Technical Report 8th Proficiency Test (2015) for … Physical Parameters of Cigarettes and Filters...

Physical Test Methods Sub-Group

Technical Report

8th Proficiency Test (2015)

for Physical Parameters

of Cigarettes and Filters

February 2017

Sub-Group Co-ordinator:

Bernhard Eitzinger, delfortgroup AG, Austria

Study Co-ordination:

CORESTA PTM Proficiency Test Coordination Group

(B. Eitzinger, J. Fiebiger, Ph. Le Men, W. Sexauer, K. Wagner)

Statistical Support:

D. Tafin-Djoko, K. Wagner, Philip Morris International Management S.A., Switzerland

Table of Contents

1. INTRODUCTION ............................................................................................................ 3

1.1 Purpose/Scope ......................................................................................................... 3

1.2 Study Summary ....................................................................................................... 3

2. RAW DATA ..................................................................................................................... 5

3. STATISTICAL EVALUATION ...................................................................................... 6

3.1 Outlier Analysis and Removal ................................................................................ 6

3.2 Laboratory means and within laboratory standard deviation after outlier

removal ................................................................................................................... 6

3.3 Global means and between laboratories standard deviation after outlier

removal ................................................................................................................... 7

3.3.1 Cigarettes ......................................................................................................................... 7

3.3.2 Filters – Evaluation 1 ................................................................................................... 8

3.3.3 Filters – Evaluation 2 ................................................................................................. 10

3.4 Laboratory Proficiency - z-scores ........................................................................ 11

4. INTERPRETATION OF SCORES/CONCLUSIONS ................................................... 11

4.1 Interpretation and conclusions regarding z-scores – laboratory proficiency ......... 11

4.1.1 Cigarettes ....................................................................................................................... 12

4.1.2 Filters – Evaluation 1 ................................................................................ 13

4.1.3 Filters – Evaluation 2 ................................................................................ 13

4.2 Interpretation and conclusions regarding z-scores – laboratory proficiency

from evaluation 2 of filter products ....................................................................... 14

5. REFERENCES ............................................................................................................... 14

6. APPENDIX ..................................................................................................................... 15

PTM-063-CTR 8th Prof. Test 2015 on Physical Parameters – February 2017 3/78

1. INTRODUCTION

1.1 Purpose/Scope

This proficiency test serves as an assessment of the capability of the participating laboratories

to properly measure physical parameters on cigarettes and filters. Although it is not required

for a proficiency test to define the measurement method, in practice all laboratories closely

followed CORESTA Recommended Methods or the respective ISO standards.

The test results allow each laboratory to evaluate its performance in comparison to other

laboratories and to derive actions for improvement. All results are presented in anonymised

form.

1.2 Study Summary

The test protocol used for this study is given in Appendix A “2015 PTM Proficiency Test –

Study Protocol” of this report, covering:

Cover sheet with participant details

List and description of evaluated products and samples

Protocol

o Preparation of samples

o Instrument set up

o Calibration of instruments

o Making measurements

o Recording and transfer of results

Table 1 - Type and Number of Products tested

The cigarette samples have been provided by the manufacturer of the respective brand. Filter

samples have been provided by Solvay Acetow GmbH.

For each of the ten products (F1-F5 and C1-C5) three sets of samples randomly taken from a

larger sample batch have been prepared and provided to the participants.


Parameters tested and subjected to statistical analysis:

Filter Products F1-F5

Filter Individual Weight (Wgt, Wt)

Filter Diameter

Filter Pressure Drop (PD) (fully encapsulated)

Cigarette Products C1-C5

Cigarette Individual Weight

Cigarette Diameter

Cigarette Draw Resistance (PD open)

Cigarette Draw Resistance (PD closed)

Cigarette Filter Ventilation (FV)

Table 2 - Measurements required for each parameter:

Evaluation 1:

For each product C1-C5 and F1-F5 three sample sets (representing as well the three days of

analysis) have been analysed for parameters as given above. Per sample 10 cigarettes or filter

rods have been measured.

Evaluation 2:

In order to potentially exclude the sample-to-sample variation, the laboratory variation was

evaluated when measuring exactly the same sample repeatedly. Therefore sample 1 of filters

F1-F5 was measured on day 1 and then re-measured on day 2 and day 3 of the study.

Remark: The measurements performed for evaluation 2 are supposed not to have a noticeable

impact on the test sample, which is valid for filter rods only.

data recording sheet 1

data recording sheet 1 and 2 data recording sheet 2

first measurement of sample 1

of product 1-5




of product 6-10

Individual measurements in

total10*10*3 + 5*10*2= 400 rods

Individual measurements

per day


of product 1-10

1*10*10 = 100 rods 1*10*10+1*10*5 = 150 rods


1*10*10+1*10*5 = 150 rods

Day 2 Day 3Day 1

second measurement of sample 1

of product 1-5

third measurement of sample 1

of product 1-5


of product 1-10


Participating companies / laboratories and related contact names:

A total of 21 laboratories provided results for this study.

Table 3 - Participating companies / laboratories

Information relevant to the interpretation of the results

Participants were asked to provide relevant data regarding instruments used, calibration of

instruments and environmental conditions in the instrument configuration sheet (for details

see Appendix A “2015 PTM Proficiency Test – Study Protocol”).

Participants followed the respective CORESTA Recommended Methods (CRM N° 6) or ISO

standards (ISO 6565, ISO 9512) to perform the measurements in the frame of this study as

given in section 5 “References” of this report.

A more detailed statistical data analysis is available for the participating laboratories on

request to the Physical Test Methods Sub Group.

2. RAW DATA

Results for cigarette samples were submitted by 20 participants. Results for filter samples

were submitted by 20 participants. One laboratory provided only cigarette data and one lab

provided only filter data. Each participant was assigned a unique code.

Once a data set was received from a laboratory, the data were inspected for any obvious

inconsistencies by the PTM proficiency test coordination group. Any inconsistencies were

reported back to the laboratory for comment or correction. In general typing errors were

corrected. The consolidated data as provided for statistical analysis are given in Appendix B

“2015 Proficiency Test – Raw Data – Laboratories encoded”.


3. STATISTICAL EVALUATION

3.1 Outlier Analysis and Removal

For this report the z-scores have been calculated as a basis to evaluate the laboratory

performance. It has to be noted that even though values from a laboratory have been excluded

by the use of Cochran and Grubbs outlier treatment, for the calculation of the global mean and

standard deviations, its performance was nevertheless evaluated. Thus the only use of outlier

detection was relative to the establishment of the assigned means and standard deviations.

Cochran’s test was applied first to eliminate laboratories with unusually high standard

deviations and then Grubbs’s test was used to detect whether the one or two highest and

lowest values in the data set qualify as outliers. If yes, the outliers were removed. Each outlier

test was applied once and after the first removal of outliers no further outliers were detected.

For the calculation of these statistics a global mean value and a global standard deviation for

each of the samples C1-C5 and F1-F5 is required. ISO 13528:2015 indicates to a substantial

part methods to obtain such a robust estimate of global mean values and standard deviations.

The number of data sets and data sets excluded from the global mean calculations are given in

Appendix C “2015 PTM Proficiency Test - Summary of data sets and outliers”.

3.2 Laboratory means and within laboratory standard deviation after

outlier removal

Summary tables of laboratory means and standard deviations after outlier removal are given

in:

Appendix D: “2015 PTM Proficiency Test - Summary of laboratory means and standard

deviations - Cigarettes”

Appendix E: “2015 PTM Proficiency Test - Summary of laboratory means and standard

deviations – Filters – Evaluation 1”

Appendix F: “2015 PTM Proficiency Test - Summary of laboratory means and standard



3.3 Global means and between laboratories standard deviation after

outlier removal

3.3.1 Cigarettes

Table 4 - Cigarette C1

Summary statistics for cigarette C1 of individual weight (mg), diameter (mm), open and

closed pressure drop (mmWG) and filter ventilation (%).







Individual Wgt Diameter Pressure Drop Open Pressure Drop Close Filter ventilation

p 19 18 19 18 19

n 30 30 30 30 30

Global Mean 502.96 5.41 87.92 279.04 88.50

Median 503.23 5.40 87.87 278.88 88.62

Sr (Average StDev) 14.548 0.022 4.390 18.474 1.263

CVSr [%] 2.892 0.405 4.993 6.621 1.427

SL (SBetweenLabs) 4.493 0.008 1.726 8.421 1.247


p 19 18 20 18 20

n 30 30 30 30 30

Global Mean 598.41 6.11 91.34 156.11 46.38

Median 598.82 6.11 91.53 156.30 46.05

Sr (Average StDev) 12.529 0.020 3.607 7.383 1.412

CVSr [%] 2.094 0.327 3.949 4.730 3.046

SL (SBetweenLabs) 4.607 0.007 1.330 3.608 0.904


p 19 18 20 18 20

n 30 30 30 30 30

Global Mean 1021.99 7.49 93.63 135.04 35.95

Median 1023.00 7.49 93.50 135.28 35.84

Sr (Average StDev) 22.493 0.021 3.273 5.797 1.682

CVSr [%] 2.201 0.284 3.496 4.293 4.678

SL (SBetweenLabs) 9.281 0.008 1.420 3.909 0.619








3.3.2 Filters – Evaluation 1

Table 9 - Filter F1 - Evaluation 1

Summary statistics for filter F1 for individual weight (mg), diameter (mm) and fully

encapsulated pressure drop (mmWG).





p 19 18 20 18 19

n 30 30 30 30 30

Global Mean 812.59 7.86 75.16 95.84 29.04

Median 813.17 7.86 74.93 95.68 28.75

Sr (Average StDev) 18.191 0.017 2.833 4.513 2.063

CVSr [%] 2.239 0.219 3.770 4.709 7.105

SL (SBetweenLabs) 6.070 0.004 0.956 1.940 1.163


p 18 18 20 17 19

n 30 30 30 30 30

Global Mean 801.73 7.88 70.94 116.55 53.07

Median 801.45 7.88 70.72 117.17 52.85

Sr (Average StDev) 16.724 0.027 2.231 4.757 1.611

CVSr [%] 2.086 0.341 3.145 4.082 3.035

SL (SBetweenLabs) 7.541 0.008 0.830 3.977 1.045

Individual Wgt Diameter PD (fully encapsulated)

p 19 16 17

n 30 30 30

Global Mean 576.921 6.716 447.763

Median 577.600 6.715 446.867

Sr (Average StDev) 8.8464 0.0082 13.0499

CVSr [%] 1.533 0.122 2.914

SL (SBetweenLabs) 4.1541 0.0040 19.1006


p 17 15 14

n 30 30 30

Global Mean 411.43 5.32 513.28

Median 411.30 5.32 515.35

Sr (Average StDev) 3.766 0.014 11.853

CVSr [%] 0.915 0.257 2.309

SL (SBetweenLabs) 1.297 0.004 6.848












p 18 19 16

n 30 30 30

Global Mean 937.80 7.80 300.81

Median 938.12 7.80 300.47

Sr (Average StDev) 9.435 0.017 7.276

CVSr [%] 1.006 0.213 2.419



p 19 19 16

n 30 30 30

Global Mean 964.17 7.81 510.20

Median 963.47 7.81 510.17

Sr (Average StDev) 8.830 0.014 10.267

CVSr [%] 0.916 0.183 2.012



p 19 18 16

n 30 30 30

Global Mean 976.55 7.80 744.64

Median 976.93 7.80 748.30

Sr (Average StDev) 7.410 0.018 13.197

CVSr [%] 0.759 0.231 1.772














p 19 16 17

n 30 30 30

Global Mean 577.10 6.72 449.03

Median 576.67 6.71 447.37

Sr (Average StDev) 8.441 0.009 13.208

CVSr [%] 1.463 0.136 2.942

SL (SBetweenLabs) 4.446 0.005 21.054


p 16 15 13

n 30 30 30

Global Mean 411.821 5.324 513.395

Median 411.767 5.323 515.800

Sr (Average StDev) 3.5184 0.0138 11.4418

CVSr [%] 0.854 0.260 2.229

SL (SBetweenLabs) 1.6976 0.0047 6.8740


p 17 18 13

n 30 30 30

Global Mean 938.56 7.80 298.89

Median 939.23 7.80 300.60

Sr (Average StDev) 9.621 0.017 6.670

CVSr [%] 1.025 0.212 2.232









3.4 Laboratory Proficiency – z-scores

To enable the calculation of z-scores the robust global mean and robust between labs standard

deviations have been calculated, using ISO Algorithm A.

The respective data are given in

Appendix G “2015 PTM Proficiency Test – Robust global mean and between laboratory

standard deviation”

Tables of the individual z-scores per product ID, test parameter and laboratory are given in:

Appendix H “2015 PTM Proficiency Test–Individual z-scores–Cigarettes”.

Appendix I “2015 PTM Proficiency Test–Individual z-scores–Filters–Evaluation 1”.

Appendix J “2015 PTM Proficiency Test–Individual z-scores–Filters–Evaluation 2”.

4. INTERPRETATION OF SCORES/CONCLUSIONS

4.1 Interpretation and conclusions regarding z-scores – laboratory

proficiency

As described in ISO 13528, in normal circumstances, over time, about 95% of z-scores will

lie in the range -2 ≤ z ≤ 2.


p 18 18 14

n 30 30 30

Global Mean 963.68 7.81 510.05

Median 964.43 7.81 510.48

Sr (Average StDev) 9.028 0.015 10.357

CVSr [%] 0.937 0.188 2.031



p 18 16 15

n 30 30 30

Global Mean 976.74 7.81 744.14

Median 975.72 7.81 743.93

Sr (Average StDev) 6.921 0.023 12.979

CVSr [%] 0.709 0.293 1.744



Occasional scores in the range 2 <|z| <3 are to be expected, at a rate of 1 in 20. Whether or not

such scores are of importance can only be decided by considering them in the context of the

other scores obtained by that laboratory. Scores where |z| >3 are to be expected at a rate of

about 1 in 300. Given this rarity, such z-scores strongly indicate that the result is not fit-for-

purpose and almost certainly requires investigation.

4.1.1 Cigarettes

Below Table 19 indicates laboratories with z-scores in the range of 2 <|z| <3 and z-scores |z|

>3 for the respective product IDs.

No laboratory presented z-scores |z| >3 for more than one parameter and product ID.

Table 19 - Laboratories with z-scores in the range of 2 <|z| <3 and z-scores |z| >3

product type

evaluation parameter laboratory

no z-score 2 <|z| <3

z-score |z| >3

cigarette 1 individual weight

4 C2 ---

11 C1; C3; C4 ---

21 C2 ---

cigarette 1 diameter

11 C5 C4

17 C1 ---

19 C2; C3 ---

21 C2 ---

cigarette 1 PD open 7 C4 ---

cigarette 1 PD closed

7 --- C5

10 C2 C1

11 C1; C3 C5

21 C1 C5

cigarette 1 FV

5 C4 ---

7 C3 ---

8 C3; C4; C5 ---

11 C1 ---

21 C3 ---





Laboratory no 7 presented z-scores |z| >3 for all product IDs for the encapsulated pressure

drop.

The values of laboratory no 7 were lower than the global mean values as the measurements

were made without a fully encapsulated sleeve in the measurement head.


product type



z-score |z| >3

filter 1 individual

weight

3 F3 ---

19 F2 ---

filter 1 diameter

4 F3 ---

8 F3

filter 1 PD open

7 --- F1; F2; F3; F4; F5

10 F3;F4 ---

21 F1 ---




Laboratory no 7 presented z-scores |z| >3 for all product IDs for the encapsulated pressure

drop. The values of laboratory no 7 were lower than the global mean values as the

measurements were made without a fully encapsulated sleeve in the measurement head.


product type



z-score |z| >3

filter 1 individual

weight

9 F2; F5 ---

15 F1 ---

filter 1 diameter --- --- ---

filter 1 PD open

7 --- F1; F2; F3; F4; F5

12 F1 ---

21 F1 ---


4.2 Interpretation and conclusions regarding z-scores – laboratory

proficiency from evaluation 2 of filter products

The mean values and standard deviation obtained for

filter evaluation (1) F1-F5 with 3 samples (sample 1 day 1, sample 2 day 2, sample 3 day

3)

filter evaluation (2) F1-F5 with sample one re-measured on day 2 and day 3 are

comparable.

Laboratories showing substantial deviations from global mean values, that is, having z-scores

greater than 3 are the same in both evaluations.

5. REFERENCES

CORESTA CRM 6:2000, Determination of Ventilation: Definitions and Measurement

Principles

CORESTA CRM 21:1991, Atmosphere for Conditioning and Testing Tobacco and

Tobacco Products

CORESTA CRM 41:2002, Determination of the Draw Resistance of Cigarettes and Filter

Rods

CORESTA Guide 4:2008, A User Guideline for the Measurement of Pressure Drop of

Cigarettes and Cigarette Filter Rods

CORESTA Guide 10:2011, A User Guideline for the Measurement of Diameter of

Cigarettes and Filter Rods

ISO 2971:2013, Cigarettes and filter rods -- Determination of nominal diameter --

Method using a non-contact optical measuring apparatus

ISO 6565:2015, Tobacco and tobacco products -- Draw resistance of cigarettes and

pressure drop of filter rods -- Standard conditions and measurement

ISO 9512:2002, Cigarettes -- Determination of ventilation -- Definitions and

measurement principles

ISO/IEC 17043:2010, Conformity assessment – General requirements for proficiency

testing.

ISO 13528:2015, Statistical methods for use in proficiency testing by interlaboratory

comparison


6. APPENDIX

Appendix A: “2015 PTM Proficiency Test – Study Protocol”

Appendix B: “2015 Proficiency Test – Raw Data – Laboratories encoded”

Appendix C: “2015 PTM Proficiency Test - Summary of data sets and outliers”

Appendix D: “2015 PTM Proficiency Test - Summary of laboratory means and standard

deviations - Cigarettes”

Appendix E: “2015 PTM Proficiency Test - Summary of laboratory means and standard


Appendix F: “2015 PTM Proficiency Test - Summary of laboratory means and standard


Appendix G: “2015 PTM Proficiency Test – Robust global mean and between laboratories

standard deviation”

Appendix H: “2015 PTM Proficiency Test – Individual z-scores Cigarettes”

Appendix I: “2015 PTM Proficiency Test – Individual z-scores Filters – Evaluation 1”

Appendix J: “2015 PTM Proficiency Test – Individual z-scores Filters – Evaluation 2”


Appendix A: “2015 PTM Proficiency Test – Study Protocol”

Cover

Products

Lab ID

Name of contact person

Company Address

Phone

Fax

E-mail address

Please select one of the 2 options and choose the "X" :

We certify having followed the protocol described in the sheet "Protocol".

We have not followed the protocol described in the paper "Protocol" and

attach to the results our own protocol.

Cover sheet for PTM Proficiency - Test 2015

product type

overall

length

tipping

paper

length diameter perforation

[mm] [mm] type

1 F1 Filter 180 − semi slim −

2 F2 Filter 120 − slim −

3 F3 Filter 126 − regular −



6 C1 Cigarette - Kent 83 32 Super slim online

7 C2 Cigarette - Davidoff 97 31 slim online

8 C3 Cigarette - Pall Mall 94 34 semi slim online

9 C4 Cigarette - JPS red 83 25 regular eperfo (offline)

10 C5 Cigarette - JPS blue 83 32 regular online

product identification


Appendix A: “2015 PTM Proficiency Test – Study Protocol” – continued

Protocol

1. Preparation of samples

1.1

1.2

1.3

e.g:

1.4

1.5

2. Instrument setup

2.1

2.2

2.3

3. Calibration of instruments

3.1

3.2

to filter rod measurements).

