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THE EFFECT OF TEMPERATURE (3N THEDIELECTRIC STRENGTH OF

VARNISHED CLOTH

BY

Ernest Henning Baii.ey

AND

Leonard George Pierce

THESIS

FOR

DEGREE OF BACHELOR OF SCIENCE

IN

ELECTRICAL ENGINEERING

COLLEGE OF ENGINEERING

UNIVERS IT Y OF^ IT^T^INOIS

PRKSENTKD JUNK 1910/w/

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UNIVERSITY OF ILLINOIS

June 1, 191)0

THIS IS TO CERTIFY THAT THE THESIS PREPARED UNDER IWY SUPERVISION BY

KBMST HEMIIG-MIMI and MOMRI) CSORGS PIERCS

ENTITLED THE EFFECT OF .TELffSRATU^ Oil THE DIELECTRIC STRSIGTH...

OF VARIIISHEI) CLOTH

IS APPROVED BY ME AS FULFILLING THIS PART OF THE REQUIREMENTS FOR THE

DEGREE OF Baohelor of Science in Electrical Enp:ineerin^

APPROVED:

HEAD OF DEPARTMENT OF. ELECTRIC.AL EIIG.IIJEERIIIG

167160

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UlUC

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INDEX.

Introduction

Object

Conditions Governing Such Tests

Description of Apparatus

Methods Used in MaXing Tests

Results

Conclusions

Explanation of Curves

Data

Curve Sheets

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INTRODUCTION.

It is only recently, (within the last ten years), that any

great amount of attention has "been paid to the materials used for

insulating. The early engineers were so fascinated with the new

phenomena with which they were dealing and which offered such tre-

mendous possi'bilities, that a detail liKe insulation was entirely

forgotten or at least passed over as of little consequence. A

much more extensive use of motors would have heen possible much

earlier had it not been so well known that they could not he de-

pended on for this very reason. That some people recognized this

defect however, is shown by a paragraph from a paper by 0' Gorman

before the Institute of Electrical Engineers in 1901 in which he

said,-

"V/e scarcely realize how unlimited afid how unexplored are

those fields of research. Suppose that by dint of mixing gums,

resins, oils, powders and solvents, we should get a perfect

dielectric, waterproof for one hundred years, fexible and exten-

sible, 30 volt resisting that the thinnest film suffices, with a

specific capacity as low as that of air, yet adjustable to a high

value; sufficiently firm not to decentralize, yet fluid enough,

when heated by an arc, to close in and seal up the fault. Sup-

pose, besides all this, we can make it at 5d. per lb. applied,

what will be the reward? Par more than the value of the three-

wire patents or the Dunlop tyre, plus the benediction of all

electricians.

The ten years that have passed since that was written have

not produced that "perfect dielectric", but they have proven the

correctness of the authors estimation of its value, and they have

added considerably to our knowledge of the siibiect which is as

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2

yet, never- the- leas, open to almost umlimited investigation. It

is only within the last few months that the design of the largest

generators yet built was changed because insulation could not be

trusted beyond a certain point.

The properties of insulating materials may be classified as

follows;-

I, Electrical properties.

A. Insulation resistance or conductivity, expressed in

ohms per cubic centimeter.

B. Disruptive or dielectric strength, measured by the

potential necessary to puncture the material.

C. Dielectric constant or* specific inductive capacity,

measured by the capacity in micro-farads of a

condenser having the particular material as the

dielectric separating the plates. (Less important

than A or B).

II. Mechanical properties.

A. Toughness to withstand mechanical strains.

B. Flexibility and freedom from brittleness.

III. Chemical properties.

A. Ability to withstand heat.

B. Ability to withstand acids.

C. Ability tc exclude moisture.

It is not possible here to discuss any but the electrical

properties except as they may be affected by the others; and of

them, the capacity effect may be ignored, it being of importance

only when insulated apparatus such as cables etc. are to be

tested. The first two properties are often confused.

"A thing insulates because it is possessed of two distinct

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properties: first, the alDtlity to stand the mechanical and elec-

trical stresses due to the voltages used; secondly, because it is

such a poor conductor that but negligibly small current can flow

through it and leak away, in other words, it will neither allow

the current to break through it nor steal through it. The first

property is called by Maxwell the dielectric strength of the

insulator; the other property is called its ohmic resistance. The

two together form its insulating power." (R. A. Fessenden, "In-

sulation and Conduction", Proceedings of American Institute of

Electrical Engineers, vol. XV, 1898).

