TASK 210 – SUBSURFACE SITE INVESTIGATION ......Task 210 – Subsurface Site Investigation -2-...

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An Employee-Owned Company

TASK 210 – SUBSURFACE SITE INVESTIGATION REPORT

CONNECTICUT DEPARTMENT OF TRANSPORTATION

BRIDGE NO. 06755, ROUTE 162 OVER TURTLE CREEK

MILFORD, CONNECTICUT

Prepared for:

Connecticut Department of Transportation

Division of Environmental Compliance

P.O. Box 317546

Newington, Connecticut 06131

Prepared by:

BL Companies, Inc.

355 Research Parkway

Meriden, Connecticut 06450

BL Companies Project Number 18EC0070

ConnDOT Project No. 83-0263

Assignment No. 318-5818

June 2019

This report was prepared by the individuals listed below. Any questions or comments regarding

the information provided herein should be directed to these individuals.

Prepared by:

__________________________________________

Wesley Johnson

Project Scientist

Reviewed by:

Joy P. Kloss, LEP, CHMM

Project Manager

Aaron L. Silva, LEP

Senior Project Manager

Task 210 – Subsurface Site Investigation -i- Project No.18EC0070

Bridge No. 06755, Route 162 over Turtle Creek June 2019

State Project No. 83-0263; Assignment No. 318-5818

TABLE OF CONTENTS

1.0 INTRODUCTION ............................................................................................................. 1

1.1 BACKGROUND AND PURPOSE ............................................................................................. 1

1.2 SCOPE OF WORK ................................................................................................................. 1

2.0 LOCAL ENVIRONMENT AND RECEPTORS ............................................................ 3

2.1 SURFICIAL GEOLOGY .......................................................................................................... 3

2.2 BEDROCK GEOLOGY ........................................................................................................... 3

2.3 GROUNDWATER .................................................................................................................. 3

2.4 SURFACE WATER ................................................................................................................ 3

3.0 FIELD INVESTIGATION AND SAMPLING METHODS .......................................... 4

3.1 SOIL BORING INSTALLATION AND SAMPLING .................................................................... 4

3.2 GROUNDWATER SAMPLING ................................................................................................ 4

4.0 REGULATORY CRITERIA ............................................................................................ 6

4.1 SOIL CRITERIA .................................................................................................................... 6

4.2 GROUNDWATER CRITERIA .................................................................................................. 7

5.0 SUMMARY AND EVALUATION OF ANALYTICAL DATA .................................... 8

5.1 SOIL SAMPLE ANALYTICAL RESULTS ................................................................................. 8

5.2 SEDIMENT SAMPLE ANALYTICAL RESULTS ........................................................................ 9

5.3 GROUNDWATER ANALYTICAL RESULTS .......................................................................... 11

5.4 QUALITY ASSURANCE (QA)/QUALITY CONTROL (QC) RESULTS .................................... 12

6.0 POTENTIAL SOURCES OF CONTAMINATION, RECEPTORS, AND

IDENTIFIED PRELIMINARY AREAS OF ENVIRONMENTAL CONCERN ...... 15

7.0 CONCLUSIONS AND RECOMMENDATIONS ......................................................... 16

8.0 LIMITATIONS ................................................................................................................ 17

9.0 REFERENCES ................................................................................................................. 18

APPENDIX A – FIGURES

Figure 1 Site Location Map

ENV-01 Site Investigation Plan

APPENDIX B – TABLES

Table 1 Sample Location Rationale and Selected Analyses

Table 2 Soil and Sediment Analytical Results

Table 3 Groundwater Analytical Results

APPENDIX C – BORING LOGS

APPENDIX D – LABORATORY ANALYTICAL REPORT

Task 210 – Subsurface Site Investigation -1- Project No.18EC0070



1.0 INTRODUCTION

BL Companies was retained by the State of Connecticut Department of Transportation

(ConnDOT) to conduct a Task 210 Subsurface Site Investigation (SSI) in support of ConnDOT

Project No. 83-0263, Bridge No. 06755, Route 162 over Turtle Creek in Milford, Connecticut.

This report provides a brief description and history of the project area, a discussion of the local

environment and receptors, the investigation rationale, a summary of the data obtained during the

investigation, an interpretation of the results with respect to the appropriate regulatory criteria,

and recommendations.

1.1 Background and Purpose

This project is located approximately 0.7 miles east of the Route 162 intersection with Route 736

in Milford, Connecticut. The project consists of the replacement of Bridge No. 06755. The

project includes the demolition and removal of the existing culvert system and the installation of

twin 8’x4’ precast concrete box culverts and associated cast-in-place structures. The site’s

location and pertinent features are depicted on the enclosed Site Location Map (Figure 1) and

Site Investigation Plan (ENV-01)

The purpose of this Task 210 SSI is to collect soil and groundwater data in order to evaluate

whether the proposed construction activities require management of contaminated soil and

groundwater.

1.2 Scope of Work

BL Companies completed a Task 210 SSI work plan, dated April 19, 2019, which was approved

by ConnDOT. The scope of work included the following tasks:

• Prior to drilling, BL Companies will complete the following: (1) obtain a ConnDOT

encroachment Permit, (2) mark the location of each proposed drilling location with

white paint, (3) contact the Call-Before-You-Dig (CBYD) utility mark-out service to

mark subsurface utilities and review exist utility plans, and (4) meet on-site to discuss

proposed drilling locations with representatives of ConnDOT and other utility

companies/agencies, if necessary.

• Completion of six soil borings B-1 through B-6 to depths ranging from 10 to 15 feet

below grade (ftbg) using a Geoprobe direct push rig.

• Installation of two temporary groundwater monitoring wells at B-3 and B-4;

• Recording lithology and field screening soil samples with a photoionization detector

(PID);

• Collection and laboratory analysis of two to three soil samples per boring, and

collection of two sediment samples, for one or more of the following:

o Volatile Organic Compounds (VOCs) by EPA Method 8260;

o Semi-Volatile Organic Compounds (SVOCs) by EPA Method 8270;

o Extractable Total Petroleum Hydrocarbons (ETPH) by CT ETPH Method;




o Total RCRA 8 Metals by EPA Methods 6010/ 7471;

o Leachable RCRA 8 Metals using synthetic precipitation leaching procedure

(SPLP);

o Polychlorinated Biphenyls (PCBs) by EPA Method 8082;

o Pesticides by EPA Method 8081; and

o Ignitability; Reactivity; and pH.

• Collection and laboratory analysis of groundwater samples from five temporary wells

for the following:

o VOCs by EPA Method 8260;

o SVOCs by EPA Method 8270;

o ETPH by CT ETPH Method;

o PCBs by EPA Method 8082;

o Pesticides by EPA Method 8081; and

o Total and Dissolved Lead, Copper, and Zinc by EPA Method 6010/7471.




2.0 LOCAL ENVIRONMENT AND RECEPTORS

2.1 Surficial Geology

According to the "Surficial Materials Map of Connecticut", dated 1992, surficial materials within

the project area are identified as salt-marsh and tidal-marsh deposits, which is described as peat

and muck interbedded with sand and silt, deposited in environments of low wave energy along

the coast and in river estuaries. Based on observations during boring installation, surficial

materials consist of varying shades of brown fine to coarse sand, silt, and peat with varying

amounts of fine to coarse gravel. Boring logs are included as Appendix C.

2.2 Bedrock Geology

According to the “Bedrock Geological Map of Connecticut”, dated 1985, the project area is

unmapped; however, surrounding areas are underlain by two types of bedrock, the Allingtown

Metavolcanics and Oronoque Schist. The Allingtown Metavolcanics is described as green, fine

grained, massive greenstone. The Oronoque Schist is described as gray to silvery, medium to

fine grained, well layered schist and granofels with small lenses of amphibolite or greenstone.

Bedrock was not encountered during this investigation.

2.3 Groundwater

Based on a review of the Water Quality Classifications Map for Milford, Connecticut, dated

October 2018, the project area has been designated by Department of Energy and Environmental

Protection (DEEP) as “GB” quality. The GB classification indicates that groundwater at the Site

is not suitable for human consumption without treatment. During this Task 210 SSI, groundwater

was encountered at depths ranging from 1.3 to 6.4 ftbg. Based on the presence of Turtle Creek,

the general direction of groundwater flow is inferred to be southwest.

2.4 Surface Water

Turtle Creek flows from north to south across New Haven Avenue and into Gulf Pond. Both

Turtle Creek and Gulf Pond are classified as “SB” surface waters, according to the above-

referenced DEEP map. Class SB surface waters are designated for use as marine fish, shellfish

and wildlife habitat, shellfish harvesting for transfer to approved areas for purification prior to

human consumption, recreation, industrial and other legitimate uses including navigation.




3.0 FIELD INVESTIGATION AND SAMPLING METHODS

This Task 210 SSI included the advancement of six soil borings, the installation of two

temporary monitoring wells, and collection and laboratory analysis of 14 soil samples, two

sediment samples, and two groundwater samples. BL Companies subcontracted Cummins

Envirotech Inc., of Old Lyme, Connecticut to advance the soil borings and install the temporary

monitoring wells. The soil borings, temporary monitoring wells, and sediment sample locations

are depicted on the Site Investigation Plan (ENV-01).

Soil and sediment samples were analyzed for regulated constituents of concern associated with

the roadway and nearby property uses. Table 1 in Appendix B provides a summary of the

sampling rationale and the laboratory analyses requested for each soil and sediment sample. The

following sections summarize the field investigation and sampling methodologies used during

this investigation.

3.1 Soil Boring Installation and Sampling

On April 30, 2019, six soil borings, identified as B-1 through B-6, were advanced to a depth of

10 to 15 ftbg using a track-mounted Geoprobe direct-push drill rig. The depths of soil borings

were based on anticipated excavation depths. Soil samples were obtained continuously during

advancement of the soil borings using a 2-inch diameter, 5-foot long, sampling device equipped

with disposable acetate liners. In addition, two sediment grab samples were collected from the

Turtle Creek culvert areas.

A representative portion of each soil core was screened with a PID to detect estimated quantities

of total VOCs in vapor emitted from the soil. The PID was equipped with a 10.6 eV bulb and

was calibrated to isobutylene standard gas (100 parts per million (ppm)). PID readings above

background (0.0 ppm) ranged from 0.1 to 36 ppm and are provided with the boring logs included

in Appendix C. Grey stained soil and a petroleum odor was noted in boring B-5 at a depth

ranging from 1.7 to 2.8 ftbg. A faint petroleum odor was additionally noted in boring B-5 at a

depth ranging from 5 to 7.4 ftbg. A faint unidentified odor was noted in boring B-4 at depths

ranging from 5.8 to 7 ftbg and 10 to13 ftbg. B-4 was also saturated with groundwater which was

stained black. Lastly, methane/organic odors were noted in borings B-1, B-3, B-5, and B-6.

Soil samples were selected for laboratory analysis based upon observations (physical evidence of

contamination and/or lithology change), the results of the field screening, and anticipated

excavation depths. The samples were submitted under proper chain of custody to Eurofins

Spectrum Analytical of Agawam, Massachusetts, a State of Connecticut Department of Public

Health certified environmental testing laboratory.

3.2 Groundwater Sampling

Following soil sampling, a 1-inch diameter PVC screen and riser pipe were inserted into borings

B-3 and B-4 as temporary groundwater wells. Prior to sampling, BL Companies developed the

wells using a peristaltic pump and dedicated tubing to improve the hydraulic connection of the

wells with the surrounding aquifer and to reduce turbidity. Samples were collected directly into




pre-preserved sample containers provided by the laboratory. Dissolved metals were collected

using an inline 0.45-micron filter.




4.0 REGULATORY CRITERIA

The soil and sediment analytical results were compared to the numeric criteria listed in the

Connecticut DEEP Remediation Standard Regulations (RSRs), sections 22a-133k-1 through 22a-

133k-3 of the Regulations of Connecticut State Agencies, dated June 2013, and compared to the

published 2015 numeric criteria for additional polluting substances not promulgated in the June

2013 RSRs. The RSRs were developed by the DEEP to define the remediation performance

standards for soil and groundwater to be protective of human health and the environment.

The RSRs apply specifically to sites at which remedial actions are required by the DEEP under

Chapters 445 or 446k of the Connecticut General Statutes (CGS) such as under an administrative

order, a transfer of an establishment under CGS Section 22a-134a, and sites that are enrolled in

the Voluntary Remediation Program under CGS Sections 22a-133x or 22a-133y.

Currently, the RSRs do not address sediment, and the Site is not regulated under any of the

above State statutes; however, BL Companies used the numeric criteria stated above as

guidelines to evaluate concentrations of regulated compounds detected in soil. DEEP defines

polluted soil as containing any substance at a concentration above the analytical detection limit.

Contaminated soil is defined as any substance whose concentration exceeds the numeric criteria

of the RSRs. Both classifications require special handling, re-use, and disposal requirements.

The following sections provide a summary of the soil and groundwater criteria utilized during

this Task 210 SSI.

4.1 Soil Criteria

Direct Exposure Criteria (DEC)

The DEC are designed to protect human health from risks associated with exposure to pollutants

in contaminated soil within 15 feet of the ground surface.

The RSRs provide two sets of DEC, one for residential land use (RES DEC) and another for

industrial/commercial land use (I/C DEC). The CTDEEP RSRs define “residential activity”

under CGS Section 22a-133k-1(a) to include any activity related to a residence or dwelling, or to

a school, hospital, day care center, playground, or outdoor recreation area. Remediation to the

RES DEC is required unless an ELUR is recorded that restricts residential use. For this project,

BL Companies compared the soil analytical results to both the RES DEC and I/C DEC.

Pollutant Mobility Criteria (PMC)

The PMC are designed to protect groundwater quality by reducing or eliminating the potential

for migration of pollutants to groundwater from contaminated soil. The RSRs provide two sets

of PMC based on the groundwater classification of the Site, as designated by DEEP. The project

is in a “GB” designated area. Therefore, soil analytical results were compared to the GB PMC,

which apply to soil located from the ground surface to the depth of the seasonal high water table.




4.2 Groundwater Criteria

Maximum Concentration Limits (MCLs) Established in DEEP General Permits for Discharge of

Groundwater Remediation Wastewater

MCLs established in DEEP General Permit for Discharge of Groundwater Remediation

Wastewater (Appendix A and B) apply to impacted groundwater that is discharged during

construction dewatering. To evaluate whether construction dewatering would require treatment

prior to discharge, BL Companies compared the groundwater analytical results to the Discharge

to Surface Water and Sanitary Sewer/POTW MCLs.




5.0 SUMMARY AND EVALUATION OF ANALYTICAL DATA

5.1 Soil Sample Analytical Results

Soil analytical results are summarized in Table 2 in Appendix B along with the regulatory

criteria. The soil analytical laboratory reports are included in Appendix D.

VOCs

All soil samples were analyzed for VOCs by EPA Method 8260. Benzene was detected in

sample B-5 (1.7-2.8’) at a concentration above the GB PMC. VOCs were detected at

concentrations below applicable RSR criteria in nine soil samples. VOCs were not detected at

concentrations above laboratory reporting limits in the remaining samples.

SVOCs

All soil samples were analyzed for SVOCs by EPA Method 8270. SVOCs were detected in

sample B-3 (0.4-2.2’) at concentrations above applicable RSR criteria. SVOCs were detected at

concentrations below applicable RSR criteria in samples B-1 (1-3’), B-4 (0.4-1.8’), and B-6 (0.4-

1.7’). SVOCs were not detected above laboratory reporting limits in the remaining samples.

ETPH

All soil samples were analyzed for ETPH by CT ETPH Method. ETPH was not detected above

laboratory reporting limits in any samples.

Metals

All soil samples were analyzed for total RCRA 8 metals for comparison to the DEC.

• Arsenic was detected in sample B-6 (0.4-1.7’) at concentrations of 23.3 mg/kg, which is

above the RES DEC and I/C DEC. Arsenic was detected in all other samples at

concentrations ranging from 1.12 to 7.35 mg/kg, which are below the RES DEC and I/C

DEC.

• Barium was detected in all samples at concentrations ranging from 5.95 to 32.8 mg/kg,

which are below the RES DEC and I/C DEC.

• Cadmium was detected in soil samples B-4 (5.4-7.4’) and B-6 (0.4-1.7’) at

concentrations of 2.9 and 0.37 mg/kg, respectively, which are below the RES DEC and

I/C DEC. Cadmium was not detected above laboratory reporting limits in the remaining

samples.

• Chromium was detected in all samples at concentrations ranging from 8.75 to 33 mg/kg,


• Lead was detected in all samples at concentrations ranging from 2.68 to 75.4 mg/kg,





• Mercury was detected in soil sample B-5 (1.7-2.8’) at a concentration of 0.03 mg/kg,

which is below the RES DEC and I/C DEC. Mercury was not detected above

laboratory reporting limits in any other samples.

• Selenium and silver were not detected above laboratory reporting limits in any soil

samples.

Soil samples were additionally analyzed for leachable RCRA 8 metals by SPLP for comparison

to the GB PMC.

• SPLP arsenic was detected in seven soil samples at concentrations ranging from 0.005

to 0.035 milligrams per liter (mg/L), which are below the GB PMC. SPLP arsenic was

not detected above laboratory reporting limits in any other samples.

• SPLP barium was detected in all soil samples at concentrations ranging from 0.013 to

0.53 mg/L, which are below the GB PMC.

• SPLP lead was detected in three soil samples at concentrations ranging from 0.013 to

0.022 mg/L, which are below the GB PMC. SPLP lead was not detected above

laboratory reporting limits in any other samples.

• SPLP cadmium, chromium, mercury, selenium, and silver were not detected above

laboratory reporting limits in any soil samples.

PCBs

All soil samples were analyzed for PCBs by EPA Method 8082. No PCBs were detected above


Pesticides

All soil samples were analyzed for pesticides by EPA Method 8081. 4,4’-DDT was detected in

soil sample B-4 (0.4-1.8’) at a concentration below the RSR criteria. 4,4’-DDT was not detected

above laboratory reporting limits in any other samples.

Reactivity, Ignitability, and Coorosivity

Each soil sample was analyzed for reactive cyanide and sulfide, ignitability, and pH. Reactive

sulfide was detected in one sample at a concentration of 49 mg/kg, however, reactivity is

negative per EPA method SW846. Based on the laboratory results, the soil does not exhibit

hazardous characteristics of reactivity, ignitability, and corrosivity.

5.2 Sediment Sample Analytical Results

Sediment analytical results are summarized in Table 2 in Appendix B along with the regulatory

criteria. The soil analytical laboratory reports are included in Appendix D.




VOCs

Each sediment sample was analyzed for VOCs by EPA Method 8260. Methyl ethyl ketone was

detected in sample SED-1 at a concentration below RSR criteria. No other VOCs were detected

at concentrations above laboratory reporting limits in the any sediment samples.

SVOCs

Each sediment sample was analyzed for SVOCs by EPA Method 8270. SVOCs were detected in

both samples at concentrations above applicable RSR criteria.

ETPH

Each sediment sample was analyzed for ETPH by CT ETPH Method. ETPH was detected in

both samples at concentrations of 370 and 180 mg/kg, which are below applicable RSR criteria.

Metals

Each sediment sample was analyzed for total RCRA 8 metals for comparison to the DEC.

• Arsenic was detected in sample SED-1 at concentrations of 52.7 mg/kg, which is above

the RES DEC and I/C DEC. Arsenic was detected in the other sediment sample at a

concentration below the RES DEC and I/C DEC.

• Barium was detected in each sample at concentrations of 95.1 and 12.1 mg/kg, which

are below the RES DEC and I/C DEC.

• Cadmium was detected in each sample at concentrations of 2.87 and 1.21 mg/kg, which

are below the RES DEC and I/C DEC.

• Chromium was detected in each sample at concentrations of 50.3 and 21.7 mg/kg,


• Lead was detected in each sample at concentrations of 48.2 and 29 mg/kg, which are

below the RES DEC and I/C DEC.

• Mercury was detected in each sample at concentrations of 17 and 2.5 mg/kg, which are

below the RES DEC and I/C DEC.

• Selenium and silver were not detected above laboratory reporting limits in either

sediment sample.

Sediment samples were additionally analyzed for leachable RCRA 8 metals by SPLP for

comparison to the GB PMC.

• SPLP arsenic was detected in each sediment sample at concentrations of 0.027 and


• SPLP barium was detected in each sediment sample at concentrations of 0.081 and





• SPLP lead was detected in SED-2 at a concentration of 0.012 mg/L, which is below the

GB PMC. SPLP lead was not detected above laboratory reporting limits in the other

sediment sample.

• SPLP cadmium, chromium, mercury, selenium, and silver were not detected above


PCBs

All soil samples were analyzed for PCBs by EPA Method 8082. No PCBs were detected above


Pesticides

All soil samples were analyzed for pesticides by EPA Method 8081. Pesticides were not

detected at concentrations above laboratory reporting limits in either sediment sample.

Reactivity, Ignitability, and Corrosivity

Each sediment sample was analyzed for reactive cyanide and sulfide, ignitability, and pH.

Reactive sulfide was detected in both samples at concentrations of 21 and 276 mg/kg; however,

reactivity is negative per EPA method SW846. Based on the laboratory results, the sediment

does not exhibit hazardous characteristics of reactivity, ignitability, and corrosivity.

5.3 Groundwater Analytical Results

Groundwater analytical results in comparison to the General Discharge Permit MCLs are

summarized Table 3 in Appendix B along with the regulatory criteria. The groundwater

analytical laboratory report is included in Appendix D.

VOCs

All groundwater samples were analyzed for VOCs by EPA Method 8260. Several VOCs were

detected in TMW-2 at various concentrations. General Permit MCLs have not been established

for these VOCs; however, total VOCs are above the total VOCs MCL for surface water, but not

sanitary sewer. Total VOCs were detected in sample TMW-1 at concentrations below the total

VOCs MCLs.

SVOCs

All groundwater samples were analyzed for SVOCs by EPA Method 8270. SVOCs were

detected in groundwater sample TMW-2 at concentrations below the General Permit MCLs.

SVOCs were not detected at concentrations above laboratory reporting limits in the remaining

sample.

ETPH

All groundwater samples were analyzed for ETPH by CT ETPH Method. ETPH was not

detected at concentrations above laboratory reporting limits in any groundwater samples.




Metals

All groundwater samples were analyzed for total and dissolved copper, lead, and zinc.

• Total copper was detected in groundwater sample TMW-1 at a concentration below the

General Permit MCLs. Total copper was not detected at a concentration above the

laboratory reporting limit in sample TMW-2. Dissolved copper was not detected at

concentrations above laboratory reporting limits in the any groundwater samples.

• Total lead was detected in groundwater sample TMW-1 at a concentration below the

General Permit MCLs. Total lead was not detected at a concentration above the

laboratory reporting limit in sample TMW-2. Dissolved lead was detected in both

samples at concentrations below the General Permit MCLs.

• Total zinc was detected in sample TMW-1 at a concentration below the General Permit

MCLs. Total zinc was not detected above laboratory reporting limits in sample TMW-

2. Dissolved zinc was detected in each sample at concentrations below the General

Permit MCLs.

PCBs

All groundwater samples were analyzed for PCBs by EPA Method 8082. PCBs were not

detected in either groundwater sample.

Pesticides

All groundwater samples were analyzed for pesticides by EPA Method 8081. Dieldrin was

detected in each sample at concentrations above the General Permit MCL for surface water.

5.4 Quality Assurance (QA)/Quality Control (QC) Results

All samples were analyzed using the DEEP Reasonable Confidence Protocol (RCP), where

applicable, and meet the RCP requirements. BL Companies also reviewed the laboratory RCP

Certification Report to evaluate the reliability of the analytical data. The case narratives do not

indicate any non-conformances that would affect the usability of the data.

Soil

One trip blank sample was prepared at the laboratory and accompanied the sample containers

during transport to evaluate the potential for cross-contamination from the surrounding

environment during transport. The trip blank sample was analyzed for VOCs. VOCs were not

detected in the trip blank sample, indicating that there was likely no cross-contamination of the

samples during transportation.

A duplicate soil sample was collected from one randomly selected soil sample location to

evaluate the accuracy of the laboratory analytical data, measured as Relative Percent Difference

(RPD) as defined by the DEEP Laboratory Quality Assurance and Quality Control Guidance

Document, dated May 2009, revised December 2010.




The duplicate sample was analyzed for VOCs, SVOCs, ETPH, PCBs, pesticides, total and SPLP

RCRA 8 metals, ignitability, reactivity, and pH. Analytical results were within the acceptable

RPD of 50 for soil samples except for the following:

• 1,2,4-Trimethylbenzene was detected at a concentration of 0.16 mg/kg in the original

sample and at 0.39 mg/kg in the duplicate sample resulting in an RPD of 83.6. Both

results are below RSR criteria. Therefore, the usability of the data is not affected.

• 1,3,5-Trimethylbenzene was detected at a concentration of 0.15 mg/kg in the original

sample and at 0.36 mg/kg in the duplicate sample resulting in an RPD of 82.4. Both


• Benzene was detected at a concentration of 0.24 mg/kg in the original sample and at 0.62

mg/kg in the duplicate sample resulting in an RPD of 88.4. Both results are above the

RSR criteria. Therefore, the usability of the data is not affected.

• Ethylbenzene was detected at a concentration of 0.11 mg/kg in the original sample and at

0.21 mg/kg in the duplicate sample resulting in an RPD of 62.5. Both results are below


• Isopropylbenzene was detected in the duplicate sample at a concentration of 0.14 mg/kg

and was not detected above the laboratory reporting limit in the original sample. Both

results are below the RSR criteria. Therefore, the usability of the data is not affected.

• Naphthalene was detected at a concentration of 0.57 mg/kg in the original sample and at

1.5 mg/kg in the duplicate sample resulting in an RPD of 89.9. Both results are below


• Total xylenes were detected at a concentration of 0.34 mg/kg in the duplicate sample and

were not detected above the laboratory reporting limit in the original sample. Both


• Mercury was detected in the original sample at a concentration of 0.03 mg/kg and was

not detected above the laboratory reporting limit in the duplicate sample. Both results are

below RSR criteria. Therefore, the usability of the data is not affected.

Groundwater

A field blank sample was collected by purging de-ionized water directly into the laboratory

provided sample containers during field sampling operations on-Site. The purpose of a field

blank sample is to evaluate the potential for on-Site field contamination. The field blank sample

was analyzed for VOCs, SVOCs, ETPH, PCBs, pesticides, and total and dissolved copper, zinc,

and lead. Dissolved zinc was detected in the field blank at a concentration well below the

General Permit MCL. No other constituents were detected in the field blank sample. All

dissolved zinc concentrations were below the General Permit MCLs; therefore, the usability of

the data is not affected.

A trip blank sample was prepared at the laboratory and accompanied the sample containers from

the laboratory, to the Site, and back to the laboratory. The purpose of a trip blank sample is to




evaluate the potential for cross-contamination during transport. The trip blank sample was

analyzed for VOCs. VOCs were not detected in the sample, indicating that there was likely no

cross-contamination of the samples during transport.

A duplicate sample was collected from TMW-1 to evaluate the accuracy of the laboratory

analytical data, measured as RPD. The duplicate sample was analyzed for VOCs, SVOCs,

ETPH, PCBs, pesticides, and total and dissolved copper, zinc, and lead. Analytical results were

within the acceptable RPD of 30 for aqueous samples except for the following:

• Cis-1,2-dichloroethene was detected in the original sample at a concentration of 2.8 µg/L

and was not detected above laboratory reporting limits in the duplicate sample. No

General Permit MCLs have been established for cis-1,2-dichloroethene. Total VOCs are

below the General Permit MCLs; therefore, the usability of the data is not affected.

• Dieldrin was detected in the original sample at a concentration of 0.024 µg/L, above the

Surface Water General Permit MCL, and was not detected at concentrations above the

laboratory reporting limit in the duplicate sample. BL Companies will conservatively use

the higher concentration as the sample result, which exceeded the General Permit MCL

for surface water.

• Dissolved lead was detected in the original sample at a concentration 2 µg/L and was not

detected above the laboratory reporting limit in the duplicate sample. Both results are

below the General Permit MCLs; therefore, the usability of the data is not affected.




6.0 POTENTIAL SOURCES OF CONTAMINATION, RECEPTORS, AND

IDENTIFIED PRELIMINARY AREAS OF ENVIRONMENTAL CONCERN

The following provides a summary of the potential sources of soil contamination identified

during completion of this Task 210 SSI, an evaluation of potential pathways for migration, and

the identification of preliminary Areas of Environmental Concern (AOECs) within the project

area.

Based on the Task 210 SSI results, the following AOECs and GWAOEC were identified:

AOEC 1 (Site Wide) – Contaminated Soil in the Vicinity of Borings B-3, B-5, and B-6

VOCs, SVOCs, and arsenic were detected at concentrations exceeding RSR criteria in the soil

samples collected at depths ranging from 0 to 3 ftbg. Therefore, any soil removed from AOEC 1

should be reused onsite within AOEC 1 or handled as controlled material. The source of the

VOCs and SVOCs is likely associated with historic adjacent property use. Arsenic is likely

naturally occurring.

Proposed work within AOEC 1 includes the replacement of Bridge No. 06755 and culverts.

Potential receptors of the impacted soil include workers involved in the construction activities.

SED AOEC – Contaminated Sediment in the vicinity of SED-1 and SED-2

SVOCs and arsenic were detected at concentrations exceeding RSR criteria in sediment samples

collected from the Turtle Creek culvert areas. Therefore, any sediment removed from SED

AOEC should be handled as controlled material. The source of the SVOCs is likely associated

with historic adjacent property use. Arsenic is likely naturally occurring.

Proposed work within SED AOEC includes the replacement of Bridge No. 06755 and culverts.

Potential receptors of the impacted sediment include workers involved in the construction

activities.

GWAOEC (Site Wide) - Contaminated Groundwater in the Vicinity of TMW-1 and

TMW-2

Total VOCs and pesticides were detected at concentrations exceeding the General Permit MCL

for Surface Water. Based on the results of this investigation, if groundwater within the

GWAOEC requires dewatering, it can be discharged to sanitary without treatment. Discharge to

surface water would require pre-treatment.




7.0 CONCLUSIONS AND RECOMMENDATIONS

Based on the analytical data collected by BL Companies, preliminary AOECs and GWAOEC

were identified within the project area, as summarized below:

• Soil within AOEC 1 contains VOCs, SVOCs, and arsenic at concentrations above

RSR criteria, and therefore is considered contaminated. This material should be

handled and managed as controlled material in accordance with DOT project

specifications.

• Sediment within SED AOEC contains SVOCs and arsenic at concentrations above

RSR criteria, and therefore is considered contaminated. This material should be

handled and managed as controlled material in accordance with DOT project

specifications.

• Groundwater within GWAOEC contains total VOCs and pesticides above the Surface

Water Discharge MCL, but below the Sanitary Sewer Discharge MCL. Therefore,

groundwater within GWAOEC will require special management or treatment if

encountered during excavations for the project.

Based on the results of this Task 210 SSI, BL Companies recommends that a Task 310 – Plans,

Specifications, and Estimates be assigned to prepare plans and specifications for the proper

management and/or disposal of controlled materials (soil, sediment, and groundwater) that may

be reused, removed, handled, transported, or disposed during construction activities and for the

establishment of appropriate worker health and safety protocols.




8.0 LIMITATIONS

The conclusions stated above are based solely on the information described in this report. The

data and observations generated during this investigation reflect the conditions found on the

project site on the dates and at the locations specified. Where visual observations are included in

the report, they represent conditions at the time of investigation, and may not be indicative of

past or future conditions. The data cannot be extrapolated to locations on the site that were not

tested, or to compounds for which tests were not conducted.

Latent conditions and other information may become evident in the future based on currently

unavailable evidence. BL Companies assumes no responsibility for such conditions or for the

inspection, engineering, or repair that might be required to discover or correct such factors.

Should such evidence arise, it should be forwarded to BL Companies so that additional

conclusions and recommendations may be evaluated as necessary.

This report has been completed solely for the benefit and individual use of the client. No part

thereof, nor any copy of the same, shall be used for any purpose by anyone other than the client.

No disclosure or reliance of this report may be made without the prior written consent of BL

Companies.




9.0 REFERENCES

1. State of Connecticut Department of Energy and Environmental Protection (CTDEEP),

Remediation Standard Regulations, Sections 22a-133k-1 through –3 of the Regulations of

Connecticut State Agencies, June 2013.

2. CTDEEP, “Water Quality Classifications Map of Milford”, October 2018.

3. CTDEEP, “Recommended Numeric Criteria for Common Additional Polluting Substances

and Certain Alternative Criteria”, December 10, 2015.

4. State of Connecticut Department of Transportation, Division of Environmental Compliance,

“On-Call Contaminated Soil/Groundwater Scopes” manual, dated 2010.

5. Rogers, John, USGS, “Bedrock Geological Map of Connecticut”, dated 1985.

6. Stone, J., USGS, “Surficial Materials Map of Connecticut”, dated 1992.

APPENDIX A

FIGURES

Figure 1 – Site Location Map

ENV-01 – Site Investigation Plan

SITE LOCATION MAP

Bridge No. 06755, Route 162 over Turtle Creek

Milford, Connecticut

Project No. 18EC0070

Base map is a reproduction of the U.S.G.S. 7.5 Minute Topographic Quadrangle of Milford, Connecticut, 2018

SITE

LOCATION

APPENDIX B

TABLES

Table 1 Sample Location Rationale and Selected Analyses

Table 2 Soil and Sediment Analytical Results

Table 3 Groundwater Analytical Results

Table 1

Sample Location Rationale and Selected Analyses

Bridge No. 06755, Route 162 Over Turtle Creek, Milford, Connecticut


Sample

IdentificationMatrix Sample Interval Location Rationale

VOCs

(8260)

SVOCs

(8270)ETPH

PCBs

(8082)

Pesticides

(8081)

Total

RCRA 8

Metals

SPLP

RCRA 8

Metals

Ignitability,

Reactivity,

pHSoil 1-3' X X X X X X X X

Soil 7.7-9' X X X X X X X X

Soil 1-2.9' X X X X X X X X

Soil 8-9.8' X X X X X X X X

0.4-2.2' X X X X X X X X

6-8' X X X X X X X X

11-13' X X X X X X X X

0.4-1.8' X X X X X X X X

5.4-7.4' X X X X X X X X

11.8-13.8' X X X X X X X X

1.7-2.8' X X X X X X X X

5-7' X X X X X X X X

0.4-1.7' X X X X X X X X

5.6-7.6' X X X X X X X X

SED-1 Sediment NATurtle Creek culvert on northside of

New Haven Ave.X X X X X X X X

SED-2 Sediment NATurtle Creek culvert on southside of

New Haven Ave.X X X X X X X X

Sample

IdentificationMatrix

Sample

Collection

Method

Location RationaleVOCs

(8260)

SVOCs

(8270)ETPH

PCBs

(8082)

Pesticides

(8081)

Total

Lead,

Copper,

and Zinc

TMW-1 Groundwater GrabNorthside of New Haven Ave, adjacent

to proposed bridge.X X X X X X

TMW-2 Groundwater GrabSouthside of New Haven Ave, adjacent

to proposed bridge.X X X X X X

X

X

Dissolved Lead,

Copper, and Zinc

B-2

B-1Southside of New Haven Ave, west of

proposed bridge.

Northside of New Haven Ave, west of

proposed bridge.

B-3 SoilNorthside of New Haven Ave, adjacent

to proposed bridge.

B-4 SoilSouthside of New Haven Ave, adjacent

to proposed bridge.

B-5 SoilSouthside of New Haven Ave, east of

proposed bridge.

B-6 SoilNorthside of New Haven Ave, east of

proposed bridge.

BL Companies Project No. 18EC0070 1 of 1 June 2019

Table 2

Soil and Sediment Analytical Results




B-1 (1-3') B-1 (7.7-9') B-2 (1-2.9') B-2 (8-9.8') B-3 (0.4-2.2') B-3 (6-8') B-3 (11-13') B-4 (0.4-1.8') B-4 (5.4-7.4') B-4 (11.8-13.8') B-5 (1.7-2.8') DUP B-5 (5-7') B-6 (0.4-1.7') B-6 (5.6-7.6') SED-1 SED-2 TRIP BLANK

4/30/2019 4/30/2019 4/30/2019 4/30/2019 4/30/2019 4/30/2019 4/30/2019 4/30/2019 4/30/2019 4/30/2019 4/30/2019 4/30/2019 4/30/2019 4/30/2019 4/30/2019 4/30/2019 4/30/2019 4/30/2019

500 2,500 2,500 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 370 180 NA

VOCs (mg/kg)

1,1-Dichloroethane 500 1,000 14 ND ND ND 0.018 ND ND ND ND ND 0.088 ND ND ND ND ND ND ND ND

1,1,1-Trichloroethane 500 1,000 40 ND ND ND 0.015 ND ND ND ND ND ND ND ND ND ND ND ND ND ND

1,2-Dichlorobenzene 500 1,000 3.1 ND ND ND ND ND ND ND ND 0.027 ND ND ND ND ND ND ND ND ND

1,2,4-Trimethylbenzene 500* 1,000* 28* ND ND ND ND ND ND ND ND ND ND 0.16 0.39 ND ND ND ND ND ND

1,3,5-Trimethylbenzene 500* 1,000* 28* ND ND ND ND ND ND ND ND ND ND 0.15 0.36 ND ND ND ND ND ND

Benzene 21 200 0.2 ND ND ND ND ND ND ND ND ND ND 0.24 0.62 0.019 ND ND ND ND ND

Carbon Disulfide 500* 1,000* 8* ND ND ND ND ND 0.0076 0.013 ND ND ND ND ND ND ND ND ND ND ND

cis-1,2-Dichloroethene 500 1,000 14 ND ND ND 0.41 ND 0.0092 ND ND 0.0047 0.13 ND ND ND ND ND ND ND ND

Chloroethane 130* 1,000* 1.5* ND ND ND ND ND ND ND ND ND 0.15 ND ND ND ND ND ND ND ND

Ethylbenzene 500 1,000 10.1 ND ND ND ND ND ND ND ND ND ND 0.11 0.21 ND ND ND ND ND ND

Isopropylbenzene 500* 1,00* 5* ND ND ND ND ND ND ND ND ND ND ND 0.14 ND ND ND ND ND ND

Methyl Ethyl Ketone 500 1,000 80 ND ND ND ND ND ND ND ND 0.059 ND 0.039 0.03 ND ND ND 0.073 ND ND

Naphthalene 1,000 2,500 56 ND ND ND ND ND ND ND ND ND ND 0.57 1.5 ND ND ND ND ND ND

Tetrachloroethene 12 110 1 ND ND 0.011 0.01 0.006 ND ND ND ND 0.0063 ND ND ND 0.016 ND ND ND ND

Total Xylenes 500 1,000 19.5 ND ND ND ND ND ND ND ND ND ND ND 0.34 ND ND ND ND ND ND

Trichloroethene 56 520 1 ND ND ND ND ND ND ND ND ND 0.011 ND ND ND ND ND ND ND ND

Vinyl chloride 0.32 3 0.4 ND ND ND 0.012 ND ND ND ND ND 0.091 ND ND ND ND ND ND ND ND

SVOCs (mg/kg)

1,000* 2,500* 84 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.1 ND NA

Acenaphthylene 1,000 2,500 84 ND ND ND ND 0.31 ND ND ND ND ND ND ND ND ND ND ND ND NA

Anthracene 1,000 2,500 400 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2.8 ND NA

Benzo(a)anthracene 1 7.8 1 0.32 ND ND ND 1.2 ND ND 0.39 ND ND ND ND ND 0.38 ND 9.3 0.92 NA

Benzo(a)pyrene 1 1 1 0.39 ND ND ND 1.2 ND ND 0.5 ND ND ND ND ND 0.43 ND 7.3 1.1 NA

Benzo(b)fluoranthene 1 7.8 1 0.28 ND ND ND 1.3 ND ND 0.45 ND ND ND ND ND 0.38 ND 8.9 1.3 NA

Benzo(g,h,i)perylene 8.4* 78* 1* ND ND ND ND 0.92 ND ND 0.48 ND ND ND ND ND 0.31 ND 4.9 0.79 NA

Benzo(k)fluoranthene 8.4 78 1 0.35 ND ND ND 1.1 ND ND 0.39 ND ND ND ND ND 0.36 ND 6.8 1.1 NA

Benzyl butyl phthalate 1,000 2,500 200 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA

Bis(2-ethylhexyl)phthalate 44 410 11 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.59 NA

Carbazole 31* 290* 1* ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2.6 ND NA

Chrysene 84* 780* 1* 0.36 ND ND ND 1.2 ND ND 0.44 ND ND ND ND ND 0.39 ND 11 1.4 NA

Dibenz(a,h)anthracene 1* 1* 1* ND ND ND ND 0.28 ND ND ND ND ND ND ND ND ND ND 1.7 ND NA

Dibenzofuran 68* 1,000* 1.4* ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.67 ND NA

Fluoranthene 1,000 2,500 56 ND ND ND ND 1.9 ND ND 0.69 ND ND ND ND ND 0.74 ND 24 3.2 NA

Fluorene 1,000 2,500 56 0.55 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.9 ND NA

Indeno(1,2,3-cd)pyrene 1* 7.8* 1* ND ND ND ND 1.1 ND ND 0.51 ND ND ND ND ND 0.37 ND 5.8 0.93 NA

2-Methylnaphthalene 270* 1,000* 5.6* ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA

Naphthalene 1,000 2,500 56 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA

Isophorone 640* 2,500* 7.4* ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA

Phenanthrene 1,000 2,500 40 ND ND ND ND 0.41 ND ND ND ND ND ND ND ND ND ND 17 ND NA

Pyrene 1,000 2,500 40 0.61 ND ND ND 1.7 ND ND 0.7 ND ND ND ND ND 0.72 ND 17 2.5 NA

Total RCRA 8 Metals (mg/kg)

Arsenic 10 10 -- 3.04 1.8 2.57 1.73 5.62 1.44 1.12 3.88 7.35 1.91 3.78 3.7 2.7 23.3 4.6 52.7 6.84 NA

Barium 4,700 140,000 -- 17.5 7.41 26.2 6.97 26 6.48 5.95 22.6 32.8 6.74 11.7 12.4 9.71 27.1 31.3 95.1 12.1 NA

Cadmium 34 1,000 -- ND ND ND ND ND ND ND ND 2.9 ND ND ND ND 0.37 ND 2.87 1.21 NA

Chromium, Total 100** 100** -- 16.1 9.56 13.3 8.75 22.4 10.1 11.8 17.4 31.8 14.5 13.7 12.7 12.7 33 30.3 50.3 21.7 NA

Lead 400 1,000 -- 75.4 2.74 5.48 3.64 42 2.93 2.9 25.3 22.1 3.76 10 14.6 2.68 45.9 7.57 48.2 29 NA

Mercury 20 610 -- ND ND ND ND ND ND ND ND ND ND 0.03 ND ND ND ND ND 0.1 NA

SPLP RCRA 8 Metals (mg/L)

Arsenic -- -- 0.5 0.005 ND ND ND ND ND ND 0.005 0.006 ND 0.014 0.013 0.006 0.035 0.028 0.027 0.006 NA

Barium -- -- 10 0.053 0.02 0.029 0.023 0.044 0.045 0.013 0.046 0.026 0.014 0.033 0.033 0.018 0.025 0.047 0.081 0.014 NA

Lead -- -- 0.15 0.022 ND ND ND 0.013 ND ND 0.02 ND ND ND ND ND ND ND ND 0.012 NA

PCBs (mg/kg) 1 10 0.005 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA

Pesticides (mg/kg)

4,4' - DDT 1.8* 17* 0.02* ND ND ND ND ND ND ND 0.012 ND ND ND ND ND ND ND ND ND NA

Corrosivity(Positive/Negative) -- -- -- Negative Negative Negative Negative Negative Negative Negative Negative Negative Negative Negative Negative Negative Negative Negative Negative Negative NA

Reactivity(Positive/Negative) -- -- -- Negative Negative Negative Negative Negative Negative Negative Negative Negative Negative Negative Negative Negative Negative Negative Negative Negative NA

Ignitability (degrees F) -- -- -- >200 >200 >200 >200 >200 >200 >200 >200 >200 >200 >200 >200 >200 >200 >200 >200 >200 NA

pH (SU) -- -- -- 6.47 6.44 6.88 6.48 7.60 7.11 7.21 7.95 7.21 7.13 7.15 7.67 6.80 9.05 7.47 7.87 7.64 NA

Reactivity Cyanide (mg/kg) -- -- -- ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA

Reactivity Sulfide (mg/kg) -- -- -- ND ND ND ND ND ND ND ND 49 ND ND ND ND ND ND 21 276 NA

CTDEEP = Connecticut Department of Energy and Environmental Protection NA = Not Analyzed

RSR = Remediation Standard Regulations NE = Not Established

RES DEC = Residential Direct Exposure Criteria * = published 2015 numeric criteria for additional polluting substances not established in 2013 RSRs

I/C DEC = Industrial-Commercial Direct Exposure Criteria ** = hexavalent chromium criteria

GB PMC = GB Pollutant Mobility Criteria *** = EPA Hazardous Regulatory Limit

mg/kg = milligrams per kilogram -- = criteria does not apply

mg/L = milligrams per liters Only detected compounds are listed on table

ND = Not detected above laboratory reporting limits Shade/Bold

Concentration of Compound in Sample

= Exceeds Numeric Criteria

ETPH (mg/kg)

Acenaphthene

Parameters

CTDEEP RSR

Numeric Criteria

I/C DECRES DEC GB PMC

BL Companies Project No. 18EC0070 June 2019

Table 3

Groundwater Analytical Results




TMW-1 DUP TMW-2 TRIP BLANK FIELD BLANK

4/30/2019 4/30/2019 4/30/2019 4/30/2019 4/30/2019

5 100 ND ND ND NA ND

50 5,000 2.8 ND 1,016.5 ND ND

cis-1,2-Dichloroethene NE NE 2.8 ND 260 ND ND

1,1,1-Trichloroethane NE NE ND ND 6.6 ND ND

1,1-Dichloroethane NE NE ND ND 230 ND ND

1,1-Dichloroethene NE NE ND ND 8.3 ND ND

1,2,4-Trimethylbenzene NE NE ND ND 5.4 ND ND

1,2-Dichlorobenzene NE NE ND ND 4.8 ND ND

1,2-Dichloroethane NE NE ND ND 1 ND ND

Chloroethane NE NE ND ND 260 ND ND

Ethylbenzene NE NE ND ND 13 ND ND

Isopropylbenzene NE NE ND ND 1.3 ND ND

m&p-Xylene NE NE ND ND 3.1 ND ND

Methylene chloride NE NE ND ND 2.2 ND ND

n-Propylbenzene NE NE ND ND 1.8 ND ND

o-Xylene NE NE ND ND 10 ND ND

Tetrachloroethene NE NE ND ND 20 ND ND

Toluene NE NE ND ND 9.2 ND NDNE NE ND ND 13.1 ND ND

Trichloroethene NE NE ND ND 35 ND ND

Trichlorotrifluoroethane NE NE ND ND 9.9 ND ND

Vinyl chloride NE NE ND ND 230 ND ND

1,2-Dichlorobenzene NE NE ND ND 2.6 NA ND

Bis(2-ethylhexyl)phthalate 5.9 NE ND ND 1.4 NA ND

Pyrene NE NE ND ND ND NA ND

Total phthalates 100 2,000 ND ND 1.4 NA ND

5 500 ND ND 4 NA ND

Dieldrin 0.0042 10 0.024 ND 0.018 NA ND

* * ND ND ND NA

Total Metals (µg/L)

Copper 48 1,000 6 7 ND NA ND

Lead 9.8 100 3 3 ND NA ND

Zinc 322 1,000 8 8 ND NA 13

Dissolved Metals (µg/L)

Copper 48 1,000 ND ND ND NA ND

Lead 9.8 100 2 ND 4 NA ND

Zinc 322 1,000 3 4 6 NA ND

MCL = maximum concentration limits listed in the DEEP General Permit for Discharge of Groundwater

mg/L = milligrams per liter

µg/L = micrograms per liter

-- = criteria does not apply

ND = Not Detected above the Laboratory Reporting Detection Limit

NE = None Established

* = Limits Established for Individual Compounds

** = Detected in the field blank indicating potential cross-contamination

Only detected compounds are listed on table

Shade/Bold

PCBs (µg/L)

Pesticides (µg/L)

= Exceeds Numeric Criteria

ETPH (mg/L)

VOCs (µg/L)

SVOCs (µg/L)

Total PAHs

Total Xylenes

Parameters

Surface Water Sanitary Sewer

General Permit MCLs Concentration of Compound in Sample

BL Companies Project No. 18EC0070 June 2019

APPENDIX C

BORING LOGS

SOIL BORING LOG Sheet 1 of 8

Cummins Envirotech Inc. Job Name/Number: Turtle Creek 18EC0070

Boring ID: B-1 6620 DT LOGGED BY: Wesley Johnson

Direct Push DRILLING DATE(S): 04/30/19

Recovery (ft)P.I.D.

(ppm)Depth

Interval

0.5

1

1.5

2

2.5

3

3.5

4

4.5

5

5.5

6

6.5

7

7.5

8

8.5

9

9.5

10

3.1

4.0

Sample

collected

1-3' bgs.

Sample

collected

7.7-9' bgs.

0-0.4' ASPHALT.

0.4-3.1'Brown fine to coarse SAND, little silt, trace fine to coarse sub-rounded gravel,

dense, dry.

0.0

0.1

0.2

End of exploration at 10' bgs.

3.1-5' No recovery.

5-6.4'Brown fine to coarse SAND, little silt, trace fine to coarse sub-rounded gravel,

dense, wet at 6' bgs.

6.4-7.7'Dark brown SILT, trace organics, trace fine to coarse sand, medium dense,

wet, methane/organic odor.

7.7-9.0'Brown fine to coarse SAND, little silt, trace fine to coarse sub-rounded gravel,

dense, saturated.

9.0-10' No recovery.

COMMENTSSample ID and

DepthDepth (ft) SOIL DESCRIPTION

Drilling Company:

Drill Rig:

Drilling Method:

Proportions Used:

Trace = 1 to 10%

Little = 10 to 20%

Some = 20 to 30%

And = 30 to 50%

BL Companies, Inc.



(203) 630-1406





Recovery (ft)P.I.D.

(ppm)Depth

Interval

0.5

1

1.5

2

2.5

3

3.5

4

4.5

5

5.5

6

6.5

7

7.5

8

8.5

1.0 9

9.5

10No recovery.

2.9-5'

2.9

Sample

collected

1-2.9' bgs.

0-0.5' Brown SILT, trace organics, trace fine to coarse sand, medium dense, dry.

0.5-2.9'Brown fine to coarse SAND, little silt, trace fine to coarse sub-angular gravel,

medium dense, wet at 1.3' bgs.

0.0-0.4

5-9.8'''Brown to grey/brown fine to coarse SAND, trace silt, medium dense,

saturated.


COMMENTS

0.4

No recovery.

0.0

9.8-10'

4.8

Drilling Company:

Drill Rig:

Drilling Method:

Sample ID and


Sample

collected

8-9.8' bgs.

Proportions Used:

Trace = 1 to 10%

Little = 10 to 20%

Some = 20 to 30%

And = 30 to 50%

BL Companies, Inc.



(203) 630-1406



Boring ID: B-3/TMW-1 6620 DT LOGGED BY: Wesley Johnson


Recovery (ft)P.I.D.

(ppm)Depth

Interval

0.5

1

1.5

2

2.5

3

3.5

4

4.5

5

5.5

6

6.5

7

7.5

8

8.5

9

9.5

10

2.2

3.8

Sample

collected

0.4-2.2' bgs.

Sample

collected

6-8' bgs.

0.0

0.0

5.8-7.1'Dark brown fine to coarse SAND, little silt, trace fine to coarse sub-angular

gravel, medium dense, wet, faint methane/organic odor.

7.1-8.8' Brown fine to coarse SAND, trace silt, medium dense, saturated.

0.4-2.2'Brown to reddish brown fine to coarse SAND, little silt, little fine to coarse

sub-angular gravel, dense, slightly damp.

1" temporary monitoring well set at 13.5' bgs

with 10' of screen. DTW=6.37' bgs.

2.2-5' No recovery.

0-0.4'Brown SILT, trace organics, trace fine to coarse sand, medium dense,

slightly damp.

5-5.8'Reddish brown fine to coarse SAND, little silt, little fine to coarse sub-angular

gravel, dense, wet.


COMMENTS

Drilling Company:

Drill Rig:

Drilling Method:

Sample ID and


Proportions Used:

Trace = 1 to 10%

Little = 10 to 20%

Some = 20 to 30%

And = 30 to 50%

BL Companies, Inc.



(203) 630-1406





Recovery (ft)P.I.D.

(ppm)Depth

IntervalCOMMENTS

Drilling Company:

Drill Rig:

Drilling Method:

Sample ID and


10.5

11

11.5

12

12.5

13

13.5

14

14.5

15

4.4 0.0

Sample

collected

11-13' bgs.Brown/grey brown fine to coarse SAND, trace silt, medium dense, saturated.

No recovery.


10-14.4'

14.4-15'

Proportions Used:

Trace = 1 to 10%

Little = 10 to 20%

Some = 20 to 30%

And = 30 to 50%

BL Companies, Inc.



(203) 630-1406





Recovery (ft)P.I.D.

(ppm)Depth

Interval

0.5

1

1.5

2

2.5

3

3.5

4

4.5

5

5.5

6

6.5

7

7.5

8

8.5

9

9.5

10

Sample

collected

0.4-1.8' bgs.

Sample

collected

5.4-7.4' bgs.

0.0

0.1

2.4

2.4

Grey/ black clayey SILT, trace fine to coarse sand, medium dense, wet,

water stained black.

Grey/black SILT, trace fine sand, medium dense, wet with water stained

black.

5.8-7'Black fine to coarse angular GRAVEL, trace silt, dense, saturated with water

stained black, faint unidentified odor.

No recovery.

CONCRETE, dry.

Brown fine to coarse SAND, little fine to coarse sub-angular gravel, trace silt,

medium dense, wet.

7-7.4'

0.4-1.8'

1.8-2.2'

5-5.5'

5.5-5.8'

2.2-2.4' - Brown fine to coarse SAND, little fine to coarse sub-angular gravel,

trace silt, medium dense, damp.

2.4-5' - No recovery.

Brown fine to coarse SAND, little fine to coarse sub-angular gravel, trace silt,

medium dense, dry.

7.4-10'

COMMENTS

0-0.4'Brown SILT, little grass/roots, trace fine to coarse SAND, medium dense,

dry.

1" temporary monitoring well set

at 14' with 10' of screen. DTW = 4.5' bgs.

Drilling Company:

Drill Rig:

Drilling Method:

Sample ID and


Proportions Used:

Trace = 1 to 10%

Little = 10 to 20%

Some = 20 to 30%

And = 30 to 50%

BL Companies, Inc.



(203) 630-1406





Recovery (ft)P.I.D.

(ppm)Depth

IntervalCOMMENTS

Drilling Company:

Drill Rig:

Drilling Method:

Sample ID and


10.5

11

11.5

12

12.5

13

13.5

14

14.5

15

Grey/brown fine SAND, some silt, medium dense, saturated, faint

unidentified odor.10-13.8'4.0

Sample

collected

11.8-13.8' bgs.

3.8



Proportions Used:

Trace = 1 to 10%

Little = 10 to 20%

Some = 20 to 30%

And = 30 to 50%

BL Companies, Inc.



(203) 630-1406





Recovery (ft)P.I.D.

(ppm)Depth

Interval

0.5

1

1.5

2

2.5

3

3.5

4

4.5

5

5.5

6

6.5

7

7.5

8

8.5

9

9.5

10

0.2

Sample

collected

1.7-2.8' bgs.

Duplicate

sample

collected.

4.8

Sample

collected

5-7' bgs.

2.8

0.1

0.1


0.4-2.8'

Brown fine to coarse SAND, little fine to coarse sub-rounded gravel, trace

silt, dense, slightly damp at 1.2' bgs. Soil stained gray, with petroleum odor,

at 1.7-2.8' bgs.

7.4-9.8'

9.8-10'

2.8-5' No recovery.

5-7.4'Grey brown fine to coarse SAND, trace fine to coarse sub-rounded gravel,

trace silt, medium dense, wet, faint petroleum odor.

Grey clayey SILT, trace organics, medium dense, wet, methane odor.

No recovery.

COMMENTS

0.0-0.4' Dark brown fine to coarse SAND, some silt, little mulch, medium dense, dry.

Drilling Company:

Drill Rig:

Drilling Method:

Sample ID and


Proportions Used:

Trace = 1 to 10%

Little = 10 to 20%

Some = 20 to 30%

And = 30 to 50%

BL Companies, Inc.



(203) 630-1406





Recovery (ft)P.I.D.

(ppm)Depth

Interval

0.5

1

1.5

2

2.5

3

3.5

4

4.5

5

5.5

6

6.5

7

7.5

8

8.5

9

9.5

10

Sample

collected

5.6-7.6' bgs.

2.1

Sample

collected

0.4-1.7' bgs.

2.7

0.7

0.2

6-22.0

36.0

6-22.0

5.6-7.7'


No recovery.

Grey/brown fine to coarse angular GRAVEL, trace fine to coarse sand, trace

silt, medium dense, wet.

Grey/brown fine to coarse angular GRAVEL, trace fine to coarse sand, trace

silt, medium dense, wet.


COMMENTS

0.0 0-0.4'Brown SILT, little organics, trace fine to coarse sand, trace asphalt, medium

dense, slightly damp.

Dark brown SILT, little organics, trace fine to coarse sand, medium dense,

damp, methane/organic odor.