3.3

3.4

3.5

In this case re-conditioning for 48 hours is not necessary.

conditioning system and stored in open boxes until next measurement day.

put #3 samples of all products into conditioning system

ISO3402 (conditioning atmosphere: (22±1)°C, (60±3)% rH)prior to the measurement. Give comments in case of deviation.

Sample 1 of product 1-5 (filter rods ) will be remeasured also on day 2 and 3 to double check the instrument and the conditioning.



Day3 measurements s. scheme 4.8

All measurements should take place in an environment according to ISO 3402 (Testing atmosphere: (22±2)°C, (60±5)% rH).Give comments in case of deviation.

Prepare for each product – see data sheet: products - 3 separate samples ( #1,#2,#3) of 10 filter rods / cigarettes.

Inspect prepared samples visually to avoid measurements of damaged samples

Samples should be unpacked and conditioned as accurately as possible for 48h (conditioning time can affect the level / results of physical parameters !) regarding

Sample 1 is measured on Day1, sample 2 on Day2 and sample 3 on Day3. Exception see 1.5.

To avoid changes in sample-moisture the samples should be transferred from conditioning environment to the instrument in tightly closed plastic boxes.

Friday :



If the difference between the measured and the defined value of the standard during a calibration check exceeds ± 0,5% of the defined value,

In case of the use of automatic calibration, no extra calibration according 3.3 is necessary.

400 mmWG and 800 mmWG nominal for filter rods

Wednesday :

Thursday :

Monday :

Tuesday :

Wednesday :

To avoid moisture changes samples being used again should be placed in tightly closed plastic boxes directly after measurement, returned to the

FV: ISO 9512

Balance in regards to the instrument suppliers recommendation

multicapillary standards for cigarette measurements

Repeat calibration check after every change in the units ( e.g. PD/FV unit: necessary changes caused by sample diameter and/or changes from cigarette

measured / actual values should be noted in the record sheet.

PD calibration should be carried out using nominally 800mmWG multicapillary standards for filter PD measurements and nominally 200mmWG

Calibration checking should use at least 2 levels of PD standards to ensure an effective linearity and leak check:

For all parameters (size, weight,PD, ventilation and diameter), the defined values should be noted in the instrument configuration sheet. The defined and the

recalibrate the instrument

If possible do not recalibrate until all products have been measured. If this is impossible, make a note in the comments column.

standards should be calibrated according the CRM41 (June 2007).

200 mmWG and 400 mmWG nominal for cigarettes

adjustment, sleeves, measuring head; for filter rods length of sleeve-holder to ensure a totally encapsulated PD measurement)

The instrument system should be arranged to make the weight measurement first, followed by diameter or PD and ventilation (the order of these last three is normally

provided by the instrument system)

Before making measurements, the instrument(s) should be set up to accept the sample being measured ( e.g. for slim products – hopper

current ISO-standards:

Diameter: ISO 2971

All specific instrument information should be recorded in the instrument configuration sheet

At the beginning of each measuring day (run of all products) all instruments have to be checked for accuracy and, if necessary, recalibrated according to

PD: ISO 6565



Protocol – continued


Protocol – continued

4 Making Measurements

4.1

4.2

4.3

4.4

4.5

4.6

4.7

4.8

third measurement of sample 1

of product 1-5


of product 1-10

Day 1

second measurement of sample 1

of product 1-5

Randomise the order of sample measurement in a practical order to avoid excessive measuring head changes.

Repeat measurements on a sample/ instrument should take place on different days - see measurement scheme 4.8

Measurement Scheme:

Measure one set of products in one measurement run on one instrument within a single day - see measurement scheme 4.8

If the mean value is not based on a sample size of N=10 ( e.g. caused by damaging a cigarette/ filter rod during the measurement or a faulty measurement)


1*10*10+1*10*5 = 150 rods

Record mean and SD for each sample of 10 cigarettes or filters, as defined in data recording sheet - see 5.1

1*10*10 = 100 rods 1*10*10+1*10*5 = 150 rods



of product 6-10

Individual measurements in

total10*10*3 + 5*10*2= 400 rods

Individual measurements

per day


of product 1-10

Measure all parameters as defined in data recording sheets

Record data and time of each measurement as defined in data recording sheet - see 5.1

data recording sheet 1 and 2 data recording sheet 2


of product 1-5

please note the deviating N in the comments column.


Day 2 Day 3


Measurements should be made using the same measurement procedures as used on routine samples (daily business).



Instrument configuration



Data recording sheet 1



Data recording sheet 2


Appendix B: “2015 PTM Proficiency Test – Raw Data – Laboratories encoded – Data sheet 1”

Laboratory 1

Lab ID Product Type Product SampleMeasure-

ment

ID No. Mean SD Mean SD Mean SD Mean SD Mean SD Mean SD

[mg] [mg] [mm] [mm] [mmWG] [mmWG] [mmWG] [mmWG] [mmWG] [mmWG] [%] [%]

1 Filter F1 1 1 575,0 11,0 6,713 0,013 447,1 13,1

1 Filter F1 2 1 577,0 11,0 6,710 0,015 446,9 11,5

1 Filter F1 3 1 580,0 8,0 6,715 0,016 449,0 10,2

1 Filter F2 1 1 413,0 2,0 5,315 0,022 506,0 12,3

1 Filter F2 2 1 411,0 3,0 5,313 0,023 506,1 10,2

1 Filter F2 3 1 410,0 5,0 5,316 0,018 505,0 8,4

1 Filter F3 1 1 942,0 12,0 7,807 0,016 301,4 9,2

1 Filter F3 2 1 940,0 10,0 7,802 0,014 303,7 8,5

1 Filter F3 3 1 941,0 7,0 7,796 0,021 302,2 6,7

1 Filter F4 1 1 963,0 8,0 7,803 0,016 505,3 8,7

1 Filter F4 2 1 964,0 12,0 7,811 0,014 507,1 12,9

1 Filter F4 3 1 960,0 9,0 7,801 0,012 511,2 12,0

1 Filter F5 1 1 976,0 5,0 7,807 0,018 741,4 6,6

1 Filter F5 2 1 977,0 9,0 7,785 0,013 750,9 14,7

1 Filter F5 3 1 980,0 9,0 7,803 0,036 762,8 20,1

1 Cigarette C1 1 1 507,0 20,0 5,410 0,024 88,8 6,4 286,3 23,8 86,8 1,2

1 Cigarette C1 2 1 499,0 14,0 5,408 0,023 88,5 3,7 278,7 17,2 87,4 0,7

1 Cigarette C1 3 1 492,0 11,0 5,400 0,023 89,0 4,4 280,4 12,6 86,7 0,7

1 Cigarette C2 1 1 605,0 14,0 6,112 0,026 92,3 3,4 157,6 7,9 45,7 0,9

1 Cigarette C2 2 1 594,0 18,0 6,114 0,019 91,3 4,0 156,9 7,7 45,4 0,9

1 Cigarette C2 3 1 602,0 14,0 6,104 0,012 91,9 2,9 157,6 8,7 46,0 1,4

1 Cigarette C3 1 1 1022,0 21,0 7,489 0,029 95,2 3,0 137,7 4,3 35,7 1,7

1 Cigarette C3 2 1 1026,0 23,0 7,480 0,019 93,2 3,4 133,7 6,0 34,6 1,8

1 Cigarette C3 3 1 1021,0 18,0 7,489 0,020 93,2 3,5 133,8 6,2 35,0 1,2

1 Cigarette C4 1 1 817,0 21,0 7,848 0,017 74,2 2,8 96,1 5,5 29,3 2,1

1 Cigarette C4 2 1 807,0 23,0 7,857 0,031 74,5 2,9 96,3 5,2 29,7 2,3

1 Cigarette C4 3 1 812,0 17,0 7,852 0,019 73,5 3,0 94,6 5,0 28,7 2,3

1 Cigarette C5 1 1 806,0 18,0 7,873 0,039 70,8 2,3 119,7 3,7 53,1 1,3

1 Cigarette C5 2 1 803,0 19,0 7,871 0,034 71,8 2,8 118,9 4,4 51,9 1,7

1 Cigarette C5 3 1 799,0 16,0 7,877 0,020 71,7 2,1 118,3 5,8 51,4 1,9

Individual Wt Diameter PD open PD closed FV PD (fully encapsulated)



Laboratory 2


ment



2 Filter F1 1 1 576,6 7,8 6,713 0,008

2 Filter F1 2 1 577,9 9,4 6,716 0,008

2 Filter F1 3 1 586,2 8,4 6,713 0,009

2 Filter F2 1 1 411,6 2,8 5,328 0,012

2 Filter F2 2 1 412,4 2,1 5,324 0,010

2 Filter F2 3 1 407,3 3,7 5,322 0,010

2 Filter F3 1 1 939,6 5,8 7,809 0,013

2 Filter F3 2 1 938,7 8,8 7,808 0,014

2 Filter F3 3 1 935,9 5,7 7,804 0,011

2 Filter F4 1 1 961,2 8,8 7,813 0,019

2 Filter F4 2 1 965,9 14,4 7,810 0,013

2 Filter F4 3 1 963,3 3,6 7,812 0,007

2 Filter F5 1 1 971,7 6,8 7,797 0,014

2 Filter F5 2 1 978,5 6,7 7,790 0,010

2 Filter F5 3 1 980,6 4,1 7,798 0,011

2 Cigarette C1 1 1 505,7 14,9 5,408 0,014 90,2 4,5 298,5 14,1 88,9 1,0

2 Cigarette C1 2 1 500,3 12,1 5,408 0,025 85,8 5,4 283,1 12,0 89,2 1,4

2 Cigarette C1 3 1 501,2 16,6 5,422 0,025 87,6 2,3 278,2 22,0 88,7 1,2

2 Cigarette C2 1 1 600,1 9,4 6,122 0,013 90,3 4,3 155,0 8,9 47,0 1,0

2 Cigarette C2 2 1 594,7 13,7 6,112 0,023 89,1 3,6 152,0 6,8 46,6 1,6

2 Cigarette C2 3 1 596,9 11,6 6,111 0,015 90,8 2,5 153,4 4,7 46,1 0,8

2 Cigarette C3 1 1 1021,9 32,5 7,502 0,011 95,3 3,3 138,9 6,8 36,8 1,9

2 Cigarette C3 2 1 1026,9 26,2 7,491 0,020 93,8 1,6 134,5 4,2 35,8 1,5

2 Cigarette C3 3 1 1018,8 22,8 7,494 0,028 94,8 3,2 137,2 4,8 36,4 1,4

2 Cigarette C4 1 1 803,8 25,8 7,857 0,021 73,8 3,9 93,7 5,2 28,0 1,3

2 Cigarette C4 2 1 818,3 12,6 7,859 0,012 75,3 3,4 95,6 4,1 28,8 2,1

2 Cigarette C4 3 1 807,9 14,6 7,850 0,011 75,1 3,7 88,8 8,0 28,4 1,5

2 Cigarette C5 1 1 796,7 12,2 7,873 0,025 72,0 2,5 118,1 4,3 52,2 1,6

2 Cigarette C5 2 1 798,3 11,5 7,868 0,026 71,4 1,9 116,4 4,5 52,7 1,5

2 Cigarette C5 3 1 792,3 14,6 7,867 0,020 70,5 2,3 114,5 4,1 52,1 1,1




Laboratory 3


ment



3 Filter F1 1 1 597,5 11,0 6,720 0,014 438,4 10,4

3 Filter F1 2 1 567,7 8,0 6,719 0,023 438,6 13,2

3 Filter F1 3 1 578,5 12,0 6,722 0,011 436,1 12,4

3 Filter F2 1 1 409,6 4,0 5,327 0,014

3 Filter F2 2 1 411,6 4,0 5,321 0,011

3 Filter F2 3 1 410,5 3,0 5,319 0,016

3 Filter F3 1 1 930,7 8,0 7,804 0,016 298,1 4,7

3 Filter F3 2 1 937,7 10,0 7,797 0,018 301,4 8,4

3 Filter F3 3 1 927,3 9,0 7,807 0,013 294,3 6,9

3 Filter F4 1 1 959,7 7,0 7,813 0,013 504,0 9,5

3 Filter F4 2 1 967,1 10,0 7,806 0,013 509,6 10,0

3 Filter F4 3 1 965,3 9,0 7,812 0,012 506,0 8,4

3 Filter F5 1 1 974,0 8,0 7,800 0,017 732,1 11,1

3 Filter F5 2 1 974,3 6,0 7,801 0,015 731,5 14,8

3 Filter F5 3 1 968,7 7,0 7,803 0,017 722,0 11,2

3 Cigarette C1 1 1 505,0 15,0 5,399 0,031 91,4 4,5 276,5 20,3 86,8 1,2

3 Cigarette C1 2 1 500,2 11,0 5,413 0,016 90,8 6,0 281,8 19,5 87,2 1,5

3 Cigarette C1 3 1 504,5 17,0 5,409 0,028 86,9 5,5 276,8 20,7 87,5 1,2

3 Cigarette C2 1 1 603,9 13,0 6,120 0,019 91,7 4,8 157,8 9,4 46,6 1,9

3 Cigarette C2 2 1 594,4 13,0 6,108 0,022 91,2 4,1 155,4 7,6 46,3 1,5

3 Cigarette C2 3 1 601,4 12,0 6,109 0,024 94,1 4,0 161,5 7,7 46,7 1,3

3 Cigarette C3 1 1 1018,8 21,0 7,503 0,020 93,6 2,8 135,8 4,3 36,1 2,0

3 Cigarette C3 2 1 1017,7 26,0 7,498 0,023 92,1 3,3 132,3 6,0 35,9 1,5

3 Cigarette C3 3 1 1028,9 22,0 7,505 0,014 92,8 3,8 135,0 7,0 36,4 1,6

3 Cigarette C4 1 1 815,3 17,0 7,864 0,021 75,3 3,5 96,4 4,5 28,7 2,2

3 Cigarette C4 2 1 807,9 19,0 7,861 0,022 75,1 3,5 95,5 5,2 28,2 2,1

3 Cigarette C4 3 1 816,3 22,0 7,865 0,023 75,2 1,8 96,4 3,4 29,3 2,2

3 Cigarette C5 1 1 804,5 15,0 7,884 0,037 70,7 2,9 117,8 5,3 52,7 1,6

3 Cigarette C5 2 1 806,2 13,0 7,897 0,028 71,0 1,6 118,8 5,0 53,0 1,9

3 Cigarette C5 3 1 794,4 16,0 7,892 0,029 70,3 1,8 116,4 4,3 52,4 1,4




Laboratory 4


ment



4 Filter F1 1 1 584,4 6,1 6,721 0,010 433,5 8,3

4 Filter F1 2 1 578,9 10,7 6,718 0,007 436,7 12,0

4 Filter F1 3 1 584,2 9,7 6,721 0,010 441,1 13,3

4 Filter F2 1 1 413,0 3,2 5,325 0,011 503,1 9,5

4 Filter F2 2 1 411,0 3,2 5,323 0,009 505,1 8,9

4 Filter F2 3 1 411,8 3,4 5,326 0,014 504,7 11,3

4 Filter F3 1 1 939,7 6,0 7,813 0,020 293,3 5,4

4 Filter F3 2 1 943,4 8,3 7,818 0,014 296,8 5,9

4 Filter F3 3 1 939,0 5,7 7,812 0,020 294,2 5,2

4 Filter F4 1 1 969,3 9,4 7,821 0,011 503,8 10,3

4 Filter F4 2 1 964,5 4,0 7,815 0,014 503,1 10,4

4 Filter F4 3 1 970,2 11,2 7,815 0,017 509,7 12,0

4 Filter F5 1 1 982,9 5,0 7,823 0,017 742,8 11,8

4 Filter F5 2 1 978,7 5,8 7,808 0,015 740,2 11,6

4 Filter F5 3 1 982,9 5,5 7,806 0,027 748,0 7,0

4 Cigarette C1 1 1 507,7 9,9 5,403 0,018 88,3 4,7 283,0 13,7 88,6 1,2

4 Cigarette C1 2 1 503,7 8,0 5,405 0,011 85,7 3,4 272,3 17,2 88,8 0,7

4 Cigarette C1 3 1 512,4 18,6 5,396 0,017 86,5 3,9 282,0 20,2 88,6 1,4

4 Cigarette C2 1 1 606,9 15,4 6,108 0,009 90,7 4,1 158,0 10,6 47,1 1,7

4 Cigarette C2 2 1 608,6 13,9 6,109 0,027 92,2 3,4 158,4 8,6 46,7 2,3

4 Cigarette C2 3 1 607,8 9,2 6,106 0,025 94,2 4,1 162,2 7,3 47,4 1,8

4 Cigarette C3 1 1 1034,1 15,0 7,484 0,025 93,4 2,5 134,0 5,8 35,4 1,3

4 Cigarette C3 2 1 1019,8 18,0 7,488 0,022 94,3 4,0 134,8 6,1 35,2 1,4

4 Cigarette C3 3 1 1040,6 28,4 7,497 0,015 93,9 2,8 136,0 3,9 36,0 2,1

4 Cigarette C4 1 1 821,6 13,6 7,853 0,016 75,2 2,9 96,3 2,9 28,8 2,1

4 Cigarette C4 2 1 819,1 15,4 7,851 0,019 74,2 3,2 95,6 5,3 29,2 1,9

4 Cigarette C4 3 1 824,0 15,5 7,856 0,013 74,9 2,7 95,2 3,6 28,1 2,0

4 Cigarette C5 1 1 816,7 20,4 7,888 0,018 70,5 1,5 117,9 4,8 53,2 1,5

4 Cigarette C5 2 1 797,3 15,0 7,872 0,027 70,3 1,4 114,7 3,4 52,4 1,1

4 Cigarette C5 3 1 817,3 16,4 7,874 0,025 71,0 1,7 119,2 3,3 54,2 1,6



Appendix B: “2015 PTM Proficiency Test – Raw Data – Laboratories encoded – data sheet 1”

Laboratory 5

It is important that every yellow marked cell of the data sheet must be filled in, to make the transfer of data to the statistics package work as efficient as possible.

