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41 bCi.S~~ <; s {l.cA£'\. i I

' ' I

\)1 ' o'\ Srfi{ I

l(3 l; ~

t\ 5tzrt( I \ r, ! l lJW I t

1 \ ll ~ ~~ . ! l_!l\.. 0"\_

4Cf bu.iUd r-J1 t\v;.:r 5?C""l'{ :JCvi'\J. 1 ! ~:., (..~ C~p p-:'Cv' S. I

U: l¥vf. bd,j 5vt--f. 1) r c. v.. ts1 c{( fn:r" l;f, 5.

5o S. ct Hcl~ \)\0-.t-~ S~"-- ., 5 .--"' vc I ~~ VIJ;n {v\ScMC

'I &v?{5/ ~

s I \,\ I'

'Sl~us) +vw'~C.h . ,. I

\o1r1 l $. rfy 5Cctrv/ l.J ( -J/ " S] (. (\;·; (_,( f1 ; (_ cJt.•r!f :>'t' .... ' ,, J.SV Iced

Page 17: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

XRF LOCA'ttON INFORMATION for

SURFICAIL SOIL SCREENING

Site: C& H Tamarack Operations Date: ___ l 1_.-_S_· _\ ;l __ _ Page5 of_JJ_ ,I f

Operator: _ _.._,:.:..:"_.,_ __________ _ ;,All I 111 1\ Data Recorder: !=wtvt-itv•>v v 1

XRF Location Run# Desimation Material Description Photo# GPSed? Comments (SS sample# if collected, hi<>h metals, etc.)

53 j (C,{ {6 ~'-' "3qD ~ Cv15C',11 c ~u::zsk I)! 1-c_ 1\cl > '

... ll v L"': biq I

<; ." ~0-t\.C\ I. II p )I \ n~: 11iG I '

v.J 6f b!A.j 5iCcj I ' 55 . ..,. \1 1' Uz /f't:e{

Js c.l-t> e, u c. ..., fJ

,, (' •I s G ' ; I 5/Cq t-/!7 ((V t( 7.:-7. ~iS!' L-t-C

5~ ,"1/1 I Vi \.0 ~ I SS--05

tu I 57 cf bl c1 ?: "5 tecc; J c-r cvdt l 10~

') (LYSU'\ i{_ 7l(7 ' ' ktcd

7S f\1\'-J 0~ blat: C; .)

10 vt! . 5 CvtY/ . IS7// I h ) .. u:ae-1 5 7 O.,:S ~.-./~-_} ,

51 J,c. i1 ''

•'I'- s, 1 k/ 5twu! ' I

'tr, I 1--C . P' l;'(_(j( ))C. I \ C I','· 1 I v

,, (\().~(.. I

u - -f-p ~c,! \<>\ t-Cf- CvJ -J-,

' ' -:P~NI I (;) ,, I ~ .

"": ,, 71frV:-'j i'". ,., (·"

! •' i \ (/; b(J")?.-t'j I

lcpJ' (,;3

\Vt I" '

{!O..C!e..- Ul r !'\ 1 1 SiiH SCvtct\

(:;lf ~~ot(~h '' • I

i rJ n~, . tt:

., 0(_1)/L.,

bus' ·r>~(tA1~0 s. r ~ ... r SCL-f'1 vr · It Cv\5e 1V c

06 f0 \.lN\c..hr- 0' (': C; \) ((,''"'' <:) S{i..r\C\. if, ec v..i ~ I/ l cl (~I)" r\i L

\ _; l, ,,,· i v l ' v [,'

Page 18: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

XRF LOCA'ttON INFORMATION for

SURFICAIL SOIL SCREENING

Site: C& H Tamarack Operations Date: /[ · S • JJ_ Paoeb of l I "- --1 I Operator:_..:::~:::-::..;C:..;,.o?__.:__ ________ _ Data Recorder: /~ f-r .. J.A/1 I 1

XRF Location Run# Desi'!llation Material Description Photo# GPSed? Comments (SS sample# if collected, hioh metals, etc.)

w qf bltr'J ''' ft-wr0~h'r,.._

1 f

' ' ' b!au( (v) sc,/

!G \ h

71 '\

, , r J'-..i . Ct

\ll tt'Y-

17 \' v

l7

Page 19: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

XRF LOCA'l tON INFORMATION for

SURFICAIL SOIL SCREENING

Site: C& H Tamarack Operations Date: I I· S · lv-. Page 7 of_l _l I

Operator:--=~\ r..........=C,~----------------- Data Recorder: / --~~~---------~t }._ J..--/1 J Y)

XRF Location Run# Designation Material Description Photo# GPSed? Comments (SS sample# if collected, hi~h metals, etc.)

N c,f Ci ( C\

cf P 1 I ({'__.,r') Ql'l s i · !~f ~V\,J

<?0 . ;',Lv

I -.

f}[ .c( ,, ' ( J ' [ Jt - '- J I

( V\)

'5 1 ~ , \ ,..

vlc-'r c- \)I.e,~ C. j . j_ itv\ C.( ., vd S

~J_ f\J .. :~\ fA_~ l \ i-< k3 c-/+-· J

<D ! l I' I ' ;;r· 1\ ll\.. tl

1SY , \ \ l S · u.,·sh'"J I l' \ /

I I ~5 {:; ka~ c ---'-~- /--~.1 - "

<6~ I \ \ ' i --:1 v . r I ~~(; A L. I

S1 . r - ('( t\ iS h \? t"Z,WY" 'S ~-"'£~

"· :~'(_...:,{"~ ...\... ' i Y\,~ lii.,L I ~~ t' b (~ L-- Y\ k r~·· t. st££( I lbJ \fad ~q ., (il f\~Y . ((.~'

\ VI) c' ?h. 'o {t . l l v-J\ i I 1] tl

' S ~Cvf'.t

, h( 0C (\. 6{ (,\.,\ i\.--0

. ;, ~; I c;cvi'\U· 1 1\ S. tic f-r tf ~ri 141.

r. "' ~0~ '\ ftlG{ 55-0b 0\ ". o-f tt.ri -1e b (' f\ C:i11-'{ sttAVI. r

\\ '1. -\T ~c k... ,J fJ '(a. Jet ~

Page 20: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

XRF LOCA 1t0N INFORMATION for

SURFICAIL SOIL SCREENING

Site: C& H Tamarack Operations Date: J I· b·f d Paoe ':S of ~--

!l Operator: ~ (T( __. Data Recorder: .dt..l k}l (\ XRF Location Run# Designation Material Description Photo# GPSed? Comments (SS sample# if collected, high metals, etc.)

Yi Nt:. cA- b 1'\ \ ~i t ~ ~ c._, ~..t-'- \j \) i\\c\.,<,

q~ I' ~ ( \". s t'l ~ s c.:.,,~\. I

CJL\ I \ ~'

05 (\, 1\jf (.' '(:

l\

\); l\c:.{', I \ \ \ \eo .. c( ss-oq N cl p,·llaAS q~ 5 n:\ vt.(

1 S ;If 1( SCL M{ I

((7 \ \ b ,,, fv\J:..IiL .SC:L V\C"\ I J~S \ f.t{ d S5-\~

cys f\e~.+ -b S l ,_J IL_ru ~ ~ s tU u "" '<- ·~ h( ":£u .. h~-'-\ I i 10 1-eu'-J

tjtj \~ brt'\ Si '+t ~u.~"t{ \ \~~ lee{~

/Cb l\.<"-~ ~ \I Cf, ~( \\ ¥\t) \

\ c \ ~ N\{Al\ o \ \c ;-.., . :,( ~ i.!'a-rc.,

l\ I ct rai 1\0.1) e

\ DJ. b(Y\ '' i)cL s· ··"

e C.C.j ~ ~.-+ lb3 rcwi\£\C.. \-1 \ Lf L{ I ('t{cl

(1\

\I'\'); c\.e (\1\..\.--0>--'L•-A 1~0 <. L \L> l.l 22~··1 T7'1 .(1; lA.A\ t"\Ct ~·ur- 21 1'\l.-s~ l .... ,h.! sc..h- t w \ ec J S s.s- 0~

Page 21: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

XRF LOCAl' tON INFORMATION for

SURFICAIL SOIL SCREENING

Site: C& H Tamarack Operations Date:_ ....:.\...:...\ ·_G_· _f :;-~-- Paae of (/

J ( ( 1:>

l ---r- I

Operator: Data Recorder: .; -il,~_ '"1-L-n '\ 1\

XRF Location Run# Designation Material Description Photo# GPSed? Comments (SS sample# if collected, high metals, etc.)

~~h' ~ I

IDCJ i h( 5 C<--1-~ I (\1\. \I\;.. It:(. fL..

...; 'il c,._ '/ bGt kcltf ~ (\;\.Sen l t.-h/~ vs--r~ ~\L l"Yf\ $11 hf$1'-r"ld

IO~ I Jti~ !tad tv I

\tl cF- P~·Ha..s ~ \'"" Y\ ? ,· I hi ~

b.,, ("-Cl..,r\(:1

IC~ ftn;..,..ttW h't/\. l \

153 1 rat(

\L o \' il

llC i' (I

~pcf I

:3 re cf\ ct\ --

j) 'p s \J~_J\-Sit:- ~lc~7&L \ll>Ct l:v\M\ [tt: ~ VI~ ~t'C1.v0l , SC<..r"~.d 103'=' le~-4 l :,57~ ~ni~' \J\~~ I 1\ l

-\hl\..1\' " 3 ~ClC (6 '"W !fo-r ~( ll i I J

' I) V'

tz; ioo \-~,~c ·tt2 (et0 3tf (.,1 sc ·1·· ( ,.vn tt-(~'0-.. " " . s 'c1.., c1 )t~

tv o-1- (- '{.... b 1 1'\ t; i I fy S t •._t\(( I

)\7 -s~~"'rs ). 06 lto.d

IIY t.~~ CJ- tC\ 1\ s·~ \~'\ S C~nd <> G\rl\\)s

117 ,, \; ,-" ~ r&\ ~-<.\ .!. t;c-.1~ \0 o-\- !'A, ll \;\c~ Sil~ SCvf'l~·

II~ \--w "'1 ~ , (•"n; C,.r - . .111 l-e.t-~.tf ct h( 117 t$rl\ Mi 11 ~ \:J ;-f\ Sl I s tvr-.4

fc vvl\t;\_&; fi,l\ --v l3fc (tt{d

Page 22: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

XRF LOCATION INFORMATION for

SURFICAIL SOIL SCREENING

Site: C& H Tamarack Operations Date: \ \ 6 ·j ;L Page~of_l t_ I , f\

Operator: ... )( i Data Recorder: r-(tt~ I (l

XRF Location Run# Designation Material Description Photo# GPSed'? Comments (SS sample# if collected, high metals, etc.)

1\,L( /I ~if! t. b lc.__t-t.. <;; h.\ UC6 5' CA/V) 'f '133 ~ ' L-f 4A ;2 7 6 ti r-s r n i 1. s~ ~ \O l\9

I ~ I'

...- ...v. A - ...... ~l0'0 u cd )-l(p CV')C(\ iL

IU f\IL "~ fK \J~1\..;i1 1'-/ SCt.,'\4 -cc.. tl f'v\ i (( Jtc~ L

id-1 /l \\

IJ.d- .N . I. ~ '"' i tl I\ J'Al \'\..(. C(. (j( j-((0. C\:t I. t\_

,'1 ..., I CtL ~~ s~- \\

\J , r ' c\1 t :;;--? \) lr\ ~ . ' ~ 'i Sw,.y} I So & ltaA ~~ CltSC: n I t. 55-13 \)~ t' \' . . -

1 ).~ ) \ J' L\10 J) b 47 A0 N . ~ ~ (.. ,+· or k I

I )~ ct t ... IAL

l 0 Si/ ~i.-rd )

\}'~ ,, " ~~s " I

1J.cl 6'Yl " 'j e:.. '' Jl

13 (, -JJ

--

Page 23: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

XRF LOCATION INFORlVIA TION • t _)

~,

Date: \ l b /J.. Page_U_orJL ~!{' Oper·a tor:_'-_.;:;;J ..=;..u_,L...:::::'--------- Data Recorder: Jb . I hAO\X\

XRF Location Run# Designation Material Description Comments

I 3 I 130(

133

) 'J L/ 11>\ (· f ~\; , tl pde - J-0 ~t{A tf '> h 1 l d ~. VHI\ Sd I" C,CtN( s ("

hI /'}t-, k\ I llt - )

13S c\ )L b YV\ -:; 1 I t'( 'S c.<.k-,c,/

I IJ 3~, s.J~uy' j ) sc:L.A'\ A

13 7 ~J . o-F 'bl~ ~· , · I~~ ~ct--¥1.£ \. ,c)") C\[c e~-::; ~( {_) !