0.4-1.7'

1.7-2.1'

2.1-5'

5-5.6'

Brown fine to coarse SAND, some fine to coarse sub-angular gravel, trace

silt, dense, damp, wet at 1.5' bgs.

Drilling Company:

Drill Rig:

Drilling Method:

Sample ID and


Proportions Used:

Trace = 1 to 10%

Little = 10 to 20%

Some = 20 to 30%

And = 30 to 50%

BL Companies, Inc.



(203) 630-1406

APPENDIX D

LABORATORY ANALYTICAL REPORT

Report Date:

09-May-19 16:45

ü Final Report

Revised Report

Laboratory Report

SC54611

BL Companies


Meriden, CT 06450

Attn: Joy Kloss

Project:

Project #:

Turtle Creek - Milford, CT

18EC0070

I attest that the information contained within the report has been reviewed for accuracy and checked against the quality control

requirements for each method. These results relate only to the sample(s) as received.

All applicable NELAC requirements have been met.

Massachusetts # M-MA138/MA1110

Connecticut # PH-0777

Florida # E87936

Maine # MA138

New Hampshire # 2972/2538

New Jersey # MA011

New York # 11393

Pennsylvania # 68-04426/68-02924

Rhode Island # LAO00348

USDA # P330-15-00375

Vermont # VT-11393

Eurofins Spectrum Analytical holds primary NELAC certification in the State of New York for the analytes as indicated with an X in the

"Cert." column within this report. Please note that the State of New York does not offer certification for all analytes. Please refer to our

website for specific certification holdings in each state.

Please note that this report contains 231 pages of analytical data plus Chain of Custody document(s). When the Laboratory Report is

indicated as revised, this report supersedes any previously dated reports for the laboratory ID(s) referenced above. Where this report

identifies subcontracted analyses, copies of the subcontractor's test report are available upon request. This report may not be

reproduced, except in full, without written approval from Eurofins Spectrum Analytical, Inc.

Eurofins Spectrum Analytical, Inc. is a NELAC accredited laboratory organization and meets NELAC testing standards. Use of the NELAC logo

however does not insure that Eurofins Spectrum Analytical, Inc. is currently accredited for the specific method or analyte indicated. Please refer to

our "Quality" web page at www.spectrum-analytical.com for a full listing of our current certifications and fields of accreditation. States in which

Eurofins Spectrum Analytical, Inc. holds NELAC certification are New York, New Hampshire, New Jersey, Pennsylvania and Florida. All analytical

work for Volatile Organic and Air analysis are transferred to and conducted at our 830 Silver Street location (PA-68-04426).

Please contact the Laboratory or Technical Director at 800-789-9115 with any questions regarding the data contained in this laboratory report.

Eurofins Spectrum Analytical, Inc. 830 Silver Street T | 413-789-9018

Agawam, MA 01001 F | 413-789-4076

www.EurofinsUS.com/Spectrum Page 1 of 231

Authorized by:

Dawn WojcikLaboratory Director

Sample Summary

Work Order:

Project:

Project Number:

SC54611

Turtle Creek - Milford, CT

18EC0070

Laboratory ID Client Sample ID Matrix Date Sampled Date Received

SC54611-01 B-1 1-3' Soil 30-Apr-19 11:10 01-May-19 12:27

SC54611-02 B-1 7.7-9' Soil 30-Apr-19 11:20 01-May-19 12:27

SC54611-03 B-2 1-2.9' Soil 30-Apr-19 12:30 01-May-19 12:27

SC54611-04 B-2 8-9.8' Soil 30-Apr-19 12:45 01-May-19 12:27

SC54611-05 B-3 0.4-2.2' Soil 30-Apr-19 13:10 01-May-19 12:27

SC54611-06 B-3 6-8' Soil 30-Apr-19 13:20 01-May-19 12:27

SC54611-07 B-3 11-13' Soil 30-Apr-19 13:40 01-May-19 12:27

SC54611-08 B-4 0.4-1.8' Soil 30-Apr-19 10:00 01-May-19 12:27

SC54611-09 B-4 5.4-7.4' Soil 30-Apr-19 10:30 01-May-19 12:27

SC54611-10 B-4 11.8-13.8' Soil 30-Apr-19 10:45 01-May-19 12:27

SC54611-11 B-5 1.7-2.8' Soil 30-Apr-19 09:10 01-May-19 12:27

SC54611-12 B-5 5-7' Soil 30-Apr-19 09:30 01-May-19 12:27

SC54611-13 B-6 0.4-1.7' Soil 30-Apr-19 14:15 01-May-19 12:27

SC54611-14 B-6 5.6-7.6' Soil 30-Apr-19 14:30 01-May-19 12:27

SC54611-15 SED-1 Sediment 30-Apr-19 16:00 01-May-19 12:27

SC54611-16 SED-2 Sediment 30-Apr-19 15:50 01-May-19 12:27

SC54611-17 DUP Soil 30-Apr-19 00:00 01-May-19 12:27

SC54611-18 Trip Blank Trip Blank 30-Apr-19 00:00 01-May-19 12:27

SC54611-19 TMW-1 Ground Water 30-Apr-19 16:20 01-May-19 12:27

SC54611-20 TMW-2 Ground Water 30-Apr-19 11:45 01-May-19 12:27

SC54611-21 DUP Ground Water 30-Apr-19 00:00 01-May-19 12:27

SC54611-22 Field Blank Ground Water 30-Apr-19 17:00 01-May-19 12:27

SC54611-23 Trip Blank Trip Blank 30-Apr-19 00:00 01-May-19 12:27

This laboratory report is not valid without an authorized signature on the cover page .

Page 2 of 23109-May-19 16:45

Reasonable Confidence Protocols

Laboratory Analysis

QA/QC Certification Form

Laboratory Name: Eurofins Spectrum Analytical, Inc. Client: BL Companies

Project Location: Turtle Creek - Milford, CT Project Number: 18EC0070

Sampling Date(s): Laboratory Sample ID(s):

SC54611-01 through SC54611-234/30/2019

RCP Methods Used:

CT ETPH

CTETPH 8015D

SW6010D

SW6010D (SPLP)

SW6010D dissolved

SW7470A (SPLP)

SW7471B

SW8081B

SW8082A

SW8260C

SW8270D

SW8270D (SIM)

SW846 1312

SW846 1312/6010C

SW846 1312/7470A

SW846 6010C

SW846 7471B

SW846 8081B

SW846 8082A

SW846 8260C

SW846 8270D

SW846 8270D SIM

1 NoYes

For each analytical method referenced in this laboratory report package, were all specified QA/QC

performance criteria followed, including the requirement to explain any criteria falling outside of acceptable

guidelines, as specified in the CT DEP method-specific Reasonable Confidence Protocol documents?ü

Were the method specified preservation and holding time requirements met?1A ü Yes No

VPH and EPH methods only: Was the VPH or EPH method conducted without significant modifications

(see Section 11.3 of respective RCP methods)?1BYes No

Were all samples received by the laboratory in a condition consistent with that described on the associated

chain-of-custody document(s)?2 ü Yes No

Were samples received at an appropriate temperature? Yes No3 ü

Were all QA/QC performance criteria specified in the Reasonable Confidence Protocol documents

achieved?4 ü Yes No

a) Were reporting limits specified or referenced on the chain-of-custody?

b) Were these reporting limits met?5

Yes No

Yes No

ü

For each analytical method referenced in this laboratory report package, were results reported for all

constituents identified in the method-specific analyte lists presented in the Reasonable Confidence Protocol

documents?

6 Yes Noü

Are project-specific matrix spikes and laboratory duplicates included in this data set?7 ü Yes No


Page 3 of 23109-May-19 16:45

Note: For all questions to which the response was "No" (with the exception of question #7), additional information must be

provided in an attached narrative. If the answer to question #1, #1A, or #1B is "No", the data package does not meet

the requirements for "Reasonable Confidence."

I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal

inquiry of those responsible for obtaining the information contained in this analytical report, such information is accurate and complete.

Dawn E. Wojcik

Laboratory Director

Date: 5/9/2019


Page 4 of 23109-May-19 16:45

CASE NARRATIVE:

Data has been reported to the RDL. This report excludes estimated concentrations detected below the RDL and above the MDL

(J-Flag).

The samples were received 0.7 degrees Celsius, please refer to the Chain of Custody for details specific to temperature upon receipt.

An infrared thermometer with a tolerance of +/- 1.0 degrees Celsius was used immediately upon receipt of the samples.

VOA vials preserved with deionized water were received frozen upon custody transfer to laboratory representative.

Low level VOC soil samples submitted in DI water or in an encore sampler were frozen on 5/1/2019 at 12:27.

If a Matrix Spike (MS), Matrix Spike Duplicate (MSD) or Duplicate (DUP) was not requested on the Chain of Custody, method

criteria may have been fulfilled with a source sample not of this Sample Delivery Group. If method or program required

MS/MSD/Dup were not performed, sufficient sample was not provided to the laboratory.

Required site-specific Matrix Spike/Matrix Spike Duplicate (MS/MSD) must be requested by the client and sufficient sample must be

submitted for the additional analyses. Samples submitted with insufficient volume/weight will not be analyzed for site specific

MS/MSD, however a batch MS/MSD may be analyzed from a non-site specific sample.

CTDEP has published a list of analytical methods which provides a series of recommended protocols for the acquisition , analysis and

reporting of analytical data in support of decisions being made utilizing the Reasonable Confidence Protocol (RCP). "Reasonable

Confidence" can be established only for those methods published by the CTDEP in the RCP guidelines. The compounds and/or

elements reported were specifically requested by the client on the Chain of Custody and in some cases may not include the full analyte

list as defined in the method. Regulatory limits may not be achieved if specific method and/or technique was not requested on the

Chain of Custody.

The CTDEP RCP requests that "all non-detects and all results below the reporting limit are reported as ND (Not Detected at the

Specified Reporting Limit)". All non-detects and all results below the reporting limit are reported as "<" (less than) the reporting limit

in this report.

If no reporting limits were specified or referenced on the chain-of-custody the laboratory's practical quantitation limits were applied.

Tetrachloro-m-xylene is recommended as a surrogate by the CTDEP RCP for the following SW846 Methods 8081, 8082 and 8151.

Eurofins Spectrum Analytical, Inc. uses Tetrachloro-m-xylene as the Internal Standard for these methods and

Dibromooctaflourobiphenyl as the surrogate.

According to CTDEP RCP Quality Assurance and Quality Control Requirements for VOCs by method 8260, SW-846 version 1,

7/28/05 Table 1A, recovery for some VOC analytes have been deemed potentially difficult.

All VOC soils samples submitted and analyzed in methanol will have a minimum dilution factor of 50. This is the minimum amount of

solvent allowed on the instrumentation without causing interference. Soils are run on a manual load instrument. 100ug of sample

(MEOH) is spiked into 5ml DI water along with the surrogate and added directly onto the instrument. Additional dilution factors may

be required to keep analyte concentration within instrument calibration range.

For this work order, the reporting limits have not been referenced or specified.

Analyses for Total Hardness, pH, and Total Residual Chlorine fall under the state of Pennsylvania code Chapter 252.6 accreditation by

rule.


Page 5 of 23109-May-19 16:45

Reactivity (40 CFR 261.23) Case Narrative:

These samples do not exhibit the characteristics of reactivity as defined in 40 CFR 261.23, sections (1), (2) and (4); however, Eurofins

Spectrum Analytical, Inc. does not test for detonation, explosive reaction or potential, or forbidden explosives as defined in 40 CFR

261.23, sections (3), (6), (7) and (8).

Reactive sulfide and cyanide are tested at a pH of 2 and not tested at all conditions between pH 2 and12.5 as stated in 40 CFR 261.23,

section (5); thus reactive cyanide and sulfide results as reported in this document can not be used to support the nonreactive properties

of these samples.

The responsibility falls on the generator to use knowledge of the waste to determine if the waste meets or does not meet the descriptive,

prose definition of reactivity.


Page 6 of 23109-May-19 16:45

SDG CommentsMetals Analysis:

The client requested a site specific list of elements which is shorter than the 6010 RCP list

8270 Semi-volatile Organics:(Grond Water)

The sample was extracted and analyzed via 8270 selective ion monitoring (SIM) as well as 8270 full scan.

Due to a suppression of the last internal standard in the low level analysis, all affected compounds are reported from the high

level analysis. This resulted in elevated reporting limits for one or more analytes.

Sample(s) required a dilution for Semivolatiles due to a matrix interference and/or the presence of a large amount of non-target

material in the sample. This resulted in elevated reporting limits that exceed the requested criteria for one or more analytes.

The holding time for pH is immediate. The sample was analyzed in the laboratory on receipt and may be considered out of hold.

Cyanide NarrationWere all QA/QC performance criteria specified in the Reasonable Confidence Protocol documents achieved? Yes.

Instrument:CD05119, CD05120, CD05121, CD05122, CD05123, CD05124, CD05125, CD05126, CD05127, CD05128, CD05129, CD05130, CD05131,

CD05132, CD05133, CD05134, CD05135

LACHAT 05/03/19-1 Dustin Harrison, Greg Danielewski, Chemist 05/03/19

The samples were distilled in accordance with the method.

The initial calibration met criteria.

The calibration check standards (ICV,CCV) were within 15% of true value and were analyzed at a frequencey of one per ten

samples.

The continuing calibration blanks (ICB,CCB) had concentrations less than the reporting level.

The method blank, laboratory control sample (LCS), and matrix spike were distilled with the samples.

QC (Batch Specific):CD05119, CD05120, CD05121, CD05122, CD05123, CD05124, CD05125, CD05126, CD05127, CD05128, CD05129, CD05130, CD05131,

CD05132, CD05133, CD05134, CD05135

Batch 477480 (CD04770)

All LCS recoveries were within 80 - 120 with the following exceptions: None.

Additional: LCS acceptance range is 80-120% for soils MS acceptance range 75-125% for soils

ETPH NarrationWere all QA/QC performance criteria specified in the Reasonable Confidence Protocol documents achieved? Yes.

Instrument:CD05131, CD05138, CD05139, CD05140, CD05141

AU-FID1 05/02/19-1 Keith Aloisa, Chemist 05/02/19

The initial calibration (ETPH426I) RSD for the compound list was less than 30% except for the following compounds: None.

As per section 7.2.3, a discrimination check standard was run (502A003_2) and contained the following outliers: None.

ETPH NarrationThe continuing calibration %D for the compound list was less than 30% except for the following compounds:

Samples: CD05131

Preceding CC 502A033 - None.

Succeeding CC 502A047 - Pentacosane 32%H (30%)CD05133, CD05134

AU-FID21 05/02/19-1 Keith Aloisa, Chemist 05/02/19



The continuing calibration %D for the compound list was less than 30% except for the following compounds:None.CD05120, CD05121, CD05122, CD05124, CD05125, CD05129, CD05130, CD05132

AU-XL1 05/02/19-1 Keith Aloisa, Chemist 05/02/19



The continuing calibration %D for the compound list was less than 30% except for the following compounds:None.CD05128




The continuing calibration %D for the compound list was less than 30% except for the following compounds:None.CD05119, CD05123, CD05126, CD05127, CD05135




The continuing calibration %D for the compound list was less than 30% except for the following compounds:None.

QC (Batch Specific):CD05120

Batch 477139 (CD04771)


All LCSD recoveries were within 60 - 120 with the following exceptions: None.

All LCS/LCSD RPDs were less than 30% with the following exceptions: None.

Additional surrogate criteria: LCS acceptance range is 60-120% MS acceptance range 50-150%. The ETPH/DRO LCS has been

normalized based on the alkane calibration.


Page 7 of 23109-May-19 16:45

CD05138, CD05139, CD05140, CD05141

Batch 477197 (CD04789)




A LCS and LCS Duplicate were performed instead of a matrix spike and matrix spike duplicate.



QC (Site Specific):

ETPH NarrationCD05119, CD05121, CD05122, CD05123, CD05124, CD05125, CD05126, CD05127, CD05128, CD05129, CD05130, CD05131, CD05132,

CD05133, CD05134, CD05135

Batch 477191 (CD05122)




All MS recoveries were within 50 - 150 with the following exceptions: None.

All MSD recoveries were within 50 - 150 with the following exceptions: None.

All MS/MSD RPDs were less than 30% with the following exceptions: None.



Mercury NarrationWere all QA/QC performance criteria specified in the analytical method achieved? No.

QC Batch 477261 (Samples: CD05120, CD05121, CD05122, CD05123, CD05124, CD05125, CD05126, CD05127, CD05128,

CD05129, CD05130, CD05131, CD05132, CD05133, CD05134, CD05135): -----

The LCS/LCSD RPD exceeds the method criteria for one or more analytes, therefore there may be variability in the

reported result. (Mercury)

Instrument:CD05119, CD05120, CD05121, CD05122, CD05123, CD05124, CD05125, CD05126, CD05127, CD05128, CD05129, CD05130, CD05131,

CD05132, CD05133, CD05134, CD05135

MERLIN 05/02/19 08:07 Rick Schweitzer, Chemist 05/02/19

The method preparation blank contains all of the acids and reagents as the samples; the instrument blanks do not.

The initial calibration met all criteria including a standard run at or below the reporting level.

All calibration verification standards (ICV, CCV) met criteria.

All calibration blank verification standards (ICB, CCB) met criteria.

The matrix spike sample is used to identify spectral interference for each batch of samples, if within 85-115%, no interference is

observed and no further action is taken.

The following Initial Calibration Verification (ICV) compounds did not meet criteria: None.

The following Continuing Calibration Verification (CCV) compounds did not meet criteria: None.CD05119, CD05120, CD05121, CD05122, CD05123, CD05124, CD05125, CD05126, CD05127, CD05128, CD05129, CD05130, CD05131,

CD05132, CD05133, CD05134, CD05135

MERLIN 05/03/19 07:42 Rick Schweitzer, Chemist 05/03/19

The method preparation blank contains all of the acids and reagents as the samples; the instrument blanks do not.

The initial calibration met all criteria including a standard run at or below the reporting level.

All calibration verification standards (ICV, CCV) met criteria.

All calibration blank verification standards (ICB, CCB) met criteria.

The matrix spike sample is used to identify spectral interference for each batch of samples, if within 85-115%, no interference is

observed and no further action is taken.


The following Continuing Calibration Verification (CCV) compounds did not meet criteria: None.

QC (Batch Specific):

Mercury NarrationCD05119

Batch 477253 (CD04926)




Additional Mercury criteria: LCS acceptance range for waters is 80-120% and for soils is 70-130%. MS acceptance range is 75-

125%.CD05119, CD05120, CD05121, CD05122, CD05123, CD05124, CD05125, CD05126, CD05127, CD05128, CD05129, CD05130, CD05131,

CD05132, CD05133

Batch 477274 (CD05046)



125%.CD05134, CD05135

Batch 477275 (CD04770)




Page 8 of 23109-May-19 16:45

125%.

QC (Site Specific):CD05120, CD05121, CD05122, CD05123, CD05124, CD05125, CD05126, CD05127, CD05128, CD05129, CD05130, CD05131, CD05132,

CD05133, CD05134, CD05135

Batch 477261 (CD05120)



All LCS/LCSD RPDs were less than 30% with the following exceptions: Mercury(31.3%)





125%.

ICP Metals NarrationWere all QA/QC performance criteria specified in the analytical method achieved? No.

QC Batch 477188 (Samples: CD05119, CD05120, CD05121, CD05122, CD05123, CD05124): -----

The Sample/Duplicate RPD exceeds the method criteria for one or more analytes, therefore there may be variability in the

reported result. (Lead)

Instrument:CD05119, CD05120, CD05121, CD05122, CD05123, CD05124

ARCOS 05/02/19 08:02 Emily Kolominskaya, Tina Hall, Chemist 05/02/19

Additional criteria for CCV and ICSAB:

ICP Metals NarrationSodium and Potassium are poor performing elements, the laboratory's in-house limits are 85-115% (CCV) and 70-130%

(ICSAB).The linear range is defined daily by the calibration range.



The following ICP Interference Check (ICSAB) compounds did not meet criteria: None.CD05125, CD05126, CD05127, CD05128, CD05129, CD05130, CD05131, CD05132, CD05133, CD05134, CD05135

ARCOS 05/03/19 07:43 Emily Kolominskaya, Tina Hall, Chemist 05/03/19

Additional criteria for CCV and ICSAB:

Sodium and Potassium are poor performing elements, the laboratory's in-house limits are 85-115% (CCV) and 70-130%

(ICSAB).The linear range is defined daily by the calibration range.



The following ICP Interference Check (ICSAB) compounds did not meet criteria: None.CD05119, CD05120, CD05121, CD05122, CD05123, CD05124, CD05125, CD05126, CD05127, CD05128, CD05129, CD05130, CD05131,

CD05132, CD05133, CD05134, CD05135, CD05138, CD05139, CD05140, CD05141

BLUE 05/02/19 08:13 Emily Kolominskaya, Tina Hall, Chemist 05/02/19


The continuing calibration standards met criteria for all the elements reported. The linear range is defined daily by the calibration

range.

The continuing calibration blanks were less than the reporting level for the elements reported.

The ICSA and ICSAB were analyzed at the beginning and end of the run and were within criteria.The linear range is defined daily

by the calibration range.



The following ICP Interference Check (ICSAB) compounds did not meet criteria: None.CD05139

BLUE 05/03/19 08:14 Emily Kolominskaya, Tina Hall, Chemist 05/03/19


The continuing calibration standards met criteria for all the elements reported. The linear range is defined daily by the calibration

range.

The continuing calibration blanks were less than the reporting level for the elements reported.

The ICSA and ICSAB were analyzed at the beginning and end of the run and were within criteria.The linear range is defined daily

by the calibration range.



The following ICP Interference Check (ICSAB) compounds did not meet criteria: None.

QC (Batch Specific):CD05138, CD05139, CD05140, CD05141

Batch 477208 (CD04790)

All LCS recoveries were within 75 - 125 with the following exceptions: None.CD05119, CD05120, CD05121, CD05122, CD05123, CD05124,

ICP Metals NarrationAll LCS recoveries were within 75 - 125 with the following exceptions: None.

QC (Site Specific):CD05119, CD05120, CD05121, CD05122, CD05123, CD05124


Page 9 of 23109-May-19 16:45

Batch 477188 (CD05119)


All MS recoveries were within 75 - 125 with the following exceptions: None.CD05138, CD05139, CD05140, CD05141

Batch 477214 (CD05138)


All MS recoveries were within 75 - 125 with the following exceptions: None.CD05125, CD05126, CD05127, CD05128, CD05129, CD05130, CD05131, CD05132, CD05133, CD05134, CD05135

Batch 477321 (CD05125)



PCB NarrationWere all QA/QC performance criteria specified in the Reasonable Confidence Protocol documents achieved? Yes.

Instrument:CD05138, CD05139, CD05140, CD05141

AU-ECD1 05/02/19-1 Saadia Chudary, Chemist 05/02/19

The initial calibration (PC416AI) RSD for the compound list was less than 20% except for the following compounds: None.

The initial calibration (PC416BI) RSD for the compound list was less than 20% except for the following compounds: None.

The continuing calibration %D for the compound list was less than 15% except for the following compounds:None.CD05119, CD05120, CD05121, CD05122, CD05123, CD05124, CD05125, CD05126, CD05127, CD05128, CD05129, CD05130, CD05133,

CD05134, CD05135




The continuing calibration %D for the compound list was less than 15% except for the following compounds:None.CD05131, CD05132






Batch 477222 (CD05298)


PCB NarrationAll LCSD recoveries were within 40 - 140 with the following exceptions: None.




CD05132, CD05133, CD05134, CD05135

Batch 477265 (CD05128)







PEST NarrationWere all QA/QC performance criteria specified in the Reasonable Confidence Protocol documents achieved? Yes.


AU-ECD4 05/02/19-1 Carol Wohlmuth, Chemist 05/02/19

The initial calibration (PS501AI) RSD for the compound list was less than 20% except for the following compounds: None.

The initial calibration (PS501BI) RSD for the compound list was less than 20% except for the following compounds: None.

The Endrin and DDT breakdown does not exceed 15% except for the following compounds:None.

The Endrin and DDT breakdown does not exceed the maximum of 20% except for the following compounds:None.

The continuing calibration %D for the compound list was less than 20% except for the following compounds:None.CD05119, CD05120, CD05121, CD05122, CD05123, CD05124, CD05125, CD05126, CD05128, CD05129, CD05130, CD05131, CD05132,

CD05133, CD05135

AU-ECD4 05/03/19-1 Keith Aloisa, Chemist 05/03/19





The continuing calibration %D for the compound list was less than 20% except for the following compounds:None.CD05127, CD05134

AU-ECD4 05/06/19-1 Keith Aloisa, Chemist 05/06/19



Page 10 of 23109-May-19 16:45






Batch 477223 (CD05138)

PEST NarrationCD05138, CD05139, CD05140, CD05141




A LCS and LCS duplicate were performed instead of a MS and MSD. Alpha and gamma chlordane were spiked and analyzed

instead of technical chlordane. Gamma chlordane recovery is reported as chlordane in the LCS and LCSD


CD05132, CD05133, CD05134, CD05135

Batch 477266 (CD05128)







SVOA NarrationWere all QA/QC performance criteria specified in the Reasonable Confidence Protocol documents achieved? No.

QC Batch 477192 (Samples: CD05119, CD05120, CD05121, CD05122, CD05123, CD05124, CD05125, CD05126, CD05127,

CD05128, CD05129, CD05130, CD05131, CD05132, CD05133, CD05134, CD05135): -----

One or more analytes is below the method criteria. A low bias for these analytes is possible. (2,4-Dinitrophenol)

The LCS/LCSD recovery is acceptable. One or more analytes in the site specific matrix spike recovery is below the

method criteria, therefore a low bias is likely. (Benzidine, Pyridine)

The QC recoveries for one or more analytes is below the method criteria. A slight low bias is likely. (Benzoic Acid)

QC Batch 477196 (Samples: CD05138, CD05139, CD05140, CD05141): -----

One or more analytes is below the method criteria. A low bias for these analytes is possible. (Benzoic acid)

Instrument:CD05123, CD05126, CD05129, CD05130, CD05131, CD05132, CD05133

CHEM05 05/02/19-1 Matt Richard, Chemist 05/02/19

For 8270 full list, the DDT breakdown and pentachlorophenol & benzidine peak tailing were evaluated in the DFTPP tune and

were found to be in control.

For 8270 BN list, benzidine peak tailing was evaluated in the DFTPP tune and was found to be in control.

Initial Calibration Evaluation (CHEM05/5_SPLIT_0418):

99% of target compounds met criteria.

The following compounds had %RSDs >20%: Naphthalene 21% (20%)

The following compounds did not meet recommended response factors: 2-Nitrophenol 0.044 (0.1), Hexachlorobenzene 0.077

SVOA Narration(0.1)

The following compounds did not meet a minimum response factors: None.

Continuing Calibration Verification (CHEM05/0502_03-5_SPLIT_0418):

Internal standard areas were within 50 to 200% of the initial calibration with the following exceptions: None.


The following compounds did not meet % deviation criteria: None.

The following compounds did not meet maximum % deviations: None.


(0.1)

The following compounds did not meet minimum response factors: None.CD05134, CD05135

CHEM06 05/02/19-2 Wes Bryon, Chemist 05/02/19






The following compounds had %RSDs >20%: None.


(0.1)






Page 11 of 23109-May-19 16:45

The following compounds did not meet % deviation criteria: 2-Nitrophenol 37%H (30%)



(0.1)

The following compounds did not meet minimum response factors: None.CD05133








The following compounds did not meet recommended response factors: None.





The following compounds did not meet % deviation criteria: None.

SVOA NarrationThe following compounds did not meet maximum % deviations: None.


The following compounds did not meet minimum response factors: None.CD05119, CD05120, CD05121, CD05122, CD05124, CD05125, CD05127, CD05128









(0.1)





The following compounds did not meet % deviation criteria: % 2,4,6-Tribromophenol 40%H (30%), 4-Nitrophenol 34%H (30%),

Benzoic acid 34%L (30%)



(0.1)

The following compounds did not meet minimum response factors: None.CD05138, CD05139, CD05140, CD05141







The following compounds had %RSDs >20%: 4-Nitrophenol 28% (20%), Benzoic acid 32% (20%)

The following compounds did not meet recommended response factors: 2-Nitrophenol 0.072 (0.1)





The following compounds did not meet % deviation criteria: N-Nitrosodimethylamine 39%L (30%)


The following compounds did not meet recommended response factors: 2-Nitrophenol 0.077 (0.1)

The following compounds did not meet minimum response factors: None.


Batch 477196 (CD05138)

SVOA NarrationCD05138, CD05139, CD05140, CD05141

All LCS recoveries were within 30 - 130 with the following exceptions: Benzoic acid(23%)

All LCSD recoveries were within 30 - 130 with the following exceptions: Benzoic acid(19%)



Additional 8270 criteria:20% of compounds can be outside of acceptance criteria as long as recovery is at least 10%. (Acid


Page 12 of 23109-May-19 16:45

surrogates acceptance range for aqueous samples: 15-110%, for soils 30-130%)

Additional 8270 criteria: 20% of compounds can be outside of acceptance criteria as long as recovery is at least 10%. (Acid



CD05132, CD05133, CD05134, CD05135

Batch 477192 (CD05126)

All LCS recoveries were within 30 - 130 with the following exceptions: 2,4-Dinitrophenol(13%), Benzoic Acid(<10%)

All LCSD recoveries were within 30 - 130 with the following exceptions: 2,4-Dinitrophenol(11%), Benzoic Acid(<10%)


All MS recoveries were within 30 - 130 with the following exceptions: Benzidine(29%), Benzoic Acid(24%), Pyridine(27%)

All MSD recoveries were within 30 - 130 with the following exceptions: Benzoic Acid(20%)


A matrix effect is suspected when a MS/MSD recovery is outside of criteria. No further action is required if LCS/LCSD

compounds are within criteria.

Additional 8270 criteria: 20% of compounds can be outside of acceptance criteria as long as recovery is at least 10%. (Acid


SVOASIM NarrationWere all QA/QC performance criteria specified in the Reasonable Confidence Protocol documents achieved? No.

QC Batch 477196 (Samples: CD05138, CD05139, CD05140, CD05141): -----

One or more analytes is below the method criteria. A low bias for these analytes is possible. (Hexachlorocyclopentadiene)




Initial Calibration Evaluation (CHEM27/27_SIM18_0419):





Continuing Calibration Verification (CHEM27/0503_18-27_SIM18_0419):



SVOASIM NarrationThe following compounds did not meet % deviation criteria: None.



The following compounds did not meet minimum response factors: None.


Batch 477196 (CD05138)

All LCS recoveries were within 30 - 130 with the following exceptions: Hexachlorocyclopentadiene(24%)

All LCSD recoveries were within 30 - 130 with the following exceptions: Hexachlorocyclopentadiene(25%)






CD05132, CD05133, CD05134, CD05135

Batch 477192 (CD05126)

All LCS recoveries were within 30 - 130 with the following exceptions: 2,4-Dinitrophenol(13%), Benzoic Acid(<10%)

All LCSD recoveries were within 30 - 130 with the following exceptions: 2,4-Dinitrophenol(11%), Benzoic Acid(<10%)


All MS recoveries were within 30 - 130 with the following exceptions: Benzidine(29%), Benzoic Acid(24%), Pyridine(27%)

All MSD recoveries were within 30 - 130 with the following exceptions: Benzoic Acid(20%)


A matrix effect is suspected when a MS/MSD recovery is outside of criteria. No further action is required if LCS/LCSD

compounds are within criteria.



VOA Narration

VOA NarrationWere all

See below for any non-conformances and issues relating to quality control samples and/or sample analysis/matrix.


Page 13 of 23109-May-19 16:45

SW7471B

Laboratory Control Samples:

477261A BSD

Mercury RPD 31.3% (30%) is outside individual acceptance criteria.

CD05120-LCS

This parameter is outside laboratory rpd specified recovery limits.

Mercury

CD05120-LCSD


Mercury

SW8081B

Blanks:

CD05138-BLK



%DCBP (Surrogate Rec)

%TCMX (Surrogate Rec)

4,4' -DDD

4,4' -DDE

4,4' -DDT

a-BHC

Alachlor

Aldrin

b-BHC

Chlordane

d-BHC

Dieldrin

Endosulfan I

Endosulfan II

Endosulfan Sulfate

Endrin

Endrin Aldehyde

Endrin ketone

g-BHC (Lindane)

Heptachlor

Heptachlor epoxide

Methoxychlor

Toxaphene


CD05138-LCS


Page 14 of 23109-May-19 16:45

SW8081B


CD05138-LCS





4,4' -DDD

4,4' -DDE

4,4' -DDT

a-BHC

Aldrin

b-BHC

Chlordane

d-BHC

Dieldrin

Endosulfan I

Endosulfan II

Endosulfan Sulfate

Endrin

Endrin Aldehyde

Endrin ketone

g-BHC (Lindane)

Heptachlor

Heptachlor epoxide

Methoxychlor

CD05138-LCSD





4,4' -DDD

4,4' -DDE

4,4' -DDT

a-BHC

Aldrin

b-BHC

Chlordane

d-BHC

Dieldrin

Endosulfan I

Endosulfan II

Endosulfan Sulfate

Endrin

Endrin Aldehyde

Endrin ketone

g-BHC (Lindane)

Heptachlor

Heptachlor epoxide

Methoxychlor

SW8082A


477222A BS


Page 15 of 23109-May-19 16:45

SW8082A


477222A BS

PCB-1221 percent recovery 0 (40-140) is outside individual acceptance criteria, but within overall method allowances. All

reported results of the following samples are considered to have a potentially low bias:

DUP

Field Blank

TMW-1

TMW-2



DUP

Field Blank

TMW-1

TMW-2



DUP

Field Blank

TMW-1

TMW-2



DUP

Field Blank

TMW-1

TMW-2



DUP

Field Blank

TMW-1

TMW-2



DUP

Field Blank

TMW-1

TMW-2



DUP

Field Blank

TMW-1

TMW-2

477265A BS


Page 16 of 23109-May-19 16:45

SW8082A


477265A BS



B-1 1-3'

B-1 7.7-9'

B-2 1-2.9'

B-2 8-9.8'

B-3 0.4-2.2'

B-3 11-13'

B-3 6-8'

B-4 0.4-1.8'

B-4 11.8-13.8'

B-4 5.4-7.4'

B-5 1.7-2.8'

B-5 5-7'

B-6 0.4-1.7'

B-6 5.6-7.6'

DUP



B-1 1-3'

B-1 7.7-9'

B-2 1-2.9'

B-2 8-9.8'

B-3 0.4-2.2'

B-3 11-13'

B-3 6-8'

B-4 0.4-1.8'

B-4 11.8-13.8'

B-4 5.4-7.4'

B-5 1.7-2.8'

B-5 5-7'

B-6 0.4-1.7'

B-6 5.6-7.6'

DUP



B-1 1-3'

B-1 7.7-9'

B-2 1-2.9'

B-2 8-9.8'

B-3 0.4-2.2'

B-3 11-13'

B-3 6-8'

B-4 0.4-1.8'

B-4 11.8-13.8'

B-4 5.4-7.4'

B-5 1.7-2.8'

B-5 5-7'

B-6 0.4-1.7'

B-6 5.6-7.6'

DUP


Page 17 of 23109-May-19 16:45

SW8082A


477265A BS



B-1 1-3'

B-1 7.7-9'

B-2 1-2.9'

B-2 8-9.8'

B-3 0.4-2.2'

B-3 11-13'

B-3 6-8'

B-4 0.4-1.8'

B-4 11.8-13.8'

B-4 5.4-7.4'

B-5 1.7-2.8'

B-5 5-7'

B-6 0.4-1.7'

B-6 5.6-7.6'

DUP



B-1 1-3'

B-1 7.7-9'

B-2 1-2.9'

B-2 8-9.8'

B-3 0.4-2.2'

B-3 11-13'

B-3 6-8'

B-4 0.4-1.8'

B-4 11.8-13.8'

B-4 5.4-7.4'

B-5 1.7-2.8'

B-5 5-7'

B-6 0.4-1.7'

B-6 5.6-7.6'

DUP



B-1 1-3'

B-1 7.7-9'

B-2 1-2.9'

B-2 8-9.8'

B-3 0.4-2.2'

B-3 11-13'

B-3 6-8'

B-4 0.4-1.8'

B-4 11.8-13.8'

B-4 5.4-7.4'

B-5 1.7-2.8'

B-5 5-7'

B-6 0.4-1.7'

B-6 5.6-7.6'

DUP


Page 18 of 23109-May-19 16:45

SW8082A


477265A BS



B-1 1-3'

B-1 7.7-9'

B-2 1-2.9'

B-2 8-9.8'

B-3 0.4-2.2'

B-3 11-13'

B-3 6-8'

B-4 0.4-1.8'

B-4 11.8-13.8'

B-4 5.4-7.4'

B-5 1.7-2.8'

B-5 5-7'

B-6 0.4-1.7'

B-6 5.6-7.6'

DUP

SW8260C


477696A BS

Bromomethane percent recovery 142 (70-130) is outside individual acceptance criteria, but within overall method allowances. All

reported results of the following samples are considered to have a potentially high bias:

TMW-1

TMW-2

Trip Blank

477712A BSD

Dichlorodifluoromethane RPD 50.4% (30%) is outside individual acceptance criteria.

CD04607-LCS


Dichlorodifluoromethane

CD04607-LCSD

This parameter is outside laboratory lcs/lcsd specified recovery limits.

1,1,2,2-Tetrachloroethane

1,2,3-Trichlorobenzene

1,2-Dibromo-3-chloropropane

Bromoform


Naphthalene



CD05131-LCSD


Dibromochloromethane

Naphthalene


Page 19 of 23109-May-19 16:45

SW8260C


CD05142-LCS


Bromomethane

CD05142-LCSD


Bromomethane

Spikes:

CD05131-MS Source: SC54611-13

This parameter is outside laboratory ms/msd specified recovery limits.

1,1-Dichloropropene

1,2,4-Trichlorobenzene

Hexachlorobutadiene

Isopropylbenzene

Naphthalene

n-Butylbenzene

p-Isopropyltoluene

sec-Butylbenzene

tert-Butylbenzene

Tetrachloroethene

CD05131-MSD Source: SC54611-13


Hexachlorobutadiene

Isopropylbenzene

Naphthalene

n-Butylbenzene

sec-Butylbenzene

Samples:

SC54611-20 TMW-2

S - Laboratory solvent, contamination is possible.

Methylene chloride

SW8270D


477192A BS


Page 20 of 23109-May-19 16:45

SW8270D


477192A BS

2,4-Dinitrophenol percent recovery 13 (30-130) is outside individual acceptance criteria, but within overall method allowances.

All reported results of the following samples are considered to have a potentially low bias:

B-1 1-3'

B-1 7.7-9'

B-2 1-2.9'

B-2 8-9.8'

B-3 0.4-2.2'

B-3 11-13'

B-3 6-8'

B-4 0.4-1.8'

B-4 11.8-13.8'

B-4 5.4-7.4'

B-5 1.7-2.8'

B-5 5-7'

B-6 0.4-1.7'

B-6 5.6-7.6'

DUP

SED-1

SED-2

Benzoic acid percent recovery <10 (30-130) is outside individual acceptance criteria, but within overall method allowances. All


B-1 1-3'

B-1 7.7-9'

B-2 1-2.9'

B-2 8-9.8'

B-3 0.4-2.2'

B-3 11-13'

B-3 6-8'

B-4 0.4-1.8'

B-4 11.8-13.8'

B-4 5.4-7.4'

B-5 1.7-2.8'

B-5 5-7'

B-6 0.4-1.7'

B-6 5.6-7.6'

DUP

SED-1

SED-2

477196A BS

Benzoic acid percent recovery 23 (30-130) is outside individual acceptance criteria, but within overall method allowances. All


DUP

Field Blank

TMW-1

TMW-2

CD05126-LCS


2,4-Dinitrophenol

Benzoic acid

CD05126-LCSD


Page 21 of 23109-May-19 16:45

SW8270D


CD05126-LCSD


2,4-Dinitrophenol

Benzoic acid

CD05138-LCS


Benzoic acid

CD05138-LCSD


Benzoic acid

Spikes:

CD05126-MS Source: SC54611-08


Benzidine

Benzoic acid

Pyridine

CD05126-MSD Source: SC54611-08


Benzoic acid

SW8270D (SIM)


477196B BS

Hexachlorocyclopentadiene percent recovery 24 (30-130) is outside individual acceptance criteria, but within overall method

allowances. All reported results of the following samples are considered to have a potentially low bias:

DUP

Field Blank

TMW-1

TMW-2

D05138-LCS


Hexachlorocyclopentadiene

D05138-LCSD


Hexachlorocyclopentadiene

SW846 1030

Samples:

SC54611-01 B-1 1-3'


Page 22 of 23109-May-19 16:45

SW846 1030

Samples:

SC54611-01 B-1 1-3'

A hold time of 24 hours has been set to expedite the analyses through the laboratory. However, the hold time for Ignitability is not

specified within the method other than to state that the samples should be analyzed as soon as possible.

Ignitability by Definition

SC54611-02 B-1 7.7-9'




SC54611-03 B-2 1-2.9'




SC54611-04 B-2 8-9.8'




SC54611-05 B-3 0.4-2.2'




SC54611-06 B-3 6-8'




SC54611-07 B-3 11-13'




SC54611-08 B-4 0.4-1.8'




SC54611-09 B-4 5.4-7.4'




SC54611-10 B-4 11.8-13.8'





Page 23 of 23109-May-19 16:45

SW846 1030

Samples:

SC54611-11 B-5 1.7-2.8'




SC54611-12 B-5 5-7'




SC54611-13 B-6 0.4-1.7'




SC54611-14 B-6 5.6-7.6'




SC54611-15 SED-1




SC54611-16 SED-2




SC54611-17 DUP





Page 24 of 23109-May-19 16:45

Sample Acceptance Check Form

Client:

Work Order:

Project:

Sample(s) received on:

BL Companies

Turtle Creek - Milford, CT / 18EC0070

SC54611

5/1/2019

Yes No N/A

Were samples received at a temperature of 6°C?

Were custody seals present?

Were custody seals intact?

ü

ü

ü

The following outlines the condition of samples for the attached Chain of Custody upon receipt.

Were samples refrigerated upon transfer to laboratory representative? ü

Were samples properly labeled (labels affixed to sample containers and include sample ID, site

location, and/or project number and the collection date)?

ü

Were sample containers received intact?

Were samples accompanied by a Chain of Custody document?

Did sample container labels agree with Chain of Custody document?

Were samples received within method-specific holding times?

ü

ü

ü

ü

Does Chain of Custody document include proper, full, and complete documentation, which shall

include sample ID, site location, and/or project number, date and time of collection, collector's name,

preservation type, sample matrix and any special remarks concerning the sample?

ü


Page 25 of 23109-May-19 16:45

Summary of Hits

Client ID: B-1 1-3'Lab ID: SC54611-01

ResultParameter Units Analytical MethodReporting LimitFlag

Arsenic SW6010D0.773.04 mg/kg

Barium SW6010D0.3917.5 mg/kg

Chromium SW6010D0.3916.1 mg/kg

Lead SW6010D0.3975.4 mg/kg

SPLP Arsenic SW6010D (SPLP)0.0040.005 mg/l

SPLP Barium SW6010D (SPLP)0.0100.053 mg/l

SPLP Lead SW6010D (SPLP)0.0100.022 mg/l

Reactivity Sulfide SW-7.320< 20 mg/kg

Benz(a)anthracene SW8270D270320 ug/kg

Benzo(a)pyrene SW8270D270390 ug/kg

Benzo(b)fluoranthene SW8270D270280 ug/kg

Benzo(k)fluoranthene SW8270D270350 ug/kg

Chrysene SW8270D270360 ug/kg

Fluoranthene SW8270D270550 ug/kg

Pyrene SW8270D270610 ug/kg

Reactivity Cyanide SW846-ReactCyn5< 5 mg/kg

Client ID: B-1 7.7-9'Lab ID: SC54611-02









Client ID: B-2 1-2.9'Lab ID: SC54611-03








Tetrachloroethene SW8260C4.811 ug/kg



Page 26 of 23109-May-19 16:45

Client ID: B-2 8-9.8'Lab ID: SC54611-04








1,1,1-Trichloroethane SW8260C5.615 ug/kg

1,1-Dichloroethane SW8260C5.618 ug/kg


Vinyl chloride SW8260C5.612 ug/kg


Client ID: B-2 8-9.8'Lab ID: SC54611-04RE1


cis-1,2-Dichloroethene SW8260C350410 ug/kg

Client ID: B-3 0.4-2.2'Lab ID: SC54611-05









Tetrachloroethene SW8260C4.66.0 ug/kg

Acenaphthylene SW8270D260310 ug/kg




Benzo(ghi)perylene SW8270D260920 ug/kg



Dibenz(a,h)anthracene SW8270D260280 ug/kg


Indeno(1,2,3-cd)pyrene SW8270D2601100 ug/kg

Phenanthrene SW8270D260410 ug/kg




Page 27 of 23109-May-19 16:45









Carbon Disulfide SW8260C4.87.6 ug/kg

cis-1,2-Dichloroethene SW8260C4.89.2 ug/kg










Carbon Disulfide SW8260C5.113 ug/kg












4,4' -DDT SW8081B7.112 ug/kg












Page 28 of 23109-May-19 16:45





Cadmium SW6010D0.412.90 mg/kg





Reactivity Sulfide SW-7.32049 mg/kg

1,2-Dichlorobenzene SW8260C4.427 ug/kg

cis-1,2-Dichloroethene SW8260C4.44.7 ug/kg

Methyl Ethyl Ketone SW8260C2659 ug/kg










1,1-Dichloroethane SW8260C5.788 ug/kg

Chloroethane SW8260C5.7150 ug/kg

cis-1,2-Dichloroethene SW8260C5.7130 ug/kg

Tetrachloroethene SW8260C5.76.3 ug/kg

Trichloroethene SW8260C5.711 ug/kg

Vinyl chloride SW8260C5.791 ug/kg











Mercury SW7471B0.030.03 mg/kg




Page 29 of 23109-May-19 16:45

Client ID: B-5 1.7-2.8'Lab ID: SC54611-11RE1


1,2,4-Trimethylbenzene SW8260C130160 ug/kg


Benzene SW8260C210240 ug/kg

Ethylbenzene SW8260C86110 ug/kg

Naphthalene SW8260C210570 ug/kg










Benzene SW8260C5.419 ug/kg
























Page 30 of 23109-May-19 16:45











Client ID: SED-1Lab ID: SC54611-15


Ext. Petroleum H.C. (C9-C36) CTETPH 8015D130370 mg/kg










Acenaphthene SW8270D5901100 ug/kg

Anthracene SW8270D5902800 ug/kg






Carbazole SW8270D8502600 ug/kg


Dibenz(a,h)anthracene SW8270D5901700 ug/kg

Dibenzofuran SW8270D590670 ug/kg

Fluorene SW8270D5901900 ug/kg



Client ID: SED-1Lab ID: SC54611-15RE1



Phenanthrene SW8270D300017000 ug/kg



Page 31 of 23109-May-19 16:45

Client ID: SED-2Lab ID: SC54611-16


Ext. Petroleum H.C. (C9-C36) CTETPH 8015D72180 mg/kg










Mercury SW7471B0.090.10 mg/kg






Bis(2-ethylhexyl)phthalate SW8270D330590 ug/kg






Client ID: DUPLab ID: SC54611-17











Benzene SW8260C340620 ug/kg

Ethylbenzene SW8260C200210 ug/kg

Isopropylbenzene SW8260C130140 ug/kg

m&p-Xylene SW8260C340340 ug/kg

Naphthalene SW8260C3401500 ug/kg

Total Xylenes SW8260C4.8340.0 ug/kg



Page 32 of 23109-May-19 16:45

Client ID: DUPLab ID: SC54611-17RE1



Client ID: TMW-1Lab ID: SC54611-19


Copper SW6010D0.0050.006 mg/l

Lead SW6010D0.0020.003 mg/l

Zinc SW6010D0.0040.008 mg/l

Lead (Dissolved) (dissolved) SW6010D dissolved0.0020.002 mg/l

Zinc (Dissolved) (dissolved) SW6010D dissolved0.0020.003 mg/l

Dieldrin SW8081B0.0010.024 ug/l

cis-1,2-Dichloroethene SW8260C1.02.8 ug/l

Client ID: TMW-2Lab ID: SC54611-20


Lead (Dissolved) (dissolved) SW6010D dissolved0.0020.004 mg/l


Dieldrin SW8081B0.0020.018 ug/l

1,1,1-Trichloroethane SW8260C1.06.6 ug/l

1,1-Dichloroethane SW8260C10230 ug/l

1,1-Dichloroethene SW8260C1.08.3 ug/l

1,2,4-Trimethylbenzene SW8260C1.05.4 ug/l

1,2-Dichlorobenzene SW8260C1.04.8 ug/l

1,2-Dichloroethane SW8260C0.601.0 ug/l

Ethylbenzene SW8260C1.013 ug/l

Isopropylbenzene SW8260C1.01.3 ug/l

m&p-Xylene SW8260C1.03.1 ug/l

Methylene chloride SW8260C1.02.2 ug/lS

n-Propylbenzene SW8260C1.01.8 ug/l

o-Xylene SW8260C1.010 ug/l

Tetrachloroethene SW8260C1.020 ug/l

Toluene SW8260C1.09.2 ug/l

Total Xylenes SW8260C1.013.1 ug/l

Trichlorotrifluoroethane SW8260C1.09.9 ug/l

1,2-Dichlorobenzene SW8270D2.42.6 ug/l

Bis(2-ethylhexyl)phthalate SW8270D0.941.4 ug/l

Client ID: TMW-2Lab ID: SC54611-20RE1


Chloroethane SW8260C10260 ug/l

Trichloroethene SW8260C1035 ug/l

Vinyl chloride SW8260C10230 ug/l


Page 33 of 23109-May-19 16:45

Client ID: TMW-2Lab ID: SC54611-20RE2


cis-1,2-Dichloroethene SW8260C20260 ug/l

Client ID: DUPLab ID: SC54611-21


Copper SW6010D0.0050.007 mg/l

Lead SW6010D0.0020.003 mg/l

Zinc SW6010D0.0040.008 mg/l


Client ID: Field BlankLab ID: SC54611-22


Zinc SW6010D0.0040.013 mg/l

Please note that because there are no reporting limits associated with hazardous waste characterizations or micro analyses , this

summary does not include hits from these analyses if included in this work order.


Page 34 of 23109-May-19 16:45

B-1 1-3'

Sample IdentificationMatrix

30-Apr-19 11:10

Collection Date/Time Received

01-May-19

Client Project #

18EC0070 SoilSC54611-01

Result AnalyzedMethod Ref. Cert.BatchPreparedDilutionAnalyte(s) Units *RDLFlagCAS No. AnalystMDL

Toxicity Characteristics

SW846 1030 02-May-1

9 10:25

01-May-1

9 16:10

N/ANegative XIgnitability by Definition 1 1900599TAIgHT

SW846 9045D 01-May-1

9 15:40

01-May-1

9 14:48

pH Units6.47 XpH 1 1900598ABWpH

Subcontracted Analyses


Prepared by method SW3545A

Analysis performed by Phoenix Environmental Labs, Inc. * - CT007

CTETPH 8015D 02-May-1

9 22:43

01-May-1

9

mg/kg 58< 58Ext. Petroleum H.C.