e - mail


ment



5 Filter F1 1 1 571,8 8,5 6,720 0,007 459,8 18,3

5 Filter F1 2 1 569,9 5,1 6,710 0,011 450,8 5,4

5 Filter F1 3 1 573,6 11,2 6,720 0,009 452,3 9,4

5 Filter F2 1 1 411,8 3,5 5,320 0,011 511,5 10,1

5 Filter F2 2 1 409,2 4,8 5,330 0,014 523,7 12,6

5 Filter F2 3 1 407,5 2,2 5,330 0,012 515,6 7,9

5 Filter F3 1 1 941,7 5,9 7,800 0,018 299,4 5,2

5 Filter F3 2 1 941,9 9,2 7,800 0,022 302,1 7,3

5 Filter F3 3 1 940,5 12,3 7,800 0,018 302,1 8,2

5 Filter F4 1 1 961,4 3,8 7,820 0,012 506,0 13,0

5 Filter F4 2 1 964,9 6,9 7,810 0,015 507,4 6,6

5 Filter F4 3 1 964,0 6,0 7,810 0,017 513,1 5,8

5 Filter F5 1 1 974,7 5,0 7,810 0,026 750,4 22,3

5 Filter F5 2 1 970,8 8,4 7,810 0,024 748,7 7,7

5 Filter F5 3 1 984,6 6,9 7,810 0,012 751,9 8,7

5 Cigarette C1 1 1 498,4 13,0 5,410 0,025 92,0 3,9 86,8 1,6

5 Cigarette C1 2 1 501,0 10,8 5,410 0,022 87,6 4,9 88,9 2,7

5 Cigarette C1 3 1 494,9 14,8 5,390 0,024 87,4 4,2 86,8 1,0

5 Cigarette C2 1 1 599,1 13,5 6,100 0,019 95,1 3,8 46,2 1,4

5 Cigarette C2 2 1 599,9 12,0 6,110 0,018 93,1 3,2 47,9 1,1

5 Cigarette C2 3 1 597,5 14,5 6,110 0,023 93,9 3,6 46,1 1,7

5 Cigarette C3 1 1 1022,8 29,6 7,500 0,014 95,5 3,6 35,0 1,8

5 Cigarette C3 2 1 1037,5 25,3 7,490 0,020 95,5 3,3 36,3 1,1

5 Cigarette C3 3 1 1013,8 20,5 7,500 0,031 94,2 2,0 36,1 2,0

5 Cigarette C4 1 1 804,6 16,0 7,850 0,010 73,6 4,1 34,7 4,7

5 Cigarette C4 2 1 812,6 14,2 7,860 0,015 75,4 2,2 30,4 2,0

5 Cigarette C4 3 1 803,9 16,0 7,850 0,013 76,3 2,1 30,4 2,3

5 Cigarette C5 1 1 796,3 20,3 7,880 0,039 70,7 2,5 53,5 3,2

5 Cigarette C5 2 1 802,7 12,9 7,890 0,026 70,5 1,6 52,6 1,7

5 Cigarette C5 3 1 802,6 27,8 7,890 0,024 71,1 2,9 54,0 3,5




Laboratory 6


ment



6 Filter F1 1 1 429,9 6,3

6 Filter F1 2 1 428,6 10,3

6 Filter F1 3 1 424,5 9,0

6 Filter F2 1 1 499,3 9,8

6 Filter F2 2 1 504,1 9,8

6 Filter F2 3 1 504,8 13,7

6 Filter F3 1 1 300,0 5,2

6 Filter F3 2 1 301,0 7,8

6 Filter F3 3 1 296,1 6,1

6 Filter F4 1 1 502,7 9,0

6 Filter F4 2 1 506,3 10,3

6 Filter F4 3 1 500,6 8,3

6 Filter F5 1 1 737,1 9,2

6 Filter F5 2 1 732,7 5,4

6 Filter F5 3 1 732,2 5,7

6 Cigarette C1 1 1 89,0 3,6 85,8 0,9

6 Cigarette C1 2 1 90,7 5,0 86,8 0,9

6 Cigarette C1 3 1 91,6 2,4 86,8 1,2

6 Cigarette C2 1 1 94,2 3,9 46,0 1,4

6 Cigarette C2 2 1 89,8 3,8 45,6 0,9

6 Cigarette C2 3 1 89,8 3,8 45,6 0,9

6 Cigarette C3 1 1 94,6 3,4 35,9 1,7

6 Cigarette C3 2 1 92,9 2,5 35,3 1,2

6 Cigarette C3 3 1 93,3 2,5 35,1 1,5

6 Cigarette C4 1 1 75,3 2,8 29,3 2,3

6 Cigarette C4 2 1 76,3 2,4 29,2 2,3

6 Cigarette C4 3 1 75,5 2,0 29,6 1,9

6 Cigarette C5 1 1 72,6 1,7 52,2 1,4

6 Cigarette C5 2 1 70,4 1,5 52,5 1,4

6 Cigarette C5 3 1 70,0 3,5 52,2 1,4




Laboratory 7


ment



7 Filter F1 1 1 579,1 6,3 6,714 0,005 396,4 13,7

7 Filter F1 2 1 578,1 10,6 6,711 0,005 408,0 7,7

7 Filter F1 3 1 578,5 9,9 6,720 0,010 403,6 8,8

7 Filter F2 1 1 413,2 3,9 5,327 0,010 473,9 10,5

7 Filter F2 2 1 412,7 4,1 5,329 0,017 477,0 11,6

7 Filter F2 3 1 413,8 4,4 5,326 0,013 465,4 11,4

7 Filter F3 1 1 932,7 12,1 7,798 0,018 285,0 5,1

7 Filter F3 2 1 934,9 5,8 7,807 0,020 285,0 5,0

7 Filter F3 3 1 943,7 13,2 7,809 0,014 282,3 9,5

7 Filter F4 1 1 967,0 8,3 7,813 0,012 464,6 6,5

7 Filter F4 2 1 961,0 7,1 7,810 0,010 466,7 8,2

7 Filter F4 3 1 962,6 9,6 7,813 0,014 456,7 9,9

7 Filter F5 1 1 978,4 5,0 7,805 0,018 646,7 25,5

7 Filter F5 2 1 976,0 7,3 7,802 0,010 659,2 12,8

7 Filter F5 3 1 979,2 8,0 7,803 0,017 638,6 23,1

7 Cigarette C1 1 1 500,0 16,0 5,392 0,027 88,9 3,7 287,1 24,2 88,1 0,9

7 Cigarette C1 2 1 497,5 18,5 5,413 0,015 84,9 5,8 289,1 26,5 89,1 1,0

7 Cigarette C1 3 1 503,2 12,6 5,397 0,022 89,1 5,3 287,1 24,2 88,9 1,1

7 Cigarette C2 1 1 603,9 14,1 6,105 0,020 92,8 2,9 162,5 6,3 47,2 1,4

7 Cigarette C2 2 1 600,2 16,0 6,112 0,019 91,6 2,3 160,7 5,9 48,7 1,5

7 Cigarette C2 3 1 606,2 11,4 6,121 0,018 92,9 2,6 160,6 9,4 46,9 2,2

7 Cigarette C3 1 1 1030,9 26,3 7,485 0,021 95,3 3,8 140,0 6,3 36,5 1,5

7 Cigarette C3 2 1 1023,5 15,8 7,491 0,030 96,0 4,0 139,8 5,9 37,3 1,8

7 Cigarette C3 3 1 1018,1 26,3 7,475 0,020 93,5 3,3 138,9 5,9 37,6 1,1

7 Cigarette C4 1 1 820,9 8,5 7,858 0,011 77,6 2,7 98,5 3,3 29,9 1,8

7 Cigarette C4 2 1 814,8 18,8 7,855 0,016 77,4 3,8 101,5 6,5 30,2 1,8

7 Cigarette C4 3 1 821,6 13,7 7,851 0,015 76,2 1,0 98,9 2,7 29,7 1,4

7 Cigarette C5 1 1 814,9 16,5 7,902 0,030 71,7 1,6 71,7 1,6 54,3 1,6

7 Cigarette C5 2 1 818,7 18,3 7,886 0,021 72,0 2,9 123,3 4,9 54,1 1,7

7 Cigarette C5 3 1 813,8 16,6 7,874 0,019 72,7 2,4 123,0 6,3 53,7 2,9




Laboratory 8


ment



8 Filter F1 1 1 577,0 5,9 6,708 0,008 445,4 9,9

8 Filter F1 2 1 577,0 5,5 6,704 0,007 447,4 10,6

8 Filter F1 3 1 578,7 12,3 6,711 0,009 447,8 12,4

8 Filter F2 1 1 409,3 3,8 5,318 0,010 515,7 12,9

8 Filter F2 2 1 412,3 4,2 5,320 0,012 512,6 14,0

8 Filter F2 3 1 411,8 3,9 5,322 0,011 505,9 13,8

8 Filter F3 1 1 936,9 7,2 7,791 0,018 301,5 6,0

8 Filter F3 2 1 940,2 21,0 7,794 0,017 299,7 11,4

8 Filter F3 3 1 936,5 10,7 7,793 0,014 298,0 7,4

8 Filter F4 1 1 965,6 8,3 7,805 0,007 509,4 7,6

8 Filter F4 2 1 964,1 10,7 7,802 0,016 511,9 12,3

8 Filter F4 3 1 973,7 6,7 7,805 0,014 515,0 8,4

8 Filter F5 1 1 981,7 4,2 7,799 0,031 754,3 12,0

8 Filter F5 2 1 979,6 8,0 7,795 0,007 747,3 11,6

8 Filter F5 3 1 980,9 6,2 7,803 0,020 750,3 10,0

8 Cigarette C1 1 1 511,9 14,7 5,423 0,019 84,7 5,5 280,9 19,6 90,1 1,5

8 Cigarette C1 2 1 516,0 12,9 5,392 0,028 82,1 9,0 288,1 18,5 90,2 2,4

8 Cigarette C1 3 1 500,5 19,8 5,378 0,042 86,3 9,0 280,2 19,4 90,0 1,1

8 Cigarette C2 1 1 592,4 8,5 6,120 0,019 88,7 3,0 153,9 8,3 48,6 1,3

8 Cigarette C2 2 1 608,2 11,1 6,126 0,018 89,8 3,1 156,1 6,5 47,0 1,3

8 Cigarette C2 3 1 596,7 13,5 6,114 0,025 92,0 3,1 159,8 7,2 48,5 1,9

8 Cigarette C3 1 1 1028,4 15,0 7,506 0,013 96,6 3,3 141,2 5,2 37,1 1,4

8 Cigarette C3 2 1 1035,9 23,9 7,495 0,024 96,8 3,2 144,0 7,2 38,1 1,2

8 Cigarette C3 3 1 1017,9 18,5 7,496 0,034 96,0 4,0 139,5 6,2 36,2 1,3

8 Cigarette C4 1 1 817,0 23,0 7,862 0,010 75,7 3,2 95,0 5,4 29,7 1,5

8 Cigarette C4 2 1 806,8 14,3 7,854 0,015 75,3 2,5 93,6 6,8 31,4 2,3

8 Cigarette C4 3 1 832,8 20,0 7,858 0,018 77,4 2,1 98,8 4,4 34,4 1,7

8 Cigarette C5 1 1 797,9 12,3 7,868 0,027 71,2 2,4 120,5 5,6 56,0 1,8

8 Cigarette C5 2 1 813,6 15,8 7,882 0,025 72,4 2,2 120,6 8,5 55,9 1,9

8 Cigarette C5 3 1 807,0 13,9 7,881 0,021 72,2 1,2 117,9 6,4 54,5 2,2




Laboratory 9


ment



9 Filter F1 1 1 576,5 8,0 6,717 0,009

9 Filter F1 2 1 573,8 6,0 6,711 0,006

9 Filter F1 3 1 568,6 4,0 6,721 0,003

9 Filter F2 1 1 416,7 4,0 5,322 0,012

9 Filter F2 2 1 411,6 4,0 5,322 0,008

9 Filter F2 3 1 413,7 3,0 5,322 0,008

9 Filter F3 1 1 943,2 16,0 7,805 0,016

9 Filter F3 2 1 938,0 13,0 7,806 0,015

9 Filter F3 3 1 940,1 9,0 7,807 0,018

9 Filter F4 1 1 966,7 9,0 7,818 0,016

9 Filter F4 2 1 969,9 9,0 7,817 0,014

9 Filter F4 3 1 962,3 9,0 7,818 0,018

9 Filter F5 1 1

9 Filter F5 2 1 980,7 10,0 7,812 0,025

9 Filter F5 3 1 983,5 5,0 7,811 0,011

9 Cigarette C1 1 1 508,7 19,0 5,400 0,019 85,3 3,4 287,2 17,0 90,0 1,8

9 Cigarette C1 2 1 506,7 9,0 5,403 0,017 85,8 5,5 269,4 13,0 89,7 1,0

9 Cigarette C1 3 1 501,2 11,0 5,390 0,031 88,6 4,4 277,8 18,1 89,5 0,9

9 Cigarette C2 1 1 600,2 13,0 6,115 0,028 91,3 4,2 157,7 8,6 46,7 1,3

9 Cigarette C2 2 1 600,5 12,0 6,099 0,021 90,8 4,2 156,8 7,2 47,1 1,5

9 Cigarette C2 3 1 604,8 12,0 6,104 0,017 91,4 5,0 160,6 9,4 47,9 1,3

9 Cigarette C3 1 1 1033,1 22,0 7,494 0,022 93,6 2,9 135,2 4,9 36,2 1,7

9 Cigarette C3 2 1 1024,8 22,0 7,494 0,021 92,1 2,1 130,0 3,9 35,5 1,6

9 Cigarette C3 3 1 1041,1 24,0 7,489 0,025 93,8 2,7 133,2 4,7 36,7 1,2

9 Cigarette C4 1 1 824,5 20,0 7,859 0,017 74,6 2,8 92,7 5,0 30,4 2,1

9 Cigarette C4 2 1 816,9 18,0 7,855 0,019 73,0 2,6 93,5 4,6 30,6 1,8

9 Cigarette C4 3 1 822,8 23,0 7,867 0,015 76,5 3,8 96,4 5,6 30,9 1,5

9 Cigarette C5 1 1 808,6 18,0 7,878 0,024 69,4 1,4 116,0 2,8 53,6 2,1

9 Cigarette C5 2 1 813,5 15,0 7,877 0,025 70,3 2,3 117,0 3,3 54,2 1,2

9 Cigarette C5 3 1 807,7 21,0 7,857 0,037 71,1 2,6 118,5 6,6 54,8 1,8




Laboratory 10


ment



10 Filter F1 1 1 574,4 5,1 6,718 0,008 460,4 10,8

10 Filter F1 2 1 566,7 11,6 6,715 0,007 441,2 11,9

10 Filter F1 3 1 572,2 6,2 6,709 0,009 455,9 10,7

10 Filter F2 1 1 412,6 4,2 5,323 0,015 525,3 14,3

10 Filter F2 2 1 412,1 3,5 5,330 0,014 525,3 13,3

10 Filter F2 3 1 410,5 4,1 5,324 0,007 523,8 12,3

10 Filter F3 1 1 937,1 9,9 7,802 0,021 312,1 5,4

10 Filter F3 2 1 933,5 9,8 7,798 0,018 307,9 6,8

10 Filter F3 3 1 937,4 7,1 7,794 0,020 309,8 5,1

10 Filter F4 1 1 964,0 6,7 7,803 0,015 521,4 8,6

10 Filter F4 2 1 961,9 8,5 7,812 0,017 517,3 7,3

10 Filter F4 3 1 962,7 9,2 7,808 0,013 520,6 9,3

10 Filter F5 1 1 972,3 8,9 7,806 0,018 751,6 18,8

10 Filter F5 2 1 977,5 7,4 7,791 0,011 757,2 17,1

10 Filter F5 3 1 970,9 9,1 7,794 0,016 746,7 12,9

10 Cigarette C1 1 1 498,9 13,2 5,412 0,023 89,7 6,1 275,3 14,4 87,7 1,2

10 Cigarette C1 2 1 494,2 9,2 5,399 0,016 88,5 3,3 248,9 6,9 86,3 1,5

10 Cigarette C1 3 1 492,5 13,5 5,402 0,027 86,9 4,5 250,8 7,0 86,8 1,1

10 Cigarette C2 1 1 588,7 11,1 6,113 0,020 90,7 3,3 160,8 6,6 45,7 1,0

10 Cigarette C2 2 1 599,7 14,6 6,121 0,025 89,8 2,4 142,2 4,7 45,3 1,5

10 Cigarette C2 3 1 591,6 9,2 6,111 0,019 88,8 3,2 140,7 5,2 45,0 1,5

10 Cigarette C3 1 1 1008,0 20,7 7,504 0,023 91,1 2,4 129,5 3,6 34,3 1,3

10 Cigarette C3 2 1 1008,4 25,3 7,492 0,020 91,5 6,0 131,9 6,5 36,4 3,4

10 Cigarette C3 3 1 1008,8 20,2 7,484 0,022 91,3 2,9 129,9 2,9 34,6 1,7

10 Cigarette C4 1 1 818,8 14,2 7,848 0,009 74,8 2,2 95,2 2,4 27,8 1,5

10 Cigarette C4 2 1 810,0 18,4 7,859 0,007 75,3 1,6 96,5 3,4 28,6 1,6

10 Cigarette C4 3 1 802,0 21,0 7,844 0,018 72,6 2,4 91,5 4,0 26,7 2,7

10 Cigarette C5 1 1 794,8 18,3 7,879 0,030 69,7 2,0 114,6 3,4 52,1 1,0

10 Cigarette C5 2 1 791,6 9,1 7,883 0,013 69,7 1,9 114,0 2,8 51,6 1,2

10 Cigarette C5 3 1 794,6 17,1 7,858 0,024 69,8 2,6 114,0 3,7 51,1 1,6




Laboratory 11


ment



11 Cigarette C1 1 1 495,9 13,7 5,399 0,1 85,6 3,1 258,9 23,7 91,0

11 Cigarette C1 2 1 493,4 14,8 5,403 0,0 84,6 4,9 262,8 22,4 91,1 1,1

11 Cigarette C1 3 1 492,2 15,8 5,398 0,1 84,0 4,5 271,4 14,2 92,2 1,8

11 Cigarette C2 1 1 598,5 10,4 6,123 0,1 90,4 2,6 161,9 6,5 48,6 2,0

11 Cigarette C2 2 1 593,2 15,9 6,123 0,1 90,2 4,5 157,9 8,1 47,8 1,7

11 Cigarette C2 3 1 585,0 10,9 6,107 0,1 89,1 3,7 156,7 5,8 47,0 1,7

11 Cigarette C3 1 1 1011,0 21,4 7,487 0,0 92,7 2,8 129,6 4,9 36,0 1,5

11 Cigarette C3 2 1 1006,0 16,1 7,476 0,1 91,9 2,5 125,6 5,7 35,4 1,6

11 Cigarette C3 3 1 989,8 16,2 7,481 0,1 89,9 5,4 124,3 8,1 36,2 1,7

11 Cigarette C4 1 1 796,0 14,1 7,842 0,1 75,4 2,7 96,2 3,0 29,1 2,3

11 Cigarette C4 2 1 791,8 15,7 7,839 0,1 74,1 2,3 94,0 4,8 30,8 2,3

11 Cigarette C4 3 1 806,6 12,7 7,840 0,1 74,2 2,7 97,7 3,3 31,8 1,7

11 Cigarette C5 1 1 790,0 11,9 7,854 0,1 71,3 1,7 111,3 4,0 54,4 1,9

11 Cigarette C5 2 1 783,1 14,0 7,854 0,1 69,9 1,9 107,7 3,5 53,9 1,4

11 Cigarette C5 3 1 786,0 16,5 7,857 0,1 70,2 2,0 110,8 5,7 55,5 1,2




Laboratory 12


ment



12 Filter F1 1 1 574,0 11,0 6,713 0,007 486,0 14,0

12 Filter F1 2 1 570,0 5,0 6,711 0,009 479,0 17,0

12 Filter F1 3 1 574,0 7,0 6,712 0,005 493,0 17,0

12 Filter F2 1 1 410,0 4,0 5,342 0,021 512,0 15,0

12 Filter F2 2 1 409,0 7,0 5,322 0,024 510,0 18,0

12 Filter F2 3 1 410,0 4,0 5,337 0,016 520,0 13,0

12 Filter F3 1 1 945,0 12,0 7,810 0,010 304,0 7,0

12 Filter F3 2 1 926,0 8,0 7,810 0,012 298,0 7,0