I 3'? £ (;o( rd. ' 0/r I ' ' ' Tv p of h . ill

13(7

f lf 0

Jl(/

J ~J_

llf 3

!lfq

/(/5

/l/0

{q7 JW 5/23/02

\

Page 24: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL SAMPLE DATA SHEET

Site: C&H TMIARACK OPERATIONS MID#: M1N000510835 Date: _ _,_._\ )_· (p__;_f :A _ _ Sample Location:-"'S=S____,.O£..... ~-'--\ ______ Weather: __ V~(.u..L..._t "'--'l\'-\.,_3....~....~.u.__<-_ _______ _

Field PersOimel:_..::::..__~\C~..~-;-....~.,(,..L, ______ Data Sheet Logger:_--:~-JtJJ--\--'<.\.>..J.b-"'1""""1 ..... D_._./'-'-1 ______ _

Sampling Time (MT): f f. ., : !J -!J Depth/Intervai:__,V'--"O=A~-_ -y--'--•< _ _,R=e=m=a=in=d=e1,_· __ () __ ~-{' __

Soil Cover: _ ____.__\ f _,_0"--L~Vf.'----=-'5"--. 4--l _,_h_u _i-:::Jtj""""""5 __ ( sand, grass) # of Samples Per Location: _ _ .___ __ _

Sampling Method: Grab: __ / __ _ Composite: _____ _ (Check all Surface Sample: Deep Sample: _ _ __ _ that apply) Trowel: ;;r-- Hand Auger: _____ _

Other (explain): _____ _________ _

Collected I# of Vials Co~ected I# of Jars Collected I# of Jars Sample Type/Bottles: ~VOA _ I _ _V_~SVOA/Pest/PCB _L_ ~Metals/Cyanide_\_

Location Reference Features: 1 ..-Landmark # l: C\ ( ( fS ~ \ (_ {l...£1 Direction: __ -=f::=--___ Distance: _ ____.3'-f-----+-Landmark #2: __________ Direction: Distance: _ _____ --.

;J

1 Soil Unit Thickness Unit Description (continue on back ifnecessa1y--->) PID Reading

(in. or ft.) (moisture, color, grain size, etc.)

~flO IS r ckK- 0 VYl ~ CU\t-l f )n f SC> > J /vLO.J ;-5 reti.Jish ),;y" s "+y ~n lv YJIU) ~'~ 'VI sc,n Ll T'( \ tt . h'et u ,~ crlJ h

Gravel - coarse 314 to 3 in. fine 3116 to 314 in.

Sand- coarse 2 to 4.75 mm. medium 0.425 to 2 mm. fine 0.074 to 0.425 mm.

Silt/Clay <0.074 nun. (use plasticity)

Photos: YIN Time of photo: l~· l({) #/Location:_J__Direction of photo: VV Photographer: .J {_rf._

RENU~S: ____________________________ _

(JW 12/9/09)

Page 25: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL SAMPLE DATA SHEET

Site: C&HTAMARACKOPERATIONS MID#: MIN000510835 Date: \ \. rJ \ ~) "·cc/l!i\ ('\( -~ ?·-L· Sample Location: SS Qct= '). ).)V :.7 IJ Weather: . )LA:&~\ :> 7

Field Personnel: \t; c ·I Av\ ·tvl \)1\ \r; Data Sheet Logger: L\ IA.:\IA -n-1 f\ Sampling Time (MT): I\\ d -~) Depth/Interval: VOA- />1 '\ Remainder- (j - cr Soil Cover: \fG\ ~I' c)\ c:{t fVi (sand, grass) #of Samples Per Location:_--t----

Sampling Method: Grab: ___ /_·___ Composite: _____ _ (Check all Smface Samp~-- Deep Sample:----,.,----that apply) Trowel:_-"'--/___ Hand Auger: _ _,IW:_:_ __ _

Other (explain):. ______________ _

Collected I # of Vials Collected I# of Jars J:t_

Collected I# of Jars , 1 Sample Type/Bottles: _L VOA __J_ _LsvoA!Pest/PCB ~Metals/Cyanide_!_

Location Reference Features: Landmark #l: __________ Direction: _______ Distance: ______ _ Landmark #2: Direction: Distance:. ______ _

Sketch:

__ / " \)~\t )

•-J

,'-' \)

Soil Unit Thickness Unit Description (continue on back ifnecessmy--->) PIDReading (in. or ft.) (moisture, color, grain size, etc.)

CCY~ r'v~ b vC<vYl Si \)~ I,, la 1\V~ Seer-vi tJ J r)(/1\_(

C\.S~ 1 \,ucod, Stt1cj 1 reD I')

Gravel - coarse 314 to 3 in. fine 3116 to 314 in.

Sand- coarse 2 to 4.75 mm. medium 0.425 to 2 mm. fme 0.074 to 0.425 111111.

Silt/Clay <0.074 mm. (use plasticity)

Photos! 'Yif'l Time of photo: \\,11 #/Location: J-- Direction of photo:") Photographer: ... \cr, \. /

REMARKS: ___________________________ _

(JW 12/9/09)

Page 26: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL SAMPLE DATA SHEET

Site: C&H TAMARACK OPERATIONS l\1ID#: MIN00051 0835 Date: ) \ /:) I)

Sample Location: SS 03 AA S I !\A) i) Weather:_C="-'-'l0'--1 =ll""C'-'-( '+/-:S~7L__ ______ _ Field Personnel: \ )ce_.;t .ihdtt:IYJ n Data Sheet Logger: ;\JA +1-LIJ1 Y\ Sampling Time (NIT): \l • 2- 7:J Depth/Interval :_,V,_,O"'A~-_LJ_,_' ' _ __!R_,e"'m"'a"'in"'d"'e"--r =-------'6"'. '-----tb=::.-__

Soil Cover: ){til \/f S (sand, grass) #of Samples Per Location: _ ___,c__ __ _

Sampling Method: Grab: / Composite: _____ _ (Check all Surface Sample: __ Deep Sample: _____ _ that apply) Trowel: v Hand Auger: _____ _

Other (explain): ______________ _

Collected I# of Vials

Sample Type/Bottles: ---1--Co9ected I# ofJars L Co)lected I# ofJars Ll

VOA _I_ 1 ~SVOA/Pest/PCB ____:I_ V Metals/Cyanide~

Location Reference F eatur~s: Landmark # 1 : __ ""tv\+--;z:J:..J__IQ"----_____ Direction: __ _,t;;=--____ Distance: Landmark #2: Jbd fv\d@ rg , Direction:_~S,"'' .,----Distance:

Sketch: _ -1 ~ ~\\ I

-+= -~~ --~ I!W--J\cl~ I

~ Vl" '---<::::/ tY --_ 4-.)- SS-b3 \\:,) 'lJ ~r / ~ -~ \

'-~I l \\ k_·,

&tJJYr(~cL(&_, ____ /\ Soil Unit Thickness Unit Description (continue on back ifnecessmy--->) PID Reading

(in. or ft.) (moisture, color, grain size, etc.)

v. 1\1\ois} b\civK 0Y1CGntc S;li 'i Swnti, /ok of \' C6l·"J

Gravel- coarse 314 to 3 in. fine 3116 to 314 in.

Sand- coarse 2 to 4.75 mm. medium 0.425 to 2 mm. fine . 0.074 to 0.425 mm.

Silt/Clay <0.074 mm. (use plasticity)

Photos: ~ Time of photo: \)::J,:i#!Location: d Direction of photo:_hl_Photographer: j 0 t...-

REMARKS: __________________________ _

(JW 1219/09)

Page 27: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL SAMPLE DATA SHEET

Site: C&H TAMARACK OPERATIONS MID#: MIN000510835 Date: t}<J ) Q. 7

S~ple c ~~. I' I' t· l . ~/· I -z

, . Weather: '- (; 1 t~ 7 •

Location: SS D, _

AtJ ,

h ... , 'f I .-.... J >

Field Personnel: J -J 1)1!1 Data Sheet Logger: I I l d u m 11 Sampling Time (MT): _ __[__j_u._

ll.\-,- ---'-"'----Depth/Interval:_cV'-'0'"-'A"-"--I 0 ~_L__ J '' __ R~em""a""in,d,e"-r c:.· ~O.LJ _-____!_j_,~J'---I c _

Soil Cover: .) c:)('-. l. 1 0 (sand, grass) # of Samples Per Location: _____ I _

J / Sampling Method: Grab:_____ Composite: _____ _ (Check all Surface Sample:---:_ Deep Sample: ____ _ that apply) Trowel: / Hand Auger: _____ _

Other (explain): _____________ _

CollJIC!ed I# of Vials Co9ected I # of Jars \ Coi\!J<:led I # of Jars Sample Type/Bottles: _V_VOA __L VSVOA/Pest/PCB -- -- _vM_( etals/Cyanide_l_

Location Reference Features: Landmark #I :_----J-!/)'\-t-'~'"'l"'~vL' _____ Direction:_----""f:-'---___ Distance: .Job ila1d$ Landmark #2: b \ c( {) Direction: Distance: "1 ' 01 ) 17 r {( .1 c; I~ I . Sketch:

c:;c;-6~

[J - ~~ 1·v. l!j. r·'G)

._J

Soil Unit Thickness Unit Description (continue on ba~k-itnecessary--->) PIDReading (in. or ft.) (moisture, color, grain size, etc.)

o-. s m c i ") +- elf( r ( i;s h lnJI] 5i I ly '5 (G/ lti'l j'rtU d

( n) sJ u d m n Li___- ro L /c

,5- I ,5 /Y1Q 1 Sf 5 rt t'/l!Sh y iri( s/ uttj ' c !11tdt-[/ied

(f 0 )J) i' '\ /{)) Yt' (il S t<.-lltl C (_, Gravel - coarse 314 to 3 in. · / · fine 3/16 to 314 in.

Sand- coarse 2 to 4.75mm. medium 0.425 to 2 mm. fine 0.074 to 0.425 mm.

Silt/Clay <0.074 Illlll. (use plasticity)

Photos: YIN Time ofphotoY{t1 #/Location:__:d_Direction of photo: l{} PhotographerJl)c _

REMARKs: on t very Cl u<Je. p ncr }o 5tli11o/, I

>1iJ. 4

J olfr'-t

c){LJYJ p /0 lvG! S bJut. · (JW 12/9/09)

Page 28: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL SAMPLE DATA SHEET

Site: C&H TAMARACK OPERATIONS MID#: MIN000510835 Date: J/. j );) Sample Location: ss OS Weather: c ( (j H cl \1 >, <Z)q D

Field Personnel: J ( f -1 Au ~~UTl/\ Data Sheet Logger:.~'-A-'--u."-'-'-~-"-[,"-G ul 1w1LJ!l-'-----~,--------SamplingTime(MT): /5,/ 1/ Depth/Interval:VOA- ).'' Remainder- 0- '7 Soil Cover: 5\C\Pj (sand, grass) #of Samples Per Location: __ _.:_/ ___ _

Sampling Method: Grab: __ ~"----- Composite: _____ _ (Check all Surface Sample:---+- Deep Sample: ____ _ that apply) Trowel: ___ \/__ Hand Auger: _____ _

Other (explain): _____________ _ ;

/

Colle~ed I# of Vials Sample Type/Bottles: _v_

Co)lected I # of Jars . _I _ v

CoUected I # of Jars 'VOA SVOA/Pest/PCB _V_!Metals/Cyanide _L

N

1 Soil Unit Thickness PID Reading

(in. or ft.) (moisture, color, grain size, etc.)

V. l'Yl o l '?-1 tLK Ia VJ'l S i/ hj ) a 11d 1 S So 11,d , (f tl L,t}l Dvu<-Jtp cl JiVLLFL-( rtH t ( SIC-·<)

Gravel - coarse 314 to 3 in. fine 3116 to 314 in.

Sand- coarse 2 to 4.75 mm. medium 0.425 to 2 mm. fine 0.074 to 0.425 mm.