At one time an insulating material was known by its ohmic

resistance; the material which on being tested allowed the small-

est amount of current tc pass through per square inch or square

centimeter was considered to be the most effective insulation.

This was quite natural, for thiugh it was of course realized that

the "breakdown" or ultimate strength was what counted, it was held

that this quality would necessarily accompany the feature of

ohmic resistance. A little investigation sufficed tc show that

this v>'as not true; that is, a substance may have a high ohmic

resistance and still have a comparatively small breakdown

strength, or vice versa. For instance, the insulation resistance

of .004 inch of air is so large as to be hard to measure at 100

volts and at 500 volts. On the other hand, the resistance of

the same thickness of paper is readily measured, but from 500 to

1000 volts are necessary tc puncture a specimen. And again, a

piece of mica has an even smaller insulation resistance, but it

will withstand a pressure of 10,000 volts. In short the two

properties do not follow the same laws and are affected differ-

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ently by various condlitions as the results of this thesis tend to

show.

OBJECT.

A very careful thesis prepared by M. S. Chester and C. V.

Crellin, University of Illinois, '97, showed quite conclusively

as have several other experiments, that a temperature of from 60

to 100 degrees Centigrade reduces the insulation resistance of all

the materials tested to a small fraction of the value at room temp-

erature. It was the intention then, to study in this thesis, the

effect of temperature on the dielectric strength. Varnished cloth

was selected as the material to "be tested, two different makes

and several thicXnesses of each being available. The 10 and 12

mil samples proved most satisfactory, since they required for

breakdown a voltage which was easily obtained and measured with

the apparatus at hand.

CONDITIONS GOVERNING SUCH TESTS.

The conditions which may affect the dielectric strength of a

material, or perhaps more accurately, the conditions which have

been suggested as having a possible effect, are so many and so

varied that as intimated before, an almost unlimited amount of

time might be spent in investigating the relations of the diferent

factors.

There are several ways of obtaining a high voltage for

dielectric tests. Direct current may be obtained with an arc

light machine, or with a number of generators in series, or by

means of many storage cells in series. Induction coils may be

used, but they present a difficulty in measuring the voltage and

do not give a constant frequency. Static machines have also been

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tried, but it is maintained by some that the results thus obtained

are not reliable as applied commercially since there is not the

power behind them that there is behind the voltage that must be

withstood by insulation under ordinary conditions. It has been

shown that in general insulation will stand up under a higher

continuous voltage than it will under an alternating one; and

some investigators have noticed that different wave forms cause

breakdowns at the same effective voltage. These observations

seem to show that rupture may depend upon the maxlnium voltage, but

in any case, to maKe results comparable one to the other, gener-

ators with similar wave shapes should be used.

Experiments by Lansdorf (Electrical World, Oct. 31. 1908)

showed that higher frequencies cause a breakdown in a shorter

time and that therefore in this work the frequency should be kept

constant. The same experimenter also showed that there is a

phenomena which he called the "fatigue" of insulation and which

causes rupture at a lower voltage if it be applied for a long

time. This fact is recognized in most commercial testing in which

the voltage is applied for one minute between each step.

The size of the terminals to be used in testing is not a

settled question. Practically all tests have been made with flat

discs with rounded edges "to prevent the undue stress which occurs

at sharp corners;" but the size varies from those which are 25mm.

in diameter with a bearing surface 15 mm. in diameter recommended

by Turner and Hobart ("Insulation of Electric Machines"), or those

used by Conant (Electrical World, July 20, 1907) which were "about

the size of a silver quarter" to those which gave Skinner the best

results and were "approximately 9 inches in diameter" (Transac-

tions of American institute of Electrical Engineers, vol. XIX).

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DESCRIPTION OF APPARATUS.

To secure the different temperatures an asbestos lined wooden

"box 22" X 22" X 9" was used. This oven was heated by 13 100 watt

porcelain heaters on a 110 volt circuit. These were placed on an

asbestos sheet about an inch above the bottom, thus making an air

space to prevent injury to the box, and were connected in groups

of 1, 2, 3, and 4 with a switch for each group. By various com-

binations of groups any desired temperature within the range of

the apparatus could be obtained and kept constant. The testing

terminals were flat 3 inch brass discs with the edges rounded to a

half inch radius mounted on the ends of hard wooden rods which

extended out through the sides of the oven, thus permitting them

to be moved from the outside. A brass helical spring working

against one side of the -box and a pin in the rod as shown in the

diagram, pressed the terminals together, the other rod being held

in place by another pin resting against the other side of the box.

