bibliographical searches and access
Digital databases
- LCC research teams bibliographical searches databases areavailable on the LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs make an appointment with the staff
Paper print collections
Paperprint collections also are available and can be read in thelibrary premises
LCCrsquos Library access is free for LCC teams and subject to anappointment for outside labs
LCC teams Access to the LCC intranet is provided
with taking office
For further information feel free to contact us
Who to contact
Marie-Heacutelegravene Gullimarie-helenegullilcc-toulousefr
0561333217
Gilles Roujasgillesroujaslcc-toulousefr
0561333140
Gaeumltan Havetgaetanhavetlcc-toulousefr
0561333140
Some advice
Where to find usLCC 205 route de Narbonne
When Opening hours
9 h to 11h30 - 13h to 17h From Monday to Friday
19
Feel free to contact us for anyquestion about analyses
options or for anydiscussion about the
best strategy to meetyour specific issues
Single ndashcrystal and powder X-Ray Diffraction - LCC
How to request an analysis
bull Prior to any analysis
Contact the staff in charge of X-Ray Diffraction measurementsfor your team or your lab
bull Single-crystal X-ray diffraction
First the staff will evaluate the quality of the sample If quality isacceptable for a X-ray diffraction measurement an appointmentwill be set up for analysis
Following information must be provided expected compound used solvents any specific information concerning the sample(air-sensitive thermal-sensitive light-sensitivehellip) analysis and required data (absolute configuration hydride locationhellip)
bull Powder X-ray diffraction
Appointments are proposed in accordance with the type of measurement (reflection capillary measurements at variable temperatures x-ray grazing incidence on thin films)
Following information must be provided sample characteristics analytical conditions (scanning range of 2theta temperaturehellip) required data (phase identification crystallites sizehellip)
Useful tips Until getting staff opinion about the quality of yoursample particularly for a single-crystal handle it as little as possible
Who to contact Laure Vendier (Mgr)
Carine DuhayonSonia Mallet-Ladeira
Tel 05 61 33 31 18Email laurevendierlcc-toulousefr
carineduhayonlcc-toulousefrladeiraictchimieups-tlsefr
Some advice
Where to find us
LCC 205 route de NarbonneX-Ray Diffraction office ground floor door B017 X-Ray Diffraction Lab basement level door GS66
When
9h to 11h30 - 14h to 17hFrom Monday to Friday except on Wednesday afternoon
20
Electrochemistry - LCC
How to request an analysis
bull For any analysis request
Analyses are carried out by appointment onlyscheduled with the staff when requesting theanalysis
On the appointed date Bring the sample and the solvent Your presence is required during the analyses
bull Sample preparation
The sample(s) must be as pure as possible correspondingto a concentration of 10-3 molL-1 in 10 mL
For each sample bring 30 mL of purified solvent
bull Results
On completion of the analyses the mostrepresentative curves are provided in paper copy
Upon request the electronic files can be emailed
Who to contactAlix Sournia-Saquet (Mgr)
Alain MoreauTel 05 61 33 31 75
Email alixsaquetlcc-toulousefralainmoreaulcc-toulousefr
Some advice
Before any analysis feel free to contact us for any
discussion or question about feasibility and conditions of
analyses
The staff can help you
- to choose the best-suited technique to your needs
- for interpretation of your data
Where to find us LCC- door B015ndash ground floor-building B205 route de Narbonne
When 9h to 11h30 -14h to 17h
From Monday to Friday
21
Magnetic Measurement and Moumlssbauer spectroscopy - LCC
How to request an analysis
bull For any analysis request
For magnetic measurements SQUID andMoumlssbauer spectroscopy please contact Jean-Franccedilois Meunier by e-mail or phone
An appointment will be set up in order to studyyour analyses requests and to define theexperimental conditions
An analysis request form will be provided by thestaff
bull Results and samples
Results are emailed as text and excel files
On completion of the analyses samples must beretrieved at LCC
Further information on equipments
lcc-toulousefrServices Spectroscopie Moumlssbauer
Lcc-toulousefr
servicesMesures
Magneacutetiques
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 10Email Jf-meunierlcc-toulousefr
Where to find usLCC door CS012
205 route de Narbonne
When 9h to 12h - 14h to 17h30
From Monday to Friday
Some advice
22
Elemental Analysis C-H-NS - LCC
How to request an analysis
For any analysis request
Each sample must be supplied with an analysis request formavailable on LCC website
wwwlcc-toulousefr gt services gt services techniques ampscientifiques gt analyses chimiques gt Formulaire
Fill in electronically and send by mail (see framed who tocontact)
Samples
- Internal in my box DEPOT CHN in the mail locker analyseselementaires
- External ship by courrier to LCC service CHN or ask anappointment
Results
Results are sent by mail Samples are not returned
Analyses
Analyses are carried out every week
10 mg of compound areneeded for 2 essays andpackaged in a vial
Sensitive samples mustbe isolated in sealedampoule
For special analysisrequests please contactservice
Sulphur is analyzed oncea year if enoughdemand
Who to contact Isabelle BorgetTel 05 61 33 32 14
mail isabelleborgetlcc-toulousefr
Where to find service LCC door B038
205 route de Narbonne
When 9h to 11h30 - 14h to 16h30
From monday to friday
on appointment
Some advice
23
Nuclear Magnetic Resonance - LCC
How to request an analysis
bull For any analysis request (except self-service equipments)
For NMR equipments (400-solid and 600 MHz) analysisand appointment requests must be emailed to Y Coppelor C Bijani
The analysis request form can be loaded from the NMRfacility webpage on the LCC website (httplcc-toulousefr)
bull Self-service equipments
All the users have to follow a training conducted by NMRfacilityrsquos staff before any use of self-service spectrometers
- for LCC teams the training and NMR user accountrequests are provided with taking office
- for outside labs please contact the LCC personneldepartment
The requests when validated must be returned directlyto A Bonnet or D Paryl in order to plan the training
The users undertake to carefully respect the operatinginstructions and the LCC memos
All the data are automatically
- made available in the LCC teamsrsquo laquo Nuage raquo file
- emailed to the user from outside labs
Feel free to contact us for any question
about analysis capabilities or for
any discussion about the best strategy to
meet your specific issues
Who to contact
Yannick Coppel (Mgr)Christian BijaniTel 05 61 17 54 27
Antoine BonnetDavid Paryl
Tel 05 61 17 54 30Email yannickcoppellcc-
toulousefrchristianbijanilcc-toulousefrantoinebonnetlcc-toulousefr
davidparyllcc-toulousefr
Some advice
Where to find us
LCC RMN Building 205 route de Narbonne Toulouse
Door 030 (Y Coppel et C Bijani)
Door 033 (F Lacassin et D Paryl)
When8h30 to 11h30 -14h to 17h
From Monday to Friday
24
Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) - LCC
How to request an analysis
bull For any analysis request
Each sample must be supplied with an analysisrequest form To request this form please contact the staff
Sample amount depends on the concentration of chemical elements to be measured in the sampleanalyzed
In the very first request please contact the staff
bull Results
Results are delivered in the letter-box of the LCC team or for outside labs made available in the ICP departmentrsquos letter-box (within the LCC entrance hall)
bull Analyses schedule
Analyses are carried out every 2 weeks
In general 10 mg per assay isneeded (provided that the
concentration is above 5 ww)
Chemical elements currentlyanalyzed (but not limited) Ag Al Au B Ba Be Bi Ca Cd Co Cr Cu Fe Ir K Li Mg Mn Na
Ni P Pb Pd Pt Ru Rh Sr Zn
Who to contact
Alain Moreau Tel 0561175850
E-mail alainmoreaulcc-toulousefr
Where to find usIPBS Bacirct A3
205 route de Narbonne
When 8h to 11h30 - 14h to 16h30From Monday to Friday (odd
week)
Some advice
25
Characterisation amp purification
4
Single Crystal X-Ray Diffraction
How to request an analysis
bull Beforehand
As soon as the crystals are obtained contact the staff of theservice so that they can evaluate the quality of the sample
If hte sample quality is judged to be sufficient to measure theX-ray diffraction an analysis request form should becomleted and submitted with the sample
bull For all analysis requests
Every sample must be accompanied by a completed analysisrequest form You will find this form on the ICT website
ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsdiffraction-des-rayons-x
Take care to specify the properties of the sample (sensitivityto air tempeacuterature lighthellip) the reagents used and theexpected crystal structure
Also specify the information that you hope to obtain from theanalysis (eg absolute configuration hellip)
While yoursquore waiting for the evaluation of the
crystal quality manipulate the
sample as little as possible and keep it
at the crystallizationtemperature until the
analysis
Who to contactNathalie Saffon (Mgr)Sonia Mallet-Ladeira
Tel 05 61 55 83 48 or 8173 Email rxictchimieups-tlsefr
Where can you find us Door 2053 2nd floor
Laboratory - Door 055 basement building 2R1
Universiteacute Paul Sabatier
When Monday Tuesday Thursday and
Friday
Some advice
5
How to request an analysis or a purification
bull For any request for analysis or purification (reverse or normal phaseionic or supercritical chromatography)
All samples must be accompanied by a fully completed form preferablydouble-sided which will be retained by the service
You will find this form on the ICT website
ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upshplc
Any sample not accompanied by this form will not be treated
bull Samples preparation
For your analysis you can prepare yourself your samples in 02 microm self-filtering vials (available on the platform) with a concentration of 1 mgmL
For your purifications you can bring the raw product
All services are provided after a validated appointment given by theplatform staff when depositing samples
bull Recovery of your results or purified samples
A generic analysis report is sent by email in PDF format
The platform staff listen to your needs for a more detailed report
Come and collect your purified products upon receipt of the results
Please note that saving the results is not guaranteed in the long term Takecare we do not guarantee the long-term storage of your results
bull Self-service devices
Any equipment can be made available after validation of the training onthe device concerned by the platform manager
To do this make an appointment one month before the desired use inorder to obtain validation of your training on time This validation is validfor a fixed period
Online booking httpglpi-ictgrr-hplc to use equipments
For the preparation of your samples
solid phase extraction cartridges
and self-filtering vials are available
Contact us in case of difficulties in filling
in the form or in defining the best
separation method suitable for your
product
Who to contactIsabelle FabingOffice 05 61 55 81 98
Lab 05 61 55 62 95email hplcictchimieups-tlsefr
Where can you find us Door 30793083 3rd floor
building 2R1 Universiteacute Paul Sabatier
When Monday to Friday
Reception
9h30-11h30 am
Some advice
6
Chromatography
copyFreacutedeacuteric MaligneICT
How to request an analysis
bull For all analysis requests on the 400 and 500 MHz NMR spectrometerssituated in the High Technology Module (MHT)Each sample must be accompanied by a fully completed laquo AnalysisRequest raquo form You can find this form on the ICT websiteictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsrmn oron the website of the NMR service (httprmn-webups-tlsefr)It is essential to make an appointment by email telephone or in personat the NMR service
bull For all analysis requests on the 300 MHz open access NMR spectrometerslocated in Building 2R1You must sign up to the NMR training before using the 300 MHz spectrometers (inscription form on the website of the NMR service httprmn-webups-tlsefr)
bull Follow the instructionsI ndash NMR Tubes
NMR tubes must meet a minimum standard of qualityBroken or damaged tubes and Economy tubes are forbidden from the service as they are too fragile
II ndash Cleaning tubes After the analysis the tubes must be washed as quickly as possible using the same solvent that was used to dissolve the analyte After several rinses the tube should be dried at room temperature or in an oven at less than 60degC
III ndash Filling the tubesFor an optimal measurement your tube should contain 600 microL of
solvent bull Results spectra can be recovered by
- downloading from the NMR server- USB stick- by email (only for 1 D analyses)
Once the analysis has been completed you must come to pick up yoursamples from the NMR service
The sensitivity of an NMR experiment depends on the
nucleus studied and the concentration of your product
If necessary during samplepreparation filter your solutions
in order to remove any suspendedsolids
The choice of solvent dependsprimarily on the solubility of your
product at room temperature
If there are several possibilities choose a solvent whose peaks do
not interfere with those of yourproduct
For more information please feelfree to contact the staff of the NMR
service
Who to contact
Marc Vedrenne (Msg)Pierre Lavedan
Steacutephane MassouCaroline ToppanClaude Andreu
Tel 05-61-55 ext 84-78 68-78Email rmnictchimieups-tlsefr
Where to find us Door 45 Ground floor High
Technology Module Universiteacute Paul Sabatier
When Monday to Friday
09h00-12h00 and 14h00-16h30
Some advice
NMR Service
copyFreacutedeacuteric MaligneICT
Mass spectrometry
How to request an analysis
bull For all analysis requests
Each sample must be accompanied by a fully completedanalysis request form You can find this form on the ICT website ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsspectrometrie-de-masse
You can also fill in all the administrative details one timeonly and save them for your future requests and you canarchive your forms
Bring the forms (preferably double-sided) and sample duringopening hours We will check with you the feasibility of theproposed analyses
bull For air-sensitive samples
Make an appointment
bull For LCMS and GCMS analyses
Make an appointment
bull How to collect your results
The results will be sent to you in pdf format Upon receivingour mail you can come and pick up your samples and formsduring opening hours
We will assess the feasibility of the
analysis with you
If you donrsquot know which method of ionization is
better suited for your molecules then leave it
blank and we will choose together
Who to contactCatherine Claparols ( Mgr)
Valeacuterie BourdonEric Leroy
Nathalie Martins-FromentTel 33 5 61 55 64 69Fax 33 5 61 55 81 16
Email spectromasseictups-tlsefr
Where to find us
Door 157 groundfloor building 2R1 Universiteacute Paul Sabatier
When
Monday-Friday 10h30-12h and 13h30-15h00
Some advice
8
copyFreacutedeacuteric MaligneICT
INFRARED Spectroscopy
How to request an analysis
bull For each analysis request
Each sample must be accompanied by a fully completedanalysis request form You can find this form on the ICT website ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsspectroscopies-infrarouge and on the door of the service
Required sample quantity 05 to 2 mg for powders 1drop for liquids 1ml for solutions (in this case you will alsoneed to supply 10-20 ml of pure solvent)
bull For infrared microscopy kinetics
Please make an appointment
bull For other analyses transmission ATR DRIFT far-IR NIR
Leave your sample at the service If unattended a box isavailable on the door to drop off your samples
bull Open access equipment for ATR analyses only
It can be used after completion of a 1h training course Makean appointment
All kinds of samples can beanalyzed solids liquids solutions blocks grains of
wheathellipyou just needto choose the right
method depending on your sample and your
study
Come and discuss with us
Extensive infrared and Raman tables and
spectral data bases are available at the
service60 000 data base spectra
are available
Who to contactCorinne Routaboul
Tel 05 61 55 64 00Email routabouictchimieups-tlsefr
Where to find us Door 1025 1st floor building 2R1
Universiteacute Paul Sabatier
When Monday-Friday 9h00-17h00
If unattended leave the sample in the deposit box on the door If youhave more than 10 samples or if you need particular techniques please make an appointment
Some advice
9
copyFreacutedeacuteric MaligneICT
TECHNOPOLYM
10
Technopolym
How to request an analysis
bull Request an analysis via the central Technopolym emailtechnopolymictchimieups-tlsefr
Following this email we will inform you about the proposedtechniques of analyse costs time of delivery requiredquantity of sample conditioning sample deposit Dependingon your expected results an appointment to discuss yourproblem may be proposed before scheduling an analysis
bull For all analysis requestsEach sample must be accompanied by a fully completed
analysis request form You can find this form on the ICT website
ictcnrsfrplateforme-de-licttechnopolym or on the Technopolym website
httptechnopolymups-tlsefr
bull For more information
Visit our website to know about our skills equipment references
TechnopolymIs a virtual technological
platform dedicated to the characterization of polymeric
materials
We propose a range of analytical techniques
molecularcharacterization phase
transitions thermal stability behavior in
solution mechanicalproperties surface characterizationhellip
Come and talk to us
Who to contactPascale Saint-Aguet
Tel 05 61 55 68 08Tel (LCC) 05 61 33 31 34
Email technopolymictchimieups-tlsefr
Some advice
Where to find us
Door 30233rd floor building 2R1 Universiteacute Paul Sabatier
Door G064 ndashLCC 205 rte de Narbonne -
When
Monday-Friday 9h-12h and
14h-17h
11
Cross-Platform Services
12
Documentation
How to make a request
bull For all document requests
You can request your document by email telephone or inperson Donrsquot forget to indicate your full name and laboratorywith the references on your request
bull Consultation and loans
The catalogue of the chemistry library is available on theintranet
ictcnrsfrdocchimie
Borrowing is possible during office hours ndash outside thesehours please make an appointment
bull For bibliographic searches and training
Make an appointment
bull Open access
You can come and work at the library ndash computers and wifi are available Visit our website
ictcnrsfrplateforme-de-lictservices-transversesaccueil-de-la-documentation
Ask the documentation service for your intranet
password from
Feel free to call the service for any problems
relating to the use of bibliographic databases
Who to contactDanielle Brunet
Tel 05 61 55 85 69Email brunetictchimieups-tlsefr
Some advice
Where to find us
Door 0145 ground floor building 2R1
Universiteacute Paul Sabatier
When
Mon-Fri 9h-12h and 14h-17h If unattended make an
appointment
13
Electronics
How to make a request
Who to contactJean-Michel Martin
Tel 05 61 55 86 93Email scicassistanceictchimieups-tlsefr
Email martinjmictchimieups-tlsefr
Feel free to ask the service for
- Modification of existingelectronic devices and
proposals for improvement
- Troubleshooting and repair of electronic
devices
- Advice on purchase of new material
bull For all installation andor maintenance of equipment with astrong electronic component
Send an email phone or contact the service in person duringoffice hours
bull For all service requests
Send an email toscicassistanceictchimieups-tlsefrstating your name office number and a brief description of the problem
bull Loan of equipment
To address the needs of users specific equipment is availablein the electronics workshop (Oscilloscope component testerssoldering ironhellip) aswell as various tools
It is possible to borrow this equipment
Where to find usDoor 1015 1st floor building 2R1 Universiteacute Paul Sabatier
When Monday-Friday office hours
If unattended make an appointment
Some advice
14
Information Technology
How to make a request
bull For all requests for connection to the network andcreation of email accounts
First see the secretary of your laboratory
bull For all service requests
Write toscicassistanceictchimieups-tlsefr
stating your name office number and a brief description of the problem
The IT service manages developsand maintains the
network and associated services
Please contact us for more information on
the services provided (automatic
backup of data access to Cambridge CCDC data sharing
etc)
Who to contactPascal Puech
Edouard IvanovtchikTel 05 61 55 68 73
Email scicassistanceictchimieups-tlsefr
Some advice
Where to find usDoor 168 ground floor building 2R1
Universiteacute Paul Sabatier
WhenMonday-Friday office hours
If unattended make an appointment
15
Scientific Glassware
How to make a request
bull For all service requests
All glassware to repair or construct must be accompanied bya fully completed form You can find this form on the ICTwebsite ictcnrsfrVerrerie-scientifique
For obvious reasons of safety and hygiene glassware must beclean free of silicon grease and in a container identified withthe name of the research group
bull Do I need to go in person
In person contact is preferred if you are new to glasswork andif your request is complex
Photos et technical drawings sent by email are onlycomplementary information as in isolation they can lead tomisunderstandings and errors
For all glass repairs construction of new
equipment or prototyping
feel free to consult the glassware service
We can provide technicaladvice as well as contacts
in specialized domains
Who to contactSteacutephane Foulon
Tel 05 61 55 61 16Email foulonictchimieups-
tlsefr
Some advice
Where to find us
Door 0194 Ground Floor Building 2R1Universiteacute Paul
Sabatier
When
Monday-Friday during office hours We recommend that
external users make an appointment
16
copyFreacutedeacuteric MaligneICT
LCC Services
17
Thermal Analyses LCC
How to request an analysis
bull For any analysis request
DTATGA or DSC analyses each sample must be suppliedwith an analysis request form duly filled out To requestthese forms please contact the staff by e-mail
In the very first request please contact the staff fordetails about the process the sample amount requiredthe packaging of samples etc
In all other cases the analyses requests and the samplescan be deposited in the Thermal Analyses Departmentrsquosletter-box (within the LCC entrance hall)
bull Air-sensitive samples
Make an appointment with the staff
bull Results
Analyses results are emailed as a text file paper copy isavailable upon request
On completion of analyses remaining of samples must bepick up at LCC
Analytical Equipments
DTATGA for measuring the mass variation as a
function of temperature
DSC for detecting the phase changes without mass loss
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 1 0Email j-fmeunierlcc-toulousefr
Some advice
Where to find usLCC - Door CS12 basement level
205 route de Narbonne
When Opening hours 9h to 11h30 - 14h to 17hfrom Monday to Friday except on wednesday
18
Library Resource Center LCC
How to make a request
bull For any information request
- LCC research teams fill out the request form available onthe LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs contact the staff by e-mail
bull For bibliographical searches and access
Digital databases
- LCC research teams bibliographical searches databases areavailable on the LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs make an appointment with the staff
Paper print collections
Paperprint collections also are available and can be read in thelibrary premises
LCCrsquos Library access is free for LCC teams and subject to anappointment for outside labs
LCC teams Access to the LCC intranet is provided
with taking office
For further information feel free to contact us
Who to contact
Marie-Heacutelegravene Gullimarie-helenegullilcc-toulousefr
0561333217
Gilles Roujasgillesroujaslcc-toulousefr
0561333140
Gaeumltan Havetgaetanhavetlcc-toulousefr
0561333140
Some advice
Where to find usLCC 205 route de Narbonne
When Opening hours
9 h to 11h30 - 13h to 17h From Monday to Friday
19
Feel free to contact us for anyquestion about analyses
options or for anydiscussion about the
best strategy to meetyour specific issues
Single ndashcrystal and powder X-Ray Diffraction - LCC
How to request an analysis
bull Prior to any analysis
Contact the staff in charge of X-Ray Diffraction measurementsfor your team or your lab
bull Single-crystal X-ray diffraction
First the staff will evaluate the quality of the sample If quality isacceptable for a X-ray diffraction measurement an appointmentwill be set up for analysis
Following information must be provided expected compound used solvents any specific information concerning the sample(air-sensitive thermal-sensitive light-sensitivehellip) analysis and required data (absolute configuration hydride locationhellip)
bull Powder X-ray diffraction
Appointments are proposed in accordance with the type of measurement (reflection capillary measurements at variable temperatures x-ray grazing incidence on thin films)
Following information must be provided sample characteristics analytical conditions (scanning range of 2theta temperaturehellip) required data (phase identification crystallites sizehellip)
Useful tips Until getting staff opinion about the quality of yoursample particularly for a single-crystal handle it as little as possible
Who to contact Laure Vendier (Mgr)
Carine DuhayonSonia Mallet-Ladeira
Tel 05 61 33 31 18Email laurevendierlcc-toulousefr
carineduhayonlcc-toulousefrladeiraictchimieups-tlsefr
Some advice
Where to find us
LCC 205 route de NarbonneX-Ray Diffraction office ground floor door B017 X-Ray Diffraction Lab basement level door GS66
When
9h to 11h30 - 14h to 17hFrom Monday to Friday except on Wednesday afternoon
20
Electrochemistry - LCC
How to request an analysis
bull For any analysis request
Analyses are carried out by appointment onlyscheduled with the staff when requesting theanalysis
On the appointed date Bring the sample and the solvent Your presence is required during the analyses
bull Sample preparation
The sample(s) must be as pure as possible correspondingto a concentration of 10-3 molL-1 in 10 mL
For each sample bring 30 mL of purified solvent
bull Results
On completion of the analyses the mostrepresentative curves are provided in paper copy
Upon request the electronic files can be emailed
Who to contactAlix Sournia-Saquet (Mgr)
Alain MoreauTel 05 61 33 31 75
Email alixsaquetlcc-toulousefralainmoreaulcc-toulousefr
Some advice
Before any analysis feel free to contact us for any
discussion or question about feasibility and conditions of
analyses
The staff can help you
- to choose the best-suited technique to your needs
- for interpretation of your data
Where to find us LCC- door B015ndash ground floor-building B205 route de Narbonne
When 9h to 11h30 -14h to 17h
From Monday to Friday
21
Magnetic Measurement and Moumlssbauer spectroscopy - LCC
How to request an analysis
bull For any analysis request
For magnetic measurements SQUID andMoumlssbauer spectroscopy please contact Jean-Franccedilois Meunier by e-mail or phone
An appointment will be set up in order to studyyour analyses requests and to define theexperimental conditions
An analysis request form will be provided by thestaff
bull Results and samples
Results are emailed as text and excel files
On completion of the analyses samples must beretrieved at LCC
Further information on equipments
lcc-toulousefrServices Spectroscopie Moumlssbauer
Lcc-toulousefr
servicesMesures
Magneacutetiques
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 10Email Jf-meunierlcc-toulousefr
Where to find usLCC door CS012
205 route de Narbonne
When 9h to 12h - 14h to 17h30
From Monday to Friday
Some advice
22
Elemental Analysis C-H-NS - LCC
How to request an analysis
For any analysis request
Each sample must be supplied with an analysis request formavailable on LCC website
wwwlcc-toulousefr gt services gt services techniques ampscientifiques gt analyses chimiques gt Formulaire
Fill in electronically and send by mail (see framed who tocontact)
Samples
- Internal in my box DEPOT CHN in the mail locker analyseselementaires
- External ship by courrier to LCC service CHN or ask anappointment
Results
Results are sent by mail Samples are not returned
Analyses
Analyses are carried out every week
10 mg of compound areneeded for 2 essays andpackaged in a vial
Sensitive samples mustbe isolated in sealedampoule
For special analysisrequests please contactservice
Sulphur is analyzed oncea year if enoughdemand
Who to contact Isabelle BorgetTel 05 61 33 32 14
mail isabelleborgetlcc-toulousefr
Where to find service LCC door B038
205 route de Narbonne
When 9h to 11h30 - 14h to 16h30
From monday to friday
on appointment
Some advice
23
Nuclear Magnetic Resonance - LCC
How to request an analysis
bull For any analysis request (except self-service equipments)
For NMR equipments (400-solid and 600 MHz) analysisand appointment requests must be emailed to Y Coppelor C Bijani
The analysis request form can be loaded from the NMRfacility webpage on the LCC website (httplcc-toulousefr)
bull Self-service equipments
All the users have to follow a training conducted by NMRfacilityrsquos staff before any use of self-service spectrometers
- for LCC teams the training and NMR user accountrequests are provided with taking office
- for outside labs please contact the LCC personneldepartment
The requests when validated must be returned directlyto A Bonnet or D Paryl in order to plan the training
The users undertake to carefully respect the operatinginstructions and the LCC memos
All the data are automatically
- made available in the LCC teamsrsquo laquo Nuage raquo file
- emailed to the user from outside labs
Feel free to contact us for any question
about analysis capabilities or for
any discussion about the best strategy to
meet your specific issues
Who to contact
Yannick Coppel (Mgr)Christian BijaniTel 05 61 17 54 27
Antoine BonnetDavid Paryl
Tel 05 61 17 54 30Email yannickcoppellcc-
toulousefrchristianbijanilcc-toulousefrantoinebonnetlcc-toulousefr
davidparyllcc-toulousefr
Some advice
Where to find us
LCC RMN Building 205 route de Narbonne Toulouse
Door 030 (Y Coppel et C Bijani)
Door 033 (F Lacassin et D Paryl)
When8h30 to 11h30 -14h to 17h
From Monday to Friday
24
Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) - LCC
How to request an analysis
bull For any analysis request
Each sample must be supplied with an analysisrequest form To request this form please contact the staff
Sample amount depends on the concentration of chemical elements to be measured in the sampleanalyzed
In the very first request please contact the staff
bull Results
Results are delivered in the letter-box of the LCC team or for outside labs made available in the ICP departmentrsquos letter-box (within the LCC entrance hall)
bull Analyses schedule
Analyses are carried out every 2 weeks
In general 10 mg per assay isneeded (provided that the
concentration is above 5 ww)
Chemical elements currentlyanalyzed (but not limited) Ag Al Au B Ba Be Bi Ca Cd Co Cr Cu Fe Ir K Li Mg Mn Na
Ni P Pb Pd Pt Ru Rh Sr Zn
Who to contact
Alain Moreau Tel 0561175850
E-mail alainmoreaulcc-toulousefr
Where to find usIPBS Bacirct A3
205 route de Narbonne
When 8h to 11h30 - 14h to 16h30From Monday to Friday (odd
week)
Some advice
25
Single Crystal X-Ray Diffraction
How to request an analysis
bull Beforehand
As soon as the crystals are obtained contact the staff of theservice so that they can evaluate the quality of the sample
If hte sample quality is judged to be sufficient to measure theX-ray diffraction an analysis request form should becomleted and submitted with the sample
bull For all analysis requests
Every sample must be accompanied by a completed analysisrequest form You will find this form on the ICT website
ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsdiffraction-des-rayons-x
Take care to specify the properties of the sample (sensitivityto air tempeacuterature lighthellip) the reagents used and theexpected crystal structure
Also specify the information that you hope to obtain from theanalysis (eg absolute configuration hellip)
While yoursquore waiting for the evaluation of the
crystal quality manipulate the
sample as little as possible and keep it
at the crystallizationtemperature until the
analysis
Who to contactNathalie Saffon (Mgr)Sonia Mallet-Ladeira
Tel 05 61 55 83 48 or 8173 Email rxictchimieups-tlsefr
Where can you find us Door 2053 2nd floor
Laboratory - Door 055 basement building 2R1
Universiteacute Paul Sabatier
When Monday Tuesday Thursday and
Friday
Some advice
5
How to request an analysis or a purification
bull For any request for analysis or purification (reverse or normal phaseionic or supercritical chromatography)
All samples must be accompanied by a fully completed form preferablydouble-sided which will be retained by the service
You will find this form on the ICT website
ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upshplc
Any sample not accompanied by this form will not be treated
bull Samples preparation
For your analysis you can prepare yourself your samples in 02 microm self-filtering vials (available on the platform) with a concentration of 1 mgmL
For your purifications you can bring the raw product
All services are provided after a validated appointment given by theplatform staff when depositing samples
bull Recovery of your results or purified samples
A generic analysis report is sent by email in PDF format
The platform staff listen to your needs for a more detailed report
Come and collect your purified products upon receipt of the results
Please note that saving the results is not guaranteed in the long term Takecare we do not guarantee the long-term storage of your results
bull Self-service devices
Any equipment can be made available after validation of the training onthe device concerned by the platform manager
To do this make an appointment one month before the desired use inorder to obtain validation of your training on time This validation is validfor a fixed period
Online booking httpglpi-ictgrr-hplc to use equipments
For the preparation of your samples