1) ~() I-tt I y,·chv\i ~ilt/Ciay <0.074 mm. (use plasticity)

Photos:~ Time of photoy:); ]()#!Location: d· Direction of photo:__i{_Photographer: At__.... REMARKS:

I ICO)L,)1q \J tJhGcw1·n7 ?o~NtvJ1?~'-

(JW 12/9/09)

Page 29: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL SAMPLE DATA SHEET

Site: C&H TAMARACK OPERATIONS MID#: .tv!IN00051 0835 Date: I ) /; / )_ Sample Location: ss {) (') Weather: C-io r,u{ LLS O_C tJ fY1~ Field Personnel: . \Lf '-' JnJ· Data Sheet Logger: /blf;Lf)1/L Sampling Time (MT): {) Cf {) (1 Depth/Interval: VOA - 3 1 1

Remainder- o-~

Soil Cover: ) fCl v'f S, ~JcQ d~ (sand, grass) #of Samples Per Location: __ __,_/ __ _

Sampling Method: Grab:_-----"V'---- Composite: _____ _ (Check all Smface Sample:L___ Deep Sample: ____ _ that apply) Trowel: / Hand Auger: _____ _

Other (explain): ______________ _

Collected I# of Vials Collected I# of Jars Collected I# of Jars Sample Type/Bottles: ~VOA _L_ ~SVOA/Pest!PCB _/_ ~Metals/Cyanide _L

Location Reference Features: / J r~/l/') j Landmark #I : _ __,__,\YI'-'-' a->12'--.,-------Direction: __ J.L_ ____ Distance: _ _,J;:-L"-'·""'---:----Landmark #2: p j liM 5 Direction: Distance:_-"~i"-'G'"'-.·, ..... ' _1

__ _

Sketch: ''~cf r lIt( --.....~.------.. __ ~ N

{c~

\ ~1~~ /

~,r Soil Unit Thickness Unit Description (continue on back if necefsmy--->) PIDReading

(in. or ft.) (moisture, color, grain size, etc.)

Gravel - coarse 314 to 3 in. fine 3116 to 314 in.

Sand - coarse 2 to 4, 7 5 mm, medium 0.425 to 2 mm. fine 0.074 to 0.425 mm.

':-;; Silt/Clay <0.074 mm. (use plasticity)

Photos: YIN Time ofphotoJY16"'1#lLocation: ;}-- Direction of photo: S (, Photographer: J (r{' REMARKS: __________________________ _

(JW 12/9/09)

Page 30: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL SAMPLE DATA SHEET

Site: C&H TAMARACK OPERATIONS MID#: MIN00051 0835 Date: /{· b ') d Sample Location: SS () ~ Weather: S 'n D W l .qfj 3.i Field Personnel: , \(;'e. ; fiV._ h1 y() {\ Data Sheet Logger: )tt.d1A..m n Sampling Time (MT): 6?;!J6 Depth/Interval: VOA- 5 '' Remainder-

Soil Cover: '3aJi/ (sand, grass) #of Samples Per Location: __ __:_ __ _

Sampling Method: Grab: __ / __ _ Composite: _____ _ (Check all Surface Sample:__ Deep Sample: ____ _ that apply) Trowel: __ \/___ Hand Auger: _____ _

Other (explain): ______________ _

Collected I# ofVial_y Collected I# of Jars / Collected I# of Jars

Sample Type/Bottles: _j_ VOA V _LSVOA/Pest/PCB_V_ VMetals/Cyanide_l_

Location Reference Features: Landmark #I: ~ \Of.J Direction: S Distance: Landmark #2: t\-;}.. ~ Direction: Distance:

Sketch:

l t,· /1} tl .:::--':.'~~ ~-

-t<J ~ ~~o' ~\:tiP:" \

. ·. I'V\- ;).(t,

r::l \ .. 1

. D .. b k'f Soil Unit Thickness Umt escn tlon

~~lh.\ contmue on a 1 necessar ---> PID Readin

(in. or ft.) (moisture, color, grain size, etc.)

rY\OIS t d%.- brfl 5 t'l fy ~a U '(! /1 !~(}

1 6 vfi/'J- ~ (f 'U( #--

Gravel · coarse 314 to 3 in. fme 3/16 to 314 in.

Sand. coarse 2 to 4.75 mm. medium 0.425 to 2 mm. fme 0.074 to 0.425 nm1.

Silt/Clay <0.074 mm. (use plasticity)

Photos: YIN Time ofphoto:c.&4D#/Location:.,)_ Direction of photo: S Photographer: Joe. REMARKS: __________________________ _

(JW 12/9/09)

Page 31: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL SAMPLE DATA SHEET

Site: C&HTAMARACKOPERATIONS .Mill#: MIN000510835 Date: _ _..:.../ _J_. b __ J ...:....) __ _ 7

Sample Location: SS () cb Weather: __ ~.:._(_\. _1 }-=-1\-'-___,~.3__,]'-----------­Field Personnel: .... ~(!f '1 .A-uhLJ1~ fl\ Data SheetLogger:----¥/___u.YLa..l ......_Ht~l:...~..r'J../..L..l..lf\~------

' (J r:. 1

I\

Sampling Time (MT): I 1 0 Depth/Interval: VOA- ' l Remainder- o -· 1

Soil Cover: YV\ l 1'\.t VO C-(L (sand, grass) #of Samples Per Location: _ ___,_ ___ _

Sampling Method: Grab: __ J __ _ Composite: _____ _ (Check all Surface Sample: Deep Sample: ____ _ that apply) Trowel: ~ Hand Auger: _____ _

Other (explain): ___________ ___ _

Collected I# of Vials Collected I # of Jars Colh:cted I# of Jars Sample Type/Bottles: V VOA _ I_ V SVOA/Pest/PCB _~.-_. Metals/Cyanide~

Location Reference Features: Landmark #1 : __________ Direction: _______ Distance: _ _____ _ Landmark #2: Direction: Distance: - - -----

Sketch: N

j -

- s ---.. 0\ \\~v( - \

Soil Unit Thickness Unit Description (continue on back ifnecessa y--->) PID Reading (in. or ft.) (moisture, color, grain size, etc.)

0·- l j\,\( I S

s -1 \J r 11 S /1 ~ ' / (n f-v { C.)C1A .~ e S .vL t\tl

c~vvu cJ,o.)..r I ( (! L(.S lvti (( {. /(. "' ,Lc h I I ~ ' tj (tis~ jvl.L f-c,(J e ~c I

Gravel - coarse 314 to 3 in, fine 3/16 to 314 in.

Sand- coarse 2 to 4.75 nun. medium 0.425 to 2 nun. fine 0.074 to 0.425 mm.

Silt/Clay <0.074 mm, (use plasticity)

Photos: YIN Time of photo: \\ , Or) #/Location:_J__Direction of photo: ,) · ~l) Photographer: j{f

REMARKS: ____________ _________________ _

(J\V 12/9/09)

Page 32: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL SAMPLE DATA SHEET

Site: C&H TAMARACK OPERATIONS MID#: MIN00051 0835 Date: } f . b J :X Sample Location: ss ~ ocl Weather: c ( 0 Ltd ,( ' -1') 3 t

Field Personnel: J l:C "-1 A~~ -kr 111

u n Data Sheet Logger: rA ~l t-(,l n'l V\

Sampling Time (MT): \0. 0 Depth/Interval: VOA ~ \I\ Remainder- a -d-.. Soil Cover: \-e l~ ve s I bJ I CJ L'/ (sand, grass) #of Samples Per Location: __ ,__ __ _

0

Sampling Method: Grab: / Composite: _____ _ (Check all Surface Sample: that apply) Trowel: v-

Deep Sample: ____ _ Hand Auger: _____ _

Other (explain): ______________ _

Coli)-Cted I# of Vials Co!Jected I # of Jars . Collected I # of Jars ) Sample Type/Bottles: _V_VOA __L _ V SVOA/Pest/PCB _l_ __ VMetals/Cyanide _ _

Location Reference Featuresi .. Landmark# 1: C Dl\ ( I~"{,_ t{, P f J 1tvt) Direction: __ ci=-:J ____ Distance:_"'=J ::=D:......:{=-> .---; _ _ _

1 Landmark #2: _ __..!'-'-'-'\_..,2'-'--r-f -------Direction: f, Distance: __ 3"""'-'6::....;L,._·> _ __ _

Sketch:

-Soil Unit Thickness Unit Description (continue

·-on back ifnecess ·1y--->) Pill Reading

(in. or ft.) (moisture, color, grain size, etc.)

I\ tD ·,sf eLk- I; n1 S u +-~ 'Cu' s 1- kJ v-n Pn s tu'tA

Gravel - coarse 314 to 3 in. fine 3116 to 314 in.

Sand- coarse 2 to 4.75 mm. medium 0.425 to 2 nun. fine 0.074 to 0.425 mm.

Silt/Clay <0.074 mm. (use plasticity)

Photos: YIN Time ofphoto: 10/),:l!Location: (J Direction ofphoto: S Photographer: JtiG

REN~S: _____________________________ _

(JW 12/9/09)

Page 33: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL SAMPLE DATA SHEET

Site: C&H TAlVIARACK OPERATIONS MID#: lvfiN000510835 Date: _ _L)_/ _{c=-() -· ..L.!.j)::::._,· _ _ _

0 Sample Location:.__,s~s~I-=-0:..___,..------Weather: Rctt n l ;:; L/ Field Persmmel: "J(Jf ·..J Au b f..,/11() Data Sheet Logger: .At. ( h(;YVl V\

Sam piing Time (MT) :. _ ___:_1 =-Z --=-' .__::L=:::..__3 "-----_-Depth/Interval :---'V~O~A...!;___-_4...:..__' ' _---"R~e~n~la~in~d=et!.._· _ _____:(J~-----=0:..____ Soil Cover: Y'Av S r"J (sand, grass) #of Samples Per Location:._~'----

Sampling Method: Grab: \_ / Composite: ____ _ _ (Check all Surface Sample:

v-Deep Sample: _____ _

that apply) Trowel: Hand Auger: _____ _ Other (explain):. ______________ _

Collected I# of -L

Vials Collected I # of Jars Coll;.cted I# of Jars

Sample Type/Bottles: ./ VOA ~SVOA!Pest/PCB_j_ \. Metals/Cyanide } -- --

Location Reference Features: Landmark #1 : ___________ Direction: _______ Distance: ______ _ Landmark #2: Direction: Distance: ______ _

" \ \ 0 /

I • I_),_

. I ,. I \ '' (l ( ) '- l . ( .. ~\ ~' \ ' \' ~

~

I,, I I .j'{r_ IV , • ' \ J

'- 1 /lt\'l'r' I ~ ~ f .._ -. \__ r'M ~ T r enct"- _ \~ 7

\

Soil Unit Thickness Unit Description (continue on back ifnecessmy--->) PID Reading (in. or ft.) (moisture, color, grain size, etc.)

o- (o {VlG ;·,t r)AL- h Y(\ sf I A! {-v\ ro YfU-1/A s tiL/l/

/{) Is o .-!' l(t vJ, ~"I' :, V'Ovk y I ai5, tr rvtLf-tu1 ell~~~- ,<; 1

·~ VOb k

Gravel - coarse 314 to 3 in. fine 3116 to 314 in.

Sand- coarse 2 to 4.75 mm. medium 0.425 to 2 mm. fine 0.074 to 0.425 nun.

Silt/Clay <0.074 rrun. (use plasticity)

Photos: YIN Time ofphoto: I2Z '1 #/Location: ). Direction of photo: £" Photographer: J&e. RENUUU<S: ______ _______________ _ _ _ _ ____ _

(JW 12/9/09)

Page 34: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL SAMPLE.DATA SHEET

Site: C&HTAMARACKOPERATIONS l'vfiD#: MIN000510835 Date: J/ h /;( Sample Location: SS I I )__.~-4-I---.-3.L........tl[ ________ _

Field Persotmel: J (lf' <.1 Au Weather:--4R--"C""'-l .1....:1

hem (\ Data Sheet Logger:.-----<.\A----L.J<:l~li ,L_F "'-'L L::....ln_,_1~1 1'-''1 _____ _ 'r)

'Jr , . ,,

Sampling Time (MT): , J Depth/Interval: VOA- J Remainder- () · ){

Soil Cover: \ C [~ \tf. S 1 hu115 (sand, grass) #of Samples Per Location: __ ...__ _ _ _

Sampling Method: Grab: J Composite: _____ _ (Check all Surface Sample:-r-- Deep Sample: ____ _ that apply) Trowel: V Hand Auger: ___ __ _

Other (explain): ______________ _

Colle.rted I # of Vials ColJ~cted I# of Jars Co~ected I # of Jars

Sample Type/Bottles: _ v_VOA _l _ \/SVONPest/PCB _ v'_ 1Metals/Cyanide_l_ -- - -

Location Referent€1 Fef\tures: . 1 ·7 / Landmark#l: 1\J l"vD l)(J ( b vuntltH'(birection: _ ___.N'-""-_ __ Distance: .......... JOb · Landmark #2: N 1 1

' · Direction: \A) Distance: I 0" l((tA d <:>

Q I

L~ •l); Sketch: '--: ~ \ I nki<-

SS-\1 ._

Soil Unit Thickness Unit Description (continue on back ifnecessmy--->) PID Reading (in. or ft.) (moisture, color, grain size, etc.) .

j'vU)IS -1 tLfc_ J;vYI Sdfy . ~' J·vutl 5tLp\c( c

( p.v' 1~, • ~) ( tLl /; , , s J 1 u.- f-clJ· , r t/ 1 r_ 1 e l v 't"' 1 • r

Gravel - coarse 314 to 3 in. fine 3/16 to 3/4 in.