(C9-C36)

1 477191APH061858

Surrogate recoveries:

50-150 % " " ""% n-Pentacosane 94 "629-99-2


Prepared by method SW3050B


SW6010D 02-May-1

9 11:53

"mg/kg 0.773.047440-38-2 Arsenic 1 477188APH06180.77

" ""mg/kg 0.3917.57440-39-3 Barium 1 ""0.39

" ""mg/kg 0.39< 0.397440-43-9 Cadmium 1 ""0.39

" ""mg/kg 0.3916.17440-47-3 Chromium 1 ""0.39

" ""mg/kg 0.3975.47439-92-1 Lead 1 ""0.39

" ""mg/kg 1.5< 1.57782-49-2 Selenium 1 ""1.5

" ""mg/kg 0.39< 0.397440-22-4 Silver 1 ""0.39




SW6010D

(SPLP)

03-May-1

9 03:06

02-May-1

9

mg/l 0.0040.0057440-38-2 SPLP Arsenic 1 477276APH06180.004

" ""mg/l 0.0100.0537440-39-3 SPLP Barium 1 ""0.010

" ""mg/l 0.005< 0.0057440-43-9 SPLP Cadmium 1 ""0.005

" ""mg/l 0.010< 0.0107440-47-3 SPLP Chromium 1 ""0.010

" ""mg/l 0.0100.0227439-92-1 SPLP Lead 1 ""0.010

" ""mg/l 0.020< 0.0207782-49-2 SPLP Selenium 1 ""0.020

" ""mg/l 0.010< 0.0107440-22-4 SPLP Silver 1 ""0.010

Prepared by method SW-7.3


SW-7.3 03-May-1

9 16:39

03-May-1

9 16:39

mg/kg 20< 20Reactivity Sulfide 1 '[none]'PH061820

Prepared by method SW1312/SW7470A


SW7470A

(SPLP)

03-May-1

9 08:07

02-May-1

9

mg/l 0.0005< 0.00057439-97-6 SPLP Mercury 1 477274APH06180.0005



SW7471B 02-May-1

9 11:16

"mg/kg 0.08< 0.087439-97-6 Mercury 1 477253APH06180.08




SW8081B 03-May-1

9 18:24

"ug/kg 7.7< 7.772-54-8 4,4' -DDD 2 477266APH06187.7


Page 35 of 23109-May-19 16:45

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01-May-19

Client Project #

18EC0070 SoilSC54611-01





SW8081B 03-May-1

9 18:24

02-May-1

9

ug/kg 7.7< 7.772-55-9 4,4' -DDE 2 477266APH06187.7

" ""ug/kg 7.7< 7.750-29-3 4,4' -DDT 2 ""7.7

" ""ug/kg 7.7< 7.7319-84-6 a-BHC 2 ""7.7

" ""ug/kg 7.7< 7.715972-60-8 Alachlor 2 ""7.7

" ""ug/kg 3.9< 3.9309-00-2 Aldrin 2 ""3.9

" ""ug/kg 7.7< 7.7319-85-7 b-BHC 2 ""7.7

" ""ug/kg 39< 3957-74-9 Chlordane 2 ""39

" ""ug/kg 7.7< 7.7319-86-8 d-BHC 2 ""7.7

" ""ug/kg 3.9< 3.960-57-1 Dieldrin 2 ""3.9

" ""ug/kg 7.7< 7.7959-98-8 Endosulfan I 2 ""7.7

" ""ug/kg 7.7< 7.733213-65-9 Endosulfan II 2 ""7.7

" ""ug/kg 7.7< 7.71031-07-8 Endosulfan sulfate 2 ""7.7

" ""ug/kg 7.7< 7.772-20-8 Endrin 2 ""7.7

" ""ug/kg 7.7< 7.77421-93-4 Endrin aldehyde 2 ""7.7

" ""ug/kg 7.7< 7.753494-70-5 Endrin ketone 2 ""7.7

" ""ug/kg 1.5< 1.558-89-9 g-BHC 2 ""1.5

" ""ug/kg 7.7< 7.776-44-8 Heptachlor 2 ""7.7

" ""ug/kg 7.7< 7.71024-57-3 Heptachlor epoxide 2 ""7.7

" ""ug/kg 39< 3972-43-5 Methoxychlor 2 ""39

" ""ug/kg 150< 1508001-35-2 Toxaphene 2 ""150


30-150 % " " ""% DCBP 61 "2051-24-3

30-150 % " " ""% TCMX 60 "877-09-8



SW8082A 04-May-1

9 01:13

"ug/kg 390< 39012674-11-2 PCB-1016 10 477265APH0618390

" ""ug/kg 390< 39011104-28-2 PCB-1221 10 ""390

" ""ug/kg 390< 39011141-16-5 PCB-1232 10 ""390

" ""ug/kg 390< 39053469-21-9 PCB-1242 10 ""390

" ""ug/kg 390< 39012672-29-6 PCB-1248 10 ""390

" ""ug/kg 390< 39011097-69-1 PCB-1254 10 ""390

" ""ug/kg 390< 39011096-82-5 PCB-1260 10 ""390

" ""ug/kg 390< 39037324-23-5 PCB-1262 10 ""390

" ""ug/kg 390< 39011100-14-4 PCB-1268 10 ""390


30-150 % " " ""% DCBP 80 "2051-24-3

30-150 % " " ""% TCMX 85 "877-09-8


Prepared by method SW8260C


SW8260C 04-May-1

9 01:24

01-May-1

9 22:12

ug/kg 5.5< 5.5630-20-6 1,1,1,2-Tetrachloroethane 1 477686APH06185.5

" ""ug/kg 5.5< 5.571-55-6 1,1,1-Trichloroethane 1 ""5.5


Page 36 of 23109-May-19 16:45

B-1 1-3'


30-Apr-19 11:10


01-May-19

Client Project #

18EC0070 SoilSC54611-01





SW8260C 04-May-1

9 01:24

01-May-1

9 22:12



" ""ug/kg 5.5< 5.575-34-3 1,1-Dichloroethane 1 ""5.5

" ""ug/kg 5.5< 5.575-35-4 1,1-Dichloroethene 1 ""5.5

" ""ug/kg 5.5< 5.5563-58-6 1,1-Dichloropropene 1 ""5.5

" ""ug/kg 5.5< 5.587-61-6 1,2,3-Trichlorobenzene 1 ""5.5

" ""ug/kg 5.5< 5.596-18-4 1,2,3-Trichloropropane 1 ""5.5


" ""ug/kg 5.5< 5.595-63-6 1,2,4-Trimethylbenzene 1 ""5.5

" ""ug/kg 5.5< 5.596-12-8 1,2-Dibromo-3-chloroprop

ane

1 ""5.5

" ""ug/kg 5.5< 5.5106-93-4 1,2-Dibromoethane 1 ""5.5

" ""ug/kg 5.5< 5.595-50-1 1,2-Dichlorobenzene 1 ""5.5


" ""ug/kg 5.5< 5.578-87-5 1,2-Dichloropropane 1 ""5.5






" ""ug/kg 5.5< 5.595-49-8 2-Chlorotoluene 1 ""5.5

" ""ug/kg 27< 27591-78-6 2-Hexanone 1 ""27

" ""ug/kg 5.5< 5.5527-84-4 2-Isopropyltoluene 1 ""5.5


" ""ug/kg 27< 27108-10-1 4-Methyl-2-pentanone 1 ""27

" ""ug/kg 270< 27067-64-1 Acetone 1 ""270

" ""ug/kg 5.5< 5.5107-13-1 Acrylonitrile 1 ""5.5

" ""ug/kg 5.5< 5.571-43-2 Benzene 1 ""5.5

" ""ug/kg 5.5< 5.5108-86-1 Bromobenzene 1 ""5.5

" ""ug/kg 5.5< 5.574-97-5 Bromochloromethane 1 ""5.5

" ""ug/kg 5.5< 5.575-27-4 Bromodichloromethane 1 ""5.5

" ""ug/kg 5.5< 5.575-25-2 Bromoform 1 ""5.5

" ""ug/kg 5.5< 5.574-83-9 Bromomethane 1 ""5.5

" ""ug/kg 5.5< 5.575-15-0 Carbon Disulfide 1 ""5.5

" ""ug/kg 5.5< 5.556-23-5 Carbon tetrachloride 1 ""5.5

" ""ug/kg 5.5< 5.5108-90-7 Chlorobenzene 1 ""5.5

" ""ug/kg 5.5< 5.575-00-3 Chloroethane 1 ""5.5

" ""ug/kg 5.5< 5.567-66-3 Chloroform 1 ""5.5

" ""ug/kg 5.5< 5.574-87-3 Chloromethane 1 ""5.5

" ""ug/kg 5.5< 5.5156-59-2 cis-1,2-Dichloroethene 1 ""5.5

" ""ug/kg 5.5< 5.510061-01-5 cis-1,3-Dichloropropene 1 ""5.5

" ""ug/kg 3.3< 3.3124-48-1 Dibromochloromethane 1 ""3.3

" ""ug/kg 5.5< 5.574-95-3 Dibromomethane 1 ""5.5

" ""ug/kg 5.5< 5.575-71-8 Dichlorodifluoromethane 1 ""5.5


Page 37 of 23109-May-19 16:45

B-1 1-3'


30-Apr-19 11:10


01-May-19

Client Project #

18EC0070 SoilSC54611-01





SW8260C 04-May-1

9 01:24

01-May-1

9 22:12

ug/kg 5.5< 5.5100-41-4 Ethylbenzene 1 477686APH06185.5

" ""ug/kg 5.5< 5.587-68-3 Hexachlorobutadiene 1 ""5.5

" ""ug/kg 5.5< 5.598-82-8 Isopropylbenzene 1 ""5.5

" ""ug/kg 5.5< 5.5179601-23-1 m&p-Xylene 1 ""5.5

" ""ug/kg 33< 3378-93-3 Methyl Ethyl Ketone 1 ""33

" ""ug/kg 11< 111634-04-4 Methyl t-butyl ether

(MTBE)

1 ""11

" ""ug/kg 11< 1175-09-2 Methylene chloride 1 ""11

" ""ug/kg 5.5< 5.591-20-3 Naphthalene 1 ""5.5

" ""ug/kg 5.5< 5.5104-51-8 n-Butylbenzene 1 ""5.5

" ""ug/kg 5.5< 5.5103-65-1 n-Propylbenzene 1 ""5.5

" ""ug/kg 5.5< 5.595-47-6 o-Xylene 1 ""5.5

" ""ug/kg 5.5< 5.599-87-6 p-Isopropyltoluene 1 ""5.5

" ""ug/kg 5.5< 5.5135-98-8 sec-Butylbenzene 1 ""5.5

" ""ug/kg 5.5< 5.5100-42-5 Styrene 1 ""5.5

" ""ug/kg 5.5< 5.598-06-6 tert-Butylbenzene 1 ""5.5

" ""ug/kg 5.5< 5.5127-18-4 Tetrachloroethene 1 ""5.5

" ""ug/kg 11< 11109-99-9 Tetrahydrofuran (THF) 1 ""11

" ""ug/kg 5.5< 5.5108-88-3 Toluene 1 ""5.5

" ""ug/kg 5.5< 5.51330-20-7 Total Xylenes 1 ""5.5

" ""ug/kg 5.5< 5.5156-60-5 trans-1,2-Dichloroethene 1 ""5.5

" ""ug/kg 5.5< 5.510061-02-6 trans-1,3-Dichloropropene 1 ""5.5

" ""ug/kg 11< 11110-57-6 trans-1,4-dichloro-2-buten

e

1 ""11

" ""ug/kg 5.5< 5.579-01-6 Trichloroethene 1 ""5.5

" ""ug/kg 5.5< 5.575-69-4 Trichlorofluoromethane 1 ""5.5

" ""ug/kg 11< 1176-13-1 Trichlorotrifluoroethane 1 ""11

" ""ug/kg 5.5< 5.575-01-4 Vinyl chloride 1 ""5.5


70-130 % " " ""% 1,2-dichlorobenzene-d4 96 "2199-69-1

70-130 % " " ""% Bromofluorobenzene 84 "460-00-4

70-130 % " " ""% Dibromofluoromethane 101 "1868-53-7

70-130 % " " ""% Toluene-d8 97 "2037-26-5




SW8270D 02-May-1

9 08:10

01-May-1

9

ug/kg 270< 27095-94-3 1,2,4,5-Tetrachlorobenzen

e

1 477192APH0618270

" ""ug/kg 270< 270120-82-1 1,2,4-Trichlorobenzene 1 ""270

" ""ug/kg 270< 27095-50-1 1,2-Dichlorobenzene 1 ""270

" ""ug/kg 380< 380122-66-7 1,2-Diphenylhydrazine 1 ""380



" ""ug/kg 270< 27095-95-4 2,4,5-Trichlorophenol 1 ""270



Page 38 of 23109-May-19 16:45

B-1 1-3'


30-Apr-19 11:10


01-May-19

Client Project #

18EC0070 SoilSC54611-01





SW8270D 02-May-1

9 08:10

01-May-1

9

ug/kg 270< 270120-83-2 2,4-Dichlorophenol 1 477192APH0618270

" ""ug/kg 270< 270105-67-9 2,4-Dimethylphenol 1 ""270

" ""ug/kg 380< 38051-28-5 2,4-Dinitrophenol 1 ""380

" ""ug/kg 270< 270121-14-2 2,4-Dinitrotoluene 1 ""270


" ""ug/kg 270< 27091-58-7 2-Chloronaphthalene 1 ""270

" ""ug/kg 270< 27095-57-8 2-Chlorophenol 1 ""270

" ""ug/kg 270< 27091-57-6 2-Methylnaphthalene 1 ""270

" ""ug/kg 270< 27095-48-7 2-Methylphenol (o-cresol) 1 ""270

" ""ug/kg 380< 38088-74-4 2-Nitroaniline 1 ""380

" ""ug/kg 270< 27088-75-5 2-Nitrophenol 1 ""270

" ""ug/kg 380< 3803&4-Methylphenol

(m&p-cresol)

1 ""380

" ""ug/kg 270< 27091-94-1 3,3'-Dichlorobenzidine 1 ""270


" ""ug/kg 380< 380534-52-1 4,6-Dinitro-2-methylphenol 1 ""380

" ""ug/kg 380< 380101-55-3 4-Bromophenyl phenyl

ether

1 ""380

" ""ug/kg 270< 27059-50-7 4-Chloro-3-methylphenol 1 ""270

" ""ug/kg 270< 270106-47-8 4-Chloroaniline 1 ""270

" ""ug/kg 270< 2707005-72-3 4-Chlorophenyl phenyl

ether

1 ""270



" ""ug/kg 270< 27083-32-9 Acenaphthene 1 ""270

" ""ug/kg 270< 270208-96-8 Acenaphthylene 1 ""270

" ""ug/kg 270< 27098-86-2 Acetophenone 1 ""270

" ""ug/kg 380< 38062-53-3 Aniline 1 ""380

" ""ug/kg 270< 270120-12-7 Anthracene 1 ""270

" ""ug/kg 27032056-55-3 Benz(a)anthracene 1 ""270

" ""ug/kg 270< 27092-87-5 Benzidine 1 ""270

" ""ug/kg 27039050-32-8 Benzo(a)pyrene 1 ""270

" ""ug/kg 270280205-99-2 Benzo(b)fluoranthene 1 ""270

" ""ug/kg 270< 270191-24-2 Benzo(ghi)perylene 1 ""270

" ""ug/kg 270350207-08-9 Benzo(k)fluoranthene 1 ""270

" ""ug/kg 760< 76065-85-0 Benzoic acid 1 ""760

" ""ug/kg 270< 27085-68-7 Benzyl butyl phthalate 1 ""270

" ""ug/kg 270< 270111-91-1 Bis(2-chloroethoxy)metha

ne

1 ""270

" ""ug/kg 380< 380111-44-4 Bis(2-chloroethyl)ether 1 ""380

" ""ug/kg 270< 27039638-32-9 Bis(2-chloroisopropyl)ethe

r

1 ""270

" ""ug/kg 270< 270117-81-7 Bis(2-ethylhexyl)phthalate 1 ""270

" ""ug/kg 380< 38086-74-8 Carbazole 1 ""380

" ""ug/kg 270360218-01-9 Chrysene 1 ""270

" ""ug/kg 270< 27053-70-3 Dibenz(a,h)anthracene 1 ""270


Page 39 of 23109-May-19 16:45

B-1 1-3'


30-Apr-19 11:10


01-May-19

Client Project #

18EC0070 SoilSC54611-01





SW8270D 02-May-1

9 08:10

01-May-1

9

ug/kg 270< 270132-64-9 Dibenzofuran 1 477192APH0618270

" ""ug/kg 270< 27084-66-2 Diethyl phthalate 1 ""270

" ""ug/kg 270< 270131-11-3 Dimethylphthalate 1 ""270

" ""ug/kg 380< 38084-74-2 Di-n-butylphthalate 1 ""380

" ""ug/kg 270< 270117-84-0 Di-n-octylphthalate 1 ""270

" ""ug/kg 270550206-44-0 Fluoranthene 1 ""270

" ""ug/kg 270< 27086-73-7 Fluorene 1 ""270

" ""ug/kg 270< 270118-74-1 Hexachlorobenzene 1 ""270

" ""ug/kg 270< 27087-68-3 Hexachlorobutadiene 1 ""270

" ""ug/kg 270< 27077-47-4 Hexachlorocyclopentadien

e

1 ""270

" ""ug/kg 270< 27067-72-1 Hexachloroethane 1 ""270

" ""ug/kg 270< 270193-39-5 Indeno(1,2,3-cd)pyrene 1 ""270

" ""ug/kg 270< 27078-59-1 Isophorone 1 ""270

" ""ug/kg 270< 27091-20-3 Naphthalene 1 ""270

" ""ug/kg 270< 27098-95-3 Nitrobenzene 1 ""270

" ""ug/kg 380< 38062-75-9 N-Nitrosodimethylamine 1 ""380

" ""ug/kg 270< 270621-64-7 N-Nitrosodi-n-propylamine 1 ""270

" ""ug/kg 380< 38086-30-6 N-Nitrosodiphenylamine 1 ""380

" ""ug/kg 380< 38082-68-8 Pentachloronitrobenzene 1 ""380

" ""ug/kg 380< 38087-86-5 Pentachlorophenol 1 ""380

" ""ug/kg 270< 27085-01-8 Phenanthrene 1 ""270

" ""ug/kg 270< 270108-95-2 Phenol 1 ""270

" ""ug/kg 270610129-00-0 Pyrene 1 ""270

" ""ug/kg 380< 380110-86-1 Pyridine 1 ""380


30-130 % " " ""% 2,4,6-Tribromophenol 111 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 68 "321-60-8

30-130 % " " ""% 2-Fluorophenol 62 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 72 "4165-60-0

30-130 % " " ""% Phenol-d5 67 "4165-62-2

30-130 % " " ""% Terphenyl-d14 69 "98904-43-9

Prepared by method SW846-%Solid


SW846-%Solid 01-May-1

9 22:20

01-May-1

9 22:20

%85Percent Solid 1 '[none]'PH0618

Prepared by method SW846-React


SW846-React 03-May-1

9 16:39

03-May-1

9 16:39

Pos/NegNegativeReactivity 1 "PH0618

Prepared by method SW846-ReactCyn


SW846-ReactCy

n

03-May-1

9 14:06

03-May-1

9

mg/kg 5< 5Reactivity Cyanide 1 477480APH06185


Page 40 of 23109-May-19 16:45

B-1 7.7-9'


30-Apr-19 11:20


01-May-19

Client Project #

18EC0070 SoilSC54611-02



SW846 1030 02-May-1

9 10:25

01-May-1

9 16:10


SW846 9045D 01-May-1

9 15:45

01-May-1

9 14:48







9 20:31

01-May-1

9


(C9-C36)

1 477139APH061860


50-150 % " " ""% n-Pentacosane 85 "629-99-2




SW6010D 02-May-1

9 13:43

"mg/kg 0.821.807440-38-2 Arsenic 1 477188APH06180.82

" ""mg/kg 0.417.417440-39-3 Barium 1 ""0.41

" ""mg/kg 0.41< 0.417440-43-9 Cadmium 1 ""0.41

" ""mg/kg 0.419.567440-47-3 Chromium 1 ""0.41

" ""mg/kg 0.412.747439-92-1 Lead 1 ""0.41

" ""mg/kg 1.6< 1.67782-49-2 Selenium 1 ""1.6

" ""mg/kg 0.41< 0.417440-22-4 Silver 1 ""0.41




SW6010D

(SPLP)

03-May-1

9 03:09

02-May-1

9

mg/l 0.004< 0.0047440-38-2 SPLP Arsenic 1 477276APH06180.004

" ""mg/l 0.0100.0207440-39-3 SPLP Barium 1 ""0.010

" ""mg/l 0.005< 0.0057440-43-9 SPLP Cadmium 1 ""0.005


" ""mg/l 0.010< 0.0107439-92-1 SPLP Lead 1 ""0.010


" ""mg/l 0.010< 0.0107440-22-4 SPLP Silver 1 ""0.010



SW-7.3 03-May-1

9 16:39

03-May-1

9 16:39




SW7470A

(SPLP)

03-May-1

9 08:09

02-May-1

9




SW7471B 02-May-1

9 13:01

"mg/kg 0.03< 0.037439-97-6 Mercury 1 477261APH06180.03




SW8081B 03-May-1

9 18:43

"ug/kg 8.1< 8.172-54-8 4,4' -DDD 2 477266APH06188.1


Page 41 of 23109-May-19 16:45

B-1 7.7-9'


30-Apr-19 11:20


01-May-19

Client Project #

18EC0070 SoilSC54611-02





SW8081B 03-May-1

9 18:43

02-May-1

9

ug/kg 8.1< 8.172-55-9 4,4' -DDE 2 477266APH06188.1

" ""ug/kg 8.1< 8.150-29-3 4,4' -DDT 2 ""8.1

" ""ug/kg 8.1< 8.1319-84-6 a-BHC 2 ""8.1

" ""ug/kg 8.1< 8.115972-60-8 Alachlor 2 ""8.1

" ""ug/kg 4.0< 4.0309-00-2 Aldrin 2 ""4.0

" ""ug/kg 8.1< 8.1319-85-7 b-BHC 2 ""8.1

" ""ug/kg 40< 4057-74-9 Chlordane 2 ""40

" ""ug/kg 8.1< 8.1319-86-8 d-BHC 2 ""8.1

" ""ug/kg 4.0< 4.060-57-1 Dieldrin 2 ""4.0




" ""ug/kg 8.1< 8.172-20-8 Endrin 2 ""8.1



" ""ug/kg 1.6< 1.658-89-9 g-BHC 2 ""1.6

" ""ug/kg 8.1< 8.176-44-8 Heptachlor 2 ""8.1



" ""ug/kg 160< 1608001-35-2 Toxaphene 2 ""160


30-150 % " " ""% DCBP 60 "2051-24-3

30-150 % " " ""% TCMX 60 "877-09-8



SW8082A 04-May-1

9 01:35

"ug/kg 400< 40012674-11-2 PCB-1016 10 477265APH0618400

" ""ug/kg 400< 40011104-28-2 PCB-1221 10 ""400

" ""ug/kg 400< 40011141-16-5 PCB-1232 10 ""400

" ""ug/kg 400< 40053469-21-9 PCB-1242 10 ""400

" ""ug/kg 400< 40012672-29-6 PCB-1248 10 ""400

" ""ug/kg 400< 40011097-69-1 PCB-1254 10 ""400

" ""ug/kg 400< 40011096-82-5 PCB-1260 10 ""400

" ""ug/kg 400< 40037324-23-5 PCB-1262 10 ""400

" ""ug/kg 400< 40011100-14-4 PCB-1268 10 ""400


30-150 % " " ""% DCBP 70 "2051-24-3

30-150 % " " ""% TCMX 77 "877-09-8




SW8260C 04-May-1

9 17:05

04-May-1

9 13:27




Page 42 of 23109-May-19 16:45

B-1 7.7-9'


30-Apr-19 11:20


01-May-19

Client Project #

18EC0070 SoilSC54611-02





SW8260C 04-May-1

9 17:05

04-May-1

9 13:27











ane

1 ""5.1











" ""ug/kg 25< 25591-78-6 2-Hexanone 1 ""25




" ""ug/kg 250< 25067-64-1 Acetone 1 ""250


" ""ug/kg 5.1< 5.171-43-2 Benzene 1 ""5.1




" ""ug/kg 5.1< 5.175-25-2 Bromoform 1 ""5.1






" ""ug/kg 5.1< 5.167-66-3 Chloroform 1 ""5.1








Page 43 of 23109-May-19 16:45

B-1 7.7-9'


30-Apr-19 11:20


01-May-19

Client Project #

18EC0070 SoilSC54611-02





SW8260C 04-May-1

9 17:05

04-May-1

9 13:27




" ""ug/kg 5.1< 5.1179601-23-1 m&p-Xylene 1 ""5.1



(MTBE)

1 ""10





" ""ug/kg 5.1< 5.195-47-6 o-Xylene 1 ""5.1



" ""ug/kg 5.1< 5.1100-42-5 Styrene 1 ""5.1




" ""ug/kg 5.1< 5.1108-88-3 Toluene 1 ""5.1





e

1 ""10









70-130 % " " ""% Toluene-d8 96 "2037-26-5




SW8270D 02-May-1

9 08:33

01-May-1

9


e

1 477192APH0618280









Page 44 of 23109-May-19 16:45

B-1 7.7-9'


30-Apr-19 11:20


01-May-19

Client Project #

18EC0070 SoilSC54611-02





SW8270D 02-May-1

9 08:33

01-May-1

9













(m&p-cresol)

1 ""410





ether

1 ""410




ether

1 ""280






" ""ug/kg 410< 41062-53-3 Aniline 1 ""410

" ""ug/kg 280< 280120-12-7 Anthracene 1 ""280

" ""ug/kg 280< 28056-55-3 Benz(a)anthracene 1 ""280

" ""ug/kg 280< 28092-87-5 Benzidine 1 ""280

" ""ug/kg 280< 28050-32-8 Benzo(a)pyrene 1 ""280

" ""ug/kg 280< 280205-99-2 Benzo(b)fluoranthene 1 ""280


" ""ug/kg 280< 280207-08-9 Benzo(k)fluoranthene 1 ""280




ne

1 ""280



r

1 ""280


" ""ug/kg 410< 41086-74-8 Carbazole 1 ""410

" ""ug/kg 280< 280218-01-9 Chrysene 1 ""280



Page 45 of 23109-May-19 16:45

B-1 7.7-9'


30-Apr-19 11:20


01-May-19

Client Project #

18EC0070 SoilSC54611-02





SW8270D 02-May-1

9 08:33

01-May-1

9






" ""ug/kg 280< 280206-44-0 Fluoranthene 1 ""280

" ""ug/kg 280< 28086-73-7 Fluorene 1 ""280




e

1 ""280



" ""ug/kg 280< 28078-59-1 Isophorone 1 ""280









" ""ug/kg 280< 280108-95-2 Phenol 1 ""280

" ""ug/kg 280< 280129-00-0 Pyrene 1 ""280

" ""ug/kg 410< 410110-86-1 Pyridine 1 ""410


30-130 % " " ""% 2,4,6-Tribromophenol 108 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 66 "321-60-8

30-130 % " " ""% 2-Fluorophenol 61 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 69 "4165-60-0

30-130 % " " ""% Phenol-d5 65 "4165-62-2

30-130 % " " ""% Terphenyl-d14 72 "98904-43-9




9 22:20

01-May-1

9 22:20





9 16:39

03-May-1

9 16:39




SW846-ReactCy

n

03-May-1

9 14:09

03-May-1

9



Page 46 of 23109-May-19 16:45

B-2 1-2.9'


30-Apr-19 12:30


01-May-19

Client Project #

18EC0070 SoilSC54611-03



SW846 1030 02-May-1

9 10:25

01-May-1

9 16:10


SW846 9045D 01-May-1

9 15:47

01-May-1

9 14:48







9 19:06

01-May-1

9


(C9-C36)

1 477191APH061862


50-150 % " " ""% n-Pentacosane 84 "629-99-2




SW6010D 02-May-1

9 13:46

"mg/kg 0.812.577440-38-2 Arsenic 1 477188APH06180.81

" ""mg/kg 0.4126.27440-39-3 Barium 1 ""0.41

" ""mg/kg 0.41< 0.417440-43-9 Cadmium 1 ""0.41

" ""mg/kg 0.4113.37440-47-3 Chromium 1 ""0.41

" ""mg/kg 0.415.487439-92-1 Lead 1 ""0.41

" ""mg/kg 1.6< 1.67782-49-2 Selenium 1 ""1.6

" ""mg/kg 0.41< 0.417440-22-4 Silver 1 ""0.41




SW6010D

(SPLP)

03-May-1

9 03:12

02-May-1

9


" ""mg/l 0.0100.0297440-39-3 SPLP Barium 1 ""0.010

" ""mg/l 0.005< 0.0057440-43-9 SPLP Cadmium 1 ""0.005


" ""mg/l 0.010< 0.0107439-92-1 SPLP Lead 1 ""0.010


" ""mg/l 0.010< 0.0107440-22-4 SPLP Silver 1 ""0.010



SW-7.3 03-May-1

9 16:40

03-May-1

9 16:40




SW7470A

(SPLP)

03-May-1

9 08:11

02-May-1

9




SW7471B 02-May-1

9 13:03

"mg/kg 0.03< 0.037439-97-6 Mercury 1 477261APH06180.03




SW8081B 03-May-1

9 19:01

"ug/kg 8.2< 8.272-54-8 4,4' -DDD 2 477266APH06188.2


Page 47 of 23109-May-19 16:45

B-2 1-2.9'


30-Apr-19 12:30


01-May-19

Client Project #

18EC0070 SoilSC54611-03





SW8081B 03-May-1

9 19:01

02-May-1

9

ug/kg 8.2< 8.272-55-9 4,4' -DDE 2 477266APH06188.2

" ""ug/kg 8.2< 8.250-29-3 4,4' -DDT 2 ""8.2

" ""ug/kg 8.2< 8.2319-84-6 a-BHC 2 ""8.2

" ""ug/kg 8.2< 8.215972-60-8 Alachlor 2 ""8.2

" ""ug/kg 4.1< 4.1309-00-2 Aldrin 2 ""4.1

" ""ug/kg 8.2< 8.2319-85-7 b-BHC 2 ""8.2

" ""ug/kg 41< 4157-74-9 Chlordane 2 ""41

" ""ug/kg 8.2< 8.2319-86-8 d-BHC 2 ""8.2

" ""ug/kg 4.1< 4.160-57-1 Dieldrin 2 ""4.1




" ""ug/kg 8.2< 8.272-20-8 Endrin 2 ""8.2



" ""ug/kg 1.6< 1.658-89-9 g-BHC 2 ""1.6

" ""ug/kg 8.2< 8.276-44-8 Heptachlor 2 ""8.2



" ""ug/kg 160< 1608001-35-2 Toxaphene 2 ""160


30-150 % " " ""% DCBP 60 "2051-24-3

30-150 % " " ""% TCMX 57 "877-09-8



SW8082A 03-May-1

9 23:45

"ug/kg 410< 41012674-11-2 PCB-1016 10 477265APH0618410

" ""ug/kg 410< 41011104-28-2 PCB-1221 10 ""410

" ""ug/kg 410< 41011141-16-5 PCB-1232 10 ""410

" ""ug/kg 410< 41053469-21-9 PCB-1242 10 ""410

" ""ug/kg 410< 41012672-29-6 PCB-1248 10 ""410

" ""ug/kg 410< 41011097-69-1 PCB-1254 10 ""410

" ""ug/kg 410< 41011096-82-5 PCB-1260 10 ""410

" ""ug/kg 410< 41037324-23-5 PCB-1262 10 ""410

" ""ug/kg 410< 41011100-14-4 PCB-1268 10 ""410


30-150 % " " ""% DCBP 72 "2051-24-3

30-150 % " " ""% TCMX 74 "877-09-8




SW8260C 04-May-1

9 01:46

01-May-1

9 22:12




Page 48 of 23109-May-19 16:45

B-2 1-2.9'


30-Apr-19 12:30


01-May-19

Client Project #

18EC0070 SoilSC54611-03





SW8260C 04-May-1

9 01:46

01-May-1

9 22:12











ane

1 ""4.8











" ""ug/kg 24< 24591-78-6 2-Hexanone 1 ""24




" ""ug/kg 240< 24067-64-1 Acetone 1 ""240


" ""ug/kg 4.8< 4.871-43-2 Benzene 1 ""4.8




" ""ug/kg 4.8< 4.875-25-2 Bromoform 1 ""4.8






" ""ug/kg 4.8< 4.867-66-3 Chloroform 1 ""4.8








Page 49 of 23109-May-19 16:45

B-2 1-2.9'


30-Apr-19 12:30


01-May-19

Client Project #

18EC0070 SoilSC54611-03





SW8260C 04-May-1

9 01:46

01-May-1

9 22:12




" ""ug/kg 4.8< 4.8179601-23-1 m&p-Xylene 1 ""4.8


" ""ug/kg 9.6< 9.61634-04-4 Methyl t-butyl ether

(MTBE)

1 ""9.6

" ""ug/kg 9.6< 9.675-09-2 Methylene chloride 1 ""9.6




" ""ug/kg 4.8< 4.895-47-6 o-Xylene 1 ""4.8



" ""ug/kg 4.8< 4.8100-42-5 Styrene 1 ""4.8


" ""ug/kg 4.811127-18-4 Tetrachloroethene 1 ""4.8

" ""ug/kg 9.6< 9.6109-99-9 Tetrahydrofuran (THF) 1 ""9.6

" ""ug/kg 4.8< 4.8108-88-3 Toluene 1 ""4.8




" ""ug/kg 9.6< 9.6110-57-6 trans-1,4-dichloro-2-buten

e

1 ""9.6



" ""ug/kg 9.6< 9.676-13-1 Trichlorotrifluoroethane 1 ""9.6






70-130 % " " ""% Toluene-d8 97 "2037-26-5




SW8270D 02-May-1

9 08:57

01-May-1

9


e

1 477192APH0618290









Page 50 of 23109-May-19 16:45

B-2 1-2.9'


30-Apr-19 12:30


01-May-19

Client Project #

18EC0070 SoilSC54611-03





SW8270D 02-May-1

9 08:57

01-May-1

9













(m&p-cresol)

1 ""410





ether

1 ""410




ether

1 ""290






" ""ug/kg 410< 41062-53-3 Aniline 1 ""410

" ""ug/kg 290< 290120-12-7 Anthracene 1 ""290


" ""ug/kg 290< 29092-87-5 Benzidine 1 ""290








ne

1 ""290



r

1 ""290


" ""ug/kg 410< 41086-74-8 Carbazole 1 ""410

" ""ug/kg 290< 290218-01-9 Chrysene 1 ""290



Page 51 of 23109-May-19 16:45

B-2 1-2.9'


30-Apr-19 12:30


01-May-19

Client Project #

18EC0070 SoilSC54611-03





SW8270D 02-May-1

9 08:57

01-May-1

9







" ""ug/kg 290< 29086-73-7 Fluorene 1 ""290




e

1 ""290



" ""ug/kg 290< 29078-59-1 Isophorone 1 ""290









" ""ug/kg 290< 290108-95-2 Phenol 1 ""290

" ""ug/kg 290< 290129-00-0 Pyrene 1 ""290

" ""ug/kg 410< 410110-86-1 Pyridine 1 ""410


30-130 % " " ""% 2,4,6-Tribromophenol 107 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 64 "321-60-8

30-130 % " " ""% 2-Fluorophenol 58 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 68 "4165-60-0

30-130 % " " ""% Phenol-d5 62 "4165-62-2

30-130 % " " ""% Terphenyl-d14 72 "98904-43-9




9 22:20

01-May-1

9 22:20





9 16:40

03-May-1

9 16:40




SW846-ReactCy

n

03-May-1

9 14:10

03-May-1

9



Page 52 of 23109-May-19 16:45

B-2 8-9.8'


30-Apr-19 12:45


01-May-19

Client Project #

18EC0070 SoilSC54611-04



SW846 1030 02-May-1

9 10:25

01-May-1

9 16:10


SW846 9045D 01-May-1

9 15:50

01-May-1

9 14:48







9 18:37

01-May-1

9


(C9-C36)

1 477191APH061860


50-150 % " " ""% n-Pentacosane 95 "629-99-2




SW6010D 02-May-1

9 13:50

"mg/kg 0.751.737440-38-2 Arsenic 1 477188APH06180.75

" ""mg/kg 0.386.977440-39-3 Barium 1 ""0.38

" ""mg/kg 0.38< 0.387440-43-9 Cadmium 1 ""0.38

" ""mg/kg 0.388.757440-47-3 Chromium 1 ""0.38

" ""mg/kg 0.383.647439-92-1 Lead 1 ""0.38

" ""mg/kg 1.5< 1.57782-49-2 Selenium 1 ""1.5

" ""mg/kg 0.38< 0.387440-22-4 Silver 1 ""0.38




SW6010D

(SPLP)

03-May-1

9 03:14

02-May-1

9


" ""mg/l 0.0100.0237440-39-3 SPLP Barium 1 ""0.010

" ""mg/l 0.005< 0.0057440-43-9 SPLP Cadmium 1 ""0.005


" ""mg/l 0.010< 0.0107439-92-1 SPLP Lead 1 ""0.010


" ""mg/l 0.010< 0.0107440-22-4 SPLP Silver 1 ""0.010



SW-7.3 03-May-1

9 16:40

03-May-1

9 16:40




SW7470A

(SPLP)

03-May-1

9 08:14

02-May-1

9




SW7471B 02-May-1

9 13:05

"mg/kg 0.03< 0.037439-97-6 Mercury 1 477261APH06180.03




SW8081B 03-May-1

9 19:20

"ug/kg 8.1< 8.172-54-8 4,4' -DDD 2 477266APH06188.1


Page 53 of 23109-May-19 16:45

B-2 8-9.8'


30-Apr-19 12:45


01-May-19

Client Project #

18EC0070 SoilSC54611-04





SW8081B 03-May-1

9 19:20

02-May-1

9

ug/kg 8.1< 8.172-55-9 4,4' -DDE 2 477266APH06188.1

" ""ug/kg 8.1< 8.150-29-3 4,4' -DDT 2 ""8.1

" ""ug/kg 8.1< 8.1319-84-6 a-BHC 2 ""8.1

" ""ug/kg 8.1< 8.115972-60-8 Alachlor 2 ""8.1

" ""ug/kg 4.0< 4.0309-00-2 Aldrin 2 ""4.0

" ""ug/kg 8.1< 8.1319-85-7 b-BHC 2 ""8.1

" ""ug/kg 40< 4057-74-9 Chlordane 2 ""40

" ""ug/kg 8.1< 8.1319-86-8 d-BHC 2 ""8.1

" ""ug/kg 4.0< 4.060-57-1 Dieldrin 2 ""4.0




" ""ug/kg 8.1< 8.172-20-8 Endrin 2 ""8.1



" ""ug/kg 1.6< 1.658-89-9 g-BHC 2 ""1.6

" ""ug/kg 8.1< 8.176-44-8 Heptachlor 2 ""8.1



" ""ug/kg 160< 1608001-35-2 Toxaphene 2 ""160


30-150 % " " ""% DCBP 63 "2051-24-3

30-150 % " " ""% TCMX 60 "877-09-8



SW8082A 04-May-1

9 00:07

"ug/kg 400< 40012674-11-2 PCB-1016 10 477265APH0618400

" ""ug/kg 400< 40011104-28-2 PCB-1221 10 ""400

" ""ug/kg 400< 40011141-16-5 PCB-1232 10 ""400

" ""ug/kg 400< 40053469-21-9 PCB-1242 10 ""400

" ""ug/kg 400< 40012672-29-6 PCB-1248 10 ""400

" ""ug/kg 400< 40011097-69-1 PCB-1254 10 ""400

" ""ug/kg 400< 40011096-82-5 PCB-1260 10 ""400

" ""ug/kg 400< 40037324-23-5 PCB-1262 10 ""400

" ""ug/kg 400< 40011100-14-4 PCB-1268 10 ""400


30-150 % " " ""% DCBP 78 "2051-24-3

30-150 % " " ""% TCMX 82 "877-09-8




SW8260C 04-May-1

9 02:07

01-May-1

9 22:12


" ""ug/kg 5.61571-55-6 1,1,1-Trichloroethane 1 ""5.6


Page 54 of 23109-May-19 16:45

B-2 8-9.8'


30-Apr-19 12:45


01-May-19

Client Project #

18EC0070 SoilSC54611-04





SW8260C 04-May-1

9 02:07

01-May-1

9 22:12



" ""ug/kg 5.61875-34-3 1,1-Dichloroethane 1 ""5.6








ane

1 ""5.6











" ""ug/kg 28< 28591-78-6 2-Hexanone 1 ""28




" ""ug/kg 280< 28067-64-1 Acetone 1 ""280


" ""ug/kg 5.6< 5.671-43-2 Benzene 1 ""5.6




" ""ug/kg 5.6< 5.675-25-2 Bromoform 1 ""5.6






" ""ug/kg 5.6< 5.667-66-3 Chloroform 1 ""5.6






" ""ug/kg 5.6< 5.6100-41-4 Ethylbenzene 1 ""5.6


Page 55 of 23109-May-19 16:45

B-2 8-9.8'


30-Apr-19 12:45


01-May-19

Client Project #

18EC0070 SoilSC54611-04





SW8260C 04-May-1

9 02:07

01-May-1

9 22:12

ug/kg 5.6< 5.687-68-3 Hexachlorobutadiene 1 477686APH06185.6


" ""ug/kg 5.6< 5.6179601-23-1 m&p-Xylene 1 ""5.6



(MTBE)

1 ""11





" ""ug/kg 5.6< 5.695-47-6 o-Xylene 1 ""5.6



" ""ug/kg 5.6< 5.6100-42-5 Styrene 1 ""5.6




" ""ug/kg 5.6< 5.6108-88-3 Toluene 1 ""5.6





e

1 ""11




" ""ug/kg 5.61275-01-4 Vinyl chloride 1 ""5.6





70-130 % " " ""% Toluene-d8 101 "2037-26-5

Re-analysis of Subcontracted Analyses


SW8260C 04-May-1

9 02:07

04-May-1

9 13:29

ug/kg 350410156-59-2 cis-1,2-Dichloroethene 50 477679APH0618350





70-130 % " " ""% Toluene-d8 97 "2037-26-5





Page 56 of 23109-May-19 16:45

B-2 8-9.8'


30-Apr-19 12:45


01-May-19

Client Project #

18EC0070 SoilSC54611-04






SW8270D 02-May-1

9 09:21

01-May-1

9


e

1 477192APH0618280








" ""ug/kg 280< 280120-83-2 2,4-Dichlorophenol 1 ""280












(m&p-cresol)

1 ""400





ether

1 ""400




ether

1 ""280






" ""ug/kg 400< 40062-53-3 Aniline 1 ""400

" ""ug/kg 280< 280120-12-7 Anthracene 1 ""280


" ""ug/kg 280< 28092-87-5 Benzidine 1 ""280







Page 57 of 23109-May-19 16:45

B-2 8-9.8'


30-Apr-19 12:45


01-May-19

Client Project #

18EC0070 SoilSC54611-04





SW8270D 02-May-1

9 09:21

01-May-1

9

ug/kg 280< 28085-68-7 Benzyl butyl phthalate 1 477192APH0618280


ne

1 ""280



r

1 ""280


" ""ug/kg 400< 40086-74-8 Carbazole 1 ""400

" ""ug/kg 280< 280218-01-9 Chrysene 1 ""280


" ""ug/kg 280< 280132-64-9 Dibenzofuran 1 ""280






" ""ug/kg 280< 28086-73-7 Fluorene 1 ""280




e

1 ""280



" ""ug/kg 280< 28078-59-1 Isophorone 1 ""280









" ""ug/kg 280< 280108-95-2 Phenol 1 ""280

" ""ug/kg 280< 280129-00-0 Pyrene 1 ""280

" ""ug/kg 400< 400110-86-1 Pyridine 1 ""400


30-130 % " " ""% 2,4,6-Tribromophenol 94 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 56 "321-60-8

30-130 % " " ""% 2-Fluorophenol 52 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 62 "4165-60-0

30-130 % " " ""% Phenol-d5 55 "4165-62-2

30-130 % " " ""% Terphenyl-d14 63 "98904-43-9




Page 58 of 23109-May-19 16:45

B-2 8-9.8'


30-Apr-19 12:45


01-May-19

Client Project #

18EC0070 SoilSC54611-04






9 22:20

01-May-1

9 22:20





9 16:40

03-May-1

9 16:40




SW846-ReactCy

n

03-May-1

9 14:11

03-May-1

9



Page 59 of 23109-May-19 16:45

B-3 0.4-2.2'


30-Apr-19 13:10


01-May-19

Client Project #

18EC0070 SoilSC54611-05



SW846 1030 02-May-1

9 10:25

01-May-1

9 16:10


SW846 9045D 01-May-1

9 15:56

01-May-1

9 14:48







9 21:47

01-May-1

9


(C9-C36)

1 477191APH061856


50-150 % " " ""% n-Pentacosane 73 "629-99-2




SW6010D 02-May-1

9 13:53

"mg/kg 0.715.627440-38-2 Arsenic 1 477188APH06180.71

" ""mg/kg 0.3626.07440-39-3 Barium 1 ""0.36

" ""mg/kg 0.36< 0.367440-43-9 Cadmium 1 ""0.36

" ""mg/kg 0.3622.47440-47-3 Chromium 1 ""0.36

" ""mg/kg 0.3642.07439-92-1 Lead 1 ""0.36

" ""mg/kg 1.4< 1.47782-49-2 Selenium 1 ""1.4

" ""mg/kg 0.36< 0.367440-22-4 Silver 1 ""0.36




SW6010D

(SPLP)

03-May-1

9 03:17

02-May-1

9


" ""mg/l 0.0100.0447440-39-3 SPLP Barium 1 ""0.010

" ""mg/l 0.005< 0.0057440-43-9 SPLP Cadmium 1 ""0.005


" ""mg/l 0.0100.0137439-92-1 SPLP Lead 1 ""0.010


" ""mg/l 0.010< 0.0107440-22-4 SPLP Silver 1 ""0.010



SW-7.3 03-May-1

9 16:40

03-May-1

9 16:40




SW7470A

(SPLP)

03-May-1

9 08:16

02-May-1

9




SW7471B 02-May-1

9 13:08

"mg/kg 0.07< 0.077439-97-6 Mercury 1 477261APH06180.07




SW8081B 03-May-1

9 20:53

"ug/kg 7.4< 7.472-54-8 4,4' -DDD 2 477266APH06187.4


Page 60 of 23109-May-19 16:45

B-3 0.4-2.2'


30-Apr-19 13:10


01-May-19

Client Project #

18EC0070 SoilSC54611-05





SW8081B 03-May-1

9 20:53

02-May-1

9

ug/kg 7.4< 7.472-55-9 4,4' -DDE 2 477266APH06187.4

" ""ug/kg 7.4< 7.450-29-3 4,4' -DDT 2 ""7.4

" ""ug/kg 7.4< 7.4319-84-6 a-BHC 2 ""7.4

" ""ug/kg 7.4< 7.415972-60-8 Alachlor 2 ""7.4

" ""ug/kg 3.7< 3.7309-00-2 Aldrin 2 ""3.7

" ""ug/kg 7.4< 7.4319-85-7 b-BHC 2 ""7.4

" ""ug/kg 37< 3757-74-9 Chlordane 2 ""37

" ""ug/kg 7.4< 7.4319-86-8 d-BHC 2 ""7.4

" ""ug/kg 3.7< 3.760-57-1 Dieldrin 2 ""3.7




" ""ug/kg 7.4< 7.472-20-8 Endrin 2 ""7.4



" ""ug/kg 1.5< 1.558-89-9 g-BHC 2 ""1.5

" ""ug/kg 7.4< 7.476-44-8 Heptachlor 2 ""7.4



" ""ug/kg 150< 1508001-35-2 Toxaphene 2 ""150


30-150 % " " ""% DCBP 68 "2051-24-3

30-150 % " " ""% TCMX 63 "877-09-8



SW8082A 04-May-1

9 07:12

"ug/kg 370< 37012674-11-2 PCB-1016 10 477265APH0618370

" ""ug/kg 370< 37011104-28-2 PCB-1221 10 ""370

" ""ug/kg 370< 37011141-16-5 PCB-1232 10 ""370

" ""ug/kg 370< 37053469-21-9 PCB-1242 10 ""370

" ""ug/kg 370< 37012672-29-6 PCB-1248 10 ""370

" ""ug/kg 370< 37011097-69-1 PCB-1254 10 ""370

" ""ug/kg 370< 37011096-82-5 PCB-1260 10 ""370

" ""ug/kg 370< 37037324-23-5 PCB-1262 10 ""370

" ""ug/kg 370< 37011100-14-4 PCB-1268 10 ""370


30-150 % " " ""% DCBP 79 "2051-24-3

30-150 % " " ""% TCMX 85 "877-09-8




SW8260C 04-May-1

9 02:29

01-May-1

9 22:12




Page 61 of 23109-May-19 16:45

B-3 0.4-2.2'


30-Apr-19 13:10


01-May-19

Client Project #

18EC0070 SoilSC54611-05





SW8260C 04-May-1

9 02:29

01-May-1

9 22:12











ane

1 ""4.6











" ""ug/kg 23< 23591-78-6 2-Hexanone 1 ""23




" ""ug/kg 230< 23067-64-1 Acetone 1 ""230


" ""ug/kg 4.6< 4.671-43-2 Benzene 1 ""4.6




" ""ug/kg 4.6< 4.675-25-2 Bromoform 1 ""4.6






" ""ug/kg 4.6< 4.667-66-3 Chloroform 1 ""4.6








Page 62 of 23109-May-19 16:45

B-3 0.4-2.2'


30-Apr-19 13:10


01-May-19

Client Project #

18EC0070 SoilSC54611-05





SW8260C 04-May-1

9 02:29

01-May-1

9 22:12




" ""ug/kg 4.6< 4.6179601-23-1 m&p-Xylene 1 ""4.6



(MTBE)

1 ""9.2





" ""ug/kg 4.6< 4.695-47-6 o-Xylene 1 ""4.6



" ""ug/kg 4.6< 4.6100-42-5 Styrene 1 ""4.6


" ""ug/kg 4.66.0127-18-4 Tetrachloroethene 1 ""4.6


" ""ug/kg 4.6< 4.6108-88-3 Toluene 1 ""4.6





e

1 ""9.2









70-130 % " " ""% Toluene-d8 100 "2037-26-5




SW8270D 02-May-1

9 05:07

01-May-1

9


e

1 477192APH0618260









Page 63 of 23109-May-19 16:45

B-3 0.4-2.2'


30-Apr-19 13:10


01-May-19

Client Project #

18EC0070 SoilSC54611-05





SW8270D 02-May-1

9 05:07

01-May-1

9













(m&p-cresol)

1 ""380





ether

1 ""380




ether

1 ""260




" ""ug/kg 260310208-96-8 Acenaphthylene 1 ""260


" ""ug/kg 380< 38062-53-3 Aniline 1 ""380

" ""ug/kg 260< 260120-12-7 Anthracene 1 ""260

" ""ug/kg 2601,20056-55-3 Benz(a)anthracene 1 ""260

" ""ug/kg 260< 26092-87-5 Benzidine 1 ""260

" ""ug/kg 2601,20050-32-8 Benzo(a)pyrene 1 ""260

" ""ug/kg 2601,300205-99-2 Benzo(b)fluoranthene 1 ""260

" ""ug/kg 260920191-24-2 Benzo(ghi)perylene 1 ""260

" ""ug/kg 2601,100207-08-9 Benzo(k)fluoranthene 1 ""260




ne

1 ""260



r

1 ""260


" ""ug/kg 380< 38086-74-8 Carbazole 1 ""380

" ""ug/kg 2601,200218-01-9 Chrysene 1 ""260

" ""ug/kg 26028053-70-3 Dibenz(a,h)anthracene 1 ""260


Page 64 of 23109-May-19 16:45

B-3 0.4-2.2'


30-Apr-19 13:10


01-May-19

Client Project #

18EC0070 SoilSC54611-05





SW8270D 02-May-1

9 05:07

01-May-1

9






" ""ug/kg 2601,900206-44-0 Fluoranthene 1 ""260

" ""ug/kg 260< 26086-73-7 Fluorene 1 ""260




e

1 ""260


" ""ug/kg 2601,100193-39-5 Indeno(1,2,3-cd)pyrene 1 ""260

" ""ug/kg 260< 26078-59-1 Isophorone 1 ""260








" ""ug/kg 26041085-01-8 Phenanthrene 1 ""260

" ""ug/kg 260< 260108-95-2 Phenol 1 ""260

" ""ug/kg 2601,700129-00-0 Pyrene 1 ""260

" ""ug/kg 380< 380110-86-1 Pyridine 1 ""380


30-130 % " " ""% 2,4,6-Tribromophenol 72 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 67 "321-60-8

30-130 % " " ""% 2-Fluorophenol 64 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 65 "4165-60-0

30-130 % " " ""% Phenol-d5 71 "4165-62-2

30-130 % " " ""% Terphenyl-d14 75 "98904-43-9




9 22:20

01-May-1

9 22:20





9 16:40

03-May-1

9 16:40




SW846-ReactCy

n

03-May-1

9 14:11

03-May-1

9



Page 65 of 23109-May-19 16:45

B-3 6-8'


30-Apr-19 13:20


01-May-19

Client Project #

18EC0070 SoilSC54611-06



SW846 1030 02-May-1

9 10:25

01-May-1

9 16:10


SW846 9045D 01-May-1

9 16:01

01-May-1

9 14:48







9 12:29

01-May-1

9


(C9-C36)

1 477191APH061859


50-150 % " " ""% n-Pentacosane 90 "629-99-2




SW6010D 02-May-1

9 13:56

"mg/kg 0.741.447440-38-2 Arsenic 1 477188APH06180.74

" ""mg/kg 0.376.487440-39-3 Barium 1 ""0.37

" ""mg/kg 0.37< 0.377440-43-9 Cadmium 1 ""0.37

" ""mg/kg 0.3710.17440-47-3 Chromium 1 ""0.37

" ""mg/kg 0.372.937439-92-1 Lead 1 ""0.37

" ""mg/kg 1.5< 1.57782-49-2 Selenium 1 ""1.5

" ""mg/kg 0.37< 0.377440-22-4 Silver 1 ""0.37




SW6010D

(SPLP)

03-May-1

9 03:20

02-May-1

9


" ""mg/l 0.0100.0457440-39-3 SPLP Barium 1 ""0.010

" ""mg/l 0.005< 0.0057440-43-9 SPLP Cadmium 1 ""0.005


" ""mg/l 0.010< 0.0107439-92-1 SPLP Lead 1 ""0.010


" ""mg/l 0.010< 0.0107440-22-4 SPLP Silver 1 ""0.010



SW-7.3 03-May-1

9 16:40

03-May-1

9 16:40




SW7470A

(SPLP)

03-May-1

9 08:22

02-May-1

9




SW7471B 02-May-1

9 13:10

"mg/kg 0.03< 0.037439-97-6 Mercury 1 477261APH06180.03




SW8081B 04-May-1

9 00:53

"ug/kg 7.8< 7.872-54-8 4,4' -DDD 2 477266APH06187.8


Page 66 of 23109-May-19 16:45

B-3 6-8'


30-Apr-19 13:20


01-May-19

Client Project #

18EC0070 SoilSC54611-06





SW8081B 04-May-1

9 00:53

02-May-1

9

ug/kg 7.8< 7.872-55-9 4,4' -DDE 2 477266APH06187.8

" ""ug/kg 7.8< 7.850-29-3 4,4' -DDT 2 ""7.8

" ""ug/kg 7.8< 7.8319-84-6 a-BHC 2 ""7.8

" ""ug/kg 7.8< 7.815972-60-8 Alachlor 2 ""7.8

" ""ug/kg 3.9< 3.9309-00-2 Aldrin 2 ""3.9

" ""ug/kg 7.8< 7.8319-85-7 b-BHC 2 ""7.8

" ""ug/kg 39< 3957-74-9 Chlordane 2 ""39

" ""ug/kg 7.8< 7.8319-86-8 d-BHC 2 ""7.8

" ""ug/kg 3.9< 3.960-57-1 Dieldrin 2 ""3.9




" ""ug/kg 7.8< 7.872-20-8 Endrin 2 ""7.8



" ""ug/kg 1.6< 1.658-89-9 g-BHC 2 ""1.6

" ""ug/kg 7.8< 7.876-44-8 Heptachlor 2 ""7.8



" ""ug/kg 160< 1608001-35-2 Toxaphene 2 ""160


30-150 % " " ""% DCBP 56 "2051-24-3

30-150 % " " ""% TCMX 54 "877-09-8



SW8082A 04-May-1

9 07:34

"ug/kg 390< 39012674-11-2 PCB-1016 10 477265APH0618390

" ""ug/kg 390< 39011104-28-2 PCB-1221 10 ""390

" ""ug/kg 390< 39011141-16-5 PCB-1232 10 ""390

" ""ug/kg 390< 39053469-21-9 PCB-1242 10 ""390

" ""ug/kg 390< 39012672-29-6 PCB-1248 10 ""390

" ""ug/kg 390< 39011097-69-1 PCB-1254 10 ""390

" ""ug/kg 390< 39011096-82-5 PCB-1260 10 ""390

" ""ug/kg 390< 39037324-23-5 PCB-1262 10 ""390

" ""ug/kg 390< 39011100-14-4 PCB-1268 10 ""390


30-150 % " " ""% DCBP 69 "2051-24-3

30-150 % " " ""% TCMX 72 "877-09-8




SW8260C 04-May-1

9 17:48

04-May-1

9 13:30




Page 67 of 23109-May-19 16:45

B-3 6-8'


30-Apr-19 13:20


01-May-19

Client Project #

18EC0070 SoilSC54611-06





SW8260C 04-May-1

9 17:48

04-May-1

9 13:30

ug/kg 190< 19079-34-5 1,1,2,2-Tetrachloroethane 50 477679APH0618190






" ""ug/kg 320< 32096-18-4 1,2,3-Trichloropropane 50 ""320


" ""ug/kg 320< 32095-63-6 1,2,4-Trimethylbenzene 50 ""320

" ""ug/kg 320< 32096-12-8 1,2-Dibromo-3-chloroprop

ane

50 ""320










" ""ug/kg 320< 32095-49-8 2-Chlorotoluene 50 ""320

" ""ug/kg 24< 24591-78-6 2-Hexanone 1 ""24

" ""ug/kg 320< 320527-84-4 2-Isopropyltoluene 50 ""320



" ""ug/kg 240< 24067-64-1 Acetone 1 ""240


" ""ug/kg 4.8< 4.871-43-2 Benzene 1 ""4.8

" ""ug/kg 320< 320108-86-1 Bromobenzene 50 ""320



" ""ug/kg 4.8< 4.875-25-2 Bromoform 1 ""4.8


" ""ug/kg 4.87.675-15-0 Carbon Disulfide 1 ""4.8




" ""ug/kg 4.8< 4.867-66-3 Chloroform 1 ""4.8


" ""ug/kg 4.89.2156-59-2 cis-1,2-Dichloroethene 1 ""4.8






Page 68 of 23109-May-19 16:45

B-3 6-8'


30-Apr-19 13:20


01-May-19

Client Project #

18EC0070 SoilSC54611-06





SW8260C 04-May-1

9 17:48

04-May-1

9 13:30



" ""ug/kg 320< 32098-82-8 Isopropylbenzene 50 ""320

" ""ug/kg 4.8< 4.8179601-23-1 m&p-Xylene 1 ""4.8



(MTBE)

1 ""9.6



" ""ug/kg 320< 320104-51-8 n-Butylbenzene 50 ""320

" ""ug/kg 320< 320103-65-1 n-Propylbenzene 50 ""320

" ""ug/kg 4.8< 4.895-47-6 o-Xylene 1 ""4.8

" ""ug/kg 320< 32099-87-6 p-Isopropyltoluene 50 ""320

" ""ug/kg 320< 320135-98-8 sec-Butylbenzene 50 ""320

" ""ug/kg 4.8< 4.8100-42-5 Styrene 1 ""4.8

" ""ug/kg 320< 32098-06-6 tert-Butylbenzene 50 ""320



" ""ug/kg 4.8< 4.8108-88-3 Toluene 1 ""4.8





e

50 ""630









70-130 % " " ""% Toluene-d8 95 "2037-26-5




70-130 % SW8260C 04-May-19 17:27 477679A04-May-1

9 13:30

% 1,2-dichlorobenzene-d4 101 PH06182199-69-1



70-130 % " " ""% Toluene-d8 97 "2037-26-5





Page 69 of 23109-May-19 16:45

B-3 6-8'


30-Apr-19 13:20


01-May-19

Client Project #

18EC0070 SoilSC54611-06






SW8270D 02-May-1

9 09:44

01-May-1

9


e

1 477192APH0618270




















(m&p-cresol)

1 ""390





ether

1 ""390




ether

1 ""270






" ""ug/kg 390< 39062-53-3 Aniline 1 ""390

" ""ug/kg 270< 270120-12-7 Anthracene 1 ""270


" ""ug/kg 270< 27092-87-5 Benzidine 1 ""270







Page 70 of 23109-May-19 16:45

B-3 6-8'


30-Apr-19 13:20


01-May-19

Client Project #

18EC0070 SoilSC54611-06





SW8270D 02-May-1

9 09:44

01-May-1

9



ne

1 ""270



r

1 ""270


" ""ug/kg 390< 39086-74-8 Carbazole 1 ""390

" ""ug/kg 270< 270218-01-9 Chrysene 1 ""270








" ""ug/kg 270< 27086-73-7 Fluorene 1 ""270




e

1 ""270



" ""ug/kg 270< 27078-59-1 Isophorone 1 ""270









" ""ug/kg 270< 270108-95-2 Phenol 1 ""270

" ""ug/kg 270< 270129-00-0 Pyrene 1 ""270

" ""ug/kg 390< 390110-86-1 Pyridine 1 ""390


30-130 % " " ""% 2,4,6-Tribromophenol 117 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 71 "321-60-8

30-130 % " " ""% 2-Fluorophenol 67 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 77 "4165-60-0

30-130 % " " ""% Phenol-d5 69 "4165-62-2

30-130 % " " ""% Terphenyl-d14 73 "98904-43-9




Page 71 of 23109-May-19 16:45

B-3 6-8'


30-Apr-19 13:20


01-May-19

Client Project #

18EC0070 SoilSC54611-06






9 22:20

01-May-1

9 22:20





9 16:40

03-May-1

9 16:40




SW846-ReactCy

n

03-May-1

9 14:12

03-May-1

9



Page 72 of 23109-May-19 16:45

B-3 11-13'


30-Apr-19 13:40


01-May-19

Client Project #

18EC0070 SoilSC54611-07



SW846 1030 02-May-1

9 10:25

01-May-1

9 16:10


SW846 9045D 01-May-1

9 16:06

01-May-1

9 14:48







9 12:01

01-May-1

9


(C9-C36)

1 477191APH061860


50-150 % " " ""% n-Pentacosane 86 "629-99-2




SW6010D 03-May-1

9 13:03

02-May-1

9

mg/kg 0.791.127440-38-2 Arsenic 1 477321APH06180.79

" ""mg/kg 0.405.957440-39-3 Barium 1 ""0.40

" ""mg/kg 0.40< 0.407440-43-9 Cadmium 1 ""0.40

" ""mg/kg 0.4011.87440-47-3 Chromium 1 ""0.40

" ""mg/kg 0.402.907439-92-1 Lead 1 ""0.40

" ""mg/kg 1.6< 1.67782-49-2 Selenium 1 ""1.6

" ""mg/kg 0.40< 0.407440-22-4 Silver 1 ""0.40




SW6010D

(SPLP)