solid phase extraction cartridges
and self-filtering vials are available
Contact us in case of difficulties in filling
in the form or in defining the best
separation method suitable for your
product
Who to contactIsabelle FabingOffice 05 61 55 81 98
Lab 05 61 55 62 95email hplcictchimieups-tlsefr
Where can you find us Door 30793083 3rd floor
building 2R1 Universiteacute Paul Sabatier
When Monday to Friday
Reception
9h30-11h30 am
Some advice
6
Chromatography
copyFreacutedeacuteric MaligneICT
How to request an analysis
bull For all analysis requests on the 400 and 500 MHz NMR spectrometerssituated in the High Technology Module (MHT)Each sample must be accompanied by a fully completed laquo AnalysisRequest raquo form You can find this form on the ICT websiteictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsrmn oron the website of the NMR service (httprmn-webups-tlsefr)It is essential to make an appointment by email telephone or in personat the NMR service
bull For all analysis requests on the 300 MHz open access NMR spectrometerslocated in Building 2R1You must sign up to the NMR training before using the 300 MHz spectrometers (inscription form on the website of the NMR service httprmn-webups-tlsefr)
bull Follow the instructionsI ndash NMR Tubes
NMR tubes must meet a minimum standard of qualityBroken or damaged tubes and Economy tubes are forbidden from the service as they are too fragile
II ndash Cleaning tubes After the analysis the tubes must be washed as quickly as possible using the same solvent that was used to dissolve the analyte After several rinses the tube should be dried at room temperature or in an oven at less than 60degC
III ndash Filling the tubesFor an optimal measurement your tube should contain 600 microL of
solvent bull Results spectra can be recovered by
- downloading from the NMR server- USB stick- by email (only for 1 D analyses)
Once the analysis has been completed you must come to pick up yoursamples from the NMR service
The sensitivity of an NMR experiment depends on the
nucleus studied and the concentration of your product
If necessary during samplepreparation filter your solutions
in order to remove any suspendedsolids
The choice of solvent dependsprimarily on the solubility of your
product at room temperature
If there are several possibilities choose a solvent whose peaks do
not interfere with those of yourproduct
For more information please feelfree to contact the staff of the NMR
service
Who to contact
Marc Vedrenne (Msg)Pierre Lavedan
Steacutephane MassouCaroline ToppanClaude Andreu
Tel 05-61-55 ext 84-78 68-78Email rmnictchimieups-tlsefr
Where to find us Door 45 Ground floor High
Technology Module Universiteacute Paul Sabatier
When Monday to Friday
09h00-12h00 and 14h00-16h30
Some advice
NMR Service
copyFreacutedeacuteric MaligneICT
Mass spectrometry
How to request an analysis
bull For all analysis requests
Each sample must be accompanied by a fully completedanalysis request form You can find this form on the ICT website ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsspectrometrie-de-masse
You can also fill in all the administrative details one timeonly and save them for your future requests and you canarchive your forms
Bring the forms (preferably double-sided) and sample duringopening hours We will check with you the feasibility of theproposed analyses
bull For air-sensitive samples
Make an appointment
bull For LCMS and GCMS analyses
Make an appointment
bull How to collect your results
The results will be sent to you in pdf format Upon receivingour mail you can come and pick up your samples and formsduring opening hours
We will assess the feasibility of the
analysis with you
If you donrsquot know which method of ionization is
better suited for your molecules then leave it
blank and we will choose together
Who to contactCatherine Claparols ( Mgr)
Valeacuterie BourdonEric Leroy
Nathalie Martins-FromentTel 33 5 61 55 64 69Fax 33 5 61 55 81 16
Email spectromasseictups-tlsefr
Where to find us
Door 157 groundfloor building 2R1 Universiteacute Paul Sabatier
When
Monday-Friday 10h30-12h and 13h30-15h00
Some advice
8
copyFreacutedeacuteric MaligneICT
INFRARED Spectroscopy
How to request an analysis
bull For each analysis request
Each sample must be accompanied by a fully completedanalysis request form You can find this form on the ICT website ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsspectroscopies-infrarouge and on the door of the service
Required sample quantity 05 to 2 mg for powders 1drop for liquids 1ml for solutions (in this case you will alsoneed to supply 10-20 ml of pure solvent)
bull For infrared microscopy kinetics
Please make an appointment
bull For other analyses transmission ATR DRIFT far-IR NIR
Leave your sample at the service If unattended a box isavailable on the door to drop off your samples
bull Open access equipment for ATR analyses only
It can be used after completion of a 1h training course Makean appointment
All kinds of samples can beanalyzed solids liquids solutions blocks grains of
wheathellipyou just needto choose the right
method depending on your sample and your
study
Come and discuss with us
Extensive infrared and Raman tables and
spectral data bases are available at the
service60 000 data base spectra
are available
Who to contactCorinne Routaboul
Tel 05 61 55 64 00Email routabouictchimieups-tlsefr
Where to find us Door 1025 1st floor building 2R1
Universiteacute Paul Sabatier
When Monday-Friday 9h00-17h00
If unattended leave the sample in the deposit box on the door If youhave more than 10 samples or if you need particular techniques please make an appointment
Some advice
9
copyFreacutedeacuteric MaligneICT
TECHNOPOLYM
10
Technopolym
How to request an analysis
bull Request an analysis via the central Technopolym emailtechnopolymictchimieups-tlsefr
Following this email we will inform you about the proposedtechniques of analyse costs time of delivery requiredquantity of sample conditioning sample deposit Dependingon your expected results an appointment to discuss yourproblem may be proposed before scheduling an analysis
bull For all analysis requestsEach sample must be accompanied by a fully completed
analysis request form You can find this form on the ICT website
ictcnrsfrplateforme-de-licttechnopolym or on the Technopolym website
httptechnopolymups-tlsefr
bull For more information
Visit our website to know about our skills equipment references
TechnopolymIs a virtual technological
platform dedicated to the characterization of polymeric
materials
We propose a range of analytical techniques
molecularcharacterization phase
transitions thermal stability behavior in
solution mechanicalproperties surface characterizationhellip
Come and talk to us
Who to contactPascale Saint-Aguet
Tel 05 61 55 68 08Tel (LCC) 05 61 33 31 34
Email technopolymictchimieups-tlsefr
Some advice
Where to find us
Door 30233rd floor building 2R1 Universiteacute Paul Sabatier
Door G064 ndashLCC 205 rte de Narbonne -
When
Monday-Friday 9h-12h and
14h-17h
11
Cross-Platform Services
12
Documentation
How to make a request
bull For all document requests
You can request your document by email telephone or inperson Donrsquot forget to indicate your full name and laboratorywith the references on your request
bull Consultation and loans
The catalogue of the chemistry library is available on theintranet
ictcnrsfrdocchimie
Borrowing is possible during office hours ndash outside thesehours please make an appointment
bull For bibliographic searches and training
Make an appointment
bull Open access
You can come and work at the library ndash computers and wifi are available Visit our website
ictcnrsfrplateforme-de-lictservices-transversesaccueil-de-la-documentation
Ask the documentation service for your intranet
password from
Feel free to call the service for any problems
relating to the use of bibliographic databases
Who to contactDanielle Brunet
Tel 05 61 55 85 69Email brunetictchimieups-tlsefr
Some advice
Where to find us
Door 0145 ground floor building 2R1
Universiteacute Paul Sabatier
When
Mon-Fri 9h-12h and 14h-17h If unattended make an
appointment
13
Electronics
How to make a request
Who to contactJean-Michel Martin
Tel 05 61 55 86 93Email scicassistanceictchimieups-tlsefr
Email martinjmictchimieups-tlsefr
Feel free to ask the service for
- Modification of existingelectronic devices and
proposals for improvement
- Troubleshooting and repair of electronic
devices
- Advice on purchase of new material
bull For all installation andor maintenance of equipment with astrong electronic component
Send an email phone or contact the service in person duringoffice hours
bull For all service requests
Send an email toscicassistanceictchimieups-tlsefrstating your name office number and a brief description of the problem
bull Loan of equipment
To address the needs of users specific equipment is availablein the electronics workshop (Oscilloscope component testerssoldering ironhellip) aswell as various tools
It is possible to borrow this equipment
Where to find usDoor 1015 1st floor building 2R1 Universiteacute Paul Sabatier
When Monday-Friday office hours
If unattended make an appointment
Some advice
14
Information Technology
How to make a request
bull For all requests for connection to the network andcreation of email accounts
First see the secretary of your laboratory
bull For all service requests
Write toscicassistanceictchimieups-tlsefr
stating your name office number and a brief description of the problem
The IT service manages developsand maintains the
network and associated services
Please contact us for more information on
the services provided (automatic
backup of data access to Cambridge CCDC data sharing
etc)
Who to contactPascal Puech
Edouard IvanovtchikTel 05 61 55 68 73
Email scicassistanceictchimieups-tlsefr
Some advice
Where to find usDoor 168 ground floor building 2R1
Universiteacute Paul Sabatier
WhenMonday-Friday office hours
If unattended make an appointment
15
Scientific Glassware
How to make a request
bull For all service requests
All glassware to repair or construct must be accompanied bya fully completed form You can find this form on the ICTwebsite ictcnrsfrVerrerie-scientifique
For obvious reasons of safety and hygiene glassware must beclean free of silicon grease and in a container identified withthe name of the research group
bull Do I need to go in person
In person contact is preferred if you are new to glasswork andif your request is complex
Photos et technical drawings sent by email are onlycomplementary information as in isolation they can lead tomisunderstandings and errors
For all glass repairs construction of new
equipment or prototyping
feel free to consult the glassware service
We can provide technicaladvice as well as contacts
in specialized domains
Who to contactSteacutephane Foulon
Tel 05 61 55 61 16Email foulonictchimieups-
tlsefr
Some advice
Where to find us
Door 0194 Ground Floor Building 2R1Universiteacute Paul
Sabatier
When
Monday-Friday during office hours We recommend that
external users make an appointment
16
copyFreacutedeacuteric MaligneICT
LCC Services
17
Thermal Analyses LCC
How to request an analysis
bull For any analysis request
DTATGA or DSC analyses each sample must be suppliedwith an analysis request form duly filled out To requestthese forms please contact the staff by e-mail
In the very first request please contact the staff fordetails about the process the sample amount requiredthe packaging of samples etc
In all other cases the analyses requests and the samplescan be deposited in the Thermal Analyses Departmentrsquosletter-box (within the LCC entrance hall)
bull Air-sensitive samples
Make an appointment with the staff
bull Results
Analyses results are emailed as a text file paper copy isavailable upon request
On completion of analyses remaining of samples must bepick up at LCC
Analytical Equipments
DTATGA for measuring the mass variation as a
function of temperature
DSC for detecting the phase changes without mass loss
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 1 0Email j-fmeunierlcc-toulousefr
Some advice
Where to find usLCC - Door CS12 basement level
205 route de Narbonne
When Opening hours 9h to 11h30 - 14h to 17hfrom Monday to Friday except on wednesday
18
Library Resource Center LCC
How to make a request
bull For any information request
- LCC research teams fill out the request form available onthe LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs contact the staff by e-mail
bull For bibliographical searches and access
Digital databases
- LCC research teams bibliographical searches databases areavailable on the LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs make an appointment with the staff
Paper print collections
Paperprint collections also are available and can be read in thelibrary premises
LCCrsquos Library access is free for LCC teams and subject to anappointment for outside labs
LCC teams Access to the LCC intranet is provided
with taking office
For further information feel free to contact us
Who to contact
Marie-Heacutelegravene Gullimarie-helenegullilcc-toulousefr
0561333217
Gilles Roujasgillesroujaslcc-toulousefr
0561333140
Gaeumltan Havetgaetanhavetlcc-toulousefr
0561333140
Some advice
Where to find usLCC 205 route de Narbonne
When Opening hours
9 h to 11h30 - 13h to 17h From Monday to Friday
19
Feel free to contact us for anyquestion about analyses
options or for anydiscussion about the
best strategy to meetyour specific issues
Single ndashcrystal and powder X-Ray Diffraction - LCC
How to request an analysis
bull Prior to any analysis
Contact the staff in charge of X-Ray Diffraction measurementsfor your team or your lab
bull Single-crystal X-ray diffraction
First the staff will evaluate the quality of the sample If quality isacceptable for a X-ray diffraction measurement an appointmentwill be set up for analysis
Following information must be provided expected compound used solvents any specific information concerning the sample(air-sensitive thermal-sensitive light-sensitivehellip) analysis and required data (absolute configuration hydride locationhellip)
bull Powder X-ray diffraction
Appointments are proposed in accordance with the type of measurement (reflection capillary measurements at variable temperatures x-ray grazing incidence on thin films)
Following information must be provided sample characteristics analytical conditions (scanning range of 2theta temperaturehellip) required data (phase identification crystallites sizehellip)
Useful tips Until getting staff opinion about the quality of yoursample particularly for a single-crystal handle it as little as possible
Who to contact Laure Vendier (Mgr)
Carine DuhayonSonia Mallet-Ladeira
Tel 05 61 33 31 18Email laurevendierlcc-toulousefr
carineduhayonlcc-toulousefrladeiraictchimieups-tlsefr
Some advice
Where to find us
LCC 205 route de NarbonneX-Ray Diffraction office ground floor door B017 X-Ray Diffraction Lab basement level door GS66
When
9h to 11h30 - 14h to 17hFrom Monday to Friday except on Wednesday afternoon
20
Electrochemistry - LCC
How to request an analysis
bull For any analysis request
Analyses are carried out by appointment onlyscheduled with the staff when requesting theanalysis
On the appointed date Bring the sample and the solvent Your presence is required during the analyses
bull Sample preparation
The sample(s) must be as pure as possible correspondingto a concentration of 10-3 molL-1 in 10 mL
For each sample bring 30 mL of purified solvent
bull Results
On completion of the analyses the mostrepresentative curves are provided in paper copy
Upon request the electronic files can be emailed
Who to contactAlix Sournia-Saquet (Mgr)
Alain MoreauTel 05 61 33 31 75
Email alixsaquetlcc-toulousefralainmoreaulcc-toulousefr
Some advice
Before any analysis feel free to contact us for any
discussion or question about feasibility and conditions of
analyses
The staff can help you
- to choose the best-suited technique to your needs
- for interpretation of your data
Where to find us LCC- door B015ndash ground floor-building B205 route de Narbonne
When 9h to 11h30 -14h to 17h
From Monday to Friday
21
Magnetic Measurement and Moumlssbauer spectroscopy - LCC
How to request an analysis
bull For any analysis request
For magnetic measurements SQUID andMoumlssbauer spectroscopy please contact Jean-Franccedilois Meunier by e-mail or phone
An appointment will be set up in order to studyyour analyses requests and to define theexperimental conditions
An analysis request form will be provided by thestaff
bull Results and samples
Results are emailed as text and excel files
On completion of the analyses samples must beretrieved at LCC
Further information on equipments
lcc-toulousefrServices Spectroscopie Moumlssbauer
Lcc-toulousefr
servicesMesures
Magneacutetiques
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 10Email Jf-meunierlcc-toulousefr
Where to find usLCC door CS012
205 route de Narbonne
When 9h to 12h - 14h to 17h30
From Monday to Friday
Some advice
22
Elemental Analysis C-H-NS - LCC
How to request an analysis
For any analysis request
Each sample must be supplied with an analysis request formavailable on LCC website
wwwlcc-toulousefr gt services gt services techniques ampscientifiques gt analyses chimiques gt Formulaire
Fill in electronically and send by mail (see framed who tocontact)
Samples
- Internal in my box DEPOT CHN in the mail locker analyseselementaires
- External ship by courrier to LCC service CHN or ask anappointment
Results
Results are sent by mail Samples are not returned
Analyses
Analyses are carried out every week
10 mg of compound areneeded for 2 essays andpackaged in a vial
Sensitive samples mustbe isolated in sealedampoule
For special analysisrequests please contactservice
Sulphur is analyzed oncea year if enoughdemand
Who to contact Isabelle BorgetTel 05 61 33 32 14
mail isabelleborgetlcc-toulousefr
Where to find service LCC door B038
205 route de Narbonne
When 9h to 11h30 - 14h to 16h30
From monday to friday
on appointment
Some advice
23
Nuclear Magnetic Resonance - LCC
How to request an analysis
bull For any analysis request (except self-service equipments)
For NMR equipments (400-solid and 600 MHz) analysisand appointment requests must be emailed to Y Coppelor C Bijani
The analysis request form can be loaded from the NMRfacility webpage on the LCC website (httplcc-toulousefr)
bull Self-service equipments
All the users have to follow a training conducted by NMRfacilityrsquos staff before any use of self-service spectrometers
- for LCC teams the training and NMR user accountrequests are provided with taking office
- for outside labs please contact the LCC personneldepartment
The requests when validated must be returned directlyto A Bonnet or D Paryl in order to plan the training
The users undertake to carefully respect the operatinginstructions and the LCC memos
All the data are automatically
- made available in the LCC teamsrsquo laquo Nuage raquo file
- emailed to the user from outside labs
Feel free to contact us for any question
about analysis capabilities or for
any discussion about the best strategy to
meet your specific issues
Who to contact
Yannick Coppel (Mgr)Christian BijaniTel 05 61 17 54 27
Antoine BonnetDavid Paryl
Tel 05 61 17 54 30Email yannickcoppellcc-
toulousefrchristianbijanilcc-toulousefrantoinebonnetlcc-toulousefr
davidparyllcc-toulousefr
Some advice
Where to find us
LCC RMN Building 205 route de Narbonne Toulouse
Door 030 (Y Coppel et C Bijani)
Door 033 (F Lacassin et D Paryl)
When8h30 to 11h30 -14h to 17h
From Monday to Friday
24
Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) - LCC
How to request an analysis
bull For any analysis request
Each sample must be supplied with an analysisrequest form To request this form please contact the staff
Sample amount depends on the concentration of chemical elements to be measured in the sampleanalyzed
In the very first request please contact the staff
bull Results
Results are delivered in the letter-box of the LCC team or for outside labs made available in the ICP departmentrsquos letter-box (within the LCC entrance hall)
bull Analyses schedule
Analyses are carried out every 2 weeks
In general 10 mg per assay isneeded (provided that the
concentration is above 5 ww)
Chemical elements currentlyanalyzed (but not limited) Ag Al Au B Ba Be Bi Ca Cd Co Cr Cu Fe Ir K Li Mg Mn Na
Ni P Pb Pd Pt Ru Rh Sr Zn
Who to contact
Alain Moreau Tel 0561175850
E-mail alainmoreaulcc-toulousefr
Where to find usIPBS Bacirct A3
205 route de Narbonne
When 8h to 11h30 - 14h to 16h30From Monday to Friday (odd
week)
Some advice
25
How to request an analysis or a purification
bull For any request for analysis or purification (reverse or normal phaseionic or supercritical chromatography)
All samples must be accompanied by a fully completed form preferablydouble-sided which will be retained by the service
You will find this form on the ICT website
ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upshplc
Any sample not accompanied by this form will not be treated
bull Samples preparation
For your analysis you can prepare yourself your samples in 02 microm self-filtering vials (available on the platform) with a concentration of 1 mgmL
For your purifications you can bring the raw product
All services are provided after a validated appointment given by theplatform staff when depositing samples
bull Recovery of your results or purified samples
A generic analysis report is sent by email in PDF format
The platform staff listen to your needs for a more detailed report
Come and collect your purified products upon receipt of the results
Please note that saving the results is not guaranteed in the long term Takecare we do not guarantee the long-term storage of your results
bull Self-service devices
Any equipment can be made available after validation of the training onthe device concerned by the platform manager
To do this make an appointment one month before the desired use inorder to obtain validation of your training on time This validation is validfor a fixed period
Online booking httpglpi-ictgrr-hplc to use equipments
For the preparation of your samples
solid phase extraction cartridges
and self-filtering vials are available
Contact us in case of difficulties in filling
in the form or in defining the best
separation method suitable for your
product
Who to contactIsabelle FabingOffice 05 61 55 81 98
Lab 05 61 55 62 95email hplcictchimieups-tlsefr
Where can you find us Door 30793083 3rd floor
building 2R1 Universiteacute Paul Sabatier
When Monday to Friday
Reception
9h30-11h30 am
Some advice
6
Chromatography
copyFreacutedeacuteric MaligneICT
How to request an analysis
bull For all analysis requests on the 400 and 500 MHz NMR spectrometerssituated in the High Technology Module (MHT)Each sample must be accompanied by a fully completed laquo AnalysisRequest raquo form You can find this form on the ICT websiteictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsrmn oron the website of the NMR service (httprmn-webups-tlsefr)It is essential to make an appointment by email telephone or in personat the NMR service
bull For all analysis requests on the 300 MHz open access NMR spectrometerslocated in Building 2R1You must sign up to the NMR training before using the 300 MHz spectrometers (inscription form on the website of the NMR service httprmn-webups-tlsefr)
bull Follow the instructionsI ndash NMR Tubes
NMR tubes must meet a minimum standard of qualityBroken or damaged tubes and Economy tubes are forbidden from the service as they are too fragile
II ndash Cleaning tubes After the analysis the tubes must be washed as quickly as possible using the same solvent that was used to dissolve the analyte After several rinses the tube should be dried at room temperature or in an oven at less than 60degC
III ndash Filling the tubesFor an optimal measurement your tube should contain 600 microL of
solvent bull Results spectra can be recovered by
- downloading from the NMR server- USB stick- by email (only for 1 D analyses)
Once the analysis has been completed you must come to pick up yoursamples from the NMR service
The sensitivity of an NMR experiment depends on the
nucleus studied and the concentration of your product
If necessary during samplepreparation filter your solutions
in order to remove any suspendedsolids
The choice of solvent dependsprimarily on the solubility of your
product at room temperature
If there are several possibilities choose a solvent whose peaks do
not interfere with those of yourproduct
For more information please feelfree to contact the staff of the NMR
service
Who to contact
Marc Vedrenne (Msg)Pierre Lavedan
Steacutephane MassouCaroline ToppanClaude Andreu
Tel 05-61-55 ext 84-78 68-78Email rmnictchimieups-tlsefr
Where to find us Door 45 Ground floor High
Technology Module Universiteacute Paul Sabatier
When Monday to Friday
09h00-12h00 and 14h00-16h30
Some advice
NMR Service
copyFreacutedeacuteric MaligneICT
Mass spectrometry
How to request an analysis
bull For all analysis requests
Each sample must be accompanied by a fully completedanalysis request form You can find this form on the ICT website ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsspectrometrie-de-masse
You can also fill in all the administrative details one timeonly and save them for your future requests and you canarchive your forms
Bring the forms (preferably double-sided) and sample duringopening hours We will check with you the feasibility of theproposed analyses
bull For air-sensitive samples
Make an appointment
bull For LCMS and GCMS analyses
Make an appointment
bull How to collect your results
The results will be sent to you in pdf format Upon receivingour mail you can come and pick up your samples and formsduring opening hours
We will assess the feasibility of the
analysis with you
If you donrsquot know which method of ionization is
better suited for your molecules then leave it
blank and we will choose together
Who to contactCatherine Claparols ( Mgr)
Valeacuterie BourdonEric Leroy
Nathalie Martins-FromentTel 33 5 61 55 64 69Fax 33 5 61 55 81 16
Email spectromasseictups-tlsefr
Where to find us
Door 157 groundfloor building 2R1 Universiteacute Paul Sabatier
When
Monday-Friday 10h30-12h and 13h30-15h00
Some advice
8
copyFreacutedeacuteric MaligneICT
INFRARED Spectroscopy
How to request an analysis
bull For each analysis request
Each sample must be accompanied by a fully completedanalysis request form You can find this form on the ICT website ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsspectroscopies-infrarouge and on the door of the service
Required sample quantity 05 to 2 mg for powders 1drop for liquids 1ml for solutions (in this case you will alsoneed to supply 10-20 ml of pure solvent)
bull For infrared microscopy kinetics
Please make an appointment
bull For other analyses transmission ATR DRIFT far-IR NIR
Leave your sample at the service If unattended a box isavailable on the door to drop off your samples
bull Open access equipment for ATR analyses only
It can be used after completion of a 1h training course Makean appointment
All kinds of samples can beanalyzed solids liquids solutions blocks grains of
wheathellipyou just needto choose the right
method depending on your sample and your
study
Come and discuss with us
Extensive infrared and Raman tables and
spectral data bases are available at the
service60 000 data base spectra
are available
Who to contactCorinne Routaboul
Tel 05 61 55 64 00Email routabouictchimieups-tlsefr
Where to find us Door 1025 1st floor building 2R1
Universiteacute Paul Sabatier
When Monday-Friday 9h00-17h00
If unattended leave the sample in the deposit box on the door If youhave more than 10 samples or if you need particular techniques please make an appointment
Some advice
9
copyFreacutedeacuteric MaligneICT
TECHNOPOLYM
10
Technopolym
How to request an analysis
bull Request an analysis via the central Technopolym emailtechnopolymictchimieups-tlsefr
Following this email we will inform you about the proposedtechniques of analyse costs time of delivery requiredquantity of sample conditioning sample deposit Dependingon your expected results an appointment to discuss yourproblem may be proposed before scheduling an analysis
bull For all analysis requestsEach sample must be accompanied by a fully completed
analysis request form You can find this form on the ICT website
ictcnrsfrplateforme-de-licttechnopolym or on the Technopolym website
httptechnopolymups-tlsefr
bull For more information
Visit our website to know about our skills equipment references
TechnopolymIs a virtual technological
platform dedicated to the characterization of polymeric
materials
We propose a range of analytical techniques
molecularcharacterization phase
transitions thermal stability behavior in
solution mechanicalproperties surface characterizationhellip
Come and talk to us
Who to contactPascale Saint-Aguet
Tel 05 61 55 68 08Tel (LCC) 05 61 33 31 34
Email technopolymictchimieups-tlsefr
Some advice
Where to find us
Door 30233rd floor building 2R1 Universiteacute Paul Sabatier
Door G064 ndashLCC 205 rte de Narbonne -
When
Monday-Friday 9h-12h and
14h-17h
11
Cross-Platform Services
12
Documentation
How to make a request
bull For all document requests
You can request your document by email telephone or inperson Donrsquot forget to indicate your full name and laboratorywith the references on your request
bull Consultation and loans
The catalogue of the chemistry library is available on theintranet
ictcnrsfrdocchimie
Borrowing is possible during office hours ndash outside thesehours please make an appointment
bull For bibliographic searches and training
Make an appointment
bull Open access
You can come and work at the library ndash computers and wifi are available Visit our website
ictcnrsfrplateforme-de-lictservices-transversesaccueil-de-la-documentation
Ask the documentation service for your intranet
password from
Feel free to call the service for any problems
relating to the use of bibliographic databases
Who to contactDanielle Brunet
Tel 05 61 55 85 69Email brunetictchimieups-tlsefr
Some advice
Where to find us
Door 0145 ground floor building 2R1
Universiteacute Paul Sabatier
When
Mon-Fri 9h-12h and 14h-17h If unattended make an
appointment
13
Electronics
How to make a request
Who to contactJean-Michel Martin
Tel 05 61 55 86 93Email scicassistanceictchimieups-tlsefr
Email martinjmictchimieups-tlsefr
Feel free to ask the service for
- Modification of existingelectronic devices and
proposals for improvement
- Troubleshooting and repair of electronic
devices
- Advice on purchase of new material
bull For all installation andor maintenance of equipment with astrong electronic component
Send an email phone or contact the service in person duringoffice hours
bull For all service requests
Send an email toscicassistanceictchimieups-tlsefrstating your name office number and a brief description of the problem
bull Loan of equipment
To address the needs of users specific equipment is availablein the electronics workshop (Oscilloscope component testerssoldering ironhellip) aswell as various tools
It is possible to borrow this equipment
Where to find usDoor 1015 1st floor building 2R1 Universiteacute Paul Sabatier
When Monday-Friday office hours
If unattended make an appointment
Some advice
14
Information Technology
How to make a request
bull For all requests for connection to the network andcreation of email accounts
First see the secretary of your laboratory
bull For all service requests
Write toscicassistanceictchimieups-tlsefr
stating your name office number and a brief description of the problem
The IT service manages developsand maintains the
network and associated services
Please contact us for more information on
the services provided (automatic
backup of data access to Cambridge CCDC data sharing
etc)
Who to contactPascal Puech
Edouard IvanovtchikTel 05 61 55 68 73
Email scicassistanceictchimieups-tlsefr
Some advice
Where to find usDoor 168 ground floor building 2R1
Universiteacute Paul Sabatier
WhenMonday-Friday office hours
If unattended make an appointment
15
Scientific Glassware
How to make a request
bull For all service requests
All glassware to repair or construct must be accompanied bya fully completed form You can find this form on the ICTwebsite ictcnrsfrVerrerie-scientifique
For obvious reasons of safety and hygiene glassware must beclean free of silicon grease and in a container identified withthe name of the research group
bull Do I need to go in person
In person contact is preferred if you are new to glasswork andif your request is complex
Photos et technical drawings sent by email are onlycomplementary information as in isolation they can lead tomisunderstandings and errors
For all glass repairs construction of new
equipment or prototyping
feel free to consult the glassware service
We can provide technicaladvice as well as contacts
in specialized domains
Who to contactSteacutephane Foulon
Tel 05 61 55 61 16Email foulonictchimieups-
tlsefr
Some advice
Where to find us
Door 0194 Ground Floor Building 2R1Universiteacute Paul
Sabatier
When
Monday-Friday during office hours We recommend that
external users make an appointment
16
copyFreacutedeacuteric MaligneICT
LCC Services
17
Thermal Analyses LCC
How to request an analysis
bull For any analysis request
DTATGA or DSC analyses each sample must be suppliedwith an analysis request form duly filled out To requestthese forms please contact the staff by e-mail
In the very first request please contact the staff fordetails about the process the sample amount requiredthe packaging of samples etc
In all other cases the analyses requests and the samplescan be deposited in the Thermal Analyses Departmentrsquosletter-box (within the LCC entrance hall)
bull Air-sensitive samples
Make an appointment with the staff
bull Results
Analyses results are emailed as a text file paper copy isavailable upon request
On completion of analyses remaining of samples must bepick up at LCC
Analytical Equipments
DTATGA for measuring the mass variation as a
function of temperature
DSC for detecting the phase changes without mass loss
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 1 0Email j-fmeunierlcc-toulousefr
Some advice
Where to find usLCC - Door CS12 basement level
205 route de Narbonne
When Opening hours 9h to 11h30 - 14h to 17hfrom Monday to Friday except on wednesday
18
Library Resource Center LCC