Sand - coarse 2 to 4.75 nm1. medium 0.425 to 2 tmn. fine 0.074 to 0.425 111111.

Silt/Clay <0.074 mm. (use plasticity)

Photos: YIN Time of photo: \J.; Cj l(#/Location:2__Direction of photo: (\} Photographer: \. \ 6f <

REMARKS: ___________ ________________ _

(J w 1 2/9/09)

Page 35: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL SAlVIPLE DATA SHEET

Site: C&H TAMARACK OPERATIONS MID#: MTN00051 0835 Date: 1/ b / Z Sample Location: SS b( < <) S ) (1 1) 0

Weather: [ .\ (J L( tGL 3 :S Field Personnel: '-.JUf -.J /ht,ht J1f) 1'1 Data Sheet Logger: JhA h Lf1111 Sampling Time (MT): \ 0: 2 ) {) Depth/Interval: VOA- 5

1

' Remainder- 0-K Soil Cover: CJ ( Cl S S (sand, grass) #of Samples Per Location: __ .:.__ __ _

Sampling Method: Grab:. __ ~--- Composite: _____ _ (Check all Surface Sample: _ _ Deep Sample: ____ _ that apply) Trowel: V Hand Auger: _____ _

Other (explain): _____________ _

Collected I # of d.-

Vials Co!Jected I # of Jars ~lected I # of Jars Sample Type/Bottles: ~ VOA _ II SVONPest/PCB __2__ __ Metals/Cyanide 2 Location Reference Features:

L L\ I Landmark # 1 : I ,/, (v\ · ]_ lp Direction: C/ Distance: Lv

Landmark #2: -p, \ \ct c S ---~~-- -~--~-----

Direction: Distance:_-->..<..d-~u..;{;'---' ____ _

Sketch:

~ i ,,_ 1 ~ ;:; ~ ~5~~~\

r1 ~-~ X

~- ~ }

"<" @ -~ *.1 ~

1 ~

~ .\.j t t l . D . . ( . b k 'f Soil Unit Thickness U rut escnptloncontmue on ac 1 necessaty---> t;S-\d- ) PID Reading

(in. or ft.) (moisture, color, grain size, etc.)

<) ,., hi {n sA.,.../, ... t·{ c ( ,;vu ,. {) ( . o- 1

C .J / <... I .) ~

r {( $'i ( 1 '{ ) C L J-l{ ( ·I _) \ly_ ( ' Stii-Lt'

J I· L-L 11 ( I {I { /{

~ L ~ )~ s ,. I f \( Gravel - coarse 314 to 3 ) )\ Li l ( I t' { I I\ ];

in. I fine 3116 to 314 in.

hf\ /u t'IU ('( )lL i~( Sand - coarse 2 to 4.75 mm. . medium 0.425 to 2 mm.

fine 0.074 to 0.425 nuu. Silt/Clay <0.074 nun. (use plasticity)

I D '.lid- 7 Photos: YIN Time ofphoto:~#/Location:_(/(...·'1 _Direction ofphoto: ___ Photographer: Jc l REMARKS: _____________________________ _

(JW 12/9/09)

Page 36: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SO~ SAMPLE DATA SHEET

Site: C&H TAMARACK OPERATIONS MID#: MIN000510835 Date: _ _,_}_/_· _fo_)_c2. _ _ _

Sample Location: SS ) ~ Weather: _ _.~~<..::.G_~...:....:Il_'\~~'1r'~~..--· --,---- ------

Field Personnel: \Cf"t- ]+,).._ hLtY) (\

Sampling Time (MT): ~ ·z, Data Sheet Logger:

l 0 Depth/Interval: VOA- ~~ 11 ·J I • Remainder- (

I

Soil Cover: \ e (A. ve::> 1 tuJ f C 6 (sand, grass) # of Samples Per Location: _ __._ ___ _

Sampling Method: Grab: __ _::_/_J __ Composite: _ ____ _ (Check all Surface Sample: _ _ Deep Sample: _ _ __ _ that apply) Trowel: ~ Hand Auger: ___ __ _

Other (explain): ____________ __ _

Collected I# of Vials Collected I# of Jars Collected I # of Jars

Sample Type/Bottles: _i_ VOA __l_ ~ SVOA/Pest/PCB j__ ~Metals/Cyanide j_

Location Referencr eatu;c;,· s_ : ~. <) E Landmark# 1: ' 1 () 16 f f f'v Direction: ____ --___ Distance:_.!.......""'-Is~-c,"_' · __ _ Landmark #2: ___ ______ :---.Direction: Distance: ____ __ _

• \l ( \._,I ll Sketch:

I lol, ,l 1/ \ li I >f~S-

' I I

I f\l

~'f/:

, I \

I

Soil Unit Thickness Unit Descriotibn (continue o~ifnecessmy--->) PID Readlng (in. or ft.) (moisture, col~r, grain size, etc.)

(\ )-11 1

b J /( 5, j) fy h. /o (J1.ul ) t l.A1.f(

t v~Ol '> . {

~} ·, ,(, , sJ~-isJ, l,l r·or/

Gravel - coarse 314 to 3 in. fine 3116 to 314 in.

Saud· coarse 2 to 4 .75 nun. medium 0.425 to 2 mm. fine 0.074 to 0.425 mm.

Silt/Clay <0.074 mm. (use plasticity)

Photos: YIN Time of photo: 11 i 10#/Location:____d:.__Direction of photo: S Photographer: \'L REMARKS: ________________ _____________ _

(JW 1219/09)

' ~

Page 37: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL SA!VIPLE DATA SHEET

Site: C&HT" AJVU\R?ERATIONS MID#: MIN000510835 1 Date:

-----~----If 0 ·JJ

Sample Locat:.:i on:-=S=S-r-_ _ __ Weather: J2./1i (\ 1\L" Field Personnei:_~---4'--------Data Sheet Logger:_-.L-[~----=-l_JH~·~:..L/TILL.!.f\_!__ _ ____ -=--_

Sampling Tin::::Le (MT) ) ~ ; Depth/Interval :_V""""O"'"'A,_.__-_-+t - ·_· _ _ R=em=ai=n=de=r_---'-(-=--~-"_t_c.~-­Soil Cover: __ _,_/-=e -'-a"'>---r---(sand, grass) # of Samples Per Location: _ ____ _

Sampling Me-tl1od: / Composite: ______ _ (Check all Deep Sample: _____ _ SamplJ--that apply) Hand Auger: ______ _

xplain): _ ___ _____ _____ _

I # of Vials _v_

CoJiected I # of Jars Collected I # of Jars Sample Type/Eottles:~A __L SVOA/Pest/PCB1 _ \_ _0v1etals/Cyanide _L_

Location Reference Fe Landmark #1 : ___ +-! _____ Direction: _ ___ __ _ Distance: Landmark #2: Direction: -------Distance:

Sketch: f ' \

-r, t. I I 1

I

' \ "'-

\

... . \ \ I

Pill Readin (in. or ft.) jre, color, grain size, etc.)

1 . l \ I \ 1 I' \ '

I' I' ' (I l b\t.-

'-..,{< (1\'( MlY r ,, {.,WI \v) S 1

i \ t-'\ - r . .. - ! ,. ' ( ( ~ r. I i.f , ; /1 , , " t" ti\A I I - .l • I ' ' I f. .

'"' > ( j i ( l «} , " J \ 1 Y 'lA· ~ I ,

? ~ J '

Gravel - coarse 3/4 to 3 in. fine 3/ 16 to 314 in.

Sand- coarse 2 to 4.75 mm. medium 0.425 to 2 mm. fine 0.074 to 0.425 mm.

I Silt/Clay <0.074 mm. (use plasticity)

/

Photos: YIN Time fO: { l' ' r

#/Location:_c_ Direction of photo: \0 Photographer: __ _

(JW J 219/09)

Page 38: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL SAMPLE DATA SHEET

I Site: C&H TAMARACK OPERATIONS MID#: MIN00051 0835 Date: /1/ <;'/t t-

t i

Location:_..-ss=,.,-~---(_ ~,__,1 _-_lc___ ____ ( Sample .. Weather: _________________ _ 1

Field Personnel: ___ ]_-&_---(;;___"'-_____ Data Sheet Logger: ______________ _

Sampling Time (MT):-:-_:_1 c;_-:_1_0_' ___ Depth/Interval:_V._,O"'A~--------"R"'e"'m"'a""in""d"'e"-r-=-------1

Soil Cover:_~·'-}_<~ __ ,_· -'-(Yc--~_«____ (sand, grass) #of Samples Per Location: __ -'-----

Sampling Method: Grab: >-- Composite: ______ _ (Check all Surface Sample:. __ Deep Sample:_c-___ _ that apply) Trowel:_--"')('------ Hand Auger: _____ _

Other (explain): ______________ _

Collected I# of Vials Collected I# of Jars Collected I# of Jars

Sample Type/Bottles: __ VOA __ __ SVOA/Pest/PCB __ ~Metals/Cyanide_/ _

Location Reference Features: Landmark #1 : ___________ Direction: _______ Distance: ______ _ Landmark #2: Direction: Distance: ______ _

Sketch:

(

Soil Unit Thickness Unit Description (continue on back if necessary--->) PIDReading (in. or ft.) (moisture, color, grain size, etc.)

"{ f'-<'>-vf:_.(l ;~ .

;'~""e;~JX::f-: ;IL.-

~n

Gravel - coarse 314 to 3 in. fme 3/16 to 314 in.

Sand- coarse 2 to 4.75 mm. ~'1 , . .t~ medium 0.425 to 2 mm.

/}• .. .vvvt~~ fme 0.074 to 0.425 mm. Silt/Clay <0.074 mm. (use plasticity)

Time of photo: ___ #/Location: __ Direction of photo: ___ Photographer: __ _ (

REMARKS: :)vt,, ,-u:~t t.~-....,_~Jc.t:.l ~ N.Y. ["' ,)- i"';j ./7--c_ s,-klh-<t;. '

(JW 12/9/09)

Page 39: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL SAMPLE DATA SHEET

Site: C&H TAMARACK OPERATIONS MID#: MIN00051 0835 Date:_-i-lj I_· -"'r'J=-· _· _:_} -"-)_, __

Sample Location:,%? hl asl-c ;) Weather:_____,_{~~ 1-t-~-].,_,_l{ '-------Field Personnel: , J {r( ·r Jht

IW-c--"u'-id.4--j-\

hi 1

D!Jil Data Sheet Logger: __ ---,,1-~_1_ ________ _

Sampling Time (MT):---,-__,l4k,l-t-.LJ~Lf,__ ___ Depth/Interval:_:V,_,O~A'-'....::-___ __,R"'e""m""a"'in"'d"'e"-r"'-____ _

Soil Cover: 5 (t._,Q {/ (sand, grass) #of Samples Per Location:_-\-----

Sampling Method: Grab:. __ -"/ __ _ Composite:-,---_____ _ (Check all Surface Sample:;r-- Deep Sample: _____ _ that apply) Trowel:. __ _.\L__'------ Hand Auger: _____ _

Other (explain): ______________ _

Collected I# of Vials C9llected I# of Jars Sample Type/Bottles: __ VOA __ v

Collected I# of Jars I SVOA/Pest/PCB_I_ _V_lMetals/Cyanide __

Location Reference F~atl!res: 3D Landmark #1 : __ _:ll-"'\"'-t\"-Cji-_____ Direction: __ _:l::-:_. ___ Distance: -~ y t\ ) Landmark #2: 7 Directio~ Distance: ______ _

Sketch: """ -..,_ '"'~"'

··, r •.• >

r 5:: -<.

(--~

·~ ... --·

-'l,. ~;-

Soil Unit Thickness Unit Description (continue on back if necessmy--->) PIDReading (in. or ft.) (moisture, color, grain size, etc.)

Gravel - coarse 314 to 3 in. fme 3/16 to 314 in.

Sand - coarse 2 to 4. 75 mm. medium 0.425 to 2 mm. fme 0.074 to 0.425 nun.