03-May-1

9 03:22

"mg/l 0.004< 0.0047440-38-2 SPLP Arsenic 1 477276APH06180.004

" ""mg/l 0.0100.0137440-39-3 SPLP Barium 1 ""0.010

" ""mg/l 0.005< 0.0057440-43-9 SPLP Cadmium 1 ""0.005


" ""mg/l 0.010< 0.0107439-92-1 SPLP Lead 1 ""0.010


" ""mg/l 0.010< 0.0107440-22-4 SPLP Silver 1 ""0.010



SW-7.3 03-May-1

9 16:40

03-May-1

9 16:40




SW7470A

(SPLP)

03-May-1

9 08:25

02-May-1

9




SW7471B 02-May-1

9 13:12

"mg/kg 0.03< 0.037439-97-6 Mercury 1 477261APH06180.03




SW8081B 03-May-1

9 21:11

"ug/kg 8.1< 8.172-54-8 4,4' -DDD 2 477266APH06188.1


Page 73 of 23109-May-19 16:45

B-3 11-13'


30-Apr-19 13:40


01-May-19

Client Project #

18EC0070 SoilSC54611-07





SW8081B 03-May-1

9 21:11

02-May-1

9

ug/kg 8.1< 8.172-55-9 4,4' -DDE 2 477266APH06188.1

" ""ug/kg 8.1< 8.150-29-3 4,4' -DDT 2 ""8.1

" ""ug/kg 8.1< 8.1319-84-6 a-BHC 2 ""8.1

" ""ug/kg 8.1< 8.115972-60-8 Alachlor 2 ""8.1

" ""ug/kg 4.1< 4.1309-00-2 Aldrin 2 ""4.1

" ""ug/kg 8.1< 8.1319-85-7 b-BHC 2 ""8.1

" ""ug/kg 41< 4157-74-9 Chlordane 2 ""41

" ""ug/kg 8.1< 8.1319-86-8 d-BHC 2 ""8.1

" ""ug/kg 4.1< 4.160-57-1 Dieldrin 2 ""4.1




" ""ug/kg 8.1< 8.172-20-8 Endrin 2 ""8.1



" ""ug/kg 1.6< 1.658-89-9 g-BHC 2 ""1.6

" ""ug/kg 8.1< 8.176-44-8 Heptachlor 2 ""8.1



" ""ug/kg 160< 1608001-35-2 Toxaphene 2 ""160


30-150 % " " ""% DCBP 56 "2051-24-3

30-150 % " " ""% TCMX 51 "877-09-8



SW8082A 04-May-1

9 06:27

"ug/kg 410< 41012674-11-2 PCB-1016 10 477265APH0618410

" ""ug/kg 410< 41011104-28-2 PCB-1221 10 ""410

" ""ug/kg 410< 41011141-16-5 PCB-1232 10 ""410

" ""ug/kg 410< 41053469-21-9 PCB-1242 10 ""410

" ""ug/kg 410< 41012672-29-6 PCB-1248 10 ""410

" ""ug/kg 410< 41011097-69-1 PCB-1254 10 ""410

" ""ug/kg 410< 41011096-82-5 PCB-1260 10 ""410

" ""ug/kg 410< 41037324-23-5 PCB-1262 10 ""410

" ""ug/kg 410< 41011100-14-4 PCB-1268 10 ""410


30-150 % " " ""% DCBP 65 "2051-24-3

30-150 % " " ""% TCMX 66 "877-09-8




SW8260C 04-May-1

9 03:13

01-May-1

9 22:12




Page 74 of 23109-May-19 16:45

B-3 11-13'


30-Apr-19 13:40


01-May-19

Client Project #

18EC0070 SoilSC54611-07





SW8260C 04-May-1

9 03:13

01-May-1

9 22:12











ane

1 ""5.1











" ""ug/kg 26< 26591-78-6 2-Hexanone 1 ""26




" ""ug/kg 260< 26067-64-1 Acetone 1 ""260


" ""ug/kg 5.1< 5.171-43-2 Benzene 1 ""5.1




" ""ug/kg 5.1< 5.175-25-2 Bromoform 1 ""5.1


" ""ug/kg 5.11375-15-0 Carbon Disulfide 1 ""5.1




" ""ug/kg 5.1< 5.167-66-3 Chloroform 1 ""5.1








Page 75 of 23109-May-19 16:45

B-3 11-13'


30-Apr-19 13:40


01-May-19

Client Project #

18EC0070 SoilSC54611-07





SW8260C 04-May-1

9 03:13

01-May-1

9 22:12




" ""ug/kg 5.1< 5.1179601-23-1 m&p-Xylene 1 ""5.1



(MTBE)

1 ""10





" ""ug/kg 5.1< 5.195-47-6 o-Xylene 1 ""5.1



" ""ug/kg 5.1< 5.1100-42-5 Styrene 1 ""5.1




" ""ug/kg 5.1< 5.1108-88-3 Toluene 1 ""5.1





e

1 ""10









70-130 % " " ""% Toluene-d8 100 "2037-26-5




SW8270D 02-May-1

9 10:08

01-May-1

9


e

1 477192APH0618290









Page 76 of 23109-May-19 16:45

B-3 11-13'


30-Apr-19 13:40


01-May-19

Client Project #

18EC0070 SoilSC54611-07





SW8270D 02-May-1

9 10:08

01-May-1

9













(m&p-cresol)

1 ""410





ether

1 ""410




ether

1 ""290






" ""ug/kg 410< 41062-53-3 Aniline 1 ""410

" ""ug/kg 290< 290120-12-7 Anthracene 1 ""290


" ""ug/kg 290< 29092-87-5 Benzidine 1 ""290








ne

1 ""290



r

1 ""290


" ""ug/kg 410< 41086-74-8 Carbazole 1 ""410

" ""ug/kg 290< 290218-01-9 Chrysene 1 ""290



Page 77 of 23109-May-19 16:45

B-3 11-13'


30-Apr-19 13:40


01-May-19

Client Project #

18EC0070 SoilSC54611-07





SW8270D 02-May-1

9 10:08

01-May-1

9







" ""ug/kg 290< 29086-73-7 Fluorene 1 ""290




e

1 ""290



" ""ug/kg 290< 29078-59-1 Isophorone 1 ""290









" ""ug/kg 290< 290108-95-2 Phenol 1 ""290

" ""ug/kg 290< 290129-00-0 Pyrene 1 ""290

" ""ug/kg 410< 410110-86-1 Pyridine 1 ""410


30-130 % " " ""% 2,4,6-Tribromophenol 112 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 69 "321-60-8

30-130 % " " ""% 2-Fluorophenol 64 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 72 "4165-60-0

30-130 % " " ""% Phenol-d5 68 "4165-62-2

30-130 % " " ""% Terphenyl-d14 71 "98904-43-9




9 22:20

01-May-1

9 22:20





9 16:40

03-May-1

9 16:40




SW846-ReactCy

n

03-May-1

9 14:13

03-May-1

9



Page 78 of 23109-May-19 16:45

B-4 0.4-1.8'


30-Apr-19 10:00


01-May-19

Client Project #

18EC0070 SoilSC54611-08



SW846 1030 02-May-1

9 10:25

01-May-1

9 16:10


SW846 9045D 01-May-1

9 16:09

01-May-1

9 14:48







9 20:25

01-May-1

9


(C9-C36)

1 477191APH061854


50-150 % " " ""% n-Pentacosane 79 "629-99-2




SW6010D 03-May-1

9 13:19

02-May-1

9

mg/kg 0.703.887440-38-2 Arsenic 1 477321APH06180.70

" ""mg/kg 0.3522.67440-39-3 Barium 1 ""0.35

" ""mg/kg 0.35< 0.357440-43-9 Cadmium 1 ""0.35

" ""mg/kg 0.3517.47440-47-3 Chromium 1 ""0.35

" ""mg/kg 0.3525.37439-92-1 Lead 1 ""0.35

" ""mg/kg 1.4< 1.47782-49-2 Selenium 1 ""1.4

" ""mg/kg 0.35< 0.357440-22-4 Silver 1 ""0.35




SW6010D

(SPLP)

03-May-1

9 03:25

"mg/l 0.0040.0057440-38-2 SPLP Arsenic 1 477276APH06180.004

" ""mg/l 0.0100.0467440-39-3 SPLP Barium 1 ""0.010

" ""mg/l 0.005< 0.0057440-43-9 SPLP Cadmium 1 ""0.005


" ""mg/l 0.0100.0207439-92-1 SPLP Lead 1 ""0.010


" ""mg/l 0.010< 0.0107440-22-4 SPLP Silver 1 ""0.010



SW-7.3 03-May-1

9 16:40

03-May-1

9 16:40




SW7470A

(SPLP)

03-May-1

9 08:27

02-May-1

9




SW7471B 02-May-1

9 13:14

"mg/kg 0.03< 0.037439-97-6 Mercury 1 477261APH06180.03




SW8081B 03-May-1

9 23:21

"ug/kg 7.1< 7.172-54-8 4,4' -DDD 2 477266APH06187.1


Page 79 of 23109-May-19 16:45

B-4 0.4-1.8'


30-Apr-19 10:00


01-May-19

Client Project #

18EC0070 SoilSC54611-08





SW8081B 03-May-1

9 23:21

02-May-1

9

ug/kg 7.1< 7.172-55-9 4,4' -DDE 2 477266APH06187.1

" ""ug/kg 7.11250-29-3 4,4' -DDT 2 ""7.1

" ""ug/kg 7.1< 7.1319-84-6 a-BHC 2 ""7.1

" ""ug/kg 7.1< 7.115972-60-8 Alachlor 2 ""7.1

" ""ug/kg 3.5< 3.5309-00-2 Aldrin 2 ""3.5

" ""ug/kg 7.1< 7.1319-85-7 b-BHC 2 ""7.1

" ""ug/kg 35< 3557-74-9 Chlordane 2 ""35

" ""ug/kg 7.1< 7.1319-86-8 d-BHC 2 ""7.1

" ""ug/kg 3.5< 3.560-57-1 Dieldrin 2 ""3.5




" ""ug/kg 7.1< 7.172-20-8 Endrin 2 ""7.1



" ""ug/kg 1.4< 1.458-89-9 g-BHC 2 ""1.4

" ""ug/kg 7.1< 7.176-44-8 Heptachlor 2 ""7.1



" ""ug/kg 140< 1408001-35-2 Toxaphene 2 ""140


30-150 % " " ""% DCBP 52 "2051-24-3

30-150 % " " ""% TCMX 53 "877-09-8



SW8082A 04-May-1

9 06:49

"ug/kg 350< 35012674-11-2 PCB-1016 10 477265APH0618350

" ""ug/kg 350< 35011104-28-2 PCB-1221 10 ""350

" ""ug/kg 350< 35011141-16-5 PCB-1232 10 ""350

" ""ug/kg 350< 35053469-21-9 PCB-1242 10 ""350

" ""ug/kg 350< 35012672-29-6 PCB-1248 10 ""350

" ""ug/kg 350< 35011097-69-1 PCB-1254 10 ""350

" ""ug/kg 350< 35011096-82-5 PCB-1260 10 ""350

" ""ug/kg 350< 35037324-23-5 PCB-1262 10 ""350

" ""ug/kg 350< 35011100-14-4 PCB-1268 10 ""350


30-150 % " " ""% DCBP 71 "2051-24-3

30-150 % " " ""% TCMX 74 "877-09-8




SW8260C 04-May-1

9 18:09

01-May-1

9 22:12




Page 80 of 23109-May-19 16:45

B-4 0.4-1.8'


30-Apr-19 10:00


01-May-19

Client Project #

18EC0070 SoilSC54611-08





SW8260C 04-May-1

9 18:09

01-May-1

9 22:12











ane

1 ""4.8











" ""ug/kg 24< 24591-78-6 2-Hexanone 1 ""24




" ""ug/kg 240< 24067-64-1 Acetone 1 ""240


" ""ug/kg 4.8< 4.871-43-2 Benzene 1 ""4.8




" ""ug/kg 4.8< 4.875-25-2 Bromoform 1 ""4.8






" ""ug/kg 4.8< 4.867-66-3 Chloroform 1 ""4.8








Page 81 of 23109-May-19 16:45

B-4 0.4-1.8'


30-Apr-19 10:00


01-May-19

Client Project #

18EC0070 SoilSC54611-08





SW8260C 04-May-1

9 18:09

01-May-1

9 22:12




" ""ug/kg 4.8< 4.8179601-23-1 m&p-Xylene 1 ""4.8



(MTBE)

1 ""9.7





" ""ug/kg 4.8< 4.895-47-6 o-Xylene 1 ""4.8



" ""ug/kg 4.8< 4.8100-42-5 Styrene 1 ""4.8




" ""ug/kg 4.8< 4.8108-88-3 Toluene 1 ""4.8





e

1 ""9.7









70-130 % " " ""% Toluene-d8 96 "2037-26-5




SW8270D 02-May-1

9 03:52

01-May-1

9


e

1 477192APH0618250









Page 82 of 23109-May-19 16:45

B-4 0.4-1.8'


30-Apr-19 10:00


01-May-19

Client Project #

18EC0070 SoilSC54611-08





SW8270D 02-May-1

9 03:52

01-May-1

9













(m&p-cresol)

1 ""360





ether

1 ""360




ether

1 ""250






" ""ug/kg 360< 36062-53-3 Aniline 1 ""360

" ""ug/kg 250< 250120-12-7 Anthracene 1 ""250


" ""ug/kg 250< 25092-87-5 Benzidine 1 ""250








ne

1 ""250



r

1 ""250


" ""ug/kg 360< 36086-74-8 Carbazole 1 ""360

" ""ug/kg 250440218-01-9 Chrysene 1 ""250



Page 83 of 23109-May-19 16:45

B-4 0.4-1.8'


30-Apr-19 10:00


01-May-19

Client Project #

18EC0070 SoilSC54611-08





SW8270D 02-May-1

9 03:52

01-May-1

9







" ""ug/kg 250< 25086-73-7 Fluorene 1 ""250




e

1 ""250


" ""ug/kg 250510193-39-5 Indeno(1,2,3-cd)pyrene 1 ""250

" ""ug/kg 250< 25078-59-1 Isophorone 1 ""250









" ""ug/kg 250< 250108-95-2 Phenol 1 ""250

" ""ug/kg 250700129-00-0 Pyrene 1 ""250

" ""ug/kg 360< 360110-86-1 Pyridine 1 ""360


30-130 % " " ""% 2,4,6-Tribromophenol 66 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 67 "321-60-8

30-130 % " " ""% 2-Fluorophenol 60 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 58 "4165-60-0

30-130 % " " ""% Phenol-d5 68 "4165-62-2

30-130 % " " ""% Terphenyl-d14 75 "98904-43-9




9 22:20

01-May-1

9 22:20





9 16:40

03-May-1

9 16:40




SW846-ReactCy

n

03-May-1

9 14:14

03-May-1

9



Page 84 of 23109-May-19 16:45

B-4 5.4-7.4'


30-Apr-19 10:30


01-May-19

Client Project #

18EC0070 SoilSC54611-09



SW846 1030 02-May-1

9 10:25

01-May-1

9 16:10


SW846 9045D 02-May-1

9 08:47

02-May-1

9 08:34

pH Units7.21 XpH 1 1900602TApH






9 19:57

01-May-1

9


(C9-C36)

1 477191APH061859


50-150 % " " ""% n-Pentacosane 82 "629-99-2




SW6010D 03-May-1

9 13:22

02-May-1

9

mg/kg 0.837.357440-38-2 Arsenic 1 477321APH06180.83

" ""mg/kg 0.4132.87440-39-3 Barium 1 ""0.41

" ""mg/kg 0.412.907440-43-9 Cadmium 1 ""0.41

" ""mg/kg 0.4131.87440-47-3 Chromium 1 ""0.41

" ""mg/kg 0.4122.17439-92-1 Lead 1 ""0.41

" ""mg/kg 1.7< 1.77782-49-2 Selenium 1 ""1.7

" ""mg/kg 0.41< 0.417440-22-4 Silver 1 ""0.41




SW6010D

(SPLP)

03-May-1

9 03:33


" ""mg/l 0.0100.0267440-39-3 SPLP Barium 1 ""0.010

" ""mg/l 0.005< 0.0057440-43-9 SPLP Cadmium 1 ""0.005


" ""mg/l 0.010< 0.0107439-92-1 SPLP Lead 1 ""0.010


" ""mg/l 0.010< 0.0107440-22-4 SPLP Silver 1 ""0.010



SW-7.3 03-May-1

9 16:38

03-May-1

9 16:38

mg/kg 2049Reactivity Sulfide 1 '[none]'PH061820



SW7470A

(SPLP)

03-May-1

9 08:29

02-May-1

9




SW7471B 02-May-1

9 13:17

"mg/kg 0.03< 0.037439-97-6 Mercury 1 477261APH06180.03




SW8081B 06-May-1

9 19:11

"ug/kg 8.0< 8.072-54-8 4,4' -DDD 2 477266APH06188.0


Page 85 of 23109-May-19 16:45

B-4 5.4-7.4'


30-Apr-19 10:30


01-May-19

Client Project #

18EC0070 SoilSC54611-09





SW8081B 06-May-1

9 19:11

02-May-1

9

ug/kg 8.0< 8.072-55-9 4,4' -DDE 2 477266APH06188.0

" ""ug/kg 8.0< 8.050-29-3 4,4' -DDT 2 ""8.0

" ""ug/kg 8.0< 8.0319-84-6 a-BHC 2 ""8.0

" ""ug/kg 8.0< 8.015972-60-8 Alachlor 2 ""8.0

" ""ug/kg 4.0< 4.0309-00-2 Aldrin 2 ""4.0

" ""ug/kg 8.0< 8.0319-85-7 b-BHC 2 ""8.0

" ""ug/kg 40< 4057-74-9 Chlordane 2 ""40

" ""ug/kg 8.0< 8.0319-86-8 d-BHC 2 ""8.0

" ""ug/kg 4.0< 4.060-57-1 Dieldrin 2 ""4.0




" ""ug/kg 8.0< 8.072-20-8 Endrin 2 ""8.0



" ""ug/kg 1.6< 1.658-89-9 g-BHC 2 ""1.6

" ""ug/kg 8.0< 8.076-44-8 Heptachlor 2 ""8.0



" ""ug/kg 160< 1608001-35-2 Toxaphene 2 ""160


30-150 % " " ""% DCBP 62 "2051-24-3

30-150 % " " ""% TCMX 54 "877-09-8



SW8082A 04-May-1

9 05:43

"ug/kg 400< 40012674-11-2 PCB-1016 10 477265APH0618400

" ""ug/kg 400< 40011104-28-2 PCB-1221 10 ""400

" ""ug/kg 400< 40011141-16-5 PCB-1232 10 ""400

" ""ug/kg 400< 40053469-21-9 PCB-1242 10 ""400

" ""ug/kg 400< 40012672-29-6 PCB-1248 10 ""400

" ""ug/kg 400< 40011097-69-1 PCB-1254 10 ""400

" ""ug/kg 400< 40011096-82-5 PCB-1260 10 ""400

" ""ug/kg 400< 40037324-23-5 PCB-1262 10 ""400

" ""ug/kg 400< 40011100-14-4 PCB-1268 10 ""400


30-150 % " " ""% DCBP 63 "2051-24-3

30-150 % " " ""% TCMX 60 "877-09-8




SW8260C 04-May-1

9 18:31

04-May-1

9 13:32




Page 86 of 23109-May-19 16:45

B-4 5.4-7.4'


30-Apr-19 10:30


01-May-19

Client Project #

18EC0070 SoilSC54611-09





SW8260C 04-May-1

9 18:31

04-May-1

9 13:32











ane

1 ""4.4


" ""ug/kg 4.42795-50-1 1,2-Dichlorobenzene 1 ""4.4









" ""ug/kg 22< 22591-78-6 2-Hexanone 1 ""22




" ""ug/kg 220< 22067-64-1 Acetone 1 ""220


" ""ug/kg 4.4< 4.471-43-2 Benzene 1 ""4.4




" ""ug/kg 4.4< 4.475-25-2 Bromoform 1 ""4.4






" ""ug/kg 4.4< 4.467-66-3 Chloroform 1 ""4.4


" ""ug/kg 4.44.7156-59-2 cis-1,2-Dichloroethene 1 ""4.4






Page 87 of 23109-May-19 16:45

B-4 5.4-7.4'


30-Apr-19 10:30


01-May-19

Client Project #

18EC0070 SoilSC54611-09





SW8260C 04-May-1

9 18:31

04-May-1

9 13:32




" ""ug/kg 4.4< 4.4179601-23-1 m&p-Xylene 1 ""4.4

" ""ug/kg 265978-93-3 Methyl Ethyl Ketone 1 ""26


(MTBE)

1 ""8.8





" ""ug/kg 4.4< 4.495-47-6 o-Xylene 1 ""4.4



" ""ug/kg 4.4< 4.4100-42-5 Styrene 1 ""4.4




" ""ug/kg 4.4< 4.4108-88-3 Toluene 1 ""4.4





e

1 ""8.8









70-130 % " " ""% Toluene-d8 96 "2037-26-5




SW8270D 02-May-1

9 10:32

01-May-1

9


e

1 477192APH0618280









Page 88 of 23109-May-19 16:45

B-4 5.4-7.4'


30-Apr-19 10:30


01-May-19

Client Project #

18EC0070 SoilSC54611-09





SW8270D 02-May-1

9 10:32

01-May-1

9













(m&p-cresol)

1 ""400





ether

1 ""400




ether

1 ""280






" ""ug/kg 400< 40062-53-3 Aniline 1 ""400

" ""ug/kg 280< 280120-12-7 Anthracene 1 ""280


" ""ug/kg 280< 28092-87-5 Benzidine 1 ""280








ne

1 ""280



r

1 ""280


" ""ug/kg 400< 40086-74-8 Carbazole 1 ""400

" ""ug/kg 280< 280218-01-9 Chrysene 1 ""280



Page 89 of 23109-May-19 16:45

B-4 5.4-7.4'


30-Apr-19 10:30


01-May-19

Client Project #

18EC0070 SoilSC54611-09





SW8270D 02-May-1

9 10:32

01-May-1

9







" ""ug/kg 280< 28086-73-7 Fluorene 1 ""280




e

1 ""280



" ""ug/kg 280< 28078-59-1 Isophorone 1 ""280









" ""ug/kg 280< 280108-95-2 Phenol 1 ""280

" ""ug/kg 280< 280129-00-0 Pyrene 1 ""280

" ""ug/kg 400< 400110-86-1 Pyridine 1 ""400


30-130 % " " ""% 2,4,6-Tribromophenol 118 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 69 "321-60-8

30-130 % " " ""% 2-Fluorophenol 64 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 71 "4165-60-0

30-130 % " " ""% Phenol-d5 68 "4165-62-2

30-130 % " " ""% Terphenyl-d14 70 "98904-43-9




9 22:20

01-May-1

9 22:20





9 16:38

03-May-1

9 16:38




SW846-ReactCy

n

03-May-1

9 14:15

03-May-1

9



Page 90 of 23109-May-19 16:45

B-4 11.8-13.8'


30-Apr-19 10:45


01-May-19

Client Project #

18EC0070 SoilSC54611-10



SW846 1030 02-May-1

9 10:25

01-May-1

9 16:10


SW846 9045D 02-May-1

9 09:01

02-May-1

9 08:34







9 23:47

01-May-1

9


(C9-C36)

1 477191APH061861


50-150 % " " ""% n-Pentacosane 82 "629-99-2




SW6010D 03-May-1

9 14:07

02-May-1

9

mg/kg 0.891.917440-38-2 Arsenic 1 477321APH06180.89

" ""mg/kg 0.456.747440-39-3 Barium 1 ""0.45

" ""mg/kg 0.45< 0.457440-43-9 Cadmium 1 ""0.45

" ""mg/kg 0.4514.57440-47-3 Chromium 1 ""0.45

" ""mg/kg 0.453.767439-92-1 Lead 1 ""0.45

" ""mg/kg 1.8< 1.87782-49-2 Selenium 1 ""1.8

" ""mg/kg 0.45< 0.457440-22-4 Silver 1 ""0.45




SW6010D

(SPLP)

03-May-1

9 03:36

"mg/l 0.004< 0.0047440-38-2 SPLP Arsenic 1 477276APH06180.004

" ""mg/l 0.0100.0147440-39-3 SPLP Barium 1 ""0.010

" ""mg/l 0.005< 0.0057440-43-9 SPLP Cadmium 1 ""0.005


" ""mg/l 0.010< 0.0107439-92-1 SPLP Lead 1 ""0.010


" ""mg/l 0.010< 0.0107440-22-4 SPLP Silver 1 ""0.010



SW-7.3 03-May-1

9 16:40

03-May-1

9 16:40




SW7470A

(SPLP)

03-May-1

9 08:31

02-May-1

9




SW7471B 02-May-1

9 13:23

"mg/kg 0.03< 0.037439-97-6 Mercury 1 477261APH06180.03




SW8081B 03-May-1

9 17:29

"ug/kg 8.2< 8.272-54-8 4,4' -DDD 2 477266APH06188.2


Page 91 of 23109-May-19 16:45

B-4 11.8-13.8'


30-Apr-19 10:45


01-May-19

Client Project #

18EC0070 SoilSC54611-10





SW8081B 03-May-1

9 17:29

02-May-1

9

ug/kg 8.2< 8.272-55-9 4,4' -DDE 2 477266APH06188.2

" ""ug/kg 8.2< 8.250-29-3 4,4' -DDT 2 ""8.2

" ""ug/kg 8.2< 8.2319-84-6 a-BHC 2 ""8.2

" ""ug/kg 8.2< 8.215972-60-8 Alachlor 2 ""8.2

" ""ug/kg 4.1< 4.1309-00-2 Aldrin 2 ""4.1

" ""ug/kg 8.2< 8.2319-85-7 b-BHC 2 ""8.2

" ""ug/kg 41< 4157-74-9 Chlordane 2 ""41

" ""ug/kg 8.2< 8.2319-86-8 d-BHC 2 ""8.2

" ""ug/kg 4.1< 4.160-57-1 Dieldrin 2 ""4.1




" ""ug/kg 8.2< 8.272-20-8 Endrin 2 ""8.2



" ""ug/kg 1.6< 1.658-89-9 g-BHC 2 ""1.6

" ""ug/kg 8.2< 8.276-44-8 Heptachlor 2 ""8.2



" ""ug/kg 160< 1608001-35-2 Toxaphene 2 ""160


30-150 % " " ""% DCBP 56 "2051-24-3

30-150 % " " ""% TCMX 50 "877-09-8



SW8082A 04-May-1

9 06:05

"ug/kg 410< 41012674-11-2 PCB-1016 10 477265APH0618410

" ""ug/kg 410< 41011104-28-2 PCB-1221 10 ""410

" ""ug/kg 410< 41011141-16-5 PCB-1232 10 ""410

" ""ug/kg 410< 41053469-21-9 PCB-1242 10 ""410

" ""ug/kg 410< 41012672-29-6 PCB-1248 10 ""410

" ""ug/kg 410< 41011097-69-1 PCB-1254 10 ""410

" ""ug/kg 410< 41011096-82-5 PCB-1260 10 ""410

" ""ug/kg 410< 41037324-23-5 PCB-1262 10 ""410

" ""ug/kg 410< 41011100-14-4 PCB-1268 10 ""410


30-150 % " " ""% DCBP 65 "2051-24-3

30-150 % " " ""% TCMX 70 "877-09-8




SW8260C 04-May-1

9 18:52

04-May-1

9 13:32




Page 92 of 23109-May-19 16:45

B-4 11.8-13.8'


30-Apr-19 10:45


01-May-19

Client Project #

18EC0070 SoilSC54611-10





SW8260C 04-May-1

9 18:52

04-May-1

9 13:32



" ""ug/kg 5.78875-34-3 1,1-Dichloroethane 1 ""5.7








ane

1 ""5.7











" ""ug/kg 28< 28591-78-6 2-Hexanone 1 ""28




" ""ug/kg 280< 28067-64-1 Acetone 1 ""280


" ""ug/kg 5.7< 5.771-43-2 Benzene 1 ""5.7




" ""ug/kg 5.7< 5.775-25-2 Bromoform 1 ""5.7





" ""ug/kg 5.715075-00-3 Chloroethane 1 ""5.7

" ""ug/kg 5.7< 5.767-66-3 Chloroform 1 ""5.7


" ""ug/kg 5.7130156-59-2 cis-1,2-Dichloroethene 1 ""5.7






Page 93 of 23109-May-19 16:45

B-4 11.8-13.8'


30-Apr-19 10:45


01-May-19

Client Project #

18EC0070 SoilSC54611-10





SW8260C 04-May-1

9 18:52

04-May-1

9 13:32




" ""ug/kg 5.7< 5.7179601-23-1 m&p-Xylene 1 ""5.7



(MTBE)

1 ""11





" ""ug/kg 5.7< 5.795-47-6 o-Xylene 1 ""5.7



" ""ug/kg 5.7< 5.7100-42-5 Styrene 1 ""5.7


" ""ug/kg 5.76.3127-18-4 Tetrachloroethene 1 ""5.7


" ""ug/kg 5.7< 5.7108-88-3 Toluene 1 ""5.7





e

1 ""11

" ""ug/kg 5.71179-01-6 Trichloroethene 1 ""5.7



" ""ug/kg 5.79175-01-4 Vinyl chloride 1 ""5.7





70-130 % " " ""% Toluene-d8 96 "2037-26-5




SW8270D 02-May-1

9 10:55

01-May-1

9


e

1 477192APH0618290









Page 94 of 23109-May-19 16:45

B-4 11.8-13.8'


30-Apr-19 10:45


01-May-19

Client Project #

18EC0070 SoilSC54611-10





SW8270D 02-May-1

9 10:55

01-May-1

9













(m&p-cresol)

1 ""410





ether

1 ""410




ether

1 ""290






" ""ug/kg 410< 41062-53-3 Aniline 1 ""410

" ""ug/kg 290< 290120-12-7 Anthracene 1 ""290


" ""ug/kg 290< 29092-87-5 Benzidine 1 ""290








ne

1 ""290



r

1 ""290


" ""ug/kg 410< 41086-74-8 Carbazole 1 ""410

" ""ug/kg 290< 290218-01-9 Chrysene 1 ""290



Page 95 of 23109-May-19 16:45

B-4 11.8-13.8'


30-Apr-19 10:45


01-May-19

Client Project #

18EC0070 SoilSC54611-10





SW8270D 02-May-1

9 10:55

01-May-1

9







" ""ug/kg 290< 29086-73-7 Fluorene 1 ""290




e

1 ""290



" ""ug/kg 290< 29078-59-1 Isophorone 1 ""290









" ""ug/kg 290< 290108-95-2 Phenol 1 ""290

" ""ug/kg 290< 290129-00-0 Pyrene 1 ""290

" ""ug/kg 410< 410110-86-1 Pyridine 1 ""410


30-130 % " " ""% 2,4,6-Tribromophenol 101 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 65 "321-60-8

30-130 % " " ""% 2-Fluorophenol 64 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 72 "4165-60-0

30-130 % " " ""% Phenol-d5 65 "4165-62-2

30-130 % " " ""% Terphenyl-d14 65 "98904-43-9




9 22:20

01-May-1

9 22:20





9 16:40

03-May-1

9 16:40




SW846-ReactCy

n

03-May-1

9 14:16

03-May-1

9



Page 96 of 23109-May-19 16:45

B-5 1.7-2.8'


30-Apr-19 09:10


01-May-19

Client Project #

18EC0070 SoilSC54611-11



SW846 1030 02-May-1

9 10:25

01-May-1

9 16:10


SW846 9045D 02-May-1

9 09:03

02-May-1

9 08:34







9 11:33

01-May-1

9


(C9-C36)

1 477191APH061857


50-150 % " " ""% n-Pentacosane 94 "629-99-2




SW6010D 03-May-1

9 14:10

02-May-1

9

mg/kg 0.693.787440-38-2 Arsenic 1 477321APH06180.69

" ""mg/kg 0.3511.77440-39-3 Barium 1 ""0.35

" ""mg/kg 0.35< 0.357440-43-9 Cadmium 1 ""0.35

" ""mg/kg 0.3513.77440-47-3 Chromium 1 ""0.35

" ""mg/kg 0.3510.07439-92-1 Lead 1 ""0.35

" ""mg/kg 1.4< 1.47782-49-2 Selenium 1 ""1.4

" ""mg/kg 0.35< 0.357440-22-4 Silver 1 ""0.35




SW6010D

(SPLP)

03-May-1

9 03:38


" ""mg/l 0.0100.0337440-39-3 SPLP Barium 1 ""0.010

" ""mg/l 0.005< 0.0057440-43-9 SPLP Cadmium 1 ""0.005


" ""mg/l 0.010< 0.0107439-92-1 SPLP Lead 1 ""0.010


" ""mg/l 0.010< 0.0107440-22-4 SPLP Silver 1 ""0.010



SW-7.3 03-May-1

9 16:40

03-May-1

9 16:40




SW7470A

(SPLP)

03-May-1

9 08:33

02-May-1

9




SW7471B 02-May-1

9 13:25

"mg/kg 0.030.037439-97-6 Mercury 1 477261APH06180.03




SW8081B 03-May-1

9 21:48

"ug/kg 7.5< 7.572-54-8 4,4' -DDD 2 477266APH06187.5


Page 97 of 23109-May-19 16:45

B-5 1.7-2.8'


30-Apr-19 09:10


01-May-19

Client Project #

18EC0070 SoilSC54611-11





SW8081B 03-May-1

9 21:48

02-May-1

9

ug/kg 7.5< 7.572-55-9 4,4' -DDE 2 477266APH06187.5

" ""ug/kg 7.5< 7.550-29-3 4,4' -DDT 2 ""7.5

" ""ug/kg 7.5< 7.5319-84-6 a-BHC 2 ""7.5

" ""ug/kg 7.5< 7.515972-60-8 Alachlor 2 ""7.5

" ""ug/kg 3.8< 3.8309-00-2 Aldrin 2 ""3.8

" ""ug/kg 7.5< 7.5319-85-7 b-BHC 2 ""7.5

" ""ug/kg 38< 3857-74-9 Chlordane 2 ""38

" ""ug/kg 7.5< 7.5319-86-8 d-BHC 2 ""7.5

" ""ug/kg 3.8< 3.860-57-1 Dieldrin 2 ""3.8




" ""ug/kg 7.5< 7.572-20-8 Endrin 2 ""7.5



" ""ug/kg 1.5< 1.558-89-9 g-BHC 2 ""1.5

" ""ug/kg 7.5< 7.576-44-8 Heptachlor 2 ""7.5



" ""ug/kg 150< 1508001-35-2 Toxaphene 2 ""150


30-150 % " " ""% DCBP 58 "2051-24-3

30-150 % " " ""% TCMX 53 "877-09-8



SW8082A 04-May-1

9 00:29

"ug/kg 380< 38012674-11-2 PCB-1016 10 477265APH0618380

" ""ug/kg 380< 38011104-28-2 PCB-1221 10 ""380

" ""ug/kg 380< 38011141-16-5 PCB-1232 10 ""380

" ""ug/kg 380< 38053469-21-9 PCB-1242 10 ""380

" ""ug/kg 380< 38012672-29-6 PCB-1248 10 ""380

" ""ug/kg 380< 38011097-69-1 PCB-1254 10 ""380

" ""ug/kg 380< 38011096-82-5 PCB-1260 10 ""380

" ""ug/kg 380< 38037324-23-5 PCB-1262 10 ""380

" ""ug/kg 380< 38011100-14-4 PCB-1268 10 ""380


30-150 % " " ""% DCBP 84 "2051-24-3

30-150 % " " ""% TCMX 80 "877-09-8




SW8260C 06-May-1

9 10:59

04-May-1

9 13:33




Page 98 of 23109-May-19 16:45

B-5 1.7-2.8'


30-Apr-19 09:10


01-May-19

Client Project #

18EC0070 SoilSC54611-11





SW8260C 06-May-1

9 10:59

04-May-1

9 13:33

ug/kg 5.1< 5.179-00-5 1,1,2-Trichloroethane 1 477679APH06185.1









" ""ug/kg 25< 25591-78-6 2-Hexanone 1 ""25


" ""ug/kg 250< 25067-64-1 Acetone 1 ""250




" ""ug/kg 5.1< 5.175-25-2 Bromoform 1 ""5.1






" ""ug/kg 5.1< 5.167-66-3 Chloroform 1 ""5.1







" ""ug/kg 5.1< 5.1179601-23-1 m&p-Xylene 1 ""5.1



(MTBE)

1 ""10


" ""ug/kg 5.1< 5.195-47-6 o-Xylene 1 ""5.1

" ""ug/kg 5.1< 5.1100-42-5 Styrene 1 ""5.1



" ""ug/kg 5.1< 5.1108-88-3 Toluene 1 ""5.1








Page 99 of 23109-May-19 16:45

B-5 1.7-2.8'


30-Apr-19 09:10


01-May-19

Client Project #

18EC0070 SoilSC54611-11





SW8260C 06-May-1

9 10:59

04-May-1

9 13:33

ug/kg 5.1< 5.175-01-4 Vinyl chloride 1 477679APH06185.1





70-130 % " " ""% Toluene-d8 94 "2037-26-5



SW8260C 06-May-1

9 10:59

06-May-1

9 10:28





" ""ug/kg 13016095-63-6 1,2,4-Trimethylbenzene 50 ""130


ane

50 ""210








" ""ug/kg 21024071-43-2 Benzene 50 ""210


" ""ug/kg 86110100-41-4 Ethylbenzene 50 ""86



" ""ug/kg 21057091-20-3 Naphthalene 50 ""210







e

50 ""430





70-130 % " " ""% Toluene-d8 97 "2037-26-5





Page 100 of 23109-May-19 16:45

B-5 1.7-2.8'


30-Apr-19 09:10


01-May-19

Client Project #

18EC0070 SoilSC54611-11






SW8270D 02-May-1

9 04:17

01-May-1

9


e

1 477192APH0618260




















(m&p-cresol)

1 ""380





ether

1 ""380




ether

1 ""260






" ""ug/kg 380< 38062-53-3 Aniline 1 ""380

" ""ug/kg 260< 260120-12-7 Anthracene 1 ""260


" ""ug/kg 260< 26092-87-5 Benzidine 1 ""260







Page 101 of 23109-May-19 16:45

B-5 1.7-2.8'


30-Apr-19 09:10


01-May-19

Client Project #

18EC0070 SoilSC54611-11





SW8270D 02-May-1

9 04:17

01-May-1

9



ne

1 ""260



r

1 ""260


" ""ug/kg 380< 38086-74-8 Carbazole 1 ""380

" ""ug/kg 260< 260218-01-9 Chrysene 1 ""260








" ""ug/kg 260< 26086-73-7 Fluorene 1 ""260




e

1 ""260



" ""ug/kg 260< 26078-59-1 Isophorone 1 ""260









" ""ug/kg 260< 260108-95-2 Phenol 1 ""260

" ""ug/kg 260< 260129-00-0 Pyrene 1 ""260

" ""ug/kg 380< 380110-86-1 Pyridine 1 ""380


30-130 % " " ""% 2,4,6-Tribromophenol 67 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 63 "321-60-8

30-130 % " " ""% 2-Fluorophenol 63 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 59 "4165-60-0

30-130 % " " ""% Phenol-d5 69 "4165-62-2

30-130 % " " ""% Terphenyl-d14 72 "98904-43-9




Page 102 of 23109-May-19 16:45

B-5 1.7-2.8'


30-Apr-19 09:10


01-May-19

Client Project #

18EC0070 SoilSC54611-11






9 22:20

01-May-1

9 22:20





9 16:40

03-May-1

9 16:40




SW846-ReactCy

n

03-May-1

9 14:17

03-May-1

9



Page 103 of 23109-May-19 16:45

B-5 5-7'


30-Apr-19 09:30


01-May-19

Client Project #

18EC0070 SoilSC54611-12



SW846 1030 02-May-1

9 10:25

01-May-1

9 16:10


SW846 9045D 02-May-1

9 09:06

02-May-1

9 08:34







9 11:05

01-May-1

9


(C9-C36)

1 477191APH061863


50-150 % " " ""% n-Pentacosane 93 "629-99-2




SW6010D 03-May-1

9 14:13

02-May-1

9

mg/kg 0.882.707440-38-2 Arsenic 1 477321APH06180.88

" ""mg/kg 0.449.717440-39-3 Barium 1 ""0.44

" ""mg/kg 0.44< 0.447440-43-9 Cadmium 1 ""0.44

" ""mg/kg 0.4412.77440-47-3 Chromium 1 ""0.44

" ""mg/kg 0.442.687439-92-1 Lead 1 ""0.44

" ""mg/kg 1.8< 1.87782-49-2 Selenium 1 ""1.8

" ""mg/kg 0.44< 0.447440-22-4 Silver 1 ""0.44




SW6010D

(SPLP)

03-May-1

9 03:41


" ""mg/l 0.0100.0187440-39-3 SPLP Barium 1 ""0.010

" ""mg/l 0.005< 0.0057440-43-9 SPLP Cadmium 1 ""0.005


" ""mg/l 0.010< 0.0107439-92-1 SPLP Lead 1 ""0.010


" ""mg/l 0.010< 0.0107440-22-4 SPLP Silver 1 ""0.010



SW-7.3 03-May-1

9 16:40

03-May-1

9 16:40




SW7470A

(SPLP)

03-May-1

9 08:36

02-May-1

9




SW7471B 02-May-1

9 13:28

"mg/kg 0.03< 0.037439-97-6 Mercury 1 477261APH06180.03




SW8081B 03-May-1

9 22:07

"ug/kg 8.6< 8.672-54-8 4,4' -DDD 2 477266APH06188.6


Page 104 of 23109-May-19 16:45

B-5 5-7'


30-Apr-19 09:30


01-May-19

Client Project #

18EC0070 SoilSC54611-12





SW8081B 03-May-1

9 22:07

02-May-1

9

ug/kg 8.6< 8.672-55-9 4,4' -DDE 2 477266APH06188.6

" ""ug/kg 8.6< 8.650-29-3 4,4' -DDT 2 ""8.6

" ""ug/kg 8.6< 8.6319-84-6 a-BHC 2 ""8.6

" ""ug/kg 8.6< 8.615972-60-8 Alachlor 2 ""8.6

" ""ug/kg 4.3< 4.3309-00-2 Aldrin 2 ""4.3

" ""ug/kg 8.6< 8.6319-85-7 b-BHC 2 ""8.6

" ""ug/kg 43< 4357-74-9 Chlordane 2 ""43

" ""ug/kg 8.6< 8.6319-86-8 d-BHC 2 ""8.6

" ""ug/kg 4.3< 4.360-57-1 Dieldrin 2 ""4.3




" ""ug/kg 8.6< 8.672-20-8 Endrin 2 ""8.6



" ""ug/kg 1.7< 1.758-89-9 g-BHC 2 ""1.7

" ""ug/kg 8.6< 8.676-44-8 Heptachlor 2 ""8.6



" ""ug/kg 170< 1708001-35-2 Toxaphene 2 ""170


30-150 % " " ""% DCBP 61 "2051-24-3

30-150 % " " ""% TCMX 55 "877-09-8



SW8082A 04-May-1

9 00:51

"ug/kg 430< 43012674-11-2 PCB-1016 10 477265APH0618430

" ""ug/kg 430< 43011104-28-2 PCB-1221 10 ""430

" ""ug/kg 430< 43011141-16-5 PCB-1232 10 ""430

" ""ug/kg 430< 43053469-21-9 PCB-1242 10 ""430

" ""ug/kg 430< 43012672-29-6 PCB-1248 10 ""430

" ""ug/kg 430< 43011097-69-1 PCB-1254 10 ""430

" ""ug/kg 430< 43011096-82-5 PCB-1260 10 ""430

" ""ug/kg 430< 43037324-23-5 PCB-1262 10 ""430

" ""ug/kg 430< 43011100-14-4 PCB-1268 10 ""430


30-150 % " " ""% DCBP 79 "2051-24-3

30-150 % " " ""% TCMX 76 "877-09-8




SW8260C 04-May-1

9 19:34

01-May-1

9 22:12




Page 105 of 23109-May-19 16:45

B-5 5-7'


30-Apr-19 09:30


01-May-19

Client Project #

18EC0070 SoilSC54611-12





SW8260C 04-May-1

9 19:34

01-May-1

9 22:12











ane

1 ""5.4











" ""ug/kg 27< 27591-78-6 2-Hexanone 1 ""27




" ""ug/kg 270< 27067-64-1 Acetone 1 ""270


" ""ug/kg 5.41971-43-2 Benzene 1 ""5.4




" ""ug/kg 5.4< 5.475-25-2 Bromoform 1 ""5.4






" ""ug/kg 5.4< 5.467-66-3 Chloroform 1 ""5.4








Page 106 of 23109-May-19 16:45

B-5 5-7'


30-Apr-19 09:30


01-May-19

Client Project #

18EC0070 SoilSC54611-12





SW8260C 04-May-1

9 19:34

01-May-1

9 22:12




" ""ug/kg 5.4< 5.4179601-23-1 m&p-Xylene 1 ""5.4



(MTBE)

1 ""11





" ""ug/kg 5.4< 5.495-47-6 o-Xylene 1 ""5.4



" ""ug/kg 5.4< 5.4100-42-5 Styrene 1 ""5.4




" ""ug/kg 5.4< 5.4108-88-3 Toluene 1 ""5.4





e

1 ""11









70-130 % " " ""% Toluene-d8 96 "2037-26-5




SW8270D 02-May-1

9 04:42

01-May-1

9


e

1 477192APH0618300









Page 107 of 23109-May-19 16:45

B-5 5-7'


30-Apr-19 09:30


01-May-19

Client Project #

18EC0070 SoilSC54611-12





SW8270D 02-May-1

9 04:42

01-May-1

9













(m&p-cresol)

1 ""430





ether

1 ""430




ether

1 ""300






" ""ug/kg 430< 43062-53-3 Aniline 1 ""430

" ""ug/kg 300< 300120-12-7 Anthracene 1 ""300


" ""ug/kg 300< 30092-87-5 Benzidine 1 ""300








ne

1 ""300



r

1 ""300


" ""ug/kg 430< 43086-74-8 Carbazole 1 ""430

" ""ug/kg 300< 300218-01-9 Chrysene 1 ""300



Page 108 of 23109-May-19 16:45

B-5 5-7'


30-Apr-19 09:30


01-May-19

Client Project #

18EC0070 SoilSC54611-12





SW8270D 02-May-1

9 04:42

01-May-1

9







" ""ug/kg 300< 30086-73-7 Fluorene 1 ""300




e

1 ""300



" ""ug/kg 300< 30078-59-1 Isophorone 1 ""300









" ""ug/kg 300< 300108-95-2 Phenol 1 ""300

" ""ug/kg 300< 300129-00-0 Pyrene 1 ""300

" ""ug/kg 430< 430110-86-1 Pyridine 1 ""430


30-130 % " " ""% 2,4,6-Tribromophenol 72 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 68 "321-60-8

30-130 % " " ""% 2-Fluorophenol 71 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 67 "4165-60-0

30-130 % " " ""% Phenol-d5 76 "4165-62-2

30-130 % " " ""% Terphenyl-d14 75 "98904-43-9




9 22:20

01-May-1

9 22:20





9 16:40

03-May-1

9 16:40




SW846-ReactCy

n

03-May-1

9 14:19

03-May-1

9



Page 109 of 23109-May-19 16:45

B-6 0.4-1.7'


30-Apr-19 14:15


01-May-19

Client Project #

18EC0070 SoilSC54611-13



SW846 1030 02-May-1

9 10:25

01-May-1

9 16:10


SW846 9045D 02-May-1

9 09:11

02-May-1

9 08:34







9 06:47

01-May-1

9


(C9-C36)

1 477191APH061853


50-150 % " " ""% n-Pentacosane 70 "629-99-2




SW6010D 03-May-1

9 14:17

02-May-1

9

mg/kg 0.6723.37440-38-2 Arsenic 1 477321APH06180.67

" ""mg/kg 0.3427.17440-39-3 Barium 1 ""0.34

" ""mg/kg 0.340.377440-43-9 Cadmium 1 ""0.34

" ""mg/kg 0.3433.07440-47-3 Chromium 1 ""0.34

" ""mg/kg 0.3445.97439-92-1 Lead 1 ""0.34

" ""mg/kg 1.3< 1.37782-49-2 Selenium 1 ""1.3

" ""mg/kg 0.34< 0.347440-22-4 Silver 1 ""0.34




SW6010D

(SPLP)

03-May-1

9 03:44


" ""mg/l 0.0100.0257440-39-3 SPLP Barium 1 ""0.010

" ""mg/l 0.005< 0.0057440-43-9 SPLP Cadmium 1 ""0.005


" ""mg/l 0.010< 0.0107439-92-1 SPLP Lead 1 ""0.010


" ""mg/l 0.010< 0.0107440-22-4 SPLP Silver 1 ""0.010



SW-7.3 03-May-1

9 16:40

03-May-1

9 16:40




SW7470A

(SPLP)

03-May-1

9 08:38

02-May-1

9




SW7471B 02-May-1

9 13:30

"mg/kg 0.03< 0.037439-97-6 Mercury 1 477261APH06180.03




SW8081B 03-May-1

9 22:26

"ug/kg 7.1< 7.172-54-8 4,4' -DDD 2 477266APH06187.1


Page 110 of 23109-May-19 16:45

B-6 0.4-1.7'


30-Apr-19 14:15


01-May-19

Client Project #

18EC0070 SoilSC54611-13





SW8081B 03-May-1

9 22:26

02-May-1

9

ug/kg 7.1< 7.172-55-9 4,4' -DDE 2 477266APH06187.1

" ""ug/kg 7.1< 7.150-29-3 4,4' -DDT 2 ""7.1

" ""ug/kg 7.1< 7.1319-84-6 a-BHC 2 ""7.1

" ""ug/kg 7.1< 7.115972-60-8 Alachlor 2 ""7.1

" ""ug/kg 3.6< 3.6309-00-2 Aldrin 2 ""3.6

" ""ug/kg 7.1< 7.1319-85-7 b-BHC 2 ""7.1

" ""ug/kg 36< 3657-74-9 Chlordane 2 ""36

" ""ug/kg 7.1< 7.1319-86-8 d-BHC 2 ""7.1

" ""ug/kg 3.6< 3.660-57-1 Dieldrin 2 ""3.6




" ""ug/kg 7.1< 7.172-20-8 Endrin 2 ""7.1



" ""ug/kg 1.4< 1.458-89-9 g-BHC 2 ""1.4

" ""ug/kg 7.1< 7.176-44-8 Heptachlor 2 ""7.1



" ""ug/kg 140< 1408001-35-2 Toxaphene 2 ""140


30-150 % " " ""% DCBP 60 "2051-24-3

30-150 % " " ""% TCMX 58 "877-09-8



SW8082A 03-May-1

9 18:40

"ug/kg 360< 36012674-11-2 PCB-1016 10 477265APH0618360

" ""ug/kg 360< 36011104-28-2 PCB-1221 10 ""360

" ""ug/kg 360< 36011141-16-5 PCB-1232 10 ""360

" ""ug/kg 360< 36053469-21-9 PCB-1242 10 ""360

" ""ug/kg 360< 36012672-29-6 PCB-1248 10 ""360

" ""ug/kg 360< 36011097-69-1 PCB-1254 10 ""360

" ""ug/kg 360< 36011096-82-5 PCB-1260 10 ""360

" ""ug/kg 360< 36037324-23-5 PCB-1262 10 ""360

" ""ug/kg 360< 36011100-14-4 PCB-1268 10 ""360


30-150 % " " ""% DCBP 84 "2051-24-3

30-150 % " " ""% TCMX 73 "877-09-8




SW8260C 05-May-1

9 19:54

03-May-1

9 22:59




Page 111 of 23109-May-19 16:45

B-6 0.4-1.7'


30-Apr-19 14:15


01-May-19

Client Project #

18EC0070 SoilSC54611-13





SW8260C 05-May-1

9 19:54

03-May-1

9 22:59











ane

1 ""5.2











" ""ug/kg 26< 26591-78-6 2-Hexanone 1 ""26




" ""ug/kg 260< 26067-64-1 Acetone 1 ""260


" ""ug/kg 5.2< 5.271-43-2 Benzene 1 ""5.2




" ""ug/kg 5.2< 5.275-25-2 Bromoform 1 ""5.2






" ""ug/kg 5.2< 5.267-66-3 Chloroform 1 ""5.2








Page 112 of 23109-May-19 16:45

B-6 0.4-1.7'


30-Apr-19 14:15


01-May-19

Client Project #

18EC0070 SoilSC54611-13





SW8260C 05-May-1

9 19:54

03-May-1

9 22:59




" ""ug/kg 5.2< 5.2179601-23-1 m&p-Xylene 1 ""5.2



(MTBE)

1 ""10





" ""ug/kg 5.2< 5.295-47-6 o-Xylene 1 ""5.2



" ""ug/kg 5.2< 5.2100-42-5 Styrene 1 ""5.2




" ""ug/kg 5.2< 5.2108-88-3 Toluene 1 ""5.2





e

1 ""10









70-130 % " " ""% Toluene-d8 97 "2037-26-5




SW8270D 02-May-1

9 05:32

01-May-1

9


e

1 477192APH0618250









Page 113 of 23109-May-19 16:45

B-6 0.4-1.7'


30-Apr-19 14:15


01-May-19

Client Project #

18EC0070 SoilSC54611-13





SW8270D 02-May-1

9 05:32

01-May-1

9













(m&p-cresol)

1 ""350





ether

1 ""350




ether

1 ""250






" ""ug/kg 350< 35062-53-3 Aniline 1 ""350

" ""ug/kg 250< 250120-12-7 Anthracene 1 ""250


" ""ug/kg 250< 25092-87-5 Benzidine 1 ""250








ne

1 ""250



r

1 ""250


" ""ug/kg 350< 35086-74-8 Carbazole 1 ""350

" ""ug/kg 250390218-01-9 Chrysene 1 ""250



Page 114 of 23109-May-19 16:45

B-6 0.4-1.7'


30-Apr-19 14:15


01-May-19

Client Project #

18EC0070 SoilSC54611-13





SW8270D 02-May-1

9 05:32

01-May-1

9







" ""ug/kg 250< 25086-73-7 Fluorene 1 ""250




e

1 ""250



" ""ug/kg 250< 25078-59-1 Isophorone 1 ""250









" ""ug/kg 250< 250108-95-2 Phenol 1 ""250

" ""ug/kg 250720129-00-0 Pyrene 1 ""250

" ""ug/kg 350< 350110-86-1 Pyridine 1 ""350


30-130 % " " ""% 2,4,6-Tribromophenol 63 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 61 "321-60-8

30-130 % " " ""% 2-Fluorophenol 64 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 63 "4165-60-0

30-130 % " " ""% Phenol-d5 69 "4165-62-2

30-130 % " " ""% Terphenyl-d14 67 "98904-43-9




9 22:20

01-May-1

9 22:20





9 16:40

03-May-1

9 16:40




SW846-ReactCy

n

03-May-1

9 14:20

03-May-1

9



Page 115 of 23109-May-19 16:45

B-6 5.6-7.6'


30-Apr-19 14:30


01-May-19

Client Project #

18EC0070 SoilSC54611-14



SW846 1030 02-May-1

9 10:25

01-May-1

9 16:10


SW846 9045D 02-May-1

9 09:12

02-May-1

9 08:34







9 16:43

01-May-1

9


(C9-C36)

1 477191APH0618110


50-150 % " " ""% n-Pentacosane 103 "629-99-2




SW6010D 03-May-1

9 14:20

02-May-1

9

mg/kg 1.64.67440-38-2 Arsenic 1 477321APH06181.6

" ""mg/kg 0.7831.37440-39-3 Barium 1 ""0.78

" ""mg/kg 0.78< 0.787440-43-9 Cadmium 1 ""0.78

" ""mg/kg 0.7830.37440-47-3 Chromium 1 ""0.78

" ""mg/kg 0.787.577439-92-1 Lead 1 ""0.78

" ""mg/kg 3.1< 3.17782-49-2 Selenium 1 ""3.1

" ""mg/kg 0.78< 0.787440-22-4 Silver 1 ""0.78




SW6010D

(SPLP)

03-May-1

9 03:46


" ""mg/l 0.0100.0477440-39-3 SPLP Barium 1 ""0.010

" ""mg/l 0.005< 0.0057440-43-9 SPLP Cadmium 1 ""0.005


" ""mg/l 0.010< 0.0107439-92-1 SPLP Lead 1 ""0.010


" ""mg/l 0.010< 0.0107440-22-4 SPLP Silver 1 ""0.010



SW-7.3 03-May-1

9 16:40

03-May-1

9 16:40




SW7470A

(SPLP)

03-May-1

9 08:40

02-May-1

9




SW7471B 02-May-1

9 13:32

"mg/kg 0.13< 0.137439-97-6 Mercury 1 477261APH06180.13




SW8081B 04-May-1

9 01:12

"ug/kg 15< 1572-54-8 4,4' -DDD 2 477266APH061815


Page 116 of 23109-May-19 16:45

B-6 5.6-7.6'


30-Apr-19 14:30


01-May-19

Client Project #

18EC0070 SoilSC54611-14





SW8081B 04-May-1

9 01:12

02-May-1

9

ug/kg 15< 1572-55-9 4,4' -DDE 2 477266APH061815

" ""ug/kg 15< 1550-29-3 4,4' -DDT 2 ""15

" ""ug/kg 15< 15319-84-6 a-BHC 2 ""15

" ""ug/kg 15< 1515972-60-8 Alachlor 2 ""15

" ""ug/kg 7.6< 7.6309-00-2 Aldrin 2 ""7.6

" ""ug/kg 15< 15319-85-7 b-BHC 2 ""15

" ""ug/kg 76< 7657-74-9 Chlordane 2 ""76

" ""ug/kg 15< 15319-86-8 d-BHC 2 ""15

" ""ug/kg 7.6< 7.660-57-1 Dieldrin 2 ""7.6

" ""ug/kg 15< 15959-98-8 Endosulfan I 2 ""15

" ""ug/kg 15< 1533213-65-9 Endosulfan II 2 ""15

" ""ug/kg 15< 151031-07-8 Endosulfan sulfate 2 ""15

" ""ug/kg 15< 1572-20-8 Endrin 2 ""15

" ""ug/kg 15< 157421-93-4 Endrin aldehyde 2 ""15

" ""ug/kg 15< 1553494-70-5 Endrin ketone 2 ""15

" ""ug/kg 3.0< 3.058-89-9 g-BHC 2 ""3.0

" ""ug/kg 15< 1576-44-8 Heptachlor 2 ""15

" ""ug/kg 15< 151024-57-3 Heptachlor epoxide 2 ""15


" ""ug/kg 300< 3008001-35-2 Toxaphene 2 ""300


30-150 % " " ""% DCBP 39 "2051-24-3

30-150 % " " ""% TCMX 39 "877-09-8



SW8082A 03-May-1

9 19:04

"ug/kg 760< 76012674-11-2 PCB-1016 10 477265APH0618760

" ""ug/kg 760< 76011104-28-2 PCB-1221 10 ""760

" ""ug/kg 760< 76011141-16-5 PCB-1232 10 ""760

" ""ug/kg 760< 76053469-21-9 PCB-1242 10 ""760

" ""ug/kg 760< 76012672-29-6 PCB-1248 10 ""760

" ""ug/kg 760< 76011097-69-1 PCB-1254 10 ""760

" ""ug/kg 760< 76011096-82-5 PCB-1260 10 ""760

" ""ug/kg 760< 76037324-23-5 PCB-1262 10 ""760

" ""ug/kg 760< 76011100-14-4 PCB-1268 10 ""760


30-150 % " " ""% DCBP 58 "2051-24-3

30-150 % " " ""% TCMX 52 "877-09-8




SW8260C 04-May-1

9 04:51

01-May-1

9 22:12


" ""ug/kg 12< 1271-55-6 1,1,1-Trichloroethane 1 ""12


Page 117 of 23109-May-19 16:45

B-6 5.6-7.6'


30-Apr-19 14:30


01-May-19

Client Project #

18EC0070 SoilSC54611-14





SW8260C 04-May-1

9 04:51

01-May-1

9 22:12

ug/kg 12< 1279-00-5 1,1,2-Trichloroethane 1 477686APH061812

" ""ug/kg 12< 1275-34-3 1,1-Dichloroethane 1 ""12

" ""ug/kg 12< 1275-35-4 1,1-Dichloroethene 1 ""12

" ""ug/kg 12< 12563-58-6 1,1-Dichloropropene 1 ""12

" ""ug/kg 12< 12106-93-4 1,2-Dibromoethane 1 ""12


" ""ug/kg 12< 1278-87-5 1,2-Dichloropropane 1 ""12



" ""ug/kg 61< 61591-78-6 2-Hexanone 1 ""61


" ""ug/kg 610< 61067-64-1 Acetone 1 ""610

" ""ug/kg 12< 12107-13-1 Acrylonitrile 1 ""12

" ""ug/kg 12< 1271-43-2 Benzene 1 ""12

" ""ug/kg 12< 1274-97-5 Bromochloromethane 1 ""12

" ""ug/kg 12< 1275-27-4 Bromodichloromethane 1 ""12

" ""ug/kg 12< 1275-25-2 Bromoform 1 ""12

" ""ug/kg 12< 1274-83-9 Bromomethane 1 ""12

" ""ug/kg 12< 1275-15-0 Carbon Disulfide 1 ""12

" ""ug/kg 12< 1256-23-5 Carbon tetrachloride 1 ""12

" ""ug/kg 12< 12108-90-7 Chlorobenzene 1 ""12

" ""ug/kg 12< 1275-00-3 Chloroethane 1 ""12

" ""ug/kg 12< 1267-66-3 Chloroform 1 ""12

" ""ug/kg 12< 1274-87-3 Chloromethane 1 ""12

" ""ug/kg 12< 12156-59-2 cis-1,2-Dichloroethene 1 ""12

" ""ug/kg 12< 1210061-01-5 cis-1,3-Dichloropropene 1 ""12


" ""ug/kg 12< 1274-95-3 Dibromomethane 1 ""12

" ""ug/kg 12< 1275-71-8 Dichlorodifluoromethane 1 ""12

" ""ug/kg 12< 12100-41-4 Ethylbenzene 1 ""12

" ""ug/kg 12< 12179601-23-1 m&p-Xylene 1 ""12



(MTBE)

1 ""25


" ""ug/kg 12< 1295-47-6 o-Xylene 1 ""12

" ""ug/kg 12< 12100-42-5 Styrene 1 ""12

" ""ug/kg 12< 12127-18-4 Tetrachloroethene 1 ""12


" ""ug/kg 12< 12108-88-3 Toluene 1 ""12

" ""ug/kg 12< 121330-20-7 Total Xylenes 1 ""12

" ""ug/kg 12< 12156-60-5 trans-1,2-Dichloroethene 1 ""12

" ""ug/kg 12< 1210061-02-6 trans-1,3-Dichloropropene 1 ""12

" ""ug/kg 12< 1279-01-6 Trichloroethene 1 ""12


Page 118 of 23109-May-19 16:45

B-6 5.6-7.6'


30-Apr-19 14:30


01-May-19

Client Project #

18EC0070 SoilSC54611-14





SW8260C 04-May-1

9 04:51

01-May-1

9 22:12

ug/kg 12< 1275-69-4 Trichlorofluoromethane 1 477686APH061812


" ""ug/kg 12< 1275-01-4 Vinyl chloride 1 ""12





70-130 % " " ""% Toluene-d8 95 "2037-26-5



SW8260C 05-May-1

9 19:09

04-May-1

9 13:34







ane

50 ""980


















e

50 ""2000





70-130 % " " ""% Toluene-d8 98 "2037-26-5





Page 119 of 23109-May-19 16:45

B-6 5.6-7.6'


30-Apr-19 14:30


01-May-19

Client Project #

18EC0070 SoilSC54611-14






SW8270D 02-May-1

9 06:22

01-May-1

9


e

5 477192APH06182600




















(m&p-cresol)

5 ""3800





ether

5 ""3800




ether

5 ""2600






" ""ug/kg 3800< 380062-53-3 Aniline 5 ""3800

" ""ug/kg 2600< 2600120-12-7 Anthracene 5 ""2600


" ""ug/kg 2600< 260092-87-5 Benzidine 5 ""2600







Page 120 of 23109-May-19 16:45

B-6 5.6-7.6'


30-Apr-19 14:30


01-May-19

Client Project #

18EC0070 SoilSC54611-14





SW8270D 02-May-1

9 06:22

01-May-1

9



ne

5 ""2600



r

5 ""2600


" ""ug/kg 3800< 380086-74-8 Carbazole 5 ""3800

" ""ug/kg 2600< 2600218-01-9 Chrysene 5 ""2600








" ""ug/kg 2600< 260086-73-7 Fluorene 5 ""2600




e

5 ""2600



" ""ug/kg 2600< 260078-59-1 Isophorone 5 ""2600









" ""ug/kg 2600< 2600108-95-2 Phenol 5 ""2600

" ""ug/kg 2600< 2600129-00-0 Pyrene 5 ""2600

" ""ug/kg 3800< 3800110-86-1 Pyridine 5 ""3800


30-130 % " " ""% 2,4,6-Tribromophenol 64 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 59 "321-60-8

30-130 % " " ""% 2-Fluorophenol 64 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 59 "4165-60-0

30-130 % " " ""% Phenol-d5 71 "4165-62-2

30-130 % " " ""% Terphenyl-d14 79 "98904-43-9




Page 121 of 23109-May-19 16:45

B-6 5.6-7.6'


30-Apr-19 14:30


01-May-19

Client Project #

18EC0070 SoilSC54611-14






9 22:20

01-May-1

9 22:20





9 16:40

03-May-1

9 16:40




SW846-ReactCy

n

03-May-1

9 14:21

03-May-1

9



Page 122 of 23109-May-19 16:45

SED-1


30-Apr-19 16:00


01-May-19

Client Project #

18EC0070 SedimentSC54611-15



SW846 1030 02-May-1

9 10:25

01-May-1

9 16:10


SW846 9045D 02-May-1

9 09:15

02-May-1

9 08:34







9 17:19

01-May-1

9

mg/kg 130370Ext. Petroleum H.C.