How to make a request
bull For any information request
- LCC research teams fill out the request form available onthe LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs contact the staff by e-mail
bull For bibliographical searches and access
Digital databases
- LCC research teams bibliographical searches databases areavailable on the LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs make an appointment with the staff
Paper print collections
Paperprint collections also are available and can be read in thelibrary premises
LCCrsquos Library access is free for LCC teams and subject to anappointment for outside labs
LCC teams Access to the LCC intranet is provided
with taking office
For further information feel free to contact us
Who to contact
Marie-Heacutelegravene Gullimarie-helenegullilcc-toulousefr
0561333217
Gilles Roujasgillesroujaslcc-toulousefr
0561333140
Gaeumltan Havetgaetanhavetlcc-toulousefr
0561333140
Some advice
Where to find usLCC 205 route de Narbonne
When Opening hours
9 h to 11h30 - 13h to 17h From Monday to Friday
19
Feel free to contact us for anyquestion about analyses
options or for anydiscussion about the
best strategy to meetyour specific issues
Single ndashcrystal and powder X-Ray Diffraction - LCC
How to request an analysis
bull Prior to any analysis
Contact the staff in charge of X-Ray Diffraction measurementsfor your team or your lab
bull Single-crystal X-ray diffraction
First the staff will evaluate the quality of the sample If quality isacceptable for a X-ray diffraction measurement an appointmentwill be set up for analysis
Following information must be provided expected compound used solvents any specific information concerning the sample(air-sensitive thermal-sensitive light-sensitivehellip) analysis and required data (absolute configuration hydride locationhellip)
bull Powder X-ray diffraction
Appointments are proposed in accordance with the type of measurement (reflection capillary measurements at variable temperatures x-ray grazing incidence on thin films)
Following information must be provided sample characteristics analytical conditions (scanning range of 2theta temperaturehellip) required data (phase identification crystallites sizehellip)
Useful tips Until getting staff opinion about the quality of yoursample particularly for a single-crystal handle it as little as possible
Who to contact Laure Vendier (Mgr)
Carine DuhayonSonia Mallet-Ladeira
Tel 05 61 33 31 18Email laurevendierlcc-toulousefr
carineduhayonlcc-toulousefrladeiraictchimieups-tlsefr
Some advice
Where to find us
LCC 205 route de NarbonneX-Ray Diffraction office ground floor door B017 X-Ray Diffraction Lab basement level door GS66
When
9h to 11h30 - 14h to 17hFrom Monday to Friday except on Wednesday afternoon
20
Electrochemistry - LCC
How to request an analysis
bull For any analysis request
Analyses are carried out by appointment onlyscheduled with the staff when requesting theanalysis
On the appointed date Bring the sample and the solvent Your presence is required during the analyses
bull Sample preparation
The sample(s) must be as pure as possible correspondingto a concentration of 10-3 molL-1 in 10 mL
For each sample bring 30 mL of purified solvent
bull Results
On completion of the analyses the mostrepresentative curves are provided in paper copy
Upon request the electronic files can be emailed
Who to contactAlix Sournia-Saquet (Mgr)
Alain MoreauTel 05 61 33 31 75
Email alixsaquetlcc-toulousefralainmoreaulcc-toulousefr
Some advice
Before any analysis feel free to contact us for any
discussion or question about feasibility and conditions of
analyses
The staff can help you
- to choose the best-suited technique to your needs
- for interpretation of your data
Where to find us LCC- door B015ndash ground floor-building B205 route de Narbonne
When 9h to 11h30 -14h to 17h
From Monday to Friday
21
Magnetic Measurement and Moumlssbauer spectroscopy - LCC
How to request an analysis
bull For any analysis request
For magnetic measurements SQUID andMoumlssbauer spectroscopy please contact Jean-Franccedilois Meunier by e-mail or phone
An appointment will be set up in order to studyyour analyses requests and to define theexperimental conditions
An analysis request form will be provided by thestaff
bull Results and samples
Results are emailed as text and excel files
On completion of the analyses samples must beretrieved at LCC
Further information on equipments
lcc-toulousefrServices Spectroscopie Moumlssbauer
Lcc-toulousefr
servicesMesures
Magneacutetiques
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 10Email Jf-meunierlcc-toulousefr
Where to find usLCC door CS012
205 route de Narbonne
When 9h to 12h - 14h to 17h30
From Monday to Friday
Some advice
22
Elemental Analysis C-H-NS - LCC
How to request an analysis
For any analysis request
Each sample must be supplied with an analysis request formavailable on LCC website
wwwlcc-toulousefr gt services gt services techniques ampscientifiques gt analyses chimiques gt Formulaire
Fill in electronically and send by mail (see framed who tocontact)
Samples
- Internal in my box DEPOT CHN in the mail locker analyseselementaires
- External ship by courrier to LCC service CHN or ask anappointment
Results
Results are sent by mail Samples are not returned
Analyses
Analyses are carried out every week
10 mg of compound areneeded for 2 essays andpackaged in a vial
Sensitive samples mustbe isolated in sealedampoule
For special analysisrequests please contactservice
Sulphur is analyzed oncea year if enoughdemand
Who to contact Isabelle BorgetTel 05 61 33 32 14
mail isabelleborgetlcc-toulousefr
Where to find service LCC door B038
205 route de Narbonne
When 9h to 11h30 - 14h to 16h30
From monday to friday
on appointment
Some advice
23
Nuclear Magnetic Resonance - LCC
How to request an analysis
bull For any analysis request (except self-service equipments)
For NMR equipments (400-solid and 600 MHz) analysisand appointment requests must be emailed to Y Coppelor C Bijani
The analysis request form can be loaded from the NMRfacility webpage on the LCC website (httplcc-toulousefr)
bull Self-service equipments
All the users have to follow a training conducted by NMRfacilityrsquos staff before any use of self-service spectrometers
- for LCC teams the training and NMR user accountrequests are provided with taking office
- for outside labs please contact the LCC personneldepartment
The requests when validated must be returned directlyto A Bonnet or D Paryl in order to plan the training
The users undertake to carefully respect the operatinginstructions and the LCC memos
All the data are automatically
- made available in the LCC teamsrsquo laquo Nuage raquo file
- emailed to the user from outside labs
Feel free to contact us for any question
about analysis capabilities or for
any discussion about the best strategy to
meet your specific issues
Who to contact
Yannick Coppel (Mgr)Christian BijaniTel 05 61 17 54 27
Antoine BonnetDavid Paryl
Tel 05 61 17 54 30Email yannickcoppellcc-
toulousefrchristianbijanilcc-toulousefrantoinebonnetlcc-toulousefr
davidparyllcc-toulousefr
Some advice
Where to find us
LCC RMN Building 205 route de Narbonne Toulouse
Door 030 (Y Coppel et C Bijani)
Door 033 (F Lacassin et D Paryl)
When8h30 to 11h30 -14h to 17h
From Monday to Friday
24
Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) - LCC
How to request an analysis
bull For any analysis request
Each sample must be supplied with an analysisrequest form To request this form please contact the staff
Sample amount depends on the concentration of chemical elements to be measured in the sampleanalyzed
In the very first request please contact the staff
bull Results
Results are delivered in the letter-box of the LCC team or for outside labs made available in the ICP departmentrsquos letter-box (within the LCC entrance hall)
bull Analyses schedule
Analyses are carried out every 2 weeks
In general 10 mg per assay isneeded (provided that the
concentration is above 5 ww)
Chemical elements currentlyanalyzed (but not limited) Ag Al Au B Ba Be Bi Ca Cd Co Cr Cu Fe Ir K Li Mg Mn Na
Ni P Pb Pd Pt Ru Rh Sr Zn
Who to contact
Alain Moreau Tel 0561175850
E-mail alainmoreaulcc-toulousefr
Where to find usIPBS Bacirct A3
205 route de Narbonne
When 8h to 11h30 - 14h to 16h30From Monday to Friday (odd
week)
Some advice
25
How to request an analysis
bull For all analysis requests on the 400 and 500 MHz NMR spectrometerssituated in the High Technology Module (MHT)Each sample must be accompanied by a fully completed laquo AnalysisRequest raquo form You can find this form on the ICT websiteictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsrmn oron the website of the NMR service (httprmn-webups-tlsefr)It is essential to make an appointment by email telephone or in personat the NMR service
bull For all analysis requests on the 300 MHz open access NMR spectrometerslocated in Building 2R1You must sign up to the NMR training before using the 300 MHz spectrometers (inscription form on the website of the NMR service httprmn-webups-tlsefr)
bull Follow the instructionsI ndash NMR Tubes
NMR tubes must meet a minimum standard of qualityBroken or damaged tubes and Economy tubes are forbidden from the service as they are too fragile
II ndash Cleaning tubes After the analysis the tubes must be washed as quickly as possible using the same solvent that was used to dissolve the analyte After several rinses the tube should be dried at room temperature or in an oven at less than 60degC
III ndash Filling the tubesFor an optimal measurement your tube should contain 600 microL of
solvent bull Results spectra can be recovered by
- downloading from the NMR server- USB stick- by email (only for 1 D analyses)
Once the analysis has been completed you must come to pick up yoursamples from the NMR service
The sensitivity of an NMR experiment depends on the
nucleus studied and the concentration of your product
If necessary during samplepreparation filter your solutions
in order to remove any suspendedsolids
The choice of solvent dependsprimarily on the solubility of your
product at room temperature
If there are several possibilities choose a solvent whose peaks do
not interfere with those of yourproduct
For more information please feelfree to contact the staff of the NMR
service
Who to contact
Marc Vedrenne (Msg)Pierre Lavedan
Steacutephane MassouCaroline ToppanClaude Andreu
Tel 05-61-55 ext 84-78 68-78Email rmnictchimieups-tlsefr
Where to find us Door 45 Ground floor High
Technology Module Universiteacute Paul Sabatier
When Monday to Friday
09h00-12h00 and 14h00-16h30
Some advice
NMR Service
copyFreacutedeacuteric MaligneICT
Mass spectrometry
How to request an analysis
bull For all analysis requests
Each sample must be accompanied by a fully completedanalysis request form You can find this form on the ICT website ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsspectrometrie-de-masse
You can also fill in all the administrative details one timeonly and save them for your future requests and you canarchive your forms
Bring the forms (preferably double-sided) and sample duringopening hours We will check with you the feasibility of theproposed analyses
bull For air-sensitive samples
Make an appointment
bull For LCMS and GCMS analyses
Make an appointment
bull How to collect your results
The results will be sent to you in pdf format Upon receivingour mail you can come and pick up your samples and formsduring opening hours
We will assess the feasibility of the
analysis with you
If you donrsquot know which method of ionization is
better suited for your molecules then leave it
blank and we will choose together
Who to contactCatherine Claparols ( Mgr)
Valeacuterie BourdonEric Leroy
Nathalie Martins-FromentTel 33 5 61 55 64 69Fax 33 5 61 55 81 16
Email spectromasseictups-tlsefr
Where to find us
Door 157 groundfloor building 2R1 Universiteacute Paul Sabatier
When
Monday-Friday 10h30-12h and 13h30-15h00
Some advice
8
copyFreacutedeacuteric MaligneICT
INFRARED Spectroscopy
How to request an analysis
bull For each analysis request
Each sample must be accompanied by a fully completedanalysis request form You can find this form on the ICT website ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsspectroscopies-infrarouge and on the door of the service
Required sample quantity 05 to 2 mg for powders 1drop for liquids 1ml for solutions (in this case you will alsoneed to supply 10-20 ml of pure solvent)
bull For infrared microscopy kinetics
Please make an appointment
bull For other analyses transmission ATR DRIFT far-IR NIR
Leave your sample at the service If unattended a box isavailable on the door to drop off your samples
bull Open access equipment for ATR analyses only
It can be used after completion of a 1h training course Makean appointment
All kinds of samples can beanalyzed solids liquids solutions blocks grains of
wheathellipyou just needto choose the right
method depending on your sample and your
study
Come and discuss with us
Extensive infrared and Raman tables and
spectral data bases are available at the
service60 000 data base spectra
are available
Who to contactCorinne Routaboul
Tel 05 61 55 64 00Email routabouictchimieups-tlsefr
Where to find us Door 1025 1st floor building 2R1
Universiteacute Paul Sabatier
When Monday-Friday 9h00-17h00
If unattended leave the sample in the deposit box on the door If youhave more than 10 samples or if you need particular techniques please make an appointment
Some advice
9
copyFreacutedeacuteric MaligneICT
TECHNOPOLYM
10
Technopolym
How to request an analysis
bull Request an analysis via the central Technopolym emailtechnopolymictchimieups-tlsefr
Following this email we will inform you about the proposedtechniques of analyse costs time of delivery requiredquantity of sample conditioning sample deposit Dependingon your expected results an appointment to discuss yourproblem may be proposed before scheduling an analysis
bull For all analysis requestsEach sample must be accompanied by a fully completed
analysis request form You can find this form on the ICT website
ictcnrsfrplateforme-de-licttechnopolym or on the Technopolym website
httptechnopolymups-tlsefr
bull For more information
Visit our website to know about our skills equipment references
TechnopolymIs a virtual technological
platform dedicated to the characterization of polymeric
materials
We propose a range of analytical techniques
molecularcharacterization phase
transitions thermal stability behavior in
solution mechanicalproperties surface characterizationhellip
Come and talk to us
Who to contactPascale Saint-Aguet
Tel 05 61 55 68 08Tel (LCC) 05 61 33 31 34
Email technopolymictchimieups-tlsefr
Some advice
Where to find us
Door 30233rd floor building 2R1 Universiteacute Paul Sabatier
Door G064 ndashLCC 205 rte de Narbonne -
When
Monday-Friday 9h-12h and
14h-17h
11
Cross-Platform Services
12
Documentation
How to make a request
bull For all document requests
You can request your document by email telephone or inperson Donrsquot forget to indicate your full name and laboratorywith the references on your request
bull Consultation and loans
The catalogue of the chemistry library is available on theintranet
ictcnrsfrdocchimie
Borrowing is possible during office hours ndash outside thesehours please make an appointment
bull For bibliographic searches and training
Make an appointment
bull Open access
You can come and work at the library ndash computers and wifi are available Visit our website
ictcnrsfrplateforme-de-lictservices-transversesaccueil-de-la-documentation
Ask the documentation service for your intranet
password from
Feel free to call the service for any problems
relating to the use of bibliographic databases
Who to contactDanielle Brunet
Tel 05 61 55 85 69Email brunetictchimieups-tlsefr
Some advice
Where to find us
Door 0145 ground floor building 2R1
Universiteacute Paul Sabatier
When
Mon-Fri 9h-12h and 14h-17h If unattended make an
appointment
13
Electronics
How to make a request
Who to contactJean-Michel Martin
Tel 05 61 55 86 93Email scicassistanceictchimieups-tlsefr
Email martinjmictchimieups-tlsefr
Feel free to ask the service for
- Modification of existingelectronic devices and
proposals for improvement
- Troubleshooting and repair of electronic
devices
- Advice on purchase of new material
bull For all installation andor maintenance of equipment with astrong electronic component
Send an email phone or contact the service in person duringoffice hours
bull For all service requests
Send an email toscicassistanceictchimieups-tlsefrstating your name office number and a brief description of the problem
bull Loan of equipment
To address the needs of users specific equipment is availablein the electronics workshop (Oscilloscope component testerssoldering ironhellip) aswell as various tools
It is possible to borrow this equipment
Where to find usDoor 1015 1st floor building 2R1 Universiteacute Paul Sabatier
When Monday-Friday office hours
If unattended make an appointment
Some advice
14
Information Technology
How to make a request
bull For all requests for connection to the network andcreation of email accounts
First see the secretary of your laboratory
bull For all service requests
Write toscicassistanceictchimieups-tlsefr
stating your name office number and a brief description of the problem
The IT service manages developsand maintains the
network and associated services
Please contact us for more information on
the services provided (automatic
backup of data access to Cambridge CCDC data sharing
etc)
Who to contactPascal Puech
Edouard IvanovtchikTel 05 61 55 68 73
Email scicassistanceictchimieups-tlsefr
Some advice
Where to find usDoor 168 ground floor building 2R1
Universiteacute Paul Sabatier
WhenMonday-Friday office hours
If unattended make an appointment
15
Scientific Glassware
How to make a request
bull For all service requests
All glassware to repair or construct must be accompanied bya fully completed form You can find this form on the ICTwebsite ictcnrsfrVerrerie-scientifique
For obvious reasons of safety and hygiene glassware must beclean free of silicon grease and in a container identified withthe name of the research group
bull Do I need to go in person
In person contact is preferred if you are new to glasswork andif your request is complex
Photos et technical drawings sent by email are onlycomplementary information as in isolation they can lead tomisunderstandings and errors
For all glass repairs construction of new
equipment or prototyping
feel free to consult the glassware service
We can provide technicaladvice as well as contacts
in specialized domains
Who to contactSteacutephane Foulon
Tel 05 61 55 61 16Email foulonictchimieups-
tlsefr
Some advice
Where to find us
Door 0194 Ground Floor Building 2R1Universiteacute Paul
Sabatier
When
Monday-Friday during office hours We recommend that
external users make an appointment
16
copyFreacutedeacuteric MaligneICT
LCC Services
17
Thermal Analyses LCC
How to request an analysis
bull For any analysis request
DTATGA or DSC analyses each sample must be suppliedwith an analysis request form duly filled out To requestthese forms please contact the staff by e-mail
In the very first request please contact the staff fordetails about the process the sample amount requiredthe packaging of samples etc
In all other cases the analyses requests and the samplescan be deposited in the Thermal Analyses Departmentrsquosletter-box (within the LCC entrance hall)
bull Air-sensitive samples
Make an appointment with the staff
bull Results
Analyses results are emailed as a text file paper copy isavailable upon request
On completion of analyses remaining of samples must bepick up at LCC
Analytical Equipments
DTATGA for measuring the mass variation as a
function of temperature
DSC for detecting the phase changes without mass loss
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 1 0Email j-fmeunierlcc-toulousefr
Some advice
Where to find usLCC - Door CS12 basement level
205 route de Narbonne
When Opening hours 9h to 11h30 - 14h to 17hfrom Monday to Friday except on wednesday
18
Library Resource Center LCC
How to make a request
bull For any information request
- LCC research teams fill out the request form available onthe LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs contact the staff by e-mail
bull For bibliographical searches and access
Digital databases
- LCC research teams bibliographical searches databases areavailable on the LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs make an appointment with the staff
Paper print collections
Paperprint collections also are available and can be read in thelibrary premises
LCCrsquos Library access is free for LCC teams and subject to anappointment for outside labs
LCC teams Access to the LCC intranet is provided
with taking office
For further information feel free to contact us
Who to contact
Marie-Heacutelegravene Gullimarie-helenegullilcc-toulousefr
0561333217
Gilles Roujasgillesroujaslcc-toulousefr
0561333140
Gaeumltan Havetgaetanhavetlcc-toulousefr
0561333140
Some advice
Where to find usLCC 205 route de Narbonne
When Opening hours
9 h to 11h30 - 13h to 17h From Monday to Friday
19
Feel free to contact us for anyquestion about analyses
options or for anydiscussion about the
best strategy to meetyour specific issues
Single ndashcrystal and powder X-Ray Diffraction - LCC
How to request an analysis
bull Prior to any analysis
Contact the staff in charge of X-Ray Diffraction measurementsfor your team or your lab
bull Single-crystal X-ray diffraction
First the staff will evaluate the quality of the sample If quality isacceptable for a X-ray diffraction measurement an appointmentwill be set up for analysis
Following information must be provided expected compound used solvents any specific information concerning the sample(air-sensitive thermal-sensitive light-sensitivehellip) analysis and required data (absolute configuration hydride locationhellip)
bull Powder X-ray diffraction
Appointments are proposed in accordance with the type of measurement (reflection capillary measurements at variable temperatures x-ray grazing incidence on thin films)
Following information must be provided sample characteristics analytical conditions (scanning range of 2theta temperaturehellip) required data (phase identification crystallites sizehellip)
Useful tips Until getting staff opinion about the quality of yoursample particularly for a single-crystal handle it as little as possible
Who to contact Laure Vendier (Mgr)
Carine DuhayonSonia Mallet-Ladeira
Tel 05 61 33 31 18Email laurevendierlcc-toulousefr
carineduhayonlcc-toulousefrladeiraictchimieups-tlsefr
Some advice
Where to find us
LCC 205 route de NarbonneX-Ray Diffraction office ground floor door B017 X-Ray Diffraction Lab basement level door GS66
When
9h to 11h30 - 14h to 17hFrom Monday to Friday except on Wednesday afternoon
20
Electrochemistry - LCC
How to request an analysis
bull For any analysis request
Analyses are carried out by appointment onlyscheduled with the staff when requesting theanalysis
On the appointed date Bring the sample and the solvent Your presence is required during the analyses
bull Sample preparation
The sample(s) must be as pure as possible correspondingto a concentration of 10-3 molL-1 in 10 mL
For each sample bring 30 mL of purified solvent
bull Results
On completion of the analyses the mostrepresentative curves are provided in paper copy
Upon request the electronic files can be emailed
Who to contactAlix Sournia-Saquet (Mgr)
Alain MoreauTel 05 61 33 31 75
Email alixsaquetlcc-toulousefralainmoreaulcc-toulousefr
Some advice
Before any analysis feel free to contact us for any
discussion or question about feasibility and conditions of
analyses
The staff can help you
- to choose the best-suited technique to your needs
- for interpretation of your data
Where to find us LCC- door B015ndash ground floor-building B205 route de Narbonne
When 9h to 11h30 -14h to 17h
From Monday to Friday
21
Magnetic Measurement and Moumlssbauer spectroscopy - LCC
How to request an analysis
bull For any analysis request
For magnetic measurements SQUID andMoumlssbauer spectroscopy please contact Jean-Franccedilois Meunier by e-mail or phone
An appointment will be set up in order to studyyour analyses requests and to define theexperimental conditions
An analysis request form will be provided by thestaff
bull Results and samples
Results are emailed as text and excel files
On completion of the analyses samples must beretrieved at LCC
Further information on equipments
lcc-toulousefrServices Spectroscopie Moumlssbauer
Lcc-toulousefr
servicesMesures
Magneacutetiques
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 10Email Jf-meunierlcc-toulousefr
Where to find usLCC door CS012
205 route de Narbonne
When 9h to 12h - 14h to 17h30
From Monday to Friday
Some advice
22
Elemental Analysis C-H-NS - LCC
How to request an analysis
For any analysis request
Each sample must be supplied with an analysis request formavailable on LCC website
wwwlcc-toulousefr gt services gt services techniques ampscientifiques gt analyses chimiques gt Formulaire
Fill in electronically and send by mail (see framed who tocontact)
Samples
- Internal in my box DEPOT CHN in the mail locker analyseselementaires
- External ship by courrier to LCC service CHN or ask anappointment
Results
Results are sent by mail Samples are not returned
Analyses
Analyses are carried out every week
10 mg of compound areneeded for 2 essays andpackaged in a vial
Sensitive samples mustbe isolated in sealedampoule
For special analysisrequests please contactservice
Sulphur is analyzed oncea year if enoughdemand
Who to contact Isabelle BorgetTel 05 61 33 32 14
mail isabelleborgetlcc-toulousefr
Where to find service LCC door B038
205 route de Narbonne
When 9h to 11h30 - 14h to 16h30
From monday to friday
on appointment
Some advice
23
Nuclear Magnetic Resonance - LCC
How to request an analysis
bull For any analysis request (except self-service equipments)
For NMR equipments (400-solid and 600 MHz) analysisand appointment requests must be emailed to Y Coppelor C Bijani
The analysis request form can be loaded from the NMRfacility webpage on the LCC website (httplcc-toulousefr)
bull Self-service equipments
All the users have to follow a training conducted by NMRfacilityrsquos staff before any use of self-service spectrometers
- for LCC teams the training and NMR user accountrequests are provided with taking office
- for outside labs please contact the LCC personneldepartment
The requests when validated must be returned directlyto A Bonnet or D Paryl in order to plan the training
The users undertake to carefully respect the operatinginstructions and the LCC memos
All the data are automatically
- made available in the LCC teamsrsquo laquo Nuage raquo file
- emailed to the user from outside labs
Feel free to contact us for any question
about analysis capabilities or for
any discussion about the best strategy to
meet your specific issues
Who to contact
Yannick Coppel (Mgr)Christian BijaniTel 05 61 17 54 27
Antoine BonnetDavid Paryl
Tel 05 61 17 54 30Email yannickcoppellcc-
toulousefrchristianbijanilcc-toulousefrantoinebonnetlcc-toulousefr
davidparyllcc-toulousefr
Some advice
Where to find us
LCC RMN Building 205 route de Narbonne Toulouse
Door 030 (Y Coppel et C Bijani)
Door 033 (F Lacassin et D Paryl)
When8h30 to 11h30 -14h to 17h
From Monday to Friday
24
Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) - LCC
How to request an analysis
bull For any analysis request
Each sample must be supplied with an analysisrequest form To request this form please contact the staff
Sample amount depends on the concentration of chemical elements to be measured in the sampleanalyzed
In the very first request please contact the staff
bull Results
Results are delivered in the letter-box of the LCC team or for outside labs made available in the ICP departmentrsquos letter-box (within the LCC entrance hall)
bull Analyses schedule
Analyses are carried out every 2 weeks
In general 10 mg per assay isneeded (provided that the
concentration is above 5 ww)
Chemical elements currentlyanalyzed (but not limited) Ag Al Au B Ba Be Bi Ca Cd Co Cr Cu Fe Ir K Li Mg Mn Na
Ni P Pb Pd Pt Ru Rh Sr Zn
Who to contact
Alain Moreau Tel 0561175850
E-mail alainmoreaulcc-toulousefr
Where to find usIPBS Bacirct A3
205 route de Narbonne
When 8h to 11h30 - 14h to 16h30From Monday to Friday (odd
week)
Some advice
25
Mass spectrometry
How to request an analysis
bull For all analysis requests
Each sample must be accompanied by a fully completedanalysis request form You can find this form on the ICT website ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsspectrometrie-de-masse
You can also fill in all the administrative details one timeonly and save them for your future requests and you canarchive your forms
Bring the forms (preferably double-sided) and sample duringopening hours We will check with you the feasibility of theproposed analyses
bull For air-sensitive samples
Make an appointment
bull For LCMS and GCMS analyses
Make an appointment
bull How to collect your results
The results will be sent to you in pdf format Upon receivingour mail you can come and pick up your samples and formsduring opening hours
We will assess the feasibility of the
analysis with you
If you donrsquot know which method of ionization is
better suited for your molecules then leave it
blank and we will choose together
Who to contactCatherine Claparols ( Mgr)
Valeacuterie BourdonEric Leroy
Nathalie Martins-FromentTel 33 5 61 55 64 69Fax 33 5 61 55 81 16
Email spectromasseictups-tlsefr
Where to find us
Door 157 groundfloor building 2R1 Universiteacute Paul Sabatier
When
Monday-Friday 10h30-12h and 13h30-15h00
Some advice
8
copyFreacutedeacuteric MaligneICT
INFRARED Spectroscopy
How to request an analysis
bull For each analysis request
Each sample must be accompanied by a fully completedanalysis request form You can find this form on the ICT website ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsspectroscopies-infrarouge and on the door of the service
Required sample quantity 05 to 2 mg for powders 1drop for liquids 1ml for solutions (in this case you will alsoneed to supply 10-20 ml of pure solvent)
bull For infrared microscopy kinetics
Please make an appointment
bull For other analyses transmission ATR DRIFT far-IR NIR
Leave your sample at the service If unattended a box isavailable on the door to drop off your samples
bull Open access equipment for ATR analyses only
It can be used after completion of a 1h training course Makean appointment
All kinds of samples can beanalyzed solids liquids solutions blocks grains of
wheathellipyou just needto choose the right
method depending on your sample and your
study
Come and discuss with us
Extensive infrared and Raman tables and
spectral data bases are available at the
service60 000 data base spectra
are available
Who to contactCorinne Routaboul
Tel 05 61 55 64 00Email routabouictchimieups-tlsefr
Where to find us Door 1025 1st floor building 2R1
Universiteacute Paul Sabatier
When Monday-Friday 9h00-17h00
If unattended leave the sample in the deposit box on the door If youhave more than 10 samples or if you need particular techniques please make an appointment
Some advice
9
copyFreacutedeacuteric MaligneICT
TECHNOPOLYM
10
Technopolym
How to request an analysis
bull Request an analysis via the central Technopolym emailtechnopolymictchimieups-tlsefr
Following this email we will inform you about the proposedtechniques of analyse costs time of delivery requiredquantity of sample conditioning sample deposit Dependingon your expected results an appointment to discuss yourproblem may be proposed before scheduling an analysis
bull For all analysis requestsEach sample must be accompanied by a fully completed
analysis request form You can find this form on the ICT website
ictcnrsfrplateforme-de-licttechnopolym or on the Technopolym website
httptechnopolymups-tlsefr
bull For more information
Visit our website to know about our skills equipment references
TechnopolymIs a virtual technological
platform dedicated to the characterization of polymeric
materials
We propose a range of analytical techniques
molecularcharacterization phase
transitions thermal stability behavior in
solution mechanicalproperties surface characterizationhellip
Come and talk to us
Who to contactPascale Saint-Aguet
Tel 05 61 55 68 08Tel (LCC) 05 61 33 31 34
Email technopolymictchimieups-tlsefr
Some advice
Where to find us
Door 30233rd floor building 2R1 Universiteacute Paul Sabatier
Door G064 ndashLCC 205 rte de Narbonne -
When
Monday-Friday 9h-12h and
14h-17h
11
Cross-Platform Services
12
Documentation
How to make a request
bull For all document requests
You can request your document by email telephone or inperson Donrsquot forget to indicate your full name and laboratorywith the references on your request
bull Consultation and loans
The catalogue of the chemistry library is available on theintranet
ictcnrsfrdocchimie
Borrowing is possible during office hours ndash outside thesehours please make an appointment
bull For bibliographic searches and training
Make an appointment
bull Open access
You can come and work at the library ndash computers and wifi are available Visit our website
ictcnrsfrplateforme-de-lictservices-transversesaccueil-de-la-documentation
Ask the documentation service for your intranet
password from
Feel free to call the service for any problems
relating to the use of bibliographic databases
Who to contactDanielle Brunet
Tel 05 61 55 85 69Email brunetictchimieups-tlsefr
Some advice
Where to find us
Door 0145 ground floor building 2R1
Universiteacute Paul Sabatier
When
Mon-Fri 9h-12h and 14h-17h If unattended make an
appointment
13
Electronics
How to make a request
Who to contactJean-Michel Martin
Tel 05 61 55 86 93Email scicassistanceictchimieups-tlsefr
Email martinjmictchimieups-tlsefr
Feel free to ask the service for
- Modification of existingelectronic devices and
proposals for improvement
- Troubleshooting and repair of electronic
devices
- Advice on purchase of new material
bull For all installation andor maintenance of equipment with astrong electronic component
Send an email phone or contact the service in person duringoffice hours
bull For all service requests
Send an email toscicassistanceictchimieups-tlsefrstating your name office number and a brief description of the problem