·sl Silt/Clay <0.074 mm. (use plasticity) (

Photos: YIN Time of photo: l b' #/Location:_2_Direction of photo: tJ Photographer: J6 (/ t:l I N ') 111 f( (

I

(JW 1219109)

Page 40: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL BORING SAMPLE DATA SHEET Page 1 of2

Site: C& H TAlVIARACK OPERATIONS Date:_+-'/ J'--J/'---...L.-:~1-/ ..L/ -=2..:___ __ _

EPA ID#: MIN000510835 Sample Location:...!:S~B:!._-__.:C::::.)-'-/_· __ _

Samplers: ___ --f-'A>!..I/0=· ___________ Data Sheet Logger:_---..!...:./J:.....:..:../) ____ _

Soil Cover __ {'t'-)=t.'.....,lc..<,)/~0+'-' ;_p..ti.u.lf.s:..f 4--/ ___ (sand, grass, staining, etc.) Weather () \) lf\/(;ct-,{- "j7 °

Location Reference Features: Landmark # 1 - - ----- - ----- Direction Distance - ---- --- ---Landmark #2 Direction Distance ____ __

Sketch:

tl? /\\ ( "t

w 66 A'\ W'i // J

( f-I;JI)

Sampling Method: Grab: ·- ------ Composite: ------:-.----(Check all Hand Auger: ____ _ Geoprobe Macrocore: _ ____;_$ _ __ _ that apply) GP Small Discrete: GP Large Discrete: _ _____ _ --

Other (explain): _______ _ _________ _

SOIL BORING LOG WITH SAl\tlPLE DESCRIPTION ON PAGE 2

Photos: ~ Photographer f\) 0 #/Location 1e , I)\ Time 1 () L>~ Direction Pur/'t}

Remarks: - ------------------------ - -----

Well Installation Infmmation: Aquifer Type: Drift or Bedrock (circle one)

Type of Well Casing: _ ______ _ Depth ofWell: _ ____ (below ground level)

Screen Type/Length: _ ___ ___ _ Static Water Level: _________ (bgl)

(JW 12/9/09)

Page 41: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL BORING SAMPLE DATA SHEET Page 2 of 2

Site: C& H TAMARACK OPERATIONS Boring/Well ID:----!:S~B::..__ _ ___!_/T~M~W~--

Sampling Time (MT): I 11{J ·. C 5 •. 11\ VOA Sample Interval:._..:....l ...:..~__----l,(!.!;in~.) in. c• ',.. 1../ r (ft.) core

t ' I ' I

#of Samples/Boring: Remaining Sample Interval: . t

....:.12_· _-2_ 2 __ -~...(l!.!;·n~.) in. '' - t..../ (ft.) core Collected I# of Vials Collected I # of Jars Collected I # of Jars

Sample Type/Bottles: _i_ VOA _I_ J SVOA/Pest/PCB_I_ __i_Metals/Cyanide_ /_

.. s Lithological Description • .........

en Q ., en

' <1) C\

0 J2 ...... bl) s:: i::~ · ~ ;> o,........ . ~:.a

0 -+-'{.),..-... <1) {.) ·a :.a C\ Comments p_,-+-' <1) s:: d cQ

r/J..S ...... <1)

~c :::)f.--< c Unit Description a...~ \

l ~~ < fYt(;(}t

1 tllirk ·lrtL/.·A /lkJ\

... , j I

1\'l ~l 1 )tHe.{ (,(_1 : H1 tv.:u...e... r .:·d\ (JJ

PI'' I ~

(11(.' ~/t I i"t.'i\ I 1\llV{~ 511 /( t( I lU t' ·I }1 t 'rU.L- t_ rotl\

{) . rt 1 t"'l f;1 ,, f- k?. ·l2''

i L. 2)'

0' ' t~ IJev; fVld) +- 1 '"~ u\ ~(\~LA ~li1d I tv' llil;~ ((!( (\ !

-· [1 {)

~I - ~."

~o: lf (

~,2 r e !itst1 J 1-

Grain size chart * - Lithological description must include: Gravel coarse 3/4 in. to 3 in.

-Moisture content- (dry, moist, very moist, or wet) fine 3/ 16 in. to 3/4 in. -Color- (black, gray, brown, tan, etc., others as necessary) Sand coarse 2 nun. to 4.75 mm. -Grain size- (clay, silt, saud, gravel, etc., see table to right) med. 0.425 mm. to 2 mm. -Other materials -(debris (type), organics, etc.) fine 0.074 nm1. to 0.425 mm. -Special characteristics - (staining, streaking, etc.) Silt/Clay < 0.074 mm. (use plasticity)

(JW 12/9/09)

Page 42: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL BORING SAMPLE DATA SHEET Page 1 of2

Site: C& H TA1VIARACK OPERATIONS Date: _ _,_/...:....,/ j,_'-=-5 .L_l.._l _-z ___ _ (M pl: ~ .<k.

EPA ID#: :MIN000510835 Sample Location:-"S=B::.._-_<'_.--z.. ___ _

Operators: ___ _;L=-..:...;~n!...:...!...; _________ _ ___ Corresponding Well: TMW J-'0 ~ ... ij Samplers: _ _ ___ /U___:._D ________ __ Data Sheet Logger:_--'-'N::....JOl<L.._. _ _ _ _ _

Soil Cover ---..:jr-(_L)-="~::.._L....,)L__ ____ (sand, grass, staining, etc.) Weather __ 6_V_I?_r_f'.:_'.J_1 _ _ .)_:____z_<!' _ _

Location Reference Features: Landmark # 1 Direction Distance ---------- --- ----- - --- - -Landmark #2 Direction . -. Distance ~

-------,~ IJ Sketch: . / , ( -;-/.:y t·l·:;

r" .. p~ . ( "· _,/

,0J .,

{ ' ( , 0 9) o'< e/'J)

Sampling Method: Grab: ------- Composite: -------':--- --(Check all Hand Auger: ____ _ Geoprobe Macrocore: __ .:.._\ _ __ _ that apply) GP Small Discrete: GP Large Discrete: ______ _ ---

Other (explain): _________________ _

SOIL BORING LOG WITH SAMPLE DESCRIPTION ON PAGE 2

Photos: {jJN Photographer___._/lv-IJ ..... O ___ #/Location .58 -6( Time I 'f~ '3 5" Direction /L(, 1 ~ Remarks: ------------- - --- ---------------

Well Installation Infonnation: ND w f> / { Aquifer Type: Drift or Bedrock (circle one)

Type ofWeJJ Casing: _______ _ Depth of Well: _____ (below ground level)

Screen Type/Length: _ ______ _ Static Water Level: _________ (bgl)

(J\V 12i9/09)

Page 43: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL BOIUNG SAMPLE DATA SHEET Page 2 of2

Site: C& H TA1VIARACK OPERATIONS Boring/Well ID: SB -6 '2... /TMW

..,o'' Sampling Time (MT): {il!B· /Y'.3~ VOA Sample Interval: 1./ 4o

() o (in.) in. _ ·,_, _ _.,(=:ft""'".) core

#of Samples/Boring: Remaining Sample Interval:22'- 3't'"' (in.) in. c>; · ll' (ft.) core CoUected I# of

L Vials Collected I# of Jars Collected I # of Jars /

Sample Type/Bottles:~ VOA 2. SVOA/Pest/PCBL__ _2_Metals/Cyanide_ V_

Lithological Description·

Conunents Unit Description

(j)'' IY\o'6t , btC!Wf\ ~~ f<;;,tJJJ,h bro£.#1) WL\ ' 'YJ ~ JJcJ~1

- 'i6 ' I ( _\' f - - ·--·

[ '.· t.·

r: j t -

'· I I ~ r~'

n .. 't~ ~ -

I --------------------------------1 -

Grain size chat1 * - Lithological description must include: Gravel coarse 3/4 in. to 3 in.

-Moisture content- (dry, moist, vety moist, or wet) fine 3/ 16 in. to 3/4 in. -Color- (black, gray, brown, tan, etc., others as necessmy) Sand coarse 2 nun. to 4.75 nun. -Grain size- (clay, silt, sand, gravel, etc., see table to right) med. 0.425 mm. to 2 nun. - Other materials -(debris (type), organics, etc.) fine 0.074 nun. to 0.425 mm. - Special characteristics -(staining, streaking, etc.) Silt/Clay < 0.074 mm. (use plasticity)

(JW 12/9/09)

Page 44: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL BORING SAMPLE DATA SHEET Page 1 of2

Site: C& H TAl\1ARACK OPERATIONS Date: --~

1/J ~.

(, / ;l----------------

EPA ID#: N1IN0005 10835 Sample Location: SB -~

Operators: _____ _,)::::......-"..<:-'--11!.J_' _______________________ Corresponding Wdl._,T'""'IV'-"'-1-.!..'W'----------

Samplers: ___ ;V_ f)_. _____________ Data Sheet Logger: __ ....:...jJ_() ____ _

Soil Cover ----"Mf-=~~_,£7 ___________ (sand, grass, staining, etc.) Weather 0\J cr< .. o.'_d rUldtl~ T •J?L'

Location Reference Features: Landmark # 1 Direction Distance ------------------------ -----Landmark #2 Direction Distance

------:--1 -

Sketch: J N

Sampling Method: Grab: __________ _ Composite: _________ _ (Check all Hand Auger: ______ _ Geoprobe Macrocore: ------'IXIt\-----­that apply) GP Small Discrete: ---- GP Large Discrete: -------'-------

Other (explain): --------------------------------

SOIL BORING LOG WITH SAtvlPLE DESCRIPTION ON PAGE 2

Photos: f:gN Photographer AJ {2 #/Location16' -:3 Time !'-If .So Direction /utI' ft: I

Remarks: -------------------------------------------------------------

1Well Installation Infotma on: /U6ti J ..-L Aquifer Type: Drift or Bedrock (circle one)

Type of Well Casing: ______________ _ Depth of Well: (below ground level)

Screen Type/Length: _____________ _ Static Water Level : (bgl)

(J\V 12/9/09)

Page 45: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL BORING SAIVIPLE DATA SHEET ..,~&g~ of 2 fr1~ I ,, ,c7rJ

Site: C& H TAMARACK OPERATIONS Boring/Well ID :___,S=B~--J-=---------''~'T=tv-"'-lW:...:...· __ _ ( I

Sampling Time (MT): /7'Li : < JD VOA Sample Interval: t}_(.) '1 (in.) in. {} - I I T (ft.) core

11 #of Samples/Boring: 3 Remaining Sample Interval: I~~: 3'1 (in.) in. (J '-l.f 1 (ft.) core

CL

ollected I# of Vials Cp llected I # of Jars CJ llected I # of Jars Sample Type/Bottles: VOA 2__ v SVOA/Pest/PCB 2. _£_Metals/Cyanide 'Z.

,.-... Lithological Description· ¢:! Q

(/) (/)

'-' ...... >

<1.) v Q eo 1=:~ ~

0 > 0,--.. ...... J2 <.) _.-.... f::::' :o

0 <1.) Q . '""""' · ~ . Q C\l

r:/1 ..5 <1.)

Comments o.- <1.) 1=: ~ ...c: ~ ......

~:.::., ~ E-<:.::- Unit Description o...P:::

-, 0 . {, (

rvl6i7f r~dt/i-:}j I 6JrJf.l, "'; /t .::xi Itt.!

·,·. ·. nw(

(} , 0

l/111

II y-

Lf' ~ \j -~ ~ II l (rft/1+ ft~dcJ/,)1 6nJLvVJ 1 I

~t( 1utt/ (),(l

I t.j''· (Yit)~t- 1 dntl\ 1

[,roLJ.JV,1 Ni,R d 1 Z?ltC{ YT p""'""'

'I I

-- l>'' ( ~;,

l ('r\t /71- I clt!J' 1\ 1br.:·lu 11 I w.ed Jilld

')6'1 II )2- .- ~

() 0

If'

Grain size chmt * -Lithological description must include: Gravel coarse 314 in. to 3 in.

-Moisture content- (dry, moist, very moist, or wet) fine 3116 in. to 314 in. - Color- (black, gray, brown, tan, etc. , others as necessaty) Saud coarse 2 mm. to 4.75 mm. -Grain size- (clay, silt, sand, gravel, etc., see table to right) med. 0.425 mm. to 2 nun. -Other materials -(debris (type), organics, etc.) fine 0.074 mm. to 0.425 mm. - Special characteristics - (staining, streaking, etc.) Silt/Clay < 0.074 mm. (use plasticity)

(JW !219109)

Page 46: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL BORING SAl'fl>LE DATA SHEET Page 1 of2

Site: C& H TAMARACK OPERATIONS Date: /1 /G / I 7_

EPA ID#: MIN00051 0835 Sample Location:-"S=B'-·-y~· · ___ _

Operators: _ _ _ ....:~=-->--'rJ_; _____________ Corresponding Well?"""T~N=1W...:..:.._ __ _

Samplers: __ __,_/V><...>o£!2 _____________ Data Sheet Logger: __ ..:...fV{)"'--- ----

Soil Cover ------,-~-4{1'---<.t_:_:V'---12--'--l _ ___ (sand, grass, stain~g, ~c.) Weather 0\J et· Co•)' /~C~ ;ll hrt6lV cJ ,; ?2"

Location Reference Features: ~ ~~ Landmark # 1 Direction ---- -------- - . ----- Distance

' ------Landmark #2 '-'Direction Distance -----,-----! .