(C9-C36)

1 477191APH0618130


50-150 % " " ""% n-Pentacosane 103 "629-99-2




SW6010D 03-May-1

9 14:23

02-May-1

9

mg/kg 1.752.77440-38-2 Arsenic 1 477321APH06181.7

" ""mg/kg 0.8395.17440-39-3 Barium 1 ""0.83

" ""mg/kg 0.832.877440-43-9 Cadmium 1 ""0.83

" ""mg/kg 0.8350.37440-47-3 Chromium 1 ""0.83

" ""mg/kg 0.8348.27439-92-1 Lead 1 ""0.83

" ""mg/kg 3.3< 3.37782-49-2 Selenium 1 ""3.3

" ""mg/kg 0.83< 0.837440-22-4 Silver 1 ""0.83




SW6010D

(SPLP)

03-May-1

9 03:49


" ""mg/l 0.0100.0817440-39-3 SPLP Barium 1 ""0.010

" ""mg/l 0.005< 0.0057440-43-9 SPLP Cadmium 1 ""0.005


" ""mg/l 0.010< 0.0107439-92-1 SPLP Lead 1 ""0.010


" ""mg/l 0.010< 0.0107440-22-4 SPLP Silver 1 ""0.010



SW-7.3 03-May-1

9 16:39

03-May-1

9 16:39




SW7470A

(SPLP)

03-May-1

9 08:42

02-May-1

9




SW7471B 02-May-1

9 13:34

"mg/kg 0.17< 0.177439-97-6 Mercury 1 477261APH06180.17




SW8081B 03-May-1

9 23:40

"ug/kg 17< 1772-54-8 4,4' -DDD 2 477266APH061817


Page 123 of 23109-May-19 16:45

SED-1


30-Apr-19 16:00


01-May-19

Client Project #






SW8081B 03-May-1

9 23:40

02-May-1

9

ug/kg 17< 1772-55-9 4,4' -DDE 2 477266APH061817

" ""ug/kg 17< 1750-29-3 4,4' -DDT 2 ""17

" ""ug/kg 17< 17319-84-6 a-BHC 2 ""17

" ""ug/kg 17< 1715972-60-8 Alachlor 2 ""17

" ""ug/kg 8.5< 8.5309-00-2 Aldrin 2 ""8.5

" ""ug/kg 17< 17319-85-7 b-BHC 2 ""17

" ""ug/kg 85< 8557-74-9 Chlordane 2 ""85

" ""ug/kg 17< 17319-86-8 d-BHC 2 ""17

" ""ug/kg 8.5< 8.560-57-1 Dieldrin 2 ""8.5

" ""ug/kg 17< 17959-98-8 Endosulfan I 2 ""17

" ""ug/kg 17< 1733213-65-9 Endosulfan II 2 ""17

" ""ug/kg 17< 171031-07-8 Endosulfan sulfate 2 ""17

" ""ug/kg 17< 1772-20-8 Endrin 2 ""17

" ""ug/kg 17< 177421-93-4 Endrin aldehyde 2 ""17

" ""ug/kg 17< 1753494-70-5 Endrin ketone 2 ""17

" ""ug/kg 3.4< 3.458-89-9 g-BHC 2 ""3.4

" ""ug/kg 17< 1776-44-8 Heptachlor 2 ""17

" ""ug/kg 17< 171024-57-3 Heptachlor epoxide 2 ""17


" ""ug/kg 340< 3408001-35-2 Toxaphene 2 ""340


30-150 % " " ""% DCBP 50 "2051-24-3

30-150 % " " ""% TCMX 55 "877-09-8



SW8082A 03-May-1

9 20:04

"ug/kg 850< 85012674-11-2 PCB-1016 10 477265APH0618850

" ""ug/kg 850< 85011104-28-2 PCB-1221 10 ""850

" ""ug/kg 850< 85011141-16-5 PCB-1232 10 ""850

" ""ug/kg 850< 85053469-21-9 PCB-1242 10 ""850

" ""ug/kg 850< 85012672-29-6 PCB-1248 10 ""850

" ""ug/kg 850< 85011097-69-1 PCB-1254 10 ""850

" ""ug/kg 850< 85011096-82-5 PCB-1260 10 ""850

" ""ug/kg 850< 85037324-23-5 PCB-1262 10 ""850

" ""ug/kg 850< 85011100-14-4 PCB-1268 10 ""850


30-150 % " " ""% DCBP 63 "2051-24-3

30-150 % " " ""% TCMX 67 "877-09-8




SW8260C 04-May-1

9 19:56

04-May-1

9 13:34




Page 124 of 23109-May-19 16:45

SED-1


30-Apr-19 16:00


01-May-19

Client Project #






SW8260C 04-May-1

9 19:56

04-May-1

9 13:34





" ""ug/kg 12< 12563-58-6 1,1-Dichloropropene 1 ""12






ane

1 ""12











" ""ug/kg 58< 58591-78-6 2-Hexanone 1 ""58




" ""ug/kg 580< 58067-64-1 Acetone 1 ""580


" ""ug/kg 12< 1271-43-2 Benzene 1 ""12




" ""ug/kg 12< 1275-25-2 Bromoform 1 ""12






" ""ug/kg 12< 1267-66-3 Chloroform 1 ""12








Page 125 of 23109-May-19 16:45

SED-1


30-Apr-19 16:00


01-May-19

Client Project #






SW8260C 04-May-1

9 19:56

04-May-1

9 13:34

ug/kg 12< 12100-41-4 Ethylbenzene 1 477679APH061812



" ""ug/kg 12< 12179601-23-1 m&p-Xylene 1 ""12



(MTBE)

1 ""23





" ""ug/kg 12< 1295-47-6 o-Xylene 1 ""12



" ""ug/kg 12< 12100-42-5 Styrene 1 ""12




" ""ug/kg 12< 12108-88-3 Toluene 1 ""12





e

1 ""23


" ""ug/kg 12< 1275-69-4 Trichlorofluoromethane 1 ""12







70-130 % " " ""% Toluene-d8 94 "2037-26-5




SW8270D 02-May-1

9 05:57

01-May-1

9


e

1 477192APH0618590









Page 126 of 23109-May-19 16:45

SED-1


30-Apr-19 16:00


01-May-19

Client Project #






SW8270D 02-May-1

9 05:57

01-May-1

9













(m&p-cresol)

1 ""850





ether

1 ""850




ether

1 ""590



" ""ug/kg 5901,10083-32-9 Acenaphthene 1 ""590



" ""ug/kg 850< 85062-53-3 Aniline 1 ""850

" ""ug/kg 5902,800120-12-7 Anthracene 1 ""590

" ""ug/kg 5909,30056-55-3 Benz(a)anthracene 1 ""590

" ""ug/kg 590< 59092-87-5 Benzidine 1 ""590



" ""ug/kg 5904,900191-24-2 Benzo(ghi)perylene 1 ""590





ne

1 ""590



r

1 ""590


" ""ug/kg 8502,60086-74-8 Carbazole 1 ""850

" ""ug/kg 59011,000218-01-9 Chrysene 1 ""590

" ""ug/kg 5901,70053-70-3 Dibenz(a,h)anthracene 1 ""590


Page 127 of 23109-May-19 16:45

SED-1


30-Apr-19 16:00


01-May-19

Client Project #






SW8270D 02-May-1

9 05:57

01-May-1

9

ug/kg 590670132-64-9 Dibenzofuran 1 477192APH0618590





" ""ug/kg 5901,90086-73-7 Fluorene 1 ""590




e

1 ""590


" ""ug/kg 5905,800193-39-5 Indeno(1,2,3-cd)pyrene 1 ""590

" ""ug/kg 590< 59078-59-1 Isophorone 1 ""590








" ""ug/kg 590< 590108-95-2 Phenol 1 ""590

" ""ug/kg 850< 850110-86-1 Pyridine 1 ""850


30-130 % " " ""% 2,4,6-Tribromophenol 59 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 46 "321-60-8

30-130 % " " ""% 2-Fluorophenol 58 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 33 "4165-60-0

30-130 % " " ""% Phenol-d5 67 "4165-62-2

30-130 % " " ""% Terphenyl-d14 80 "98904-43-9



SW8270D 02-May-1

9 18:16

01-May-1

9

ug/kg 300024,000206-44-0 Fluoranthene 5 477192APH06183000

" ""ug/kg 300017,00085-01-8 Phenanthrene 5 ""3000

" ""ug/kg 300017,000129-00-0 Pyrene 5 ""3000


30-130 % " " ""% 2,4,6-Tribromophenol 53 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 45 "321-60-8

30-130 % " " ""% 2-Fluorophenol 48 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 27 "4165-60-0

30-130 % " " ""% Phenol-d5 49 "4165-62-2

30-130 % " " ""% Terphenyl-d14 62 "98904-43-9




Page 128 of 23109-May-19 16:45

SED-1


30-Apr-19 16:00


01-May-19

Client Project #







9 22:20

01-May-1

9 22:20





9 16:39

03-May-1

9 16:39




SW846-ReactCy

n

03-May-1

9 14:22

03-May-1

9



Page 129 of 23109-May-19 16:45

SED-2


30-Apr-19 15:50


01-May-19

Client Project #




SW846 1030 02-May-1

9 10:25

01-May-1

9 16:10


SW846 9045D 02-May-1

9 09:18

02-May-1

9 08:34







9 18:14

01-May-1

9

mg/kg 72180Ext. Petroleum H.C.

(C9-C36)

1 477191APH061872


50-150 % " " ""% n-Pentacosane 95 "629-99-2




SW6010D 03-May-1

9 14:26

02-May-1

9

mg/kg 0.946.847440-38-2 Arsenic 1 477321APH06180.94

" ""mg/kg 0.4712.17440-39-3 Barium 1 ""0.47

" ""mg/kg 0.471.217440-43-9 Cadmium 1 ""0.47

" ""mg/kg 0.4721.77440-47-3 Chromium 1 ""0.47

" ""mg/kg 0.4729.07439-92-1 Lead 1 ""0.47

" ""mg/kg 1.9< 1.97782-49-2 Selenium 1 ""1.9

" ""mg/kg 0.47< 0.477440-22-4 Silver 1 ""0.47




SW6010D

(SPLP)

03-May-1

9 03:52


" ""mg/l 0.0100.0147440-39-3 SPLP Barium 1 ""0.010

" ""mg/l 0.005< 0.0057440-43-9 SPLP Cadmium 1 ""0.005


" ""mg/l 0.0100.0127439-92-1 SPLP Lead 1 ""0.010


" ""mg/l 0.010< 0.0107440-22-4 SPLP Silver 1 ""0.010



SW-7.3 03-May-1

9 16:39

03-May-1

9 16:39




SW7470A

(SPLP)

03-May-1

9 09:26

02-May-1

9




SW7471B 02-May-1

9 13:36

"mg/kg 0.090.107439-97-6 Mercury 1 477261APH06180.09




SW8081B 06-May-1

9 18:52

"ug/kg 9.4< 9.472-54-8 4,4' -DDD 2 477266APH06189.4


Page 130 of 23109-May-19 16:45

SED-2


30-Apr-19 15:50


01-May-19

Client Project #






SW8081B 06-May-1

9 18:52

02-May-1

9

ug/kg 9.4< 9.472-55-9 4,4' -DDE 2 477266APH06189.4

" ""ug/kg 9.4< 9.450-29-3 4,4' -DDT 2 ""9.4

" ""ug/kg 9.4< 9.4319-84-6 a-BHC 2 ""9.4

" ""ug/kg 9.4< 9.415972-60-8 Alachlor 2 ""9.4

" ""ug/kg 4.7< 4.7309-00-2 Aldrin 2 ""4.7

" ""ug/kg 9.4< 9.4319-85-7 b-BHC 2 ""9.4

" ""ug/kg 47< 4757-74-9 Chlordane 2 ""47

" ""ug/kg 9.4< 9.4319-86-8 d-BHC 2 ""9.4

" ""ug/kg 4.7< 4.760-57-1 Dieldrin 2 ""4.7




" ""ug/kg 9.4< 9.472-20-8 Endrin 2 ""9.4



" ""ug/kg 1.9< 1.958-89-9 g-BHC 2 ""1.9

" ""ug/kg 9.4< 9.476-44-8 Heptachlor 2 ""9.4



" ""ug/kg 190< 1908001-35-2 Toxaphene 2 ""190


30-150 % " " ""% DCBP 62 "2051-24-3

30-150 % " " ""% TCMX 58 "877-09-8



SW8082A 03-May-1

9 19:42

"ug/kg 470< 47012674-11-2 PCB-1016 10 477265APH0618470

" ""ug/kg 470< 47011104-28-2 PCB-1221 10 ""470

" ""ug/kg 470< 47011141-16-5 PCB-1232 10 ""470

" ""ug/kg 470< 47053469-21-9 PCB-1242 10 ""470

" ""ug/kg 470< 47012672-29-6 PCB-1248 10 ""470

" ""ug/kg 470< 47011097-69-1 PCB-1254 10 ""470

" ""ug/kg 470< 47011096-82-5 PCB-1260 10 ""470

" ""ug/kg 470< 47037324-23-5 PCB-1262 10 ""470

" ""ug/kg 470< 47011100-14-4 PCB-1268 10 ""470


30-150 % " " ""% DCBP 67 "2051-24-3

30-150 % " " ""% TCMX 68 "877-09-8




SW8260C 04-May-1

9 20:17

04-May-1

9 13:35




Page 131 of 23109-May-19 16:45

SED-2


30-Apr-19 15:50


01-May-19

Client Project #






SW8260C 04-May-1

9 20:17

04-May-1

9 13:35

ug/kg 7.0< 7.079-00-5 1,1,2-Trichloroethane 1 477679APH06187.0









" ""ug/kg 35< 35591-78-6 2-Hexanone 1 ""35


" ""ug/kg 350< 35067-64-1 Acetone 1 ""350


" ""ug/kg 7.0< 7.071-43-2 Benzene 1 ""7.0



" ""ug/kg 7.0< 7.075-25-2 Bromoform 1 ""7.0






" ""ug/kg 7.0< 7.067-66-3 Chloroform 1 ""7.0








" ""ug/kg 7.0< 7.0179601-23-1 m&p-Xylene 1 ""7.0



(MTBE)

1 ""14


" ""ug/kg 7.0< 7.095-47-6 o-Xylene 1 ""7.0

" ""ug/kg 7.0< 7.0100-42-5 Styrene 1 ""7.0



" ""ug/kg 7.0< 7.0108-88-3 Toluene 1 ""7.0






Page 132 of 23109-May-19 16:45

SED-2


30-Apr-19 15:50


01-May-19

Client Project #






SW8260C 04-May-1

9 20:17

04-May-1

9 13:35

ug/kg 7.0< 7.075-69-4 Trichlorofluoromethane 1 477679APH06187.0







70-130 % " " ""% Toluene-d8 90 "2037-26-5



SW8260C 04-May-1

9 20:17

01-May-1

9 22:12







ane

50 ""470


















e

50 ""930





70-130 % " " ""% Toluene-d8 99 "2037-26-5





Page 133 of 23109-May-19 16:45

SED-2


30-Apr-19 15:50


01-May-19

Client Project #







SW8270D 03-May-1

9 03:55

01-May-1

9


e

1 477192APH0618330




















(m&p-cresol)

1 ""470





ether

1 ""470




ether

1 ""330






" ""ug/kg 470< 47062-53-3 Aniline 1 ""470

" ""ug/kg 330< 330120-12-7 Anthracene 1 ""330


" ""ug/kg 330< 33092-87-5 Benzidine 1 ""330







Page 134 of 23109-May-19 16:45

SED-2


30-Apr-19 15:50


01-May-19

Client Project #






SW8270D 03-May-1

9 03:55

01-May-1

9



ne

1 ""330



r

1 ""330

" ""ug/kg 330590117-81-7 Bis(2-ethylhexyl)phthalate 1 ""330

" ""ug/kg 470< 47086-74-8 Carbazole 1 ""470

" ""ug/kg 3301,400218-01-9 Chrysene 1 ""330







" ""ug/kg 3303,200206-44-0 Fluoranthene 1 ""330

" ""ug/kg 330< 33086-73-7 Fluorene 1 ""330




e

1 ""330



" ""ug/kg 330< 33078-59-1 Isophorone 1 ""330









" ""ug/kg 330< 330108-95-2 Phenol 1 ""330

" ""ug/kg 3302,500129-00-0 Pyrene 1 ""330

" ""ug/kg 470< 470110-86-1 Pyridine 1 ""470


30-130 % " " ""% 2,4,6-Tribromophenol 93 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 58 "321-60-8

30-130 % " " ""% 2-Fluorophenol 53 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 53 "4165-60-0

30-130 % " " ""% Phenol-d5 63 "4165-62-2

30-130 % " " ""% Terphenyl-d14 77 "98904-43-9




Page 135 of 23109-May-19 16:45

SED-2


30-Apr-19 15:50


01-May-19

Client Project #







9 22:20

01-May-1

9 22:20





9 16:39

03-May-1

9 16:39




SW846-ReactCy

n

03-May-1

9 14:23

03-May-1

9



Page 136 of 23109-May-19 16:45

DUP


30-Apr-19 00:00


01-May-19

Client Project #

18EC0070 SoilSC54611-17



SW846 1030 02-May-1

9 10:25

01-May-1

9 16:10


SW846 9045D 02-May-1

9 09:19

02-May-1

9 08:34







9 16:15

01-May-1

9


(C9-C36)

1 477191APH061857


50-150 % " " ""% n-Pentacosane 91 "629-99-2




SW6010D 03-May-1

9 14:30

02-May-1

9

mg/kg 0.683.707440-38-2 Arsenic 1 477321APH06180.68

" ""mg/kg 0.3412.47440-39-3 Barium 1 ""0.34

" ""mg/kg 0.34< 0.347440-43-9 Cadmium 1 ""0.34

" ""mg/kg 0.3412.77440-47-3 Chromium 1 ""0.34

" ""mg/kg 0.3414.67439-92-1 Lead 1 ""0.34

" ""mg/kg 1.4< 1.47782-49-2 Selenium 1 ""1.4

" ""mg/kg 0.34< 0.347440-22-4 Silver 1 ""0.34




SW6010D

(SPLP)

03-May-1

9 03:54


" ""mg/l 0.0100.0337440-39-3 SPLP Barium 1 ""0.010

" ""mg/l 0.005< 0.0057440-43-9 SPLP Cadmium 1 ""0.005


" ""mg/l 0.010< 0.0107439-92-1 SPLP Lead 1 ""0.010


" ""mg/l 0.010< 0.0107440-22-4 SPLP Silver 1 ""0.010



SW-7.3 03-May-1

9 16:40

03-May-1

9 16:40




SW7470A

(SPLP)

03-May-1

9 09:28

02-May-1

9




SW7471B 02-May-1

9 13:39

"mg/kg 0.07< 0.077439-97-6 Mercury 1 477261APH06180.07




SW8081B 03-May-1

9 23:03

"ug/kg 7.7< 7.772-54-8 4,4' -DDD 2 477266APH06187.7


Page 137 of 23109-May-19 16:45

DUP


30-Apr-19 00:00


01-May-19

Client Project #

18EC0070 SoilSC54611-17





SW8081B 03-May-1

9 23:03

02-May-1

9

ug/kg 7.7< 7.772-55-9 4,4' -DDE 2 477266APH06187.7

" ""ug/kg 7.7< 7.750-29-3 4,4' -DDT 2 ""7.7

" ""ug/kg 7.7< 7.7319-84-6 a-BHC 2 ""7.7

" ""ug/kg 7.7< 7.715972-60-8 Alachlor 2 ""7.7

" ""ug/kg 3.9< 3.9309-00-2 Aldrin 2 ""3.9

" ""ug/kg 7.7< 7.7319-85-7 b-BHC 2 ""7.7

" ""ug/kg 39< 3957-74-9 Chlordane 2 ""39

" ""ug/kg 7.7< 7.7319-86-8 d-BHC 2 ""7.7

" ""ug/kg 3.9< 3.960-57-1 Dieldrin 2 ""3.9




" ""ug/kg 7.7< 7.772-20-8 Endrin 2 ""7.7



" ""ug/kg 1.5< 1.558-89-9 g-BHC 2 ""1.5

" ""ug/kg 7.7< 7.776-44-8 Heptachlor 2 ""7.7



" ""ug/kg 150< 1508001-35-2 Toxaphene 2 ""150


30-150 % " " ""% DCBP 58 "2051-24-3

30-150 % " " ""% TCMX 49 "877-09-8



SW8082A 03-May-1

9 23:23

"ug/kg 390< 39012674-11-2 PCB-1016 10 477265APH0618390

" ""ug/kg 390< 39011104-28-2 PCB-1221 10 ""390

" ""ug/kg 390< 39011141-16-5 PCB-1232 10 ""390

" ""ug/kg 390< 39053469-21-9 PCB-1242 10 ""390

" ""ug/kg 390< 39012672-29-6 PCB-1248 10 ""390

" ""ug/kg 390< 39011097-69-1 PCB-1254 10 ""390

" ""ug/kg 390< 39011096-82-5 PCB-1260 10 ""390

" ""ug/kg 390< 39037324-23-5 PCB-1262 10 ""390

" ""ug/kg 390< 39011100-14-4 PCB-1268 10 ""390


30-150 % " " ""% DCBP 81 "2051-24-3

30-150 % " " ""% TCMX 80 "877-09-8




SW8260C 04-May-1

9 07:03

01-May-1

9 22:12

ug/kg 34039095-63-6 1,2,4-Trimethylbenzene 50 477686APH0618340



Page 138 of 23109-May-19 16:45

DUP


30-Apr-19 00:00


01-May-19

Client Project #

18EC0070 SoilSC54611-17





SW8260C 04-May-1

9 07:03

01-May-1

9 22:12

ug/kg 34062071-43-2 Benzene 50 477686APH0618340

" ""ug/kg 200210100-41-4 Ethylbenzene 50 ""200

" ""ug/kg 13014098-82-8 Isopropylbenzene 50 ""130

" ""ug/kg 340340179601-23-1 m&p-Xylene 50 ""340

" ""ug/kg 3401,50091-20-3 Naphthalene 50 ""340

" ""ug/kg 4.8340.01330-20-7 Total Xylenes 1 ""4.8





70-130 % " " ""% Toluene-d8 98 "2037-26-5



SW8260C 05-May-1

9 20:38

04-May-1

9 13:36



" ""ug/kg 2.9< 2.979-34-5 1,1,2,2-Tetrachloroethane 1 ""2.9









ane

1 ""4.8










" ""ug/kg 24< 24591-78-6 2-Hexanone 1 ""24




" ""ug/kg 240< 24067-64-1 Acetone 1 ""240






Page 139 of 23109-May-19 16:45

DUP


30-Apr-19 00:00


01-May-19

Client Project #

18EC0070 SoilSC54611-17





SW8260C 05-May-1

9 20:38

04-May-1

9 13:36

ug/kg 4.8< 4.875-25-2 Bromoform 1 477684APH06184.8






" ""ug/kg 4.8< 4.867-66-3 Chloroform 1 ""4.8










(MTBE)

1 ""9.5




" ""ug/kg 4.8< 4.895-47-6 o-Xylene 1 ""4.8



" ""ug/kg 4.8< 4.8100-42-5 Styrene 1 ""4.8




" ""ug/kg 4.8< 4.8108-88-3 Toluene 1 ""4.8




e

1 ""9.5









70-130 % " " ""% Toluene-d8 95 "2037-26-5





Page 140 of 23109-May-19 16:45

DUP


30-Apr-19 00:00


01-May-19

Client Project #

18EC0070 SoilSC54611-17






SW8270D 03-May-1

9 04:22

01-May-1

9


e

1 477192APH0618260




















(m&p-cresol)

1 ""380





ether

1 ""380




ether

1 ""260






" ""ug/kg 380< 38062-53-3 Aniline 1 ""380

" ""ug/kg 260< 260120-12-7 Anthracene 1 ""260


" ""ug/kg 260< 26092-87-5 Benzidine 1 ""260







Page 141 of 23109-May-19 16:45

DUP


30-Apr-19 00:00


01-May-19

Client Project #

18EC0070 SoilSC54611-17





SW8270D 03-May-1

9 04:22

01-May-1

9



ne

1 ""260



r

1 ""260


" ""ug/kg 380< 38086-74-8 Carbazole 1 ""380

" ""ug/kg 260< 260218-01-9 Chrysene 1 ""260








" ""ug/kg 260< 26086-73-7 Fluorene 1 ""260




e

1 ""260



" ""ug/kg 260< 26078-59-1 Isophorone 1 ""260









" ""ug/kg 260< 260108-95-2 Phenol 1 ""260

" ""ug/kg 260< 260129-00-0 Pyrene 1 ""260

" ""ug/kg 380< 380110-86-1 Pyridine 1 ""380


30-130 % " " ""% 2,4,6-Tribromophenol 103 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 61 "321-60-8

30-130 % " " ""% 2-Fluorophenol 48 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 53 "4165-60-0

30-130 % " " ""% Phenol-d5 46 "4165-62-2

30-130 % " " ""% Terphenyl-d14 76 "98904-43-9




Page 142 of 23109-May-19 16:45

DUP


30-Apr-19 00:00


01-May-19

Client Project #

18EC0070 SoilSC54611-17






9 22:20

01-May-1

9 22:20





9 16:40

03-May-1

9 16:40




SW846-ReactCy

n

03-May-1

9 14:24

03-May-1

9



Page 143 of 23109-May-19 16:45

Trip Blank


30-Apr-19 00:00


01-May-19

Client Project #

18EC0070 Trip BlankSC54611-18






SW8260C 04-May-1

9 00:40

01-May-1

9 22:12



" ""ug/kg 3.0< 3.079-34-5 1,1,2,2-Tetrachloroethane 1 ""3.0










ane

1 ""5.0











" ""ug/kg 25< 25591-78-6 2-Hexanone 1 ""25




" ""ug/kg 250< 25067-64-1 Acetone 1 ""250


" ""ug/kg 5.0< 5.071-43-2 Benzene 1 ""5.0




" ""ug/kg 5.0< 5.075-25-2 Bromoform 1 ""5.0






" ""ug/kg 5.0< 5.067-66-3 Chloroform 1 ""5.0





Page 144 of 23109-May-19 16:45

Trip Blank


30-Apr-19 00:00


01-May-19

Client Project #






SW8260C 04-May-1

9 00:40

01-May-1

9 22:12

ug/kg 3.0< 3.0124-48-1 Dibromochloromethane 1 477686APH06183.0






" ""ug/kg 5.0< 5.0179601-23-1 m&p-Xylene 1 ""5.0



(MTBE)

1 ""10





" ""ug/kg 5.0< 5.095-47-6 o-Xylene 1 ""5.0



" ""ug/kg 5.0< 5.0100-42-5 Styrene 1 ""5.0




" ""ug/kg 5.0< 5.0108-88-3 Toluene 1 ""5.0





e

1 ""10









70-130 % " " ""% Toluene-d8 101 "2037-26-5



SW8260C 04-May-1

9 01:02

01-May-1

9 22:12



" ""ug/kg 250< 25079-34-5 1,1,2,2-Tetrachloroethane 50 ""250





Page 145 of 23109-May-19 16:45

Trip Blank


30-Apr-19 00:00


01-May-19

Client Project #






SW8260C 04-May-1

9 01:02

01-May-1

9 22:12

ug/kg 250< 250563-58-6 1,1-Dichloropropene 50 477686APH0618250






ane

50 ""250











" ""ug/kg 1300< 1300591-78-6 2-Hexanone 50 ""1300




" ""ug/kg 5000< 500067-64-1 Acetone 50 ""5000


" ""ug/kg 250< 25071-43-2 Benzene 50 ""250




" ""ug/kg 250< 25075-25-2 Bromoform 50 ""250






" ""ug/kg 250< 25067-66-3 Chloroform 50 ""250




" ""ug/kg 250< 250124-48-1 Dibromochloromethane 50 ""250



" ""ug/kg 250< 250100-41-4 Ethylbenzene 50 ""250



" ""ug/kg 250< 250179601-23-1 m&p-Xylene 50 ""250


Page 146 of 23109-May-19 16:45

Trip Blank


30-Apr-19 00:00


01-May-19

Client Project #






SW8260C 04-May-1

9 01:02

01-May-1

9 22:12

ug/kg 3000< 300078-93-3 Methyl Ethyl Ketone 50 477686APH06183000


(MTBE)

50 ""250





" ""ug/kg 250< 25095-47-6 o-Xylene 50 ""250



" ""ug/kg 250< 250100-42-5 Styrene 50 ""250




" ""ug/kg 250< 250108-88-3 Toluene 50 ""250





e

50 ""500


" ""ug/kg 250< 25075-69-4 Trichlorofluoromethane 50 ""250







70-130 % " " ""% Toluene-d8 99 "2037-26-5


Page 147 of 23109-May-19 16:45

TMW-1


30-Apr-19 16:20


01-May-19

Client Project #

18EC0070 Ground WaterSC54611-19




Prepared by method SW3510C/SW3520C



9 00:54

01-May-1

9

mg/l 0.066< 0.066Ext. Petroleum H.C.

(C9-C36)

1 477197APH06180.066


50-150 % " " ""% n-Pentacosane 78 "629-99-2


Prepared by method SW3005A/SW3010A


SW6010D 02-May-1

9 22:50

"mg/l 0.0050.0067440-50-8 Copper 1 477208APH06180.005

" ""mg/l 0.0020.0037439-92-1 Lead 1 ""0.002

" ""mg/l 0.0040.0087440-66-6 Zinc 1 ""0.004




SW6010D

dissolved

03-May-1

9 01:14

"mg/l 0.005< 0.0057440-50-8 Copper (Dissolved) 1 477214APH06180.005

" ""mg/l 0.0020.0027439-92-1 Lead (Dissolved) 1 ""0.002

" ""mg/l 0.0020.0037440-66-6 Zinc (Dissolved) 1 ""0.002




SW8081B 02-May-1

9 19:24

"ug/l 0.047< 0.04772-54-8 4,4' -DDD 1 477223APH06180.047

" ""ug/l 0.047< 0.04772-55-9 4,4' -DDE 1 ""0.047

" ""ug/l 0.047< 0.04750-29-3 4,4' -DDT 1 ""0.047

" ""ug/l 0.024< 0.024319-84-6 a-BHC 1 ""0.024

" ""ug/l 0.071< 0.07115972-60-8 Alachlor 1 ""0.071

" ""ug/l 0.005< 0.005309-00-2 Aldrin 1 ""0.005

" ""ug/l 0.005< 0.005319-85-7 b-BHC 1 ""0.005

" ""ug/l 0.28< 0.2857-74-9 Chlordane 1 ""0.28

" ""ug/l 0.024< 0.024319-86-8 d-BHC 1 ""0.024

" ""ug/l 0.0010.02460-57-1 Dieldrin 1 ""0.001

" ""ug/l 0.047< 0.047959-98-8 Endosulfan I 1 ""0.047

" ""ug/l 0.047< 0.04733213-65-9 Endosulfan II 1 ""0.047

" ""ug/l 0.047< 0.0471031-07-8 Endosulfan Sulfate 1 ""0.047

" ""ug/l 0.047< 0.04772-20-8 Endrin 1 ""0.047

" ""ug/l 0.047< 0.0477421-93-4 Endrin Aldehyde 1 ""0.047

" ""ug/l 0.047< 0.04753494-70-5 Endrin ketone 1 ""0.047

" ""ug/l 0.024< 0.02458-89-9 g-BHC (Lindane) 1 ""0.024

" ""ug/l 0.024< 0.02476-44-8 Heptachlor 1 ""0.024

" ""ug/l 0.024< 0.0241024-57-3 Heptachlor epoxide 1 ""0.024

" ""ug/l 0.094< 0.09472-43-5 Methoxychlor 1 ""0.094

" ""ug/l 0.94< 0.948001-35-2 Toxaphene 1 ""0.94


30-150 % " " ""%DCBP (Surrogate Rec) 99 "2051-24-3


Page 148 of 23109-May-19 16:45

TMW-1


30-Apr-19 16:20


01-May-19

Client Project #





Analysis performed by Phoenix Environmental Labs, Inc. * - PH0618

30-150 % SW8081B 02-May-19 19:24 477223A01-May-1

9

%TCMX (Surrogate Rec) 81 PH0618877-09-8



SW8082A 02-May-1

9 21:28

"ug/l 0.094< 0.09412674-11-2 PCB-1016 1 477222APH06180.094

" ""ug/l 0.094< 0.09411104-28-2 PCB-1221 1 ""0.094

" ""ug/l 0.094< 0.09411141-16-5 PCB-1232 1 ""0.094

" ""ug/l 0.094< 0.09453469-21-9 PCB-1242 1 ""0.094

" ""ug/l 0.094< 0.09412672-29-6 PCB-1248 1 ""0.094

" ""ug/l 0.094< 0.09411097-69-1 PCB-1254 1 ""0.094

" ""ug/l 0.094< 0.09411096-82-5 PCB-1260 1 ""0.094

" ""ug/l 0.094< 0.09437324-23-5 PCB-1262 1 ""0.094

" ""ug/l 0.094< 0.09411100-14-4 PCB-1268 1 ""0.094


30-150 % " " ""% DCBP 64 "2051-24-3

30-150 % " " ""% TCMX 77 "877-09-8




SW8260C 04-May-1

9 02:35

01-May-1

9 22:19

ug/l 1.0< 1.0630-20-6 1,1,1,2-Tetrachloroethane 1 477696APH06181.0

" ""ug/l 1.0< 1.071-55-6 1,1,1-Trichloroethane 1 ""1.0

" ""ug/l 0.50< 0.5079-34-5 1,1,2,2-Tetrachloroethane 1 ""0.50


" ""ug/l 1.0< 1.075-34-3 1,1-Dichloroethane 1 ""1.0

" ""ug/l 1.0< 1.075-35-4 1,1-Dichloroethene 1 ""1.0

" ""ug/l 1.0< 1.0563-58-6 1,1-Dichloropropene 1 ""1.0

" ""ug/l 1.0< 1.087-61-6 1,2,3-Trichlorobenzene 1 ""1.0

" ""ug/l 1.0< 1.096-18-4 1,2,3-Trichloropropane 1 ""1.0


" ""ug/l 1.0< 1.095-63-6 1,2,4-Trimethylbenzene 1 ""1.0

" ""ug/l 1.0< 1.096-12-8 1,2-Dibromo-3-chloroprop

ane

1 ""1.0

" ""ug/l 1.0< 1.0106-93-4 1,2-Dibromoethane 1 ""1.0

" ""ug/l 1.0< 1.095-50-1 1,2-Dichlorobenzene 1 ""1.0


" ""ug/l 1.0< 1.078-87-5 1,2-Dichloropropane 1 ""1.0






" ""ug/l 1.0< 1.095-49-8 2-Chlorotoluene 1 ""1.0

" ""ug/l 5.0< 5.0591-78-6 2-Hexanone 1 ""5.0

" ""ug/l 1.0< 1.0527-84-4 2-Isopropyltoluene 1 ""1.0


Page 149 of 23109-May-19 16:45

TMW-1


30-Apr-19 16:20


01-May-19

Client Project #






SW8260C 04-May-1

9 02:35

01-May-1

9 22:19

ug/l 1.0< 1.0106-43-4 4-Chlorotoluene 1 477696APH06181.0

" ""ug/l 5.0< 5.0108-10-1 4-Methyl-2-pentanone 1 ""5.0

" ""ug/l 25< 2567-64-1 Acetone 1 ""25

" ""ug/l 1.0< 1.0107-13-1 Acrylonitrile 1 ""1.0

" ""ug/l 0.70< 0.7071-43-2 Benzene 1 ""0.70

" ""ug/l 1.0< 1.0108-86-1 Bromobenzene 1 ""1.0

" ""ug/l 1.0< 1.074-97-5 Bromochloromethane 1 ""1.0

" ""ug/l 0.50< 0.5075-27-4 Bromodichloromethane 1 ""0.50

" ""ug/l 1.0< 1.075-25-2 Bromoform 1 ""1.0

" ""ug/l 1.0< 1.074-83-9 Bromomethane 1 ""1.0

" ""ug/l 5.0< 5.075-15-0 Carbon Disulfide 1 ""5.0

" ""ug/l 1.0< 1.056-23-5 Carbon tetrachloride 1 ""1.0

" ""ug/l 1.0< 1.0108-90-7 Chlorobenzene 1 ""1.0

" ""ug/l 1.0< 1.075-00-3 Chloroethane 1 ""1.0

" ""ug/l 1.0< 1.067-66-3 Chloroform 1 ""1.0

" ""ug/l 1.0< 1.074-87-3 Chloromethane 1 ""1.0

" ""ug/l 1.02.8156-59-2 cis-1,2-Dichloroethene 1 ""1.0

" ""ug/l 0.40< 0.4010061-01-5 cis-1,3-Dichloropropene 1 ""0.40

" ""ug/l 0.50< 0.50124-48-1 Dibromochloromethane 1 ""0.50

" ""ug/l 1.0< 1.074-95-3 Dibromomethane 1 ""1.0

" ""ug/l 1.0< 1.075-71-8 Dichlorodifluoromethane 1 ""1.0

" ""ug/l 1.0< 1.0100-41-4 Ethylbenzene 1 ""1.0

" ""ug/l 0.40< 0.4087-68-3 Hexachlorobutadiene 1 ""0.40

" ""ug/l 1.0< 1.098-82-8 Isopropylbenzene 1 ""1.0

" ""ug/l 1.0< 1.0179601-23-1 m&p-Xylene 1 ""1.0

" ""ug/l 5.0< 5.078-93-3 Methyl ethyl ketone 1 ""5.0

" ""ug/l 1.0< 1.01634-04-4 Methyl t-butyl ether

(MTBE)

1 ""1.0

" ""ug/l 1.0< 1.075-09-2 Methylene chloride 1 ""1.0

" ""ug/l 1.0< 1.091-20-3 Naphthalene 1 ""1.0

" ""ug/l 1.0< 1.0104-51-8 n-Butylbenzene 1 ""1.0

" ""ug/l 1.0< 1.0103-65-1 n-Propylbenzene 1 ""1.0

" ""ug/l 1.0< 1.095-47-6 o-Xylene 1 ""1.0

" ""ug/l 1.0< 1.099-87-6 p-Isopropyltoluene 1 ""1.0

" ""ug/l 1.0< 1.0135-98-8 sec-Butylbenzene 1 ""1.0

" ""ug/l 1.0< 1.0100-42-5 Styrene 1 ""1.0

" ""ug/l 1.0< 1.098-06-6 tert-Butylbenzene 1 ""1.0

" ""ug/l 1.0< 1.0127-18-4 Tetrachloroethene 1 ""1.0

" ""ug/l 2.5< 2.5109-99-9 Tetrahydrofuran (THF) 1 ""2.5

" ""ug/l 1.0< 1.0108-88-3 Toluene 1 ""1.0

" ""ug/l 1.0< 1.01330-20-7 Total Xylenes 1 ""1.0

" ""ug/l 1.0< 1.0156-60-5 trans-1,2-Dichloroethene 1 ""1.0

" ""ug/l 0.40< 0.4010061-02-6 trans-1,3-Dichloropropene 1 ""0.40


Page 150 of 23109-May-19 16:45

TMW-1


30-Apr-19 16:20


01-May-19

Client Project #






SW8260C 04-May-1

9 02:35

01-May-1

9 22:19

ug/l 5.0< 5.0110-57-6 trans-1,4-dichloro-2-buten

e

1 477696APH06185.0

" ""ug/l 1.0< 1.079-01-6 Trichloroethene 1 ""1.0

" ""ug/l 1.0< 1.075-69-4 Trichlorofluoromethane 1 ""1.0

" ""ug/l 1.0< 1.076-13-1 Trichlorotrifluoroethane 1 ""1.0

" ""ug/l 1.0< 1.075-01-4 Vinyl chloride 1 ""1.0





70-130 % " " ""% Toluene-d8 93 "2037-26-5




SW8270D 05-May-1

9 22:05

01-May-1

9

ug/l 3.3< 3.395-94-3 1,2,4,5-Tetrachlorobenzen

e

1 477196APH06183.3



" ""ug/l 4.7< 4.7122-66-7 1,2-Diphenylhydrazine 1 ""4.7



" ""ug/l 0.94< 0.9495-95-4 2,4,5-Trichlorophenol 1 ""0.94


" ""ug/l 0.94< 0.94120-83-2 2,4-Dichlorophenol 1 ""0.94

" ""ug/l 0.94< 0.94105-67-9 2,4-Dimethylphenol 1 ""0.94

" ""ug/l 0.94< 0.9451-28-5 2,4-Dinitrophenol 1 ""0.94

" ""ug/l 4.7< 4.7121-14-2 2,4-Dinitrotoluene 1 ""4.7


" ""ug/l 4.7< 4.791-58-7 2-Chloronaphthalene 1 ""4.7

" ""ug/l 0.94< 0.9495-57-8 2-Chlorophenol 1 ""0.94

" ""ug/l 0.94< 0.9495-48-7 2-Methylphenol (o-cresol) 1 ""0.94

" ""ug/l 4.7< 4.788-74-4 2-Nitroaniline 1 ""4.7

" ""ug/l 0.94< 0.9488-75-5 2-Nitrophenol 1 ""0.94

" ""ug/l 9.4< 9.43&4-Methylphenol

(m&p-cresol)

1 ""9.4

" ""ug/l 4.7< 4.791-94-1 3,3'-Dichlorobenzidine 1 ""4.7


" ""ug/l 0.94< 0.94534-52-1 4,6-Dinitro-2-methylphenol 1 ""0.94

" ""ug/l 4.7< 4.7101-55-3 4-Bromophenyl phenyl

ether

1 ""4.7

" ""ug/l 0.94< 0.9459-50-7 4-Chloro-3-methylphenol 1 ""0.94

" ""ug/l 4.7< 4.7106-47-8 4-Chloroaniline 1 ""4.7

" ""ug/l 0.94< 0.947005-72-3 4-Chlorophenyl phenyl

ether

1 ""0.94


" ""ug/l 0.94< 0.94100-02-7 4-Nitrophenol 1 ""0.94


Page 151 of 23109-May-19 16:45

TMW-1


30-Apr-19 16:20


01-May-19

Client Project #






SW8270D 05-May-1

9 22:05

01-May-1

9

ug/l 4.7< 4.798-86-2 Acetophenone 1 477196APH06184.7

" ""ug/l 4.7< 4.762-53-3 Aniline 1 ""4.7

" ""ug/l 4.7< 4.792-87-5 Benzidine 1 ""4.7

" ""ug/l 47< 4765-85-0 Benzoic acid 1 ""47

" ""ug/l 4.7< 4.785-68-7 Benzyl butyl phthalate 1 ""4.7

" ""ug/l 4.7< 4.7111-91-1 Bis(2-chloroethoxy)metha

ne

1 ""4.7

" ""ug/l 0.94< 0.94111-44-4 Bis(2-chloroethyl)ether 1 ""0.94

" ""ug/l 4.7< 4.739638-32-9 Bis(2-chloroisopropyl)ethe

r

1 ""4.7

" ""ug/l 0.94< 0.94117-81-7 Bis(2-ethylhexyl)phthalate 1 ""0.94

" ""ug/l 4.7< 4.786-74-8 Carbazole 1 ""4.7

" ""ug/l 0.94< 0.94132-64-9 Dibenzofuran 1 ""0.94

" ""ug/l 4.7< 4.784-66-2 Diethyl phthalate 1 ""4.7

" ""ug/l 4.7< 4.7131-11-3 Dimethylphthalate 1 ""4.7

" ""ug/l 4.7< 4.784-74-2 Di-n-butylphthalate 1 ""4.7

" ""ug/l 4.7< 4.7117-84-0 Di-n-octylphthalate 1 ""4.7

" ""ug/l 0.94< 0.9467-72-1 Hexachloroethane 1 ""0.94

" ""ug/l 4.7< 4.778-59-1 Isophorone 1 ""4.7

" ""ug/l 4.7< 4.762-75-9 N-Nitrosodimethylamine 1 ""4.7

" ""ug/l 4.7< 4.7621-64-7 N-Nitrosodi-n-propylamine 1 ""4.7

" ""ug/l 4.7< 4.786-30-6 N-Nitrosodiphenylamine 1 ""4.7

" ""ug/l 2.4< 2.482-68-8 Pentachloronitrobenzene 1 ""2.4

" ""ug/l 0.94< 0.94108-95-2 Phenol 1 ""0.94


15-110 % " " ""% 2,4,6-Tribromophenol 88 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 68 "321-60-8

15-110 % " " ""% 2-Fluorophenol 59 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 76 "4165-60-0

15-110 % " " ""% Phenol-d5 61 "4165-62-2

30-130 % " " ""% Terphenyl-d14 64 "98904-43-9



SW8270D (SIM) 03-May-1

9 15:00

"ug/l 0.47< 0.4791-57-6 2-Methylnaphthalene 1 477196BPH06180.47

" ""ug/l 0.47< 0.4783-32-9 Acenaphthene 1 ""0.47

" ""ug/l 0.28< 0.28208-96-8 Acenaphthylene 1 ""0.28

" ""ug/l 0.47< 0.47120-12-7 Anthracene 1 ""0.47

" ""ug/l 0.05< 0.0556-55-3 Benz(a)anthracene 1 ""0.05

" ""ug/l 0.19< 0.1950-32-8 Benzo(a)pyrene 1 ""0.19

" ""ug/l 0.07< 0.07205-99-2 Benzo(b)fluoranthene 1 ""0.07

" ""ug/l 0.45< 0.45191-24-2 Benzo(ghi)perylene 1 ""0.45

" ""ug/l 0.28< 0.28207-08-9 Benzo(k)fluoranthene 1 ""0.28

" ""ug/l 0.47< 0.47218-01-9 Chrysene 1 ""0.47

" ""ug/l 0.09< 0.0953-70-3 Dibenz(a,h)anthracene 1 ""0.09


Page 152 of 23109-May-19 16:45

TMW-1


30-Apr-19 16:20


01-May-19

Client Project #







9 15:00

01-May-1

9

ug/l 0.47< 0.47206-44-0 Fluoranthene 1 477196BPH06180.47

" ""ug/l 0.47< 0.4786-73-7 Fluorene 1 ""0.47

" ""ug/l 0.06< 0.06118-74-1 Hexachlorobenzene 1 ""0.06


" ""ug/l 0.47< 0.4777-47-4 Hexachlorocyclopentadien

e

1 ""0.47

" ""ug/l 0.09< 0.09193-39-5 Indeno(1,2,3-cd)pyrene 1 ""0.09

" ""ug/l 0.47< 0.4791-20-3 Naphthalene 1 ""0.47

" ""ug/l 0.47< 0.4798-95-3 Nitrobenzene 1 ""0.47

" ""ug/l 0.47< 0.4787-86-5 Pentachlorophenol 1 ""0.47

" ""ug/l 0.06< 0.0685-01-8 Phenanthrene 1 ""0.06

" ""ug/l 0.47< 0.47129-00-0 Pyrene 1 ""0.47

" ""ug/l 0.47< 0.47110-86-1 Pyridine 1 ""0.47


15-110 % " " ""% 2,4,6-Tribromophenol 97 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 73 "321-60-8

15-110 % " " ""% 2-Fluorophenol 67 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 68 "4165-60-0

15-110 % " " ""% Phenol-d5 70 "4165-62-2

30-130 % " " ""% Terphenyl-d14 85 "98904-43-9


Page 153 of 23109-May-19 16:45

TMW-2


30-Apr-19 11:45


01-May-19

Client Project #








9 01:29

01-May-1

9


(C9-C36)