bull Loan of equipment
To address the needs of users specific equipment is availablein the electronics workshop (Oscilloscope component testerssoldering ironhellip) aswell as various tools
It is possible to borrow this equipment
Where to find usDoor 1015 1st floor building 2R1 Universiteacute Paul Sabatier
When Monday-Friday office hours
If unattended make an appointment
Some advice
14
Information Technology
How to make a request
bull For all requests for connection to the network andcreation of email accounts
First see the secretary of your laboratory
bull For all service requests
Write toscicassistanceictchimieups-tlsefr
stating your name office number and a brief description of the problem
The IT service manages developsand maintains the
network and associated services
Please contact us for more information on
the services provided (automatic
backup of data access to Cambridge CCDC data sharing
etc)
Who to contactPascal Puech
Edouard IvanovtchikTel 05 61 55 68 73
Email scicassistanceictchimieups-tlsefr
Some advice
Where to find usDoor 168 ground floor building 2R1
Universiteacute Paul Sabatier
WhenMonday-Friday office hours
If unattended make an appointment
15
Scientific Glassware
How to make a request
bull For all service requests
All glassware to repair or construct must be accompanied bya fully completed form You can find this form on the ICTwebsite ictcnrsfrVerrerie-scientifique
For obvious reasons of safety and hygiene glassware must beclean free of silicon grease and in a container identified withthe name of the research group
bull Do I need to go in person
In person contact is preferred if you are new to glasswork andif your request is complex
Photos et technical drawings sent by email are onlycomplementary information as in isolation they can lead tomisunderstandings and errors
For all glass repairs construction of new
equipment or prototyping
feel free to consult the glassware service
We can provide technicaladvice as well as contacts
in specialized domains
Who to contactSteacutephane Foulon
Tel 05 61 55 61 16Email foulonictchimieups-
tlsefr
Some advice
Where to find us
Door 0194 Ground Floor Building 2R1Universiteacute Paul
Sabatier
When
Monday-Friday during office hours We recommend that
external users make an appointment
16
copyFreacutedeacuteric MaligneICT
LCC Services
17
Thermal Analyses LCC
How to request an analysis
bull For any analysis request
DTATGA or DSC analyses each sample must be suppliedwith an analysis request form duly filled out To requestthese forms please contact the staff by e-mail
In the very first request please contact the staff fordetails about the process the sample amount requiredthe packaging of samples etc
In all other cases the analyses requests and the samplescan be deposited in the Thermal Analyses Departmentrsquosletter-box (within the LCC entrance hall)
bull Air-sensitive samples
Make an appointment with the staff
bull Results
Analyses results are emailed as a text file paper copy isavailable upon request
On completion of analyses remaining of samples must bepick up at LCC
Analytical Equipments
DTATGA for measuring the mass variation as a
function of temperature
DSC for detecting the phase changes without mass loss
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 1 0Email j-fmeunierlcc-toulousefr
Some advice
Where to find usLCC - Door CS12 basement level
205 route de Narbonne
When Opening hours 9h to 11h30 - 14h to 17hfrom Monday to Friday except on wednesday
18
Library Resource Center LCC
How to make a request
bull For any information request
- LCC research teams fill out the request form available onthe LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs contact the staff by e-mail
bull For bibliographical searches and access
Digital databases
- LCC research teams bibliographical searches databases areavailable on the LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs make an appointment with the staff
Paper print collections
Paperprint collections also are available and can be read in thelibrary premises
LCCrsquos Library access is free for LCC teams and subject to anappointment for outside labs
LCC teams Access to the LCC intranet is provided
with taking office
For further information feel free to contact us
Who to contact
Marie-Heacutelegravene Gullimarie-helenegullilcc-toulousefr
0561333217
Gilles Roujasgillesroujaslcc-toulousefr
0561333140
Gaeumltan Havetgaetanhavetlcc-toulousefr
0561333140
Some advice
Where to find usLCC 205 route de Narbonne
When Opening hours
9 h to 11h30 - 13h to 17h From Monday to Friday
19
Feel free to contact us for anyquestion about analyses
options or for anydiscussion about the
best strategy to meetyour specific issues
Single ndashcrystal and powder X-Ray Diffraction - LCC
How to request an analysis
bull Prior to any analysis
Contact the staff in charge of X-Ray Diffraction measurementsfor your team or your lab
bull Single-crystal X-ray diffraction
First the staff will evaluate the quality of the sample If quality isacceptable for a X-ray diffraction measurement an appointmentwill be set up for analysis
Following information must be provided expected compound used solvents any specific information concerning the sample(air-sensitive thermal-sensitive light-sensitivehellip) analysis and required data (absolute configuration hydride locationhellip)
bull Powder X-ray diffraction
Appointments are proposed in accordance with the type of measurement (reflection capillary measurements at variable temperatures x-ray grazing incidence on thin films)
Following information must be provided sample characteristics analytical conditions (scanning range of 2theta temperaturehellip) required data (phase identification crystallites sizehellip)
Useful tips Until getting staff opinion about the quality of yoursample particularly for a single-crystal handle it as little as possible
Who to contact Laure Vendier (Mgr)
Carine DuhayonSonia Mallet-Ladeira
Tel 05 61 33 31 18Email laurevendierlcc-toulousefr
carineduhayonlcc-toulousefrladeiraictchimieups-tlsefr
Some advice
Where to find us
LCC 205 route de NarbonneX-Ray Diffraction office ground floor door B017 X-Ray Diffraction Lab basement level door GS66
When
9h to 11h30 - 14h to 17hFrom Monday to Friday except on Wednesday afternoon
20
Electrochemistry - LCC
How to request an analysis
bull For any analysis request
Analyses are carried out by appointment onlyscheduled with the staff when requesting theanalysis
On the appointed date Bring the sample and the solvent Your presence is required during the analyses
bull Sample preparation
The sample(s) must be as pure as possible correspondingto a concentration of 10-3 molL-1 in 10 mL
For each sample bring 30 mL of purified solvent
bull Results
On completion of the analyses the mostrepresentative curves are provided in paper copy
Upon request the electronic files can be emailed
Who to contactAlix Sournia-Saquet (Mgr)
Alain MoreauTel 05 61 33 31 75
Email alixsaquetlcc-toulousefralainmoreaulcc-toulousefr
Some advice
Before any analysis feel free to contact us for any
discussion or question about feasibility and conditions of
analyses
The staff can help you
- to choose the best-suited technique to your needs
- for interpretation of your data
Where to find us LCC- door B015ndash ground floor-building B205 route de Narbonne
When 9h to 11h30 -14h to 17h
From Monday to Friday
21
Magnetic Measurement and Moumlssbauer spectroscopy - LCC
How to request an analysis
bull For any analysis request
For magnetic measurements SQUID andMoumlssbauer spectroscopy please contact Jean-Franccedilois Meunier by e-mail or phone
An appointment will be set up in order to studyyour analyses requests and to define theexperimental conditions
An analysis request form will be provided by thestaff
bull Results and samples
Results are emailed as text and excel files
On completion of the analyses samples must beretrieved at LCC
Further information on equipments
lcc-toulousefrServices Spectroscopie Moumlssbauer
Lcc-toulousefr
servicesMesures
Magneacutetiques
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 10Email Jf-meunierlcc-toulousefr
Where to find usLCC door CS012
205 route de Narbonne
When 9h to 12h - 14h to 17h30
From Monday to Friday
Some advice
22
Elemental Analysis C-H-NS - LCC
How to request an analysis
For any analysis request
Each sample must be supplied with an analysis request formavailable on LCC website
wwwlcc-toulousefr gt services gt services techniques ampscientifiques gt analyses chimiques gt Formulaire
Fill in electronically and send by mail (see framed who tocontact)
Samples
- Internal in my box DEPOT CHN in the mail locker analyseselementaires
- External ship by courrier to LCC service CHN or ask anappointment
Results
Results are sent by mail Samples are not returned
Analyses
Analyses are carried out every week
10 mg of compound areneeded for 2 essays andpackaged in a vial
Sensitive samples mustbe isolated in sealedampoule
For special analysisrequests please contactservice
Sulphur is analyzed oncea year if enoughdemand
Who to contact Isabelle BorgetTel 05 61 33 32 14
mail isabelleborgetlcc-toulousefr
Where to find service LCC door B038
205 route de Narbonne
When 9h to 11h30 - 14h to 16h30
From monday to friday
on appointment
Some advice
23
Nuclear Magnetic Resonance - LCC
How to request an analysis
bull For any analysis request (except self-service equipments)
For NMR equipments (400-solid and 600 MHz) analysisand appointment requests must be emailed to Y Coppelor C Bijani
The analysis request form can be loaded from the NMRfacility webpage on the LCC website (httplcc-toulousefr)
bull Self-service equipments
All the users have to follow a training conducted by NMRfacilityrsquos staff before any use of self-service spectrometers
- for LCC teams the training and NMR user accountrequests are provided with taking office
- for outside labs please contact the LCC personneldepartment
The requests when validated must be returned directlyto A Bonnet or D Paryl in order to plan the training
The users undertake to carefully respect the operatinginstructions and the LCC memos
All the data are automatically
- made available in the LCC teamsrsquo laquo Nuage raquo file
- emailed to the user from outside labs
Feel free to contact us for any question
about analysis capabilities or for
any discussion about the best strategy to
meet your specific issues
Who to contact
Yannick Coppel (Mgr)Christian BijaniTel 05 61 17 54 27
Antoine BonnetDavid Paryl
Tel 05 61 17 54 30Email yannickcoppellcc-
toulousefrchristianbijanilcc-toulousefrantoinebonnetlcc-toulousefr
davidparyllcc-toulousefr
Some advice
Where to find us
LCC RMN Building 205 route de Narbonne Toulouse
Door 030 (Y Coppel et C Bijani)
Door 033 (F Lacassin et D Paryl)
When8h30 to 11h30 -14h to 17h
From Monday to Friday
24
Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) - LCC
How to request an analysis
bull For any analysis request
Each sample must be supplied with an analysisrequest form To request this form please contact the staff
Sample amount depends on the concentration of chemical elements to be measured in the sampleanalyzed
In the very first request please contact the staff
bull Results
Results are delivered in the letter-box of the LCC team or for outside labs made available in the ICP departmentrsquos letter-box (within the LCC entrance hall)
bull Analyses schedule
Analyses are carried out every 2 weeks
In general 10 mg per assay isneeded (provided that the
concentration is above 5 ww)
Chemical elements currentlyanalyzed (but not limited) Ag Al Au B Ba Be Bi Ca Cd Co Cr Cu Fe Ir K Li Mg Mn Na
Ni P Pb Pd Pt Ru Rh Sr Zn
Who to contact
Alain Moreau Tel 0561175850
E-mail alainmoreaulcc-toulousefr
Where to find usIPBS Bacirct A3
205 route de Narbonne
When 8h to 11h30 - 14h to 16h30From Monday to Friday (odd
week)
Some advice
25
INFRARED Spectroscopy
How to request an analysis
bull For each analysis request
Each sample must be accompanied by a fully completedanalysis request form You can find this form on the ICT website ictcnrsfrplateforme-de-lictcaracterisation-purification-site-upsspectroscopies-infrarouge and on the door of the service
Required sample quantity 05 to 2 mg for powders 1drop for liquids 1ml for solutions (in this case you will alsoneed to supply 10-20 ml of pure solvent)
bull For infrared microscopy kinetics
Please make an appointment
bull For other analyses transmission ATR DRIFT far-IR NIR
Leave your sample at the service If unattended a box isavailable on the door to drop off your samples
bull Open access equipment for ATR analyses only
It can be used after completion of a 1h training course Makean appointment
All kinds of samples can beanalyzed solids liquids solutions blocks grains of
wheathellipyou just needto choose the right
method depending on your sample and your
study
Come and discuss with us
Extensive infrared and Raman tables and
spectral data bases are available at the
service60 000 data base spectra
are available
Who to contactCorinne Routaboul
Tel 05 61 55 64 00Email routabouictchimieups-tlsefr
Where to find us Door 1025 1st floor building 2R1
Universiteacute Paul Sabatier
When Monday-Friday 9h00-17h00
If unattended leave the sample in the deposit box on the door If youhave more than 10 samples or if you need particular techniques please make an appointment
Some advice
9
copyFreacutedeacuteric MaligneICT
TECHNOPOLYM
10
Technopolym
How to request an analysis
bull Request an analysis via the central Technopolym emailtechnopolymictchimieups-tlsefr
Following this email we will inform you about the proposedtechniques of analyse costs time of delivery requiredquantity of sample conditioning sample deposit Dependingon your expected results an appointment to discuss yourproblem may be proposed before scheduling an analysis
bull For all analysis requestsEach sample must be accompanied by a fully completed
analysis request form You can find this form on the ICT website
ictcnrsfrplateforme-de-licttechnopolym or on the Technopolym website
httptechnopolymups-tlsefr
bull For more information
Visit our website to know about our skills equipment references
TechnopolymIs a virtual technological
platform dedicated to the characterization of polymeric
materials
We propose a range of analytical techniques
molecularcharacterization phase
transitions thermal stability behavior in
solution mechanicalproperties surface characterizationhellip
Come and talk to us
Who to contactPascale Saint-Aguet
Tel 05 61 55 68 08Tel (LCC) 05 61 33 31 34
Email technopolymictchimieups-tlsefr
Some advice
Where to find us
Door 30233rd floor building 2R1 Universiteacute Paul Sabatier
Door G064 ndashLCC 205 rte de Narbonne -
When
Monday-Friday 9h-12h and
14h-17h
11
Cross-Platform Services
12
Documentation
How to make a request
bull For all document requests
You can request your document by email telephone or inperson Donrsquot forget to indicate your full name and laboratorywith the references on your request
bull Consultation and loans
The catalogue of the chemistry library is available on theintranet
ictcnrsfrdocchimie
Borrowing is possible during office hours ndash outside thesehours please make an appointment
bull For bibliographic searches and training
Make an appointment
bull Open access
You can come and work at the library ndash computers and wifi are available Visit our website
ictcnrsfrplateforme-de-lictservices-transversesaccueil-de-la-documentation
Ask the documentation service for your intranet
password from
Feel free to call the service for any problems
relating to the use of bibliographic databases
Who to contactDanielle Brunet
Tel 05 61 55 85 69Email brunetictchimieups-tlsefr
Some advice
Where to find us
Door 0145 ground floor building 2R1
Universiteacute Paul Sabatier
When
Mon-Fri 9h-12h and 14h-17h If unattended make an
appointment
13
Electronics
How to make a request
Who to contactJean-Michel Martin
Tel 05 61 55 86 93Email scicassistanceictchimieups-tlsefr
Email martinjmictchimieups-tlsefr
Feel free to ask the service for
- Modification of existingelectronic devices and
proposals for improvement
- Troubleshooting and repair of electronic
devices
- Advice on purchase of new material
bull For all installation andor maintenance of equipment with astrong electronic component
Send an email phone or contact the service in person duringoffice hours
bull For all service requests
Send an email toscicassistanceictchimieups-tlsefrstating your name office number and a brief description of the problem
bull Loan of equipment
To address the needs of users specific equipment is availablein the electronics workshop (Oscilloscope component testerssoldering ironhellip) aswell as various tools
It is possible to borrow this equipment
Where to find usDoor 1015 1st floor building 2R1 Universiteacute Paul Sabatier
When Monday-Friday office hours
If unattended make an appointment
Some advice
14
Information Technology
How to make a request
bull For all requests for connection to the network andcreation of email accounts
First see the secretary of your laboratory
bull For all service requests
Write toscicassistanceictchimieups-tlsefr
stating your name office number and a brief description of the problem
The IT service manages developsand maintains the
network and associated services
Please contact us for more information on
the services provided (automatic
backup of data access to Cambridge CCDC data sharing
etc)
Who to contactPascal Puech
Edouard IvanovtchikTel 05 61 55 68 73
Email scicassistanceictchimieups-tlsefr
Some advice
Where to find usDoor 168 ground floor building 2R1
Universiteacute Paul Sabatier
WhenMonday-Friday office hours
If unattended make an appointment
15
Scientific Glassware
How to make a request
bull For all service requests
All glassware to repair or construct must be accompanied bya fully completed form You can find this form on the ICTwebsite ictcnrsfrVerrerie-scientifique
For obvious reasons of safety and hygiene glassware must beclean free of silicon grease and in a container identified withthe name of the research group
bull Do I need to go in person
In person contact is preferred if you are new to glasswork andif your request is complex
Photos et technical drawings sent by email are onlycomplementary information as in isolation they can lead tomisunderstandings and errors
For all glass repairs construction of new
equipment or prototyping
feel free to consult the glassware service
We can provide technicaladvice as well as contacts
in specialized domains
Who to contactSteacutephane Foulon
Tel 05 61 55 61 16Email foulonictchimieups-
tlsefr
Some advice
Where to find us
Door 0194 Ground Floor Building 2R1Universiteacute Paul
Sabatier
When
Monday-Friday during office hours We recommend that
external users make an appointment
16
copyFreacutedeacuteric MaligneICT
LCC Services
17
Thermal Analyses LCC
How to request an analysis
bull For any analysis request
DTATGA or DSC analyses each sample must be suppliedwith an analysis request form duly filled out To requestthese forms please contact the staff by e-mail
In the very first request please contact the staff fordetails about the process the sample amount requiredthe packaging of samples etc
In all other cases the analyses requests and the samplescan be deposited in the Thermal Analyses Departmentrsquosletter-box (within the LCC entrance hall)
bull Air-sensitive samples
Make an appointment with the staff
bull Results
Analyses results are emailed as a text file paper copy isavailable upon request
On completion of analyses remaining of samples must bepick up at LCC
Analytical Equipments
DTATGA for measuring the mass variation as a
function of temperature
DSC for detecting the phase changes without mass loss
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 1 0Email j-fmeunierlcc-toulousefr
Some advice
Where to find usLCC - Door CS12 basement level
205 route de Narbonne
When Opening hours 9h to 11h30 - 14h to 17hfrom Monday to Friday except on wednesday
18
Library Resource Center LCC
How to make a request
bull For any information request
- LCC research teams fill out the request form available onthe LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs contact the staff by e-mail
bull For bibliographical searches and access
Digital databases
- LCC research teams bibliographical searches databases areavailable on the LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs make an appointment with the staff
Paper print collections
Paperprint collections also are available and can be read in thelibrary premises
LCCrsquos Library access is free for LCC teams and subject to anappointment for outside labs
LCC teams Access to the LCC intranet is provided
with taking office
For further information feel free to contact us
Who to contact
Marie-Heacutelegravene Gullimarie-helenegullilcc-toulousefr
0561333217
Gilles Roujasgillesroujaslcc-toulousefr
0561333140
Gaeumltan Havetgaetanhavetlcc-toulousefr
0561333140
Some advice
Where to find usLCC 205 route de Narbonne
When Opening hours
9 h to 11h30 - 13h to 17h From Monday to Friday
19
Feel free to contact us for anyquestion about analyses
options or for anydiscussion about the
best strategy to meetyour specific issues
Single ndashcrystal and powder X-Ray Diffraction - LCC
How to request an analysis
bull Prior to any analysis
Contact the staff in charge of X-Ray Diffraction measurementsfor your team or your lab
bull Single-crystal X-ray diffraction
First the staff will evaluate the quality of the sample If quality isacceptable for a X-ray diffraction measurement an appointmentwill be set up for analysis
Following information must be provided expected compound used solvents any specific information concerning the sample(air-sensitive thermal-sensitive light-sensitivehellip) analysis and required data (absolute configuration hydride locationhellip)
bull Powder X-ray diffraction
Appointments are proposed in accordance with the type of measurement (reflection capillary measurements at variable temperatures x-ray grazing incidence on thin films)
Following information must be provided sample characteristics analytical conditions (scanning range of 2theta temperaturehellip) required data (phase identification crystallites sizehellip)
Useful tips Until getting staff opinion about the quality of yoursample particularly for a single-crystal handle it as little as possible
Who to contact Laure Vendier (Mgr)
Carine DuhayonSonia Mallet-Ladeira
Tel 05 61 33 31 18Email laurevendierlcc-toulousefr
carineduhayonlcc-toulousefrladeiraictchimieups-tlsefr
Some advice
Where to find us
LCC 205 route de NarbonneX-Ray Diffraction office ground floor door B017 X-Ray Diffraction Lab basement level door GS66
When
9h to 11h30 - 14h to 17hFrom Monday to Friday except on Wednesday afternoon
20
Electrochemistry - LCC
How to request an analysis
bull For any analysis request
Analyses are carried out by appointment onlyscheduled with the staff when requesting theanalysis
On the appointed date Bring the sample and the solvent Your presence is required during the analyses
bull Sample preparation
The sample(s) must be as pure as possible correspondingto a concentration of 10-3 molL-1 in 10 mL
For each sample bring 30 mL of purified solvent
bull Results
On completion of the analyses the mostrepresentative curves are provided in paper copy
Upon request the electronic files can be emailed
Who to contactAlix Sournia-Saquet (Mgr)
Alain MoreauTel 05 61 33 31 75
Email alixsaquetlcc-toulousefralainmoreaulcc-toulousefr
Some advice
Before any analysis feel free to contact us for any
discussion or question about feasibility and conditions of
analyses
The staff can help you
- to choose the best-suited technique to your needs
- for interpretation of your data
Where to find us LCC- door B015ndash ground floor-building B205 route de Narbonne
When 9h to 11h30 -14h to 17h
From Monday to Friday
21
Magnetic Measurement and Moumlssbauer spectroscopy - LCC
How to request an analysis
bull For any analysis request
For magnetic measurements SQUID andMoumlssbauer spectroscopy please contact Jean-Franccedilois Meunier by e-mail or phone
An appointment will be set up in order to studyyour analyses requests and to define theexperimental conditions
An analysis request form will be provided by thestaff
bull Results and samples
Results are emailed as text and excel files
On completion of the analyses samples must beretrieved at LCC
Further information on equipments
lcc-toulousefrServices Spectroscopie Moumlssbauer
Lcc-toulousefr
servicesMesures
Magneacutetiques
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 10Email Jf-meunierlcc-toulousefr
Where to find usLCC door CS012
205 route de Narbonne
When 9h to 12h - 14h to 17h30
From Monday to Friday
Some advice
22
Elemental Analysis C-H-NS - LCC
How to request an analysis
For any analysis request
Each sample must be supplied with an analysis request formavailable on LCC website
wwwlcc-toulousefr gt services gt services techniques ampscientifiques gt analyses chimiques gt Formulaire
Fill in electronically and send by mail (see framed who tocontact)
Samples
- Internal in my box DEPOT CHN in the mail locker analyseselementaires
- External ship by courrier to LCC service CHN or ask anappointment
Results
Results are sent by mail Samples are not returned
Analyses
Analyses are carried out every week
10 mg of compound areneeded for 2 essays andpackaged in a vial
Sensitive samples mustbe isolated in sealedampoule
For special analysisrequests please contactservice
Sulphur is analyzed oncea year if enoughdemand
Who to contact Isabelle BorgetTel 05 61 33 32 14
mail isabelleborgetlcc-toulousefr
Where to find service LCC door B038
205 route de Narbonne
When 9h to 11h30 - 14h to 16h30
From monday to friday
on appointment
Some advice
23
Nuclear Magnetic Resonance - LCC
How to request an analysis
bull For any analysis request (except self-service equipments)
For NMR equipments (400-solid and 600 MHz) analysisand appointment requests must be emailed to Y Coppelor C Bijani
The analysis request form can be loaded from the NMRfacility webpage on the LCC website (httplcc-toulousefr)
bull Self-service equipments
All the users have to follow a training conducted by NMRfacilityrsquos staff before any use of self-service spectrometers
- for LCC teams the training and NMR user accountrequests are provided with taking office
- for outside labs please contact the LCC personneldepartment
The requests when validated must be returned directlyto A Bonnet or D Paryl in order to plan the training
The users undertake to carefully respect the operatinginstructions and the LCC memos
All the data are automatically
- made available in the LCC teamsrsquo laquo Nuage raquo file
- emailed to the user from outside labs
Feel free to contact us for any question
about analysis capabilities or for
any discussion about the best strategy to
meet your specific issues
Who to contact
Yannick Coppel (Mgr)Christian BijaniTel 05 61 17 54 27
Antoine BonnetDavid Paryl
Tel 05 61 17 54 30Email yannickcoppellcc-
toulousefrchristianbijanilcc-toulousefrantoinebonnetlcc-toulousefr
davidparyllcc-toulousefr
Some advice
Where to find us
LCC RMN Building 205 route de Narbonne Toulouse
Door 030 (Y Coppel et C Bijani)
Door 033 (F Lacassin et D Paryl)
When8h30 to 11h30 -14h to 17h
From Monday to Friday
24
Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) - LCC
How to request an analysis
bull For any analysis request
Each sample must be supplied with an analysisrequest form To request this form please contact the staff
Sample amount depends on the concentration of chemical elements to be measured in the sampleanalyzed
In the very first request please contact the staff
bull Results
Results are delivered in the letter-box of the LCC team or for outside labs made available in the ICP departmentrsquos letter-box (within the LCC entrance hall)
bull Analyses schedule
Analyses are carried out every 2 weeks
In general 10 mg per assay isneeded (provided that the
concentration is above 5 ww)
Chemical elements currentlyanalyzed (but not limited) Ag Al Au B Ba Be Bi Ca Cd Co Cr Cu Fe Ir K Li Mg Mn Na
Ni P Pb Pd Pt Ru Rh Sr Zn
Who to contact
Alain Moreau Tel 0561175850
E-mail alainmoreaulcc-toulousefr
Where to find usIPBS Bacirct A3
205 route de Narbonne
When 8h to 11h30 - 14h to 16h30From Monday to Friday (odd
week)
Some advice
25
TECHNOPOLYM
10
Technopolym
How to request an analysis
bull Request an analysis via the central Technopolym emailtechnopolymictchimieups-tlsefr
Following this email we will inform you about the proposedtechniques of analyse costs time of delivery requiredquantity of sample conditioning sample deposit Dependingon your expected results an appointment to discuss yourproblem may be proposed before scheduling an analysis
bull For all analysis requestsEach sample must be accompanied by a fully completed
analysis request form You can find this form on the ICT website
ictcnrsfrplateforme-de-licttechnopolym or on the Technopolym website
httptechnopolymups-tlsefr
bull For more information
Visit our website to know about our skills equipment references
TechnopolymIs a virtual technological
platform dedicated to the characterization of polymeric
materials
We propose a range of analytical techniques
molecularcharacterization phase
transitions thermal stability behavior in
solution mechanicalproperties surface characterizationhellip
Come and talk to us
Who to contactPascale Saint-Aguet
Tel 05 61 55 68 08Tel (LCC) 05 61 33 31 34
Email technopolymictchimieups-tlsefr
Some advice
Where to find us
Door 30233rd floor building 2R1 Universiteacute Paul Sabatier
Door G064 ndashLCC 205 rte de Narbonne -
When
Monday-Friday 9h-12h and
14h-17h
11
Cross-Platform Services
12
Documentation
How to make a request
bull For all document requests
You can request your document by email telephone or inperson Donrsquot forget to indicate your full name and laboratorywith the references on your request
bull Consultation and loans
The catalogue of the chemistry library is available on theintranet
ictcnrsfrdocchimie
Borrowing is possible during office hours ndash outside thesehours please make an appointment
bull For bibliographic searches and training
Make an appointment
bull Open access
You can come and work at the library ndash computers and wifi are available Visit our website
ictcnrsfrplateforme-de-lictservices-transversesaccueil-de-la-documentation
Ask the documentation service for your intranet
password from
Feel free to call the service for any problems
relating to the use of bibliographic databases
Who to contactDanielle Brunet
Tel 05 61 55 85 69Email brunetictchimieups-tlsefr
Some advice
Where to find us
Door 0145 ground floor building 2R1
Universiteacute Paul Sabatier
When
Mon-Fri 9h-12h and 14h-17h If unattended make an
appointment
13
Electronics
How to make a request
Who to contactJean-Michel Martin
Tel 05 61 55 86 93Email scicassistanceictchimieups-tlsefr
Email martinjmictchimieups-tlsefr
Feel free to ask the service for
- Modification of existingelectronic devices and
proposals for improvement
- Troubleshooting and repair of electronic
devices
- Advice on purchase of new material
bull For all installation andor maintenance of equipment with astrong electronic component
Send an email phone or contact the service in person duringoffice hours
bull For all service requests
Send an email toscicassistanceictchimieups-tlsefrstating your name office number and a brief description of the problem
bull Loan of equipment
To address the needs of users specific equipment is availablein the electronics workshop (Oscilloscope component testerssoldering ironhellip) aswell as various tools
It is possible to borrow this equipment
Where to find usDoor 1015 1st floor building 2R1 Universiteacute Paul Sabatier
When Monday-Friday office hours
If unattended make an appointment
Some advice
14
Information Technology
How to make a request
bull For all requests for connection to the network andcreation of email accounts
First see the secretary of your laboratory
bull For all service requests
Write toscicassistanceictchimieups-tlsefr
stating your name office number and a brief description of the problem
The IT service manages developsand maintains the
network and associated services
Please contact us for more information on
the services provided (automatic
backup of data access to Cambridge CCDC data sharing
etc)
Who to contactPascal Puech
Edouard IvanovtchikTel 05 61 55 68 73
Email scicassistanceictchimieups-tlsefr
Some advice
Where to find usDoor 168 ground floor building 2R1
Universiteacute Paul Sabatier
WhenMonday-Friday office hours
If unattended make an appointment
15
Scientific Glassware
How to make a request
bull For all service requests
All glassware to repair or construct must be accompanied bya fully completed form You can find this form on the ICTwebsite ictcnrsfrVerrerie-scientifique
For obvious reasons of safety and hygiene glassware must beclean free of silicon grease and in a container identified withthe name of the research group
bull Do I need to go in person
In person contact is preferred if you are new to glasswork andif your request is complex
Photos et technical drawings sent by email are onlycomplementary information as in isolation they can lead tomisunderstandings and errors
For all glass repairs construction of new
equipment or prototyping
feel free to consult the glassware service
We can provide technicaladvice as well as contacts
in specialized domains
Who to contactSteacutephane Foulon
Tel 05 61 55 61 16Email foulonictchimieups-
tlsefr
Some advice
Where to find us
Door 0194 Ground Floor Building 2R1Universiteacute Paul
Sabatier
When
Monday-Friday during office hours We recommend that
external users make an appointment
16
copyFreacutedeacuteric MaligneICT
LCC Services
17
Thermal Analyses LCC
How to request an analysis
bull For any analysis request
DTATGA or DSC analyses each sample must be suppliedwith an analysis request form duly filled out To requestthese forms please contact the staff by e-mail
In the very first request please contact the staff fordetails about the process the sample amount requiredthe packaging of samples etc
In all other cases the analyses requests and the samplescan be deposited in the Thermal Analyses Departmentrsquosletter-box (within the LCC entrance hall)
bull Air-sensitive samples
Make an appointment with the staff
bull Results
Analyses results are emailed as a text file paper copy isavailable upon request