,! ¥ ~ Sketch: :~· ~

C) .. - ~~

. fJ-.'I).Y(il 1( ~~ , . ~~~vrj

Sampling Method: Grab: - - - ---- Composite:------,------­(Check all Hand Auger: ____ _ Geoprobe Macrocore: _ _y_;ri~---that apply) GP Small Discrete: GP Large Discrete: ______ _ - - -

Other (explain): ___ _ _ ____________ _

SOIL BORING LOG WITH SAMPLE DESCRIPTION ON PAGE 2

Photos: &IN Photographer !J(} #/Location c;£ ·l/ Time I '3 ~ 0 0 Direction----'A'-->..L-1 _ _ _

Remarks: ----------- ----- - - --- - ----- ------

Well Installation Information: fv6 }II..JL.. · Aquifer Type: Drift or Bedrock (circle one)

Type of Well Casing: _______ _ Depth of.Well: (below ground level)

Screen Type/Length: _______ _ Static Water Level: _ _________ (bgl)

(JW 1219/09)

Page 47: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL BORING SAMPLE DATA SHEET Page 2 of2

Site: C& H TAMARACK OPERATIONS Boring/Well ID: SB L/- /TMW ~ 2.S:t ,,1 I

Sampling Time (MT): IJ.{Y/ VOA Sample Interval: (in.) in. ~ -8 (ft.) core

1 2211 3U'' · I

#of Samples/Boring: Remaining Sample Interval: - 'f... Cin.) in. Lf ~& 1 (ft.) core

Collected I# of Vials Cpllected I # of Jars Collected I# of Jars

Sample Type/Bottles: L VOA _ {_ _v_ SVOA/Pest/PCB+ _L_Metals/Cyanide_J_

Lithological Description*

Q eo ...... ~ ~:a Q ...... t1.>

ro Comments Unit Description ~~

c~ D

( ·~1'' ''"';\:'­CJ II

o .o fP"'

1'2 I

·-r

Grain size chart *-Lithological description must include: Gravel coarse 314 in. to 3 in.

-Moisture content- (dty, moist, very moist, or wet) fine 3116 in. to 314 in. - Color- (black, gray, brown, tan, etc., others as necessmy) Sand coarse 2 nun. to 4.75 mm. -Grain size- (clay, silt, sand, gravel, etc., see table to right) med. 0.425 mm. to 2 mm. -Other niaterials -(debris (type), organics, etc.) fine 0.074 mm. to 0.425 nm1.

- Special characteristics -(staining, streaking, etc.) Silt/Clay < 0.074 nun. (use plasticity)

(JW 1219109)

Page 48: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL BORING SAMPLE DATA SHEET Page 1 of2

Site: C& H TAMARACK OPERATIONS Date: /1 / 5! I 2 ••

EPA ID#: MIN000510835 Sample Location:-"S"'B'---·0_$ ___ _

Operators:. ____ L""'.f',_.t_c'l,_,· ______________ Conesponding Well: TMW · 3

Samplers: __ ____,_/V_,_,_,O"-----__________ Data Sheet Logger: _ _,_/V__;_O _____ _

Soil Cover --"--tf"'{t"-1'-~~:,t-·1 _____ (sand, grass, staining, etc.) Weather (JJ {> r <" 4-';T 3:? u

j

Location Reference Features: Landmark #1 _____________ Direction _____ Distance _____ _ Landmark #2 _____________ Direction Distance _____ _

Sketch:

Sampling Method: Grab:_______ Composite: --.,-------..---­(Check all Hand Auger:_____ Geoprobe Macrocore: _ ___,i.X'-'------that apply) GP Small Discrete: ___ GP Large Discrete: ______ _

Other (explain): _________________ _

SOIL BORING LOG WITH SAMPLE DESCRIPTION ON PAGE 2

Photos: & Photographer--!f-=-u-"'0 ___ •_ #/Location55 . .:_,')Time n·. 5u Direction AJorik\

Remarks: _______________________________ _

Well Installation Information: vc Aquifer Type: Drift or Bedrock (circle one)

• l I f1 1. '53

I Type of Well Casing: __ 1._ __ ... r__.i_.'J"-"-· f':___ Depth of Well: (below ground level)

f'\)( ' Screen Type/Length: _..J_L__I'-'-1-'-' 111

_· ·.L·J,_,(c:..>\,__ 'I J Static Water Level: IY , (J 0' (bgl)

(JW !2/9109)

Page 49: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL BORING SAMPLE DATA SHEET Page 2 of2

Site: C& H TAMARACK OPERATIONS Boring/Well ID:____,S,_,Bo!.__·_:cl~~·),__u/T'"'M"'-.!.W'---·~:")"---f L .

Sampling Time (MT): /J.' 5o VOA Sample Interval:_::_•;::_)_' '_--.~.Ci!!!n"...) in. (> - f (ft.) core d . 1 t f

#of Samples/Boring: Remaining Sample Interval: 2b· <jl' (in.) in. 0-'1 (ft.) core Collected I # of

L Vi~ls

__ Collected I# of Jars

L ' Collected I# of Jars

Sample Type/Bottles: _l_VOA i SVOA/Pest/PCB _J_ Metals/Cyanide v'

Lithological Description <ll

] <ll

·a :Ed Comments ::;:J t-< ~ Unit Description

-( D t' tlil;\yt (AI\r \'\ 1

lt((u 11, fV-~t\ 1 ·:xntJ 6 -~--·---------------------·-:---·------------------------~---

rnch t -r 1

t>dttf)h b0u., n 11\'t..u( 1 1 :'A'4·r/

t r {) 1 (\:· v~( 1\

Lf2 j'

tJTT___ • !J .·

.

~- ------------/1 Ail((------------------. fYlt•) t- I i"~O f\ f\ bmtui1 .1 ( r'cl db"'. . br Ct» n 5(1, ()o,' 1 1d ft1 r d/

o.o 1!'411

Y-'1 - l

II'

Grain size chm1 *-Lithological description must include: Gravel coarse 314 in. to 3 in.

-Moisture content- (d1y, moist, ve1y moist, or wet) fine 3116 in. to 314 in. -Color- (black, gray, brown, tan, etc., others as necessmy) Sand coarse 2 mm. to 4.75 mm. - Grain size - (clay, silt, sand, gravel, etc., see table to right) med. 0.425 mm. to 2 mm. -Other materials -(debris (type), organics, etc.) fme 0.074 nnn. to 0.425 mm. -Special characteristics- (staining, streaking, etc.) Silt/Clay < 0.074 1mn. (use plasticity)

(JW 1219/09)

Page 50: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL BORING SAMPLE DATA SHEET Page 1 of2

Site: C& H TAMARACK OPERATIONS Date:. _ __,_)_,_.)/,_,.5..,_/'--'-/_"2 ___ _ ·.,' .. ' ~ o ' l . I ~,- ,,.

EPA ID#: MIN000510835 '•' · Sampl~iocation: SB :"§§f 0 C.

0 perators: __ ----"~""9"-'-'-·----,-------~--'--Conesponding 0.· Well: TMW- ..., '-Samplers: __ _,."!.L _____________ Data Sheet Logger: __ --')J--'-1)'------

Soil Cover __,S,.,Awll~q'r-----~d;;;;;SJ,.grass, staining, etc.) Weather diJ !y t rt ~ } ')":2 •

Location Reference Features:

Landmark #1 ---------,----~.- Direction'-' ~-.,------ Distance_'_. ___ _ Landmark #2 · · · \ · · t 'Direl;tion · · ., l /;' l Distance-····· ...

Sketch: '', . ·, l.i-(~~)-1/)

M

, •.· .. .. .

. I

. . '.

p~;~ i.

' f:;_e~ (t')

2& ..

Sampling Method: Grab: ,conmqsite;,, ~---'' '"''-"""----(Check all Hand_A_n_g_el-·: ""·· -. -c,;'"l -.. -, ~-.. '· '· 'Geoprobe M~ci'ocore: --\~A·, ___ _

that apply) GP Small Discrete: GP Large Discrete:·_: ______ _ Other (explain): _________________ _

,, .. SOIL BORING LOG WITH SAMPLE DESGEJPH~,pN ·PAOJ? ~;.) ,, 1... ' 1' .;< •

Photos: YIN Photographer /\)_[) #/Location5/3 · CRTime II; 4?} Direction_c.:A.Jc..; __

Remarks: --------------------------------

''TIM " l Well Installation Info11'llation:

- ')._ 1 •" cv Aquifer Type: Drift or Bedrock (circle one)

I I I I ., Type of Well Casing: . t ; ; " t Depth of Well: __,_/1_.:.__ ___ (below ground level)

Screep Type/Length: ---J.. " l_,.....'Cf 6,_· ~')'-"16"'-'-J .1 _ Static Water Level: -~~-"''"'-'-..:.G,:,...:.,L{-=-=() __ (bgl)

(JW 12/9/09)

Page 51: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL BORING SAMPLE DATA SHEET Page 2 of2 ·'

Site: C& H TAMARACK OPERATIONS Boring/Well ID: SB • 0~ /TMW ' . I ,

Sampling :rime (MT): 10?' 'I~ VOA Sample Interval: ?12'' (in.) in. 0 .. 'i I (ft.) core . . .

n·. 1! ll '

# ofSamples/Borin~: J Remaining Sample Interval: 2Z .. '-1 "J"" 1(in.),in. 0· lf (ft.) core . Collected I # of

_i_ Vials Collected I# of Jars J Co_ll~te9 I# of Jars V

Sample Type/Bottles: VQA -l-SVOA/Pest/PCB_ _ _£_Metals/Cyanide __ . _J_ I

. 1

,.-... Lithological Description* ~ Q .

en t . . ...__, . .,, ~

4) Bgp s::<i3

,,

> 0 > 0,.-... ..... 12 ~:.a 0 <1) (..)

<1) .