1 477197APH06180.066


50-150 % " " ""% n-Pentacosane 77 "629-99-2




SW6010D 03-May-1

9 15:50

"mg/l 0.025< 0.0257440-50-8 Copper 5 477208APH06180.025

" ""mg/l 0.010< 0.0107439-92-1 Lead 5 ""0.010

" ""mg/l 0.020< 0.0207440-66-6 Zinc 5 ""0.020




SW6010D

dissolved

03-May-1

9 01:33


" ""mg/l 0.0020.0047439-92-1 Lead (Dissolved) 1 ""0.002





SW8081B 02-May-1

9 19:42

"ug/l 0.049< 0.04972-54-8 4,4' -DDD 1 477223APH06180.049

" ""ug/l 0.049< 0.04972-55-9 4,4' -DDE 1 ""0.049

" ""ug/l 0.049< 0.04950-29-3 4,4' -DDT 1 ""0.049

" ""ug/l 0.025< 0.025319-84-6 a-BHC 1 ""0.025

" ""ug/l 0.074< 0.07415972-60-8 Alachlor 1 ""0.074

" ""ug/l 0.010< 0.010309-00-2 Aldrin 1 ""0.010

" ""ug/l 0.005< 0.005319-85-7 b-BHC 1 ""0.005

" ""ug/l 0.29< 0.2957-74-9 Chlordane 1 ""0.29

" ""ug/l 0.025< 0.025319-86-8 d-BHC 1 ""0.025

" ""ug/l 0.0020.01860-57-1 Dieldrin 1 ""0.002

" ""ug/l 0.049< 0.049959-98-8 Endosulfan I 1 ""0.049



" ""ug/l 0.049< 0.04972-20-8 Endrin 1 ""0.049



" ""ug/l 0.025< 0.02558-89-9 g-BHC (Lindane) 1 ""0.025

" ""ug/l 0.025< 0.02576-44-8 Heptachlor 1 ""0.025



" ""ug/l 0.98< 0.988001-35-2 Toxaphene 1 ""0.98




Page 154 of 23109-May-19 16:45

TMW-2


30-Apr-19 11:45


01-May-19

Client Project #






30-150 % SW8081B 02-May-19 19:42 477223A01-May-1

9




SW8082A 02-May-1

9 21:50

"ug/l 0.098< 0.09812674-11-2 PCB-1016 1 477222APH06180.098

" ""ug/l 0.098< 0.09811104-28-2 PCB-1221 1 ""0.098

" ""ug/l 0.098< 0.09811141-16-5 PCB-1232 1 ""0.098

" ""ug/l 0.098< 0.09853469-21-9 PCB-1242 1 ""0.098

" ""ug/l 0.098< 0.09812672-29-6 PCB-1248 1 ""0.098

" ""ug/l 0.098< 0.09811097-69-1 PCB-1254 1 ""0.098

" ""ug/l 0.098< 0.09811096-82-5 PCB-1260 1 ""0.098

" ""ug/l 0.098< 0.09837324-23-5 PCB-1262 1 ""0.098

" ""ug/l 0.098< 0.09811100-14-4 PCB-1268 1 ""0.098


30-150 % " " ""% DCBP 71 "2051-24-3

30-150 % " " ""% TCMX 99 "877-09-8




SW8260C 04-May-1

9 03:00

01-May-1

9 22:19


" ""ug/l 1.06.671-55-6 1,1,1-Trichloroethane 1 ""1.0



" ""ug/l 1023075-34-3 1,1-Dichloroethane 10 ""10

" ""ug/l 1.08.375-35-4 1,1-Dichloroethene 1 ""1.0





" ""ug/l 1.05.495-63-6 1,2,4-Trimethylbenzene 1 ""1.0


ane

1 ""1.0


" ""ug/l 1.04.895-50-1 1,2-Dichlorobenzene 1 ""1.0

" ""ug/l 0.601.0107-06-2 1,2-Dichloroethane 1 ""0.60








" ""ug/l 5.0< 5.0591-78-6 2-Hexanone 1 ""5.0



Page 155 of 23109-May-19 16:45

TMW-2


30-Apr-19 11:45


01-May-19

Client Project #






SW8260C 04-May-1

9 03:00

01-May-1

9 22:19



" ""ug/l 25< 2567-64-1 Acetone 1 ""25


" ""ug/l 0.70< 0.7071-43-2 Benzene 1 ""0.70




" ""ug/l 1.0< 1.075-25-2 Bromoform 1 ""1.0





" ""ug/l 1.0< 1.067-66-3 Chloroform 1 ""1.0






" ""ug/l 1.013100-41-4 Ethylbenzene 1 ""1.0


" ""ug/l 1.01.398-82-8 Isopropylbenzene 1 ""1.0

" ""ug/l 1.03.1179601-23-1 m&p-Xylene 1 ""1.0



(MTBE)

1 ""1.0

" ""ug/l 1.02.275-09-2 Methylene chloride 1 ""1.0S

" ""ug/l 1.0< 1.091-20-3 Naphthalene 1 ""1.0


" ""ug/l 1.01.8103-65-1 n-Propylbenzene 1 ""1.0

" ""ug/l 1.01095-47-6 o-Xylene 1 ""1.0



" ""ug/l 1.0< 1.0100-42-5 Styrene 1 ""1.0


" ""ug/l 1.020127-18-4 Tetrachloroethene 1 ""1.0


" ""ug/l 1.09.2108-88-3 Toluene 1 ""1.0

" ""ug/l 1.013.11330-20-7 Total Xylenes 1 ""1.0



" ""ug/l 5.0< 5.0110-57-6 trans-1,4-dichloro-2-buten

e

1 ""5.0



Page 156 of 23109-May-19 16:45

TMW-2


30-Apr-19 11:45


01-May-19

Client Project #






SW8260C 04-May-1

9 03:00

01-May-1

9 22:19

ug/l 1.09.976-13-1 Trichlorotrifluoroethane 1 477696APH06181.0





70-130 % " " ""% Toluene-d8 108 "2037-26-5



SW8260C 04-May-1

9 15:53

04-May-1

9 12:29

ug/l 1026075-00-3 Chloroethane 10 477712APH061810

" ""ug/l 103579-01-6 Trichloroethene 10 ""10

" ""ug/l 1023075-01-4 Vinyl chloride 10 ""10





70-130 % " " ""% Toluene-d8 100 "2037-26-5



SW8260C 06-May-1

9 14:07

05-May-1

9 16:25

ug/l 20260156-59-2 cis-1,2-Dichloroethene 20 477847APH061820





70-130 % " " ""% Toluene-d8 102 "2037-26-5




SW8270D 05-May-1

9 22:55

01-May-1

9


e

1 477196APH06183.3


" ""ug/l 2.42.695-50-1 1,2-Dichlorobenzene 1 ""2.4














Page 157 of 23109-May-19 16:45

TMW-2


30-Apr-19 11:45


01-May-19

Client Project #






SW8270D 05-May-1

9 22:55

01-May-1

9

ug/l 0.94< 0.9495-48-7 2-Methylphenol (o-cresol) 1 477196APH06180.94


" ""ug/l 0.94< 0.9488-75-5 2-Nitrophenol 1 ""0.94


(m&p-cresol)

1 ""9.4





ether

1 ""4.7




ether

1 ""0.94


" ""ug/l 0.94< 0.94100-02-7 4-Nitrophenol 1 ""0.94

" ""ug/l 4.7< 4.798-86-2 Acetophenone 1 ""4.7

" ""ug/l 4.7< 4.762-53-3 Aniline 1 ""4.7

" ""ug/l 4.7< 4.792-87-5 Benzidine 1 ""4.7

" ""ug/l 47< 4765-85-0 Benzoic acid 1 ""47



ne

1 ""4.7



r

1 ""4.7

" ""ug/l 0.941.4117-81-7 Bis(2-ethylhexyl)phthalate 1 ""0.94

" ""ug/l 4.7< 4.786-74-8 Carbazole 1 ""4.7







" ""ug/l 4.7< 4.778-59-1 Isophorone 1 ""4.7





" ""ug/l 0.94< 0.94108-95-2 Phenol 1 ""0.94


15-110 % " " ""% 2,4,6-Tribromophenol 79 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 59 "321-60-8

15-110 % " " ""% 2-Fluorophenol 51 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 63 "4165-60-0


Page 158 of 23109-May-19 16:45

TMW-2


30-Apr-19 11:45


01-May-19

Client Project #






15-110 % SW8270D 05-May-19 22:55 477196A01-May-1

9

% Phenol-d5 56 PH06184165-62-2

30-130 % " " ""% Terphenyl-d14 49 "98904-43-9




9 15:22




" ""ug/l 0.47< 0.47120-12-7 Anthracene 1 ""0.47






" ""ug/l 0.47< 0.47218-01-9 Chrysene 1 ""0.47


" ""ug/l 0.47< 0.47206-44-0 Fluoranthene 1 ""0.47

" ""ug/l 0.47< 0.4786-73-7 Fluorene 1 ""0.47




e

1 ""0.47


" ""ug/l 0.47< 0.4791-20-3 Naphthalene 1 ""0.47




" ""ug/l 0.47< 0.47129-00-0 Pyrene 1 ""0.47

" ""ug/l 0.47< 0.47110-86-1 Pyridine 1 ""0.47


15-110 % " " ""% 2,4,6-Tribromophenol 98 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 70 "321-60-8

15-110 % " " ""% 2-Fluorophenol 64 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 69 "4165-60-0

15-110 % " " ""% Phenol-d5 72 "4165-62-2

30-130 % " " ""% Terphenyl-d14 78 "98904-43-9


Page 159 of 23109-May-19 16:45

DUP


30-Apr-19 00:00


01-May-19

Client Project #








9 02:05

01-May-1

9


(C9-C36)

1 477197APH06180.066


50-150 % " " ""% n-Pentacosane 79 "629-99-2




SW6010D 02-May-1

9 22:56

"mg/l 0.0050.0077440-50-8 Copper 1 477208APH06180.005

" ""mg/l 0.0020.0037439-92-1 Lead 1 ""0.002

" ""mg/l 0.0040.0087440-66-6 Zinc 1 ""0.004




SW6010D

dissolved

03-May-1

9 01:36


" ""mg/l 0.002< 0.0027439-92-1 Lead (Dissolved) 1 ""0.002





SW8081B 02-May-1

9 18:47

"ug/l 0.047< 0.04772-54-8 4,4' -DDD 1 477223APH06180.047

" ""ug/l 0.047< 0.04772-55-9 4,4' -DDE 1 ""0.047

" ""ug/l 0.047< 0.04750-29-3 4,4' -DDT 1 ""0.047

" ""ug/l 0.023< 0.023319-84-6 a-BHC 1 ""0.023

" ""ug/l 0.070< 0.07015972-60-8 Alachlor 1 ""0.070

" ""ug/l 0.005< 0.005309-00-2 Aldrin 1 ""0.005

" ""ug/l 0.005< 0.005319-85-7 b-BHC 1 ""0.005

" ""ug/l 0.28< 0.2857-74-9 Chlordane 1 ""0.28

" ""ug/l 0.023< 0.023319-86-8 d-BHC 1 ""0.023

" ""ug/l 0.001< 0.00160-57-1 Dieldrin 1 ""0.001

" ""ug/l 0.047< 0.047959-98-8 Endosulfan I 1 ""0.047



" ""ug/l 0.047< 0.04772-20-8 Endrin 1 ""0.047



" ""ug/l 0.023< 0.02358-89-9 g-BHC (Lindane) 1 ""0.023

" ""ug/l 0.023< 0.02376-44-8 Heptachlor 1 ""0.023



" ""ug/l 0.93< 0.938001-35-2 Toxaphene 1 ""0.93




Page 160 of 23109-May-19 16:45

DUP


30-Apr-19 00:00


01-May-19

Client Project #






30-150 % SW8081B 02-May-19 18:47 477223A01-May-1

9




SW8082A 02-May-1

9 20:44

"ug/l 0.093< 0.09312674-11-2 PCB-1016 1 477222APH06180.093

" ""ug/l 0.093< 0.09311104-28-2 PCB-1221 1 ""0.093

" ""ug/l 0.093< 0.09311141-16-5 PCB-1232 1 ""0.093

" ""ug/l 0.093< 0.09353469-21-9 PCB-1242 1 ""0.093

" ""ug/l 0.093< 0.09312672-29-6 PCB-1248 1 ""0.093

" ""ug/l 0.093< 0.09311097-69-1 PCB-1254 1 ""0.093

" ""ug/l 0.093< 0.09311096-82-5 PCB-1260 1 ""0.093

" ""ug/l 0.093< 0.09337324-23-5 PCB-1262 1 ""0.093

" ""ug/l 0.093< 0.09311100-14-4 PCB-1268 1 ""0.093


30-150 % " " ""% DCBP 69 "2051-24-3

30-150 % " " ""% TCMX 83 "877-09-8




SW8260C 04-May-1

9 13:38

04-May-1

9 11:25













ane

1 ""1.0











" ""ug/l 5.0< 5.0591-78-6 2-Hexanone 1 ""5.0



Page 161 of 23109-May-19 16:45

DUP


30-Apr-19 00:00


01-May-19

Client Project #






SW8260C 04-May-1

9 13:38

04-May-1

9 11:25



" ""ug/l 25< 2567-64-1 Acetone 1 ""25


" ""ug/l 0.70< 0.7071-43-2 Benzene 1 ""0.70




" ""ug/l 1.0< 1.075-25-2 Bromoform 1 ""1.0






" ""ug/l 1.0< 1.067-66-3 Chloroform 1 ""1.0


" ""ug/l 1.0< 1.0156-59-2 cis-1,2-Dichloroethene 1 ""1.0








" ""ug/l 1.0< 1.0179601-23-1 m&p-Xylene 1 ""1.0



(MTBE)

1 ""1.0


" ""ug/l 1.0< 1.091-20-3 Naphthalene 1 ""1.0



" ""ug/l 1.0< 1.095-47-6 o-Xylene 1 ""1.0



" ""ug/l 1.0< 1.0100-42-5 Styrene 1 ""1.0




" ""ug/l 1.0< 1.0108-88-3 Toluene 1 ""1.0





Page 162 of 23109-May-19 16:45

DUP


30-Apr-19 00:00


01-May-19

Client Project #






SW8260C 04-May-1

9 13:38

04-May-1

9 11:25


e

1 477712APH06185.0









70-130 % " " ""% Toluene-d8 100 "2037-26-5




SW8270D 05-May-1

9 23:20

01-May-1

9


e

1 477196APH06183.3

















" ""ug/l 0.94< 0.9488-75-5 2-Nitrophenol 1 ""0.94


(m&p-cresol)

1 ""9.4





ether

1 ""4.7




ether

1 ""0.94


" ""ug/l 0.94< 0.94100-02-7 4-Nitrophenol 1 ""0.94


Page 163 of 23109-May-19 16:45

DUP


30-Apr-19 00:00


01-May-19

Client Project #






SW8270D 05-May-1

9 23:20

01-May-1

9

ug/l 4.7< 4.798-86-2 Acetophenone 1 477196APH06184.7

" ""ug/l 4.7< 4.762-53-3 Aniline 1 ""4.7

" ""ug/l 4.7< 4.792-87-5 Benzidine 1 ""4.7

" ""ug/l 47< 4765-85-0 Benzoic acid 1 ""47



ne

1 ""4.7



r

1 ""4.7


" ""ug/l 4.7< 4.786-74-8 Carbazole 1 ""4.7







" ""ug/l 4.7< 4.778-59-1 Isophorone 1 ""4.7





" ""ug/l 0.94< 0.94108-95-2 Phenol 1 ""0.94


15-110 % " " ""% 2,4,6-Tribromophenol 72 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 56 "321-60-8

15-110 % " " ""% 2-Fluorophenol 43 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 54 "4165-60-0

15-110 % " " ""% Phenol-d5 21 "4165-62-2

30-130 % " " ""% Terphenyl-d14 52 "98904-43-9




9 15:45




" ""ug/l 0.47< 0.47120-12-7 Anthracene 1 ""0.47






" ""ug/l 0.47< 0.47218-01-9 Chrysene 1 ""0.47



Page 164 of 23109-May-19 16:45

DUP


30-Apr-19 00:00


01-May-19

Client Project #







9 15:45

01-May-1

9

ug/l 0.47< 0.47206-44-0 Fluoranthene 1 477196BPH06180.47

" ""ug/l 0.47< 0.4786-73-7 Fluorene 1 ""0.47




e

1 ""0.47


" ""ug/l 0.47< 0.4791-20-3 Naphthalene 1 ""0.47




" ""ug/l 0.47< 0.47129-00-0 Pyrene 1 ""0.47

" ""ug/l 0.47< 0.47110-86-1 Pyridine 1 ""0.47


15-110 % " " ""% 2,4,6-Tribromophenol 94 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 72 "321-60-8

15-110 % " " ""% 2-Fluorophenol 55 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 65 "4165-60-0

15-110 % " " ""% Phenol-d5 30 "4165-62-2

30-130 % " " ""% Terphenyl-d14 81 "98904-43-9


Page 165 of 23109-May-19 16:45

Field Blank


30-Apr-19 17:00


01-May-19

Client Project #








9 02:40

01-May-1

9


(C9-C36)

1 477197APH06180.066


50-150 % " " ""% n-Pentacosane 80 "629-99-2




SW6010D 02-May-1

9 22:58

"mg/l 0.005< 0.0057440-50-8 Copper 1 477208APH06180.005

" ""mg/l 0.002< 0.0027439-92-1 Lead 1 ""0.002

" ""mg/l 0.0040.0137440-66-6 Zinc 1 ""0.004




SW6010D

dissolved

03-May-1

9 01:38


" ""mg/l 0.002< 0.0027439-92-1 Lead (Dissolved) 1 ""0.002

" ""mg/l 0.002< 0.0027440-66-6 Zinc (Dissolved) 1 ""0.002




SW8081B 02-May-1

9 19:05

"ug/l 0.047< 0.04772-54-8 4,4' -DDD 1 477223APH06180.047

" ""ug/l 0.047< 0.04772-55-9 4,4' -DDE 1 ""0.047

" ""ug/l 0.047< 0.04750-29-3 4,4' -DDT 1 ""0.047

" ""ug/l 0.023< 0.023319-84-6 a-BHC 1 ""0.023

" ""ug/l 0.070< 0.07015972-60-8 Alachlor 1 ""0.070

" ""ug/l 0.001< 0.001309-00-2 Aldrin 1 ""0.001

" ""ug/l 0.005< 0.005319-85-7 b-BHC 1 ""0.005

" ""ug/l 0.28< 0.2857-74-9 Chlordane 1 ""0.28

" ""ug/l 0.023< 0.023319-86-8 d-BHC 1 ""0.023

" ""ug/l 0.001< 0.00160-57-1 Dieldrin 1 ""0.001

" ""ug/l 0.047< 0.047959-98-8 Endosulfan I 1 ""0.047



" ""ug/l 0.047< 0.04772-20-8 Endrin 1 ""0.047



" ""ug/l 0.023< 0.02358-89-9 g-BHC (Lindane) 1 ""0.023

" ""ug/l 0.023< 0.02376-44-8 Heptachlor 1 ""0.023



" ""ug/l 0.93< 0.938001-35-2 Toxaphene 1 ""0.93




Page 166 of 23109-May-19 16:45

Field Blank


30-Apr-19 17:00


01-May-19

Client Project #






30-150 % SW8081B 02-May-19 19:05 477223A01-May-1

9




SW8082A 02-May-1

9 21:06

"ug/l 0.093< 0.09312674-11-2 PCB-1016 1 477222APH06180.093

" ""ug/l 0.093< 0.09311104-28-2 PCB-1221 1 ""0.093

" ""ug/l 0.093< 0.09311141-16-5 PCB-1232 1 ""0.093

" ""ug/l 0.093< 0.09353469-21-9 PCB-1242 1 ""0.093

" ""ug/l 0.093< 0.09312672-29-6 PCB-1248 1 ""0.093

" ""ug/l 0.093< 0.09311097-69-1 PCB-1254 1 ""0.093

" ""ug/l 0.093< 0.09311096-82-5 PCB-1260 1 ""0.093

" ""ug/l 0.093< 0.09337324-23-5 PCB-1262 1 ""0.093

" ""ug/l 0.093< 0.09311100-14-4 PCB-1268 1 ""0.093


30-150 % " " ""% DCBP 75 "2051-24-3

30-150 % " " ""% TCMX 79 "877-09-8




SW8260C 04-May-1

9 14:01

04-May-1

9 11:25













ane

1 ""1.0











" ""ug/l 5.0< 5.0591-78-6 2-Hexanone 1 ""5.0



Page 167 of 23109-May-19 16:45

Field Blank


30-Apr-19 17:00


01-May-19

Client Project #






SW8260C 04-May-1

9 14:01

04-May-1

9 11:25



" ""ug/l 25< 2567-64-1 Acetone 1 ""25


" ""ug/l 0.70< 0.7071-43-2 Benzene 1 ""0.70




" ""ug/l 1.0< 1.075-25-2 Bromoform 1 ""1.0






" ""ug/l 1.0< 1.067-66-3 Chloroform 1 ""1.0










" ""ug/l 1.0< 1.0179601-23-1 m&p-Xylene 1 ""1.0



(MTBE)

1 ""1.0


" ""ug/l 1.0< 1.091-20-3 Naphthalene 1 ""1.0



" ""ug/l 1.0< 1.095-47-6 o-Xylene 1 ""1.0



" ""ug/l 1.0< 1.0100-42-5 Styrene 1 ""1.0




" ""ug/l 1.0< 1.0108-88-3 Toluene 1 ""1.0





Page 168 of 23109-May-19 16:45

Field Blank


30-Apr-19 17:00


01-May-19

Client Project #






SW8260C 04-May-1

9 14:01

04-May-1

9 11:25


e

1 477712APH06185.0









70-130 % " " ""% Toluene-d8 101 "2037-26-5




SW8270D 05-May-1

9 23:45

01-May-1

9


e

1 477196APH06183.3
















" ""ug/l 0.94< 0.9488-75-5 2-Nitrophenol 1 ""0.94


(m&p-cresol)

1 ""9.4





ether

1 ""4.7




ether

1 ""0.94


" ""ug/l 0.94< 0.94100-02-7 4-Nitrophenol 1 ""0.94

" ""ug/l 4.7< 4.798-86-2 Acetophenone 1 ""4.7


Page 169 of 23109-May-19 16:45

Field Blank


30-Apr-19 17:00


01-May-19

Client Project #






SW8270D 05-May-1

9 23:45

01-May-1

9

ug/l 4.7< 4.762-53-3 Aniline 1 477196APH06184.7

" ""ug/l 4.7< 4.792-87-5 Benzidine 1 ""4.7

" ""ug/l 47< 4765-85-0 Benzoic acid 1 ""47



ne

1 ""4.7



r

1 ""4.7


" ""ug/l 4.7< 4.786-74-8 Carbazole 1 ""4.7







" ""ug/l 4.7< 4.778-59-1 Isophorone 1 ""4.7





" ""ug/l 0.94< 0.94108-95-2 Phenol 1 ""0.94


15-110 % " " ""% 2,4,6-Tribromophenol 64 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 58 "321-60-8

15-110 % " " ""% 2-Fluorophenol 50 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 64 "4165-60-0

15-110 % " " ""% Phenol-d5 54 "4165-62-2

30-130 % " " ""% Terphenyl-d14 52 "98904-43-9



SW8270D 05-May-1

9 23:45

01-May-1

9

ug/l 2.4< 2.4541-73-1 1,3-Dichlorobenzene 1 477196APH06182.4





9 16:07

01-May-1

9

ug/l 0.47< 0.4791-57-6 2-Methylnaphthalene 1 477196BPH06180.47



" ""ug/l 0.47< 0.47120-12-7 Anthracene 1 ""0.47





Page 170 of 23109-May-19 16:45

Field Blank


30-Apr-19 17:00


01-May-19

Client Project #







9 16:07

01-May-1

9

ug/l 0.45< 0.45191-24-2 Benzo(ghi)perylene 1 477196BPH06180.45


" ""ug/l 0.47< 0.47218-01-9 Chrysene 1 ""0.47


" ""ug/l 0.47< 0.47206-44-0 Fluoranthene 1 ""0.47

" ""ug/l 0.47< 0.4786-73-7 Fluorene 1 ""0.47




e

1 ""0.47


" ""ug/l 0.47< 0.4791-20-3 Naphthalene 1 ""0.47




" ""ug/l 0.47< 0.47129-00-0 Pyrene 1 ""0.47

" ""ug/l 0.47< 0.47110-86-1 Pyridine 1 ""0.47


15-110 % " " ""% 2,4,6-Tribromophenol 91 "118-79-6

30-130 % " " ""% 2-Fluorobiphenyl 68 "321-60-8

15-110 % " " ""% 2-Fluorophenol 69 "367-12-4

30-130 % " " ""% Nitrobenzene-d5 70 "4165-60-0

15-110 % " " ""% Phenol-d5 73 "4165-62-2

30-130 % " " ""% Terphenyl-d14 82 "98904-43-9


Page 171 of 23109-May-19 16:45

Trip Blank


30-Apr-19 00:00


01-May-19

Client Project #







SW8260C 03-May-1

9 22:03

01-May-1

9 19:42













ane

1 ""1.0











" ""ug/l 5.0< 5.0591-78-6 2-Hexanone 1 ""5.0




" ""ug/l 25< 2567-64-1 Acetone 1 ""25


" ""ug/l 0.70< 0.7071-43-2 Benzene 1 ""0.70




" ""ug/l 1.0< 1.075-25-2 Bromoform 1 ""1.0






" ""ug/l 1.0< 1.067-66-3 Chloroform 1 ""1.0





Page 172 of 23109-May-19 16:45

Trip Blank


30-Apr-19 00:00


01-May-19

Client Project #






SW8260C 03-May-1

9 22:03

01-May-1

9 19:42

ug/l 0.50< 0.50124-48-1 Dibromochloromethane 1 477696APH06180.50






" ""ug/l 1.0< 1.0179601-23-1 m&p-Xylene 1 ""1.0



(MTBE)

1 ""1.0


" ""ug/l 1.0< 1.091-20-3 Naphthalene 1 ""1.0



" ""ug/l 1.0< 1.095-47-6 o-Xylene 1 ""1.0



" ""ug/l 1.0< 1.0100-42-5 Styrene 1 ""1.0




" ""ug/l 1.0< 1.0108-88-3 Toluene 1 ""1.0




" ""ug/l 5.0< 5.0110-57-6 trans-1,4-dichloro-2-buten

e

1 ""5.0









70-130 % " " ""% Toluene-d8 91 "2037-26-5


Page 173 of 23109-May-19 16:45

Toxicity Characteristics - Quality Control

Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitFlagAnalyte(s) *RDL

SW846 1030

Batch 1900599 - General Preparation

Duplicate (1900599-DUP1) Prepared: 01-May-19 Analyzed: 02-May-19Source: SC54611-01

35N/A NegativeNegativeIgnitability by Definition

SW846 9045D


Duplicate (1900598-DUP1) Prepared & Analyzed: 01-May-19Source: SC54611-02

52pH Units 6.446.57pH

Reference (1900598-SRM1) Prepared & Analyzed: 01-May-19

6.00 97.5-102.

5

pH Units6.04 101pH


6.00 97.5-102.

5

pH Units6.13 102pH


Duplicate (1900602-DUP1) Prepared & Analyzed: 02-May-19Source: SC54611-09

51pH Units 7.217.29pH


6.00 97.5-102.

5

pH Units6.09 102pH


6.00 97.5-102.

5

pH Units6.10 102pH


Page 174 of 23109-May-19 16:45

Subcontracted Analyses - Quality Control

Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


CTETPH 8015D

Batch 477139A - SW3545A

Blank (CD04771-BLK) Prepared: 01-May-19 Analyzed: 02-May-19

-mg/kgND NDExt. Petroleum H.C. (C9-C36) 50

50 50-150Surrogate: % n-Pentacosane 59 mg/kg 59

LCS (CD04771-LCS) Prepared: 01-May-19 Analyzed: 02-May-19

1900 3060-120mg/kg2278 120Ext. Petroleum H.C. (C9-C36) 50

50 50-150Surrogate: % n-Pentacosane 55.62 mg/kg 111

LCS Dup (CD04771-LCSD) Prepared: 01-May-19 Analyzed: 02-May-19Source: CD04771-LCS

1900 3060-120 16.2mg/kg1945 102Ext. Petroleum H.C. (C9-C36) 50


Batch 477191A - SW3545A


-mg/kgND NDExt. Petroleum H.C. (C9-C36) 50

50 50-150Surrogate: % n-Pentacosane 44 mg/kg 44


1900 3060-120mg/kg1697 89Ext. Petroleum H.C. (C9-C36) 50



1900 3060-120 22.9mg/kg2129 112Ext. Petroleum H.C. (C9-C36) 50


Matrix Spike (CD05122-MS) Prepared: 01-May-19 Analyzed: 03-May-19Source: SC54611-04

1900 3050-150mg/kg BRL2404 127Ext. Petroleum H.C. (C9-C36) 50


Matrix Spike Dup (CD05122-MSD) Prepared: 01-May-19 Analyzed: 03-May-19Source: SC54611-04

1900 3050-150 9.1mg/kg BRL2205 116Ext. Petroleum H.C. (C9-C36) 50


Batch 477197A - SW3510C/SW3520C


-mg/lND NDExt. Petroleum H.C. (C9-C36) 0.10

50 50-150Surrogate: % n-Pentacosane 79 mg/l 79


1900 3060-120mg/l1733 91Ext. Petroleum H.C. (C9-C36) 0.10

50 50-150Surrogate: % n-Pentacosane 48.93 mg/l 98


1900 3060-120 2.2mg/l1699 89Ext. Petroleum H.C. (C9-C36) 0.10

50 50-150Surrogate: % n-Pentacosane 44.46 mg/l 89

SW6010D

Batch 477188A - SW3050B


-mg/kg< 0.33 BRLSilver 0.33

-mg/kg< 0.33 BRLLead 0.33

-mg/kg< 0.33 BRLChromium 0.33

-mg/kg< 0.33 BRLCadmium 0.33

-mg/kg< 1.3 BRLSelenium 1.3

-mg/kg< 0.33 BRLBarium 0.33

-mg/kg< 0.67 BRLArsenic 0.67

Duplicate (CD05119-DUP) Prepared: 01-May-19 Analyzed: 02-May-19Source: SC54611-01


Page 175 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW6010D

Batch 477188A - SW3050B


30- NCmg/kg2.88Arsenic 0.77

30- NCmg/kg BRL< 0.39Cadmium 0.39

30- NCmg/kg BRL< 1.5Selenium 1.5

30- 20.8mg/kg14.2Barium 0.39

30- NCmg/kg BRL< 0.39Silver 0.39

30- 46.6mg/kg46.9Lead 0.39

30- 12.5mg/kg14.2Chromium 0.39


71.1 3075-125mg/kg77.12 108Silver 0.33

49.9 3075-125mg/kg48.13 96.5Selenium 1.3

73.8 3075-125mg/kg88.54 120Lead 0.33

202 3075-125mg/kg230.0 114Arsenic 0.67

167 3075-125mg/kg197.3 118Chromium 0.33

141 3075-125mg/kg156.0 111Cadmium 0.33

270 3075-125mg/kg311.3 115Barium 0.33


318 3075-125mg/kg309.7 96.4Arsenic 0.67

159 3075-125mg/kg187.0 108Chromium 0.33

318 3075-125mg/kg405.8 104Lead 0.33

159 3075-125mg/kg BRL132.3 83.1Selenium 1.3

39.75 3075-125mg/kg BRL39.02 98.2Silver 0.33

159 3075-125mg/kg BRL164.8 103Cadmium 0.33

159 3075-125mg/kg186.8 106Barium 0.33

Batch 477208A - SW3005A/SW3010A


-mg/l< 0.004 BRLZinc 0.004

-mg/l< 0.005 BRLCopper 0.005

-mg/l< 0.002 BRLLead 0.002


1 2075-125mg/l1.049 105Zinc 0.004

1 2075-125mg/l1.023 102Copper 0.005

2 2075-125mg/l2.085 104Lead 0.002

Batch 477321A - SW3050B


-mg/kg< 0.32 BRLCadmium 0.32

-mg/kg< 0.32 BRLBarium 0.32

-mg/kg< 0.32 BRLLead 0.32

-mg/kg< 0.65 BRLArsenic 0.65

-mg/kg< 1.3 BRLSelenium 1.3

-mg/kg< 0.32 BRLChromium 0.32

-mg/kg< 0.32 BRLSilver 0.32


30- 14.9mg/kg6.91Barium 0.43

30- NCmg/kg BRL< 0.43Silver 0.43

30- NCmg/kg1.47Arsenic 0.86

30- NCmg/kg BRL< 1.7Selenium 1.7

30- 15.6mg/kg2.48Lead 0.43

30- 21.0mg/kg9.56Chromium 0.43

30- NCmg/kg BRL< 0.43Cadmium 0.43


Page 176 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW6010D

Batch 477321A - SW3050B


167 3075-125mg/kg187.2 112Chromium 0.32

83.6 3075-125mg/kg84.82 101Lead 0.32

49.9 3075-125mg/kg45.74 91.7Selenium 1.3

71.1 3075-125mg/kg73.99 104Silver 0.32

202 3075-125mg/kg216.5 107Arsenic 0.65

270 3075-125mg/kg297.2 110Barium 0.32

141 3075-125mg/kg152.5 108Cadmium 0.32


308.6 3075-125mg/kg301.8 97.4Arsenic 0.65

154.3 3075-125mg/kg BRL164.7 107Cadmium 0.32

154.3 3075-125mg/kg175.4 106Chromium 0.32

308.6 3075-125mg/kg337.3 108Lead 0.32

38.58 3075-125mg/kg BRL39.00 101Silver 0.32

154.3 3075-125mg/kg168.4 105Barium 0.32

154.3 3075-125mg/kg BRL133.6 86.6Selenium 1.3

SW6010D (SPLP)

Batch 477276A - SW3010A


-mg/l< 0.010 BRLSPLP Silver 0.010

-mg/l< 0.010 BRLSPLP Barium 0.010

-mg/l< 0.005 BRLSPLP Cadmium 0.005

-mg/l< 0.010 BRLSPLP Chromium 0.010

-mg/l< 0.020 BRLSPLP Selenium 0.020

-mg/l< 0.010 BRLSPLP Lead 0.010

-mg/l< 0.004 BRLSPLP Arsenic 0.004


1 2075-125mg/l1.031 103SPLP Selenium 0.020

0.25 2075-125mg/l0.2456 98.2SPLP Silver 0.010

2 2075-125mg/l1.991 99.6SPLP Lead 0.010

1 2075-125mg/l0.9771 97.7SPLP Chromium 0.010

1 2075-125mg/l1.007 101SPLP Cadmium 0.005

1 2075-125mg/l1.043 104SPLP Barium 0.010

2 2075-125mg/l2.003 100SPLP Arsenic 0.004

SW7470A (SPLP)