On completion of analyses remaining of samples must bepick up at LCC
Analytical Equipments
DTATGA for measuring the mass variation as a
function of temperature
DSC for detecting the phase changes without mass loss
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 1 0Email j-fmeunierlcc-toulousefr
Some advice
Where to find usLCC - Door CS12 basement level
205 route de Narbonne
When Opening hours 9h to 11h30 - 14h to 17hfrom Monday to Friday except on wednesday
18
Library Resource Center LCC
How to make a request
bull For any information request
- LCC research teams fill out the request form available onthe LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs contact the staff by e-mail
bull For bibliographical searches and access
Digital databases
- LCC research teams bibliographical searches databases areavailable on the LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs make an appointment with the staff
Paper print collections
Paperprint collections also are available and can be read in thelibrary premises
LCCrsquos Library access is free for LCC teams and subject to anappointment for outside labs
LCC teams Access to the LCC intranet is provided
with taking office
For further information feel free to contact us
Who to contact
Marie-Heacutelegravene Gullimarie-helenegullilcc-toulousefr
0561333217
Gilles Roujasgillesroujaslcc-toulousefr
0561333140
Gaeumltan Havetgaetanhavetlcc-toulousefr
0561333140
Some advice
Where to find usLCC 205 route de Narbonne
When Opening hours
9 h to 11h30 - 13h to 17h From Monday to Friday
19
Feel free to contact us for anyquestion about analyses
options or for anydiscussion about the
best strategy to meetyour specific issues
Single ndashcrystal and powder X-Ray Diffraction - LCC
How to request an analysis
bull Prior to any analysis
Contact the staff in charge of X-Ray Diffraction measurementsfor your team or your lab
bull Single-crystal X-ray diffraction
First the staff will evaluate the quality of the sample If quality isacceptable for a X-ray diffraction measurement an appointmentwill be set up for analysis
Following information must be provided expected compound used solvents any specific information concerning the sample(air-sensitive thermal-sensitive light-sensitivehellip) analysis and required data (absolute configuration hydride locationhellip)
bull Powder X-ray diffraction
Appointments are proposed in accordance with the type of measurement (reflection capillary measurements at variable temperatures x-ray grazing incidence on thin films)
Following information must be provided sample characteristics analytical conditions (scanning range of 2theta temperaturehellip) required data (phase identification crystallites sizehellip)
Useful tips Until getting staff opinion about the quality of yoursample particularly for a single-crystal handle it as little as possible
Who to contact Laure Vendier (Mgr)
Carine DuhayonSonia Mallet-Ladeira
Tel 05 61 33 31 18Email laurevendierlcc-toulousefr
carineduhayonlcc-toulousefrladeiraictchimieups-tlsefr
Some advice
Where to find us
LCC 205 route de NarbonneX-Ray Diffraction office ground floor door B017 X-Ray Diffraction Lab basement level door GS66
When
9h to 11h30 - 14h to 17hFrom Monday to Friday except on Wednesday afternoon
20
Electrochemistry - LCC
How to request an analysis
bull For any analysis request
Analyses are carried out by appointment onlyscheduled with the staff when requesting theanalysis
On the appointed date Bring the sample and the solvent Your presence is required during the analyses
bull Sample preparation
The sample(s) must be as pure as possible correspondingto a concentration of 10-3 molL-1 in 10 mL
For each sample bring 30 mL of purified solvent
bull Results
On completion of the analyses the mostrepresentative curves are provided in paper copy
Upon request the electronic files can be emailed
Who to contactAlix Sournia-Saquet (Mgr)
Alain MoreauTel 05 61 33 31 75
Email alixsaquetlcc-toulousefralainmoreaulcc-toulousefr
Some advice
Before any analysis feel free to contact us for any
discussion or question about feasibility and conditions of
analyses
The staff can help you
- to choose the best-suited technique to your needs
- for interpretation of your data
Where to find us LCC- door B015ndash ground floor-building B205 route de Narbonne
When 9h to 11h30 -14h to 17h
From Monday to Friday
21
Magnetic Measurement and Moumlssbauer spectroscopy - LCC
How to request an analysis
bull For any analysis request
For magnetic measurements SQUID andMoumlssbauer spectroscopy please contact Jean-Franccedilois Meunier by e-mail or phone
An appointment will be set up in order to studyyour analyses requests and to define theexperimental conditions
An analysis request form will be provided by thestaff
bull Results and samples
Results are emailed as text and excel files
On completion of the analyses samples must beretrieved at LCC
Further information on equipments
lcc-toulousefrServices Spectroscopie Moumlssbauer
Lcc-toulousefr
servicesMesures
Magneacutetiques
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 10Email Jf-meunierlcc-toulousefr
Where to find usLCC door CS012
205 route de Narbonne
When 9h to 12h - 14h to 17h30
From Monday to Friday
Some advice
22
Elemental Analysis C-H-NS - LCC
How to request an analysis
For any analysis request
Each sample must be supplied with an analysis request formavailable on LCC website
wwwlcc-toulousefr gt services gt services techniques ampscientifiques gt analyses chimiques gt Formulaire
Fill in electronically and send by mail (see framed who tocontact)
Samples
- Internal in my box DEPOT CHN in the mail locker analyseselementaires
- External ship by courrier to LCC service CHN or ask anappointment
Results
Results are sent by mail Samples are not returned
Analyses
Analyses are carried out every week
10 mg of compound areneeded for 2 essays andpackaged in a vial
Sensitive samples mustbe isolated in sealedampoule
For special analysisrequests please contactservice
Sulphur is analyzed oncea year if enoughdemand
Who to contact Isabelle BorgetTel 05 61 33 32 14
mail isabelleborgetlcc-toulousefr
Where to find service LCC door B038
205 route de Narbonne
When 9h to 11h30 - 14h to 16h30
From monday to friday
on appointment
Some advice
23
Nuclear Magnetic Resonance - LCC
How to request an analysis
bull For any analysis request (except self-service equipments)
For NMR equipments (400-solid and 600 MHz) analysisand appointment requests must be emailed to Y Coppelor C Bijani
The analysis request form can be loaded from the NMRfacility webpage on the LCC website (httplcc-toulousefr)
bull Self-service equipments
All the users have to follow a training conducted by NMRfacilityrsquos staff before any use of self-service spectrometers
- for LCC teams the training and NMR user accountrequests are provided with taking office
- for outside labs please contact the LCC personneldepartment
The requests when validated must be returned directlyto A Bonnet or D Paryl in order to plan the training
The users undertake to carefully respect the operatinginstructions and the LCC memos
All the data are automatically
- made available in the LCC teamsrsquo laquo Nuage raquo file
- emailed to the user from outside labs
Feel free to contact us for any question
about analysis capabilities or for
any discussion about the best strategy to
meet your specific issues
Who to contact
Yannick Coppel (Mgr)Christian BijaniTel 05 61 17 54 27
Antoine BonnetDavid Paryl
Tel 05 61 17 54 30Email yannickcoppellcc-
toulousefrchristianbijanilcc-toulousefrantoinebonnetlcc-toulousefr
davidparyllcc-toulousefr
Some advice
Where to find us
LCC RMN Building 205 route de Narbonne Toulouse
Door 030 (Y Coppel et C Bijani)
Door 033 (F Lacassin et D Paryl)
When8h30 to 11h30 -14h to 17h
From Monday to Friday
24
Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) - LCC
How to request an analysis
bull For any analysis request
Each sample must be supplied with an analysisrequest form To request this form please contact the staff
Sample amount depends on the concentration of chemical elements to be measured in the sampleanalyzed
In the very first request please contact the staff
bull Results
Results are delivered in the letter-box of the LCC team or for outside labs made available in the ICP departmentrsquos letter-box (within the LCC entrance hall)
bull Analyses schedule
Analyses are carried out every 2 weeks
In general 10 mg per assay isneeded (provided that the
concentration is above 5 ww)
Chemical elements currentlyanalyzed (but not limited) Ag Al Au B Ba Be Bi Ca Cd Co Cr Cu Fe Ir K Li Mg Mn Na
Ni P Pb Pd Pt Ru Rh Sr Zn
Who to contact
Alain Moreau Tel 0561175850
E-mail alainmoreaulcc-toulousefr
Where to find usIPBS Bacirct A3
205 route de Narbonne
When 8h to 11h30 - 14h to 16h30From Monday to Friday (odd
week)
Some advice
25
Technopolym
How to request an analysis
bull Request an analysis via the central Technopolym emailtechnopolymictchimieups-tlsefr
Following this email we will inform you about the proposedtechniques of analyse costs time of delivery requiredquantity of sample conditioning sample deposit Dependingon your expected results an appointment to discuss yourproblem may be proposed before scheduling an analysis
bull For all analysis requestsEach sample must be accompanied by a fully completed
analysis request form You can find this form on the ICT website
ictcnrsfrplateforme-de-licttechnopolym or on the Technopolym website
httptechnopolymups-tlsefr
bull For more information
Visit our website to know about our skills equipment references
TechnopolymIs a virtual technological
platform dedicated to the characterization of polymeric
materials
We propose a range of analytical techniques
molecularcharacterization phase
transitions thermal stability behavior in
solution mechanicalproperties surface characterizationhellip
Come and talk to us
Who to contactPascale Saint-Aguet
Tel 05 61 55 68 08Tel (LCC) 05 61 33 31 34
Email technopolymictchimieups-tlsefr
Some advice
Where to find us
Door 30233rd floor building 2R1 Universiteacute Paul Sabatier
Door G064 ndashLCC 205 rte de Narbonne -
When
Monday-Friday 9h-12h and
14h-17h
11
Cross-Platform Services
12
Documentation
How to make a request
bull For all document requests
You can request your document by email telephone or inperson Donrsquot forget to indicate your full name and laboratorywith the references on your request
bull Consultation and loans
The catalogue of the chemistry library is available on theintranet
ictcnrsfrdocchimie
Borrowing is possible during office hours ndash outside thesehours please make an appointment
bull For bibliographic searches and training
Make an appointment
bull Open access
You can come and work at the library ndash computers and wifi are available Visit our website
ictcnrsfrplateforme-de-lictservices-transversesaccueil-de-la-documentation
Ask the documentation service for your intranet
password from
Feel free to call the service for any problems
relating to the use of bibliographic databases
Who to contactDanielle Brunet
Tel 05 61 55 85 69Email brunetictchimieups-tlsefr
Some advice
Where to find us
Door 0145 ground floor building 2R1
Universiteacute Paul Sabatier
When
Mon-Fri 9h-12h and 14h-17h If unattended make an
appointment
13
Electronics
How to make a request
Who to contactJean-Michel Martin
Tel 05 61 55 86 93Email scicassistanceictchimieups-tlsefr
Email martinjmictchimieups-tlsefr
Feel free to ask the service for
- Modification of existingelectronic devices and
proposals for improvement
- Troubleshooting and repair of electronic
devices
- Advice on purchase of new material
bull For all installation andor maintenance of equipment with astrong electronic component
Send an email phone or contact the service in person duringoffice hours
bull For all service requests
Send an email toscicassistanceictchimieups-tlsefrstating your name office number and a brief description of the problem
bull Loan of equipment
To address the needs of users specific equipment is availablein the electronics workshop (Oscilloscope component testerssoldering ironhellip) aswell as various tools
It is possible to borrow this equipment
Where to find usDoor 1015 1st floor building 2R1 Universiteacute Paul Sabatier
When Monday-Friday office hours
If unattended make an appointment
Some advice
14
Information Technology
How to make a request
bull For all requests for connection to the network andcreation of email accounts
First see the secretary of your laboratory
bull For all service requests
Write toscicassistanceictchimieups-tlsefr
stating your name office number and a brief description of the problem
The IT service manages developsand maintains the
network and associated services
Please contact us for more information on
the services provided (automatic
backup of data access to Cambridge CCDC data sharing
etc)
Who to contactPascal Puech
Edouard IvanovtchikTel 05 61 55 68 73
Email scicassistanceictchimieups-tlsefr
Some advice
Where to find usDoor 168 ground floor building 2R1
Universiteacute Paul Sabatier
WhenMonday-Friday office hours
If unattended make an appointment
15
Scientific Glassware
How to make a request
bull For all service requests
All glassware to repair or construct must be accompanied bya fully completed form You can find this form on the ICTwebsite ictcnrsfrVerrerie-scientifique
For obvious reasons of safety and hygiene glassware must beclean free of silicon grease and in a container identified withthe name of the research group
bull Do I need to go in person
In person contact is preferred if you are new to glasswork andif your request is complex
Photos et technical drawings sent by email are onlycomplementary information as in isolation they can lead tomisunderstandings and errors
For all glass repairs construction of new
equipment or prototyping
feel free to consult the glassware service
We can provide technicaladvice as well as contacts
in specialized domains
Who to contactSteacutephane Foulon
Tel 05 61 55 61 16Email foulonictchimieups-
tlsefr
Some advice
Where to find us
Door 0194 Ground Floor Building 2R1Universiteacute Paul
Sabatier
When
Monday-Friday during office hours We recommend that
external users make an appointment
16
copyFreacutedeacuteric MaligneICT
LCC Services
17
Thermal Analyses LCC
How to request an analysis
bull For any analysis request
DTATGA or DSC analyses each sample must be suppliedwith an analysis request form duly filled out To requestthese forms please contact the staff by e-mail
In the very first request please contact the staff fordetails about the process the sample amount requiredthe packaging of samples etc
In all other cases the analyses requests and the samplescan be deposited in the Thermal Analyses Departmentrsquosletter-box (within the LCC entrance hall)
bull Air-sensitive samples
Make an appointment with the staff
bull Results
Analyses results are emailed as a text file paper copy isavailable upon request
On completion of analyses remaining of samples must bepick up at LCC
Analytical Equipments
DTATGA for measuring the mass variation as a
function of temperature
DSC for detecting the phase changes without mass loss
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 1 0Email j-fmeunierlcc-toulousefr
Some advice
Where to find usLCC - Door CS12 basement level
205 route de Narbonne
When Opening hours 9h to 11h30 - 14h to 17hfrom Monday to Friday except on wednesday
18
Library Resource Center LCC
How to make a request
bull For any information request
- LCC research teams fill out the request form available onthe LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs contact the staff by e-mail
bull For bibliographical searches and access
Digital databases
- LCC research teams bibliographical searches databases areavailable on the LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs make an appointment with the staff
Paper print collections
Paperprint collections also are available and can be read in thelibrary premises
LCCrsquos Library access is free for LCC teams and subject to anappointment for outside labs
LCC teams Access to the LCC intranet is provided
with taking office
For further information feel free to contact us
Who to contact
Marie-Heacutelegravene Gullimarie-helenegullilcc-toulousefr
0561333217
Gilles Roujasgillesroujaslcc-toulousefr
0561333140
Gaeumltan Havetgaetanhavetlcc-toulousefr
0561333140
Some advice
Where to find usLCC 205 route de Narbonne
When Opening hours
9 h to 11h30 - 13h to 17h From Monday to Friday
19
Feel free to contact us for anyquestion about analyses
options or for anydiscussion about the
best strategy to meetyour specific issues
Single ndashcrystal and powder X-Ray Diffraction - LCC
How to request an analysis
bull Prior to any analysis
Contact the staff in charge of X-Ray Diffraction measurementsfor your team or your lab
bull Single-crystal X-ray diffraction
First the staff will evaluate the quality of the sample If quality isacceptable for a X-ray diffraction measurement an appointmentwill be set up for analysis
Following information must be provided expected compound used solvents any specific information concerning the sample(air-sensitive thermal-sensitive light-sensitivehellip) analysis and required data (absolute configuration hydride locationhellip)
bull Powder X-ray diffraction
Appointments are proposed in accordance with the type of measurement (reflection capillary measurements at variable temperatures x-ray grazing incidence on thin films)
Following information must be provided sample characteristics analytical conditions (scanning range of 2theta temperaturehellip) required data (phase identification crystallites sizehellip)
Useful tips Until getting staff opinion about the quality of yoursample particularly for a single-crystal handle it as little as possible
Who to contact Laure Vendier (Mgr)
Carine DuhayonSonia Mallet-Ladeira
Tel 05 61 33 31 18Email laurevendierlcc-toulousefr
carineduhayonlcc-toulousefrladeiraictchimieups-tlsefr
Some advice
Where to find us
LCC 205 route de NarbonneX-Ray Diffraction office ground floor door B017 X-Ray Diffraction Lab basement level door GS66
When
9h to 11h30 - 14h to 17hFrom Monday to Friday except on Wednesday afternoon
20
Electrochemistry - LCC
How to request an analysis
bull For any analysis request
Analyses are carried out by appointment onlyscheduled with the staff when requesting theanalysis
On the appointed date Bring the sample and the solvent Your presence is required during the analyses
bull Sample preparation
The sample(s) must be as pure as possible correspondingto a concentration of 10-3 molL-1 in 10 mL
For each sample bring 30 mL of purified solvent
bull Results
On completion of the analyses the mostrepresentative curves are provided in paper copy
Upon request the electronic files can be emailed
Who to contactAlix Sournia-Saquet (Mgr)
Alain MoreauTel 05 61 33 31 75
Email alixsaquetlcc-toulousefralainmoreaulcc-toulousefr
Some advice
Before any analysis feel free to contact us for any
discussion or question about feasibility and conditions of
analyses
The staff can help you
- to choose the best-suited technique to your needs
- for interpretation of your data
Where to find us LCC- door B015ndash ground floor-building B205 route de Narbonne
When 9h to 11h30 -14h to 17h
From Monday to Friday
21
Magnetic Measurement and Moumlssbauer spectroscopy - LCC
How to request an analysis
bull For any analysis request
For magnetic measurements SQUID andMoumlssbauer spectroscopy please contact Jean-Franccedilois Meunier by e-mail or phone
An appointment will be set up in order to studyyour analyses requests and to define theexperimental conditions
An analysis request form will be provided by thestaff
bull Results and samples
Results are emailed as text and excel files
On completion of the analyses samples must beretrieved at LCC
Further information on equipments
lcc-toulousefrServices Spectroscopie Moumlssbauer
Lcc-toulousefr
servicesMesures
Magneacutetiques
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 10Email Jf-meunierlcc-toulousefr
Where to find usLCC door CS012
205 route de Narbonne
When 9h to 12h - 14h to 17h30
From Monday to Friday
Some advice
22
Elemental Analysis C-H-NS - LCC
How to request an analysis
For any analysis request
Each sample must be supplied with an analysis request formavailable on LCC website
wwwlcc-toulousefr gt services gt services techniques ampscientifiques gt analyses chimiques gt Formulaire
Fill in electronically and send by mail (see framed who tocontact)
Samples
- Internal in my box DEPOT CHN in the mail locker analyseselementaires
- External ship by courrier to LCC service CHN or ask anappointment
Results
Results are sent by mail Samples are not returned
Analyses
Analyses are carried out every week
10 mg of compound areneeded for 2 essays andpackaged in a vial
Sensitive samples mustbe isolated in sealedampoule
For special analysisrequests please contactservice
Sulphur is analyzed oncea year if enoughdemand
Who to contact Isabelle BorgetTel 05 61 33 32 14
mail isabelleborgetlcc-toulousefr
Where to find service LCC door B038
205 route de Narbonne
When 9h to 11h30 - 14h to 16h30
From monday to friday
on appointment
Some advice
23
Nuclear Magnetic Resonance - LCC
How to request an analysis
bull For any analysis request (except self-service equipments)
For NMR equipments (400-solid and 600 MHz) analysisand appointment requests must be emailed to Y Coppelor C Bijani
The analysis request form can be loaded from the NMRfacility webpage on the LCC website (httplcc-toulousefr)
bull Self-service equipments
All the users have to follow a training conducted by NMRfacilityrsquos staff before any use of self-service spectrometers
- for LCC teams the training and NMR user accountrequests are provided with taking office
- for outside labs please contact the LCC personneldepartment
The requests when validated must be returned directlyto A Bonnet or D Paryl in order to plan the training
The users undertake to carefully respect the operatinginstructions and the LCC memos
All the data are automatically
- made available in the LCC teamsrsquo laquo Nuage raquo file
- emailed to the user from outside labs
Feel free to contact us for any question
about analysis capabilities or for
any discussion about the best strategy to
meet your specific issues
Who to contact
Yannick Coppel (Mgr)Christian BijaniTel 05 61 17 54 27
Antoine BonnetDavid Paryl
Tel 05 61 17 54 30Email yannickcoppellcc-
toulousefrchristianbijanilcc-toulousefrantoinebonnetlcc-toulousefr
davidparyllcc-toulousefr
Some advice
Where to find us
LCC RMN Building 205 route de Narbonne Toulouse
Door 030 (Y Coppel et C Bijani)
Door 033 (F Lacassin et D Paryl)
When8h30 to 11h30 -14h to 17h
From Monday to Friday
24
Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) - LCC
How to request an analysis
bull For any analysis request
Each sample must be supplied with an analysisrequest form To request this form please contact the staff
Sample amount depends on the concentration of chemical elements to be measured in the sampleanalyzed
In the very first request please contact the staff
bull Results
Results are delivered in the letter-box of the LCC team or for outside labs made available in the ICP departmentrsquos letter-box (within the LCC entrance hall)
bull Analyses schedule
Analyses are carried out every 2 weeks
In general 10 mg per assay isneeded (provided that the
concentration is above 5 ww)
Chemical elements currentlyanalyzed (but not limited) Ag Al Au B Ba Be Bi Ca Cd Co Cr Cu Fe Ir K Li Mg Mn Na
Ni P Pb Pd Pt Ru Rh Sr Zn
Who to contact
Alain Moreau Tel 0561175850
E-mail alainmoreaulcc-toulousefr
Where to find usIPBS Bacirct A3
205 route de Narbonne
When 8h to 11h30 - 14h to 16h30From Monday to Friday (odd
week)
Some advice
25
Cross-Platform Services
12
Documentation
How to make a request
bull For all document requests
You can request your document by email telephone or inperson Donrsquot forget to indicate your full name and laboratorywith the references on your request
bull Consultation and loans
The catalogue of the chemistry library is available on theintranet
ictcnrsfrdocchimie
Borrowing is possible during office hours ndash outside thesehours please make an appointment
bull For bibliographic searches and training
Make an appointment
bull Open access
You can come and work at the library ndash computers and wifi are available Visit our website
ictcnrsfrplateforme-de-lictservices-transversesaccueil-de-la-documentation
Ask the documentation service for your intranet
password from
Feel free to call the service for any problems
relating to the use of bibliographic databases
Who to contactDanielle Brunet
Tel 05 61 55 85 69Email brunetictchimieups-tlsefr
Some advice
Where to find us
Door 0145 ground floor building 2R1
Universiteacute Paul Sabatier
When
Mon-Fri 9h-12h and 14h-17h If unattended make an
appointment
13
Electronics
How to make a request
Who to contactJean-Michel Martin
Tel 05 61 55 86 93Email scicassistanceictchimieups-tlsefr
Email martinjmictchimieups-tlsefr
Feel free to ask the service for
- Modification of existingelectronic devices and
proposals for improvement
- Troubleshooting and repair of electronic
devices
- Advice on purchase of new material
bull For all installation andor maintenance of equipment with astrong electronic component
Send an email phone or contact the service in person duringoffice hours
bull For all service requests
Send an email toscicassistanceictchimieups-tlsefrstating your name office number and a brief description of the problem
bull Loan of equipment
To address the needs of users specific equipment is availablein the electronics workshop (Oscilloscope component testerssoldering ironhellip) aswell as various tools
It is possible to borrow this equipment
Where to find usDoor 1015 1st floor building 2R1 Universiteacute Paul Sabatier
When Monday-Friday office hours
If unattended make an appointment
Some advice
14
Information Technology
How to make a request
bull For all requests for connection to the network andcreation of email accounts
First see the secretary of your laboratory
bull For all service requests
Write toscicassistanceictchimieups-tlsefr
stating your name office number and a brief description of the problem
The IT service manages developsand maintains the
network and associated services
Please contact us for more information on
the services provided (automatic
backup of data access to Cambridge CCDC data sharing
etc)
Who to contactPascal Puech
Edouard IvanovtchikTel 05 61 55 68 73
Email scicassistanceictchimieups-tlsefr
Some advice
Where to find usDoor 168 ground floor building 2R1
Universiteacute Paul Sabatier
WhenMonday-Friday office hours
If unattended make an appointment
15
Scientific Glassware
How to make a request
bull For all service requests
All glassware to repair or construct must be accompanied bya fully completed form You can find this form on the ICTwebsite ictcnrsfrVerrerie-scientifique
For obvious reasons of safety and hygiene glassware must beclean free of silicon grease and in a container identified withthe name of the research group
bull Do I need to go in person
In person contact is preferred if you are new to glasswork andif your request is complex
Photos et technical drawings sent by email are onlycomplementary information as in isolation they can lead tomisunderstandings and errors
For all glass repairs construction of new
equipment or prototyping
feel free to consult the glassware service
We can provide technicaladvice as well as contacts
in specialized domains
Who to contactSteacutephane Foulon
Tel 05 61 55 61 16Email foulonictchimieups-
tlsefr
Some advice
Where to find us
Door 0194 Ground Floor Building 2R1Universiteacute Paul
Sabatier
When
Monday-Friday during office hours We recommend that
external users make an appointment
16
copyFreacutedeacuteric MaligneICT
LCC Services
17
Thermal Analyses LCC
How to request an analysis
bull For any analysis request
DTATGA or DSC analyses each sample must be suppliedwith an analysis request form duly filled out To requestthese forms please contact the staff by e-mail
In the very first request please contact the staff fordetails about the process the sample amount requiredthe packaging of samples etc
In all other cases the analyses requests and the samplescan be deposited in the Thermal Analyses Departmentrsquosletter-box (within the LCC entrance hall)
bull Air-sensitive samples
Make an appointment with the staff
bull Results
Analyses results are emailed as a text file paper copy isavailable upon request
On completion of analyses remaining of samples must bepick up at LCC
Analytical Equipments
DTATGA for measuring the mass variation as a
function of temperature
DSC for detecting the phase changes without mass loss
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 1 0Email j-fmeunierlcc-toulousefr
Some advice
Where to find usLCC - Door CS12 basement level
205 route de Narbonne
When Opening hours 9h to 11h30 - 14h to 17hfrom Monday to Friday except on wednesday
18
Library Resource Center LCC
How to make a request
bull For any information request
- LCC research teams fill out the request form available onthe LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs contact the staff by e-mail
bull For bibliographical searches and access
Digital databases
- LCC research teams bibliographical searches databases areavailable on the LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs make an appointment with the staff
Paper print collections
Paperprint collections also are available and can be read in thelibrary premises
LCCrsquos Library access is free for LCC teams and subject to anappointment for outside labs
LCC teams Access to the LCC intranet is provided
with taking office
For further information feel free to contact us
Who to contact
Marie-Heacutelegravene Gullimarie-helenegullilcc-toulousefr
0561333217
Gilles Roujasgillesroujaslcc-toulousefr
0561333140
Gaeumltan Havetgaetanhavetlcc-toulousefr
0561333140
Some advice
Where to find usLCC 205 route de Narbonne
When Opening hours
9 h to 11h30 - 13h to 17h From Monday to Friday
19
Feel free to contact us for anyquestion about analyses
options or for anydiscussion about the
best strategy to meetyour specific issues
Single ndashcrystal and powder X-Ray Diffraction - LCC
How to request an analysis
bull Prior to any analysis
Contact the staff in charge of X-Ray Diffraction measurementsfor your team or your lab
bull Single-crystal X-ray diffraction
First the staff will evaluate the quality of the sample If quality isacceptable for a X-ray diffraction measurement an appointmentwill be set up for analysis
Following information must be provided expected compound used solvents any specific information concerning the sample(air-sensitive thermal-sensitive light-sensitivehellip) analysis and required data (absolute configuration hydride locationhellip)
bull Powder X-ray diffraction
Appointments are proposed in accordance with the type of measurement (reflection capillary measurements at variable temperatures x-ray grazing incidence on thin films)
Following information must be provided sample characteristics analytical conditions (scanning range of 2theta temperaturehellip) required data (phase identification crystallites sizehellip)
Useful tips Until getting staff opinion about the quality of yoursample particularly for a single-crystal handle it as little as possible
Who to contact Laure Vendier (Mgr)
Carine DuhayonSonia Mallet-Ladeira
Tel 05 61 33 31 18Email laurevendierlcc-toulousefr
carineduhayonlcc-toulousefrladeiraictchimieups-tlsefr
Some advice
Where to find us
LCC 205 route de NarbonneX-Ray Diffraction office ground floor door B017 X-Ray Diffraction Lab basement level door GS66
When
9h to 11h30 - 14h to 17hFrom Monday to Friday except on Wednesday afternoon
20
Electrochemistry - LCC
How to request an analysis
bull For any analysis request
Analyses are carried out by appointment onlyscheduled with the staff when requesting theanalysis
On the appointed date Bring the sample and the solvent Your presence is required during the analyses
bull Sample preparation
The sample(s) must be as pure as possible correspondingto a concentration of 10-3 molL-1 in 10 mL
For each sample bring 30 mL of purified solvent
bull Results
On completion of the analyses the mostrepresentative curves are provided in paper copy
Upon request the electronic files can be emailed
Who to contactAlix Sournia-Saquet (Mgr)
Alain MoreauTel 05 61 33 31 75
Email alixsaquetlcc-toulousefralainmoreaulcc-toulousefr
Some advice
Before any analysis feel free to contact us for any
discussion or question about feasibility and conditions of
analyses
The staff can help you
- to choose the best-suited technique to your needs
- for interpretation of your data
Where to find us LCC- door B015ndash ground floor-building B205 route de Narbonne
When 9h to 11h30 -14h to 17h
From Monday to Friday
21
Magnetic Measurement and Moumlssbauer spectroscopy - LCC
How to request an analysis
bull For any analysis request
For magnetic measurements SQUID andMoumlssbauer spectroscopy please contact Jean-Franccedilois Meunier by e-mail or phone
An appointment will be set up in order to studyyour analyses requests and to define theexperimental conditions
An analysis request form will be provided by thestaff
bull Results and samples
Results are emailed as text and excel files
On completion of the analyses samples must beretrieved at LCC
Further information on equipments
lcc-toulousefrServices Spectroscopie Moumlssbauer
Lcc-toulousefr
servicesMesures
Magneacutetiques
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 10Email Jf-meunierlcc-toulousefr
Where to find usLCC door CS012
205 route de Narbonne
When 9h to 12h - 14h to 17h30
From Monday to Friday
Some advice
22
Elemental Analysis C-H-NS - LCC
How to request an analysis
For any analysis request
Each sample must be supplied with an analysis request formavailable on LCC website
wwwlcc-toulousefr gt services gt services techniques ampscientifiques gt analyses chimiques gt Formulaire
Fill in electronically and send by mail (see framed who tocontact)
Samples
- Internal in my box DEPOT CHN in the mail locker analyseselementaires
- External ship by courrier to LCC service CHN or ask anappointment
Results
Results are sent by mail Samples are not returned
Analyses
Analyses are carried out every week
10 mg of compound areneeded for 2 essays andpackaged in a vial
Sensitive samples mustbe isolated in sealedampoule