o..~=: s:: ·a (..) ,.-... Comments :B Cl d ~

........ <1) .. en ...... ~:.::- ;:::q ..... :.::- Unit Description A..~

c.; c. "' 1\16 i ~t-, rec\~.~h browY) , ~,4 o.o ~c1n4

~· -.. l ~~·' .- rrtOl~t- td.oiJh b'fotuy\ I ~~ c .u .

~~~ tvi~h +.-~('~ 1 ra~~

~·-r- ,, 4"" 2

/ -. . - "~ -~'\-I ~ 0 h b'(OLu~ I"' ~4 '

I

;tt/Jtd ' . .,~,

-\-rtlt 1

e. '(OL-~ ' . '

It ,

Y6"3~ 12. .-r , ft\6l~t"1 ~·1 ~., (o~re\~,.,,~~ l . ' :~~"

. . .. ..... ~ -~

-'.

. . ,, '

Grain size chm1 * -Lithological description must include: Gravel coarse 3/4 in. to 3 in.

-Moisture content- (d1y, moist, ve1y moist, or wet) fine 3/ 16 in. to 3/4 in. - Color- (black, gray, brown, tan, etc., others as necessmy) Sand co'a'rse 2 mm. to 4.75 nm\-- Grain size- (clay, silt, sand, gravel, etc., see table to right) med. 0.425 mm. to 2 mm., . -Other materials -(debris (type), organics, etc.) fine 0.074 nun. to 0.425 mm. - Special characteristics -(staining, streaking, etc.) Silt/Clay < 0.074 nun. (use plasticity)

', (J w 12/9/09)

Page 52: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL BORING SAMPLE DATA SHEET Page 1 of2

Site: C& H TAMARACK OPERATIONS Date:-----!....LI{_,_/ G=-+---"-j /_2-__ EPA ID#: MIN00051 0835 Sample Location:...:::S=B'--... _8 ______ _

Operators: ___ -=-l-......>......;Vl:.....:....._', _ ____________ Conesponding Well~-==-=-N=t·....:..;w ___ _

Samplers: __ ---J.A...>..L:){):.....::.._ ___________ Data Sheet Logger: __ .:...JfV._OL.__ _ _ _ _

Soil Cover --j -ti·,..,,G._"'L...25.L..._ _____ (sand, grass, staining, etc.) Weather -~0 ll_e....:...r_cCl.--'-''J'--'-+-f/....!..,q...L,'-"-=--i·~tl __

Location Reference Features: Landmark # 1 Direction Distance - --- - - ------ - - ---- - - ---Landmark #2 Direction Distance -----

Sketch: 1 t=hu}

Sampling Method: Grab: - ------ Composite:-----....,.....--­(Check all Hand Auger: ____ _ Geoprobe Macrocore: ---'~o'\-----that apply) GP Small Discrete: GP Large Discrete: _ _ ____ _ --

Other (explain): - - ----------------

SOIL BORING LOG WITH SAl\IIPLE DESCRIPTION ON PAGE 2

Photos: frpN Photographer-----'N'-----0 ___ #/Location 56· cJ ~ime I :5: t.../"') Direction /UcJr'/1 Remarks: ----- --- --- ----------------------

Well Installation Infmmation: Aquifer Type: Drift or Bedrock (circle one)

Type of Well Casing: _______ _ Depth of Well: (below ground level)

Screen Type/Length: _______ _ Static Water Level: _____... (bgl)

(JW 12/9/09)

Page 53: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL BORING SAMPLE DATA SHEET Page 2 of 2

Site: C& H T At'\fARACK OPERATIONS Boring/Well ID: SB - <0 ~MW 21"11 I

Sampling Time (MT):_--'-/ .J.£5_: '~~~- 'VOA Sample Interval:_-___ I • -l.,;(m=· :..:..<.)in. 6 ·'i (ft.) core

' #of Samples/Boring: / Remaining Sample Interval:2i~3Y" (in.) in. c- '.Y' (ft.) core

Colldcted I# of Vials Collected I# of Jars Collected I # of Jars

Sample Type/Bottles: J_ VOA --!- _j_sVOA/Pest/PCB_j__ _d_Metals/Cyanide_L

,..-... Lithological Description • ¢:l c (/)

(/) '--' <!)

<!) 0 en

~~ ;> 0 ;> o,........ ..G .......

~:a 0 O..'E

{.) <!) ~

. ~

<!) ·a ...... {.),-... 0 d

(/),...... ~:.::., .;::J :.a (lj Comments ......... v

, t- ... '--' Unit Description p...~

u ~ rYtut'?t , da,K- b1DCJ.J Vl, M.RL\ ":Xutt.{

trtJ~ 3

t y-(J. \)Q. \ O,D

rr""'

'{_ 1 I

~ '/ :}1 ~~ 1-ru.d:C +ru.~~flf;,

-ct>•<l

c -;, -

-:b r--Ml.ll':>t- -brc)(J.JY1 , 1

vrod 1 ::xt ;cJ '

a .c

~ {1,.-t /I v

D~ ~CtiJLL, t\1 /'\/) e (I :)t'/ 1

'i1t{ If:. 1(

't' - 1- '--(2" ~tl. -r- ;~ / I ~ ~~ brOVJ I'\ l V\1$?0 -y;11t{

0 _. CJ

ff' YVJ ,, . ;7_'8

,, (II oi 1;f-' red:! ,. ?h ' b m;r>'j I <% •LI k I ~i' fllut))... , ·t mt ~ 3 ntJ.t

li ' - 1--ttj 1- 'if_ . .. -

.

Grain size chart *-Lithologica l descript ion must include: Gravel coarse 3/4 in . to 3 in.

- Moisture content· (dry, moist, very moist, or wet) tine 3/ 16 in. to 314 in. - Color - (black, gray, brown, tau, etc., others as necessary) Sand coarse 2 mm. to 4.75 mm. -Grain size- (clay, silt, sand, grave l, etc., see table to right) med. 0.425 mm. to 2 mm. -Other materials -(debris (type), organics, etc.) fine 0.074 nm1. to 0.425 mm. - Special characteristics - (staining, streaking, etc.) Silt/Clay < 0.074 mm. (use plasticity)

(JW 12/9/09)

Page 54: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL BORING SAMPLE DATA SHEET Page 1 of2

Site: C& H T Al'-'IARACK OPERATIONS · Date:_ ----"/-+'/ ~:.._::h'--'L'--'-!_l __ _

EPAID#: tvJIN000510835 Sample Location:-==S=B::__-_t.-'-J _ _ _ _

Operators: ___ _:.~__,___·fe. __ ll_; _ ___________ Corresponding Wel!:'"_,Jk~~-"W'------

Samplers: ____ --=-/u-=--=-D __________ Data Sheet Logger: _ _.LjV_ O ____----

_ _

Soil Cover ¥U'J'J /Mf<'l? (sand, grass, staining, etc.) Weather OUel'ro;i/5-/)trt.-U/,a/1 J 2 .:_,

Location Reference Features: Landmark # 1 -------------- Direction Distance -----Landmark #2 Direction -----

Sketch:

Sampling Method: Grab: ------- Composite: - -----Fr---­

(Check all Hand Auger: _____ _ Geoprobe Macrocore: ---¥-A.l.---that apply) GP Small Discrete: GP Large Discrete: _ _____ _ ---

Other (explain):-------------------

SOIL BORING LOG WITH SAMPLE DESCRIPTION ON PAGE 2

Photos: (J IN Photographer----'/v~{? ___ #/Location.A11_ Time / 2: IS - Direction /uc'>~'"f ft Remarks: ------------------ -------------

Well Installation Information: W Yle. A,quHer Type: Drift or Bedrock (circle one)

Type of Well Casing:..----- Depth of Well:" ____ p low ground level)

Screen Type/Length : -------~ Static Water Level:------;------ (bgl)

(JW 1219/09)

Page 55: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL BORING SAMPLE DATA SHEET Page 2 of2

Site: C& H TAMARACK OPERATIONS Boring/Well ID: SB -'/ /TMW-1

1 Sampling Time (MT): 12: I '7 - VOA Sample Interval: ') 6 ' (in.) in. '-1 ~ <c; (ft.) core . I _j I I • I

#of Samples/Boring: Remaining Sample Interval: Zo -If#' (in.) in. Lf · f;. (ft.) core Collected I # of Vi~ls Collected I # of Jars 1 Collected I # of Jars /

Sample Type/Bottles: _I_VOA _ \/_ _ /_ SVOA/Pest/PCB_CI_ _ _/ Metals/Cyanidey_

,-_, Lithological Description • ¢::! c C/l

C/l '--/ 11)

11) -Q en ~~ > 12 ~ 0 > 8---:- ..... u ,-_, ~;a 0 11) ·a :.a Q Comments d ro Cll.5 p.,+-' 11) ~

~;,::::_ ::JE-<v Unit Description A:~ 0 c I'' f>1ol-Jf I da }' ~- 6etun I ~t~ 6:~1/L{

w:fh frac.c?.. 17$rl''!:1 (}. ,.,.,

'#'"" tl' f-J:ui?f-,

J te~lJ f;l, brcc:i} YJ 1 11'4' c/ ~a4

Lf .-~t'l IJ)'

(. ~ II 1}¥)!-j /- r -f>c/d/f h bf'tJtu rJ; /)'lrc) :XL JJc! (} . 7 P/1'1

~I 3' to~ ,.,

c r-J.d~·}, Y"l ' .. i1 + bf?:•J(JJ 11, 111 P~ 5o 1.c-{

f (1 . o //'"(

·2~f ,_ ·-f<.l'k

-..,..~ Vf?JY i-'}1!6.'1f I , fdJ i ~}1 btvUJfl

~4 ~~~Ll 6 6

36 I fl 1111

(l-1- . . ,

Grain size chm1 * - Lithological description must include: Gravel coarse 314 in. to 3 in.

-Moisture content - (d1y, moist, very moist, or wet) fine 3/16 in. to 314 in. - Color - (black, gray, brown, tan, etc., others as necessmy) Sand coarse 2 mm. to 4.75 nUll.

- Grain size- (clay, silt, sand, gravel, etc., see table to right) med. 0.425 nun. to 2 nun. -Other materials -(debris (type), organics, etc.) fine 0.074 mm. to 0.425 rnm. - Special characteristics- (staining, streaking, etc.) Silt/Clay < 0.074 nun. (use plasticity)

(JW 12/9109)

Page 56: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL BORING SAMPLE DATA SHEET ·Page I of2

Site: C& H TAMARACK OPERATIONS Date: / J / 5/J2

EPA ID#: MIN000510835 Sample Location:-'S""B'------'-'/ Q,.,\ ___ _

Operators: ___ __,L"-"·...ll.l;~ _____________ Conesponding Well: TMW-

Samplers:. ____ IV_f> ___________ Data Sheet Logger:____,_A,.,_)_,!')=-------

Soil Cover b I{ Ct~tJ /)14V<' \ (sand, grass, staining, etc.) Weather (\ile'r( 1\.5 t f2''

Location Reference Features: Landmark #I _____________ Direction _____ Distance ____ _ Landmark #2 Direction Distance ____ _

Sketch:

/

(·);~UI\J se,·l0 ' · .. ····'

"' / \ \ ,zf/\

Sampling Method: Grab:...,.-______ Composite: =------.,.,------(Check all Hand Auger: _____ Geoprobe Macrocore: __ ()(,__ ___ _ that apply) GP Small Discrete:___ GP Large Discrete: ______ _

Other (explain): _________________ _

SOIL BORING LOG WITH SAMPLE DESCRIPTION ON PAGE 2

Photos: &JN Photographer_.,;N'-"-"0"'-- #!Location:6~ )(l Time J 5'. 2.C. Direction /Vo • -1 ~

Remarks: ----------------------~---------

Well Installation Inf01mation: (\J 0 !Jv..J: /( Aquifer Type: Drift or Bedrock (circle one)

Type of Well Casing: _______ _ Depth of Well: _____ (below ground level)

Screen Type/Length: _______ _ Static Water Level: _________ (bgl)

(JW 12/9/09)

Page 57: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL BORING SAMPLE DATA SHEET Page 2 of2

Site: C& H TAMARACK OPERATIONS Boring/Well ID: SB-10 ITMW·Ot-f

'< (_. Sampling Time (MT): J A 2 U VOA Sample Interval:_-'-'! :?:__" _ ____,_(I'-". n"".) in. I " I / • ,' > (ft.) core

1

#of Samples/Boring: / Remaining Sample Interval: 0 '-n '' (in.) in. 'I~ (ft.) core Collected I# of Vials Collected I# of Jars j Collected I# of Jars

Sample Type/Bottles: _J_ VOA __!__ _}_SVOA/Pest/PCB__ _L Metals/Cyanide V Lithological Description·

"' ] "'

·a ~ :.a u ~ Comments ~ ::::> t- :.::.. Unit Description

( L" fo'\<i'J\, dor K: brown, ftNic/ :'.iiMt..{

/1," 1-·--·--.-----------------+ n.Y\\

lc i.,'' ..... ' - . . ...... - ·--~···-·--·--·--------·---!') \ '(J /llt0\:1\ , dctr l\ broUJM, 1'\.<."d , "Xt.ttf

ho ~~ rorf\ 4

r-. ' {; --

I J 2 ·-

@,()

Grain size chart * -Lithological description must include: Gravel coarse 314 in. to 3 in.

-Moisture content- (dry, moist, ve1y moist, or wet) fme 3116 in. to 314 in. -Color- (black, gray, brown, tan, etc., others as necessary) Sand coarse 2 mm. to 4.75 nllll.

. -Grain size- (clay, silt, sand, gravel, etc., see table to right) med. 0.425 mm. to 2 nnn . -Other materials -(debris (type), organics, etc.) fme 0.074 mm. to 0.425 mm. -Special characteristics- (staining, streaking, etc.) Silt/Clay < 0.074 mm. (use plasticity)

(JW 1219109)

Page 58: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL BORING SAMPLE DATA SHEET Page 1 of2

Site: C& H T AIVIARACK OPERATIONS Date: _ __.!l__:_l_J./_· L=-- .~-/_:...!_;._' ___ _

EPA ID#: :MIN00051 0835 Sample Location:....!oS~B~~-· ..!...!//'----- --

Operators: ____ _!:L=--"....:..' ';_1 ;_i _ _______ ____ Corresponding Well: TMW·~

Sarnplers:. _ ___ -----'1'---'-'--00 ----------Data Sheet Logger: _ ___!_/J=---n -----

Soil Cover _ __,y=· __o.l_;_t/1'--J---'-------- (sand, grass, staining, etc.) Weather --....:!.~~()!..!..<..:...'• '....:::.iw,nllf1---3~(=-i ... _ _ _

Location Reference Features: Landmark # 1 Direction Distance _____ _ - ------- ------ -----Landmark #2 Direction Distance -----

Sketch:

\

----( l

I I

Sampling Method: Grab: I

·------- Composite: -------,.-T---(Check all Hand Auger: _ ___ _ Geoprobe Macrocore: _ ______.R._,__ __ _

that apply) GP Small Discrete: GP Large Discrete: _ _ ____ _ - --Other (explain): _________________ _

SOIL BORING LOG vVITH SA!VlPLE DESCRIPTION ON PAGE 2

Photos( y1N Photographer---~.IJ_O=----- #/Locatior6& ·// Time 8: 3')- Direction tJ Remarks: - ---------- - --- ------- ---------

Well Installation Information: Aquifer Type: Drift or Bedrock (circle one)

l !\ Type of Well Casing: _ ___:_f'v_ft_:__ ___ _ ;]I Depth ofWell: r; v Lf (below ground level)

Screen Type/Length: _ _ _,/4-\_I.._A_,__ __ _ Static Water Level: /lJ d (bgl)

(J \V 12/9/09)

Page 59: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL BORING SAMPLE DATA SHEET Page 2 of2 I

Site: C& H TAMARACK OPERATIONS Boring/Well ID :,-----!S:::.=B:::....·_-4l j _ _!_/T~M=...!.!W'----.--;---':r:f_;___

0 ' l I • I Sampling Time (MT): (} : 3 '5" VOA Sample Interval: ~J

'' (J (in.) in. ( l ·

I

L•

J (ft.) core

I Interval: . I

#of Samples/Boring: Remaining Sample •

22 - .3 (.. 11 (in.) in. C:r li (ft.) core

Collected I# of Vials Collected I # of Jars Collected I# of Jars 1 Sample Type/Bottles:~ VOA L _l_SVOA/Pest/PCBL _f_Metals/Cyanide_ V_

,-.., Lithological Description • ~ c (/J

(/J '-" 4)

4) Cl eo

12 ......... ~~

~ ;>

0 ;> 8 r-:- ..... (.) __...... ~;a 0 ~ ·a :.a Cl d (1;$

4) Comments

0.~ ~ ......... 4)

{/) ......... P:::v •r::J f-cc Unit Description 0-.~

c !;I>'

3~ ,. r.J

(ft · \-:>~ l b rlJUJf\, Yv\_()(\ /~ .. aitd1

(L O

e. -~-vl\ ~~~~- c\ t l t j, bfa\.u'dl, ~xr n cl f (Jf/\

4, "I-11 :, UJ

' I

/,' H, 1

1t ~t t~ l ( -? (L't1\~ ('I.Y(

r~(u~ 1 ~ {f. 2(\ ~

.

Grain size chm1 * -Lithological description must include: Gravel coarse 3/4 in. to 3 in.

-Moisture content - (dty , moist, very moist, or wet) fme 3/ 16 in. to 3/4 in. - Color- (black, gray, brown, tan, etc., others as necessmy) Sand coarse 2 mm. to 4.75 mm. -Grain size - (clay, silt, sand, gravel, etc., see table to right) med. 0.425 mm. to 2 mm. -Other materials -(debris (type), organics, etc.) fine 0.074 nun. to 0.425 mm. - Special characteristics - (staining, streaking, etc.) Silt/Clay < 0.074 nun. (use plasticity)

(JW 12/9/09)

Page 60: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL BORING SAl\'IPLE DATA SHEET Page 1 of2

Site: C& H TAMARACK OPERATIONS Date: // / (o /1 2

EPA ID#: MIN000510835 Sample Location:-'=S=B:.......·~~I,_.-=2 ___ _

Operators: __ --F<~..L..----------------Conesponding Well":""'NVl'w-

Samplers: __ ---..:.}J-=-Q..L.__ ____________ Data Sheet Logger:_--"-'/l)~Q'--------. : ~

Soil Cover --,~+''(_ti_~?;)'--::r------ (sand, grass, staining, etc.) Weather ---'='---'---'----=...:.,-/--~-=------/

Location Reference Features: Landmark # 1 Direction Distance ------------- ------- ----------Landmark #2 Direction Distance --------

Sketch:

. tl~ ~ \l )V'

~ i (II j;-/ 2 ,1:',, - I ?'-

I '(.,\\ ) It \.. ' I);// \

\ ' I

', '

Sampling Method: Grab: Composite: _ ___ ___ _ _ _ -------------(Check all Hand Auger: ____ _ Geoprobe Macrocore: __ _:_K_,_' _ _ _

that apply) GP Small Discrete: GP Large Discrete: ___________ _ --

Other (explain): __________ _ _ _ ____ _

SOIL BORING LOG WITH SA1\1PLE DESCRIPTION ON PAGE 2

Photos: f:iJN Photographer--+~A...,._/ .:...._lO _____ #/Location '5(S-)2y-ime /D ;·5) Direction A..;6 !' fr?

Remarks: -------------------- ---------- ---

Well Installation Infonnation: /uJ"fl Q.. Aquifer Type: Drift or Bedrock (circle one)

Type of Well Casing: _ ______ _ Depth of Well: (below ground level)

Screen Type/Length: ______ _ _ Static Water Level: (bgl)

(JW' 12/9/09)

Page 61: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL BORING SAMPLE DATA SHEET Page 2 of2

Site: C& H T AMAR-A;CK OPE~ONS Boring/W ell!D: SB - /2. rrMw-;o s ? .1 t""' /,,j./fo ... , 0

Sampling Time (MT): }(_~~ VOA Sample Interval: .~1' 1 Cin.) in. 'i- ~ (ft.) core II 11 t

) \!

#of Samples/Boring: Remaining Sample Interva!:.L'7 3C::- (in.) in. if -] (ft.) core Collected I # ofVi~ls Collected I# of Jars I Collected I# of Jars . 1

Sample Type/Bottles: _J_ VOA _j_ j_sVOA/Pest/PCB/__ ~Metals/CyanideV __

Lithological Description·

c ~ v v ;> .fj

g 0......... ....... (.) .........

d ·a :.a Comments d ~ :.::::... /? f-< :.::::... Unit Description

CD' () -'!~ Mob+- brow'f\, 1 ~q)J~))\

/

r

ID

Grain size chart *-Lithological description must include: Gravel coarse 314 in. to 3 in.

-Moisture content- (dty, moist, vety moist, or wet) fine 3/16 in. to 314 in. - Color- (black, gray, brown, tan, etc., others as necessmy) Sand coarse 2 nm1. to 4.75 mm. - Grain size- (clay, silt, sand, gravel, etc., see table to right) med. 0.425 nun. to 2 mm. -Other materials -(debris (type), organics, etc.) fine 0.074 mm. to 0.425 rnm. - Special characteristics- (staining, streaking, etc.) Silt/Clay < 0.074 mm. (use plasticity)

• (JW 1219109)

I ' J

Page 62: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

GROUNDWATER SAMPLING DATA SHEET

Site: C&H TAM A RACK OPERATIONS MID # MlN00051 0835 Date: 11&) z-1 I

Field Personnel: 7/ti~ Data Sheet Logger: TIJ-[j WeU Number: Tm W ,_.D l

Aquifer Typ~ Bedrock Weather: OC/t ¥C C!<AJ-(-~ 3/~sponding Boring: N/ 11--11

Type of Well (Casing): / jJ £/'(!_ Stick-up (Ground to TOC (ft.)): /t t/:?!7" I 1

Screen Type & Length: t.- J1V L--Y oJI.fo{of 1

Casing Elevation(ft.): _______ _

Depth ofWell (ft.): / 15" Toe Ground Elevation (ft.): ________ _

Static Water Level (ft.): (-) fd, 2>0 /-k.)PurgeMethod: fdvliJMn'? et'f J2y;~ Length of Water Column (ft.):(=) Purge Start Time: g',· 3S Ji.o ~ Volume/Ft.(based on dia): (x) Sampling Method: _ _;>::::..___:_,~'-'--'--=:::------

One Volume (gal.): (=). ______ Sampling Sta1t Time:____,S=· --~ .... J:S<,..;;;;_ _______ _

Sample Type: Grab X Composite ___ _ In-line Filter:_i{lli)~N==-£.__-------Collected I# of Vials . s;ollected I# of Jars 2-- , <)>llected I# of Jars -f/

Sample Type/Bottles: __K_ VOA L._ _-{_SVOA/Pest/PCB__ _)(_ Metals/Cyanide_/_

77~ B:So I L Well Voi./Ft. I -Vol. Removed

(e_) Vol. I I,_Y.:....:o=I.-=2_.,_V-'-'o=I.'-"3 __ ,__,_V=ol,_. 4,___,__...:.Y=ol""'. 5"---l Dia. (in.)· I gal/ft. I

I L ~ I I 0.75 1 o.023 I

Tempc<atwe 0 ' 1.0 1 o.041 1

1.25 I o. I pH I "'1 ·Sb I I

o64

h-rx>s(tl~)~ 3~3 1 'Conductivity~ S:CJ 2' I t

1.5 1 o.o92 I I 1 2.0 I 0.163 I I I Others: V = 0.04 1 x (d/ x h

1~ 1 I I I V = volume (gal.)