12 Filter F3 3 1 939,0 11,0 7,808 0,012 306,0 7,0

12 Filter F4 1 1 970,0 10,0 7,814 0,015 520,0 12,0

12 Filter F4 2 1 961,0 8,0 7,825 0,017 509,0 9,0

12 Filter F4 3 1 966,0 10,0 7,817 0,017 518,0 10,0

12 Filter F5 1 1 977,0 9,0 7,805 0,013 752,0 15,0

12 Filter F5 2 1 972,0 12,0 7,806 0,012 744,0 20,0

12 Filter F5 3 1 974,0 10,0 7,816 0,030 752,0 16,0

12 Cigarette C1 1 1 503,0 11,0 5,425 0,024 91,0 4,0 277,0 21,0 88,4 1,8

12 Cigarette C1 2 1 499,0 10,0 5,405 0,016 91,0 5,0 270,0 16,0 88,2 1,0

12 Cigarette C1 3 1 500,0 20,0 5,413 0,030 92,0 5,0 271,0 15,0 89,9 1,2

12 Cigarette C2 1 1 595,0 11,0 6,107 0,017 91,0 3,0 153,0 7,0 46,1 1,2

12 Cigarette C2 2 1 595,0 11,0 6,105 0,018 91,0 3,0 150,0 7,0 44,9 1,3

12 Cigarette C2 3 1 598,0 12,0 6,118 0,023 94,0 3,0 160,0 6,0 47,3 0,8

12 Cigarette C3 1 1 1014,0 29,0 7,506 0,016 92,0 2,0 133,0 6,0 36,6 2,0

12 Cigarette C3 2 1 1015,0 17,0 7,509 0,024 92,0 3,0 127,0 10,0 35,5 2,1

12 Cigarette C3 3 1 1009,0 13,0 7,504 0,019 93,0 2,0 130,0 7,0 34,5 1,9

12 Cigarette C4 1 1 798,0 22,0 7,857 0,017 77,0 3,0 95,0 6,0 27,4 1,9

12 Cigarette C4 2 1 809,0 19,0 7,866 0,014 73,0 2,0 90,0 3,0 26,3 1,7

12 Cigarette C4 3 1 820,0 22,0 7,860 0,019 76,0 3,0 95,0 3,0 28,0 2,4

12 Cigarette C5 1 1 800,0 15,0 7,878 0,020 72,0 2,0 118,0 6,0 52,7 1,8

12 Cigarette C5 2 1 799,0 9,0 7,908 0,025 70,0 2,0 115,0 5,0 52,3 1,2

12 Cigarette C5 3 1 791,0 28,0 7,873 0,030 72,0 3,0 117,0 5,0 52,7 1,1




Laboratory 13


ment



13 Filter F1 1 1 577,3 12,0 6,725 0,011 441,2 13,6

13 Filter F1 2 1 569,4 13,0 6,725 0,007 436,8 16,3

13 Filter F1 3 1 568,3 7,0 6,717 0,007 453,9 8,6

13 Filter F2 1 1 410,8 3,0 5,328 0,011 518,6 9,0

13 Filter F2 2 1 410,9 4,0 5,331 0,019 518,6 11,3

13 Filter F2 3 1 412,0 5,0 5,324 0,021 519,0 13,7

13 Filter F3 1 1 933,8 13,0 7,809 0,010 301,0 12,0

13 Filter F3 2 1 934,0 8,0 7,792 0,015 305,3 5,4

13 Filter F3 3 1 941,2 7,0 7,802 0,012 304,7 4,5

13 Filter F4 1 1 952,3 10,0 7,806 0,014 510,0 12,3

13 Filter F4 2 1 962,6 11,0 7,805 0,016 506,7 10,9

13 Filter F4 3 1 964,6 7,0 7,808 0,015 512,6 8,7

13 Filter F5 1 1 969,0 7,0 7,802 0,012 745,7 13,1

13 Filter F5 2 1 967,2 6,0 7,805 0,014 739,3 16,2

13 Filter F5 3 1 976,8 9,0 7,805 0,018 751,6 16,0




Laboratory 14


ment



14 Filter F1 1 1 583,9 8,8 6,715 0,007 458,3 15,4

14 Filter F1 2 1 580,7 9,0 6,716 0,008 451,1 14,4

14 Filter F1 3 1 577,4 6,2 6,713 0,006 450,4 8,8

14 Filter F2 1 1 411,6 2,5 5,327 0,011 520,1 6,6

14 Filter F2 2 1 411,2 2,1 5,321 0,010 518,1 9,3

14 Filter F2 3 1 409,8 4,0 5,321 0,026 519,0 14,4

14 Filter F3 1 1 939,0 11,5 7,799 0,018 301,9 5,9

14 Filter F3 2 1 944,7 7,3 7,797 0,016 305,9 8,6

14 Filter F3 3 1 940,1 8,5 7,797 0,020 306,1 6,6

14 Filter F4 1 1 955,0 12,0 7,809 0,014 504,9 17,1

14 Filter F4 2 1 964,8 10,2 7,812 0,019 512,2 8,7

14 Filter F4 3 1 961,9 11,0 7,814 0,013 514,6 12,5

14 Filter F5 1 1 975,2 6,8 7,805 0,020 738,8 13,6

14 Filter F5 2 1 976,8 6,4 7,803 0,010 735,3 9,8

14 Filter F5 3 1 975,2 8,9 7,803 0,022 739,0 13,7

14 Cigarette C1 1 1 507,1 14,4 5,405 0,026 86,0 4,3 278,6 12,7 88,8 1,2

14 Cigarette C1 2 1 507,5 14,8 5,414 0,022 84,9 3,9 280,5 17,8 88,5 1,8

14 Cigarette C1 3 1 498,5 12,0 5,395 0,026 83,7 6,0 273,4 12,4 88,5 1,1

14 Cigarette C2 1 1 601,1 13,3 6,116 0,016 89,4 3,4 153,3 7,5 45,5 0,6

14 Cigarette C2 2 1 598,3 8,7 6,116 0,025 90,0 4,3 156,6 8,4 46,6 1,4

14 Cigarette C2 3 1 600,9 9,6 6,131 0,017 89,6 3,2 153,5 4,0 45,7 1,0

14 Cigarette C3 1 1 1040,5 27,7 7,489 0,021 95,9 4,0 141,5 7,1 36,4 1,9

14 Cigarette C3 2 1 1022,5 20,0 7,492 0,015 91,8 3,4 134,1 5,2 35,8 2,0

14 Cigarette C3 3 1 1026,2 21,3 7,493 0,024 92,0 3,9 134,3 6,7 35,9 1,0

14 Cigarette C4 1 1 816,4 24,2 7,852 0,010 72,4 4,0 93,9 4,4 29,3 2,0

14 Cigarette C4 2 1 817,9 15,3 7,853 0,015 75,0 2,2 97,9 4,3 29,3 1,4

14 Cigarette C4 3 1 815,0 17,7 7,852 0,013 72,7 1,7 93,2 2,7 28,4 1,9

14 Cigarette C5 1 1 810,0 27,9 7,870 0,030 70,5 2,4 118,9 6,4 53,2 1,7

14 Cigarette C5 2 1 807,9 10,9 7,873 0,025 70,7 2,2 119,1 3,2 52,7 1,8

14 Cigarette C5 3 1 798,0 16,9 7,877 0,027 70,5 2,8 117,4 5,4 52,7 1,5




Laboratory 15


ment



15 Filter F1 1 1 588,0 8,0 6,717 0,006 445,0 16,0

15 Filter F1 2 1 587,0 8,0 6,721 0,005 447,0 6,0

15 Filter F1 3 1 573,0 12,0 6,725 0,011 436,0 15,0

15 Filter F2 1 1

15 Filter F2 2 1

15 Filter F2 3 1

15 Filter F3 1 1 938,0 10,0 7,811 0,018 296,0 8,0

15 Filter F3 2 1 940,0 9,0 7,799 0,015 301,0 6,0

15 Filter F3 3 1 941,0 9,0 7,811 0,011 301,0 7,0

15 Filter F4 1 1 973,0 9,0 7,810 0,020 510,0 11,0

15 Filter F4 2 1 966,0 8,0 7,814 0,013 509,0 9,0

15 Filter F4 3 1 964,0 5,0 7,811 0,013 509,0 10,0

15 Filter F5 1 1 983,0 7,0 7,811 0,026 743,0 14,0

15 Filter F5 2 1 976,0 5,0 7,807 0,010 734,0 8,0

15 Filter F5 3 1 979,0 7,0 7,811 0,015 741,0 13,0

15 Cigarette C1 1 1 506,5 10,1 5,425 0,023 87,0 3,7 281,5 15,9 88,9 1,1

15 Cigarette C1 2 1 507,0 12,2 5,406 0,014 89,0 3,6 275,9 17,3 88,2 1,4

15 Cigarette C1 3 1 505,0 18,9 5,407 0,008 87,0 3,6 269,2 27,4 87,8 2,2

15 Cigarette C2 1 1 598,4 13,1 6,096 0,026 91,0 3,5 155,0 7,2 45,8 1,3

15 Cigarette C2 2 1 593,3 9,1 6,107 0,016 92,0 3,8 157,4 7,2 46,3 1,6

15 Cigarette C2 3 1 596,9 11,2 6,106 0,012 88,0 4,3 149,8 9,1 45,7 1,7

15 Cigarette C3 1 1 1009,5 21,6 7,488 0,016 90,0 3,6 130,0 6,1 35,7 2,2

15 Cigarette C3 2 1 1029,7 37,1 7,492 0,026 93,0 3,7 135,7 7,5 36,7 1,5

15 Cigarette C3 3 1 1017,8 17,9 7,496 0,024 92,0 2,1 130,1 3,1 34,2 1,2

15 Cigarette C4 1 1 820,7 18,0 7,866 0,011 76,0 2,8 96,6 4,2 28,1 1,7

15 Cigarette C4 2 1 812,3 21,0 7,851 0,021 74,0 3,6 94,5 6,6 28,1 2,1

15 Cigarette C4 3 1 808,7 16,5 7,862 0,022 74,0 3,3 93,2 3,9 27,9 2,3

15 Cigarette C5 1 1 785,7 53,9 7,878 0,030 71,0 1,4 118,2 3,8 52,5 1,6

15 Cigarette C5 2 1 809,3 12,4 7,891 0,032 71,0 1,8 118,6 5,3 53,4 1,8

15 Cigarette C5 3 1 810,2 20,9 7,867 0,023 70,0 2,9 116,0 6,9 52,7 2,1




Laboratory 16


ment



16 Filter F1 1 1 574,4 8,5 6,715 0,004 431,3 10,9

16 Filter F1 2 1 582,5 10,5 6,719 0,006 439,3 12,8

16 Filter F1 3 1 575,9 12,1 6,706 0,007 433,5 17,8

16 Filter F2 1 1 410,2 3,7 5,325 0,016 506,2 9,8

16 Filter F2 2 1 408,8 4,6 5,322 0,009 506,1 17,4

16 Filter F2 3 1 412,2 2,5 5,320 0,017 510,1 11,3

16 Filter F3 1 1 941,9 12,1 7,805 0,018 302,2 7,3

16 Filter F3 2 1 934,9 7,0 7,806 0,020 295,7 6,0

16 Filter F3 3 1 937,7 7,6 7,808 0,016 298,7 5,0

16 Filter F4 1 1 959,7 5,4 7,803 0,012 508,0 9,9

16 Filter F4 2 1 963,2 8,0 7,817 0,014 503,4 10,2

16 Filter F4 3 1 962,2 7,2 7,811 0,013 504,1 10,4

16 Filter F5 1 1 971,8 8,7 7,817 0,030 734,9 13,5

16 Filter F5 2 1 969,1 7,3 7,797 0,011 737,0 12,3

16 Filter F5 3 1 969,4 10,0 7,803 0,011 734,9 17,3

16 Cigarette C1 1 1 496,0 9,9 5,421 0,021 87,0 3,9 270,5 16,0 87,6 1,1

16 Cigarette C1 2 1 500,1 22,0 5,414 0,015 86,6 3,7 273,7 20,1 88,3 1,2

16 Cigarette C1 3 1 509,8 13,8 5,422 0,017 84,9 4,3 277,7 16,6 88,9 1,8

16 Cigarette C2 1 1 589,1 7,9 6,115 0,016 91,9 4,1 156,5 7,4 45,4 1,8

16 Cigarette C2 2 1 602,7 14,2 6,114 0,011 91,4 4,8 157,7 8,6 47,3 1,5

16 Cigarette C2 3 1 599,3 14,2 6,100 0,016 92,5 5,3 153,8 8,1 45,3 1,2

16 Cigarette C3 1 1 1009,8 21,3 7,490 0,026 92,1 2,3 131,9 3,9 34,9 1,7

16 Cigarette C3 2 1 1026,3 25,1 7,497 0,023 91,2 4,1 133,4 5,4 37,4 1,6

16 Cigarette C3 3 1 1024,6 18,6 7,492 0,023 93,4 2,8 134,2 4,3 36,1 1,2

16 Cigarette C4 1 1 813,6 15,1 7,857 0,023 74,8 3,6 94,7 5,0 27,7 1,9

16 Cigarette C4 2 1 814,6 20,6 7,858 0,016 75,0 2,5 96,1 4,1 28,8 2,3

16 Cigarette C4 3 1 804,3 21,9 7,856 0,020 73,7 2,3 93,5 4,4 28,0 3,4

16 Cigarette C5 1 1 793,3 14,9 7,870 0,013 69,9 1,9 115,6 5,2 52,3 1,7

16 Cigarette C5 2 1 796,0 10,2 7,863 0,032 69,4 4,7 116,9 7,5 54,3 1,6

16 Cigarette C5 3 1 787,4 19,6 7,871 0,018 70,4 1,8 115,9 4,1 53,2 1,2




Laboratory 17


ment



17 Filter F1 1 1 579,2 10,7 6,714 0,009 457,4 16,1

17 Filter F1 2 1 586,5 5,5 6,710 0,016 453,4 12,4

17 Filter F1 3 1 575,1 10,6 6,715 0,005 451,0 16,4

17 Filter F2 1 1 411,4 3,2 5,333 0,010 524,4 9,2

17 Filter F2 2 1 414,1 3,5 5,330 0,013 518,0 8,3

17 Filter F2 3 1 408,4 2,1 5,325 0,007 507,7 9,8

17 Filter F3 1 1 940,7 7,4 7,809 0,015 306,4 6,3

17 Filter F3 2 1 940,4 11,4 7,801 0,019 301,7 9,6

17 Filter F3 3 1 934,2 11,3 7,797 0,011 297,6 8,7

17 Filter F4 1 1 963,2 4,1 7,818 0,009 520,3 6,6

17 Filter F4 2 1 959,3 12,1 7,818 0,009 508,3 10,6

17 Filter F4 3 1 964,6 6,6 7,811 0,011 509,6 8,9

17 Filter F5 1 1 973,5 8,1 7,804 0,014 759,7 13,4

17 Filter F5 2 1 973,4 7,9 7,802 0,013 743,2 15,1

17 Filter F5 3 1 977,9 5,9 7,814 0,014 746,1 6,9

17 Cigarette C1 1 1 507,3 19,0 5,428 0,014 87,9 4,8 285,7 20,6 87,8 1,6

17 Cigarette C1 2 1 509,0 15,8 5,409 0,021 87,2 3,9 287,2 24,5 88,1 1,5

17 Cigarette C1 3 1 503,3 16,6 5,426 0,026 87,3 3,4 276,6 25,7 88,1 1,6

17 Cigarette C2 1 1 593,4 12,4 6,120 0,014 88,8 3,8 150,0 9,4 45,4 2,0

17 Cigarette C2 2 1 597,4 11,1 6,121 0,016 88,9 3,1 150,6 4,4 44,7 1,2

17 Cigarette C2 3 1 590,7 9,1 6,098 0,015 88,8 2,1 149,3 4,6 44,9 1,1

17 Cigarette C3 1 1 1032,9 26,3 7,500 0,027 93,0 2,8 134,4 6,3 35,4 1,7

17 Cigarette C3 2 1 1030,0 19,1 7,508 0,024 93,2 1,9 135,5 4,5 35,4 1,6

17 Cigarette C3 3 1 1038,2 22,1 7,518 0,018 94,0 3,9 136,7 6,1 35,7 2,0

17 Cigarette C4 1 1 810,4 21,3 7,858 0,011 75,4 2,6 95,9 4,5 28,1 1,8

17 Cigarette C4 2 1 799,4 15,2 7,854 0,010 74,8 3,4 95,2 4,3 27,7 1,6

17 Cigarette C4 3 1 813,8 16,6 7,865 0,017 74,1 2,5 94,3 3,6 27,9 1,8

17 Cigarette C5 1 1 802,4 19,6 7,886 0,036 71,0 2,2 115,1 4,3 50,9 1,9

17 Cigarette C5 2 1 801,4 11,8 7,870 0,037 70,1 1,8 118,3 3,7 52,9 0,7

17 Cigarette C5 3 1 804,7 22,8 7,880 0,023 69,9 2,4 114,1 5,6 51,3 1,6




Laboratory 18


ment



18 Filter F1 1 1 577,2 7,3 6,725 0,007

18 Filter F1 2 1 581,1 6,0 6,713 0,017

18 Filter F1 3 1 582,8 4,0 6,726 0,014

18 Filter F2 1 1

18 Filter F2 2 1

18 Filter F2 3 1

18 Filter F3 1 1 946,0 8,8 7,809 0,014

18 Filter F3 2 1 931,0 8,1 7,811 0,016

18 Filter F3 3 1 922,5 6,3 7,810 0,015

18 Filter F4 1 1 956,6 8,5 7,819 0,009

18 Filter F4 2 1 966,1 6,3 7,818 0,010

18 Filter F4 3 1 967,7 5,7 7,812 0,013

18 Filter F5 1 1 975,9 7,1 7,807 0,006

18 Filter F5 2 1 978,9 6,8 7,801 0,010

18 Filter F5 3 1 977,6 8,1 7,803 0,016

18 Cigarette C1 1 1 508,8 13,6 5,393 0,012 88,2 3,7 290,4 11,2 90,3 1,0

18 Cigarette C1 2 1 503,0 7,1 5,402 0,017 90,7 3,8 286,8 11,0 89,4 1,0

18 Cigarette C1 3 1 500,9 13,6 5,393 0,020 87,6 3,8 281,0 12,1 89,2 0,9

18 Cigarette C2 1 1 588,1 10,6 6,123 0,024 92,4 1,6 154,6 3,1 45,3 1,0

18 Cigarette C2 2 1 598,3 12,3 6,103 0,024 92,0 2,9 153,7 7,0 45,3 1,2

18 Cigarette C2 3 1 595,0 11,6 6,113 0,017 91,0 2,8 153,7 6,3 45,7 1,1

18 Cigarette C3 1 1 1024,4 17,5 7,499 0,018 96,5 3,3 137,3 5,2 35,1 1,2

18 Cigarette C3 2 1 1032,2 23,9 7,504 0,025 94,4 3,8 135,5 6,5 35,8 1,3

18 Cigarette C3 3 1 1022,4 16,2 7,493 0,024 94,0 3,3 134,6 5,8 35,7 1,6

18 Cigarette C4 1 1 813,0 13,9 7,851 0,017 75,6 1,7 96,9 2,8 29,2 1,8

18 Cigarette C4 2 1 812,9 19,3 7,854 0,021 75,9 2,9 96,6 4,1 29,2 1,7

18 Cigarette C4 3 1 815,1 15,6 7,850 0,024 75,2 3,8 94,4 4,5 27,5 1,6

18 Cigarette C5 1 1 804,0 12,6 7,882 0,020 72,9 2,1 120,8 4,7 53,5 1,2

18 Cigarette C5 2 1 794,1 9,6 7,880 0,021 70,9 2,3 116,2 3,9 52,6 1,9

18 Cigarette C5 3 1 803,4 11,7 7,872 0,024 71,5 1,0 118,4 2,7 53,0 1,1




Laboratory 19


ment



19 Filter F1 1 1 578,0 8,0 6,720 0,010 442,2 11,8