For special analysisrequests please contactservice
Sulphur is analyzed oncea year if enoughdemand
Who to contact Isabelle BorgetTel 05 61 33 32 14
mail isabelleborgetlcc-toulousefr
Where to find service LCC door B038
205 route de Narbonne
When 9h to 11h30 - 14h to 16h30
From monday to friday
on appointment
Some advice
23
Nuclear Magnetic Resonance - LCC
How to request an analysis
bull For any analysis request (except self-service equipments)
For NMR equipments (400-solid and 600 MHz) analysisand appointment requests must be emailed to Y Coppelor C Bijani
The analysis request form can be loaded from the NMRfacility webpage on the LCC website (httplcc-toulousefr)
bull Self-service equipments
All the users have to follow a training conducted by NMRfacilityrsquos staff before any use of self-service spectrometers
- for LCC teams the training and NMR user accountrequests are provided with taking office
- for outside labs please contact the LCC personneldepartment
The requests when validated must be returned directlyto A Bonnet or D Paryl in order to plan the training
The users undertake to carefully respect the operatinginstructions and the LCC memos
All the data are automatically
- made available in the LCC teamsrsquo laquo Nuage raquo file
- emailed to the user from outside labs
Feel free to contact us for any question
about analysis capabilities or for
any discussion about the best strategy to
meet your specific issues
Who to contact
Yannick Coppel (Mgr)Christian BijaniTel 05 61 17 54 27
Antoine BonnetDavid Paryl
Tel 05 61 17 54 30Email yannickcoppellcc-
toulousefrchristianbijanilcc-toulousefrantoinebonnetlcc-toulousefr
davidparyllcc-toulousefr
Some advice
Where to find us
LCC RMN Building 205 route de Narbonne Toulouse
Door 030 (Y Coppel et C Bijani)
Door 033 (F Lacassin et D Paryl)
When8h30 to 11h30 -14h to 17h
From Monday to Friday
24
Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) - LCC
How to request an analysis
bull For any analysis request
Each sample must be supplied with an analysisrequest form To request this form please contact the staff
Sample amount depends on the concentration of chemical elements to be measured in the sampleanalyzed
In the very first request please contact the staff
bull Results
Results are delivered in the letter-box of the LCC team or for outside labs made available in the ICP departmentrsquos letter-box (within the LCC entrance hall)
bull Analyses schedule
Analyses are carried out every 2 weeks
In general 10 mg per assay isneeded (provided that the
concentration is above 5 ww)
Chemical elements currentlyanalyzed (but not limited) Ag Al Au B Ba Be Bi Ca Cd Co Cr Cu Fe Ir K Li Mg Mn Na
Ni P Pb Pd Pt Ru Rh Sr Zn
Who to contact
Alain Moreau Tel 0561175850
E-mail alainmoreaulcc-toulousefr
Where to find usIPBS Bacirct A3
205 route de Narbonne
When 8h to 11h30 - 14h to 16h30From Monday to Friday (odd
week)
Some advice
25
Documentation
How to make a request
bull For all document requests
You can request your document by email telephone or inperson Donrsquot forget to indicate your full name and laboratorywith the references on your request
bull Consultation and loans
The catalogue of the chemistry library is available on theintranet
ictcnrsfrdocchimie
Borrowing is possible during office hours ndash outside thesehours please make an appointment
bull For bibliographic searches and training
Make an appointment
bull Open access
You can come and work at the library ndash computers and wifi are available Visit our website
ictcnrsfrplateforme-de-lictservices-transversesaccueil-de-la-documentation
Ask the documentation service for your intranet
password from
Feel free to call the service for any problems
relating to the use of bibliographic databases
Who to contactDanielle Brunet
Tel 05 61 55 85 69Email brunetictchimieups-tlsefr
Some advice
Where to find us
Door 0145 ground floor building 2R1
Universiteacute Paul Sabatier
When
Mon-Fri 9h-12h and 14h-17h If unattended make an
appointment
13
Electronics
How to make a request
Who to contactJean-Michel Martin
Tel 05 61 55 86 93Email scicassistanceictchimieups-tlsefr
Email martinjmictchimieups-tlsefr
Feel free to ask the service for
- Modification of existingelectronic devices and
proposals for improvement
- Troubleshooting and repair of electronic
devices
- Advice on purchase of new material
bull For all installation andor maintenance of equipment with astrong electronic component
Send an email phone or contact the service in person duringoffice hours
bull For all service requests
Send an email toscicassistanceictchimieups-tlsefrstating your name office number and a brief description of the problem
bull Loan of equipment
To address the needs of users specific equipment is availablein the electronics workshop (Oscilloscope component testerssoldering ironhellip) aswell as various tools
It is possible to borrow this equipment
Where to find usDoor 1015 1st floor building 2R1 Universiteacute Paul Sabatier
When Monday-Friday office hours
If unattended make an appointment
Some advice
14
Information Technology
How to make a request
bull For all requests for connection to the network andcreation of email accounts
First see the secretary of your laboratory
bull For all service requests
Write toscicassistanceictchimieups-tlsefr
stating your name office number and a brief description of the problem
The IT service manages developsand maintains the
network and associated services
Please contact us for more information on
the services provided (automatic
backup of data access to Cambridge CCDC data sharing
etc)
Who to contactPascal Puech
Edouard IvanovtchikTel 05 61 55 68 73
Email scicassistanceictchimieups-tlsefr
Some advice
Where to find usDoor 168 ground floor building 2R1
Universiteacute Paul Sabatier
WhenMonday-Friday office hours
If unattended make an appointment
15
Scientific Glassware
How to make a request
bull For all service requests
All glassware to repair or construct must be accompanied bya fully completed form You can find this form on the ICTwebsite ictcnrsfrVerrerie-scientifique
For obvious reasons of safety and hygiene glassware must beclean free of silicon grease and in a container identified withthe name of the research group
bull Do I need to go in person
In person contact is preferred if you are new to glasswork andif your request is complex
Photos et technical drawings sent by email are onlycomplementary information as in isolation they can lead tomisunderstandings and errors
For all glass repairs construction of new
equipment or prototyping
feel free to consult the glassware service
We can provide technicaladvice as well as contacts
in specialized domains
Who to contactSteacutephane Foulon
Tel 05 61 55 61 16Email foulonictchimieups-
tlsefr
Some advice
Where to find us
Door 0194 Ground Floor Building 2R1Universiteacute Paul
Sabatier
When
Monday-Friday during office hours We recommend that
external users make an appointment
16
copyFreacutedeacuteric MaligneICT
LCC Services
17
Thermal Analyses LCC
How to request an analysis
bull For any analysis request
DTATGA or DSC analyses each sample must be suppliedwith an analysis request form duly filled out To requestthese forms please contact the staff by e-mail
In the very first request please contact the staff fordetails about the process the sample amount requiredthe packaging of samples etc
In all other cases the analyses requests and the samplescan be deposited in the Thermal Analyses Departmentrsquosletter-box (within the LCC entrance hall)
bull Air-sensitive samples
Make an appointment with the staff
bull Results
Analyses results are emailed as a text file paper copy isavailable upon request
On completion of analyses remaining of samples must bepick up at LCC
Analytical Equipments
DTATGA for measuring the mass variation as a
function of temperature
DSC for detecting the phase changes without mass loss
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 1 0Email j-fmeunierlcc-toulousefr
Some advice
Where to find usLCC - Door CS12 basement level
205 route de Narbonne
When Opening hours 9h to 11h30 - 14h to 17hfrom Monday to Friday except on wednesday
18
Library Resource Center LCC
How to make a request
bull For any information request
- LCC research teams fill out the request form available onthe LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs contact the staff by e-mail
bull For bibliographical searches and access
Digital databases
- LCC research teams bibliographical searches databases areavailable on the LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs make an appointment with the staff
Paper print collections
Paperprint collections also are available and can be read in thelibrary premises
LCCrsquos Library access is free for LCC teams and subject to anappointment for outside labs
LCC teams Access to the LCC intranet is provided
with taking office
For further information feel free to contact us
Who to contact
Marie-Heacutelegravene Gullimarie-helenegullilcc-toulousefr
0561333217
Gilles Roujasgillesroujaslcc-toulousefr
0561333140
Gaeumltan Havetgaetanhavetlcc-toulousefr
0561333140
Some advice
Where to find usLCC 205 route de Narbonne
When Opening hours
9 h to 11h30 - 13h to 17h From Monday to Friday
19
Feel free to contact us for anyquestion about analyses
options or for anydiscussion about the
best strategy to meetyour specific issues
Single ndashcrystal and powder X-Ray Diffraction - LCC
How to request an analysis
bull Prior to any analysis
Contact the staff in charge of X-Ray Diffraction measurementsfor your team or your lab
bull Single-crystal X-ray diffraction
First the staff will evaluate the quality of the sample If quality isacceptable for a X-ray diffraction measurement an appointmentwill be set up for analysis
Following information must be provided expected compound used solvents any specific information concerning the sample(air-sensitive thermal-sensitive light-sensitivehellip) analysis and required data (absolute configuration hydride locationhellip)
bull Powder X-ray diffraction
Appointments are proposed in accordance with the type of measurement (reflection capillary measurements at variable temperatures x-ray grazing incidence on thin films)
Following information must be provided sample characteristics analytical conditions (scanning range of 2theta temperaturehellip) required data (phase identification crystallites sizehellip)
Useful tips Until getting staff opinion about the quality of yoursample particularly for a single-crystal handle it as little as possible
Who to contact Laure Vendier (Mgr)
Carine DuhayonSonia Mallet-Ladeira
Tel 05 61 33 31 18Email laurevendierlcc-toulousefr
carineduhayonlcc-toulousefrladeiraictchimieups-tlsefr
Some advice
Where to find us
LCC 205 route de NarbonneX-Ray Diffraction office ground floor door B017 X-Ray Diffraction Lab basement level door GS66
When
9h to 11h30 - 14h to 17hFrom Monday to Friday except on Wednesday afternoon
20
Electrochemistry - LCC
How to request an analysis
bull For any analysis request
Analyses are carried out by appointment onlyscheduled with the staff when requesting theanalysis
On the appointed date Bring the sample and the solvent Your presence is required during the analyses
bull Sample preparation
The sample(s) must be as pure as possible correspondingto a concentration of 10-3 molL-1 in 10 mL
For each sample bring 30 mL of purified solvent
bull Results
On completion of the analyses the mostrepresentative curves are provided in paper copy
Upon request the electronic files can be emailed
Who to contactAlix Sournia-Saquet (Mgr)
Alain MoreauTel 05 61 33 31 75
Email alixsaquetlcc-toulousefralainmoreaulcc-toulousefr
Some advice
Before any analysis feel free to contact us for any
discussion or question about feasibility and conditions of
analyses
The staff can help you
- to choose the best-suited technique to your needs
- for interpretation of your data
Where to find us LCC- door B015ndash ground floor-building B205 route de Narbonne
When 9h to 11h30 -14h to 17h
From Monday to Friday
21
Magnetic Measurement and Moumlssbauer spectroscopy - LCC
How to request an analysis
bull For any analysis request
For magnetic measurements SQUID andMoumlssbauer spectroscopy please contact Jean-Franccedilois Meunier by e-mail or phone
An appointment will be set up in order to studyyour analyses requests and to define theexperimental conditions
An analysis request form will be provided by thestaff
bull Results and samples
Results are emailed as text and excel files
On completion of the analyses samples must beretrieved at LCC
Further information on equipments
lcc-toulousefrServices Spectroscopie Moumlssbauer
Lcc-toulousefr
servicesMesures
Magneacutetiques
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 10Email Jf-meunierlcc-toulousefr
Where to find usLCC door CS012
205 route de Narbonne
When 9h to 12h - 14h to 17h30
From Monday to Friday
Some advice
22
Elemental Analysis C-H-NS - LCC
How to request an analysis
For any analysis request
Each sample must be supplied with an analysis request formavailable on LCC website
wwwlcc-toulousefr gt services gt services techniques ampscientifiques gt analyses chimiques gt Formulaire
Fill in electronically and send by mail (see framed who tocontact)
Samples
- Internal in my box DEPOT CHN in the mail locker analyseselementaires
- External ship by courrier to LCC service CHN or ask anappointment
Results
Results are sent by mail Samples are not returned
Analyses
Analyses are carried out every week
10 mg of compound areneeded for 2 essays andpackaged in a vial
Sensitive samples mustbe isolated in sealedampoule
For special analysisrequests please contactservice
Sulphur is analyzed oncea year if enoughdemand
Who to contact Isabelle BorgetTel 05 61 33 32 14
mail isabelleborgetlcc-toulousefr
Where to find service LCC door B038
205 route de Narbonne
When 9h to 11h30 - 14h to 16h30
From monday to friday
on appointment
Some advice
23
Nuclear Magnetic Resonance - LCC
How to request an analysis
bull For any analysis request (except self-service equipments)
For NMR equipments (400-solid and 600 MHz) analysisand appointment requests must be emailed to Y Coppelor C Bijani
The analysis request form can be loaded from the NMRfacility webpage on the LCC website (httplcc-toulousefr)
bull Self-service equipments
All the users have to follow a training conducted by NMRfacilityrsquos staff before any use of self-service spectrometers
- for LCC teams the training and NMR user accountrequests are provided with taking office
- for outside labs please contact the LCC personneldepartment
The requests when validated must be returned directlyto A Bonnet or D Paryl in order to plan the training
The users undertake to carefully respect the operatinginstructions and the LCC memos
All the data are automatically
- made available in the LCC teamsrsquo laquo Nuage raquo file
- emailed to the user from outside labs
Feel free to contact us for any question
about analysis capabilities or for
any discussion about the best strategy to
meet your specific issues
Who to contact
Yannick Coppel (Mgr)Christian BijaniTel 05 61 17 54 27
Antoine BonnetDavid Paryl
Tel 05 61 17 54 30Email yannickcoppellcc-
toulousefrchristianbijanilcc-toulousefrantoinebonnetlcc-toulousefr
davidparyllcc-toulousefr
Some advice
Where to find us
LCC RMN Building 205 route de Narbonne Toulouse
Door 030 (Y Coppel et C Bijani)
Door 033 (F Lacassin et D Paryl)
When8h30 to 11h30 -14h to 17h
From Monday to Friday
24
Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) - LCC
How to request an analysis
bull For any analysis request
Each sample must be supplied with an analysisrequest form To request this form please contact the staff
Sample amount depends on the concentration of chemical elements to be measured in the sampleanalyzed
In the very first request please contact the staff
bull Results
Results are delivered in the letter-box of the LCC team or for outside labs made available in the ICP departmentrsquos letter-box (within the LCC entrance hall)
bull Analyses schedule
Analyses are carried out every 2 weeks
In general 10 mg per assay isneeded (provided that the
concentration is above 5 ww)
Chemical elements currentlyanalyzed (but not limited) Ag Al Au B Ba Be Bi Ca Cd Co Cr Cu Fe Ir K Li Mg Mn Na
Ni P Pb Pd Pt Ru Rh Sr Zn
Who to contact
Alain Moreau Tel 0561175850
E-mail alainmoreaulcc-toulousefr
Where to find usIPBS Bacirct A3
205 route de Narbonne
When 8h to 11h30 - 14h to 16h30From Monday to Friday (odd
week)
Some advice
25
Electronics
How to make a request
Who to contactJean-Michel Martin
Tel 05 61 55 86 93Email scicassistanceictchimieups-tlsefr
Email martinjmictchimieups-tlsefr
Feel free to ask the service for
- Modification of existingelectronic devices and
proposals for improvement
- Troubleshooting and repair of electronic
devices
- Advice on purchase of new material
bull For all installation andor maintenance of equipment with astrong electronic component
Send an email phone or contact the service in person duringoffice hours
bull For all service requests
Send an email toscicassistanceictchimieups-tlsefrstating your name office number and a brief description of the problem
bull Loan of equipment
To address the needs of users specific equipment is availablein the electronics workshop (Oscilloscope component testerssoldering ironhellip) aswell as various tools
It is possible to borrow this equipment
Where to find usDoor 1015 1st floor building 2R1 Universiteacute Paul Sabatier
When Monday-Friday office hours
If unattended make an appointment
Some advice
14
Information Technology
How to make a request
bull For all requests for connection to the network andcreation of email accounts
First see the secretary of your laboratory
bull For all service requests
Write toscicassistanceictchimieups-tlsefr
stating your name office number and a brief description of the problem
The IT service manages developsand maintains the
network and associated services
Please contact us for more information on
the services provided (automatic
backup of data access to Cambridge CCDC data sharing
etc)
Who to contactPascal Puech
Edouard IvanovtchikTel 05 61 55 68 73
Email scicassistanceictchimieups-tlsefr
Some advice
Where to find usDoor 168 ground floor building 2R1
Universiteacute Paul Sabatier
WhenMonday-Friday office hours
If unattended make an appointment
15
Scientific Glassware
How to make a request
bull For all service requests
All glassware to repair or construct must be accompanied bya fully completed form You can find this form on the ICTwebsite ictcnrsfrVerrerie-scientifique
For obvious reasons of safety and hygiene glassware must beclean free of silicon grease and in a container identified withthe name of the research group
bull Do I need to go in person
In person contact is preferred if you are new to glasswork andif your request is complex
Photos et technical drawings sent by email are onlycomplementary information as in isolation they can lead tomisunderstandings and errors
For all glass repairs construction of new
equipment or prototyping
feel free to consult the glassware service
We can provide technicaladvice as well as contacts
in specialized domains
Who to contactSteacutephane Foulon
Tel 05 61 55 61 16Email foulonictchimieups-
tlsefr
Some advice
Where to find us
Door 0194 Ground Floor Building 2R1Universiteacute Paul
Sabatier
When
Monday-Friday during office hours We recommend that
external users make an appointment
16
copyFreacutedeacuteric MaligneICT
LCC Services
17
Thermal Analyses LCC
How to request an analysis
bull For any analysis request
DTATGA or DSC analyses each sample must be suppliedwith an analysis request form duly filled out To requestthese forms please contact the staff by e-mail
In the very first request please contact the staff fordetails about the process the sample amount requiredthe packaging of samples etc
In all other cases the analyses requests and the samplescan be deposited in the Thermal Analyses Departmentrsquosletter-box (within the LCC entrance hall)
bull Air-sensitive samples
Make an appointment with the staff
bull Results
Analyses results are emailed as a text file paper copy isavailable upon request
On completion of analyses remaining of samples must bepick up at LCC
Analytical Equipments
DTATGA for measuring the mass variation as a
function of temperature
DSC for detecting the phase changes without mass loss
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 1 0Email j-fmeunierlcc-toulousefr
Some advice
Where to find usLCC - Door CS12 basement level
205 route de Narbonne
When Opening hours 9h to 11h30 - 14h to 17hfrom Monday to Friday except on wednesday
18
Library Resource Center LCC
How to make a request
bull For any information request
- LCC research teams fill out the request form available onthe LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs contact the staff by e-mail
bull For bibliographical searches and access
Digital databases
- LCC research teams bibliographical searches databases areavailable on the LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs make an appointment with the staff
Paper print collections
Paperprint collections also are available and can be read in thelibrary premises
LCCrsquos Library access is free for LCC teams and subject to anappointment for outside labs
LCC teams Access to the LCC intranet is provided
with taking office
For further information feel free to contact us
Who to contact
Marie-Heacutelegravene Gullimarie-helenegullilcc-toulousefr
0561333217
Gilles Roujasgillesroujaslcc-toulousefr
0561333140
Gaeumltan Havetgaetanhavetlcc-toulousefr
0561333140
Some advice
Where to find usLCC 205 route de Narbonne
When Opening hours
9 h to 11h30 - 13h to 17h From Monday to Friday
19
Feel free to contact us for anyquestion about analyses
options or for anydiscussion about the
best strategy to meetyour specific issues
Single ndashcrystal and powder X-Ray Diffraction - LCC
How to request an analysis
bull Prior to any analysis
Contact the staff in charge of X-Ray Diffraction measurementsfor your team or your lab
bull Single-crystal X-ray diffraction
First the staff will evaluate the quality of the sample If quality isacceptable for a X-ray diffraction measurement an appointmentwill be set up for analysis
Following information must be provided expected compound used solvents any specific information concerning the sample(air-sensitive thermal-sensitive light-sensitivehellip) analysis and required data (absolute configuration hydride locationhellip)
bull Powder X-ray diffraction
Appointments are proposed in accordance with the type of measurement (reflection capillary measurements at variable temperatures x-ray grazing incidence on thin films)
Following information must be provided sample characteristics analytical conditions (scanning range of 2theta temperaturehellip) required data (phase identification crystallites sizehellip)
Useful tips Until getting staff opinion about the quality of yoursample particularly for a single-crystal handle it as little as possible
Who to contact Laure Vendier (Mgr)
Carine DuhayonSonia Mallet-Ladeira
Tel 05 61 33 31 18Email laurevendierlcc-toulousefr
carineduhayonlcc-toulousefrladeiraictchimieups-tlsefr
Some advice
Where to find us
LCC 205 route de NarbonneX-Ray Diffraction office ground floor door B017 X-Ray Diffraction Lab basement level door GS66
When
9h to 11h30 - 14h to 17hFrom Monday to Friday except on Wednesday afternoon
20
Electrochemistry - LCC
How to request an analysis
bull For any analysis request
Analyses are carried out by appointment onlyscheduled with the staff when requesting theanalysis
On the appointed date Bring the sample and the solvent Your presence is required during the analyses
bull Sample preparation
The sample(s) must be as pure as possible correspondingto a concentration of 10-3 molL-1 in 10 mL
For each sample bring 30 mL of purified solvent
bull Results
On completion of the analyses the mostrepresentative curves are provided in paper copy
Upon request the electronic files can be emailed
Who to contactAlix Sournia-Saquet (Mgr)
Alain MoreauTel 05 61 33 31 75
Email alixsaquetlcc-toulousefralainmoreaulcc-toulousefr
Some advice
Before any analysis feel free to contact us for any
discussion or question about feasibility and conditions of
analyses
The staff can help you
- to choose the best-suited technique to your needs
- for interpretation of your data
Where to find us LCC- door B015ndash ground floor-building B205 route de Narbonne
When 9h to 11h30 -14h to 17h
From Monday to Friday
21
Magnetic Measurement and Moumlssbauer spectroscopy - LCC
How to request an analysis
bull For any analysis request
For magnetic measurements SQUID andMoumlssbauer spectroscopy please contact Jean-Franccedilois Meunier by e-mail or phone
An appointment will be set up in order to studyyour analyses requests and to define theexperimental conditions
An analysis request form will be provided by thestaff
bull Results and samples
Results are emailed as text and excel files
On completion of the analyses samples must beretrieved at LCC
Further information on equipments
lcc-toulousefrServices Spectroscopie Moumlssbauer
Lcc-toulousefr
servicesMesures
Magneacutetiques
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 10Email Jf-meunierlcc-toulousefr
Where to find usLCC door CS012
205 route de Narbonne
When 9h to 12h - 14h to 17h30
From Monday to Friday
Some advice
22
Elemental Analysis C-H-NS - LCC
How to request an analysis
For any analysis request
Each sample must be supplied with an analysis request formavailable on LCC website
wwwlcc-toulousefr gt services gt services techniques ampscientifiques gt analyses chimiques gt Formulaire
Fill in electronically and send by mail (see framed who tocontact)
Samples
- Internal in my box DEPOT CHN in the mail locker analyseselementaires
- External ship by courrier to LCC service CHN or ask anappointment
Results
Results are sent by mail Samples are not returned
Analyses
Analyses are carried out every week
10 mg of compound areneeded for 2 essays andpackaged in a vial
Sensitive samples mustbe isolated in sealedampoule
For special analysisrequests please contactservice
Sulphur is analyzed oncea year if enoughdemand
Who to contact Isabelle BorgetTel 05 61 33 32 14
mail isabelleborgetlcc-toulousefr
Where to find service LCC door B038
205 route de Narbonne
When 9h to 11h30 - 14h to 16h30
From monday to friday
on appointment
Some advice
23
Nuclear Magnetic Resonance - LCC
How to request an analysis
bull For any analysis request (except self-service equipments)
For NMR equipments (400-solid and 600 MHz) analysisand appointment requests must be emailed to Y Coppelor C Bijani
The analysis request form can be loaded from the NMRfacility webpage on the LCC website (httplcc-toulousefr)
bull Self-service equipments
All the users have to follow a training conducted by NMRfacilityrsquos staff before any use of self-service spectrometers
- for LCC teams the training and NMR user accountrequests are provided with taking office
- for outside labs please contact the LCC personneldepartment
The requests when validated must be returned directlyto A Bonnet or D Paryl in order to plan the training
The users undertake to carefully respect the operatinginstructions and the LCC memos
All the data are automatically
- made available in the LCC teamsrsquo laquo Nuage raquo file
- emailed to the user from outside labs
Feel free to contact us for any question
about analysis capabilities or for
any discussion about the best strategy to
meet your specific issues
Who to contact
Yannick Coppel (Mgr)Christian BijaniTel 05 61 17 54 27
Antoine BonnetDavid Paryl
Tel 05 61 17 54 30Email yannickcoppellcc-
toulousefrchristianbijanilcc-toulousefrantoinebonnetlcc-toulousefr
davidparyllcc-toulousefr
Some advice
Where to find us
LCC RMN Building 205 route de Narbonne Toulouse
Door 030 (Y Coppel et C Bijani)
Door 033 (F Lacassin et D Paryl)
When8h30 to 11h30 -14h to 17h
From Monday to Friday
24
Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) - LCC
How to request an analysis
bull For any analysis request
Each sample must be supplied with an analysisrequest form To request this form please contact the staff
Sample amount depends on the concentration of chemical elements to be measured in the sampleanalyzed
In the very first request please contact the staff
bull Results
Results are delivered in the letter-box of the LCC team or for outside labs made available in the ICP departmentrsquos letter-box (within the LCC entrance hall)
bull Analyses schedule
Analyses are carried out every 2 weeks
In general 10 mg per assay isneeded (provided that the
concentration is above 5 ww)
Chemical elements currentlyanalyzed (but not limited) Ag Al Au B Ba Be Bi Ca Cd Co Cr Cu Fe Ir K Li Mg Mn Na
Ni P Pb Pd Pt Ru Rh Sr Zn
Who to contact
Alain Moreau Tel 0561175850
E-mail alainmoreaulcc-toulousefr
Where to find usIPBS Bacirct A3
205 route de Narbonne
When 8h to 11h30 - 14h to 16h30From Monday to Friday (odd
week)
Some advice
25
Information Technology
How to make a request
bull For all requests for connection to the network andcreation of email accounts
First see the secretary of your laboratory
bull For all service requests
Write toscicassistanceictchimieups-tlsefr
stating your name office number and a brief description of the problem
The IT service manages developsand maintains the
network and associated services
Please contact us for more information on
the services provided (automatic
backup of data access to Cambridge CCDC data sharing
etc)
Who to contactPascal Puech
Edouard IvanovtchikTel 05 61 55 68 73
Email scicassistanceictchimieups-tlsefr
Some advice
Where to find usDoor 168 ground floor building 2R1
Universiteacute Paul Sabatier
WhenMonday-Friday office hours
If unattended make an appointment
15
Scientific Glassware
How to make a request
bull For all service requests
All glassware to repair or construct must be accompanied bya fully completed form You can find this form on the ICTwebsite ictcnrsfrVerrerie-scientifique
For obvious reasons of safety and hygiene glassware must beclean free of silicon grease and in a container identified withthe name of the research group
bull Do I need to go in person
In person contact is preferred if you are new to glasswork andif your request is complex
Photos et technical drawings sent by email are onlycomplementary information as in isolation they can lead tomisunderstandings and errors
For all glass repairs construction of new
equipment or prototyping
feel free to consult the glassware service
We can provide technicaladvice as well as contacts
in specialized domains
Who to contactSteacutephane Foulon
Tel 05 61 55 61 16Email foulonictchimieups-
tlsefr
Some advice
Where to find us
Door 0194 Ground Floor Building 2R1Universiteacute Paul
Sabatier
When
Monday-Friday during office hours We recommend that
external users make an appointment
16
copyFreacutedeacuteric MaligneICT
LCC Services
17
Thermal Analyses LCC
How to request an analysis
bull For any analysis request
DTATGA or DSC analyses each sample must be suppliedwith an analysis request form duly filled out To requestthese forms please contact the staff by e-mail
In the very first request please contact the staff fordetails about the process the sample amount requiredthe packaging of samples etc
In all other cases the analyses requests and the samplescan be deposited in the Thermal Analyses Departmentrsquosletter-box (within the LCC entrance hall)
bull Air-sensitive samples
Make an appointment with the staff
bull Results
Analyses results are emailed as a text file paper copy isavailable upon request
On completion of analyses remaining of samples must bepick up at LCC
Analytical Equipments
DTATGA for measuring the mass variation as a
function of temperature
DSC for detecting the phase changes without mass loss
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 1 0Email j-fmeunierlcc-toulousefr
Some advice
Where to find usLCC - Door CS12 basement level
205 route de Narbonne
When Opening hours 9h to 11h30 - 14h to 17hfrom Monday to Friday except on wednesday
18
Library Resource Center LCC
How to make a request
bull For any information request
- LCC research teams fill out the request form available onthe LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs contact the staff by e-mail
bull For bibliographical searches and access
Digital databases
- LCC research teams bibliographical searches databases areavailable on the LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs make an appointment with the staff
Paper print collections
Paperprint collections also are available and can be read in thelibrary premises
LCCrsquos Library access is free for LCC teams and subject to anappointment for outside labs
LCC teams Access to the LCC intranet is provided
with taking office
For further information feel free to contact us
Who to contact
Marie-Heacutelegravene Gullimarie-helenegullilcc-toulousefr
0561333217
Gilles Roujasgillesroujaslcc-toulousefr
0561333140
Gaeumltan Havetgaetanhavetlcc-toulousefr
0561333140
Some advice
Where to find usLCC 205 route de Narbonne
When Opening hours
9 h to 11h30 - 13h to 17h From Monday to Friday
19
Feel free to contact us for anyquestion about analyses
options or for anydiscussion about the
best strategy to meetyour specific issues
Single ndashcrystal and powder X-Ray Diffraction - LCC
How to request an analysis
bull Prior to any analysis
Contact the staff in charge of X-Ray Diffraction measurementsfor your team or your lab
bull Single-crystal X-ray diffraction
First the staff will evaluate the quality of the sample If quality isacceptable for a X-ray diffraction measurement an appointmentwill be set up for analysis
Following information must be provided expected compound used solvents any specific information concerning the sample(air-sensitive thermal-sensitive light-sensitivehellip) analysis and required data (absolute configuration hydride locationhellip)
bull Powder X-ray diffraction
Appointments are proposed in accordance with the type of measurement (reflection capillary measurements at variable temperatures x-ray grazing incidence on thin films)
Following information must be provided sample characteristics analytical conditions (scanning range of 2theta temperaturehellip) required data (phase identification crystallites sizehellip)
Useful tips Until getting staff opinion about the quality of yoursample particularly for a single-crystal handle it as little as possible
Who to contact Laure Vendier (Mgr)