Batch 477274A - SW1312/SW7470A


-mg/l< 0.0002 BRLSPLP Mercury 0.0002


0.0025 2080-120mg/l0.002472 98.9SPLP Mercury 0.0002

Batch 477275A - SW1312/SW7470A


-mg/l< 0.0002 BRLSPLP Mercury 0.0002


0.0025 2080-120mg/l0.002417 96.7SPLP Mercury 0.0002

SW7471B

Batch 477253A - SW7471B

Blank (CD04926-BLK) Prepared & Analyzed: 02-May-19

-mg/kg< 0.03 BRLMercury 0.03


Page 177 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW7471B

Batch 477253A - SW7471B

LCS (CD04926-LCS) Prepared & Analyzed: 02-May-19

3.71 3070-130mg/kg4.758 128Mercury 0.03

LCS Dup (CD04926-LCSD) Prepared & Analyzed: 02-May-19Source: CD04926-LCS

3.71 3070-130 11.6mg/kg4.218 114Mercury 0.03

Batch 477261A - SW7471B


-mg/kg< 0.03 BRLMercury 0.03

Duplicate (CD05120-DUP) Prepared & Analyzed: 02-May-19Source: SC54611-02

30- NCmg/kg BRL< 0.03Mercury 0.03


3.71 3070-130mg/kgr3.114 83.9Mercury 0.03


3.71 3070-130 31.3mg/kgr4.259 115Mercury 0.03

Matrix Spike (CD05120-MS) Prepared & Analyzed: 02-May-19Source: SC54611-02

0.166666625 3075-125mg/kg BRL0.1962 118Mercury 0.03

Matrix Spike Dup (CD05120-MSD) Prepared & Analyzed: 02-May-19Source: SC54611-02

0.15625 3075-125 7.9mg/kg BRL0.1708 109Mercury 0.03

SW8081B

Batch 477223A - SW3510C


-ug/lc5ND NDChlordane 0.050

-ug/lc5ND NDHeptachlor epoxide 0.005

-ug/lc5ND NDHeptachlor 0.005

-ug/lc5ND NDg-BHC (Lindane) 0.002

-ug/lc5ND NDEndrin ketone 0.005

-ug/lc5ND NDEndrin Aldehyde 0.005

-ug/lc5ND NDEndrin 0.005

-ug/lc5ND NDEndosulfan Sulfate 0.005

-ug/lc5ND NDEndosulfan II 0.005

-ug/lc5ND NDEndosulfan I 0.005

-ug/lc5ND NDd-BHC 0.005

-ug/lc5ND NDb-BHC 0.002

-ug/lc5ND NDAldrin 0.002

-ug/lc5ND NDAlachlor 0.005

-ug/lc5ND NDa-BHC 0.002

-ug/lc5ND ND4,4' -DDT 0.003

-ug/lc5ND ND4,4' -DDE 0.003

-ug/lc5ND ND4,4' -DDD 0.003

-ug/lc5ND NDToxaphene 0.20

-ug/lc5ND NDMethoxychlor 0.005

-ug/lc5ND NDDieldrin 0.002

100 30-150Surrogate: %DCBP (Surrogate Rec) 97 ug/lc5 97

100 30-150Surrogate: %TCMX (Surrogate Rec) 83 ug/lc5 83


100 2040-140ug/lc5113.2 113Methoxychlor 0.005

100 2040-140ug/lc573.62 74Endrin ketone 0.005

100 2040-140ug/lc589.92 90Endrin 0.005

100 2040-140ug/lc589.38 894,4' -DDE 0.003

100 2040-140ug/lc597.05 974,4' -DDT 0.003

100 2040-140ug/lc564.84 65a-BHC 0.002


Page 178 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8081B

Batch 477223A - SW3510C


100 2040-140ug/lc562.94 63Aldrin 0.002

100 2040-140ug/lc562.90 63b-BHC 0.002

100 2040-140ug/lc578.13 78Endosulfan Sulfate 0.005

100 2040-140ug/lc567.29 67d-BHC 0.005

100 2040-140ug/lc597.84 984,4' -DDD 0.003

100 2040-140ug/lc558.57 59g-BHC (Lindane) 0.002

100 2040-140ug/lc560.83 61Heptachlor 0.005

100 2040-140ug/lc579.41 79Dieldrin 0.002

100 2040-140ug/lc567.87 68Heptachlor epoxide 0.005

100 2040-140ug/lc576.79 77Endosulfan I 0.005

100 2040-140ug/lc567.87 68Endrin Aldehyde 0.005

100 2040-140ug/lc573.26 73Endosulfan II 0.005

100 2040-140ug/lc573.45 73Chlordane 0.050

100 30-150Surrogate: %DCBP (Surrogate Rec) 94.05 ug/lc5 94

100 30-150Surrogate: %TCMX (Surrogate Rec) 86.81 ug/lc5 87


100 2040-140 2.5ug/lc580.83 81Dieldrin 0.002

100 2040-140 7.1ug/lc573.17 73Heptachlor epoxide 0.005

100 2040-140 1.7ug/lc560.37 60g-BHC (Lindane) 0.002

100 2040-140 2.9ug/lc569.76 70Endrin Aldehyde 0.005

100 2040-140 1.8ug/lc5115.0 115Methoxychlor 0.005

100 2040-140 0.0ug/lc590.02 90Endrin 0.005

100 2040-140 1.3ug/lc579.02 79Endosulfan Sulfate 0.005

100 2040-140 4.0ug/lc576.23 76Endosulfan II 0.005

100 2040-140 3.2ug/lc563.35 63Heptachlor 0.005

100 2040-140 9.7ug/lc5108.1 1084,4' -DDD 0.003

100 2040-140 0.0ug/lc566.67 67d-BHC 0.005

100 2040-140 7.9ug/lc578.61 79Chlordane 0.050

100 2040-140 1.6ug/lc564.47 64b-BHC 0.002

100 2040-140 1.6ug/lc563.84 64Aldrin 0.002

100 2040-140 3.0ug/lc567.11 67a-BHC 0.002

100 2040-140 2.0ug/lc599.38 994,4' -DDT 0.003

100 2040-140 3.3ug/lc592.32 924,4' -DDE 0.003

100 2040-140 2.6ug/lc575.28 75Endosulfan I 0.005

100 2040-140 4.0ug/lc576.59 77Endrin ketone 0.005

100 30-150Surrogate: %DCBP (Surrogate Rec) 92.04 ug/lc5 92

100 30-150Surrogate: %TCMX (Surrogate Rec) 84.49 ug/lc5 84

Batch 477266A - SW3545A


-ug/kgND NDAlachlor 3.3

-ug/kgND NDEndrin ketone 3.3

-ug/kgND NDEndrin 3.3

-ug/kgND NDEndosulfan II 3.3

-ug/kgND NDEndosulfan I 3.3

-ug/kgND NDDieldrin 1.0

-ug/kgND NDd-BHC 3.3

-ug/kgND NDChlordane 33

-ug/kgND NDg-BHC 1.0

-ug/kgND NDAldrin 1.0


Page 179 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8081B

Batch 477266A - SW3545A


-ug/kgND NDEndrin aldehyde 3.3

-ug/kgND NDa-BHC 1.0

-ug/kgND ND4,4' -DDT 1.7

-ug/kgND ND4,4' -DDE 1.7

-ug/kgND ND4,4' -DDD 1.7

-ug/kgND NDb-BHC 1.0

-ug/kgND NDHeptachlor epoxide 3.3

-ug/kgND NDMethoxychlor 3.3

-ug/kgND NDToxaphene 130

-ug/kgND NDHeptachlor 3.3

-ug/kgND NDEndosulfan sulfate 3.3

100 30-150Surrogate: % DCBP 75 ug/kg 75

100 30-150Surrogate: % TCMX 78 ug/kg 78


50 3040-140ug/kg43.12 86b-BHC 1.0

50 3040-140ug/kg48.24 96Endosulfan I 3.3

50 3040-140ug/kg50.87 102Heptachlor 3.3

50 3040-140ug/kg48.14 96Dieldrin 1.0

50 3040-140ug/kg48.06 96Endrin ketone 3.3

50 3040-140ug/kg44.46 89Endosulfan II 3.3

50 3040-140ug/kg42.08 84Endosulfan sulfate 3.3

50 3040-140ug/kg44.07 88Endrin 3.3

50 3040-140ug/kg33.83 68Endrin aldehyde 3.3

50 3040-140ug/kg46.36 93Chlordane 33

50 3040-140ug/kg45.76 92Aldrin 1.0

50 3040-140ug/kg40.85 82a-BHC 1.0

50 3040-140ug/kg40.85 824,4' -DDT 1.7

50 3040-140ug/kg50.71 1014,4' -DDE 1.7

50 3040-140ug/kg40.99 824,4' -DDD 1.7

50 3040-140ug/kg49.09 98Methoxychlor 3.3

50 3040-140ug/kg46.51 93Heptachlor epoxide 3.3

50 3040-140ug/kg47.32 95d-BHC 3.3

50 3040-140ug/kg46.24 92g-BHC 1.0

100 30-150Surrogate: % DCBP 88.62 ug/kg 89

100 30-150Surrogate: % TCMX 78.15 ug/kg 78


50 3040-140 8.9ug/kg37.34 75a-BHC 1.0

50 3040-140 5.0ug/kg38.95 784,4' -DDD 1.7

50 3040-140 7.6ug/kg38.18 764,4' -DDT 1.7

50 3040-140 7.9ug/kg42.68 85Aldrin 1.0

50 3040-140 8.5ug/kg39.67 79b-BHC 1.0

50 3040-140 7.8ug/kg42.91 86Chlordane 33

50 3040-140 8.8ug/kg43.73 87d-BHC 3.3

50 3040-140 7.6ug/kg44.72 89Dieldrin 1.0

50 3040-140 11.0ug/kg43.22 86Endosulfan I 3.3

50 3040-140 9.4ug/kg40.70 81Endosulfan II 3.3

50 3040-140 7.4ug/kg39.10 78Endosulfan sulfate 3.3

50 3040-140 9.5ug/kg40.12 80Endrin 3.3

50 3040-140 7.6ug/kg44.52 89Endrin ketone 3.3

50 3040-140 7.9ug/kg42.46 85g-BHC 1.0


Page 180 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8081B

Batch 477266A - SW3545A


50 3040-140 9.2ug/kg46.73 93Heptachlor 3.3

50 3040-140 7.8ug/kg43.23 86Heptachlor epoxide 3.3

50 3040-140 9.6ug/kg44.61 89Methoxychlor 3.3

50 3040-140 23.0ug/kg27.01 54Endrin aldehyde 3.3

50 3040-140 7.2ug/kg46.82 944,4' -DDE 1.7




50 3030-150ug/kg BRL29.95 60Methoxychlor 3.3

50 3030-150ug/kg BRL29.69 59b-BHC 1.0

50 3030-150ug/kg BRL21.47 43Endrin aldehyde 3.3

50 3030-150ug/kg BRL30.55 61Endrin 3.3

50 3030-150ug/kg BRL33.70 67Endosulfan I 3.3

50 3030-150ug/kg BRL26.67 53Endosulfan sulfate 3.3

50 3030-150ug/kg BRL33.58 67Aldrin 1.0

50 3030-150ug/kg BRL33.72 67Heptachlor epoxide 3.3

50 3030-150ug/kg BRL37.44 67Heptachlor 3.3

50 3030-150ug/kg BRL34.76 69g-BHC 1.0

50 3030-150ug/kg BRL31.30 61Endosulfan II 3.3

50 3030-150ug/kg BRL28.33 57Endrin ketone 3.3

50 3030-150ug/kg BRL29.54 594,4' -DDD 1.7

50 3030-150ug/kg BRL32.11 64d-BHC 3.3

50 3030-150ug/kg BRL29.72 594,4' -DDE 1.7

50 3030-150ug/kg BRL28.64 554,4' -DDT 1.7

50 3030-150ug/kg BRL32.98 66Chlordane 33

50 3030-150ug/kg BRL28.20 56a-BHC 1.0

50 3030-150ug/kg BRL32.25 65Dieldrin 1.0




50 3030-150 8.6ug/kg BRL40.63 73Heptachlor 3.3

50 3030-150 8.3ug/kg BRL37.66 75g-BHC 1.0

50 3030-150 11.0ug/kg BRL33.40 67Methoxychlor 3.3

50 3030-150 8.6ug/kg BRL36.35 73Heptachlor epoxide 3.3

50 3030-150 8.1ug/kg BRL31.85 64b-BHC 1.0

50 3030-150 9.9ug/kg BRL36.85 74Aldrin 1.0

50 3030-150 7.3ug/kg BRL35.67 71Chlordane 33

50 3030-150 6.9ug/kg BRL30.00 60a-BHC 1.0

50 3030-150 9.0ug/kg BRL34.97 70d-BHC 3.3

50 3030-150 7.9ug/kg BRL34.00 66Endosulfan II 3.3

50 3030-150 7.4ug/kg BRL34.90 70Dieldrin 1.0

50 3030-150 5.8ug/kg BRL35.72 71Endosulfan I 3.3

50 3030-150 9.7ug/kg BRL32.59 654,4' -DDE 1.7

50 3030-150 8.7ug/kg BRL31.15 604,4' -DDT 1.7

50 3030-150 10.0ug/kg BRL31.40 63Endrin ketone 3.3

50 3030-150 9.4ug/kg BRL33.43 67Endrin 3.3

50 3030-150 9.7ug/kg BRL32.29 654,4' -DDD 1.7

50 3030-150 7.3ug/kg BRL28.76 57Endosulfan sulfate 3.3

50 3030-150 2.3ug/kg BRL21.91 44Endrin aldehyde 3.3


Page 181 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8081B

Batch 477266A - SW3545A




SW8082A

Batch 477222A - SW3510C


-ug/lND NDPCB-1016 0.050









100 30-150Surrogate: % DCBP 79 ug/l 79

100 30-150Surrogate: % TCMX 82 ug/l 82


500 2040-140ug/lNDPCB-1254 0.050

500 2040-140ug/lNDPCB-1268 0.050

500 2040-140ug/l449.6 90PCB-1016 0.050

500 2040-140ug/lNDPCB-1221 0.050

500 2040-140ug/lNDPCB-1232 0.050

500 2040-140ug/lNDPCB-1242 0.050

500 2040-140ug/lNDPCB-1248 0.050

2040-140ug/lNDPCB-1262 0.050

500 2040-140ug/l467.6 94PCB-1260 0.050

40 30-150Surrogate: % TCMX 43.93 ug/l 110

40 30-150Surrogate: % DCBP 38.32 ug/l 96


500 2040-140ug/lNDPCB-1268 0.050

500 2040-140ug/lNDPCB-1221 0.050

500 2040-140ug/lNDPCB-1232 0.050

500 2040-140ug/lNDPCB-1242 0.050

500 2040-140ug/lNDPCB-1248 0.050

500 2040-140ug/lNDPCB-1254 0.050

500 2040-140 0.0ug/l468.1 94PCB-1260 0.050

2040-140ug/lNDPCB-1262 0.050

500 2040-140 0.0ug/l448.7 90PCB-1016 0.050

40 30-150Surrogate: % TCMX 41.70 ug/l 104

40 30-150Surrogate: % DCBP 38.52 ug/l 96

Batch 477265A - SW3545A


2500 -ug/kgND NDPCB-1016 33

2500 -ug/kgND NDPCB-1260 33

100 30-150Surrogate: % DCBP 80 ug/kg 80

100 30-150Surrogate: % TCMX 79 ug/kg 79


3040-140ug/kgNDPCB-1262 33


Page 182 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8082A

Batch 477265A - SW3545A


500 3040-140ug/kg259.3 52PCB-1016 33

500 3040-140ug/kgNDPCB-1221 33

500 3040-140ug/kgNDPCB-1232 33

500 3040-140ug/kgNDPCB-1242 33

500 3040-140ug/kgNDPCB-1248 33

500 3040-140ug/kg450.9 90PCB-1260 33

500 3040-140ug/kgNDPCB-1268 33

500 3040-140ug/kgNDPCB-1254 33




500 3040-140 23.7ug/kg330.1 66PCB-1016 33

500 3040-140ug/kgNDPCB-1221 33

500 3040-140ug/kgNDPCB-1232 33

500 3040-140ug/kgNDPCB-1268 33

500 3040-140ug/kgNDPCB-1248 33

500 3040-140ug/kgNDPCB-1254 33

500 3040-140 25.0ug/kg352.4 70PCB-1260 33

3040-140ug/kgNDPCB-1262 33

500 3040-140ug/kgNDPCB-1242 33




3040-140ug/kg BRLNDPCB-1232 33


500 3040-140ug/kg BRL242.0 48PCB-1016 33




500 3040-140ug/kg BRL245.5 49PCB-1260 33







500 3040-140 26.5ug/kg BRL318.7 64PCB-1260 33






500 3040-140 23.9ug/kg BRL305.6 61PCB-1016 33




SW8260C

Batch 477679A - SW8260C


Page 183 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477679A - SW8260C


-ug/kgND NDo-Xylene 2.0

-ug/kgND NDEthylbenzene 1.0

-ug/kgND NDHexachlorobutadiene 5.0

-ug/kgND NDIsopropylbenzene 1.0

-ug/kgND NDm&p-Xylene 2.0

-ug/kgND NDMethyl Ethyl Ketone 5.0

-ug/kgND NDMethyl t-butyl ether (MTBE) 1.0

-ug/kgND NDMethylene chloride 5.0

-ug/kgND NDNaphthalene 5.0

-ug/kgND NDn-Butylbenzene 1.0

-ug/kgND NDn-Propylbenzene 1.0

-ug/kgND NDDichlorodifluoromethane 5.0

-ug/kgND NDBromodichloromethane 5.0

-ug/kgND ND2,2-Dichloropropane 5.0

-ug/kgND ND2-Chlorotoluene 5.0

-ug/kgND ND2-Hexanone 25

-ug/kgND ND2-Isopropyltoluene 5.0


-ug/kgND ND4-Methyl-2-pentanone 25

-ug/kgND NDAcetone 10

-ug/kgND NDAcrylonitrile 5.0

-ug/kgND NDBenzene 1.0

-ug/kgND NDDibromomethane 5.0

-ug/kgND NDBromochloromethane 5.0

-ug/kgND NDDibromochloromethane 3.0

-ug/kgND NDBromoform 5.0

-ug/kgND NDBromomethane 5.0

-ug/kgND NDCarbon Disulfide 5.0

-ug/kgND NDCarbon tetrachloride 5.0

-ug/kgND NDChlorobenzene 5.0

-ug/kgND NDChloroethane 5.0

-ug/kgND NDChloroform 5.0

-ug/kgND NDChloromethane 5.0

-ug/kgND NDcis-1,2-Dichloroethene 5.0

-ug/kgND NDcis-1,3-Dichloropropene 5.0

-ug/kgND NDBromobenzene 5.0

-ug/kgND ND1,1-Dichloroethene 5.0

-ug/kgND ND1,2-Dichlorobenzene 5.0

-ug/kgND NDtert-Butylbenzene 1.0

-ug/kgND ND1,2-Dibromo-3-chloropropane 5.0

-ug/kgND ND1,2,4-Trimethylbenzene 1.0

-ug/kgND ND1,2,4-Trichlorobenzene 5.0

-ug/kgND ND1,2,3-Trichloropropane 5.0

-ug/kgND NDp-Isopropyltoluene 1.0

-ug/kgND ND1,1-Dichloropropene 5.0

-ug/kgND ND1,2-Dichloroethane 5.0


-ug/kgND ND1,1,2-Trichloroethane 5.0

-ug/kgND ND1,1,2,2-Tetrachloroethane 3.0



Page 184 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477679A - SW8260C



-ug/kgND NDTrichlorofluoromethane 5.0


-ug/kgND NDTrichloroethene 5.0

-ug/kgND NDsec-Butylbenzene 1.0




-ug/kgND ND1,2-Dibromoethane 5.0

-ug/kgND NDTetrachloroethene 5.0


-ug/kgND NDTetrahydrofuran (THF) 5.0

-ug/kgND NDToluene 1.0

-ug/kgND NDStyrene 5.0

-ug/kgND NDtrans-1,2-Dichloroethene 5.0

-ug/kgND NDtrans-1,3-Dichloropropene 5.0

-ug/kgND NDtrans-1,4-dichloro-2-butene 5.0

-ug/kgND NDVinyl chloride 5.0

-ug/kgND NDTrichlorotrifluoroethane 5.0


50 70-130Surrogate: % Toluene-d8 96 ug/kg 96

50 70-130Surrogate: % Dibromofluoromethane 98 ug/kg 98

50 70-130Surrogate: % Bromofluorobenzene 97 ug/kg 97

50 70-130Surrogate: % 1,2-dichlorobenzene-d4 101 ug/kg 101


50 3070-130ug/kg51.30 1031,2,3-Trichloropropane 5.0

50 3070-130ug/kg49.17 98Acetone 10

50 3070-130ug/kg47.47 95Bromomethane 5.0

50 3070-130ug/kg51.30 1031,4-Dichlorobenzene 5.0

50 3070-130ug/kg58.69 1172,2-Dichloropropane 5.0

50 3070-130ug/kg50.94 1022-Chlorotoluene 5.0

50 3070-130ug/kg51.54 1032-Hexanone 25

50 3070-130ug/kg51.29 1032-Isopropyltoluene 5.0


50 3070-130ug/kg53.11 1064-Methyl-2-pentanone 25

50 3070-130ug/kg51.65 1031,3,5-Trimethylbenzene 1.0

50 3070-130ug/kg50.74 101Acrylonitrile 5.0

50 3070-130ug/kg51.01 102Benzene 1.0

50 3070-130ug/kg50.71 101Bromobenzene 5.0

50 3070-130ug/kg52.59 105Bromochloromethane 5.0

50 3070-130ug/kg56.04 112Bromodichloromethane 5.0



50 3070-130ug/kg53.82 1081,2,3-Trichlorobenzene 5.0

50 3070-130ug/kg45.62 91Vinyl chloride 5.0

50 3070-130ug/kg55.13 1101,1,1,2-Tetrachloroethane 5.0

50 3070-130ug/kg55.43 1111,1,1-Trichloroethane 5.0



50 3070-130ug/kg54.39 1091,1-Dichloroethane 5.0


Page 185 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477679A - SW8260C



50 3070-130ug/kg54.32 1091,1-Dichloropropene 5.0

50 3070-130ug/kg52.08 104Carbon Disulfide 5.0


50 3070-130ug/kg55.05 1101,2-Dibromo-3-chloropropane 5.0

50 3070-130ug/kg52.10 1041,2-Dibromoethane 5.0




50 3070-130ug/kg52.65 1051,1-Dichloroethene 5.0

50 3070-130ug/kg51.84 104Tetrachloroethene 5.0

50 3070-130ug/kg58.57 117Bromoform 5.0

50 3070-130ug/kg54.18 108n-Butylbenzene 1.0

50 3070-130ug/kg51.10 102n-Propylbenzene 1.0

50 3070-130ug/kg51.35 103o-Xylene 2.0

50 3070-130ug/kg53.32 107p-Isopropyltoluene 1.0

50 3070-130ug/kg54.03 108sec-Butylbenzene 1.0

50 3070-130ug/kg50.32 101Methylene chloride 5.0

50 3070-130ug/kg51.61 103tert-Butylbenzene 1.0

50 3070-130ug/kg54.05 108Methyl t-butyl ether (MTBE) 1.0

125 3070-130ug/kg126.7 101Tetrahydrofuran (THF) 5.0

50 3070-130ug/kg49.14 98Toluene 1.0

50 3070-130ug/kg53.94 108trans-1,2-Dichloroethene 5.0

50 3070-130ug/kg54.42 109trans-1,3-Dichloropropene 5.0

250 3070-130ug/kg276.7 111trans-1,4-dichloro-2-butene 5.0

50 3070-130ug/kg52.58 105Trichloroethene 5.0

50 3070-130ug/kg53.03 106Styrene 5.0

50 3070-130ug/kg52.14 104Dibromomethane 5.0

50 3070-130ug/kg49.84 100Carbon tetrachloride 5.0

50 3070-130ug/kg51.13 102Chlorobenzene 5.0

50 3070-130ug/kg51.46 103Chloroethane 5.0

50 3070-130ug/kg54.44 109Chloroform 5.0

50 3070-130ug/kg40.29 81Chloromethane 5.0

50 3070-130ug/kg58.10 116cis-1,2-Dichloroethene 5.0

50 3070-130ug/kg54.46 109Naphthalene 5.0

50 3070-130ug/kg58.80 118Dibromochloromethane 3.0

50 3070-130ug/kg50.64 101Trichlorotrifluoroethane 5.0

50 3070-130ug/kg47.68 95Dichlorodifluoromethane 5.0

50 3070-130ug/kg51.10 102Ethylbenzene 1.0

50 3070-130ug/kg54.37 109Hexachlorobutadiene 5.0

50 3070-130ug/kg51.13 102Isopropylbenzene 1.0

100 3070-130ug/kg101.8 102m&p-Xylene 2.0

50 3070-130ug/kg51.40 103Methyl Ethyl Ketone 5.0

50 3070-130ug/kg54.18 108cis-1,3-Dichloropropene 5.0

50 3070-130ug/kg48.58 97Trichlorofluoromethane 5.0

50 70-130Surrogate: % Dibromofluoromethane 51.16 ug/kg 102

50 70-130Surrogate: % Bromofluorobenzene 51.85 ug/kg 104

50 70-130Surrogate: % 1,2-dichlorobenzene-d4 50.23 ug/kg 100

50 70-130Surrogate: % Toluene-d8 49.49 ug/kg 99



Page 186 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477679A - SW8260C


50 3070-130 2.0ug/kg51.37 103Acrylonitrile 5.0

50 3070-130 1.9ug/kg52.92 1061,3-Dichlorobenzene 5.0

50 3070-130 1.9ug/kg53.04 1061,3-Dichloropropane 5.0



50 3070-130 2.9ug/kg52.44 1052-Chlorotoluene 5.0

50 3070-130 1.0ug/kg52.21 1042-Hexanone 25

50 3070-130 2.9ug/kg53.05 1062-Isopropyltoluene 5.0


50 3070-130 1.0ug/kg49.59 99Acetone 10


50 3070-130 1.9ug/kg51.77 104Benzene 1.0

50 3070-130 2.9ug/kg52.08 104Bromobenzene 5.0

50 3070-130 1.9ug/kg53.52 107Bromochloromethane 5.0

50 3070-130 1.7ug/kg59.67 119Bromoform 5.0

50 3070-130 1.9ug/kg53.75 1084-Methyl-2-pentanone 25

50 3070-130 1.0ug/kg52.07 1041,2,3-Trichloropropane 5.0

50 3070-130 3.6ug/kg56.82 1141,1,1,2-Tetrachloroethane 5.0

50 3070-130 0.9ug/kg55.97 1121,1,1-Trichloroethane 5.0



50 3070-130 0.9ug/kg55.09 1101,1-Dichloroethane 5.0

50 3070-130 2.8ug/kg53.98 1081,1-Dichloroethene 5.0


50 3070-130 1.8ug/kg54.76 1101,2,3-Trichlorobenzene 5.0

50 3070-130 2.9ug/kg52.90 1061,3,5-Trimethylbenzene 1.0



50 3070-130 0.9ug/kg55.74 1111,2-Dibromo-3-chloropropane 5.0

50 3070-130 3.8ug/kg53.87 1081,2-Dibromoethane 5.0

50 3070-130 2.1ug/kg48.61 97Bromomethane 5.0


50 3070-130 1.8ug/kg55.47 1111,1-Dichloropropene 5.0

50 3070-130 3.0ug/kg50.34 101Toluene 1.0

50 3070-130 1.8ug/kg54.99 110n-Butylbenzene 1.0

50 3070-130 1.8ug/kg57.22 114Bromodichloromethane 5.0

50 3070-130 2.9ug/kg52.91 106o-Xylene 2.0

50 3070-130 1.9ug/kg54.50 109p-Isopropyltoluene 1.0

50 3070-130 2.7ug/kg55.54 111sec-Butylbenzene 1.0

50 3070-130 3.7ug/kg54.77 110Styrene 5.0

50 3070-130 3.8ug/kg53.64 107tert-Butylbenzene 1.0

50 3070-130 1.9ug/kg53.18 106Carbon Disulfide 5.0

125 3070-130 1.0ug/kg127.3 102Tetrahydrofuran (THF) 5.0

50 3070-130 1.8ug/kg55.65 111Naphthalene 5.0

50 3070-130 2.7ug/kg55.28 111trans-1,2-Dichloroethene 5.0

50 3070-130 1.8ug/kg55.26 111trans-1,3-Dichloropropene 5.0

250 3070-130 0.9ug/kg281.0 112trans-1,4-dichloro-2-butene 5.0

50 3070-130 1.9ug/kg53.71 107Trichloroethene 5.0

50 3070-130 2.0ug/kg49.51 99Trichlorofluoromethane 5.0

50 3070-130 2.9ug/kg51.78 104Trichlorotrifluoroethane 5.0


Page 187 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477679A - SW8260C


50 3070-130 1.1ug/kg46.23 92Vinyl chloride 5.0

50 3070-130 1.9ug/kg52.78 106Tetrachloroethene 5.0

50 3070-130 2.5ug/kg60.30 121Dibromochloromethane 3.0

50 3070-130 16.5ug/kg59.07 118Carbon tetrachloride 5.0

50 3070-130 2.9ug/kg52.31 105Chlorobenzene 5.0

50 3070-130 1.0ug/kg52.06 104Chloroethane 5.0

50 3070-130 0.9ug/kg55.17 110Chloroform 5.0

50 3070-130 1.2ug/kg41.03 82Chloromethane 5.0

50 3070-130 2.9ug/kg52.44 105n-Propylbenzene 1.0

50 3070-130 1.8ug/kg55.08 110cis-1,3-Dichloropropene 5.0

50 3070-130 1.0ug/kg50.79 102Methylene chloride 5.0

50 3070-130 1.9ug/kg53.03 106Dibromomethane 5.0

50 3070-130 2.1ug/kg48.44 97Dichlorodifluoromethane 5.0

50 3070-130 2.9ug/kg52.66 105Ethylbenzene 1.0

50 3070-130 2.7ug/kg55.92 112Hexachlorobutadiene 5.0

50 3070-130 2.9ug/kg52.59 105Isopropylbenzene 1.0

100 3070-130 1.0ug/kg103.4 103m&p-Xylene 2.0

50 3070-130 0.0ug/kg51.61 103Methyl Ethyl Ketone 5.0

50 3070-130 0.9ug/kg54.65 109Methyl t-butyl ether (MTBE) 1.0

50 3070-130 16.8ug/kg48.80 98cis-1,2-Dichloroethene 5.0






50 3070-130ug/kg BRL51.55 1031,1,2,2-Tetrachloroethane 3.0

50 3070-130ug/kg BRL39.73 791,1-Dichloroethene 5.0

50 3070-130ug/kg BRL50.93 1021,1,2-Trichloroethane 5.0



50 3070-130ug/kg BRL53.68 1071,1-Dichloropropene 5.0

50 3070-130ug/kg BRL52.24 1041,2,3-Trichlorobenzene 5.0

50 3070-130ug/kg BRL52.94 1061,1-Dichloroethane 5.0

50 3070-130ug/kg BRL51.60 103o-Xylene 2.0


50 3070-130ug/kg BRL53.26 107cis-1,3-Dichloropropene 5.0

50 3070-130ug/kg BRL56.68 113Dibromochloromethane 3.0

50 3070-130ug/kg BRL51.50 103Dibromomethane 5.0

50 3070-130ug/kg BRL57.23 114Dichlorodifluoromethane 5.0

50 3070-130ug/kg BRL50.61 101Ethylbenzene 1.0

50 3070-130ug/kg BRL56.38 113Hexachlorobutadiene 5.0

50 3070-130ug/kg BRL50.22 100Isopropylbenzene 1.0

100 3070-130ug/kg BRL100.2 100m&p-Xylene 2.0

50 3070-130ug/kg BRL49.92 100Methyl Ethyl Ketone 5.0

50 3070-130ug/kg BRL49.44 99Methyl t-butyl ether (MTBE) 1.0

50 3070-130ug/kg BRL51.08 102Methylene chloride 5.0

50 3070-130ug/kg BRL53.53 107Naphthalene 5.0

50 3070-130ug/kg BRL43.35 87Chloromethane 5.0

50 3070-130ug/kg BRL49.26 99Toluene 1.0

50 3070-130ug/kg BRL49.58 991,2,3-Trichloropropane 5.0


Page 188 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477679A - SW8260C


50 3070-130ug/kg BRL50.47 101Vinyl chloride 5.0

50 3070-130ug/kg BRL44.29 89Trichlorotrifluoroethane 5.0

50 3070-130ug/kg BRL50.97 102Trichlorofluoromethane 5.0

50 3070-130ug/kg BRL51.82 104Trichloroethene 5.0

50 3070-130ug/kg BRL52.75 106n-Butylbenzene 1.0

50 3070-130ug/kg BRL52.78 106trans-1,3-Dichloropropene 5.0

50 3070-130ug/kg BRL50.24 100n-Propylbenzene 1.0

50 3070-130ug/kg BRL51.70 103Tetrachloroethene 5.0

50 3070-130ug/kg BRL51.76 104tert-Butylbenzene 1.0

50 3070-130ug/kg BRL52.40 105Styrene 5.0

50 3070-130ug/kg BRL53.85 108sec-Butylbenzene 1.0

50 3070-130ug/kg BRL52.95 106p-Isopropyltoluene 1.0

125 3070-130ug/kg BRL121.9 98Tetrahydrofuran (THF) 5.0

250 3070-130ug/kg BRL251.9 101trans-1,4-dichloro-2-butene 5.0


50 3070-130ug/kg BRL52.42 105trans-1,2-Dichloroethene 5.0

50 3070-130ug/kg BRL45.90 92Chloroform 5.0

50 3070-130ug/kg BRL50.89 1021,2,4-Trimethylbenzene 1.0

50 3070-130ug/kg BRL53.03 1061,2-Dibromo-3-chloropropane 5.0

50 3070-130ug/kg BRL50.69 1011,2-Dichlorobenzene 5.0


50 3070-130ug/kg BRL51.06 1021,2-Dichloropropane 5.0






50 3070-130ug/kg BRL49.97 1002-Chlorotoluene 5.0

50 3070-130ug/kg BRL47.99 962-Hexanone 25

50 3070-130ug/kg BRL51.81 104Bromomethane 5.0

50 3070-130ug/kg BRL56.36 113Chloroethane 5.0

50 3070-130ug/kg BRL50.29 101Chlorobenzene 5.0

50 3070-130ug/kg BRL51.22 1021,2-Dibromoethane 5.0

50 3070-130ug/kg BRL51.91 1042-Isopropyltoluene 5.0

50 3070-130ug/kg BRL47.44 95Carbon tetrachloride 5.0


50 3070-130ug/kg BRL55.85 112Bromoform 5.0

50 3070-130ug/kg BRL54.95 110Bromodichloromethane 5.0

50 3070-130ug/kg BRL50.39 101Acrylonitrile 5.0

50 3070-130ug/kg BRL44.36 89Bromochloromethane 5.0


50 3070-130ug/kg BRL50.16 100Bromobenzene 5.0

50 3070-130ug/kg BRL49.83 1004-Methyl-2-pentanone 25

50 3070-130ug/kg BRL50.13 100Benzene 1.0

50 3070-130ug/kg BRL37.81 76Acetone 10







Page 189 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477679A - SW8260C


50 3070-130 1.0ug/kg BRL50.49 101Isopropylbenzene 1.0

100 3070-130 0.0ug/kg BRL100.2 100m&p-Xylene 2.0

50 3070-130 2.0ug/kg BRL48.79 98Methyl Ethyl Ketone 5.0

50 3070-130 0.0ug/kg BRL53.10 106n-Butylbenzene 1.0

50 3070-130 0.0ug/kg BRL50.87 102Methylene chloride 5.0

50 3070-130 1.0ug/kg BRL50.65 101n-Propylbenzene 1.0

50 3070-130 0.9ug/kg BRL54.21 108Naphthalene 5.0

50 3070-130 0.9ug/kg BRL56.75 114Hexachlorobutadiene 5.0

50 3070-130 1.1ug/kg BRL46.28 93Chloroform 5.0

50 3070-130 0.0ug/kg BRL51.58 103o-Xylene 2.0

50 3070-130 2.0ug/kg BRL48.58 97Methyl t-butyl ether (MTBE) 1.0

50 3070-130 0.0ug/kg BRL50.57 101Ethylbenzene 1.0

50 3070-130 0.9ug/kg BRL57.63 115Dichlorodifluoromethane 5.0

50 3070-130 0.0ug/kg BRL51.25 103Dibromomethane 5.0

50 3070-130 0.9ug/kg BRL56.04 112Dibromochloromethane 3.0

50 3070-130 0.9ug/kg BRL52.93 106cis-1,3-Dichloropropene 5.0

50 3070-130 1.2ug/kg BRL43.10 86Chloromethane 5.0

50 3070-130 5.5ug/kg BRL53.71 107Chloroethane 5.0

50 3070-130 0.0ug/kg BRL50.33 101Chlorobenzene 5.0

50 3070-130 0.0ug/kg BRL53.25 106p-Isopropyltoluene 1.0

50 3070-130 16.4ug/kg BRL55.81 112Carbon tetrachloride 5.0



50 3070-130 0.0ug/kg BRL44.62 89Trichlorotrifluoroethane 5.0

50 3070-130 0.9ug/kg BRL54.57 109Bromodichloromethane 5.0

50 3070-130 0.9ug/kg BRL55.27 111Bromoform 5.0

50 3070-130 0.9ug/kg BRL54.43 1091,1,1,2-Tetrachloroethane 5.0

50 3070-130 0.0ug/kg BRL53.50 1071,1,1-Trichloroethane 5.0

50 3070-130 1.0ug/kg BRL48.85 981,2,3-Trichloropropane 5.0

50 3070-130 1.9ug/kg BRL53.15 1061,2,3-Trichlorobenzene 5.0

50 3070-130 0.0ug/kg BRL53.59 1071,1-Dichloropropene 5.0

50 3070-130 1.3ug/kg BRL40.02 801,1-Dichloroethene 5.0

50 3070-130 0.9ug/kg BRL52.52 1051,1-Dichloroethane 5.0


50 3070-130 1.0ug/kg BRL50.18 100Vinyl chloride 5.0

50 3070-130 0.9ug/kg BRL54.37 109sec-Butylbenzene 1.0

50 3070-130 5.0ug/kg BRL48.71 97Trichlorofluoromethane 5.0

50 3070-130 1.0ug/kg BRL52.34 105Trichloroethene 5.0

250 3070-130 0.0ug/kg BRL252.3 101trans-1,4-dichloro-2-butene 5.0

50 3070-130 2.9ug/kg BRL51.75 103trans-1,3-Dichloropropene 5.0

50 3070-130 0.0ug/kg BRL52.48 105trans-1,2-Dichloroethene 5.0

50 3070-130 0.0ug/kg BRL49.54 99Toluene 1.0

125 3070-130 1.0ug/kg BRL121.0 97Tetrahydrofuran (THF) 5.0

50 3070-130 2.9ug/kg BRL52.76 106Tetrachloroethene 5.0

50 3070-130 0.0ug/kg BRL52.12 104tert-Butylbenzene 1.0

50 3070-130 0.0ug/kg BRL52.40 105Styrene 5.0


50 3070-130 0.0ug/kg BRL50.88 1021,2-Dibromoethane 5.0

50 3070-130 5.9ug/kg BRL49.14 98Bromomethane 5.0



Page 190 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477679A - SW8260C


50 3070-130 0.0ug/kg BRL52.81 1061,2-Dibromo-3-chloropropane 5.0

50 3070-130 0.0ug/kg BRL50.46 1011,2-Dichlorobenzene 5.0


50 3070-130 0.0ug/kg BRL51.12 1021,2-Dichloropropane 5.0

50 3070-130 1.0ug/kg BRL51.04 1021,3,5-Trimethylbenzene 1.0





50 3070-130 1.0ug/kg BRL50.42 101Bromobenzene 5.0


50 3070-130 2.0ug/kg BRL50.86 1022-Chlorotoluene 5.0

50 3070-130 2.3ug/kg BRL43.55 87Bromochloromethane 5.0

50 3070-130 1.0ug/kg BRL50.25 101Benzene 1.0

50 3070-130 1.0ug/kg BRL49.89 100Acrylonitrile 5.0

50 3070-130 4.0ug/kg BRL36.54 73Acetone 10

50 3070-130 1.0ug/kg BRL49.67 994-Methyl-2-pentanone 25


50 3070-130 0.0ug/kg BRL52.19 1042-Isopropyltoluene 5.0

50 3070-130 0.0ug/kg BRL48.20 962-Hexanone 25





Batch 477684A - SW8260C



























Page 191 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477684A - SW8260C





















































Page 192 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477684A - SW8260C


50 3070-130ug/kg49.60 99o-Xylene 2.0






100 3070-130ug/kg94.56 95m&p-Xylene 2.0









50 3070-130ug/kg49.36 99Styrene 5.0




50 3070-130ug/kg47.75 96Toluene 1.0
































Page 193 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477684A - SW8260C










50 3070-130ug/kg52.31 105Bromoform 5.0

50 3070-130ug/kg45.73 91Chloroform 5.0



50 3070-130ug/kg48.44 97Benzene 1.0


50 3070-130ug/kg48.07 96Acetone 10




50 3070-130ug/kg55.46 1112-Hexanone 25







50 3070-130 5.3ug/kg45.72 91Acetone 10



50 3070-130 2.7ug/kg54.16 1082-Hexanone 25



50 3070-130 0.0ug/kg52.67 105Bromoform 5.0




50 3070-130 1.0ug/kg49.21 98Benzene 1.0
















Page 194 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477684A - SW8260C











50 3070-130 3.0ug/kg51.18 102o-Xylene 2.0


50 3070-130 2.0ug/kg50.49 101Styrene 5.0



50 3070-130 2.1ug/kg49.15 98Toluene 1.0













50 3070-130 2.2ug/kg46.34 93Chloroform 5.0




50 3070-130 1.9ug/kg52.64 105Dibromochloromethane 3.0






100 3070-130 3.1ug/kg97.69 98m&p-Xylene 2.0












Batch 477686A - SW8260C


Page 195 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477686A - SW8260C





















































Page 196 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477686A - SW8260C




































50 3070-130ug/kg60.89 122Benzene 1.0


50 3070-130ug/kg45.84 92Acetone 10















Page 197 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477686A - SW8260C








50 3070-130ug/kg49.67 992-Hexanone 25



50 3070-130ug/kg61.70 123Bromoform 5.0

100 3070-130ug/kg120.2 120m&p-Xylene 2.0







50 3070-130ug/kg61.67 123o-Xylene 2.0



50 3070-130ug/kg61.83 124Styrene 5.0




50 3070-130ug/kg60.15 120Toluene 1.0














50 3070-130ug/kg56.94 114Chloroform 5.0













Page 198 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477686A - SW8260C
























100 3070-130 1.7ug/kg122.0 122m&p-Xylene 2.0




50 3070-130 8.5ug/kgl67.34 135Naphthalene 5.0



50 3070-130 2.4ug/kg63.22 126o-Xylene 2.0



50 3070-130 0.8ug/kg62.29 125Styrene 5.0




50 3070-130 1.7ug/kg60.98 122Toluene 1.0















Page 199 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477686A - SW8260C



50 3070-130 3.9ug/kgl65.62 131Dibromochloromethane 3.0


50 3070-130 7.3ug/kg49.51 99Acetone 10


50 3070-130 0.8ug/kg61.37 123Benzene 1.0

50 3070-130 0.9ug/kg57.43 115Chloroform 5.0


50 3070-130 12.3ug/kg55.98 1122-Hexanone 25








50 3070-130 5.5ug/kg65.03 130Bromoform 5.0









50 3070-130ug/kg BRL57.75 116trans-1,3-Dichloropropene 5.0

250 3070-130ug/kg BRL277.3 111trans-1,4-dichloro-2-butene 5.0

50 3070-130ug/kg BRL64.54 129Trichloroethene 5.0

50 3070-130ug/kg BRL43.92 88Trichlorofluoromethane 5.0

50 3070-130ug/kg BRL58.22 116Trichlorotrifluoroethane 5.0

50 3070-130ug/kg BRL48.92 98Vinyl chloride 5.0

50 3070-130ug/kg BRL64.43 129trans-1,2-Dichloroethene 5.0


50 3070-130ug/kg BRL45.75 92Carbon Disulfide 5.0

50 3070-130ug/kg BRL60.27 121Dichlorodifluoromethane 5.0

50 3070-130ug/kg BRL58.60 1174-Methyl-2-pentanone 25

50 3070-130ug/kg BRL45.49 91Acetone 10

50 3070-130ug/kg BRL56.14 112Acrylonitrile 5.0

50 3070-130ug/kg BRL63.40 127Benzene 1.0

50 3070-130ug/kg BRL62.76 126Bromobenzene 5.0

50 3070-130ug/kg BRL60.35 121Bromochloromethane 5.0

50 3070-130ug/kg BRL58.22 116Bromodichloromethane 5.0

50 3070-130ug/kg BRL59.27 1192-Isopropyltoluene 5.0

50 3070-130ug/kg BRL50.77 102Bromomethane 5.0

50 3070-130ug/kg BRL53.46 1072-Hexanone 25

50 3070-130ug/kg BRL57.99 116Carbon tetrachloride 5.0

50 3070-130ug/kg BRL61.98 124Chlorobenzene 5.0

50 3070-130ug/kg BRL50.13 100Chloroethane 5.0

50 3070-130ug/kg BRL59.47 119Chloroform 5.0

50 3070-130ug/kg BRL43.74 87Chloromethane 5.0


Page 200 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477686A - SW8260C



50 3070-130ug/kg BRL59.67 119cis-1,3-Dichloropropene 5.0

50 3070-130ug/kg BRL62.44 125Toluene 1.0

50 3070-130ug/kg BRL58.79 118Dibromomethane 5.0

50 3070-130ug/kg BRL56.96 114Bromoform 5.0







50 3070-130ug/kg BRL62.61 1251,1-Dichloroethene 5.0

50 3070-130ug/kgm BRL65.60 1311,1-Dichloropropene 5.0



50 3070-130ug/kgm BRL65.82 1321,2,4-Trichlorobenzene 5.0

50 3070-130ug/kg BRL60.18 120Dibromochloromethane 3.0

50 3070-130ug/kg BRL57.97 1161,2-Dibromo-3-chloropropane 5.0

50 3070-130ug/kg BRL61.42 1231,2-Dibromoethane 5.0








50 3070-130ug/kg BRL61.49 1231,2,3-Trichloropropane 5.0

50 3070-130ug/kg BRL63.15 126n-Propylbenzene 1.0

50 3070-130ug/kg BRL60.96 122cis-1,2-Dichloroethene 5.0

50 3070-130ug/kgm BRL65.91 132Isopropylbenzene 1.0

100 3070-130ug/kg BRL125.9 126m&p-Xylene 2.0

50 3070-130ug/kg BRL55.16 110Methyl Ethyl Ketone 5.0

50 3070-130ug/kg BRL52.88 106Methyl t-butyl ether (MTBE) 1.0

50 3070-130ug/kg BRL55.22 110Methylene chloride 5.0

50 3070-130ug/kgm BRL66.92 134Hexachlorobutadiene 5.0

50 3070-130ug/kgm BRL67.19 134n-Butylbenzene 1.0

50 3070-130ug/kg BRL62.02 124Ethylbenzene 1.0

50 3070-130ug/kg BRL64.90 130o-Xylene 2.0

50 3070-130ug/kgm BRL66.36 133p-Isopropyltoluene 1.0

50 3070-130ug/kgm BRL67.06 134sec-Butylbenzene 1.0

50 3070-130ug/kg BRL64.17 128Styrene 5.0

50 3070-130ug/kgm BRL65.42 131tert-Butylbenzene 1.0

50 3070-130ug/kgm65.53 131Tetrachloroethene 5.0

125 3070-130ug/kg BRL140.0 112Tetrahydrofuran (THF) 5.0

50 3070-130ug/kgm BRL67.45 135Naphthalene 5.0







Page 201 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477686A - SW8260C


50 3070-130 2.5ug/kg BRL58.42 117Dibromochloromethane 3.0

50 3070-130 2.2ug/kgm BRL66.13 132Naphthalene 5.0

50 3070-130 2.3ug/kgm BRL65.45 131Hexachlorobutadiene 5.0

50 3070-130 3.4ug/kg BRL58.60 117Dichlorodifluoromethane 5.0

50 3070-130 1.6ug/kg BRL61.19 122Ethylbenzene 1.0

50 3070-130 2.6ug/kg BRL57.42 115Dibromomethane 5.0

50 3070-130 0.8ug/kgm BRL65.27 131Isopropylbenzene 1.0

50 3070-130 3.1ug/kg BRL63.18 126o-Xylene 2.0

100 3070-130 2.4ug/kg BRL123.2 123m&p-Xylene 2.0

50 3070-130 5.6ug/kg BRL52.03 104Methyl Ethyl Ketone 5.0

50 3070-130 2.8ug/kg BRL53.59 107Methylene chloride 5.0

50 3070-130 2.3ug/kgm BRL65.40 131n-Butylbenzene 1.0

50 3070-130 0.0ug/kg BRL62.83 126n-Propylbenzene 1.0

50 3070-130 0.8ug/kg BRL58.87 118cis-1,3-Dichloropropene 5.0

50 3070-130 2.4ug/kg BRL61.86 124Benzene 1.0

50 3070-130 3.8ug/kg BRL51.08 102Methyl t-butyl ether (MTBE) 1.0

50 3070-130 2.3ug/kg BRL65.11 130p-Isopropyltoluene 1.0



50 3070-130 8.8ug/kg BRL49.09 982-Hexanone 25

50 3070-130 3.4ug/kg BRL57.51 1152-Isopropyltoluene 5.0


50 3070-130 6.2ug/kg BRL54.76 1104-Methyl-2-pentanone 25

50 3070-130 1.1ug/kg BRL45.03 90Acetone 10

50 3070-130 5.5ug/kg BRL53.15 106Acrylonitrile 5.0

50 3070-130 2.5ug/kg BRL59.24 118Bromochloromethane 5.0

50 3070-130 2.4ug/kg BRL61.61 123Bromobenzene 5.0

50 3070-130 1.7ug/kg BRL60.13 120cis-1,2-Dichloroethene 5.0

50 3070-130 0.9ug/kg BRL57.47 115Bromodichloromethane 5.0

50 3070-130 4.5ug/kg BRL54.42 109Bromoform 5.0

50 3070-130 4.0ug/kg BRL48.77 98Bromomethane 5.0

50 3070-130 4.3ug/kg BRL47.76 96Carbon Disulfide 5.0

50 3070-130 2.6ug/kg BRL56.72 113Carbon tetrachloride 5.0

50 3070-130 2.4ug/kg BRL60.58 121Chlorobenzene 5.0

50 3070-130 5.1ug/kg BRL47.45 95Chloroethane 5.0

50 3070-130 1.7ug/kg BRL58.42 117Chloroform 5.0

50 3070-130 1.1ug/kg BRL43.78 88Chloromethane 5.0

50 3070-130 0.9ug/kg BRL57.59 115Trichlorotrifluoroethane 5.0

50 3070-130 5.0ug/kg BRL58.72 1171,2-Dibromoethane 5.0


50 3070-130 1.5ug/kgm BRL65.92 132sec-Butylbenzene 1.0

50 3070-130 1.5ug/kg BRL64.48 1291,1-Dichloropropene 5.0

50 3070-130 1.6ug/kg BRL63.53 127Trichloroethene 5.0

50 3070-130 7.6ug/kg BRL57.07 1141,2,3-Trichloropropane 5.0



50 3070-130 3.5ug/kg BRL55.84 1121,2-Dibromo-3-chloropropane 5.0

50 3070-130 1.6ug/kg BRL61.36 1231,1-Dichloroethene 5.0




Page 202 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477686A - SW8260C








50 3070-130 0.8ug/kg BRL63.76 128trans-1,2-Dichloroethene 5.0

50 3070-130 3.2ug/kg BRL62.17 124Styrene 5.0

50 3070-130 2.3ug/kg BRL63.77 128tert-Butylbenzene 1.0



50 3070-130 1.6ug/kg BRL61.44 123Toluene 1.0


50 3070-130 2.6ug/kg BRL56.30 113trans-1,3-Dichloropropene 5.0

250 3070-130 7.5ug/kg BRL257.2 103trans-1,4-dichloro-2-butene 5.0


125 3070-130 9.3ug/kg BRL127.3 102Tetrahydrofuran (THF) 5.0


50 3070-130 1.1ug/kg BRL43.25 87Trichlorofluoromethane 5.0

50 3070-130 0.0ug/kg BRL48.90 98Vinyl chloride 5.0





Batch 477696A - SW8260C


-ug/lND ND1,4-Dichlorobenzene 1.0

-ug/lND ND1,2,4-Trimethylbenzene 1.0

-ug/lND ND1,2-Dibromo-3-chloropropane 1.0

-ug/lND ND1,2-Dibromoethane 1.0


-ug/lND ND1,2-Dichloroethane 1.0

-ug/lND ND1,2-Dichloropropane 1.0


-ug/lND ND1,2,4-Trichlorobenzene 1.0


-ug/lND ND1,1-Dichloroethene 1.0


-ug/lND ND2-Chlorotoluene 1.0

-ug/lND ND2-Hexanone 5.0

-ug/lND NDo-Xylene 1.0


-ug/lND ND1,1,1-Trichloroethane 1.0

-ug/lND NDm&p-Xylene 1.0

-ug/lND NDMethyl ethyl ketone 5.0

-ug/lND NDMethyl t-butyl ether (MTBE) 1.0

-ug/lND NDMethylene chloride 1.0

-ug/lND NDNaphthalene 1.0

-ug/lND NDn-Butylbenzene 1.0



Page 203 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477696A - SW8260C


-ug/lND ND1,1,1,2-Tetrachloroethane 1.0

-ug/lND ND1,2,3-Trichloropropane 1.0




-ug/lND NDp-Isopropyltoluene 1.0

-ug/lND ND1,1-Dichloropropene 1.0

-ug/lND NDtrans-1,4-dichloro-2-butene 5.0

-ug/lND NDn-Propylbenzene 1.0

-ug/lND NDDibromomethane 1.0

-ug/lND NDsec-Butylbenzene 1.0

-ug/lND NDCarbon tetrachloride 1.0

-ug/lND NDChloroethane 1.0

-ug/lND NDChloroform 1.0

-ug/lND NDChloromethane 1.0

-ug/lND NDcis-1,2-Dichloroethene 1.0

-ug/lND NDBromomethane 1.0

-ug/lND NDDibromochloromethane 0.50

-ug/lND NDCarbon Disulfide 1.0

-ug/lND NDDichlorodifluoromethane 1.0

-ug/lND NDEthylbenzene 1.0

-ug/lND NDHexachlorobutadiene 0.40

-ug/lND NDVinyl chloride 1.0

-ug/lND NDTrichlorotrifluoroethane 1.0

-ug/lND NDTrichlorofluoromethane 1.0

-ug/lND NDTrichloroethene 1.0

-ug/lND NDcis-1,3-Dichloropropene 0.40

-ug/lND ND4-Methyl-2-pentanone 5.0

-ug/lND NDStyrene 1.0

-ug/lND NDtert-Butylbenzene 1.0

-ug/lND NDTetrachloroethene 1.0

-ug/lND NDTetrahydrofuran (THF) 2.5

-ug/lND NDToluene 1.0

-ug/lND NDtrans-1,2-Dichloroethene 1.0

-ug/lND NDtrans-1,3-Dichloropropene 0.40

-ug/lND NDIsopropylbenzene 1.0

-ug/lND ND2-Isopropyltoluene 1.0

-ug/lND NDChlorobenzene 1.0


-ug/lND NDBromoform 1.0

-ug/lND NDAcetone 5.0

-ug/lND NDAcrylonitrile 5.0

-ug/lND NDBenzene 0.70

-ug/lND NDBromobenzene 1.0

-ug/lND NDBromochloromethane 1.0

-ug/lND NDBromodichloromethane 0.50

10 70-130Surrogate: % Bromofluorobenzene 96 ug/l 96

10 70-130Surrogate: % Dibromofluoromethane 98 ug/l 98

10 70-130Surrogate: % Toluene-d8 92 ug/l 92

10 70-130Surrogate: % 1,2-dichlorobenzene-d4 95 ug/l 95


Page 204 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477696A - SW8260C


10 3070-130ug/l10.48 105p-Isopropyltoluene 1.0

10 3070-130ug/l10.41 104Benzene 0.70

10 3070-130ug/l10.61 106Carbon tetrachloride 1.0

10 3070-130ug/l10.35 1032-Chlorotoluene 1.0

10 3070-130ug/l10.50 1052-Hexanone 5.0

10 3070-130ug/l10.39 1042-Isopropyltoluene 1.0


10 3070-130ug/l10.75 1074-Methyl-2-pentanone 5.0

10 3070-130ug/l10.66 1071,4-Dichlorobenzene 1.0

10 3070-130ug/l10.51 105Acrylonitrile 5.0

10 3070-130ug/l10.78 1081,3-Dichloropropane 1.0

10 3070-130ug/l11.03 110Bromobenzene 1.0

10 3070-130ug/l10.61 106Bromochloromethane 1.0

10 3070-130ug/l10.93 109Bromodichloromethane 0.50

10 3070-130ug/l11.37 114Bromoform 1.0

10 3070-130ug/ll14.24 142Bromomethane 1.0

10 3070-130ug/l10.94 1091,1,1,2-Tetrachloroethane 1.0

10 3070-130ug/l9.518 95Acetone 5.0

10 3070-130ug/l12.15 1221,2-Dibromo-3-chloropropane 1.0

10 3070-130ug/l10.50 1051,1,1-Trichloroethane 1.0



10 3070-130ug/l10.50 1051,1-Dichloroethane 1.0

10 3070-130ug/l11.03 1101,1-Dichloroethene 1.0

10 3070-130ug/l10.87 1091,2,3-Trichlorobenzene 1.0


10 3070-130ug/l10.41 1041,2,4-Trimethylbenzene 1.0

10 3070-130ug/l10.77 108Chlorobenzene 1.0

10 3070-130ug/l10.87 1091,2-Dibromoethane 1.0







10 3070-130ug/l10.73 107trans-1,3-Dichloropropene 0.40

10 3070-130ug/l10.72 107Carbon Disulfide 1.0

10 3070-130ug/l10.85 109sec-Butylbenzene 1.0

10 3070-130ug/l10.97 110Styrene 1.0

10 3070-130ug/l10.45 104tert-Butylbenzene 1.0

10 3070-130ug/l11.49 115Tetrachloroethene 1.0

25 3070-130ug/l24.91 100Tetrahydrofuran (THF) 2.5

10 3070-130ug/l10.43 104n-Butylbenzene 1.0

10 3070-130ug/l10.92 109trans-1,2-Dichloroethene 1.0

10 3070-130ug/l11.40 114Naphthalene 1.0

50 3070-130ug/l58.34 117trans-1,4-dichloro-2-butene 5.0

10 3070-130ug/l11.24 112Trichloroethene 1.0

10 3070-130ug/l9.698 97Trichlorofluoromethane 1.0

10 3070-130ug/l10.94 109Trichlorotrifluoroethane 1.0

10 3070-130ug/l10.57 106Vinyl chloride 1.0


Page 205 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477696A - SW8260C


10 3070-130ug/l10.55 106n-Propylbenzene 1.0

10 3070-130ug/l10.91 109Toluene 1.0

10 3070-130ug/l10.79 108Ethylbenzene 1.0

10 3070-130ug/l10.60 106Chloroethane 1.0

10 3070-130ug/l10.41 104Chloroform 1.0

10 3070-130ug/l8.638 86Chloromethane 1.0

10 3070-130ug/l10.65 106cis-1,2-Dichloroethene 1.0

10 3070-130ug/l10.97 110cis-1,3-Dichloropropene 0.40

10 3070-130ug/l11.60 116Dibromochloromethane 0.50

10 3070-130ug/l10.83 108o-Xylene 1.0

10 3070-130ug/l11.25 113Dichlorodifluoromethane 1.0

10 3070-130ug/l10.81 1081,1-Dichloropropene 1.0

10 3070-130ug/l11.28 113Hexachlorobutadiene 0.40

10 3070-130ug/l10.50 105Isopropylbenzene 1.0

20 3070-130ug/l21.10 106m&p-Xylene 1.0

10 3070-130ug/l10.70 107Methyl ethyl ketone 5.0

10 3070-130ug/l11.22 112Methyl t-butyl ether (MTBE) 1.0

10 3070-130ug/l10.04 100Methylene chloride 1.0

10 3070-130ug/l10.82 108Dibromomethane 1.0

10 3070-130ug/l10.05 1001,2,3-Trichloropropane 1.0

10 70-130Surrogate: % Bromofluorobenzene 9.954 ug/l 100

10 70-130Surrogate: % Dibromofluoromethane 10.15 ug/l 102

10 70-130Surrogate: % Toluene-d8 10.02 ug/l 100

10 70-130Surrogate: % 1,2-dichlorobenzene-d4 10.05 ug/l 101


10 3070-130 1.8ug/l11.08 1111,2,3-Trichlorobenzene 1.0

10 3070-130 3.8ug/l10.65 1071,3,5-Trimethylbenzene 1.0

10 3070-130 0.9ug/l11.10 1111,2-Dichloropropane 1.0

10 3070-130 7.3ug/l12.80 1281,2-Dichloroethane 1.0

10 3070-130 2.7ug/l11.20 1121,2-Dichlorobenzene 1.0

10 3070-130 1.8ug/l11.11 1111,2-Dibromoethane 1.0

10 3070-130 4.0ug/l12.72 1271,2-Dibromo-3-chloropropane 1.0


10 3070-130 3.0ug/l10.33 1031,2,3-Trichloropropane 1.0


10 3070-130 2.7ug/l11.11 1111,1-Dichloropropene 1.0


10 3070-130 0.9ug/l11.38 1141,1,2,2-Tetrachloroethane 0.50

10 3070-130 2.8ug/l10.76 1081,1,1-Trichloroethane 1.0


10 3070-130 4.3ug/l9.053 91Acetone 5.0

10 3070-130 3.7ug/l10.97 110Carbon tetrachloride 1.0

10 3070-130 0.9ug/l10.85 108Carbon Disulfide 1.0

10 3070-130 8.8ug/ll15.50 155Bromomethane 1.0

10 3070-130 2.6ug/l11.72 117Bromoform 1.0

10 3070-130 0.9ug/l11.01 110Bromodichloromethane 0.50

10 3070-130 0.0ug/l10.62 106Bromochloromethane 1.0

10 3070-130 3.6ug/l11.40 114Bromobenzene 1.0


10 3070-130 2.9ug/l10.19 102Acrylonitrile 5.0


Page 206 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477696A - SW8260C



10 3070-130 2.8ug/l11.01 1104-Methyl-2-pentanone 5.0

10 3070-130 2.9ug/l10.40 1044-Chlorotoluene 1.0

10 3070-130 3.8ug/l10.81 1082-Isopropyltoluene 1.0

10 3070-130 3.7ug/l10.91 1092-Hexanone 5.0




10 3070-130 1.0ug/l10.54 105Benzene 0.70

10 3070-130 4.4ug/l11.48 1151,1-Dichloroethene 1.0

10 3070-130 3.7ug/l11.01 110n-Propylbenzene 1.0

10 3070-130 0.0ug/l10.84 108o-Xylene 1.0

10 3070-130 2.8ug/l10.81 108p-Isopropyltoluene 1.0

10 3070-130 2.7ug/l11.17 112sec-Butylbenzene 1.0

10 3070-130 0.9ug/l11.06 111Styrene 1.0

10 3070-130 2.8ug/l10.71 107tert-Butylbenzene 1.0

10 3070-130 0.9ug/l11.61 116Tetrachloroethene 1.0

10 3070-130 3.8ug/l10.80 108n-Butylbenzene 1.0

10 3070-130 2.7ug/l11.18 112Toluene 1.0

25 3070-130 3.0ug/l25.68 103Tetrahydrofuran (THF) 2.5

10 3070-130 0.9ug/l10.84 108trans-1,3-Dichloropropene 0.40

50 3070-130 3.4ug/l60.51 121trans-1,4-dichloro-2-butene 5.0

10 3070-130 1.8ug/l11.40 114Trichloroethene 1.0

10 3070-130 3.0ug/l10.04 100Trichlorofluoromethane 1.0

10 3070-130 2.7ug/l11.23 112Trichlorotrifluoroethane 1.0

10 3070-130 4.6ug/l11.07 111Vinyl chloride 1.0


10 3070-130 0.9ug/l10.89 109Chlorobenzene 1.0

10 3070-130 5.2ug/l11.88 119Dichlorodifluoromethane 1.0

10 3070-130 2.6ug/l11.69 117Naphthalene 1.0

10 3070-130 1.0ug/l10.46 105Chloroform 1.0

10 3070-130 3.4ug/l8.917 89Chloromethane 1.0

10 3070-130 1.9ug/l10.79 108cis-1,2-Dichloroethene 1.0

10 3070-130 0.9ug/l11.08 111cis-1,3-Dichloropropene 0.40

10 3070-130 1.7ug/l11.76 118Dibromochloromethane 0.50

10 3070-130 1.8ug/l11.13 111trans-1,2-Dichloroethene 1.0

10 3070-130 0.9ug/l10.92 109Dibromomethane 1.0

10 3070-130 1.9ug/l10.80 108Chloroethane 1.0

10 3070-130 1.8ug/l11.03 110Ethylbenzene 1.0

10 3070-130 3.5ug/l11.71 117Hexachlorobutadiene 0.40

10 3070-130 3.7ug/l10.90 109Isopropylbenzene 1.0

20 3070-130 2.8ug/l21.75 109m&p-Xylene 1.0

10 3070-130 0.9ug/l10.59 106Methyl ethyl ketone 5.0

10 3070-130 1.8ug/l11.35 114Methyl t-butyl ether (MTBE) 1.0

10 3070-130 3.0ug/l10.27 103Methylene chloride 1.0





Batch 477712A - SW8260C


Page 207 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477712A - SW8260C


-ug/lND ND1,1-Dichloropropene 1.0


-ug/lND ND1,2-Dibromoethane 1.0

-ug/lND ND1,2-Dibromo-3-chloropropane 1.0



-ug/lND ND1,2,3-Trichloropropane 1.0


-ug/lND ND1,1-Dichloroethene 1.0






-ug/lND ND4-Methyl-2-pentanone 5.0


-ug/lND NDp-Isopropyltoluene 1.0

-ug/lND NDDibromomethane 1.0

-ug/lND NDDichlorodifluoromethane 1.0

-ug/lND NDEthylbenzene 1.0


-ug/lND NDIsopropylbenzene 1.0

-ug/lND NDm&p-Xylene 1.0

-ug/lND NDMethyl ethyl ketone 5.0


-ug/lND NDMethylene chloride 1.0

-ug/lND ND2-Isopropyltoluene 1.0

-ug/lND NDn-Butylbenzene 1.0

-ug/lND NDDibromochloromethane 0.50

-ug/lND NDo-Xylene 1.0

-ug/lND NDMethyl t-butyl ether (MTBE) 1.0

-ug/lND NDsec-Butylbenzene 1.0

-ug/lND NDStyrene 1.0

-ug/lND NDtert-Butylbenzene 1.0

-ug/lND NDTetrachloroethene 1.0

-ug/lND NDTetrahydrofuran (THF) 2.5

-ug/lND NDToluene 1.0

-ug/lND NDtrans-1,2-Dichloroethene 1.0

-ug/lND NDVinyl chloride 1.0

-ug/lND NDTrichlorotrifluoroethane 1.0

-ug/lND NDTrichlorofluoromethane 1.0

-ug/lND NDTrichloroethene 1.0

-ug/lND NDtrans-1,4-dichloro-2-butene 5.0

-ug/lND NDn-Propylbenzene 1.0

-ug/lND ND2-Hexanone 5.0







Page 208 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477712A - SW8260C



-ug/lND NDcis-1,3-Dichloropropene 0.40


-ug/lND NDtrans-1,3-Dichloropropene 0.40

-ug/lND NDAcetone 5.0

-ug/lND NDAcrylonitrile 5.0

-ug/lND NDBenzene 0.70

-ug/lND NDBromobenzene 1.0

-ug/lND NDChlorobenzene 1.0


-ug/lND NDBromochloromethane 1.0


-ug/lND NDChloromethane 1.0

-ug/lND NDChloroethane 1.0

-ug/lND NDCarbon tetrachloride 1.0

-ug/lND NDCarbon Disulfide 1.0

-ug/lND NDBromomethane 1.0

-ug/lND NDBromoform 1.0

-ug/lND NDBromodichloromethane 0.50

-ug/lND NDChloroform 1.0






10 3070-130ug/l8.834 88Vinyl chloride 1.0

10 3070-130ug/l11.18 112Tetrachloroethene 1.0

10 3070-130ug/l11.72 117o-Xylene 1.0

10 3070-130ug/l11.71 117p-Isopropyltoluene 1.0

10 3070-130ug/l11.97 120sec-Butylbenzene 1.0

10 3070-130ug/l11.77 118Styrene 1.0

10 3070-130ug/l11.46 115tert-Butylbenzene 1.0

25 3070-130ug/l27.36 109Tetrahydrofuran (THF) 2.5

10 3070-130ug/l11.53 115Toluene 1.0

10 3070-130ug/l11.70 117trans-1,2-Dichloroethene 1.0

10 3070-130ug/l11.93 119trans-1,3-Dichloropropene 0.40

50 3070-130ug/l57.94 116trans-1,4-dichloro-2-butene 5.0

10 3070-130ug/l11.30 113Trichloroethene 1.0

10 3070-130ug/l10.50 105Trichlorotrifluoroethane 1.0

10 3070-130ug/l11.14 111Methyl t-butyl ether (MTBE) 1.0

10 3070-130ug/l11.49 115n-Propylbenzene 1.0

10 3070-130ug/l7.943 79Trichlorofluoromethane 1.0

10 3070-130ug/l11.11 111Acrylonitrile 5.0




10 3070-130ug/l11.51 1152-Hexanone 5.0

10 3070-130ug/l10.28 1032-Isopropyltoluene 1.0


10 3070-130ug/l10.99 110Carbon tetrachloride 1.0


Page 209 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477712A - SW8260C


10 3070-130ug/l9.061 91Acetone 5.0


10 3070-130ug/l11.34 113Benzene 0.70

10 3070-130ug/l11.53 115Bromobenzene 1.0

10 3070-130ug/l11.64 116Bromochloromethane 1.0

10 3070-130ug/l11.93 119Bromodichloromethane 0.50

10 3070-130ug/l12.40 124Bromoform 1.0

10 3070-130ug/l11.08 111Bromomethane 1.0