19 Filter F1 2 1 578,0 12,0 6,720 0,010 447,6 12,2

19 Filter F1 3 1 579,0 12,0 6,720 0,010 447,0 12,8

19 Filter F2 1 1 415,0 4,0 5,330 0,010 507,5 15,0

19 Filter F2 2 1 415,0 4,0 5,330 0,020 510,3 13,5

19 Filter F2 3 1 412,0 2,0 5,330 0,020 502,3 6,1

19 Filter F3 1 1 944,0 6,0 7,800 0,020 300,7 7,8

19 Filter F3 2 1 938,0 11,0 7,810 0,020 301,1 9,7

19 Filter F3 3 1 939,0 9,0 7,790 0,020 302,3 7,8

19 Filter F4 1 1 965,0 9,0 7,810 0,010 511,2 10,6

19 Filter F4 2 1 970,0 11,0 7,810 0,020 517,9 11,9

19 Filter F4 3 1 967,0 12,0 7,810 0,020 508,8 12,7

19 Filter F5 1 1 979,0 8,0 7,810 0,040 742,9 11,9

19 Filter F5 2 1 982,0 5,0 7,800 0,010 753,0 8,5

19 Filter F5 3 1 980,0 9,0 7,810 0,030 750,1 12,1

19 Cigarette C1 1 1 509,0 10,0 5,400 0,020 91,0 5,0 269,0 17,0 88,0 0,8

19 Cigarette C1 2 1 500,0 16,0 5,400 0,020 87,0 4,0 287,0 19,0 85,2 1,3

19 Cigarette C1 3 1 498,0 14,0 5,400 0,020 88,0 4,0 280,0 21,0 87,8 1,0

19 Cigarette C2 1 1 593,0 11,0 6,090 0,020 93,0 3,0 156,0 6,0 45,4 1,2

19 Cigarette C2 2 1 596,0 12,0 6,100 0,020 94,0 2,0 161,0 4,0 45,6 1,2

19 Cigarette C2 3 1 587,0 13,0 6,090 0,020 92,0 3,0 156,0 5,0 45,5 1,1

19 Cigarette C3 1 1 1014,0 22,0 7,470 0,010 96,0 2,0 142,0 5,0 36,6 1,8

19 Cigarette C3 2 1 997,0 24,0 7,470 0,010 92,0 3,0 133,0 7,0 35,7 1,8

19 Cigarette C3 3 1 1004,0 18,0 7,480 0,010 97,0 4,0 143,0 5,0 36,5 2,5

19 Cigarette C4 1 1 809,0 15,0 7,850 0,020 78,0 3,0 100,0 4,0 29,0 2,1

19 Cigarette C4 2 1 799,0 22,0 7,850 0,020 77,0 3,0 98,0 4,0 27,8 1,3

19 Cigarette C4 3 1 803,0 16,0 7,850 0,020 76,0 2,0 96,0 5,0 27,5 2,6

19 Cigarette C5 1 1 796,0 18,0 7,880 0,020 73,0 3,0 122,0 5,0 53,0 0,9

19 Cigarette C5 2 1 804,0 15,0 7,880 0,040 72,0 2,0 118,0 4,0 51,9 0,9

19 Cigarette C5 3 1 791,0 14,0 7,880 0,030 72,0 2,0 120,0 4,0 52,5 1,3




Laboratory 20


ment



20 Filter F1 1 1 570,6 6,2 6,712 0,004 463,4 19,0

20 Filter F1 2 1 571,1 5,0 6,717 0,011 462,5 18,9

20 Filter F1 3 1 578,4 8,4 6,703 0,008 467,9 11,7

20 Filter F2 1 1 410,5 4,5 5,317 0,015 521,1 15,7

20 Filter F2 2 1 411,6 4,0 5,325 0,014 511,8 11,0

20 Filter F2 3 1 411,9 3,7 5,312 0,014 524,1 8,6

20 Filter F3 1 1 929,5 9,0 7,796 0,016 297,8 9,7

20 Filter F3 2 1 936,0 8,2 7,804 0,019 297,2 7,1

20 Filter F3 3 1 940,6 10,9 7,808 0,016 299,8 7,3

20 Filter F4 1 1 963,8 10,8 7,807 0,019 516,6 13,1

20 Filter F4 2 1 962,7 6,1 7,809 0,014 507,3 7,9

20 Filter F4 3 1 962,3 6,4 7,804 0,013 511,9 9,3

20 Filter F5 1 1 974,3 5,7 7,799 0,010 751,8 8,6

20 Filter F5 2 1 969,6 5,5 7,794 0,011 739,6 15,3

20 Filter F5 3 1 976,0 8,6 7,812 0,020 752,4 15,4

20 Cigarette C1 1 1 501,1 8,5 5,393 0,020 85,5 4,1 284,4 14,2 88,8 0,9

20 Cigarette C1 2 1 502,7 9,9 5,388 0,021 87,2 3,0 282,5 11,5 88,5 0,9

20 Cigarette C1 3 1 506,9 14,0 5,407 0,016 87,0 4,2 282,8 13,1 88,3 1,0

20 Cigarette C2 1 1 597,8 15,0 6,103 0,017 90,8 2,4 154,7 4,8 45,8 1,6

20 Cigarette C2 2 1 598,4 8,1 6,121 0,025 90,8 3,4 155,6 7,6 45,6 1,1

20 Cigarette C2 3 1 601,3 14,6 6,111 0,027 92,2 3,7 157,3 8,0 45,9 1,0

20 Cigarette C3 1 1 1019,4 24,1 7,494 0,018 94,1 2,7 136,8 5,0 35,8 1,8

20 Cigarette C3 2 1 1034,5 28,2 7,487 0,013 93,2 3,3 135,0 6,6 35,0 1,2

20 Cigarette C3 3 1 1005,4 18,8 7,471 0,014 92,0 3,1 134,7 6,4 36,3 2,0

20 Cigarette C4 1 1 811,2 19,5 7,849 0,019 75,3 2,5 98,3 3,5 29,5 1,6

20 Cigarette C4 2 1 813,6 12,8 7,847 0,013 74,4 3,0 98,3 4,2 30,7 2,2

20 Cigarette C4 3 1 817,5 22,7 7,853 0,017 76,1 2,1 99,1 5,2 29,2 3,1

20 Cigarette C5 1 1 801,8 12,3 7,867 0,026 69,0 2,1 116,1 4,8 52,8 1,9

20 Cigarette C5 2 1 794,4 21,6 7,856 0,021 69,3 2,2 115,7 4,2 52,1 1,8

20 Cigarette C5 3 1 807,4 16,9 7,861 0,026 70,2 2,4 116,8 4,6 52,2 0,8




Laboratory 21


ment



21 Filter F1 1 1 570,0 7,0 6,710 0,007 484,6 11,7

21 Filter F1 2 1 570,4 8,3 6,721 0,009 483,0 21,2

21 Filter F1 3 1 571,5 5,9 6,723 0,005 474,7 14,2

21 Filter F2 1 1 413,0 3,7 5,320 0,013 525,4 8,1

21 Filter F2 2 1 410,5 4,0 5,317 0,018 513,4 12,2

21 Filter F2 3 1 411,4 4,4 5,322 0,015 516,2 12,8

21 Filter F3 1 1 936,0 9,1 7,810 0,018 301,1 7,0

21 Filter F3 2 1 936,0 7,2 7,800 0,018 296,1 3,9

21 Filter F3 3 1 931,0 9,7 7,808 0,013 294,7 8,5

21 Filter F4 1 1 965,0 9,3 7,810 0,016 513,6 9,9

21 Filter F4 2 1 968,0 10,9 7,820 0,013 509,8 10,0

21 Filter F4 3 1 964,8 10,0 7,805 0,013 511,2 9,1

21 Filter F5 1 1 976,0 6,8 7,810 0,018 746,7 10,5

21 Filter F5 2 1 980,8 9,2 7,807 0,011 752,9 15,8

21 Filter F5 3 1 979,0 3,9 7,810 0,031 749,7 10,9

21 Cigarette C1 1 1 511,3 22,9 5,404 0,016 88,4 3,1 290,2 24,9 89,0 0,9

21 Cigarette C1 2 1 511,4 12,3 5,398 0,027 87,5 5,6 301,8 16,2 89,5 1,0

21 Cigarette C1 3 1 510,9 19,7 5,419 0,018 91,2 4,4 291,4 28,1 88,9 0,9

21 Cigarette C2 1 1 615,9 17,3 6,137 0,022 93,6 4,9 163,6 8,3 47,5 1,5

21 Cigarette C2 2 1 602,6 14,0 6,119 0,017 91,3 4,4 160,2 10,3 48,0 1,4

21 Cigarette C2 3 1 604,6 14,2 6,120 0,017 92,7 4,9 162,3 10,0 47,3 1,7

21 Cigarette C3 1 1 1030,7 22,2 7,494 0,021 94,7 3,0 140,0 5,1 37,3 1,0

21 Cigarette C3 2 1 1032,3 23,8 7,480 0,022 94,4 2,4 140,7 3,7 37,6 1,5

21 Cigarette C3 3 1 1035,0 15,7 7,497 0,017 96,9 4,8 141,7 7,1 36,5 2,2

21 Cigarette C4 1 1 809,1 15,9 7,845 0,020 74,9 2,8 96,9 3,5 29,2 2,5

21 Cigarette C4 2 1 816,1 17,5 7,859 0,016 76,1 2,4 99,8 3,9 30,7 2,4

21 Cigarette C4 3 1 829,7 22,0 7,864 0,017 78,6 2,5 101,6 4,3 29,2 3,3

21 Cigarette C5 1 1 814,7 23,5 7,868 0,021 71,7 2,0 125,8 7,4 55,0 2,1

21 Cigarette C5 2 1 808,1 10,6 7,858 0,028 71,4 1,4 123,2 3,6 54,8 1,1

21 Cigarette C5 3 1 814,3 15,7 7,872 0,022 73,3 1,6 124,5 6,4 53,7 2,6



Appendix B: “2015 PTM Proficiency Test–Raw Data – Laboratories encoded –

Data sheet 2”

Laboratory 1 and 2


ment

ID No. Mean SD Mean SD Mean SD

[mg] [mg] [mm] [mm] [mmWG] [mmWG]

1 Filter F1 1 1 575,0 11,0 6,713 0,013 447,1 13,1

1 Filter F1 1 2 576,0 11,0 6,712 0,015 447,1 12,9

1 Filter F1 1 3 576,0 11,0 6,708 0,015 448,6 12,9

1 Filter F2 1 1 413,0 2,0 5,315 0,022 506,0 12,3

1 Filter F2 1 2 412,0 2,0 5,321 0,017 504,4 11,8

1 Filter F2 1 3 412,0 2,0 5,311 0,019 506,0 12,3

1 Filter F3 1 1 942,0 12,0 7,807 0,016 301,4 9,2

1 Filter F3 1 2 934,0 6,0 7,798 0,014 299,8 5,5

1 Filter F3 1 3 933,0 7,0 7,801 0,019 300,6 6,7

1 Filter F4 1 1 963,0 8,0 7,803 0,016 505,3 8,7

1 Filter F4 1 2 963,0 12,0 7,805 0,018 507,2 12,9

1 Filter F4 1 3 962,0 12,0 7,807 0,015 506,3 12,5

1 Filter F5 1 1 976,0 5,0 7,807 0,018 741,4 6,6

1 Filter F5 1 2 972,0 5,0 7,810 0,023 748,9 10,9

1 Filter F5 1 3 975,0 7,0 7,803 0,043 753,8 21,1

2 Filter F1 1 1 576,6 7,8 6,713 0,008

2 Filter F1 1 2 576,6 7,9 6,713 0,007

2 Filter F1 1 3 576,1 8,1 6,713 0,009

2 Filter F2 1 1 411,6 2,8 5,328 0,012

2 Filter F2 1 2 411,7 3,5 5,318 0,015

2 Filter F2 1 3 412,0 3,8 5,321 0,012

2 Filter F3 1 1 939,6 5,8 7,809 0,013

2 Filter F3 1 2 939,2 5,3 7,804 0,012

2 Filter F3 1 3 938,9 5,7 7,804 0,014

2 Filter F4 1 1 961,2 8,8 7,813 0,019

2 Filter F4 1 2 960,6 9,0 7,812 0,017

2 Filter F4 1 3 960,4 9,0 7,813 0,019

2 Filter F5 1 1 971,7 6,8 7,797 0,014

2 Filter F5 1 2 971,2 6,9 7,795 0,014

2 Filter F5 1 3 970,8 6,8 7,797 0,019

DiameterIndividual Wt PD (fully

encapsulated)



Data sheet 2”

Laboratory 3 and 4


ment



3 Filter F1 1 1 597,5 11,0 6,720 0,014 438,4 10,4

3 Filter F1 1 2 567,7 8,0 6,719 0,023 438,6 13,2

3 Filter F1 1 3 578,5 12,0 6,722 0,011 436,1 12,4

3 Filter F2 1 1 409,6 4,0 5,327 0,014

3 Filter F2 1 2 411,6 4,0 5,321 0,011

3 Filter F2 1 3 410,5 3,0 5,319 0,016

3 Filter F3 1 1 930,7 8,0 7,804 0,016 298,1 4,7

3 Filter F3 1 2 937,7 10,0 7,797 0,018 301,4 8,4

3 Filter F3 1 3 927,3 9,0 7,807 0,013 294,3 6,9

3 Filter F4 1 1 959,7 7,0 7,813 0,013 504,0 9,5

3 Filter F4 1 2 967,1 10,0 7,806 0,013 509,6 10,0

3 Filter F4 1 3 965,3 9,0 7,812 0,012 506,0 8,4

3 Filter F5 1 1 974,0 8,0 7,800 0,017 732,1 11,1

3 Filter F5 1 2 974,3 6,0 7,801 0,015 731,5 14,8

3 Filter F5 1 3 968,7 7,0 7,803 0,017 722,0 11,2

4 Filter F1 1 1 584,4 6,1 6,721 0,010 433,5 8,3

4 Filter F1 1 2 584,2 6,1 6,719 0,009 437,9 8,2

4 Filter F1 1 3 583,7 6,9 6,720 0,017 440,1 6,9

4 Filter F2 1 1 413,0 3,2 5,325 0,011 503,1 9,5

4 Filter F2 1 2 412,9 3,2 5,324 0,010 506,6 9,5

4 Filter F2 1 3 412,8 3,2 5,327 0,009 503,2 8,8

4 Filter F3 1 1 939,7 6,0 7,813 0,020 293,3 5,4

4 Filter F3 1 2 939,0 5,9 7,812 0,018 294,0 5,3

4 Filter F3 1 3 939,2 5,8 7,812 0,020 294,2 5,3

4 Filter F4 1 1 969,3 9,4 7,821 0,011 503,8 10,3

4 Filter F4 1 2 968,9 9,3 7,821 0,012 503,0 10,0

4 Filter F4 1 3 968,9 9,2 7,819 0,010 504,2 10,0

4 Filter F5 1 1 982,9 5,0 7,823 0,017 742,8 11,8

4 Filter F5 1 2 981,9 5,0 7,824 0,022 740,7 11,6

4 Filter F5 1 3 982,7 5,0 7,825 0,027 742,1 11,0


encapsulated)



Data sheet 2”

Laboratory 5 and 6


ment



5 Filter F1 1 1 571,8 8,5 6,720 0,007 459,8 18,3

5 Filter F1 1 2 572,9 7,8 6,720 0,007 456,4 15,7

5 Filter F1 1 3 574,7 11,2 6,720 0,009 453,5 8,9

5 Filter F2 1 1 411,8 3,5 5,320 0,011 511,5 10,1

5 Filter F2 1 2 409,8 3,9 5,320 0,017 520,9 12,9

5 Filter F2 1 3 410,6 4,1 5,330 0,017 523,7 11,6

5 Filter F3 1 1 941,7 5,9 7,800 0,018 299,4 5,2

5 Filter F3 1 2 940,4 8,7 7,810 0,019 296,5 5,8

5 Filter F3 1 3 935,9 6,2 7,800 0,022 304,2 2,9

5 Filter F4 1 1 961,4 3,8 7,820 0,012 506,0 13,0

5 Filter F4 1 2 960,5 7,2 7,820 0,017 511,5 10,1

5 Filter F4 1 3 962,0 7,1 7,820 0,012 512,3 6,1

5 Filter F5 1 1 974,7 5,0 7,810 0,026 750,4 22,3

5 Filter F5 1 2 978,1 7,9 7,820 0,034 753,6 18,7

5 Filter F5 1 3 978,0 8,0 7,810 0,020 747,5 10,6

6 Filter F1 1 1 429,9 6,3

6 Filter F1 1 2 436,1 9,8

6 Filter F1 1 3 434,6 7,9

6 Filter F2 1 1 499,3 9,8

6 Filter F2 1 2 506,9 9,8

6 Filter F2 1 3 504,9 9,6

6 Filter F3 1 1 300,0 5,2

6 Filter F3 1 2 297,5 7,6

6 Filter F3 1 3 295,2 6,1

6 Filter F4 1 1 502,7 9,0

6 Filter F4 1 2 502,6 7,6

6 Filter F4 1 3 498,8 8,0

6 Filter F5 1 1 737,1 9,2

6 Filter F5 1 2 736,0 9,4

6 Filter F5 1 3 732,3 8,4


encapsulated)



Data sheet 2”

Laboratory 7 and 8


ment



7 Filter F1 1 1 579,1 6,3 6,714 0,005 396,4 13,7

7 Filter F1 1 2 578,5 6,2 6,711 0,004 397,1 13,8

7 Filter F1 1 3 579,0 6,2 6,712 0,004 393,8 12,6

7 Filter F2 1 1 413,2 3,9 5,328 0,010 473,9 10,5

7 Filter F2 1 2 412,8 3,9 5,325 0,009 478,6 8,9

7 Filter F2 1 3 412,8 3,9 5,328 0,011 472,1 13,0

7 Filter F3 1 1 932,7 12,1 7,798 0,018 285,0 5,1

7 Filter F3 1 2 932,7 12,2 7,802 0,015 284,7 5,6

7 Filter F3 1 3 933,3 12,0 7,796 0,017 282,9 5,4

7 Filter F4 1 1 967,0 8,3 7,813 0,012 464,6 6,5

7 Filter F4 1 2 966,1 8,3 7,811 0,016 464,1 9,1

7 Filter F4 1 3 966,9 8,3 7,806 0,011 462,6 6,7

7 Filter F5 1 1 978,4 5,0 7,805 0,018 646,7 25,5

7 Filter F5 1 2 977,5 5,2 7,823 0,022 628,0 28,9

7 Filter F5 1 3 978,3 5,4 7,814 0,038 626,6 26,8

8 Filter F1 1 1 577,0 5,9 6,708 0,008 445,4 9,9

8 Filter F1 1 2 578,3 5,6 6,709 0,010 450,3 9,6

8 Filter F1 1 3 578,4 5,9 6,713 0,008 446,4 10,0

8 Filter F2 1 1 409,3 3,8 5,318 0,010 515,7 12,9

8 Filter F2 1 2 409,1 3,5 5,320 0,013 515,6 15,3

8 Filter F2 1 3 410,7 3,6 5,324 0,011 516,1 14,4

8 Filter F3 1 1 936,9 7,2 7,791 0,018 301,5 6,0

8 Filter F3 1 2 937,4 7,5 7,796 0,017 300,2 5,5

8 Filter F3 1 3 940,6 7,6 7,792 0,023 301,9 5,4

8 Filter F4 1 1 965,6 8,3 7,805 0,007 509,4 7,6

8 Filter F4 1 2 965,9 8,1 7,813 0,011 508,4 7,8

8 Filter F4 1 3 965,9 8,2 7,809 0,011 508,3 7,5

8 Filter F5 1 1 981,7 4,2 7,799 0,031 754,3 12,0

8 Filter F5 1 2 984,3 4,4 7,800 0,018 752,9 12,4

8 Filter F5 1 3 985,0 4,2 7,811 0,034 749,7 12,6


encapsulated)