A series of holes drilled in this second rod allowed the length-

ening or shortening of the portion within the box and consequently

a variation in the pressure applied. The leads to the terminals

were brought in through porcelain tubes in each end of the oven

and were connected to the discs by means of set screws. The

thenuometer was hung through a hole in the top of the box, so that

the bulb was on a level with the teminals and about three inches

from them. Access was had to the terminals by means of a small

door 6 inches square in the front of the oven. This did not

cause an excessive lowering of temperature while the test pieces

were being changed. Hooks were provided in the top on which test

pieces could be hung so that they could become heated to the tem-

perature at which the tests were being made.

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The voltage was obtained from a General Electric 7.5 Kw. 60

cycle 110 volt synchronous converter used as an alternator and

belted to a Direct Current motor. The machine voltage was stepped

up in a 100 to 1 ratio 50 watt potential transformer whose normal

voltage was 11,000 volts. This capacity was sufficient since the

test pieces, being only small sheets 4.5 inches square, required

nc charging current. The breakdown voltage was determined by

reading the voltage on the low side and assuming that the ratio

was correct. The transformer was protected by a one ampere fuse

in the generator side.

METHODS USED IN MAKING TESTS.

The method used in making the tests in this thesis was as

follows:- A number of test pieces were hung in the oven which was

then heated to a temperature at which tests were to be made. When

the oven reached the desired temperature a test piece was placed

between the terminals. The circuit was then closed with no field

excltaticn on the alternator, and the voltage raised step by step

at one minute Intervals. When the dielectric strength of the

insulation was nearly reached the steps were reduced to 250 volts

each. After a sample had been punctured it was removed and

labeled, its number, the temperature, and the breakdown voltage

were recorded on a data sheet and also on the label stuck on the

the test piece. From 5 to 10 samples were tested for each tem-

perature, the nimber depending on the variability of the punctur-

ing voltage.

The e.ra. f. was controlled by varying the field excitation of

the generator by means of a stove pipe rheostat because this

method does not change the wave shape as would a resistance in

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in the main circuit. The voltage applied to the insulation was

always started from zero and gradually brought up to a value near

the dielectric sti-ength of the piece being tested, because in

closing a high voltage circuit the arc produced at the switch has

a frequency equal to the natural period of the circuit which in

this case was very high. This frequency causes an instantaneous

rise in voltage which thus breaks down the insulation at a higher

value than the voltmeter indicates.

Since high voltages are commonly alternating and 60 cycles

is a standard frequency, the tests were made for those conditions

alone. The method of regulating the temperature depended merely

on careful watching of the thermometer and some practice. With a

little care the variation could be limited to a maxiinum of two

degrees, which was sufficiently accurate for these tests. The

pressure on the insulation was kept constant also, being roughly

1.5 pounds per square inch.

RESULTS.

The dielectric strength of the insulation at room temperature

was found to vary as much as 50 per cent sometimes, due probably

to inaccuracies in the application of the varnish, so that at the

outset it was found that results could only be obtained by avera-

ging several tests. All the points on the curves then, are aver-

ages of at least 5 tests though some of them include as high as 10,

Though the edges of the electrodes were rounded off and con-

siderable care was taken to polish them, there was still a good

deal of "corona" around their circumference with voltages higher

than 3000 volts. Apparently this did not affect the results at

the lower temperatures because usually rupture occured well within

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10

the circumference of the terminals, "but never very close to their

center. At high temperatures, above 150 degrees Centigrade, this

corona seemed to have a greater burning effect which was evidenced

by a darker colored ring on the sample where the edges of the

electrodes had been and the punctures were more apt to occur here.

The results obtained by others as to the effect of temper-

ature on insulation resistance is shewn by a typical curve on

Plate I. Information gathered from still other sources as to the

dielectric stength indicated that it would be affected similarly

and that between 70 and 80 degrees Centigrade the breakdown volt-

age might be expected to become very much smaller than at normal

temperatures, in fact, it was expected that it would fall to about

one- tenth of its initial strength. The curves drawn from the data

taken do not bear out this supposition, although at 200 degrees

Centigrade the dielectric strength is in general only about one-

third of what it is at normal temperature.