Carine DuhayonSonia Mallet-Ladeira
Tel 05 61 33 31 18Email laurevendierlcc-toulousefr
carineduhayonlcc-toulousefrladeiraictchimieups-tlsefr
Some advice
Where to find us
LCC 205 route de NarbonneX-Ray Diffraction office ground floor door B017 X-Ray Diffraction Lab basement level door GS66
When
9h to 11h30 - 14h to 17hFrom Monday to Friday except on Wednesday afternoon
20
Electrochemistry - LCC
How to request an analysis
bull For any analysis request
Analyses are carried out by appointment onlyscheduled with the staff when requesting theanalysis
On the appointed date Bring the sample and the solvent Your presence is required during the analyses
bull Sample preparation
The sample(s) must be as pure as possible correspondingto a concentration of 10-3 molL-1 in 10 mL
For each sample bring 30 mL of purified solvent
bull Results
On completion of the analyses the mostrepresentative curves are provided in paper copy
Upon request the electronic files can be emailed
Who to contactAlix Sournia-Saquet (Mgr)
Alain MoreauTel 05 61 33 31 75
Email alixsaquetlcc-toulousefralainmoreaulcc-toulousefr
Some advice
Before any analysis feel free to contact us for any
discussion or question about feasibility and conditions of
analyses
The staff can help you
- to choose the best-suited technique to your needs
- for interpretation of your data
Where to find us LCC- door B015ndash ground floor-building B205 route de Narbonne
When 9h to 11h30 -14h to 17h
From Monday to Friday
21
Magnetic Measurement and Moumlssbauer spectroscopy - LCC
How to request an analysis
bull For any analysis request
For magnetic measurements SQUID andMoumlssbauer spectroscopy please contact Jean-Franccedilois Meunier by e-mail or phone
An appointment will be set up in order to studyyour analyses requests and to define theexperimental conditions
An analysis request form will be provided by thestaff
bull Results and samples
Results are emailed as text and excel files
On completion of the analyses samples must beretrieved at LCC
Further information on equipments
lcc-toulousefrServices Spectroscopie Moumlssbauer
Lcc-toulousefr
servicesMesures
Magneacutetiques
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 10Email Jf-meunierlcc-toulousefr
Where to find usLCC door CS012
205 route de Narbonne
When 9h to 12h - 14h to 17h30
From Monday to Friday
Some advice
22
Elemental Analysis C-H-NS - LCC
How to request an analysis
For any analysis request
Each sample must be supplied with an analysis request formavailable on LCC website
wwwlcc-toulousefr gt services gt services techniques ampscientifiques gt analyses chimiques gt Formulaire
Fill in electronically and send by mail (see framed who tocontact)
Samples
- Internal in my box DEPOT CHN in the mail locker analyseselementaires
- External ship by courrier to LCC service CHN or ask anappointment
Results
Results are sent by mail Samples are not returned
Analyses
Analyses are carried out every week
10 mg of compound areneeded for 2 essays andpackaged in a vial
Sensitive samples mustbe isolated in sealedampoule
For special analysisrequests please contactservice
Sulphur is analyzed oncea year if enoughdemand
Who to contact Isabelle BorgetTel 05 61 33 32 14
mail isabelleborgetlcc-toulousefr
Where to find service LCC door B038
205 route de Narbonne
When 9h to 11h30 - 14h to 16h30
From monday to friday
on appointment
Some advice
23
Nuclear Magnetic Resonance - LCC
How to request an analysis
bull For any analysis request (except self-service equipments)
For NMR equipments (400-solid and 600 MHz) analysisand appointment requests must be emailed to Y Coppelor C Bijani
The analysis request form can be loaded from the NMRfacility webpage on the LCC website (httplcc-toulousefr)
bull Self-service equipments
All the users have to follow a training conducted by NMRfacilityrsquos staff before any use of self-service spectrometers
- for LCC teams the training and NMR user accountrequests are provided with taking office
- for outside labs please contact the LCC personneldepartment
The requests when validated must be returned directlyto A Bonnet or D Paryl in order to plan the training
The users undertake to carefully respect the operatinginstructions and the LCC memos
All the data are automatically
- made available in the LCC teamsrsquo laquo Nuage raquo file
- emailed to the user from outside labs
Feel free to contact us for any question
about analysis capabilities or for
any discussion about the best strategy to
meet your specific issues
Who to contact
Yannick Coppel (Mgr)Christian BijaniTel 05 61 17 54 27
Antoine BonnetDavid Paryl
Tel 05 61 17 54 30Email yannickcoppellcc-
toulousefrchristianbijanilcc-toulousefrantoinebonnetlcc-toulousefr
davidparyllcc-toulousefr
Some advice
Where to find us
LCC RMN Building 205 route de Narbonne Toulouse
Door 030 (Y Coppel et C Bijani)
Door 033 (F Lacassin et D Paryl)
When8h30 to 11h30 -14h to 17h
From Monday to Friday
24
Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) - LCC
How to request an analysis
bull For any analysis request
Each sample must be supplied with an analysisrequest form To request this form please contact the staff
Sample amount depends on the concentration of chemical elements to be measured in the sampleanalyzed
In the very first request please contact the staff
bull Results
Results are delivered in the letter-box of the LCC team or for outside labs made available in the ICP departmentrsquos letter-box (within the LCC entrance hall)
bull Analyses schedule
Analyses are carried out every 2 weeks
In general 10 mg per assay isneeded (provided that the
concentration is above 5 ww)
Chemical elements currentlyanalyzed (but not limited) Ag Al Au B Ba Be Bi Ca Cd Co Cr Cu Fe Ir K Li Mg Mn Na
Ni P Pb Pd Pt Ru Rh Sr Zn
Who to contact
Alain Moreau Tel 0561175850
E-mail alainmoreaulcc-toulousefr
Where to find usIPBS Bacirct A3
205 route de Narbonne
When 8h to 11h30 - 14h to 16h30From Monday to Friday (odd
week)
Some advice
25
Scientific Glassware
How to make a request
bull For all service requests
All glassware to repair or construct must be accompanied bya fully completed form You can find this form on the ICTwebsite ictcnrsfrVerrerie-scientifique
For obvious reasons of safety and hygiene glassware must beclean free of silicon grease and in a container identified withthe name of the research group
bull Do I need to go in person
In person contact is preferred if you are new to glasswork andif your request is complex
Photos et technical drawings sent by email are onlycomplementary information as in isolation they can lead tomisunderstandings and errors
For all glass repairs construction of new
equipment or prototyping
feel free to consult the glassware service
We can provide technicaladvice as well as contacts
in specialized domains
Who to contactSteacutephane Foulon
Tel 05 61 55 61 16Email foulonictchimieups-
tlsefr
Some advice
Where to find us
Door 0194 Ground Floor Building 2R1Universiteacute Paul
Sabatier
When
Monday-Friday during office hours We recommend that
external users make an appointment
16
copyFreacutedeacuteric MaligneICT
LCC Services
17
Thermal Analyses LCC
How to request an analysis
bull For any analysis request
DTATGA or DSC analyses each sample must be suppliedwith an analysis request form duly filled out To requestthese forms please contact the staff by e-mail
In the very first request please contact the staff fordetails about the process the sample amount requiredthe packaging of samples etc
In all other cases the analyses requests and the samplescan be deposited in the Thermal Analyses Departmentrsquosletter-box (within the LCC entrance hall)
bull Air-sensitive samples
Make an appointment with the staff
bull Results
Analyses results are emailed as a text file paper copy isavailable upon request
On completion of analyses remaining of samples must bepick up at LCC
Analytical Equipments
DTATGA for measuring the mass variation as a
function of temperature
DSC for detecting the phase changes without mass loss
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 1 0Email j-fmeunierlcc-toulousefr
Some advice
Where to find usLCC - Door CS12 basement level
205 route de Narbonne
When Opening hours 9h to 11h30 - 14h to 17hfrom Monday to Friday except on wednesday
18
Library Resource Center LCC
How to make a request
bull For any information request
- LCC research teams fill out the request form available onthe LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs contact the staff by e-mail
bull For bibliographical searches and access
Digital databases
- LCC research teams bibliographical searches databases areavailable on the LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs make an appointment with the staff
Paper print collections
Paperprint collections also are available and can be read in thelibrary premises
LCCrsquos Library access is free for LCC teams and subject to anappointment for outside labs
LCC teams Access to the LCC intranet is provided
with taking office
For further information feel free to contact us
Who to contact
Marie-Heacutelegravene Gullimarie-helenegullilcc-toulousefr
0561333217
Gilles Roujasgillesroujaslcc-toulousefr
0561333140
Gaeumltan Havetgaetanhavetlcc-toulousefr
0561333140
Some advice
Where to find usLCC 205 route de Narbonne
When Opening hours
9 h to 11h30 - 13h to 17h From Monday to Friday
19
Feel free to contact us for anyquestion about analyses
options or for anydiscussion about the
best strategy to meetyour specific issues
Single ndashcrystal and powder X-Ray Diffraction - LCC
How to request an analysis
bull Prior to any analysis
Contact the staff in charge of X-Ray Diffraction measurementsfor your team or your lab
bull Single-crystal X-ray diffraction
First the staff will evaluate the quality of the sample If quality isacceptable for a X-ray diffraction measurement an appointmentwill be set up for analysis
Following information must be provided expected compound used solvents any specific information concerning the sample(air-sensitive thermal-sensitive light-sensitivehellip) analysis and required data (absolute configuration hydride locationhellip)
bull Powder X-ray diffraction
Appointments are proposed in accordance with the type of measurement (reflection capillary measurements at variable temperatures x-ray grazing incidence on thin films)
Following information must be provided sample characteristics analytical conditions (scanning range of 2theta temperaturehellip) required data (phase identification crystallites sizehellip)
Useful tips Until getting staff opinion about the quality of yoursample particularly for a single-crystal handle it as little as possible
Who to contact Laure Vendier (Mgr)
Carine DuhayonSonia Mallet-Ladeira
Tel 05 61 33 31 18Email laurevendierlcc-toulousefr
carineduhayonlcc-toulousefrladeiraictchimieups-tlsefr
Some advice
Where to find us
LCC 205 route de NarbonneX-Ray Diffraction office ground floor door B017 X-Ray Diffraction Lab basement level door GS66
When
9h to 11h30 - 14h to 17hFrom Monday to Friday except on Wednesday afternoon
20
Electrochemistry - LCC
How to request an analysis
bull For any analysis request
Analyses are carried out by appointment onlyscheduled with the staff when requesting theanalysis
On the appointed date Bring the sample and the solvent Your presence is required during the analyses
bull Sample preparation
The sample(s) must be as pure as possible correspondingto a concentration of 10-3 molL-1 in 10 mL
For each sample bring 30 mL of purified solvent
bull Results
On completion of the analyses the mostrepresentative curves are provided in paper copy
Upon request the electronic files can be emailed
Who to contactAlix Sournia-Saquet (Mgr)
Alain MoreauTel 05 61 33 31 75
Email alixsaquetlcc-toulousefralainmoreaulcc-toulousefr
Some advice
Before any analysis feel free to contact us for any
discussion or question about feasibility and conditions of
analyses
The staff can help you
- to choose the best-suited technique to your needs
- for interpretation of your data
Where to find us LCC- door B015ndash ground floor-building B205 route de Narbonne
When 9h to 11h30 -14h to 17h
From Monday to Friday
21
Magnetic Measurement and Moumlssbauer spectroscopy - LCC
How to request an analysis
bull For any analysis request
For magnetic measurements SQUID andMoumlssbauer spectroscopy please contact Jean-Franccedilois Meunier by e-mail or phone
An appointment will be set up in order to studyyour analyses requests and to define theexperimental conditions
An analysis request form will be provided by thestaff
bull Results and samples
Results are emailed as text and excel files
On completion of the analyses samples must beretrieved at LCC
Further information on equipments
lcc-toulousefrServices Spectroscopie Moumlssbauer
Lcc-toulousefr
servicesMesures
Magneacutetiques
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 10Email Jf-meunierlcc-toulousefr
Where to find usLCC door CS012
205 route de Narbonne
When 9h to 12h - 14h to 17h30
From Monday to Friday
Some advice
22
Elemental Analysis C-H-NS - LCC
How to request an analysis
For any analysis request
Each sample must be supplied with an analysis request formavailable on LCC website
wwwlcc-toulousefr gt services gt services techniques ampscientifiques gt analyses chimiques gt Formulaire
Fill in electronically and send by mail (see framed who tocontact)
Samples
- Internal in my box DEPOT CHN in the mail locker analyseselementaires
- External ship by courrier to LCC service CHN or ask anappointment
Results
Results are sent by mail Samples are not returned
Analyses
Analyses are carried out every week
10 mg of compound areneeded for 2 essays andpackaged in a vial
Sensitive samples mustbe isolated in sealedampoule
For special analysisrequests please contactservice
Sulphur is analyzed oncea year if enoughdemand
Who to contact Isabelle BorgetTel 05 61 33 32 14
mail isabelleborgetlcc-toulousefr
Where to find service LCC door B038
205 route de Narbonne
When 9h to 11h30 - 14h to 16h30
From monday to friday
on appointment
Some advice
23
Nuclear Magnetic Resonance - LCC
How to request an analysis
bull For any analysis request (except self-service equipments)
For NMR equipments (400-solid and 600 MHz) analysisand appointment requests must be emailed to Y Coppelor C Bijani
The analysis request form can be loaded from the NMRfacility webpage on the LCC website (httplcc-toulousefr)
bull Self-service equipments
All the users have to follow a training conducted by NMRfacilityrsquos staff before any use of self-service spectrometers
- for LCC teams the training and NMR user accountrequests are provided with taking office
- for outside labs please contact the LCC personneldepartment
The requests when validated must be returned directlyto A Bonnet or D Paryl in order to plan the training
The users undertake to carefully respect the operatinginstructions and the LCC memos
All the data are automatically
- made available in the LCC teamsrsquo laquo Nuage raquo file
- emailed to the user from outside labs
Feel free to contact us for any question
about analysis capabilities or for
any discussion about the best strategy to
meet your specific issues
Who to contact
Yannick Coppel (Mgr)Christian BijaniTel 05 61 17 54 27
Antoine BonnetDavid Paryl
Tel 05 61 17 54 30Email yannickcoppellcc-
toulousefrchristianbijanilcc-toulousefrantoinebonnetlcc-toulousefr
davidparyllcc-toulousefr
Some advice
Where to find us
LCC RMN Building 205 route de Narbonne Toulouse
Door 030 (Y Coppel et C Bijani)
Door 033 (F Lacassin et D Paryl)
When8h30 to 11h30 -14h to 17h
From Monday to Friday
24
Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) - LCC
How to request an analysis
bull For any analysis request
Each sample must be supplied with an analysisrequest form To request this form please contact the staff
Sample amount depends on the concentration of chemical elements to be measured in the sampleanalyzed
In the very first request please contact the staff
bull Results
Results are delivered in the letter-box of the LCC team or for outside labs made available in the ICP departmentrsquos letter-box (within the LCC entrance hall)
bull Analyses schedule
Analyses are carried out every 2 weeks
In general 10 mg per assay isneeded (provided that the
concentration is above 5 ww)
Chemical elements currentlyanalyzed (but not limited) Ag Al Au B Ba Be Bi Ca Cd Co Cr Cu Fe Ir K Li Mg Mn Na
Ni P Pb Pd Pt Ru Rh Sr Zn
Who to contact
Alain Moreau Tel 0561175850
E-mail alainmoreaulcc-toulousefr
Where to find usIPBS Bacirct A3
205 route de Narbonne
When 8h to 11h30 - 14h to 16h30From Monday to Friday (odd
week)
Some advice
25
LCC Services
17
Thermal Analyses LCC
How to request an analysis
bull For any analysis request
DTATGA or DSC analyses each sample must be suppliedwith an analysis request form duly filled out To requestthese forms please contact the staff by e-mail
In the very first request please contact the staff fordetails about the process the sample amount requiredthe packaging of samples etc
In all other cases the analyses requests and the samplescan be deposited in the Thermal Analyses Departmentrsquosletter-box (within the LCC entrance hall)
bull Air-sensitive samples
Make an appointment with the staff
bull Results
Analyses results are emailed as a text file paper copy isavailable upon request
On completion of analyses remaining of samples must bepick up at LCC
Analytical Equipments
DTATGA for measuring the mass variation as a
function of temperature
DSC for detecting the phase changes without mass loss
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 1 0Email j-fmeunierlcc-toulousefr
Some advice
Where to find usLCC - Door CS12 basement level
205 route de Narbonne
When Opening hours 9h to 11h30 - 14h to 17hfrom Monday to Friday except on wednesday
18
Library Resource Center LCC
How to make a request
bull For any information request
- LCC research teams fill out the request form available onthe LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs contact the staff by e-mail
bull For bibliographical searches and access
Digital databases
- LCC research teams bibliographical searches databases areavailable on the LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs make an appointment with the staff
Paper print collections
Paperprint collections also are available and can be read in thelibrary premises
LCCrsquos Library access is free for LCC teams and subject to anappointment for outside labs
LCC teams Access to the LCC intranet is provided
with taking office
For further information feel free to contact us
Who to contact
Marie-Heacutelegravene Gullimarie-helenegullilcc-toulousefr
0561333217
Gilles Roujasgillesroujaslcc-toulousefr
0561333140
Gaeumltan Havetgaetanhavetlcc-toulousefr
0561333140
Some advice
Where to find usLCC 205 route de Narbonne
When Opening hours
9 h to 11h30 - 13h to 17h From Monday to Friday
19
Feel free to contact us for anyquestion about analyses
options or for anydiscussion about the
best strategy to meetyour specific issues
Single ndashcrystal and powder X-Ray Diffraction - LCC
How to request an analysis
bull Prior to any analysis
Contact the staff in charge of X-Ray Diffraction measurementsfor your team or your lab
bull Single-crystal X-ray diffraction
First the staff will evaluate the quality of the sample If quality isacceptable for a X-ray diffraction measurement an appointmentwill be set up for analysis
Following information must be provided expected compound used solvents any specific information concerning the sample(air-sensitive thermal-sensitive light-sensitivehellip) analysis and required data (absolute configuration hydride locationhellip)
bull Powder X-ray diffraction
Appointments are proposed in accordance with the type of measurement (reflection capillary measurements at variable temperatures x-ray grazing incidence on thin films)
Following information must be provided sample characteristics analytical conditions (scanning range of 2theta temperaturehellip) required data (phase identification crystallites sizehellip)
Useful tips Until getting staff opinion about the quality of yoursample particularly for a single-crystal handle it as little as possible
Who to contact Laure Vendier (Mgr)
Carine DuhayonSonia Mallet-Ladeira
Tel 05 61 33 31 18Email laurevendierlcc-toulousefr
carineduhayonlcc-toulousefrladeiraictchimieups-tlsefr
Some advice
Where to find us
LCC 205 route de NarbonneX-Ray Diffraction office ground floor door B017 X-Ray Diffraction Lab basement level door GS66
When
9h to 11h30 - 14h to 17hFrom Monday to Friday except on Wednesday afternoon
20
Electrochemistry - LCC
How to request an analysis
bull For any analysis request
Analyses are carried out by appointment onlyscheduled with the staff when requesting theanalysis
On the appointed date Bring the sample and the solvent Your presence is required during the analyses
bull Sample preparation
The sample(s) must be as pure as possible correspondingto a concentration of 10-3 molL-1 in 10 mL
For each sample bring 30 mL of purified solvent
bull Results
On completion of the analyses the mostrepresentative curves are provided in paper copy
Upon request the electronic files can be emailed
Who to contactAlix Sournia-Saquet (Mgr)
Alain MoreauTel 05 61 33 31 75
Email alixsaquetlcc-toulousefralainmoreaulcc-toulousefr
Some advice
Before any analysis feel free to contact us for any
discussion or question about feasibility and conditions of
analyses
The staff can help you
- to choose the best-suited technique to your needs
- for interpretation of your data
Where to find us LCC- door B015ndash ground floor-building B205 route de Narbonne
When 9h to 11h30 -14h to 17h
From Monday to Friday
21
Magnetic Measurement and Moumlssbauer spectroscopy - LCC
How to request an analysis
bull For any analysis request
For magnetic measurements SQUID andMoumlssbauer spectroscopy please contact Jean-Franccedilois Meunier by e-mail or phone
An appointment will be set up in order to studyyour analyses requests and to define theexperimental conditions
An analysis request form will be provided by thestaff
bull Results and samples
Results are emailed as text and excel files
On completion of the analyses samples must beretrieved at LCC
Further information on equipments
lcc-toulousefrServices Spectroscopie Moumlssbauer
Lcc-toulousefr
servicesMesures
Magneacutetiques
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 10Email Jf-meunierlcc-toulousefr
Where to find usLCC door CS012
205 route de Narbonne
When 9h to 12h - 14h to 17h30
From Monday to Friday
Some advice
22
Elemental Analysis C-H-NS - LCC
How to request an analysis
For any analysis request
Each sample must be supplied with an analysis request formavailable on LCC website
wwwlcc-toulousefr gt services gt services techniques ampscientifiques gt analyses chimiques gt Formulaire
Fill in electronically and send by mail (see framed who tocontact)
Samples
- Internal in my box DEPOT CHN in the mail locker analyseselementaires
- External ship by courrier to LCC service CHN or ask anappointment
Results
Results are sent by mail Samples are not returned
Analyses
Analyses are carried out every week
10 mg of compound areneeded for 2 essays andpackaged in a vial
Sensitive samples mustbe isolated in sealedampoule
For special analysisrequests please contactservice
Sulphur is analyzed oncea year if enoughdemand
Who to contact Isabelle BorgetTel 05 61 33 32 14
mail isabelleborgetlcc-toulousefr
Where to find service LCC door B038
205 route de Narbonne
When 9h to 11h30 - 14h to 16h30
From monday to friday
on appointment
Some advice
23
Nuclear Magnetic Resonance - LCC
How to request an analysis
bull For any analysis request (except self-service equipments)
For NMR equipments (400-solid and 600 MHz) analysisand appointment requests must be emailed to Y Coppelor C Bijani
The analysis request form can be loaded from the NMRfacility webpage on the LCC website (httplcc-toulousefr)
bull Self-service equipments
All the users have to follow a training conducted by NMRfacilityrsquos staff before any use of self-service spectrometers
- for LCC teams the training and NMR user accountrequests are provided with taking office
- for outside labs please contact the LCC personneldepartment
The requests when validated must be returned directlyto A Bonnet or D Paryl in order to plan the training
The users undertake to carefully respect the operatinginstructions and the LCC memos
All the data are automatically
- made available in the LCC teamsrsquo laquo Nuage raquo file
- emailed to the user from outside labs
Feel free to contact us for any question
about analysis capabilities or for
any discussion about the best strategy to
meet your specific issues
Who to contact
Yannick Coppel (Mgr)Christian BijaniTel 05 61 17 54 27
Antoine BonnetDavid Paryl
Tel 05 61 17 54 30Email yannickcoppellcc-
toulousefrchristianbijanilcc-toulousefrantoinebonnetlcc-toulousefr
davidparyllcc-toulousefr
Some advice
Where to find us
LCC RMN Building 205 route de Narbonne Toulouse
Door 030 (Y Coppel et C Bijani)
Door 033 (F Lacassin et D Paryl)
When8h30 to 11h30 -14h to 17h
From Monday to Friday
24
Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) - LCC
How to request an analysis
bull For any analysis request
Each sample must be supplied with an analysisrequest form To request this form please contact the staff
Sample amount depends on the concentration of chemical elements to be measured in the sampleanalyzed
In the very first request please contact the staff
bull Results
Results are delivered in the letter-box of the LCC team or for outside labs made available in the ICP departmentrsquos letter-box (within the LCC entrance hall)
bull Analyses schedule
Analyses are carried out every 2 weeks
In general 10 mg per assay isneeded (provided that the
concentration is above 5 ww)
Chemical elements currentlyanalyzed (but not limited) Ag Al Au B Ba Be Bi Ca Cd Co Cr Cu Fe Ir K Li Mg Mn Na
Ni P Pb Pd Pt Ru Rh Sr Zn
Who to contact
Alain Moreau Tel 0561175850
E-mail alainmoreaulcc-toulousefr
Where to find usIPBS Bacirct A3
205 route de Narbonne
When 8h to 11h30 - 14h to 16h30From Monday to Friday (odd
week)
Some advice
25
Thermal Analyses LCC
How to request an analysis
bull For any analysis request
DTATGA or DSC analyses each sample must be suppliedwith an analysis request form duly filled out To requestthese forms please contact the staff by e-mail
In the very first request please contact the staff fordetails about the process the sample amount requiredthe packaging of samples etc
In all other cases the analyses requests and the samplescan be deposited in the Thermal Analyses Departmentrsquosletter-box (within the LCC entrance hall)
bull Air-sensitive samples
Make an appointment with the staff
bull Results
Analyses results are emailed as a text file paper copy isavailable upon request
On completion of analyses remaining of samples must bepick up at LCC
Analytical Equipments
DTATGA for measuring the mass variation as a
function of temperature
DSC for detecting the phase changes without mass loss
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 1 0Email j-fmeunierlcc-toulousefr
Some advice
Where to find usLCC - Door CS12 basement level
205 route de Narbonne
When Opening hours 9h to 11h30 - 14h to 17hfrom Monday to Friday except on wednesday
18
Library Resource Center LCC
How to make a request
bull For any information request
- LCC research teams fill out the request form available onthe LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs contact the staff by e-mail
bull For bibliographical searches and access
Digital databases
- LCC research teams bibliographical searches databases areavailable on the LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs make an appointment with the staff
Paper print collections
Paperprint collections also are available and can be read in thelibrary premises
LCCrsquos Library access is free for LCC teams and subject to anappointment for outside labs
LCC teams Access to the LCC intranet is provided
with taking office
For further information feel free to contact us
Who to contact
Marie-Heacutelegravene Gullimarie-helenegullilcc-toulousefr
0561333217
Gilles Roujasgillesroujaslcc-toulousefr
0561333140
Gaeumltan Havetgaetanhavetlcc-toulousefr
0561333140
Some advice
Where to find usLCC 205 route de Narbonne
When Opening hours
9 h to 11h30 - 13h to 17h From Monday to Friday
19
Feel free to contact us for anyquestion about analyses
options or for anydiscussion about the
best strategy to meetyour specific issues
Single ndashcrystal and powder X-Ray Diffraction - LCC
How to request an analysis
bull Prior to any analysis
Contact the staff in charge of X-Ray Diffraction measurementsfor your team or your lab
bull Single-crystal X-ray diffraction
First the staff will evaluate the quality of the sample If quality isacceptable for a X-ray diffraction measurement an appointmentwill be set up for analysis
Following information must be provided expected compound used solvents any specific information concerning the sample(air-sensitive thermal-sensitive light-sensitivehellip) analysis and required data (absolute configuration hydride locationhellip)
bull Powder X-ray diffraction
Appointments are proposed in accordance with the type of measurement (reflection capillary measurements at variable temperatures x-ray grazing incidence on thin films)
Following information must be provided sample characteristics analytical conditions (scanning range of 2theta temperaturehellip) required data (phase identification crystallites sizehellip)
Useful tips Until getting staff opinion about the quality of yoursample particularly for a single-crystal handle it as little as possible
Who to contact Laure Vendier (Mgr)
Carine DuhayonSonia Mallet-Ladeira
Tel 05 61 33 31 18Email laurevendierlcc-toulousefr
carineduhayonlcc-toulousefrladeiraictchimieups-tlsefr
Some advice
Where to find us
LCC 205 route de NarbonneX-Ray Diffraction office ground floor door B017 X-Ray Diffraction Lab basement level door GS66
When
9h to 11h30 - 14h to 17hFrom Monday to Friday except on Wednesday afternoon
20
Electrochemistry - LCC
How to request an analysis
bull For any analysis request
Analyses are carried out by appointment onlyscheduled with the staff when requesting theanalysis
On the appointed date Bring the sample and the solvent Your presence is required during the analyses
bull Sample preparation
The sample(s) must be as pure as possible correspondingto a concentration of 10-3 molL-1 in 10 mL
For each sample bring 30 mL of purified solvent
bull Results
On completion of the analyses the mostrepresentative curves are provided in paper copy
Upon request the electronic files can be emailed
Who to contactAlix Sournia-Saquet (Mgr)
Alain MoreauTel 05 61 33 31 75
Email alixsaquetlcc-toulousefralainmoreaulcc-toulousefr
Some advice
Before any analysis feel free to contact us for any
discussion or question about feasibility and conditions of
analyses
The staff can help you
- to choose the best-suited technique to your needs
- for interpretation of your data
Where to find us LCC- door B015ndash ground floor-building B205 route de Narbonne
When 9h to 11h30 -14h to 17h
From Monday to Friday
21
Magnetic Measurement and Moumlssbauer spectroscopy - LCC
How to request an analysis
bull For any analysis request
For magnetic measurements SQUID andMoumlssbauer spectroscopy please contact Jean-Franccedilois Meunier by e-mail or phone
An appointment will be set up in order to studyyour analyses requests and to define theexperimental conditions
An analysis request form will be provided by thestaff
bull Results and samples
Results are emailed as text and excel files
On completion of the analyses samples must beretrieved at LCC
Further information on equipments
lcc-toulousefrServices Spectroscopie Moumlssbauer
Lcc-toulousefr
servicesMesures
Magneacutetiques
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 10Email Jf-meunierlcc-toulousefr
Where to find usLCC door CS012
205 route de Narbonne
When 9h to 12h - 14h to 17h30
From Monday to Friday
Some advice
22
Elemental Analysis C-H-NS - LCC
How to request an analysis
For any analysis request
Each sample must be supplied with an analysis request formavailable on LCC website
wwwlcc-toulousefr gt services gt services techniques ampscientifiques gt analyses chimiques gt Formulaire
Fill in electronically and send by mail (see framed who tocontact)
Samples
- Internal in my box DEPOT CHN in the mail locker analyseselementaires
- External ship by courrier to LCC service CHN or ask anappointment
Results
Results are sent by mail Samples are not returned
Analyses
Analyses are carried out every week
10 mg of compound areneeded for 2 essays andpackaged in a vial
Sensitive samples mustbe isolated in sealedampoule
For special analysisrequests please contactservice
Sulphur is analyzed oncea year if enoughdemand
Who to contact Isabelle BorgetTel 05 61 33 32 14
mail isabelleborgetlcc-toulousefr
Where to find service LCC door B038
205 route de Narbonne
When 9h to 11h30 - 14h to 16h30
From monday to friday
on appointment
Some advice
23
Nuclear Magnetic Resonance - LCC
How to request an analysis
bull For any analysis request (except self-service equipments)
For NMR equipments (400-solid and 600 MHz) analysisand appointment requests must be emailed to Y Coppelor C Bijani
The analysis request form can be loaded from the NMRfacility webpage on the LCC website (httplcc-toulousefr)
bull Self-service equipments
All the users have to follow a training conducted by NMRfacilityrsquos staff before any use of self-service spectrometers
- for LCC teams the training and NMR user accountrequests are provided with taking office
- for outside labs please contact the LCC personneldepartment
The requests when validated must be returned directlyto A Bonnet or D Paryl in order to plan the training
The users undertake to carefully respect the operatinginstructions and the LCC memos
All the data are automatically
- made available in the LCC teamsrsquo laquo Nuage raquo file
- emailed to the user from outside labs
Feel free to contact us for any question
about analysis capabilities or for
any discussion about the best strategy to
meet your specific issues
Who to contact
Yannick Coppel (Mgr)Christian BijaniTel 05 61 17 54 27
Antoine BonnetDavid Paryl
Tel 05 61 17 54 30Email yannickcoppellcc-
toulousefrchristianbijanilcc-toulousefrantoinebonnetlcc-toulousefr
davidparyllcc-toulousefr
Some advice
Where to find us