Data sheet 2”

Laboratory 9 and 10


ment



9 Filter F1 1 1 576,5 8,0 6,717 0,009

9 Filter F1 1 2 575,7 8,0 6,718 0,008

9 Filter F1 1 3 577,8 7,0 6,716 0,010

9 Filter F2 1 1 416,7 4,0 5,322 0,012

9 Filter F2 1 2 416,1 4,0 5,319 0,008

9 Filter F2 1 3 415,9 4,0 5,319 0,011

9 Filter F3 1 1 943,2 16,0 7,805 0,016

9 Filter F3 1 2 940,4 16,0 7,806 0,017

9 Filter F3 1 3 941,6 16,0 7,806 0,015

9 Filter F4 1 1 966,7 9,0 7,818 0,016

9 Filter F4 1 2 968,3 9,0 7,817 0,017

9 Filter F4 1 3 967,0 9,0 7,814 0,011

9 Filter F5 1 1

9 Filter F5 1 2 986,4 8,0 7,804 0,011

9 Filter F5 1 3 988,1 8,0 7,833

10 Filter F1 1 1 574,4 5,1 6,718 0,008 460,4 10,8

10 Filter F1 1 2 574,8 5,2 6,714 0,008 461,4 10,5

10 Filter F1 1 3 574,7 5,3 6,712 0,010 461,7 10,7


encapsulated)



Data sheet 2”

Laboratory 11 and 12


ment



11 Filter F1 1 1

12 Filter F1 1 1 574,0 11,0 6,713 0,007 486,0 14,0

12 Filter F1 1 2 574,0 11,0 6,710 0,013 484,0 14,0

12 Filter F1 1 3 574,0 11,0 6,707 0,013 486,0 14,0

12 Filter F2 1 1 410,0 4,0 5,342 0,021 512,0 15,0

12 Filter F2 1 2 410,0 4,0 5,326 0,011 513,0 15,0

12 Filter F2 1 3 410,0 4,0 5,325 0,027 515,0 16,0

12 Filter F3 1 1 945,0 12,0 7,810 0,010 304,0 7,0

12 Filter F3 1 2 945,0 12,0 7,810 0,010 305,0 7,0

12 Filter F3 1 3 945,0 12,0 7,811 0,010 305,0 7,0

12 Filter F4 1 1 970,0 10,0 7,814 0,015 520,0 12,0

12 Filter F4 1 2 970,0 10,0 7,815 0,014 521,0 12,0

12 Filter F4 1 3 970,0 10,0 7,814 0,018 523,0 12,0

12 Filter F5 1 1 977,0 9,0 7,805 0,013 752,0 15,0

12 Filter F5 1 2 977,0 9,0 7,806 0,013 756,0 15,0

12 Filter F5 1 3 977,0 9,0 7,807 0,016 758,0 15,0


encapsulated)



Data sheet 2”



ment



13 Filter F1 1 1 577,3 12,0 6,725 0,011 441,2 13,6

13 Filter F1 1 2 570,3 12,0 6,724 0,013 447,1 16,1

13 Filter F1 1 3 574,3 12,0 6,724 0,012 448,2 16,5

13 Filter F2 1 1 410,8 3,0 5,328 0,011 518,6 9,0

13 Filter F2 1 2 410,4 3,0 5,329 0,013 516,9 9,0

13 Filter F2 1 3 411,2 3,0 5,326 0,013 516,8 8,0

13 Filter F3 1 1 933,8 13,0 7,809 0,010 301,0 12,0

13 Filter F3 1 2 938,3 13,0 7,810 302,1 11,6

13 Filter F3 1 3 938,8 13,0 7,811 0,010 302,2 11,3

13 Filter F4 1 1 952,3 10,0 7,806 0,014 510,0 12,3

13 Filter F4 1 2 956,1 10,0 7,804 0,018 512,1 12,3

13 Filter F4 1 3 956,7 11,0 7,807 0,019 511,0 12,6

13 Filter F5 1 1 969,0 7,0 7,802 0,012 745,7 13,1

13 Filter F5 1 2 976,0 6,0 7,809 0,022 748,6 13,4

13 Filter F5 1 3 969,3 7,0 7,816 0,024 750,2 13,4

14 Filter F1 1 1 583,9 8,8 6,715 0,007 458,3 15,4

14 Filter F1 1 2 582,7 8,5 6,715 0,006 458,5 15,7

14 Filter F1 1 3 583,9 8,5 6,716 0,007 458,5 15,7

14 Filter F2 1 1 411,6 2,5 5,327 0,011 520,1 6,6

14 Filter F2 1 2 412,5 2,5 5,328 0,017 520,3 7,0

14 Filter F2 1 3 413,1 2,8 5,338 0,020 520,8 7,2

14 Filter F3 1 1 939,0 11,5 7,799 0,018 301,9 5,9

14 Filter F3 1 2 938,3 11,5 7,802 0,022 302,8 5,9

14 Filter F3 1 3 940,0 11,5 7,802 0,013 302,7 6,3

14 Filter F4 1 1 955,0 12,0 7,809 0,014 504,9 17,1

14 Filter F4 1 2 955,1 12,1 7,813 0,018 504,3 17,4

14 Filter F4 1 3 956,0 12,1 7,810 0,021 505,1 16,9

14 Filter F5 1 1 975,2 6,8 7,805 0,020 738,8 13,6

14 Filter F5 1 2 975,0 7,3 7,817 0,024 738,9 13,9

14 Filter F5 1 3 976,3 7,4 7,808 0,023 736,2 12,3


encapsulated)



Data sheet 2”



ment



15 Filter F1 1 1 588,0 8,0 6,717 0,006 445,0 16,0

15 Filter F1 1 2 587,0 8,0 6,714 0,006 447,0 15,0

15 Filter F1 1 3 587,0 7,0 6,714 0,007 449,0 14,0

15 Filter F2 1 1

15 Filter F2 1 2

15 Filter F2 1 3

15 Filter F3 1 1 938,0 10,0 7,811 0,018 296,0 8,0

15 Filter F3 1 2 938,0 11,0 7,808 0,019 296,0 8,0

15 Filter F3 1 3 935,0 10,0 7,805 0,019 296,0 7,0

15 Filter F4 1 1 973,0 9,0 7,810 0,020 510,0 11,0

15 Filter F4 1 2 971,0 9,0 7,809 0,017 512,0 11,0

15 Filter F4 1 3 970,0 9,0 7,807 0,017 512,0 11,0

15 Filter F5 1 1 983,0 7,0 7,811 0,026 743,0 14,0

15 Filter F5 1 2 981,0 7,0 7,812 0,033 746,0 14,0

15 Filter F5 1 3 979,0 6,0 7,816 0,043 741,0 13,0

16 Filter F1 1 1 574,4 8,5 6,715 0,004 431,3 10,9

16 Filter F1 1 2 574,9 8,6 6,719 0,008 433,2 10,8

16 Filter F1 1 3 573,3 8,2 6,711 0,011 436,7 10,2

16 Filter F2 1 1 410,2 3,7 5,325 0,016 506,2 9,8

16 Filter F2 1 2 409,2 3,6 5,322 0,015 509,1 10,3

16 Filter F2 1 3 409,7 3,8 5,324 0,017 507,2 10,0

16 Filter F3 1 1 941,9 12,1 7,805 0,018 302,2 7,3

16 Filter F3 1 2 941,9 11,9 7,802 0,021 303,3 7,3

16 Filter F3 1 3 942,0 12,4 7,803 0,021 303,4 7,5

16 Filter F4 1 1 959,7 5,4 7,803 0,012 508,0 9,9

16 Filter F4 1 2 959,7 5,1 7,809 0,014 508,5 9,4

16 Filter F4 1 3 959,7 5,0 7,806 0,011 509,0 9,5

16 Filter F5 1 1 971,8 8,7 7,817 0,030 734,9 13,5

16 Filter F5 1 2 973,3 8,5 7,819 0,032 736,5 12,3

16 Filter F5 1 3 973,0 8,5 7,820 0,033 732,8 14,4


encapsulated)



Data sheet 2”



ment



17 Filter F1 1 1 579,2 10,7 6,714 0,009 457,4 16,1

17 Filter F1 1 2 576,3 8,4 6,713 0,008 444,8 15,7

17 Filter F1 1 3 577,5 10,2 6,717 0,007 446,3 17,3

17 Filter F2 1 1 411,4 3,2 5,333 0,010 524,4 9,2

17 Filter F2 1 2 411,9 2,3 5,330 0,012 516,2 8,3

17 Filter F2 1 3 412,0 2,7 5,329 0,011 513,9 8,0

17 Filter F3 1 1 940,7 7,4 7,809 0,015 306,4 6,3

17 Filter F3 1 2 940,8 6,8 7,811 0,012 300,5 5,6

17 Filter F3 1 3 940,6 7,2 7,810 0,012 300,5 6,2

17 Filter F4 1 1 963,2 4,1 7,818 0,009 520,3 6,6

17 Filter F4 1 2 963,7 4,1 7,812 0,007 510,3 4,5

17 Filter F4 1 3 963,4 3,9 7,814 0,011 508,9 6,3

17 Filter F5 1 1 973,5 8,1 7,804 0,014 759,7 13,4

17 Filter F5 1 2 973,3 7,6 7,816 0,035 743,7 12,7

17 Filter F5 1 3 973,4 8,0 7,815 0,033 743,0 12,9

18 Filter F1 1 1 577,2 7,3 6,725 0,007

18 Filter F1 1 2 577,0 6,3 6,720 0,011

18 Filter F1 1 3 576,4 6,7 6,721 0,014

18 Filter F2 1 1

18 Filter F2 1 2

18 Filter F2 1 3

18 Filter F3 1 1 946,0 8,8 7,809 0,014

18 Filter F3 1 2 945,4 8,7 7,803 0,013

18 Filter F3 1 3 939,9 5,8 7,799 0,015

18 Filter F4 1 1 956,6 8,5 7,819 0,009

18 Filter F4 1 2 958,5 8,9 7,817 0,016

18 Filter F4 1 3 962,3 5,7 7,818 0,018

18 Filter F5 1 1 975,9 7,1 7,807 0,006

18 Filter F5 1 2 974,3 6,2 7,814 0,011

18 Filter F5 1 3 977,6 6,5 7,808 0,012


encapsulated)



Data sheet 2”



ment



19 Filter F1 1 1 578,0 8,0 6,720 0,010 442,2 11,8

19 Filter F1 1 2 577,0 9,0 6,710 0,020 442,4 13,0

19 Filter F1 1 3 578,0 10,0 6,720 0,010 446,3 15,7

19 Filter F2 1 1 415,0 4,0 5,330 0,010 507,5 15,0

19 Filter F2 1 2 412,0 3,0 5,330 0,020 504,9 11,7

19 Filter F2 1 3 414,0 4,0 5,330 0,010 508,2 14,9

19 Filter F3 1 1 944,0 6,0 7,800 0,020 300,7 7,8

19 Filter F3 1 2 944,0 6,0 7,800 0,020 303,1 7,3

19 Filter F3 1 3 941,0 7,0 7,810 0,020 299,2 9,8

19 Filter F4 1 1 965,0 9,0 7,810 0,010 511,2 10,6

19 Filter F4 1 2 966,0 11,0 7,820 0,010 516,2 11,6

19 Filter F4 1 3 964,0 11,0 7,820 0,010 511,4 13,6

19 Filter F5 1 1 979,0 8,0 7,810 0,040 742,9 11,9

19 Filter F5 1 2 978,0 8,0 7,820 0,040 745,6 14,2

19 Filter F5 1 3 978,0 8,0 7,820 0,050 741,8 13,3

20 Filter F1 1 1 570,6 6,2 6,712 0,004 463,4 19,0

20 Filter F1 1 2 570,4 6,0 6,711 0,003 459,3 19,0

20 Filter F1 1 3 571,9 6,0 6,710 0,005 469,8 14,5

20 Filter F2 1 1 410,5 4,5 5,317 0,015 521,1 15,7

20 Filter F2 1 2 410,8 4,3 5,318 0,015 515,7 15,4

20 Filter F2 1 3 411,8 4,5 5,317 0,014 522,1 15,7

20 Filter F3 1 1 929,5 9,0 7,796 0,016 297,8 9,7

20 Filter F3 1 2 930,6 8,7 7,800 0,017 294,2 9,8

20 Filter F3 1 3 932,0 8,5 7,799 0,019 295,9 9,7

20 Filter F4 1 1 963,8 10,8 7,807 0,019 516,6 13,1

20 Filter F4 1 2 964,5 10,9 7,809 0,019 511,1 12,7

20 Filter F4 1 3 966,3 11,1 7,809 0,019 515,2 12,6

20 Filter F5 1 1 974,3 5,7 7,799 0,010 751,8 8,6

20 Filter F5 1 2 973,5 5,6 7,820 0,030 745,6 9,7

20 Filter F5 1 3 975,6 5,7 7,823 0,034 752,5 10,2


encapsulated)



Data sheet 2”

Laboratory 21


ment



21 Filter F1 1 1 570,0 7,0 6,710 0,007 484,6 11,7

21 Filter F1 1 2 569,4 6,3 6,708 0,006 488,7 11,8

21 Filter F1 1 3 570,7 6,8 6,707 0,008 494,6 11,5

21 Filter F2 1 1 413,0 3,7 5,320 0,013 525,4 8,1

21 Filter F2 1 2 412,6 3,3 5,323 0,017 521,0 8,3

21 Filter F2 1 3 412,2 3,9 5,324 0,017 522,1 8,2

21 Filter F3 1 1 936,0 9,1 7,810 0,018 301,1 7,0

21 Filter F3 1 2 935,4 8,6 7,806 0,013 299,0 7,0

21 Filter F3 1 3 934,5 9,5 7,808 0,015 298,6 7,0

21 Filter F4 1 1 964,7 9,3 7,810 0,016 513,6 9,9

21 Filter F4 1 2 965,0 9,5 7,813 0,015 511,5 9,8

21 Filter F4 1 3 964,8 8,9 7,818 0,011 509,9 10,1

21 Filter F5 1 1 975,5 6,8 7,810 0,018 746,7 10,5

21 Filter F5 1 2 976,0 7,1 7,799 0,007 742,9 10,2

21 Filter F5 1 3 974,0 7,4 7,808 0,019 742,2 10,0


encapsulated)


Appendix C: “2015 PTM Proficiency Test – Summary of data sets and outliers”


Appendix D: “2015 PTM Proficiency Test – Summary of laboratory means and standard deviations - Cigarettes”

Outliers are excluded

Summary statistics per laboratory for cigarette C1 for individual weight (mg), diameter (mm), open and closed pressure drop (mmWG) and

filter ventilation (%).

product ID

Laboratory Mean Within Days SD Mean Within Days SD Mean Within Days SD Mean Within Days SD Mean Within Days SD

1 499.33 15.4596 5.41 0.0233 88.77 4.9669 281.80 18.4485 86.96 0.9034

2 502.40 14.6513 5.41 0.0220 87.87 4.2701 286.60 16.6013 88.93 1.2111

3 503.23 14.5488 5.41 0.0258 89.70 5.3697 278.37 20.1728 87.18 1.3087

4 507.93 13.0124 5.40 0.0156 86.83 4.0357 279.10 17.2392 88.67 1.1387

5 498.09 12.9849 5.40 0.0237 89.00 4.3535

6 90.43 3.7947 86.47 0.9885

7 500.23 15.8851 5.40 0.0219 87.63 5.0221 287.77 24.9902 88.71 0.9989

8 509.47 16.0704 5.40 0.0310 283.07 19.1595 90.09 1.7284

9 505.53 13.6991 5.40 0.0229 86.57 4.4797 278.13 16.1852 89.73 1.2757

10 495.20 12.1261 5.40 0.0225 88.37 4.7732 258.33 10.0659 86.93 1.2780

11 493.83 14.7916 84.73 4.2375 264.37 20.5353 91.43 1.4722

12 500.67 14.3875 5.41 0.0240 91.33 4.6904 272.67 17.5309 88.83 1.3760

14 504.37 13.7889 5.40 0.0247 84.87 4.8201 277.50 14.5131 88.62 1.3651

15 506.17 14.2368 5.41 0.0162 87.67 3.6336 275.53 20.8395 88.30 1.6296

16 501.97 16.0463 5.42 0.0178 86.17 3.9745 273.97 17.6595 88.27 1.4012

17 506.53 17.1872 5.42 0.0209 87.47 4.0747 283.17 23.7002 88.00 1.5674

18 504.23 11.8441 5.40 0.0163 88.83 3.7864 286.07 11.4601 89.63 0.9617

19 502.33 13.5647 5.40 0.0200 88.67 4.3589 278.67 19.0700 87.00 1.0536

20 503.57 11.0493 5.40 0.0191 86.57 3.8057 283.23 12.9808 88.51 0.9376

21 511.20 18.8307 5.41 0.0209 89.03 4.4844 294.47 23.6083 89.14 0.9445

Individual Wgt Diameter Pressure Drop Open Pressure Drop Close

C1

Filter ventilation


Appendix D: “2015 PTM Proficiency Test – Summary of laboratory means and standard deviations - Cigarettes” – continued