10 3070-130ug/l10.16 102Carbon Disulfide 1.0

10 3070-130ug/l11.10 1114-Methyl-2-pentanone 5.0


10 3070-130ug/l13.00 130Naphthalene 1.0

10 3070-130ug/l11.56 116n-Butylbenzene 1.0







10 3070-130ug/l11.60 1161,1-Dichloropropene 1.0


10 3070-130ug/l11.62 1161,2,3-Trichloropropane 1.0



10 3070-130ug/l12.48 1251,2-Dibromo-3-chloropropane 1.0

10 3070-130ug/l12.29 1231,2-Dibromoethane 1.0



10 3070-130ug/l11.73 1171,1-Dichloroethene 1.0


10 3070-130ug/l11.01 110Methylene chloride 1.0

10 3070-130ug/l11.65 117Methyl ethyl ketone 5.0


10 3070-130ug/l11.38 114Isopropylbenzene 1.0

10 3070-130ug/l11.35 114Ethylbenzene 1.0

10 3070-130ug/lr8.892 89Dichlorodifluoromethane 1.0

10 3070-130ug/l11.56 116Dibromomethane 1.0

10 3070-130ug/l12.43 124Dibromochloromethane 0.50

10 3070-130ug/l11.99 120cis-1,3-Dichloropropene 0.40


10 3070-130ug/l7.618 76Chloromethane 1.0

10 3070-130ug/l10.80 108Chloroform 1.0

10 3070-130ug/l9.096 91Chloroethane 1.0

10 3070-130ug/l11.18 112Chlorobenzene 1.0

20 3070-130ug/l22.71 114m&p-Xylene 1.0







Page 210 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477712A - SW8260C


10 3070-130 6.8ug/l12.08 121Benzene 0.70

10 3070-130 7.8ug/l12.01 120Bromomethane 1.0



10 3070-130 4.3ug/l12.01 1202-Hexanone 5.0

10 3070-130 6.6ug/l10.97 1102-Isopropyltoluene 1.0


10 3070-130 7.0ug/l11.92 1194-Methyl-2-pentanone 5.0


10 3070-130 5.3ug/l11.65 117Acrylonitrile 5.0


10 3070-130 5.1ug/l12.09 121Bromobenzene 1.0

10 3070-130 8.3ug/l12.62 126Bromochloromethane 1.0

10 3070-130 4.9ug/l12.46 125Bromodichloromethane 0.50

10 3070-130 23.3ug/l11.48 115Acetone 5.0

10 3070-130 6.8ug/l12.22 122Isopropylbenzene 1.0

10 3070-130 6.1ug/ll13.61 1361,1,2,2-Tetrachloroethane 0.50




10 3070-130 7.4ug/l12.60 1261,1-Dichloroethene 1.0

10 3070-130 7.5ug/l12.52 1251,1-Dichloropropene 1.0

10 3070-130 8.6ug/ll13.35 1341,2,3-Trichlorobenzene 1.0



10 3070-130 6.6ug/l10.85 109Carbon Disulfide 1.0



10 3070-130 4.7ug/ll13.14 1311,2-Dibromo-3-chloropropane 1.0

10 3070-130 4.8ug/l12.92 1291,2-Dibromoethane 1.0





10 3070-130 11.4ug/l12.99 1301,2,3-Trichloropropane 1.0

10 3070-130 5.0ug/l12.44 124Styrene 1.0

10 3070-130 7.9ug/l11.86 119Methylene chloride 1.0


10 3070-130 7.0ug/ll13.33 133Bromoform 1.0

10 3070-130 5.8ug/l12.36 124trans-1,2-Dichloroethene 1.0

10 3070-130 5.1ug/l12.06 121Toluene 1.0

25 3070-130 2.7ug/l27.97 112Tetrahydrofuran (THF) 2.5

10 3070-130 6.0ug/l12.02 120Trichloroethene 1.0

10 3070-130 5.9ug/l12.16 122tert-Butylbenzene 1.0

50 3070-130 9.1ug/l63.33 127trans-1,4-dichloro-2-butene 5.0

10 3070-130 5.7ug/l12.67 127sec-Butylbenzene 1.0

10 3070-130 4.2ug/l12.25 122p-Isopropyltoluene 1.0

10 3070-130 5.8ug/l12.39 124o-Xylene 1.0

10 3070-130 5.9ug/l12.15 122n-Propylbenzene 1.0

10 3070-130 5.9ug/l12.29 123n-Butylbenzene 1.0


Page 211 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477712A - SW8260C


10 3070-130 9.5ug/ll14.28 143Naphthalene 1.0

10 3070-130 7.7ug/l12.13 121Tetrachloroethene 1.0


10 3070-130 7.0ug/l11.76 118Carbon tetrachloride 1.0

10 3070-130 5.1ug/l11.95 120Ethylbenzene 1.0

10 3070-130 50.4ug/ll, r14.93 149Dichlorodifluoromethane 1.0

20 3070-130 5.1ug/l24.06 120m&p-Xylene 1.0

10 3070-130 7.5ug/l12.45 125Dibromomethane 1.0

10 3070-130 7.3ug/l12.77 128trans-1,3-Dichloropropene 0.40

10 3070-130 5.7ug/l12.75 127cis-1,3-Dichloropropene 0.40

10 3070-130 7.3ug/l8.521 85Trichlorofluoromethane 1.0

10 3070-130 6.4ug/l8.073 81Chloromethane 1.0

10 3070-130 9.7ug/l11.87 119Chloroform 1.0

10 3070-130 11.4ug/l10.15 102Chloroethane 1.0

10 3070-130 6.1ug/l11.88 119Chlorobenzene 1.0

10 3070-130 9.0ug/l12.78 128Methyl ethyl ketone 5.0

10 3070-130 7.0ug/l11.89 119Methyl t-butyl ether (MTBE) 1.0

10 3070-130 7.7ug/l9.511 95Vinyl chloride 1.0

10 3070-130 5.6ug/l11.07 111Trichlorotrifluoroethane 1.0

10 3070-130 4.7ug/l12.99 130Dibromochloromethane 0.50





Batch 477836A - SW8260C



























Page 212 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477836A - SW8260C









50 3070-130ug/kg44.70 89Benzene 1.0































50 3070-130 9.6ug/kg48.76 98Benzene 1.0













Page 213 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8260C

Batch 477836A - SW8260C

















Batch 477847A - SW8260C



















SW8270D

Batch 477192A - SW3545A


-ug/kgND NDAcetophenone 230

-ug/kgND NDPyridine 230

-ug/kgND NDPyrene 230

-ug/kgND NDPhenol 230

-ug/kgND NDPhenanthrene 130

-ug/kgND NDPentachlorophenol 230

-ug/kgND NDPentachloronitrobenzene 230

-ug/kgND NDN-Nitrosodiphenylamine 130

-ug/kgND NDAcenaphthylene 130

-ug/kgND ND3-Nitroaniline 330

-ug/kgND ND4,6-Dinitro-2-methylphenol 230


Page 214 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8270D

Batch 477192A - SW3545A


-ug/kgND ND4-Bromophenyl phenyl ether 230

-ug/kgND ND4-Chloro-3-methylphenol 230

-ug/kgND ND4-Chloroaniline 230

-ug/kgND ND4-Chlorophenyl phenyl ether 230


-ug/kgND NDBenzyl butyl phthalate 230

-ug/kgND NDAcenaphthene 230

-ug/kgND ND2-Nitrophenol 230

-ug/kgND NDAniline 330

-ug/kgND NDBenz(a)anthracene 230

-ug/kgND NDBenzidine 330

-ug/kgND NDBenzo(a)pyrene 130

-ug/kgND NDBenzo(b)fluoranthene 160

-ug/kgND NDBenzo(ghi)perylene 230

-ug/kgND NDBenzo(k)fluoranthene 230

-ug/kgND NDBenzoic acid 330

-ug/kgND ND4-Nitrophenol 230

-ug/kgND ND2,4-Dinitrophenol 230

-ug/kgND ND1,2,4,5-Tetrachlorobenzene 230

-ug/kgND ND1,2,4-Trichlorobenzene 230

-ug/kgND ND1,2-Dichlorobenzene 180

-ug/kgND ND1,2-Diphenylhydrazine 230



-ug/kgND NDAnthracene 230

-ug/kgND ND2,4,6-Trichlorophenol 130

-ug/kgND ND3,3'-Dichlorobenzidine 130

-ug/kgND ND2,4-Dimethylphenol 230

-ug/kgND ND3&4-Methylphenol (m&p-cresol) 230

-ug/kgND ND2,4-Dinitrotoluene 130

-ug/kgND ND2,6-Dinitrotoluene 130

-ug/kgND ND2-Chloronaphthalene 230

-ug/kgND ND2-Chlorophenol 230

-ug/kgND ND2-Methylnaphthalene 230

-ug/kgND ND2-Methylphenol (o-cresol) 230


-ug/kgND ND2,4-Dichlorophenol 130

-ug/kgND NDN-Nitrosodi-n-propylamine 130

-ug/kgND NDHexachlorobenzene 130

-ug/kgND NDBis(2-chloroethoxy)methane 230

-ug/kgND NDHexachloroethane 130

-ug/kgND ND2,4,5-Trichlorophenol 230

-ug/kgND NDIndeno(1,2,3-cd)pyrene 230

-ug/kgND NDIsophorone 130

-ug/kgND NDNitrobenzene 130

-ug/kgND NDNaphthalene 230

-ug/kgND NDHexachlorocyclopentadiene 230

-ug/kgND NDHexachlorobutadiene 230

-ug/kgND NDN-Nitrosodimethylamine 230

-ug/kgND NDFluorene 230


Page 215 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8270D

Batch 477192A - SW3545A


-ug/kgND NDFluoranthene 230

-ug/kgND NDBis(2-chloroethyl)ether 130

-ug/kgND NDChrysene 230

-ug/kgND NDDibenz(a,h)anthracene 130

-ug/kgND NDDibenzofuran 230

-ug/kgND NDBis(2-ethylhexyl)phthalate 230

-ug/kgND NDBis(2-chloroisopropyl)ether 230

-ug/kgND NDCarbazole 230

-ug/kgND NDDi-n-octylphthalate 230

-ug/kgND NDDiethyl phthalate 230

-ug/kgND NDDimethylphthalate 230

-ug/kgND NDDi-n-butylphthalate 670

75 30-130Surrogate: % Phenol-d5 65 ug/kg 65

50 30-130Surrogate: % Nitrobenzene-d5 58 ug/kg 58

75 30-130Surrogate: % 2-Fluorophenol 58 ug/kg 58

75 30-130Surrogate: % 2,4,6-Tribromophenol 58 ug/kg 58

50 30-130Surrogate: % 2-Fluorobiphenyl 65 ug/kg 65

50 30-130Surrogate: % Terphenyl-d14 71 ug/kg 71


50 3030-130ug/kg42.39 85Di-n-butylphthalate 670

50 3030-130ug/kg37.00 74Dibenzofuran 230

50 3030-130ug/kg37.75 76Dimethylphthalate 230

50 3030-130ug/kg37.80 76Di-n-octylphthalate 230

50 3030-130ug/kg39.84 80Diethyl phthalate 230

50 3030-130ug/kg50.93 102Dibenz(a,h)anthracene 130

50 3030-130ug/kg38.51 77Chrysene 230

50 3030-130ug/kg37.25 74Carbazole 230

50 3030-130ug/kg39.76 80Bis(2-ethylhexyl)phthalate 230

50 3030-130ug/kg29.96 60Bis(2-chloroisopropyl)ether 230

50 3030-130ug/kg30.73 61Bis(2-chloroethyl)ether 130

50 3030-130ug/kg32.88 66Bis(2-chloroethoxy)methane 230

50 3030-130ug/kg37.14 74Benzyl butyl phthalate 230

50 3030-130ug/kg38.84 78Fluoranthene 230

50 3030-130ug/kg42.11 84Benzo(k)fluoranthene 230

50 3030-130ug/kg24.21 48N-Nitrosodimethylamine 230

50 3030-130ug/kgl1.128 <10Benzoic acid 330

50 3030-130ug/kg34.89 70Nitrobenzene 130

50 3030-130ug/kg16.09 32Pyridine 230

50 3030-130ug/kg39.31 79Pyrene 230

50 3030-130ug/kg37.06 74Phenol 230

50 3030-130ug/kg35.97 72Phenanthrene 130

50 3030-130ug/kg25.43 51Pentachlorophenol 230

50 3030-130ug/kg37.40 75Pentachloronitrobenzene 230

50 3030-130ug/kg38.57 77N-Nitrosodiphenylamine 130

50 3030-130ug/kg30.73 61Naphthalene 230

50 3030-130ug/kg38.81 784-Chlorophenyl phenyl ether 230

50 3030-130ug/kg38.83 78Fluorene 230

50 3030-130ug/kg41.52 83Benzo(ghi)perylene 230

50 3030-130ug/kg31.00 62Isophorone 130

50 3030-130ug/kg40.72 81Indeno(1,2,3-cd)pyrene 230


Page 216 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8270D

Batch 477192A - SW3545A


50 3030-130ug/kg26.93 54Hexachloroethane 130

50 3030-130ug/kg32.87 66Hexachlorocyclopentadiene 230

50 3030-130ug/kg30.77 62Hexachlorobutadiene 230

50 3030-130ug/kg33.49 67Hexachlorobenzene 130

50 3030-130ug/kg36.69 73N-Nitrosodi-n-propylamine 130

50 3030-130ug/kg26.48 531,3-Dichlorobenzene 230

50 3030-130ug/kg32.76 662-Methylnaphthalene 230

50 3030-130ug/kg35.81 722-Chlorophenol 230

50 3030-130ug/kg44.01 88Benzo(b)fluoranthene 160

50 3030-130ug/kg44.22 882,6-Dinitrotoluene 130

50 3030-130ug/kg39.58 794-Nitrophenol 230

50 3030-130ug/kg32.86 661,2,4,5-Tetrachlorobenzene 230

50 3030-130ug/kg30.95 621,2,4-Trichlorobenzene 230

50 3030-130ug/kg35.75 722-Methylphenol (o-cresol) 230

50 3030-130ug/kg39.75 791,2-Diphenylhydrazine 230

50 3030-130ug/kg34.64 692-Chloronaphthalene 230


50 3030-130ug/kg37.74 752,4,5-Trichlorophenol 230

50 3030-130ug/kg41.02 822,4,6-Trichlorophenol 130

50 3030-130ug/kg36.23 722,4-Dichlorophenol 130

50 3030-130ug/kg37.50 752,4-Dimethylphenol 230

50 3030-130ug/kgl6.727 132,4-Dinitrophenol 230

50 3030-130ug/kg41.03 822,4-Dinitrotoluene 130


50 3030-130ug/kg39.70 794-Chloro-3-methylphenol 230

50 3030-130ug/kg37.65 75Benzo(a)pyrene 130

50 3030-130ug/kg25.41 51Benzidine 330

50 3030-130ug/kg39.69 79Benz(a)anthracene 230

50 3030-130ug/kg37.73 75Anthracene 230

50 3030-130ug/kg29.25 58Aniline 330

50 3030-130ug/kg31.98 64Acetophenone 230

50 3030-130ug/kg36.07 72Acenaphthylene 130

50 3030-130ug/kg35.42 71Acenaphthene 230

50 3030-130ug/kg37.60 754-Chloroaniline 230

50 3030-130ug/kg52.77 1062-Nitroaniline 330

50 3030-130ug/kg18.81 384,6-Dinitro-2-methylphenol 230

50 3030-130ug/kg39.61 792-Nitrophenol 230

50 3030-130ug/kg38.09 763&4-Methylphenol (m&p-cresol) 230



50 3030-130ug/kg38.49 774-Bromophenyl phenyl ether 230

50 3030-130ug/kg48.14 963,3'-Dichlorobenzidine 130

50 30-130Surrogate: % 2-Fluorobiphenyl 33.05 ug/kg 66

75 30-130Surrogate: % 2-Fluorophenol 48.90 ug/kg 65

50 30-130Surrogate: % Nitrobenzene-d5 32.47 ug/kg 65

75 30-130Surrogate: % 2,4,6-Tribromophenol 56.25 ug/kg 75

75 30-130Surrogate: % Phenol-d5 54.13 ug/kg 72

50 30-130Surrogate: % Terphenyl-d14 36.38 ug/kg 73


50 3030-130 1.3ug/kg38.96 782-Nitrophenol 230


Page 217 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8270D

Batch 477192A - SW3545A


50 3030-130 1.6ug/kg31.41 631,2,4-Trichlorobenzene 230

50 3030-130 1.5ug/kg33.68 671,2,4,5-Tetrachlorobenzene 230

50 3030-130 1.3ug/kg39.39 794-Chlorophenyl phenyl ether 230

50 3030-130 16.7ug/kgl5.301 112,4-Dinitrophenol 230

50 3030-130 NCug/kgl1.256 <10Benzoic acid 330

50 3030-130 0.0ug/kg42.16 84Benzo(k)fluoranthene 230

50 3030-130 5.8ug/kg44.02 88Benzo(ghi)perylene 230

50 3030-130 3.4ug/kg45.32 91Benzo(b)fluoranthene 160

50 3030-130 1.3ug/kg38.04 76Benzo(a)pyrene 130

50 3030-130 7.5ug/kg27.62 55Benzidine 330

50 3030-130 1.3ug/kg40.10 80Benz(a)anthracene 230

50 3030-130 2.6ug/kg38.27 77Anthracene 230

50 3030-130 3.5ug/kg28.01 56Aniline 330

50 3030-130 0.0ug/kg31.96 64Acetophenone 230

50 3030-130 1.4ug/kg36.37 73Acenaphthylene 130

50 3030-130 2.8ug/kg36.26 73Acenaphthene 230

50 3030-130 1.5ug/kg32.44 65Bis(2-chloroethoxy)methane 230

50 3030-130 4.1ug/kg50.03 1003,3'-Dichlorobenzidine 130

50 3030-130 2.4ug/kg41.83 842,4-Dinitrotoluene 130

50 3030-130 1.1ug/kg44.34 892,6-Dinitrotoluene 130

50 3030-130 2.9ug/kg35.41 712-Chloronaphthalene 230

50 3030-130 1.4ug/kg35.56 712-Chlorophenol 230

50 3030-130 1.5ug/kg33.44 672-Methylnaphthalene 230

50 3030-130 1.3ug/kg38.78 784-Nitrophenol 230

50 3030-130 1.3ug/kg37.47 753&4-Methylphenol (m&p-cresol) 230

50 3030-130 3.5ug/kg42.29 854-Nitroaniline 230


50 3030-130 20.3ug/kg15.68 314,6-Dinitro-2-methylphenol 230

50 3030-130 2.6ug/kg37.41 754-Bromophenyl phenyl ether 230

50 3030-130 1.3ug/kg39.00 784-Chloro-3-methylphenol 230

50 3030-130 1.3ug/kg37.14 744-Chloroaniline 230

50 3030-130 3.2ug/kg31.36 63Bis(2-chloroethyl)ether 130


50 3030-130 6.3ug/kg33.08 66Hexachlorobutadiene 230

50 3030-130 2.8ug/kg34.84 702-Methylphenol (o-cresol) 230

50 3030-130 5.2ug/kg29.69 591,2-Dichlorobenzene 180

50 3030-130 17.1ug/kg18.97 38Pyridine 230

50 3030-130 9.6ug/kg43.34 87Pyrene 230

50 3030-130 2.7ug/kg35.96 72Phenol 230

50 3030-130 1.4ug/kg36.57 73Phenanthrene 130

50 3030-130 1.9ug/kg26.19 52Pentachlorophenol 230

50 3030-130 0.0ug/kg37.68 75Pentachloronitrobenzene 230

50 3030-130 4.2ug/kg34.87 70N-Nitrosodi-n-propylamine 130

50 3030-130 2.9ug/kg34.09 68Nitrobenzene 130

50 3030-130 3.2ug/kg31.50 63Naphthalene 230

50 3030-130 1.6ug/kg30.58 61Isophorone 130

50 3030-130 4.8ug/kg42.74 85Indeno(1,2,3-cd)pyrene 230

50 3030-130 4.1ug/kg35.59 71Benzyl butyl phthalate 230

50 3030-130 1.3ug/kg38.29 77Dimethylphthalate 230

50 3030-130 5.1ug/kg28.71 57Bis(2-chloroisopropyl)ether 230


Page 218 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8270D

Batch 477192A - SW3545A


50 3030-130 1.3ug/kg39.59 79Bis(2-ethylhexyl)phthalate 230

50 3030-130 5.3ug/kg38.79 78Carbazole 230

50 3030-130 1.3ug/kg39.09 78Chrysene 230

50 3030-130 4.8ug/kg53.36 107Dibenz(a,h)anthracene 130

50 3030-130 5.4ug/kg28.30 57Hexachloroethane 130

50 3030-130 2.5ug/kg40.91 82Diethyl phthalate 230

50 3030-130 6.3ug/kg30.85 62Hexachlorocyclopentadiene 230

50 3030-130 2.3ug/kg43.49 87Di-n-butylphthalate 670

50 3030-130 1.3ug/kg37.60 75Di-n-octylphthalate 230

50 3030-130 7.4ug/kg42.12 84Fluoranthene 230

50 3030-130 2.5ug/kg39.77 80Fluorene 230

50 3030-130 0.0ug/kg33.30 67Hexachlorobenzene 130

50 3030-130 9.9ug/kg26.49 53N-Nitrosodimethylamine 230

50 3030-130 1.3ug/kg37.54 75Dibenzofuran 230

50 3030-130 2.6ug/kg39.59 79N-Nitrosodiphenylamine 130

50 3030-130 1.3ug/kg38.14 762,4-Dimethylphenol 230

50 3030-130 1.3ug/kg39.19 781,2-Diphenylhydrazine 230


50 3030-130 2.6ug/kg38.35 772,4,5-Trichlorophenol 230

50 3030-130 2.5ug/kg40.24 802,4,6-Trichlorophenol 130

50 3030-130 1.4ug/kg35.61 712,4-Dichlorophenol 130









50 3030-130ug/kg BRL22.56 451,2-Dichlorobenzene 180

50 3030-130ug/kg BRL27.16 541,2,4-Trichlorobenzene 230

50 3030-130ug/kg BRL30.50 611,2,4,5-Tetrachlorobenzene 230

50 3030-130ug/kg BRL26.44 53Nitrobenzene 130

50 3030-130ug/kg40.81 69Chrysene 230

50 3030-130ug/kg45.54 77Indeno(1,2,3-cd)pyrene 230

50 3030-130ug/kg BRL26.55 53Isophorone 130

50 3030-130ug/kg BRL32.65 652,4-Dichlorophenol 130

50 3030-130ug/kg BRL21.51 43Hexachloroethane 130

50 3030-130ug/kg BRL27.79 56Hexachlorocyclopentadiene 230

50 3030-130ug/kg BRL31.65 63Hexachlorobenzene 130

50 3030-130ug/kg48.15 77Fluoranthene 230

50 3030-130ug/kg BRL26.57 53Naphthalene 230

50 3030-130ug/kg BRL37.61 752,4-Dinitrotoluene 130

50 3030-130ug/kgm BRL13.67 27Pyridine 230

50 3030-130ug/kg47.21 75Pyrene 230

50 3030-130ug/kg BRL28.86 58Phenol 230

50 3030-130ug/kg BRL37.13 69Phenanthrene 130

50 3030-130ug/kg BRL25.11 50Pentachlorophenol 230

50 3030-130ug/kg BRL34.86 70Pentachloronitrobenzene 230

50 3030-130ug/kg BRL35.73 71N-Nitrosodiphenylamine 130


Page 219 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8270D

Batch 477192A - SW3545A


50 3030-130ug/kg BRL34.80 702,4,5-Trichlorophenol 230

50 3030-130ug/kg BRL19.57 39N-Nitrosodimethylamine 230

50 3030-130ug/kg BRL31.24 621,2-Diphenylhydrazine 230

50 3030-130ug/kg BRL33.98 682,4-Dinitrophenol 230

50 3030-130ug/kg BRL34.56 692,4-Dimethylphenol 230

50 3030-130ug/kg BRL35.84 72Fluorene 230

50 3030-130ug/kg BRL35.89 722,4,6-Trichlorophenol 130

50 3030-130ug/kg BRL35.33 71Di-n-octylphthalate 230



50 3030-130ug/kg BRL28.12 56N-Nitrosodi-n-propylamine 130

50 3030-130ug/kg40.65 67Benzo(a)pyrene 130

50 3030-130ug/kg BRL32.78 664-Chloroaniline 230

50 3030-130ug/kg BRL27.17 54Hexachlorobutadiene 230

50 3030-130ug/kg BRL36.87 744-Nitroaniline 230

50 3030-130ug/kg BRL36.27 734-Nitrophenol 230

50 3030-130ug/kg BRL32.37 65Acenaphthene 230

50 3030-130ug/kg BRL33.67 61Acenaphthylene 130

50 3030-130ug/kg BRL25.79 52Acetophenone 230

50 3030-130ug/kg BRL24.62 49Aniline 330

50 3030-130ug/kg BRL36.63 73Anthracene 230

50 3030-130ug/kg BRL39.27 79Di-n-butylphthalate 670

50 3030-130ug/kgm BRL14.44 29Benzidine 330

50 3030-130ug/kg BRL35.63 714-Chloro-3-methylphenol 230

50 3030-130ug/kg47.41 82Benzo(b)fluoranthene 160

50 3030-130ug/kg45.69 78Benzo(ghi)perylene 230

50 3030-130ug/kg41.36 72Benzo(k)fluoranthene 230

50 3030-130ug/kgm BRL11.96 24Benzoic acid 330

50 3030-130ug/kg BRL33.09 66Benzyl butyl phthalate 230

50 3030-130ug/kg BRL27.70 55Bis(2-chloroethoxy)methane 230

50 3030-130ug/kg BRL22.36 45Bis(2-chloroethyl)ether 130

50 3030-130ug/kg BRL22.43 45Bis(2-chloroisopropyl)ether 230

50 3030-130ug/kg BRL36.56 70Bis(2-ethylhexyl)phthalate 230

50 3030-130ug/kg BRL35.57 71Carbazole 230

50 3030-130ug/kg41.84 73Benz(a)anthracene 230

50 3030-130ug/kg BRL31.54 632-Methylphenol (o-cresol) 230

50 3030-130ug/kg BRL33.68 67Dimethylphthalate 230

50 3030-130ug/kg BRL35.98 72Diethyl phthalate 230

50 3030-130ug/kg BRL34.06 68Dibenzofuran 230

50 3030-130ug/kg BRL52.19 101Dibenz(a,h)anthracene 130

50 3030-130ug/kg BRL39.15 782,6-Dinitrotoluene 130

50 3030-130ug/kg BRL31.45 632-Chloronaphthalene 230

50 3030-130ug/kg BRL35.44 714-Chlorophenyl phenyl ether 230

50 3030-130ug/kg BRL29.11 582-Methylnaphthalene 230

50 3030-130ug/kg BRL35.31 714-Bromophenyl phenyl ether 230


50 3030-130ug/kg BRL31.11 623&4-Methylphenol (m&p-cresol) 230

50 3030-130ug/kg BRL52.03 1043,3'-Dichlorobenzidine 130


50 3030-130ug/kg BRL46.03 924,6-Dinitro-2-methylphenol 230


Page 220 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8270D

Batch 477192A - SW3545A


50 3030-130ug/kg BRL28.64 572-Chlorophenol 230

50 3030-130ug/kg BRL33.11 662-Nitrophenol 230








50 3030-130 0.0ug/kg BRL33.07 662-Nitrophenol 230

50 3030-130 3.3ug/kg BRL29.66 591,2,4,5-Tetrachlorobenzene 230

50 3030-130 1.8ug/kg BRL27.31 551,2,4-Trichlorobenzene 230

50 3030-130 8.5ug/kg BRL24.41 491,2-Dichlorobenzene 180

50 3030-130 7.8ug/kg BRL33.51 671,2-Diphenylhydrazine 230


50 3030-130 4.3ug/kg BRL34.35 69Diethyl phthalate 230

50 3030-130 1.8ug/kg BRL27.77 56Bis(2-chloroethoxy)methane 230

50 3030-130 2.2ug/kg BRL23.02 46Bis(2-chloroethyl)ether 130

50 3030-130 4.3ug/kg BRL23.49 47Bis(2-chloroisopropyl)ether 230

50 3030-130 4.4ug/kg BRL35.11 67Bis(2-ethylhexyl)phthalate 230

50 3030-130 4.3ug/kg BRL33.84 68Carbazole 230

50 3030-130 9.1ug/kg37.63 63Chrysene 230

50 3030-130 5.5ug/kg BRL26.51 53Hexachlorocyclopentadiene 230

50 3030-130 4.5ug/kg BRL32.74 65Dibenzofuran 230

50 3030-130 7.2ug/kg38.93 67Benzo(k)fluoranthene 230

50 3030-130 1.5ug/kg BRL32.90 66Dimethylphthalate 230

50 3030-130 5.2ug/kg BRL37.29 75Di-n-butylphthalate 670

50 3030-130 2.9ug/kg BRL34.31 69Di-n-octylphthalate 230

50 3030-130 18.4ug/kg42.04 64Fluoranthene 230

50 3030-130 4.3ug/kg BRL34.51 69Fluorene 230

50 3030-130 4.9ug/kg BRL29.80 60Hexachlorobenzene 130

50 3030-130 1.6ug/kg BRL32.19 642-Methylphenol (o-cresol) 230

50 3030-130 5.1ug/kg BRL49.86 96Dibenz(a,h)anthracene 130

50 3030-130 4.0ug/kg BRL25.46 51Aniline 330

50 3030-130 4.3ug/kg BRL34.08 684-Chloro-3-methylphenol 230

50 3030-130 3.1ug/kg BRL32.13 644-Chloroaniline 230

50 3030-130 4.3ug/kg BRL34.10 684-Bromophenyl phenyl ether 230

50 3030-130 4.3ug/kg BRL34.24 684-Chlorophenyl phenyl ether 230

50 3030-130 1.4ug/kg BRL36.69 734-Nitroaniline 230

50 3030-130 8.6ug/kg BRL33.70 674-Nitrophenol 230

50 3030-130 3.1ug/kg BRL31.52 63Acenaphthene 230

50 3030-130 3.1ug/kg BRL32.19 64Benzyl butyl phthalate 230

50 3030-130 3.8ug/kg BRL27.09 54Acetophenone 230

50 3030-130 18.2ug/kgm BRL10.06 20Benzoic acid 330

50 3030-130 5.6ug/kg BRL34.69 69Anthracene 230

50 3030-130 8.6ug/kg38.92 67Benz(a)anthracene 230

50 3030-130 12.9ug/kg BRL16.31 33Benzidine 330

50 3030-130 11.0ug/kg37.09 60Benzo(a)pyrene 130

50 3030-130 15.8ug/kg41.49 70Benzo(b)fluoranthene 160

50 3030-130 6.6ug/kg43.44 73Benzo(ghi)perylene 230


Page 221 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8270D

Batch 477192A - SW3545A


50 3030-130 6.7ug/kg BRL22.93 46Hexachloroethane 130

50 3030-130 3.3ug/kg BRL32.71 59Acenaphthylene 130

50 3030-130 2.9ug/kg BRL50.31 1013,3'-Dichlorobenzidine 130

50 3030-130 2.9ug/kg BRL33.83 682,4,5-Trichlorophenol 230

50 3030-130 1.4ug/kg BRL35.45 712,4,6-Trichlorophenol 130

50 3030-130 1.6ug/kg BRL32.06 642,4-Dichlorophenol 130

50 3030-130 2.9ug/kg BRL33.43 672,4-Dimethylphenol 230

50 3030-130 17.6ug/kg BRL28.64 572,4-Dinitrophenol 230

50 3030-130 5.5ug/kg BRL35.73 712,4-Dinitrotoluene 130

50 3030-130 2.6ug/kg BRL38.23 762,6-Dinitrotoluene 130

50 3030-130 1.6ug/kg BRL31.05 622-Chloronaphthalene 230

50 3030-130 3.4ug/kg BRL29.67 592-Chlorophenol 230

50 3030-130 0.0ug/kg BRL29.03 582-Methylnaphthalene 230

50 3030-130 3.6ug/kg BRL27.84 56Hexachlorobutadiene 230

50 3030-130 3.2ug/kg BRL31.92 643&4-Methylphenol (m&p-cresol) 230



50 3030-130 5.9ug/kg BRL33.15 66Pentachloronitrobenzene 230

50 3030-130 5.5ug/kg BRL28.09 56Nitrobenzene 130

50 3030-130 9.8ug/kg BRL21.31 43N-Nitrosodimethylamine 230


50 3030-130 1.9ug/kg BRL27.24 54Naphthalene 230

50 3030-130 12.7ug/kg BRL40.40 814,6-Dinitro-2-methylphenol 230

50 3030-130 2.9ug/kg BRL34.74 69N-Nitrosodiphenylamine 130

50 3030-130 3.5ug/kg BRL28.80 58N-Nitrosodi-n-propylamine 130

50 3030-130 12.8ug/kg BRL22.22 44Pentachlorophenol 230

50 3030-130 9.1ug/kg BRL34.15 63Phenanthrene 130

50 3030-130 3.4ug/kg BRL30.08 60Phenol 230

50 3030-130 6.7ug/kg43.26 72Indeno(1,2,3-cd)pyrene 230

50 3030-130 17.4ug/kg41.58 63Pyrene 230

50 3030-130 10.5ug/kg BRL15.16 30Pyridine 230

50 3030-130 0.0ug/kg BRL26.32 53Isophorone 130







Batch 477196A - SW3520C


-ug/lND ND4-Chloro-3-methylphenol 1.0

-ug/lND NDCarbazole 5.0

-ug/lND ND4-Chloroaniline 3.5

-ug/lND ND4-Chlorophenyl phenyl ether 1.0

-ug/lND ND4-Nitroaniline 5.0

-ug/lND ND4-Nitrophenol 1.0

-ug/lND NDAcetophenone 3.5

-ug/lND NDAniline 3.5

-ug/lND NDBenzidine 4.5

-ug/lND NDBenzoic acid 10


Page 222 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8270D

Batch 477196A - SW3520C


-ug/lND NDBenzyl butyl phthalate 1.5

-ug/lND NDBis(2-chloroethoxy)methane 3.5

-ug/lND NDBis(2-chloroethyl)ether 1.0

-ug/lND ND4-Bromophenyl phenyl ether 3.5

-ug/lND NDBis(2-ethylhexyl)phthalate 1.5

-ug/lND NDN-Nitrosodiphenylamine 3.5

-ug/lND NDDibenzofuran 3.5

-ug/lND NDDiethyl phthalate 1.5

-ug/lND NDDimethylphthalate 1.5

-ug/lND NDDi-n-butylphthalate 1.5

-ug/lND NDDi-n-octylphthalate 1.5

-ug/lND NDHexachloroethane 3.5

-ug/lND NDIsophorone 3.5

-ug/lND NDN-Nitrosodimethylamine 1.0

-ug/lND NDN-Nitrosodi-n-propylamine 3.5

-ug/lND NDPentachloronitrobenzene 5.0

-ug/lND ND4,6-Dinitro-2-methylphenol 1.0

-ug/lND NDBis(2-chloroisopropyl)ether 1.0

-ug/lND ND2,4-Dimethylphenol 1.0


-ug/lND NDPhenol 1.0

-ug/lND ND1,2,4,5-Tetrachlorobenzene 3.5



-ug/lND ND1,2-Diphenylhydrazine 1.6



-ug/lND ND2,4,5-Trichlorophenol 1.0

-ug/lND ND2,4-Dichlorophenol 1.0

-ug/lND ND2,4-Dinitrophenol 1.0

-ug/lND ND2,4-Dinitrotoluene 3.5

-ug/lND ND2,6-Dinitrotoluene 3.5

-ug/lND ND2-Chloronaphthalene 3.5

-ug/lND ND2-Chlorophenol 1.0

-ug/lND ND2-Methylphenol (o-cresol) 1.0


-ug/lND ND2-Nitrophenol 1.0

-ug/lND ND3&4-Methylphenol (m&p-cresol) 1.0

-ug/lND ND3,3'-Dichlorobenzidine 5.0

-ug/lND ND2,4,6-Trichlorophenol 1.0

7.5 15-110Surrogate: % 2-Fluorophenol 53 ug/l 53

5 30-130Surrogate: % 2-Fluorobiphenyl 63 ug/l 63

7.5 15-110Surrogate: % Phenol-d5 59 ug/l 59

5 30-130Surrogate: % Nitrobenzene-d5 67 ug/l 67

7.5 15-110Surrogate: % 2,4,6-Tribromophenol 69 ug/l 69

5 30-130Surrogate: % Terphenyl-d14 64 ug/l 64


50 2015-130ug/l41.78 844-Nitrophenol 1.0

50 2030-130ug/l30.82 62Acetophenone 3.5

50 2030-130ug/l28.07 56Aniline 3.5


Page 223 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8270D

Batch 477196A - SW3520C


50 2030-130ug/l44.17 88Benzidine 4.5

50 2030-130ug/ll11.55 23Benzoic acid 10

50 2030-130ug/l36.79 74Benzyl butyl phthalate 1.5

50 2030-130ug/l30.77 62Bis(2-chloroethoxy)methane 3.5

50 2030-130ug/l24.49 49Bis(2-chloroethyl)ether 1.0

50 2030-130ug/l22.57 45Bis(2-chloroisopropyl)ether 1.0

50 2030-130ug/l39.90 80Bis(2-ethylhexyl)phthalate 1.5

50 2030-130ug/l38.22 76Carbazole 5.0

50 2015-130ug/l27.32 55Phenol 1.0

50 2030-130ug/l36.24 72Diethyl phthalate 1.5

50 2030-130ug/l33.89 68Dimethylphthalate 1.5

50 2030-130ug/l37.18 74Di-n-butylphthalate 1.5

50 2030-130ug/l39.78 80Di-n-octylphthalate 1.5

50 2030-130ug/l26.46 53Hexachloroethane 3.5

50 2030-130ug/l29.81 60Isophorone 3.5

50 2030-130ug/l17.59 35N-Nitrosodimethylamine 1.0

50 2030-130ug/l32.32 65N-Nitrosodi-n-propylamine 3.5

50 2030-130ug/l31.75 63N-Nitrosodiphenylamine 3.5

50 2030-130ug/l37.43 75Pentachloronitrobenzene 5.0

50 2030-130ug/l37.71 754-Nitroaniline 5.0

50 2030-130ug/l39.63 792,4-Dinitrotoluene 3.5

50 2030-130ug/l33.34 67Dibenzofuran 3.5

50 2030-130ug/l28.12 562-Chlorophenol 1.0

50 2030-130ug/l29.33 591,2,4,5-Tetrachlorobenzene 3.5



50 2030-130ug/l32.90 661,2-Diphenylhydrazine 1.6



50 2030-130ug/l40.45 812,4,5-Trichlorophenol 1.0

50 2030-130ug/l38.07 762,4,6-Trichlorophenol 1.0

50 2030-130ug/l34.05 682,4-Dichlorophenol 1.0

50 2030-130ug/l35.21 702,4-Dimethylphenol 1.0

50 2030-130ug/l31.54 632-Chloronaphthalene 3.5

50 2030-130ug/l38.74 772,6-Dinitrotoluene 3.5

50 2030-130ug/l34.62 694-Chlorophenyl phenyl ether 1.0

50 2030-130ug/l32.23 642-Methylphenol (o-cresol) 1.0


50 2030-130ug/l31.23 622-Nitrophenol 1.0

50 2030-130ug/l34.74 693&4-Methylphenol (m&p-cresol) 1.0

50 2030-130ug/l37.64 753,3'-Dichlorobenzidine 5.0


50 2030-130ug/l40.46 814,6-Dinitro-2-methylphenol 1.0

50 2030-130ug/l34.21 684-Bromophenyl phenyl ether 3.5

50 2030-130ug/l38.71 774-Chloro-3-methylphenol 1.0

50 2030-130ug/l36.52 734-Chloroaniline 3.5

50 2030-130ug/l34.66 692,4-Dinitrophenol 1.0

75 15-110Surrogate: % Phenol-d5 38.36 ug/l 51

50 30-130Surrogate: % 2-Fluorobiphenyl 30.72 ug/l 61

75 15-110Surrogate: % 2-Fluorophenol 33.06 ug/l 44


Page 224 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8270D

Batch 477196A - SW3520C


50 30-130Surrogate: % Nitrobenzene-d5 28.68 ug/l 57

50 30-130Surrogate: % Terphenyl-d14 31.32 ug/l 63

75 15-110Surrogate: % 2,4,6-Tribromophenol 55.62 ug/l 74


50 2030-130 2.2ug/l21.79 44Bis(2-chloroisopropyl)ether 1.0

50 2030-130 4.2ug/l23.69 47Bis(2-chloroethyl)ether 1.0

50 2030-130 3.3ug/l29.91 60Bis(2-chloroethoxy)methane 3.5

50 2030-130 7.8ug/l40.05 80Benzyl butyl phthalate 1.5

50 2030-130 19.0ug/ll9.600 19Benzoic acid 10

50 2030-130 6.6ug/l46.93 94Benzidine 4.5

50 2030-130 0.0ug/l28.24 56Aniline 3.5

50 2030-130 0.0ug/l39.98 80Bis(2-ethylhexyl)phthalate 1.5

50 2030-130 5.2ug/l39.37 794-Nitroaniline 5.0

50 2030-130 8.5ug/l36.94 74Dimethylphthalate 1.5

50 2030-130 0.0ug/l36.51 734-Chloroaniline 3.5

50 2030-130 8.7ug/l41.86 844-Chloro-3-methylphenol 1.0

50 2030-130 4.7ug/l32.60 65Acetophenone 3.5

50 2030-130 8.8ug/l41.57 83Carbazole 5.0

50 2030-130 4.3ug/l35.42 714-Bromophenyl phenyl ether 3.5

50 2030-130 8.0ug/l38.75 78Diethyl phthalate 1.5

50 2030-130 9.7ug/l37.93 764-Chlorophenyl phenyl ether 1.0

50 2030-130 6.5ug/l39.43 79Di-n-butylphthalate 1.5

50 2030-130 1.3ug/l39.69 79Di-n-octylphthalate 1.5

50 2030-130 9.9ug/l24.10 48Hexachloroethane 3.5

50 2030-130 3.3ug/l31.20 62Isophorone 3.5

50 2030-130 2.8ug/l17.79 36N-Nitrosodimethylamine 1.0

50 2030-130 10.2ug/l35.76 72N-Nitrosodi-n-propylamine 3.5

50 2030-130 10.5ug/l34.91 70N-Nitrosodiphenylamine 3.5

50 2030-130 3.9ug/l38.95 78Pentachloronitrobenzene 5.0

50 2015-130 15.7ug/l23.41 47Phenol 1.0

50 2030-130 5.8ug/l35.47 71Dibenzofuran 3.5


50 2015-130 10.2ug/l46.43 934-Nitrophenol 1.0


50 2030-130 9.4ug/l44.46 894,6-Dinitro-2-methylphenol 1.0

50 2030-130 4.4ug/l34.56 691,2-Diphenylhydrazine 1.6



50 2030-130 4.8ug/l42.31 852,4,5-Trichlorophenol 1.0

50 2030-130 6.4ug/l40.25 812,4,6-Trichlorophenol 1.0

50 2030-130 0.0ug/l33.93 682,4-Dichlorophenol 1.0

50 2030-130 0.0ug/l35.10 702,4-Dimethylphenol 1.0

50 2030-130 1.5ug/l34.25 682,4-Dinitrophenol 1.0

50 2030-130 9.9ug/l42.43 852,6-Dinitrotoluene 3.5

50 2030-130 1.6ug/l32.21 642-Chloronaphthalene 3.5

50 2030-130 7.4ug/l26.01 522-Chlorophenol 1.0

50 2030-130 3.1ug/l32.76 662-Methylphenol (o-cresol) 1.0


50 2030-130 3.3ug/l29.82 602-Nitrophenol 1.0

50 2030-130 3.3ug/l30.59 611,2,4,5-Tetrachlorobenzene 3.5


Page 225 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8270D

Batch 477196A - SW3520C


50 2030-130 8.3ug/l37.27 753&4-Methylphenol (m&p-cresol) 1.0

50 2030-130 2.6ug/l38.55 773,3'-Dichlorobenzidine 5.0


50 2030-130 8.5ug/l42.87 862,4-Dinitrotoluene 3.5

75 15-110Surrogate: % 2-Fluorophenol 27.46 ug/l 37


75 15-110Surrogate: % Phenol-d5 33.32 ug/l 44



75 15-110Surrogate: % 2,4,6-Tribromophenol 57.87 ug/l 77

SW8270D (SIM)

Batch 477196B - SW3520C

Blank (D05138-BLK) Prepared: 01-May-19 Analyzed: 03-May-19

-ug/lND NDIndeno(1,2,3-cd)pyrene 0.50

-ug/lND NDChrysene 0.50

-ug/lND NDPyrene 0.50

-ug/lND NDDibenz(a,h)anthracene 0.50

-ug/lND NDFluoranthene 0.50

-ug/lND NDFluorene 0.50

-ug/lND NDHexachlorobenzene 0.50

-ug/lND NDHexachlorocyclopentadiene 0.50


-ug/lND NDNitrobenzene 0.50

-ug/lND NDPentachlorophenol 0.50

-ug/lND NDPhenanthrene 0.50

-ug/lND NDBenzo(a)pyrene 0.50


-ug/lND NDBenzo(b)fluoranthene 0.50

-ug/lND NDBenz(a)anthracene 0.50

-ug/lND NDAnthracene 0.50

-ug/lND NDAcenaphthylene 0.50

-ug/lND NDAcenaphthene 0.50

-ug/lND ND2-Methylnaphthalene 0.50

-ug/lND NDBenzo(ghi)perylene 0.50

-ug/lND NDBenzo(k)fluoranthene 0.50

5 30-130Surrogate: % Nitrobenzene-d5 58 ug/l 58

7.5 15-110Surrogate: % 2-Fluorophenol 61 ug/l 61

7.5 15-110Surrogate: % 2,4,6-Tribromophenol 86 ug/l 86

7.5 15-110Surrogate: % Phenol-d5 64 ug/l 64

5 30-130Surrogate: % Terphenyl-d14 84 ug/l 84

5 30-130Surrogate: % 2-Fluorobiphenyl 65 ug/l 65

LCS (D05138-LCS) Prepared: 01-May-19 Analyzed: 03-May-19

5 2030-130ug/l4.596 92Chrysene 0.50

5 2030-130ug/l5.322 106Dibenz(a,h)anthracene 0.50

5 2030-130ug/l4.529 91Fluoranthene 0.50

5 2030-130ug/l4.325 87Fluorene 0.50

5 2030-130ug/l4.543 91Hexachlorobenzene 0.50


5 2030-130ug/l4.739 95Indeno(1,2,3-cd)pyrene 0.50


Page 226 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW8270D (SIM)

Batch 477196B - SW3520C

LCS (D05138-LCS) Prepared: 01-May-19 Analyzed: 03-May-19

5 2030-130ug/l3.573 71Nitrobenzene 0.50

5 2030-130ug/l3.662 73Pentachlorophenol 0.50

5 2030-130ug/l5.023 100Benzo(k)fluoranthene 0.50

5 2030-130ug/l4.650 93Pyrene 0.50

5 2030-130ug/ll1.205 24Hexachlorocyclopentadiene 0.50

5 2030-130ug/l3.960 79Phenanthrene 0.50

5 2030-130ug/l4.698 94Benzo(b)fluoranthene 0.50

5 2030-130ug/l4.306 86Benzo(a)pyrene 0.50

5 2030-130ug/l4.067 81Benz(a)anthracene 0.50

5 2030-130ug/l4.425 88Anthracene 0.50

5 2030-130ug/l3.956 79Acenaphthylene 0.50

5 2030-130ug/l4.006 80Acenaphthene 0.50

5 2030-130ug/l3.663 732-Methylnaphthalene 0.50

5 2030-130ug/l2.985 60Naphthalene 0.50

5 2030-130ug/l4.349 87Benzo(ghi)perylene 0.50

7.5 15-110Surrogate: % Phenol-d5 4.701 ug/l 63



7.5 15-110Surrogate: % 2,4,6-Tribromophenol 7.466 ug/l 100


7.5 15-110Surrogate: % 2-Fluorophenol 4.287 ug/l 57

LCS Dup (D05138-LCSD) Prepared: 01-May-19 Analyzed: 03-May-19Source: CD05138-LCS

5 2030-130 5.5ug/l5.580 112Dibenz(a,h)anthracene 0.50

5 2030-130 6.4ug/l4.845 97Fluoranthene 0.50

5 2030-130 1.1ug/l4.417 88Fluorene 0.50

5 2030-130 9.4ug/l4.995 100Hexachlorobenzene 0.50


5 2030-130 4.1ug/ll1.259 25Hexachlorocyclopentadiene 0.50

5 2030-130 8.1ug/l5.156 103Indeno(1,2,3-cd)pyrene 0.50

5 2030-130 1.7ug/l2.948 59Naphthalene 0.50

5 2030-130 1.4ug/l3.484 70Nitrobenzene 0.50

5 2030-130 6.6ug/l3.920 78Pentachlorophenol 0.50

5 2030-130 5.3ug/l4.868 97Chrysene 0.50

5 2030-130 8.2ug/l5.056 101Pyrene 0.50

5 2030-130 2.7ug/l3.737 752-Methylnaphthalene 0.50

5 2030-130 8.5ug/l4.301 86Phenanthrene 0.50

5 2030-130 5.6ug/l4.583 92Benzo(ghi)perylene 0.50

5 2030-130 7.2ug/l5.071 101Benzo(b)fluoranthene 0.50

5 2030-130 8.9ug/l4.709 94Benzo(a)pyrene 0.50

5 2030-130 7.1ug/l4.341 87Benz(a)anthracene 0.50

5 2030-130 9.7ug/l4.844 97Anthracene 0.50

5 2030-130 2.5ug/l4.116 82Acenaphthene 0.50

5 2030-130 6.8ug/l5.359 107Benzo(k)fluoranthene 0.50

5 2030-130 1.3ug/l3.989 80Acenaphthylene 0.50


7.5 15-110Surrogate: % 2,4,6-Tribromophenol 7.900 ug/l 105


7.5 15-110Surrogate: % 2-Fluorophenol 3.629 ug/l 48

7.5 15-110Surrogate: % Phenol-d5 4.174 ug/l 56



Page 227 of 23109-May-19 16:45


Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD


SW846-ReactCyn

Batch 477480A - SW846-ReactCyn


-mg/kg< 0.05 BRLReactivity Cyanide 0.05


0.47 3085-115mg/kg0.4600 97.9Reactivity Cyanide 0.05


Page 228 of 23109-May-19 16:45

Analyte(s) Column % Breakdown Limit


Page 229 of 23109-May-19 16:45

Notes and Definitions

A LCS and LCS duplicate were performed instead of a MS and MSD. Alpha and gamma chlordane were spiked and

analyzed instead of technical chlordane. Gamma chlordane recovery is reported as chlordane in the LCS and LCSD

c5

A hold time of 24 hours has been set to expedite the analyses through the laboratory. However, the hold time for

Ignitability is not specified within the method other than to state that the samples should be analyzed as soon as possible.

IgHT

This parameter is outside laboratory lcs/lcsd specified recovery limits.l

This parameter is outside laboratory ms/msd specified recovery limits.m

This parameter is outside laboratory rpd specified recovery limits.r

S - Laboratory solvent, contamination is possible.S

RPD Relative Percent Difference

dry Sample results reported on a dry weight basis

Not ReportedNR

[2C] Indicates concentration was reported from the secondary, confirmation column.

The method for pH does not stipulate a specific holding time other than to state that the samples should be analyzed as

soon as possible. For aqueous samples the 40 CFR 136 specifies a holding time of 15 minutes from sampling to analysis.

Therefore all aqueous pH samples not analyzed in the field are considered out of hold time at the time of sample receipt.

All soil samples are analyzed as soon as possible after sample receipt.

pH

Interpretation of Total Petroleum Hydrocarbon Report

Petroleum identification is determined by comparing the GC fingerprint obtained from the sample with a library of GC fingerprints

obtained from analyses of various petroleum products. Possible match categories are as follows:

Gasoline - includes regular, unleaded, premium, etc.

Fuel Oil #2 - includes home heating oil, #2 fuel oil, and diesel

Fuel Oil #4 - includes #4 fuel oil

Fuel Oil #6 - includes #6 fuel oil and bunker "C" oil

Motor Oil - includes virgin and waste automobile oil

Ligroin - includes mineral spirits, petroleum naphtha, vm&p naphtha

Aviation Fuel - includes kerosene, Jet A and JP-4

Other Oil - includes lubricating and cutting oil, and silicon oil

At times, the unidentified petroleum product is quantified using a calibration that most closely approximates the distribution of

compounds in the sample. When this occurs, the result is qualified as Calculated as.


Page 230 of 23109-May-19 16:45

Laboratory Control Sample (LCS): A known matrix spiked with compound(s) representative of the target analytes, which is used to

document laboratory performance.

Matrix Duplicate: An intra-laboratory split sample which is used to document the precision of a method in a given sample matrix.

Matrix Spike: An aliquot of a sample spiked with a known concentration of target analyte(s). The spiking occurs prior to sample

preparation and analysis. A matrix spike is used to document the bias of a method in a given sample matrix.

Method Blank: An analyte-free matrix to which all reagents are added in the same volumes or proportions as used in sample

processing. The method blank should be carried through the complete sample preparation and analytical procedure. The method blank

is used to document contamination resulting from the analytical process.

Method Detection Limit (MDL): The minimum concentration of a substance that can be measured and reported with 99% confidence

that the analyte concentration is greater than zero and is determined from analysis of a sample in a given matrix type containing the

analyte.

Reportable Detection Limit (RDL): The lowest concentration that can be reliably achieved within specified limits of precision and

accuracy during routine laboratory operating conditions. For many analytes the RDL analyte concentration is selected as the lowest

non-zero standard in the calibration curve. While the RDL is approximately 5 to 10 times the MDL, the RDL for each sample takes

into account the sample volume/weight, extract/digestate volume, cleanup procedures and, if applicable, dry weight correction. Sample

RDLs are highly matrix-dependent.

Surrogate: An organic compound which is similar to the target analyte(s) in chemical composition and behavior in the analytical

process, but which is not normally found in environmental samples. These compounds are spiked into all blanks, standards, and

samples prior to analysis. Percent recoveries are calculated for each surrogate.

Continuing Calibration Verification: The calibration relationship established during the initial calibration must be verified at periodic

intervals. Concentrations, intervals, and criteria are method specific.


Page 231 of 23109-May-19 16:45

11 Almgren Drive

Agawam, MA 01001

(413) 789-9018

This preceding chain of custody has been amended to include the client requested additional analyses as noted below:

Laboratory ID Client ID Analysis Added

SC54611-19 TMW-1 SVOCs by SIM 5/2/2019

SC54611-20 TMW-2 SVOCs by SIM 5/2/2019

SC54611-21 DUP SVOCs by SIM 5/2/2019

SC54611-22 Field Blank SVOCs by SIM 5/2/2019

Batch Summary

'[none]'


SC54611-01 (B-1 1-3')

SC54611-02 (B-1 7.7-9')

SC54611-03 (B-2 1-2.9')

SC54611-04 (B-2 8-9.8')

SC54611-05 (B-3 0.4-2.2')

SC54611-06 (B-3 6-8')

SC54611-07 (B-3 11-13')

SC54611-08 (B-4 0.4-1.8')

SC54611-09 (B-4 5.4-7.4')

SC54611-10 (B-4 11.8-13.8')

SC54611-11 (B-5 1.7-2.8')

SC54611-12 (B-5 5-7')

SC54611-13 (B-6 0.4-1.7')

SC54611-14 (B-6 5.6-7.6')

SC54611-15 (SED-1)

SC54611-16 (SED-2)

SC54611-17 (DUP)

1900598


1900598-DUP1

1900598-SRM1

1900598-SRM2

SC54611-01 (B-1 1-3')

SC54611-02 (B-1 7.7-9')

SC54611-03 (B-2 1-2.9')

SC54611-04 (B-2 8-9.8')

SC54611-05 (B-3 0.4-2.2')

SC54611-06 (B-3 6-8')

SC54611-07 (B-3 11-13')

SC54611-08 (B-4 0.4-1.8')

1900599


1900599-DUP1

SC54611-01 (B-1 1-3')

SC54611-02 (B-1 7.7-9')

SC54611-03 (B-2 1-2.9')

SC54611-04 (B-2 8-9.8')

SC54611-05 (B-3 0.4-2.2')

SC54611-06 (B-3 6-8')

SC54611-07 (B-3 11-13')

SC54611-08 (B-4 0.4-1.8')

SC54611-09 (B-4 5.4-7.4')

SC54611-10 (B-4 11.8-13.8')

SC54611-11 (B-5 1.7-2.8')

SC54611-12 (B-5 5-7')

SC54611-13 (B-6 0.4-1.7')

SC54611-14 (B-6 5.6-7.6')

SC54611-15 (SED-1)

SC54611-16 (SED-2)

SC54611-17 (DUP)

1900602


1900602-DUP1

1900602-SRM1

1900602-SRM2

SC54611-09 (B-4 5.4-7.4')

SC54611-10 (B-4 11.8-13.8')

SC54611-11 (B-5 1.7-2.8')

SC54611-12 (B-5 5-7')

SC54611-13 (B-6 0.4-1.7')

SC54611-14 (B-6 5.6-7.6')

SC54611-15 (SED-1)

SC54611-16 (SED-2)

SC54611-17 (DUP)

477139A


CD04771-BLK

CD04771-LCS

CD04771-LCSD

SC54611-02 (B-1 7.7-9')

477188A


CD05119-BLK

CD05119-DUP

CD05119-LCS

CD05119-MS

SC54611-01 (B-1 1-3')

SC54611-02 (B-1 7.7-9')

SC54611-03 (B-2 1-2.9')

SC54611-04 (B-2 8-9.8')

SC54611-05 (B-3 0.4-2.2')

SC54611-06 (B-3 6-8')

477191A


CD05122-BLK

CD05122-LCS

CD05122-LCSD

CD05122-MS

CD05122-MSD

SC54611-01 (B-1 1-3')

SC54611-03 (B-2 1-2.9')

SC54611-04 (B-2 8-9.8')

SC54611-05 (B-3 0.4-2.2')

SC54611-06 (B-3 6-8')

SC54611-07 (B-3 11-13')

SC54611-08 (B-4 0.4-1.8')

SC54611-09 (B-4 5.4-7.4')

SC54611-10 (B-4 11.8-13.8')

SC54611-11 (B-5 1.7-2.8')

SC54611-12 (B-5 5-7')

SC54611-13 (B-6 0.4-1.7')

SC54611-14 (B-6 5.6-7.6')

SC54611-15 (SED-1)

SC54611-16 (SED-2)

SC54611-17 (DUP)

477192A


CD05126-BLK

CD05126-LCS

CD05126-LCSD

CD05126-MS

CD05126-MSD

SC54611-01 (B-1 1-3')

SC54611-02 (B-1 7.7-9')

SC54611-03 (B-2 1-2.9')

SC54611-04 (B-2 8-9.8')

SC54611-05 (B-3 0.4-2.2')

SC54611-06 (B-3 6-8')

SC54611-07 (B-3 11-13')

SC54611-08 (B-4 0.4-1.8')

SC54611-09 (B-4 5.4-7.4')

SC54611-10 (B-4 11.8-13.8')

SC54611-11 (B-5 1.7-2.8')

SC54611-12 (B-5 5-7')

SC54611-13 (B-6 0.4-1.7')

SC54611-14 (B-6 5.6-7.6')

SC54611-15 (SED-1)

SC54611-15RE1 (SED-1)

SC54611-16 (SED-2)

SC54611-17 (DUP)

477196A


CD05138-BLK

CD05138-LCS

CD05138-LCSD

SC54611-19 (TMW-1)

SC54611-20 (TMW-2)

SC54611-21 (DUP)

SC54611-22 (Field Blank)

SC54611-22RE1 (Field Blank)

477196B


D05138-BLK

D05138-LCS

D05138-LCSD

SC54611-19 (TMW-1)

SC54611-20 (TMW-2)

SC54611-21 (DUP)


477197A


CD04789-BLK

CD04789-LCS

CD04789-LCSD

SC54611-19 (TMW-1)

SC54611-20 (TMW-2)

SC54611-21 (DUP)


477208A


CD04790-BLK

CD04790-LCS

SC54611-19 (TMW-1)

SC54611-20 (TMW-2)

SC54611-21 (DUP)


477214A


SC54611-19 (TMW-1)

SC54611-20 (TMW-2)

SC54611-21 (DUP)


477222A


CD05298-BLK

CD05298-LCS

CD05298-LCSD

SC54611-19 (TMW-1)

SC54611-20 (TMW-2)

SC54611-21 (DUP)


477223A


CD05138-BLK

CD05138-LCS

CD05138-LCSD

SC54611-19 (TMW-1)

SC54611-20 (TMW-2)

SC54611-21 (DUP)


477253A


CD04926-BLK

CD04926-LCS

CD04926-LCSD

SC54611-01 (B-1 1-3')

477261A


CD05120-BLK

CD05120-DUP

CD05120-LCS

CD05120-LCSD

CD05120-MS

CD05120-MSD

SC54611-02 (B-1 7.7-9')

SC54611-03 (B-2 1-2.9')

SC54611-04 (B-2 8-9.8')

SC54611-05 (B-3 0.4-2.2')

SC54611-06 (B-3 6-8')

SC54611-07 (B-3 11-13')

SC54611-08 (B-4 0.4-1.8')

SC54611-09 (B-4 5.4-7.4')

SC54611-10 (B-4 11.8-13.8')

SC54611-11 (B-5 1.7-2.8')

SC54611-12 (B-5 5-7')

SC54611-13 (B-6 0.4-1.7')

SC54611-14 (B-6 5.6-7.6')

SC54611-15 (SED-1)

SC54611-16 (SED-2)

SC54611-17 (DUP)

477265A


CD05128-BLK

CD05128-LCS

CD05128-LCSD

CD05128-MS

CD05128-MSD

SC54611-01 (B-1 1-3')

SC54611-02 (B-1 7.7-9')

SC54611-03 (B-2 1-2.9')

SC54611-04 (B-2 8-9.8')

SC54611-05 (B-3 0.4-2.2')

SC54611-06 (B-3 6-8')

SC54611-07 (B-3 11-13')

SC54611-08 (B-4 0.4-1.8')

SC54611-09 (B-4 5.4-7.4')

SC54611-10 (B-4 11.8-13.8')

SC54611-11 (B-5 1.7-2.8')

SC54611-12 (B-5 5-7')

SC54611-13 (B-6 0.4-1.7')

SC54611-14 (B-6 5.6-7.6')

SC54611-15 (SED-1)

SC54611-16 (SED-2)

SC54611-17 (DUP)

477266A


CD05128-BLK

CD05128-LCS

CD05128-LCSD

CD05128-MS

CD05128-MSD

SC54611-01 (B-1 1-3')

SC54611-02 (B-1 7.7-9')

SC54611-03 (B-2 1-2.9')

SC54611-04 (B-2 8-9.8')

SC54611-05 (B-3 0.4-2.2')

SC54611-06 (B-3 6-8')

SC54611-07 (B-3 11-13')

SC54611-08 (B-4 0.4-1.8')

SC54611-09 (B-4 5.4-7.4')

SC54611-10 (B-4 11.8-13.8')

SC54611-11 (B-5 1.7-2.8')

SC54611-12 (B-5 5-7')

SC54611-13 (B-6 0.4-1.7')

SC54611-14 (B-6 5.6-7.6')

SC54611-15 (SED-1)

SC54611-16 (SED-2)

SC54611-17 (DUP)

477274A


CD05046-BLK

CD05046-LCS

SC54611-01 (B-1 1-3')

SC54611-02 (B-1 7.7-9')

SC54611-03 (B-2 1-2.9')

SC54611-04 (B-2 8-9.8')

SC54611-05 (B-3 0.4-2.2')

SC54611-06 (B-3 6-8')

SC54611-07 (B-3 11-13')

SC54611-08 (B-4 0.4-1.8')

SC54611-09 (B-4 5.4-7.4')

SC54611-10 (B-4 11.8-13.8')

SC54611-11 (B-5 1.7-2.8')

SC54611-12 (B-5 5-7')

SC54611-13 (B-6 0.4-1.7')

SC54611-14 (B-6 5.6-7.6')

SC54611-15 (SED-1)

477275A


CD04770-BLK

CD04770-LCS

SC54611-16 (SED-2)

SC54611-17 (DUP)

477276A


CD04771-BLK

CD04771-LCS

SC54611-01 (B-1 1-3')

SC54611-02 (B-1 7.7-9')

SC54611-03 (B-2 1-2.9')

SC54611-04 (B-2 8-9.8')

SC54611-05 (B-3 0.4-2.2')

SC54611-06 (B-3 6-8')

SC54611-07 (B-3 11-13')

SC54611-08 (B-4 0.4-1.8')

SC54611-09 (B-4 5.4-7.4')

SC54611-10 (B-4 11.8-13.8')

SC54611-11 (B-5 1.7-2.8')

SC54611-12 (B-5 5-7')

SC54611-13 (B-6 0.4-1.7')

SC54611-14 (B-6 5.6-7.6')

SC54611-15 (SED-1)

SC54611-16 (SED-2)

SC54611-17 (DUP)

477321A


CD05125-BLK

CD05125-DUP

CD05125-LCS

CD05125-MS

SC54611-07 (B-3 11-13')

SC54611-08 (B-4 0.4-1.8')

SC54611-09 (B-4 5.4-7.4')

SC54611-10 (B-4 11.8-13.8')

SC54611-11 (B-5 1.7-2.8')

SC54611-12 (B-5 5-7')

SC54611-13 (B-6 0.4-1.7')

SC54611-14 (B-6 5.6-7.6')

SC54611-15 (SED-1)

SC54611-16 (SED-2)

SC54611-17 (DUP)

477480A


CD04770-BLK

CD04770-LCS

SC54611-01 (B-1 1-3')

SC54611-02 (B-1 7.7-9')

SC54611-03 (B-2 1-2.9')

SC54611-04 (B-2 8-9.8')

SC54611-05 (B-3 0.4-2.2')

SC54611-06 (B-3 6-8')

SC54611-07 (B-3 11-13')

SC54611-08 (B-4 0.4-1.8')

SC54611-09 (B-4 5.4-7.4')

SC54611-10 (B-4 11.8-13.8')

SC54611-11 (B-5 1.7-2.8')

SC54611-12 (B-5 5-7')

SC54611-13 (B-6 0.4-1.7')

SC54611-14 (B-6 5.6-7.6')

SC54611-15 (SED-1)

SC54611-16 (SED-2)

SC54611-17 (DUP)

477679A


CD05124-BLK

CD05124-LCS

CD05124-LCSD

CD05124-MS

CD05124-MSD

SC54611-02 (B-1 7.7-9')

SC54611-04RE1 (B-2 8-9.8')

SC54611-06 (B-3 6-8')

SC54611-06RE1 (B-3 6-8')

SC54611-08 (B-4 0.4-1.8')

SC54611-09 (B-4 5.4-7.4')

SC54611-10 (B-4 11.8-13.8')

SC54611-11 (B-5 1.7-2.8')

SC54611-12 (B-5 5-7')

SC54611-15 (SED-1)

SC54611-16 (SED-2)

477684A


CD06242-BLK

CD06242-LCS

CD06242-LCSD

SC54611-13 (B-6 0.4-1.7')

SC54611-14RE1 (B-6 5.6-7.6')

SC54611-17RE1 (DUP)

477686A


CD05131-BLK

CD05131-LCS

CD05131-LCSD

CD05131-MS

CD05131-MSD

SC54611-01 (B-1 1-3')

SC54611-03 (B-2 1-2.9')

SC54611-04 (B-2 8-9.8')

SC54611-05 (B-3 0.4-2.2')

SC54611-07 (B-3 11-13')

SC54611-14 (B-6 5.6-7.6')

SC54611-16RE1 (SED-2)

SC54611-17 (DUP)

SC54611-18 (Trip Blank)

SC54611-18RE1 (Trip Blank)

477696A


CD05142-BLK

CD05142-LCS

CD05142-LCSD

SC54611-19 (TMW-1)

SC54611-20 (TMW-2)

SC54611-23 (Trip Blank)

477712A


CD04607-BLK

CD04607-LCS

CD04607-LCSD

SC54611-20RE1 (TMW-2)

SC54611-21 (DUP)


477836A


CD05158-BLK

CD05158-LCS

CD05158-LCSD

SC54611-11RE1 (B-5 1.7-2.8')

477847A


CD05277-BLK

CD05277-LCS

CD05277-LCSD

SC54611-20RE2 (TMW-2)

TASK 210 – SUBSURFACE SITE INVESTIGATION ......Task 210 – Subsurface Site Investigation -2-...

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Transcript of TASK 210 – SUBSURFACE SITE INVESTIGATION ......Task 210 – Subsurface Site Investigation -2-...