When this had been discovered, it was thought that possibly

at higher voltages this phenomena would appear. Three thicknesses

were accordingly tested. These samples withstood from 12,000 to

18,000 volts at room temperature, but showed the same relative

falling off in dielectric strength as did the single thicknesses.

It was then suggested that the length of time that the voltage

was applied might be the deciding factor. A few tests were then

made in which the voltage was applied for 30 minute intervals.

Although the insulation broke down at a slightly lower value, the

relative decrease In dielectric strength with the increase of

temperature was approximately the same.

When testing samples of three thicknesses the results were

much more uniform. This was no doubt due to the automatic averag-

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11 '

ing of the dielectric stength by the three layers.

There i3 a difficulty in this work in saying ^ust what causes

breakdown. Some writers nave attributed it to a charring of the

insulation due to the passage of current through the material

until it becomes a sufficiently good conductor to allow a large

current to flow. Others say there is a sort of mechanical shear-

ing effect which causes rupture. The holes made by the voltage

were Invariably circular as shown by a magnifying glass and were

always charred around the edges. This might point to the correct-

ness of the first theory above, but the burning might just as well

have occurred during the passage of the large current after the

voltage had actually caused a mechanical strain in the material.

The holes made by the higher voltages were all very small, mere

pin pricks, but the lower values caused holes as large as l/S2 of

an inch in diameter. In this connection it might be mentioned

that when a piece of varnished cloth was held between two pointed

terminals attached to a high tension magneto, the voltage appar-

ently went through, but no holes could be seen. The same termin-

als made very fine holes in paper.

Not only does the temperature of the surrounding air affect

the insulation, but the terminals and the te^t pieces themselves

get hot due to the passage of the leakage current through them.

Thus it was found that a piece tested at room temperature for

some time, when taken out was not, probably having a temperature

of from 60 to 80 degrees Centigrade. It would seem quite logical

for such heat to tend to cause breakdown at an apparently lower

temperature than really existed, so here again is an element of

uncertainty which would be most difficult to eliminate.

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12

CONCLUSIONS.

The dielectric strength gradually decreases with a rise in

temperature.

The dielectric strength decreases more rapidly with temper-

atures above 100 degrees Centigrade than it does for temperatures

"below 80 degrees Centigrade.

Assuivdng that Plate I shows the true relation between tem-

perature and insulation resistance, the dielectric strength of

varnished cloth does not decrease as rapidly with a rise of

temperature as does the insulation resistance.

T;;'hile at temperatures of about 25 degrees Centigrade the

insulation stands up under as great a pressure when applied for

30 minutes as it does when applied for only 1 minute, it will not

do this at the higher temperatures, but breaks down under a

relatively lower voltage as the temperature increases.

Specimens of three thicknesses have only about twice the

dielectric strength of a single thickness. This is roughly true

throughout the range of temperatures.

Corona has an effect on the insulation. It appears to char

the insulation at the higher temperatures, the charring being

greater as the temperature increases.

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13

Curves.

Plate I. Effect of temperature on insulation resistance of

shellaced cotton canvas as given "by Chester an'i Crellin.

Plate II. Variation of dielectric strength with temperature in

per cent of strength at 25 degrees Centigrade.

Plates III, IV, and V. Actual dielectric strength plotted against

temperature. Ill for single thickness of cloth manu-

factured by Standard Underground Cable co. IV for

single thickness of "Linonite" varnished cloth. V for

three thicknesses of each.

Plate VI. Wave shape of generator used.

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14

DATA.

standard Undergroxmd Cable Co.

Varnished Cloth

Temperaturedegrees

CentigradeSingle thickness

7 mil 10 mil 12 mil

Threethickness

30 mil

25 3770 5940 7850 12750

60 4060 5400 6900 12750

80 3325 5120 6900 9660

100 3250 4830 6300 6000

110 3400 4670 5500

125 3400 5100

150 3130 4050

175 3200 3650

200 2450

Linonite

3100

Temperaturedegrees

CentigradeSingle thickness10 mil 12 mil

Three30 mil

thicknesses36 mil

S5 6900 7150 14000 18000

60 6100 7050 12000 12600

80 6400 6040 11500

100 6300 6250 10800 10940

125 5000 5800

150 4400 5200 7250 7375

175 3900 4650 5600

200 3320 3900 5580

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