product ID


1 600.33 15.4488 6.11 0.0198 91.83 3.4627 157.37 8.1115 45.70 1.0881

2 597.23 11.6991 6.12 0.0175 90.07 3.5449 153.47 7.0128 46.57 1.1832

3 599.90 12.6754 6.11 0.0218 92.33 4.3147 158.23 8.2747 46.52 1.5940

4 607.77 13.1023 6.11 0.0219 92.37 3.8807 159.53 8.9370 47.07 1.9511

5 598.82 13.3598 6.11 0.0201 94.03 3.5421 46.73 1.4213

6 91.27 3.8235 45.76 1.0480

7 603.43 13.9615 6.11 0.0190 92.43 2.6027 161.27 7.3486 47.58 1.7281

8 599.10 11.2207 6.12 0.0207 90.17 3.0670 156.60 7.3707 48.02 1.5027

9 601.83 12.3423 6.11 0.0224 91.17 4.4890 158.37 8.4330 47.20 1.3584

10 593.33 11.8464 6.12 0.0215 89.77 2.9939 147.90 5.5585 45.33 1.3540

11 592.23 12.6462 89.90 3.6833 158.83 6.8678 47.82 1.8099

12 596.00 11.3431 6.11 0.0195 92.00 3.0000 154.33 6.6833 46.10 1.1210

14 600.10 10.7198 6.12 0.0197 89.67 3.6647 154.47 6.8995 45.90 1.0403

15 596.20 11.2526 6.10 0.0189 90.33 3.8807 154.07 7.8844 45.93 1.5137

16 597.03 12.4591 6.11 0.0145 91.93 4.7589 156.00 8.0484 46.00 1.5199

17 593.83 10.9511 6.11 0.0150 88.83 3.0800 149.97 6.5544 45.00 1.4888

18 593.80 11.5195 6.11 0.0221 91.80 2.4927 154.00 5.7172 45.45 1.0992

19 592.00 12.0277 6.09 0.0200 93.00 2.7080 157.67 5.0662 45.50 1.1676

20 599.17 12.9585 6.11 0.0234 91.27 3.2151 155.87 6.9474 45.75 1.2309

21 607.70 15.2417 6.13 0.0188 92.53 4.7392 162.03 9.5739 47.59 1.5524

Filter ventilation

C2

Individual Wgt Diameter Pressure Drop Open Pressure Drop Close






product ID


1 1023.00 20.7686 7.49 0.0231 93.87 3.3071 135.07 5.5657 35.09 1.6018

2 1022.53 27.4623 7.50 0.0209 94.63 2.8101 136.87 5.3827 36.33 1.6145

3 1021.80 23.1012 7.50 0.0194 92.83 3.3252 134.37 5.8734 36.15 1.6924

4 1031.50 21.2568 7.49 0.0211 93.87 3.1670 134.93 5.3560 35.53 1.6391

5 1024.70 25.4069 7.50 0.0228 95.07 3.0557 35.80 1.6783

6 93.60 2.8200 35.45 1.4574

7 1024.17 23.3311 7.48 0.0241 94.93 3.7331 139.57 6.0633 37.12 1.4847

8 1027.40 19.4804 7.50 0.0248 96.47 3.5180 141.57 6.2535 37.12 1.3103

9 1033.00 22.6863 7.49 0.0225 93.17 2.6030 132.80 4.5103 36.12 1.5455

10 1008.40 22.1857 7.49 0.0217 91.30 4.0894 130.43 4.6051 35.10 2.3195

11 1002.27 18.0703 91.50 3.7969 126.50 6.3799 35.87 1.5692

12 1012.67 20.8087 7.51 0.0199 92.33 2.3805 130.00 7.8528 35.53 2.0017

14 1029.73 23.2449 7.49 0.0203 93.23 3.7758 136.63 6.3859 36.05 1.6959

15 1019.00 26.8538 7.49 0.0224 91.67 3.2177 131.93 5.8615 35.53 1.6875

16 1020.23 21.8301 7.49 0.0240 92.23 3.1591 133.17 4.5775 36.13 1.5155

17 1033.70 22.6930 7.51 0.0233 93.40 2.9811 135.53 5.6906 35.50 1.7748

18 1026.33 19.4905 7.50 0.0226 94.97 3.4780 135.80 5.8338 35.51 1.3655

19 1005.00 21.4787 7.47 0.0100 95.00 3.1091 139.33 5.7446 36.27 2.0599

20 1019.77 24.0103 7.48 0.0152 93.10 3.0436 135.50 6.0421 35.66 1.6760

21 1032.67 20.8628 7.49 0.0201 95.33 3.5496 140.80 5.4806 37.16 1.6309


C3






product ID


1 812.00 20.4858 7.85 0.0232 74.07 2.9011 95.67 5.2374 29.22 2.2325

2 810.00 18.5971 7.86 0.0153 74.73 3.6724 92.70 5.9958 28.40 1.6683

3 813.17 19.4422 7.86 0.0220 75.20 3.0408 96.10 4.4291 28.75 2.1774

4 821.57 14.8590 7.85 0.0162 74.77 2.9405 95.70 4.0604 28.70 2.0017

5 807.03 15.4305 7.85 0.0128 75.10 2.9473

6 75.70 2.4057 29.36 2.1616

7 819.10 14.2830 7.85 0.0142 77.07 2.7490 99.63 4.4901 29.95 1.6776

8 818.87 19.4378 7.86 0.0146 76.13 2.6394 95.80 5.6202 31.81 1.8496

9 821.40 20.4369 7.86 0.0172 74.70 3.0848 94.20 5.0809 30.64 1.8339

10 810.27 18.0850 7.85 0.0123 74.23 2.0944 94.40 3.3327 27.70 2.0083

11 798.13 14.2196 74.57 2.5736 95.97 3.7829 30.58 2.1139

12 809.00 21.0476 7.86 0.0168 75.33 2.7080 93.33 4.2426 27.23 2.0216

14 816.43 19.4338 7.85 0.0128 73.37 2.8125 95.00 3.8790 29.03 1.8066

15 813.90 18.5944 7.86 0.0187 74.67 3.2501 94.77 5.0468 28.03 2.0213

16 810.83 19.4249 7.86 0.0199 74.50 2.8577 94.77 4.5155 28.17 2.6115

17 807.87 17.8912 7.86 0.0130 74.77 2.8618 95.13 4.1513 27.90 1.7359

18 813.67 16.4315 7.85 0.0209 75.57 2.9263 95.97 3.8458 28.63 1.6825

19 803.67 17.9351 7.85 0.0200 77.00 2.7080 98.00 4.3589 28.10 2.0704

20 814.10 18.7917 7.85 0.0165 75.27 2.5599 98.57 4.3562 29.78 2.3762

21 818.30 18.6464 7.86 0.0177 76.53 2.5723 99.43 3.9137 29.69 2.7461

Pressure Drop Close Filter ventilation

C4

Individual Wgt Diameter Pressure Drop Open






product ID


1 802.67 17.7106 7.87 0.0320 71.43 2.4180 118.97 4.7149 52.12 1.6471

2 795.77 12.8355 7.87 0.0238 71.30 2.2472 116.33 4.3031 52.33 1.4166

3 801.70 14.7196 7.89 0.0316 70.67 2.1764 117.67 4.8847 52.69 1.6375

4 810.43 17.4176 7.88 0.0237 70.60 1.5384 117.27 3.8940 53.27 1.4166

5 800.53 21.2010 7.89 0.0304 70.77 2.3958

6 71.00 2.3787 52.32 1.4234

7 815.80 17.1532 7.89 0.0238 72.13 2.3582 106.00 4.7029 54.03 2.1442

8 806.17 14.0729 7.88 0.0242 71.93 2.0033 55.45 1.9565

9 809.93 18.1659 7.87 0.0292 70.27 2.1377 117.17 4.5480 54.20 1.7191

10 793.67 15.3852 7.87 0.0234 69.73 2.1886 114.20 3.3211 51.60 1.2910

11 786.37 14.2579 70.47 1.8708 109.93 4.4996 54.57 1.5015

12 796.67 19.0613 7.89 0.0253 71.33 2.3805 116.67 5.3541 52.57 1.4012

14 805.30 19.8564 7.87 0.0274 70.57 2.4792 118.47 5.1756 52.85 1.6523

15 7.88 0.0286 70.67 2.1299 117.60 5.4815 52.87 1.8626

16 792.23 15.3862 7.87 0.0225 69.90 3.1059 116.13 5.7764 53.27 1.5155

17 802.83 18.6480 7.88 0.0326 70.33 2.1479 115.83 4.6022 51.70 1.4900

18 800.50 11.3568 7.88 0.0218 71.77 1.9000 118.47 3.8713 53.06 1.4801

19 797.00 15.7586 7.88 0.0311 72.33 2.3805 120.00 4.3589 52.47 1.0504

20 801.20 17.3538 7.86 0.0244 69.50 2.2368 116.20 4.5402 52.36 1.5735

21 812.37 17.4270 7.87 0.0239 72.13 1.6852 124.50 6.0189 54.52 2.0243

Pressure Drop CloseIndividual Wgt Diameter Pressure Drop Open Filter ventilation

C5


Appendix E: “2015 PTM Proficiency Test – Summary of laboratory means and standard deviations – Filters – Evaluation 1”


Summary statistics per laboratory for filter F1 for individual weight (mg), diameter (mm) and fully encapsulated pressure drop (mmWG).

product ID

Laboratory Mean Within Days SD Mean Within Days SD Mean Within Days SD

1 577.33 10.0995 447.67 11.6605

2 580.23 8.5588 6.71 0.0083

3 581.23 10.4722 437.70 12.0576

4 582.50 9.0515 6.72 0.0091 437.10 11.3985

5 571.76 8.6133 6.72 0.0091 454.30 12.2563

6 427.67 8.7005

7 578.57 9.1183 6.72 0.0071 402.67 10.3867

8 577.57 8.4922 6.71 0.0080 446.87 11.0171

9 572.97 6.2183 6.72 0.0065

10 571.10 8.1447 6.71 0.0080 452.50 11.1466

12 572.67 8.0623 6.71 0.0072 486.00 16.0624

13 571.67 10.9848 6.72 0.0085 443.97 13.2238

14 580.67 8.1010 6.71 0.0070 453.27 13.1904

15 582.67 9.5219 6.72 0.0078 442.67 13.1276

16 577.60 10.4708 6.71 0.0058 434.70 14.1361

17 580.27 9.2574 6.71 0.0110 453.93 15.0768

18 580.37 5.9501

19 578.33 10.8321 6.72 0.0100 445.60 12.2629

20 573.37 6.6833 6.71 0.0082 464.60 16.8829

21 570.63 7.1344 6.72 0.0072 480.77 16.2067


F1


Appendix E: “2015 PTM Proficiency Test – Summary of laboratory means and standard deviations – Filters – Evaluation 1” -

continued



productID


1 411.33 3.5590 505.70 10.4226

2 410.43 2.9405 5.32 0.0107

3 410.57 3.6968 5.32 0.0138

4 411.93 3.2680 5.32 0.0115 504.30 9.9524

5 409.51 3.6285 5.33 0.0124 516.93 10.3734

6 502.73 11.2263

7 413.23 4.1384 5.33 0.0136

8 411.13 3.9703 5.32 0.0110 511.40 13.5751

9 414.00 3.6968 5.32 0.0095

10 411.73 3.9455 5.33 0.0125 524.80 13.3250

12 409.67 5.1962 514.00 15.4704

13 411.23 4.0825 5.33 0.0175 518.73 11.4946

14 410.87 2.9811 5.32 0.0173 519.07 10.6052

16 410.40 3.7014 5.32 0.0144 507.47 13.2475

17 411.30 2.9944 5.33 0.0103 516.70 9.1209

19 414.00 3.4641 5.33 0.0173 506.70 12.1665

20 411.33 4.0800 5.32 0.0143 519.00 12.1305

21 411.63 4.0435 5.32 0.0155 518.33 11.2293

F2



Appendix E: “2015 PTM Proficiency Test – Summary of laboratory means and standard deviations – Filters – Evaluation 1” –

continued



productID


1 941.00 9.8826 7.80 0.0173 302.43 8.2012

2 938.07 6.9179 7.81 0.0127

3 931.90 9.0370 7.80 0.0158 297.93 6.8376

4 940.70 6.7671 7.81 0.0182 294.77 5.5079

5 941.38 9.5010 7.80 0.0194 301.20 7.0025

6 299.03 6.4390

7 937.10 10.8672 7.80 0.0175

8 7.79 0.0164 299.73 8.5775

9 7.81 0.0163

10 936.00 9.0270 7.80 0.0197 309.93 5.8141

12 936.67 10.4722 7.81 0.0114 302.67 7.0000

13 936.33 9.6954 7.80 0.0125 303.67 8.0293

14 941.27 9.2698 7.80 0.0181 304.63 7.1258

15 939.67 9.3452 7.81 0.0149 299.33 7.0475

16 938.17 9.1864 7.81 0.0181 298.87 6.1722

17 938.43 10.2047 7.80 0.0154 301.90 8.3175

18 933.17 7.7900 7.81 0.0150

19 940.33 8.9069 7.80 0.0200 301.37 8.4984

20 935.37 9.4349 7.80 0.0171 298.27 8.1197

21 934.33 8.7319 7.81 0.0165 297.30 6.7444

F3




continued



productID


1 962.33 9.8150 7.81 0.0141 507.87 11.3446

2 963.47 9.9626 7.81 0.0139

3 964.03 8.7560 7.81 0.0127 506.53 9.3240

4 968.00 8.7521 7.82 0.0142 505.53 10.9278

5 963.42 5.6881 7.81 0.0148 508.83 9.0410

6 503.20 9.2572

7 963.53 8.3956 7.81 0.0121

8 967.80 8.7230 7.80 0.0129 512.10 9.6542

9 966.30 9.0000 7.82 0.0160

10 962.87 8.2012 7.81 0.0151 519.77 8.4408

12 965.67 9.3808 7.82 0.0164 515.67 10.4083

13 959.83 9.4868 7.81 0.0150 509.77 10.7361

14 960.57 11.0911 7.81 0.0156 510.57 13.2206

15 967.67 7.5277 7.81 0.0157 509.33 10.0333

16 961.70 6.9522 7.81 0.0130 505.17 10.1687

17 962.37 8.3022 7.82 0.0097 512.73 8.8531

18 963.47 6.9508 7.82 0.0110

19 967.33 10.7393 7.81 0.0173 512.63 11.7609

20 962.93 8.0583 7.81 0.0156 511.93 10.3362

21 965.93 10.0879 7.81 0.0141 511.53 9.6751

F4




continued



productID


1 977.67 7.8951 7.80 0.0244 751.70 14.8735

2 976.93 5.9983 7.80 0.0118

3 972.33 7.0475 7.80 0.0164 728.53 12.4859

4 981.50 5.4433 7.81 0.0204 743.67 10.3730

5 976.69 6.9114 7.81 0.0216 750.33 14.4783

6 734.00 7.0039

7 977.85 6.8792 7.80 0.0154

8 980.73 6.3267 7.80 0.0217 750.63 11.2333

9 982.10 7.9057 7.81 0.0190

10 973.57 8.5006 7.80 0.0153 751.83 16.4546

12 974.33 10.4083 7.81 0.0201 749.33 17.1367

13 971.00 7.4386 7.80 0.0149 745.53 15.1663

14 975.73 7.4478 7.80 0.0181 737.70 12.4992

15 979.33 6.4031 7.81 0.0183 739.33 11.9583

16 970.10 8.7365 7.81 0.0195 735.60 14.5239

17 974.93 7.3673 7.81 0.0137 749.67 12.3177

18 977.47 7.3625 7.80 0.0117

19 980.33 7.5277 748.67 10.9309

20 973.30 6.7503 7.80 0.0144 747.93 13.4810

21 978.60 6.9783 7.81 0.0216 749.77 12.6320


F5


Appendix F: “2015 PTM Proficiency Test – Summary of laboratory means and standard deviations – Filters – Evaluation 2”



productID


1 575.67 11.0000 447.60 12.9670

2 576.43 7.9343 6.71 0.0080

3 581.23 10.4722 437.70 12.0576

4 584.10 6.3778 6.72 0.0125 437.17 7.8260

5 573.17 9.2823 6.72 0.0077 456.57 14.8226

6 433.53 8.1088

7 578.87 6.2167 6.71 0.0044 395.77 13.3483

8 577.90 5.8017 6.71 0.0087 447.37 9.8348

9 576.67 7.6811

10 574.63 5.2006 6.71 0.0087 461.17 10.6674

12 574.00 11.0000 6.71 0.0114 485.33 14.0000

13 573.97 12.0000 6.72 0.0120 445.50 15.4534

14 583.50 8.6012 6.72 0.0067 458.43 15.6006

15 587.33 7.6811 6.72 0.0064 447.00 15.0222

16 574.20 8.4350 6.72 0.0082 433.73 10.6378

17 577.67 9.8165 6.71 0.0080 449.50 16.3808

18 576.87 6.7823 6.72 0.0112

19 577.67 9.0370 6.72 0.0141 443.63 13.5908

20 570.97 6.0674 6.71 0.0041 464.17 17.6281

21 570.03 6.7065 6.71 0.0070 489.30 11.6673


F1


Appendix F: “2015 PTM Proficiency Test – Summary of laboratory means and standard deviations – Filters – Evaluation 2” -

continued



productID


1 412.33 2.0000 5.32 0.0194 505.47 12.1356

2 411.77 3.3926 5.32 0.0131

3 410.57 3.6968 5.32 0.0138

4 412.90 3.2000 5.33 0.0100 504.30 9.2725

5 410.73 3.8133 5.32 0.0153 518.70 11.5899

6 503.70 9.7270

7 412.93 3.9000 5.33 0.0100

8 409.70 3.6355 5.32 0.0114 515.80 14.2345

9 416.23 4.0000 5.32 0.0103

12 410.00 4.0000 513.33 15.3406

13 410.80 3.0000 5.33 0.0124 517.43 8.6795

14 412.40 2.6038 5.33 0.0164 520.40 6.9378

16 409.70 3.7009 5.32 0.0160 507.50 10.0354

17 411.77 2.7580 5.33 0.0110 518.17 8.5153

19 413.67 3.6968 5.33 0.0141 506.87 13.9443

20 411.03 4.4343 5.32 0.0147 519.63 15.6006

21 412.60 3.6419 5.32 0.0158 522.83 8.2004


F2


Appendix F: “2015 PTM Proficiency Test – Summary of laboratory means and standard deviations – Filters – Evaluation 2” -

continued



productID


1 936.33 8.7369 7.80 0.0165 300.60 7.2979

2 939.23 5.6042 7.81 0.0130

3 931.90 9.0370 7.80 0.0158 297.93 6.8376

4 939.30 5.9006 7.81 0.0194 293.83 5.3335

5 939.31 7.0216 7.80 0.0197 300.03 4.7990

6 297.57 6.3903

7 932.90 12.0970 7.80 0.0167

8 938.30 7.4353 7.79 0.0195 301.20 5.6394

9 941.73 16.0000 7.81 0.0158

12 945.00 12.0000 7.81 0.0100 304.67 7.0000

13 7.81 0.0100

14 939.10 11.5000 7.80 0.0180 302.47 6.0363

15 937.00 10.3441 7.81 0.0187 296.00 7.6811

16 941.93 12.1351 7.80 0.0200 302.97 7.3673

17 940.70 7.1377 7.81 0.0131 302.47 6.0412

18 943.77 7.8810 7.80 0.0139

19 943.00 6.3509 7.80 0.0200 301.00 8.3657

20 930.70 8.7358 7.80 0.0174

21 935.30 9.0741 7.81 0.0155 299.57 7.0000

F3



Appendix F: “2015 PTM Proficiency Test – Summary of laboratory means and standard deviations – Filters – Evaluation 2”-

continued



productID


1 962.67 10.8321 7.81 0.0164 506.27 11.5232

2 960.73 8.9338 7.81 0.0184

3 964.03 8.7560 7.81 0.0127 506.53 9.3240

4 969.03 9.3004 7.82 0.0110 503.67 10.1010

5 961.31 6.2388 7.82 0.0139 509.93 10.1275

6 501.37 8.2170

7 966.67 8.3000 7.81 0.0132 outlier outlier

8 965.80 8.2004 7.81 0.0098 508.70 7.6344

9 967.33 9.0000 7.82 0.0146

12 970.00 10.0000 7.81 0.0158 521.33 12.0000

13 955.03 10.3441 7.81 0.0171 511.03 12.4008

14 955.37 12.0668 7.81 0.0179 outlier outlier

15 971.33 9.0000 7.81 0.0181 511.33 11.0000

16 959.70 5.1695 7.81 0.0124 508.50 9.6024

17 963.43 4.0344 7.81 0.0091 513.17 5.8737

18 959.13 7.8379 7.82 0.0147

19 965.00 10.3763 7.82 0.0100 512.93 11.9806

20 964.87 10.9340 7.81 0.0190 514.30 12.8018

21 964.83 9.2367 7.81 0.0142 511.67 9.9341

F4



Appendix F: “2015 PTM Proficiency Test – Summary of laboratory means and standard deviations – Filters – Evaluation 2”-

continued



productID


1 974.33 5.7446 7.81 0.0300 748.03 14.2312

2 971.23 6.8335 7.80 0.0158

3 972.33 7.0475 7.80 0.0164 728.53 12.4859

4 982.50 5.0000 7.82 0.0224 741.87 11.4717

5 976.92 7.1347 7.81 0.0273 750.50 17.8824

6 735.13 9.0438

7 978.07 5.2026 7.81 0.0274

8 983.67 4.2677 7.80 0.0285 752.30 12.3359

9 987.25 8.0000 7.82 0.0108

12 977.00 9.0000 7.81 0.0141 755.33 15.0000

13 971.43 6.6833 7.81 0.0200 748.17 13.3008

14 975.50 7.1715 7.81 0.0224 737.97 13.2848

15 981.00 6.6833 743.33 13.6748

16 972.70 8.5672 7.82 0.0317 734.73 13.4276

17 973.40 7.9030 7.81 0.0289 748.80 13.0033

18 975.93 6.5965 7.81 0.0100

19 978.33 8.0000 743.43 13.1527

20 974.47 5.6669 7.81 0.0268 749.97 9.5235

21 975.17 7.1042 7.81 0.0156 743.93 10.2354


F5


Appendix G: “2015 PTM Proficiency Test – Robust global mean and between laboratories standard deviation”

Robust mean values and standard deviations for all cigarettes and filters with respect to individual weight (mg), diameter (mm), open and

close pressure drop (mmWG) and fully encapsulated pressure drop (mmWG).