LCC RMN Building 205 route de Narbonne Toulouse
Door 030 (Y Coppel et C Bijani)
Door 033 (F Lacassin et D Paryl)
When8h30 to 11h30 -14h to 17h
From Monday to Friday
24
Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) - LCC
How to request an analysis
bull For any analysis request
Each sample must be supplied with an analysisrequest form To request this form please contact the staff
Sample amount depends on the concentration of chemical elements to be measured in the sampleanalyzed
In the very first request please contact the staff
bull Results
Results are delivered in the letter-box of the LCC team or for outside labs made available in the ICP departmentrsquos letter-box (within the LCC entrance hall)
bull Analyses schedule
Analyses are carried out every 2 weeks
In general 10 mg per assay isneeded (provided that the
concentration is above 5 ww)
Chemical elements currentlyanalyzed (but not limited) Ag Al Au B Ba Be Bi Ca Cd Co Cr Cu Fe Ir K Li Mg Mn Na
Ni P Pb Pd Pt Ru Rh Sr Zn
Who to contact
Alain Moreau Tel 0561175850
E-mail alainmoreaulcc-toulousefr
Where to find usIPBS Bacirct A3
205 route de Narbonne
When 8h to 11h30 - 14h to 16h30From Monday to Friday (odd
week)
Some advice
25
Library Resource Center LCC
How to make a request
bull For any information request
- LCC research teams fill out the request form available onthe LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs contact the staff by e-mail
bull For bibliographical searches and access
Digital databases
- LCC research teams bibliographical searches databases areavailable on the LCC website (laquo intranet raquo section laquo Documentation raquo)
- Outside labs make an appointment with the staff
Paper print collections
Paperprint collections also are available and can be read in thelibrary premises
LCCrsquos Library access is free for LCC teams and subject to anappointment for outside labs
LCC teams Access to the LCC intranet is provided
with taking office
For further information feel free to contact us
Who to contact
Marie-Heacutelegravene Gullimarie-helenegullilcc-toulousefr
0561333217
Gilles Roujasgillesroujaslcc-toulousefr
0561333140
Gaeumltan Havetgaetanhavetlcc-toulousefr
0561333140
Some advice
Where to find usLCC 205 route de Narbonne
When Opening hours
9 h to 11h30 - 13h to 17h From Monday to Friday
19
Feel free to contact us for anyquestion about analyses
options or for anydiscussion about the
best strategy to meetyour specific issues
Single ndashcrystal and powder X-Ray Diffraction - LCC
How to request an analysis
bull Prior to any analysis
Contact the staff in charge of X-Ray Diffraction measurementsfor your team or your lab
bull Single-crystal X-ray diffraction
First the staff will evaluate the quality of the sample If quality isacceptable for a X-ray diffraction measurement an appointmentwill be set up for analysis
Following information must be provided expected compound used solvents any specific information concerning the sample(air-sensitive thermal-sensitive light-sensitivehellip) analysis and required data (absolute configuration hydride locationhellip)
bull Powder X-ray diffraction
Appointments are proposed in accordance with the type of measurement (reflection capillary measurements at variable temperatures x-ray grazing incidence on thin films)
Following information must be provided sample characteristics analytical conditions (scanning range of 2theta temperaturehellip) required data (phase identification crystallites sizehellip)
Useful tips Until getting staff opinion about the quality of yoursample particularly for a single-crystal handle it as little as possible
Who to contact Laure Vendier (Mgr)
Carine DuhayonSonia Mallet-Ladeira
Tel 05 61 33 31 18Email laurevendierlcc-toulousefr
carineduhayonlcc-toulousefrladeiraictchimieups-tlsefr
Some advice
Where to find us
LCC 205 route de NarbonneX-Ray Diffraction office ground floor door B017 X-Ray Diffraction Lab basement level door GS66
When
9h to 11h30 - 14h to 17hFrom Monday to Friday except on Wednesday afternoon
20
Electrochemistry - LCC
How to request an analysis
bull For any analysis request
Analyses are carried out by appointment onlyscheduled with the staff when requesting theanalysis
On the appointed date Bring the sample and the solvent Your presence is required during the analyses
bull Sample preparation
The sample(s) must be as pure as possible correspondingto a concentration of 10-3 molL-1 in 10 mL
For each sample bring 30 mL of purified solvent
bull Results
On completion of the analyses the mostrepresentative curves are provided in paper copy
Upon request the electronic files can be emailed
Who to contactAlix Sournia-Saquet (Mgr)
Alain MoreauTel 05 61 33 31 75
Email alixsaquetlcc-toulousefralainmoreaulcc-toulousefr
Some advice
Before any analysis feel free to contact us for any
discussion or question about feasibility and conditions of
analyses
The staff can help you
- to choose the best-suited technique to your needs
- for interpretation of your data
Where to find us LCC- door B015ndash ground floor-building B205 route de Narbonne
When 9h to 11h30 -14h to 17h
From Monday to Friday
21
Magnetic Measurement and Moumlssbauer spectroscopy - LCC
How to request an analysis
bull For any analysis request
For magnetic measurements SQUID andMoumlssbauer spectroscopy please contact Jean-Franccedilois Meunier by e-mail or phone
An appointment will be set up in order to studyyour analyses requests and to define theexperimental conditions
An analysis request form will be provided by thestaff
bull Results and samples
Results are emailed as text and excel files
On completion of the analyses samples must beretrieved at LCC
Further information on equipments
lcc-toulousefrServices Spectroscopie Moumlssbauer
Lcc-toulousefr
servicesMesures
Magneacutetiques
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 10Email Jf-meunierlcc-toulousefr
Where to find usLCC door CS012
205 route de Narbonne
When 9h to 12h - 14h to 17h30
From Monday to Friday
Some advice
22
Elemental Analysis C-H-NS - LCC
How to request an analysis
For any analysis request
Each sample must be supplied with an analysis request formavailable on LCC website
wwwlcc-toulousefr gt services gt services techniques ampscientifiques gt analyses chimiques gt Formulaire
Fill in electronically and send by mail (see framed who tocontact)
Samples
- Internal in my box DEPOT CHN in the mail locker analyseselementaires
- External ship by courrier to LCC service CHN or ask anappointment
Results
Results are sent by mail Samples are not returned
Analyses
Analyses are carried out every week
10 mg of compound areneeded for 2 essays andpackaged in a vial
Sensitive samples mustbe isolated in sealedampoule
For special analysisrequests please contactservice
Sulphur is analyzed oncea year if enoughdemand
Who to contact Isabelle BorgetTel 05 61 33 32 14
mail isabelleborgetlcc-toulousefr
Where to find service LCC door B038
205 route de Narbonne
When 9h to 11h30 - 14h to 16h30
From monday to friday
on appointment
Some advice
23
Nuclear Magnetic Resonance - LCC
How to request an analysis
bull For any analysis request (except self-service equipments)
For NMR equipments (400-solid and 600 MHz) analysisand appointment requests must be emailed to Y Coppelor C Bijani
The analysis request form can be loaded from the NMRfacility webpage on the LCC website (httplcc-toulousefr)
bull Self-service equipments
All the users have to follow a training conducted by NMRfacilityrsquos staff before any use of self-service spectrometers
- for LCC teams the training and NMR user accountrequests are provided with taking office
- for outside labs please contact the LCC personneldepartment
The requests when validated must be returned directlyto A Bonnet or D Paryl in order to plan the training
The users undertake to carefully respect the operatinginstructions and the LCC memos
All the data are automatically
- made available in the LCC teamsrsquo laquo Nuage raquo file
- emailed to the user from outside labs
Feel free to contact us for any question
about analysis capabilities or for
any discussion about the best strategy to
meet your specific issues
Who to contact
Yannick Coppel (Mgr)Christian BijaniTel 05 61 17 54 27
Antoine BonnetDavid Paryl
Tel 05 61 17 54 30Email yannickcoppellcc-
toulousefrchristianbijanilcc-toulousefrantoinebonnetlcc-toulousefr
davidparyllcc-toulousefr
Some advice
Where to find us
LCC RMN Building 205 route de Narbonne Toulouse
Door 030 (Y Coppel et C Bijani)
Door 033 (F Lacassin et D Paryl)
When8h30 to 11h30 -14h to 17h
From Monday to Friday
24
Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) - LCC
How to request an analysis
bull For any analysis request
Each sample must be supplied with an analysisrequest form To request this form please contact the staff
Sample amount depends on the concentration of chemical elements to be measured in the sampleanalyzed
In the very first request please contact the staff
bull Results
Results are delivered in the letter-box of the LCC team or for outside labs made available in the ICP departmentrsquos letter-box (within the LCC entrance hall)
bull Analyses schedule
Analyses are carried out every 2 weeks
In general 10 mg per assay isneeded (provided that the
concentration is above 5 ww)
Chemical elements currentlyanalyzed (but not limited) Ag Al Au B Ba Be Bi Ca Cd Co Cr Cu Fe Ir K Li Mg Mn Na
Ni P Pb Pd Pt Ru Rh Sr Zn
Who to contact
Alain Moreau Tel 0561175850
E-mail alainmoreaulcc-toulousefr
Where to find usIPBS Bacirct A3
205 route de Narbonne
When 8h to 11h30 - 14h to 16h30From Monday to Friday (odd
week)
Some advice
25
Feel free to contact us for anyquestion about analyses
options or for anydiscussion about the
best strategy to meetyour specific issues
Single ndashcrystal and powder X-Ray Diffraction - LCC
How to request an analysis
bull Prior to any analysis
Contact the staff in charge of X-Ray Diffraction measurementsfor your team or your lab
bull Single-crystal X-ray diffraction
First the staff will evaluate the quality of the sample If quality isacceptable for a X-ray diffraction measurement an appointmentwill be set up for analysis
Following information must be provided expected compound used solvents any specific information concerning the sample(air-sensitive thermal-sensitive light-sensitivehellip) analysis and required data (absolute configuration hydride locationhellip)
bull Powder X-ray diffraction
Appointments are proposed in accordance with the type of measurement (reflection capillary measurements at variable temperatures x-ray grazing incidence on thin films)
Following information must be provided sample characteristics analytical conditions (scanning range of 2theta temperaturehellip) required data (phase identification crystallites sizehellip)
Useful tips Until getting staff opinion about the quality of yoursample particularly for a single-crystal handle it as little as possible
Who to contact Laure Vendier (Mgr)
Carine DuhayonSonia Mallet-Ladeira
Tel 05 61 33 31 18Email laurevendierlcc-toulousefr
carineduhayonlcc-toulousefrladeiraictchimieups-tlsefr
Some advice
Where to find us
LCC 205 route de NarbonneX-Ray Diffraction office ground floor door B017 X-Ray Diffraction Lab basement level door GS66
When
9h to 11h30 - 14h to 17hFrom Monday to Friday except on Wednesday afternoon
20
Electrochemistry - LCC
How to request an analysis
bull For any analysis request
Analyses are carried out by appointment onlyscheduled with the staff when requesting theanalysis
On the appointed date Bring the sample and the solvent Your presence is required during the analyses
bull Sample preparation
The sample(s) must be as pure as possible correspondingto a concentration of 10-3 molL-1 in 10 mL
For each sample bring 30 mL of purified solvent
bull Results
On completion of the analyses the mostrepresentative curves are provided in paper copy
Upon request the electronic files can be emailed
Who to contactAlix Sournia-Saquet (Mgr)
Alain MoreauTel 05 61 33 31 75
Email alixsaquetlcc-toulousefralainmoreaulcc-toulousefr
Some advice
Before any analysis feel free to contact us for any
discussion or question about feasibility and conditions of
analyses
The staff can help you
- to choose the best-suited technique to your needs
- for interpretation of your data
Where to find us LCC- door B015ndash ground floor-building B205 route de Narbonne
When 9h to 11h30 -14h to 17h
From Monday to Friday
21
Magnetic Measurement and Moumlssbauer spectroscopy - LCC
How to request an analysis
bull For any analysis request
For magnetic measurements SQUID andMoumlssbauer spectroscopy please contact Jean-Franccedilois Meunier by e-mail or phone
An appointment will be set up in order to studyyour analyses requests and to define theexperimental conditions
An analysis request form will be provided by thestaff
bull Results and samples
Results are emailed as text and excel files
On completion of the analyses samples must beretrieved at LCC
Further information on equipments
lcc-toulousefrServices Spectroscopie Moumlssbauer
Lcc-toulousefr
servicesMesures
Magneacutetiques
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 10Email Jf-meunierlcc-toulousefr
Where to find usLCC door CS012
205 route de Narbonne
When 9h to 12h - 14h to 17h30
From Monday to Friday
Some advice
22
Elemental Analysis C-H-NS - LCC
How to request an analysis
For any analysis request
Each sample must be supplied with an analysis request formavailable on LCC website
wwwlcc-toulousefr gt services gt services techniques ampscientifiques gt analyses chimiques gt Formulaire
Fill in electronically and send by mail (see framed who tocontact)
Samples
- Internal in my box DEPOT CHN in the mail locker analyseselementaires
- External ship by courrier to LCC service CHN or ask anappointment
Results
Results are sent by mail Samples are not returned
Analyses
Analyses are carried out every week
10 mg of compound areneeded for 2 essays andpackaged in a vial
Sensitive samples mustbe isolated in sealedampoule
For special analysisrequests please contactservice
Sulphur is analyzed oncea year if enoughdemand
Who to contact Isabelle BorgetTel 05 61 33 32 14
mail isabelleborgetlcc-toulousefr
Where to find service LCC door B038
205 route de Narbonne
When 9h to 11h30 - 14h to 16h30
From monday to friday
on appointment
Some advice
23
Nuclear Magnetic Resonance - LCC
How to request an analysis
bull For any analysis request (except self-service equipments)
For NMR equipments (400-solid and 600 MHz) analysisand appointment requests must be emailed to Y Coppelor C Bijani
The analysis request form can be loaded from the NMRfacility webpage on the LCC website (httplcc-toulousefr)
bull Self-service equipments
All the users have to follow a training conducted by NMRfacilityrsquos staff before any use of self-service spectrometers
- for LCC teams the training and NMR user accountrequests are provided with taking office
- for outside labs please contact the LCC personneldepartment
The requests when validated must be returned directlyto A Bonnet or D Paryl in order to plan the training
The users undertake to carefully respect the operatinginstructions and the LCC memos
All the data are automatically
- made available in the LCC teamsrsquo laquo Nuage raquo file
- emailed to the user from outside labs
Feel free to contact us for any question
about analysis capabilities or for
any discussion about the best strategy to
meet your specific issues
Who to contact
Yannick Coppel (Mgr)Christian BijaniTel 05 61 17 54 27
Antoine BonnetDavid Paryl
Tel 05 61 17 54 30Email yannickcoppellcc-
toulousefrchristianbijanilcc-toulousefrantoinebonnetlcc-toulousefr
davidparyllcc-toulousefr
Some advice
Where to find us
LCC RMN Building 205 route de Narbonne Toulouse
Door 030 (Y Coppel et C Bijani)
Door 033 (F Lacassin et D Paryl)
When8h30 to 11h30 -14h to 17h
From Monday to Friday
24
Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) - LCC
How to request an analysis
bull For any analysis request
Each sample must be supplied with an analysisrequest form To request this form please contact the staff
Sample amount depends on the concentration of chemical elements to be measured in the sampleanalyzed
In the very first request please contact the staff
bull Results
Results are delivered in the letter-box of the LCC team or for outside labs made available in the ICP departmentrsquos letter-box (within the LCC entrance hall)
bull Analyses schedule
Analyses are carried out every 2 weeks
In general 10 mg per assay isneeded (provided that the
concentration is above 5 ww)
Chemical elements currentlyanalyzed (but not limited) Ag Al Au B Ba Be Bi Ca Cd Co Cr Cu Fe Ir K Li Mg Mn Na
Ni P Pb Pd Pt Ru Rh Sr Zn
Who to contact
Alain Moreau Tel 0561175850
E-mail alainmoreaulcc-toulousefr
Where to find usIPBS Bacirct A3
205 route de Narbonne
When 8h to 11h30 - 14h to 16h30From Monday to Friday (odd
week)
Some advice
25
Electrochemistry - LCC
How to request an analysis
bull For any analysis request
Analyses are carried out by appointment onlyscheduled with the staff when requesting theanalysis
On the appointed date Bring the sample and the solvent Your presence is required during the analyses
bull Sample preparation
The sample(s) must be as pure as possible correspondingto a concentration of 10-3 molL-1 in 10 mL
For each sample bring 30 mL of purified solvent
bull Results
On completion of the analyses the mostrepresentative curves are provided in paper copy
Upon request the electronic files can be emailed
Who to contactAlix Sournia-Saquet (Mgr)
Alain MoreauTel 05 61 33 31 75
Email alixsaquetlcc-toulousefralainmoreaulcc-toulousefr
Some advice
Before any analysis feel free to contact us for any
discussion or question about feasibility and conditions of
analyses
The staff can help you
- to choose the best-suited technique to your needs
- for interpretation of your data
Where to find us LCC- door B015ndash ground floor-building B205 route de Narbonne
When 9h to 11h30 -14h to 17h
From Monday to Friday
21
Magnetic Measurement and Moumlssbauer spectroscopy - LCC
How to request an analysis
bull For any analysis request
For magnetic measurements SQUID andMoumlssbauer spectroscopy please contact Jean-Franccedilois Meunier by e-mail or phone
An appointment will be set up in order to studyyour analyses requests and to define theexperimental conditions
An analysis request form will be provided by thestaff
bull Results and samples
Results are emailed as text and excel files
On completion of the analyses samples must beretrieved at LCC
Further information on equipments
lcc-toulousefrServices Spectroscopie Moumlssbauer
Lcc-toulousefr
servicesMesures
Magneacutetiques
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 10Email Jf-meunierlcc-toulousefr
Where to find usLCC door CS012
205 route de Narbonne
When 9h to 12h - 14h to 17h30
From Monday to Friday
Some advice
22
Elemental Analysis C-H-NS - LCC
How to request an analysis
For any analysis request
Each sample must be supplied with an analysis request formavailable on LCC website
wwwlcc-toulousefr gt services gt services techniques ampscientifiques gt analyses chimiques gt Formulaire
Fill in electronically and send by mail (see framed who tocontact)
Samples
- Internal in my box DEPOT CHN in the mail locker analyseselementaires
- External ship by courrier to LCC service CHN or ask anappointment
Results
Results are sent by mail Samples are not returned
Analyses
Analyses are carried out every week
10 mg of compound areneeded for 2 essays andpackaged in a vial
Sensitive samples mustbe isolated in sealedampoule
For special analysisrequests please contactservice
Sulphur is analyzed oncea year if enoughdemand
Who to contact Isabelle BorgetTel 05 61 33 32 14
mail isabelleborgetlcc-toulousefr
Where to find service LCC door B038
205 route de Narbonne
When 9h to 11h30 - 14h to 16h30
From monday to friday
on appointment
Some advice
23
Nuclear Magnetic Resonance - LCC
How to request an analysis
bull For any analysis request (except self-service equipments)
For NMR equipments (400-solid and 600 MHz) analysisand appointment requests must be emailed to Y Coppelor C Bijani
The analysis request form can be loaded from the NMRfacility webpage on the LCC website (httplcc-toulousefr)
bull Self-service equipments
All the users have to follow a training conducted by NMRfacilityrsquos staff before any use of self-service spectrometers
- for LCC teams the training and NMR user accountrequests are provided with taking office
- for outside labs please contact the LCC personneldepartment
The requests when validated must be returned directlyto A Bonnet or D Paryl in order to plan the training
The users undertake to carefully respect the operatinginstructions and the LCC memos
All the data are automatically
- made available in the LCC teamsrsquo laquo Nuage raquo file
- emailed to the user from outside labs
Feel free to contact us for any question
about analysis capabilities or for
any discussion about the best strategy to
meet your specific issues
Who to contact
Yannick Coppel (Mgr)Christian BijaniTel 05 61 17 54 27
Antoine BonnetDavid Paryl
Tel 05 61 17 54 30Email yannickcoppellcc-
toulousefrchristianbijanilcc-toulousefrantoinebonnetlcc-toulousefr
davidparyllcc-toulousefr
Some advice
Where to find us
LCC RMN Building 205 route de Narbonne Toulouse
Door 030 (Y Coppel et C Bijani)
Door 033 (F Lacassin et D Paryl)
When8h30 to 11h30 -14h to 17h
From Monday to Friday
24
Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) - LCC
How to request an analysis
bull For any analysis request
Each sample must be supplied with an analysisrequest form To request this form please contact the staff
Sample amount depends on the concentration of chemical elements to be measured in the sampleanalyzed
In the very first request please contact the staff
bull Results
Results are delivered in the letter-box of the LCC team or for outside labs made available in the ICP departmentrsquos letter-box (within the LCC entrance hall)
bull Analyses schedule
Analyses are carried out every 2 weeks
In general 10 mg per assay isneeded (provided that the
concentration is above 5 ww)
Chemical elements currentlyanalyzed (but not limited) Ag Al Au B Ba Be Bi Ca Cd Co Cr Cu Fe Ir K Li Mg Mn Na
Ni P Pb Pd Pt Ru Rh Sr Zn
Who to contact
Alain Moreau Tel 0561175850
E-mail alainmoreaulcc-toulousefr
Where to find usIPBS Bacirct A3
205 route de Narbonne
When 8h to 11h30 - 14h to 16h30From Monday to Friday (odd
week)
Some advice
25
Magnetic Measurement and Moumlssbauer spectroscopy - LCC
How to request an analysis
bull For any analysis request
For magnetic measurements SQUID andMoumlssbauer spectroscopy please contact Jean-Franccedilois Meunier by e-mail or phone
An appointment will be set up in order to studyyour analyses requests and to define theexperimental conditions
An analysis request form will be provided by thestaff
bull Results and samples
Results are emailed as text and excel files
On completion of the analyses samples must beretrieved at LCC
Further information on equipments
lcc-toulousefrServices Spectroscopie Moumlssbauer
Lcc-toulousefr
servicesMesures
Magneacutetiques
Who to contactJean-Franccedilois Meunier
Tel 05 61 33 31 10Email Jf-meunierlcc-toulousefr
Where to find usLCC door CS012
205 route de Narbonne
When 9h to 12h - 14h to 17h30
From Monday to Friday
Some advice
22
Elemental Analysis C-H-NS - LCC
How to request an analysis
For any analysis request
Each sample must be supplied with an analysis request formavailable on LCC website
wwwlcc-toulousefr gt services gt services techniques ampscientifiques gt analyses chimiques gt Formulaire
Fill in electronically and send by mail (see framed who tocontact)
Samples
- Internal in my box DEPOT CHN in the mail locker analyseselementaires
- External ship by courrier to LCC service CHN or ask anappointment
Results
Results are sent by mail Samples are not returned
Analyses
Analyses are carried out every week
10 mg of compound areneeded for 2 essays andpackaged in a vial
Sensitive samples mustbe isolated in sealedampoule
For special analysisrequests please contactservice
Sulphur is analyzed oncea year if enoughdemand
Who to contact Isabelle BorgetTel 05 61 33 32 14
mail isabelleborgetlcc-toulousefr
Where to find service LCC door B038
205 route de Narbonne
When 9h to 11h30 - 14h to 16h30
From monday to friday
on appointment
Some advice
23
Nuclear Magnetic Resonance - LCC
How to request an analysis
bull For any analysis request (except self-service equipments)
For NMR equipments (400-solid and 600 MHz) analysisand appointment requests must be emailed to Y Coppelor C Bijani
The analysis request form can be loaded from the NMRfacility webpage on the LCC website (httplcc-toulousefr)
bull Self-service equipments
All the users have to follow a training conducted by NMRfacilityrsquos staff before any use of self-service spectrometers
- for LCC teams the training and NMR user accountrequests are provided with taking office
- for outside labs please contact the LCC personneldepartment
The requests when validated must be returned directlyto A Bonnet or D Paryl in order to plan the training
The users undertake to carefully respect the operatinginstructions and the LCC memos
All the data are automatically
- made available in the LCC teamsrsquo laquo Nuage raquo file
- emailed to the user from outside labs
Feel free to contact us for any question
about analysis capabilities or for
any discussion about the best strategy to
meet your specific issues
Who to contact
Yannick Coppel (Mgr)Christian BijaniTel 05 61 17 54 27
Antoine BonnetDavid Paryl
Tel 05 61 17 54 30Email yannickcoppellcc-
toulousefrchristianbijanilcc-toulousefrantoinebonnetlcc-toulousefr
davidparyllcc-toulousefr
Some advice
Where to find us
LCC RMN Building 205 route de Narbonne Toulouse
Door 030 (Y Coppel et C Bijani)
Door 033 (F Lacassin et D Paryl)
When8h30 to 11h30 -14h to 17h
From Monday to Friday
24
Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) - LCC
How to request an analysis
bull For any analysis request
Each sample must be supplied with an analysisrequest form To request this form please contact the staff
Sample amount depends on the concentration of chemical elements to be measured in the sampleanalyzed
In the very first request please contact the staff
bull Results
Results are delivered in the letter-box of the LCC team or for outside labs made available in the ICP departmentrsquos letter-box (within the LCC entrance hall)
bull Analyses schedule
Analyses are carried out every 2 weeks
In general 10 mg per assay isneeded (provided that the
concentration is above 5 ww)
Chemical elements currentlyanalyzed (but not limited) Ag Al Au B Ba Be Bi Ca Cd Co Cr Cu Fe Ir K Li Mg Mn Na
Ni P Pb Pd Pt Ru Rh Sr Zn
Who to contact
Alain Moreau Tel 0561175850
E-mail alainmoreaulcc-toulousefr
Where to find usIPBS Bacirct A3
205 route de Narbonne
When 8h to 11h30 - 14h to 16h30From Monday to Friday (odd
week)
Some advice
25
Elemental Analysis C-H-NS - LCC
How to request an analysis
For any analysis request
Each sample must be supplied with an analysis request formavailable on LCC website
wwwlcc-toulousefr gt services gt services techniques ampscientifiques gt analyses chimiques gt Formulaire
Fill in electronically and send by mail (see framed who tocontact)
Samples
- Internal in my box DEPOT CHN in the mail locker analyseselementaires
- External ship by courrier to LCC service CHN or ask anappointment
Results
Results are sent by mail Samples are not returned
Analyses
Analyses are carried out every week
10 mg of compound areneeded for 2 essays andpackaged in a vial
Sensitive samples mustbe isolated in sealedampoule
For special analysisrequests please contactservice
Sulphur is analyzed oncea year if enoughdemand
Who to contact Isabelle BorgetTel 05 61 33 32 14
mail isabelleborgetlcc-toulousefr
Where to find service LCC door B038
205 route de Narbonne
When 9h to 11h30 - 14h to 16h30
From monday to friday
on appointment
Some advice
23
Nuclear Magnetic Resonance - LCC
How to request an analysis
bull For any analysis request (except self-service equipments)
For NMR equipments (400-solid and 600 MHz) analysisand appointment requests must be emailed to Y Coppelor C Bijani
The analysis request form can be loaded from the NMRfacility webpage on the LCC website (httplcc-toulousefr)
bull Self-service equipments
All the users have to follow a training conducted by NMRfacilityrsquos staff before any use of self-service spectrometers
- for LCC teams the training and NMR user accountrequests are provided with taking office
- for outside labs please contact the LCC personneldepartment
The requests when validated must be returned directlyto A Bonnet or D Paryl in order to plan the training
The users undertake to carefully respect the operatinginstructions and the LCC memos
All the data are automatically
- made available in the LCC teamsrsquo laquo Nuage raquo file
- emailed to the user from outside labs
Feel free to contact us for any question
about analysis capabilities or for
any discussion about the best strategy to
meet your specific issues
Who to contact
Yannick Coppel (Mgr)Christian BijaniTel 05 61 17 54 27
Antoine BonnetDavid Paryl
Tel 05 61 17 54 30Email yannickcoppellcc-
toulousefrchristianbijanilcc-toulousefrantoinebonnetlcc-toulousefr
davidparyllcc-toulousefr
Some advice
Where to find us
LCC RMN Building 205 route de Narbonne Toulouse
Door 030 (Y Coppel et C Bijani)
Door 033 (F Lacassin et D Paryl)
When8h30 to 11h30 -14h to 17h
From Monday to Friday
24
Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) - LCC
How to request an analysis
bull For any analysis request
Each sample must be supplied with an analysisrequest form To request this form please contact the staff
Sample amount depends on the concentration of chemical elements to be measured in the sampleanalyzed
In the very first request please contact the staff
bull Results
Results are delivered in the letter-box of the LCC team or for outside labs made available in the ICP departmentrsquos letter-box (within the LCC entrance hall)
bull Analyses schedule
Analyses are carried out every 2 weeks
In general 10 mg per assay isneeded (provided that the
concentration is above 5 ww)
Chemical elements currentlyanalyzed (but not limited) Ag Al Au B Ba Be Bi Ca Cd Co Cr Cu Fe Ir K Li Mg Mn Na
Ni P Pb Pd Pt Ru Rh Sr Zn
Who to contact
Alain Moreau Tel 0561175850
E-mail alainmoreaulcc-toulousefr
Where to find usIPBS Bacirct A3
205 route de Narbonne
When 8h to 11h30 - 14h to 16h30From Monday to Friday (odd
week)
Some advice
25
Nuclear Magnetic Resonance - LCC
How to request an analysis
bull For any analysis request (except self-service equipments)
For NMR equipments (400-solid and 600 MHz) analysisand appointment requests must be emailed to Y Coppelor C Bijani
The analysis request form can be loaded from the NMRfacility webpage on the LCC website (httplcc-toulousefr)
bull Self-service equipments
All the users have to follow a training conducted by NMRfacilityrsquos staff before any use of self-service spectrometers
- for LCC teams the training and NMR user accountrequests are provided with taking office
- for outside labs please contact the LCC personneldepartment
The requests when validated must be returned directlyto A Bonnet or D Paryl in order to plan the training
The users undertake to carefully respect the operatinginstructions and the LCC memos
All the data are automatically
- made available in the LCC teamsrsquo laquo Nuage raquo file
- emailed to the user from outside labs
Feel free to contact us for any question
about analysis capabilities or for
any discussion about the best strategy to
meet your specific issues
Who to contact
Yannick Coppel (Mgr)Christian BijaniTel 05 61 17 54 27
Antoine BonnetDavid Paryl
Tel 05 61 17 54 30Email yannickcoppellcc-
toulousefrchristianbijanilcc-toulousefrantoinebonnetlcc-toulousefr
davidparyllcc-toulousefr
Some advice
Where to find us
LCC RMN Building 205 route de Narbonne Toulouse
Door 030 (Y Coppel et C Bijani)
Door 033 (F Lacassin et D Paryl)
When8h30 to 11h30 -14h to 17h
From Monday to Friday
24
Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) - LCC
How to request an analysis
bull For any analysis request
Each sample must be supplied with an analysisrequest form To request this form please contact the staff
Sample amount depends on the concentration of chemical elements to be measured in the sampleanalyzed
In the very first request please contact the staff
bull Results
Results are delivered in the letter-box of the LCC team or for outside labs made available in the ICP departmentrsquos letter-box (within the LCC entrance hall)
bull Analyses schedule
Analyses are carried out every 2 weeks
In general 10 mg per assay isneeded (provided that the
concentration is above 5 ww)
Chemical elements currentlyanalyzed (but not limited) Ag Al Au B Ba Be Bi Ca Cd Co Cr Cu Fe Ir K Li Mg Mn Na
Ni P Pb Pd Pt Ru Rh Sr Zn
Who to contact
Alain Moreau Tel 0561175850
E-mail alainmoreaulcc-toulousefr
Where to find usIPBS Bacirct A3
205 route de Narbonne
When 8h to 11h30 - 14h to 16h30From Monday to Friday (odd
week)
Some advice
25
Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) - LCC
How to request an analysis
bull For any analysis request
Each sample must be supplied with an analysisrequest form To request this form please contact the staff
Sample amount depends on the concentration of chemical elements to be measured in the sampleanalyzed
In the very first request please contact the staff
bull Results
Results are delivered in the letter-box of the LCC team or for outside labs made available in the ICP departmentrsquos letter-box (within the LCC entrance hall)
bull Analyses schedule
Analyses are carried out every 2 weeks
In general 10 mg per assay isneeded (provided that the
concentration is above 5 ww)
Chemical elements currentlyanalyzed (but not limited) Ag Al Au B Ba Be Bi Ca Cd Co Cr Cu Fe Ir K Li Mg Mn Na
Ni P Pb Pd Pt Ru Rh Sr Zn
Who to contact
Alain Moreau Tel 0561175850
E-mail alainmoreaulcc-toulousefr
Where to find usIPBS Bacirct A3
205 route de Narbonne
When 8h to 11h30 - 14h to 16h30From Monday to Friday (odd
week)
Some advice
25
![2017 Annual Report Annual Report€¦ · 153654 TOPPAN Citrix Systems AR_Text_Insert ] Sig 1 153654 TOPPAN Citrix Systems AR_Text_Insert] Sig 6 Annual Report 2017 Citrix Systems,](https://static.fdocuments.us/doc/165x107/5f915465f08f414b6d44852f/2017-annual-report-annual-report-153654-toppan-citrix-systems-artextinsert-sig.jpg)