Cigarette Filter - Evaluation 1 Filter - Evaluation 2

Product ID Parameter

Robust Global

Mean (ISO-

Algorithm A)

Robust

Between Labs

Stdev (ISO-

Algorithm A) Product ID Parameter

Robust Global

Mean (ISO-

Algorithm A)

Robust

Between Labs

Stdev (ISO-

Algorithm A) Product ID Parameter

Robust Global

Mean (ISO-

Algorithm A)

Robust

Between Labs

Stdev (ISO-

Algorithm A)

C1 Diameter 5.40 0.0077 F1 Diameter 7.80 0.0055 F1 Diameter 7.81 0.0068

C1 Filter Ventilation 88.39 1.2490 F1 Pressure Drop PD encaps 744.02 8.4582 F1 Pressure_Drop 743.35 8.8874

C1 RTD (PD closed) 279.69 6.8449 F1 Weigth 976.59 3.8987 F1 Weigth 976.47 4.3907

C1 RTD (PD open) 87.73 2.0035 F2 Diameter 7.81 0.0048 F2 Diameter 7.81 0.0054

C1 Individual Weigth 503.08 4.5471 F2 Pressure Drop PD encaps 509.56 4.5181 F2 Pressure_Drop 508.87 5.2359

C2 Diameter 6.11 0.0063 F2 Weigth 964.18 2.7783 F2 Weigth 963.82 4.8017

C2 Filter Ventilation 46.37 1.0108 F3 Diameter 7.80 0.0048 F3 Diameter 7.80 0.0050

C2 RTD (PD closed) 156.32 3.4725 F3 Pressure Drop PD encaps 300.22 3.4810 F3 Pressure_Drop 299.50 3.7121

C2 RTD (PD open) 91.32 1.3961 F3 Weigth 937.89 2.9757 F3 Weigth 938.54 4.4027

C2 Individual Weigth 598.12 4.5713 F4 Diameter 5.32 0.0048 F4 Diameter 5.32 0.0054

C3 Diameter 7.49 0.0086 F4 Pressure Drop PD encaps 512.37 8.4753 F4 Pressure_Drop 512.40 8.5828

C3 Filter Ventilation 35.90 0.5879 F4 Weigth 411.34 1.2746 F4 Weigth 411.68 1.5559

C3 RTD (PD closed) 135.17 4.0604 F5 Diameter 6.72 0.0044 F5 Diameter 6.72 0.0048

C3 RTD (PD open) 93.60 1.5485 F5 Pressure Drop PD encaps 447.47 14.7314 F5 Pressure_Drop 448.99 15.1722

C3 Individual Weigth 1022.50 9.3966 F5 Weigth 576.92 4.7082 F5 Weigth 576.89 4.5227

C4 Diameter 7.85 0.0048

C4 Filter Ventilation 29.07 1.2306

C4 RTD (PD closed) 95.76 2.0106

C4 RTD (PD open) 75.13 0.9351

C4 Individual Weigth 812.88 6.1654

C5 Diameter 7.88 0.0095

C5 Filter Ventilation 53.04 1.0563

C5 RTD (PD closed) 117.14 2.3240

C5 RTD (PD open) 70.94 0.9365

C5 Individual Weigth 801.81 7.4825


Appendix H: “2015 PTM Proficiency Test – Individual z-scores Cigarettes”

data

sheet

laboratory

no

z-score

C1

z-score

C2

z-score

C3

z-score

C4

z-score

C5

1 1 -0.823 0.484 0.054 -0.143 0.115

1 2 -0.149 -0.194 0.004 -0.468 -0.807

1 3 0.034 0.389 -0.074 0.046 -0.014

1 4 1.068 2.110 0.958 1.408 1.153

1 5 -1.096 0.152 0.235 -0.950 -0.170

1 6 --- --- --- --- ---

1 7 -0.625 1.162 0.178 1.008 1.870

1 8 1.405 0.214 0.522 0.970 0.583

1 9 0.540 0.812 1.118 1.381 1.086

1 10 -1.732 -1.047 -1.500 -0.425 -1.088

1 11 -2.033 -1.288 -2.153 -2.393 -2.063

1 12 -0.530 -0.464 -1.046 -0.630 -0.687

1 14 0.284 0.433 0.770 0.576 0.467

1 15 0.679 -0.420 -0.372 0.165 -0.010

1 16 -0.244 -0.238 -0.241 -0.333 -1.279

1 17 0.760 -0.938 1.192 -0.814 0.137

1 18 0.254 -0.945 0.408 0.127 -0.175

1 19 -0.164 -1.339 -1.862 -1.495 -0.642

1 20 0.108 0.229 -0.290 0.197 -0.081

1 21 1.786 2.095 1.082 0.878 1.411

Cigarette - Individual weight

data

sheet

laboratory

no

z-score

C1

z-score

C2

z-score

C3

z-score

C4

z-score

C5

1 1 0.132 -0.322 -0.772 -0.538 -0.212

1 2 0.998 0.471 0.357 0.084 -0.669

1 3 0.262 0.048 1.097 1.744 1.617

1 4 -0.473 -0.692 -0.344 -0.331 0.246

1 5 -0.214 -0.851 0.474 -0.331 1.160

1 6 --- --- --- --- ---

1 7 -0.560 0.101 -1.045 -0.054 1.231

1 8 -0.922 1.291 0.739 0.586 0.136

1 9 -0.949 -0.956 -0.032 1.122 -0.528

1 10 -0.084 0.471 0.084 -0.953 -0.247

1 11 -0.646 0.894 -1.317 -3.028 -2.181

1 12 1.214 -0.322 1.603 1.260 1.125

1 14 -0.041 1.423 -0.149 -0.538 -0.247

1 15 0.998 -1.432 -0.071 0.983 0.316

1 16 1.820 -0.375 0.045 0.430 -0.810

1 17 2.079 0.154 1.875 0.845 0.316

1 18 -1.165 0.154 0.707 -0.676 0.246

1 19 -0.646 -2.965 -2.252 -1.022 0.457

1 20 -1.165 -0.058 -1.006 -1.091 -1.513

1 21 0.262 2.110 -0.266 0.223 -1.021

Cigarette -Diameter


Appendix H: “2015 PTM Proficiency Test – Individual z-scores Cigarettes” - continued

data

sheet

laboratory

no

z-score

C1

z-score

C2

z-score

C3

z-score

C4

z-score

C5

1 1 0.517 0.365 0.174 -1.139 0.523

1 2 0.067 -0.901 0.669 -0.426 0.381

1 3 0.983 0.723 -0.494 0.073 -0.296

1 4 -0.448 0.747 0.174 -0.390 -0.367

1 5 0.633 1.941 0.949 -0.034 -0.189

1 6 1.349 -0.041 0.001 0.608 0.060

1 7 -0.049 0.795 0.863 2.070 1.270

1 8 -1.679 -0.829 1.853 1.071 1.057

1 9 -0.581 -0.113 -0.278 -0.461 -0.723

1 10 0.317 -1.116 -1.484 -0.961 -1.292

1 11 -1.496 -1.020 -1.355 -0.604 -0.509

1 12 1.798 0.484 -0.817 0.216 0.416

1 14 -1.430 -1.187 -0.235 -1.887 -0.403

1 15 -0.032 -0.710 -1.247 -0.497 -0.296

1 16 -0.781 0.436 -0.881 -0.675 -1.114

1 17 -0.132 -1.784 -0.128 -0.390 -0.652

1 18 0.550 0.341 0.884 0.465 0.879

1 19 0.467 1.200 0.906 1.998 1.484

1 20 -0.581 -0.041 -0.321 0.145 -1.542

1 21 0.650 0.866 1.121 1.499 1.270

Cigarette - RTD (PD open)

data

sheet

laboratory

no

z-score

C1

z-score

C2

z-score

C3

z-score

C4

z-score

C5

1 1 0.308 0.300 -0.026 -0.046 0.785

1 2 1.009 -0.823 0.418 -1.521 -0.348

1 3 -0.193 0.550 -0.198 0.170 0.225

1 4 -0.086 0.924 -0.058 -0.029 0.053

1 5 --- --- --- --- ---

1 6 --- --- --- --- ---

1 7 1.180 1.423 1.083 1.927 -4.795

1 8 0.493 0.080 1.575 0.020 1.086

1 9 -0.228 0.588 -0.584 -0.775 0.010

1 10 -3.120 -2.426 -1.167 -0.676 -1.266

1 11 -2.239 0.723 -2.135 0.103 -3.102

1 12 -1.026 -0.573 -1.273 -1.206 -0.205

1 14 -0.320 -0.535 0.360 -0.377 0.569

1 15 -0.607 -0.650 -0.797 -0.493 0.197

1 16 -0.836 -0.093 -0.494 -0.493 -0.435

1 17 0.508 -1.831 0.089 -0.311 -0.564

1 18 0.931 -0.669 0.155 0.103 0.569

1 19 -0.150 0.387 1.025 1.115 1.229

1 20 0.517 -0.132 0.081 1.396 -0.406

1 21 2.159 1.644 1.386 1.828 3.166

Cigarette - RTD (PD closed)


Appendix H: “2015 PTM Proficiency Test – Individual z-scores Cigarettes” - continued

data

sheet

laboratory

no

z-score

C1

z-score

C2

z-score

C3

z-score

C4

z-score

C5

1 1 -1.147 -0.662 -1.375 0.122 -0.867

1 2 0.436 0.195 0.740 -0.542 -0.668

1 3 -0.965 0.149 0.422 -0.260 -0.327

1 4 0.222 0.690 -0.621 -0.298 0.215

1 5 -0.712 0.360 -0.167 2.248 0.310

1 6 -1.536 -0.603 -0.763 0.241 -0.681

1 7 0.260 1.194 2.072 0.715 0.941

1 8 1.364 1.629 2.078 2.229 2.279

1 9 1.071 0.821 0.377 1.279 1.099

1 10 -1.165 -1.025 -1.358 -1.111 -1.362

1 11 2.437 1.438 -0.048 1.227 1.449

1 12 0.356 -0.267 -0.621 -1.490 -0.447

1 14 0.185 -0.465 0.252 -0.027 -0.176

1 15 -0.071 -0.432 -0.621 -0.840 -0.163

1 16 -0.098 -0.366 0.400 -0.731 0.215

1 17 -0.312 -1.355 -0.678 -0.948 -1.268

1 18 0.991 -0.913 -0.655 -0.357 0.020

1 19 -1.112 -0.860 0.626 -0.785 -0.542

1 20 0.094 -0.610 -0.411 0.582 -0.646

1 21 0.604 1.211 2.140 0.509 1.399

Cigarette - FV


Appendix I: “2015 PTM Proficiency Test – Individual z-scores Filters – Evaluation 1”

data

sheet

laboratory

no

z-score

F1

z-score

F2

z-score

F3

z-score

F4

z-score

F5

1 1 0.088 -0.007 1.044 1.112 0.277

1 2 0.704 -0.713 0.058 1.128 0.089

1 3 0.916 -0.608 -2.014 0.992 -1.091

1 4 1.185 0.464 0.943 0.991 1.260

1 5 -1.097 -1.437 1.172 0.644 0.027

1 6 --- --- --- --- ---

1 7 0.350 1.484 -0.267 0.951 0.324

1 8 0.137 -0.164 -0.009 0.988 1.064

1 9 -0.840 2.085 0.854 1.019 1.414

1 10 -1.236 0.307 -0.636 -0.775

1 12 -0.903 -1.315 -0.412 1.062 -0.578

1 13 -1.116 -0.085 -0.524 1.074 -1.433

1 14 0.796 -0.373 1.134 1.256 -0.219

1 15 1.220 --- 0.596 0.853 0.705

1 16 0.144 -0.739 0.092 0.787 -1.664

1 17 0.711 -0.033 0.181 0.940 -0.424

1 18 0.732 --- -1.588 0.787 0.226

1 19 0.300 2.085 0.820 1.216 0.961

1 20 -0.755 -0.007 -0.849 0.913 -0.843

1 21 -1.335 0.228 -1.196 1.142 0.516

Filter - Individual Weight

data

sheet

laboratory

no

z-score

F1

z-score

F2

z-score

F3

z-score

F4

z-score

F5

1 1 -0.761 -2.007 -0.413 -1.335 -1.146

1 2 -0.460 0.093 0.688 0.042 -1.748

1 3 0.970 -0.397 -0.206 -0.233 -0.604

1 4 0.894 0.093 2.201 1.144 1.383

1 5 0.142 0.513 -0.757 0.386 0.961

1 6 --- --- --- --- ---

1 7 -0.234 0.653 0.206 0.111 -0.243

1 8 -1.890 -0.887 -2.270 -1.541 -1.025

1 9 0.067 -0.467 0.482 1.267 1.232

1 10 -0.460 0.303 -1.169 -0.784 -1.387

1 12 -0.912 1.984 1.169 1.488 0.781

1 13 1.421 0.723 -0.550 -1.059 -0.122

1 14 -0.310 -0.257 -1.238 0.042 -0.183

1 15 1.120 --- 0.688 0.042 0.901

1 16 -0.611 -0.397 0.550 -0.233 0.179

1 17 -0.686 1.073 -0.275 0.868 0.359

1 18 1.195 --- 1.307 1.006 -0.183

1 19 0.894 1.213 -0.757 -0.302 0.359

1 20 -1.213 -1.307 -0.206 -0.991 -0.544

1 21 0.443 -0.957 0.482 0.042 0.781

Filter - Diameter


Appendix I: “2015 PTM Proficiency Test – Individual z-scores Filters – Evaluation 1” - continued

data

sheet

laboratory

no

z-score

F1

z-score

F2

z-score

F3

z-score

F4

z-score

F5

1 1 0.013 -0.787 0.635 -0.375 0.908

1 2 --- --- --- --- ---

1 3 -0.663 --- -0.658 -0.670 -1.831

1 4 -0.704 -0.952 -1.567 -0.891 -0.042

1 5 0.463 0.539 0.281 -0.161 0.746

1 6 -1.345 -1.137 -0.342 -1.408 -1.185

1 7 -3.042 -4.751 -4.632 -10.379 -11.333

1 8 -0.041 -0.114 -0.140 0.562 0.782

1 9 --- --- --- --- ---

1 10 0.341 1.467 2.790 2.259 0.924

1 12 2.615 0.193 0.702 1.352 0.628

1 13 -0.238 0.751 0.989 0.046 0.179

1 14 0.393 0.790 1.267 0.223 -0.747

1 15 -0.326 --- -0.255 -0.050 -0.554

1 16 -0.867 -0.578 -0.389 -0.972 -0.996

1 17 0.439 0.511 0.482 0.702 0.667

1 18 --- --- --- --- ---

1 19 -0.127 -0.669 0.329 0.680 0.549

1 20 1.163 0.782 -0.562 0.525 0.462

1 21 2.260 0.704 -0.840 0.437 0.679

Filter - PD encapsulated


Appendix J: “2015 PTM Proficiency Test – Individual z-scores Filters – Evaluation 2”

data

sheet

laboratory

no

z-score

F1

z-score

F2

z-score

F3

z-score

F4

z-score

F5

2 1 -0.270 0.419 -0.502 -0.241 -0.486

2 2 -0.100 0.054 0.157 -0.643 -1.192

2 3 0.961 -0.717 -1.509 0.044 -0.942

2 4 1.595 0.783 0.172 1.085 1.374

2 5 -0.822 -0.612 0.175 -0.524 0.103

2 6 --- --- --- --- ---

2 7 0.438 0.804 -1.281 0.592 0.364

2 8 0.224 -1.274 -0.055 0.412 1.639

2 9 -0.049 2.925 0.725 0.731 2.456

2 10 -0.498 --- --- 1.287 0.121

2 12 -0.638 -1.081 1.467 --- ---

2 13 -0.646 -0.567 -0.358 -1.830 -1.147

2 14 1.462 0.461 0.127 -1.761 -0.221

2 15 2.310 --- -0.350 1.564 1.032

2 16 -0.594 -1.274 0.770 -0.859 -0.858

2 17 0.173 0.054 0.490 -0.081 -0.699

2 18 -0.004 --- 1.187 -0.977 -0.122

2 19 0.173 1.276 1.013 0.245 0.425

2 20 -1.309 -0.417 -1.781 0.217 -0.456

2 21 -1.515 0.590 -0.736 0.211 -0.296

Filter - Individual Weight

data

sheet

laboratory

no

z-score

F1

z-score

F2

z-score

F3

z-score

F4

z-score

F5

2 1 -0.869 -1.630 -0.523 -1.330 -0.595

2 2 -0.455 -0.391 0.207 0.078 -2.113

2 3 1.063 -0.391 -0.390 -0.350 -1.378

2 4 0.994 0.166 1.535 1.487 1.950

2 5 0.994 -0.206 -0.257 1.426 0.384

2 6 --- --- --- --- ---

2 7 -0.593 0.476 -1.187 -0.412 0.482

2 8 -1.077 -0.701 -2.315 -0.595 -1.085

2 9 0.373 -0.825 0.207 0.752 1.143

2 10 -0.110 --- --- --- ---

2 12 -1.077 1.219 1.137 0.385 -0.693

2 13 1.892 0.600 1.070 -1.208 -0.252

2 14 0.028 1.219 -0.722 -0.289 -0.106

2 15 -0.041 --- 0.672 -0.657 0.335

2 16 -0.041 -0.144 -0.257 -1.147 1.167

2 17 -0.110 1.157 1.070 0.446 0.139

2 18 1.408 --- -0.191 1.058 -0.155

2 19 0.304 1.033 -0.257 0.813 0.874

2 20 -0.869 -1.320 -1.253 -0.718 0.482

2 21 -1.422 -0.391 0.672 0.262 -0.742

Filter - Diameter


Appendix J: “2015 PTM Proficiency Test – Individual z-scores Filters – Evaluation 2”- continued

data

sheet

laboratory

no

z-score

F1

z-score

F2

z-score

F3

z-score

F4

z-score

F5

2 1 -0.091 -0.808 0.295 -0.497 0.527

2 2 --- --- --- --- ---

2 3 -0.744 --- -0.423 -0.446 -1.667

2 4 -0.779 -0.944 -1.528 -0.994 -0.166

2 5 0.500 0.733 0.142 0.203 0.805

2 6 -1.019 -1.014 -0.522 -1.433 -0.924

2 7 -3.508 -4.374 -4.123 -8.614 -12.330

2 8 -0.107 0.396 0.457 -0.032 1.008

2 9 --- --- --- --- ---

2 10 0.803 --- --- --- ---

2 12 2.396 0.108 1.391 2.381 1.349

2 13 -0.230 0.586 0.609 0.413 0.542

2 14 0.623 0.932 0.798 -0.784 -0.605

2 15 -0.131 -0.944 0.471 -0.001

2 16 -1.005 -0.571 0.933 -0.070 -0.969

2 17 0.034 0.671 0.798 0.821 0.614

2 18 --- --- --- --- ---

2 19 -0.353 -0.645 0.403 0.776 0.010

2 20 1.000 0.842 -0.953 1.037 0.745

2 21 2.657 1.215 0.017 0.534 0.066

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Technical Report 8th Proficiency Test (2015) for … Physical Parameters of Cigarettes and Filters...

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