~~~~~~~~~~-~~ ) j d = diameter (in.)

j h = hieght (ft.)

Direction: Distance: ----- -----Direction: -----Distance: -------

Sketch:

Photos:@r Time of photo / 0./0#/Location:

Remarks: lfu ' 5 A1tv\_f L. e-J ~

Page 63: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

lvJ-/l ·.~JfJc:f:.; ~ SOIL BORING SAMPLE DATA SHEET Page I of2

Site: C& H TAMARACK OPERATIONS Date:_-----'--''J/__!_/-"'-'J-"--/_1_{ __ _

EPA ID#: MIN000510835 Sample Location:JSi!BL·=:==:___

Operators: ___ _::L""e'"'r-'-'-1•' ______________ Conesponding Well: TMW- '' I

Samplers: ___ __,?J-'<--!-'-----------Data Sheet Logger: _ _.l""J_,_Q.£__ ____ _

Soil Cover---"'~--xcil·_...~I-"'J'-I,J'-"jt'Y"'i<'-"'l'.L·1 __ (sand, grass, staining, etc.) Weather _ ___,(>,_U,_,P:Jiv"<---'4-L"z~-} __ jf-·_,_7_'·_

Location Reference Features: Landmark #I _____________ Direction _____ Distance ____ _ Landmark #2 Direction Distance ____ _

Sketch:

~~) •L

•· ~

r:-\ ~~ 'I ~

~-~

Sampling Method: Grab:·-,------- Composite:=-----------(Check all Hand Auger:_____ Geoprobe Macrocore: _____ _ that apply) GP Small Discrete: ___ GP Large Discrete: ______ _

Other (explain): _________________ _

SOIL BORING LOG WITH SAMPLE DESCRIPTION ON PAGE 2

Photos: YIN Photographer ______ #/Location Time ____ Direction~----

Remarks: --------------------------------

Well Installation Information: vc Aquifer Type: Drift or Bedrock (circle one)

fl /1

Type of Well Casing:-/------:-;:-/(,'f-!-JJrv<" 1·c,..,"'+r

, __ _ Depth of Well: }l , '/t• ' (below ground level)

Screen Type/Length: _I_" __ I_!J_-_1 _I "_.f __ _ Static Water Level: -"-'-'"'-)"'-j~_-_' _____ (bgl)

(JW 12/9/09)

Page 64: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL BORING SAMPLE DATA SHEET Page 2 of2

Site: C& H TAMARACK OPERATIONS Boring/Well ID :____,S""B'----------'--"/T'-"M"'-'-'W'-----o_,j'---

Sampling Time (MT): _ _,_/1,:._;/ A~-- VOA Sample Interval: (in.) in. __ __j(Jo.'ft"-1.) core

# of Samples/Boring: /VA Remaining Sample Interval: (in.) in. -----'("'ft"".) core Collected I# of Vials Collected I# of Jars Collected I# of Jars

Sample Type/Bottles: -/1/J_ VOA _·_ ~VOA/Pest!PCB __ __Metals/Cyanide __

Lithological Description'

Comments Unit Description ;

( ,,

(1, (>

1!"1

l-(·-I

..

\ j2. ---

Grain size chart *-Lithological description must include: Gravel coarse 314 in. to 3 in.

· Moisture content · (dry, moist, very moist, or wet) fme 3116 in. to 314 in. ·Color· (black, gray, brown, tan, etc., others as necessary) Sand coarse 2 mm. to 4.75 mm. ·Grain size· (clay, silt, sand, gravel, etc., see table to right) med. 0.425 mm. to 2 mm. -Other materials -(debris (type), organics, etc.) fine 0.074 tm.n. to 0.425 mm. -Special characteristics- (staining, streaking, etc.) Sili/Ciay < 0.074 mm. (use plasticity)

(JW 1219109)

Page 65: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

GROUNDWATER SAMPLING DATA SHEET

Site: C&H TAMARACK OPERATIONS MID# rvrrN00051 0835 Date: /(-0 3-.- 12 Field Persmmel: 'l ft-0 Data Sheet Logger: / ,.1 /~ W~ll Number: Tl?t W-t3~~

Q A-35~L {71/lw -oZ-Aquiter Type: I& I Bedrock Weather: ()I) cvv eu ~ t ~ Corresponding Boring: :5.13 -() G:.

J 1 1

Type ofWell (Casing): (? V {_- Stick-up (Ground to TOC (ft.)): 0.-l.f 6 ~~ ~ •I Screen Type & Length: !: --~-1-1 1 '/ r /l Y' ;fl~ L,:O ,f Top /o -r-ofCasingElevation(ft.): _______ _

.;,L ) ' ~ ~ Depth ofWell (ft.): II' 1Lf ~Ground Elevation (ft.): _____ ~---Static Water Level (ft.): (-) 1 "09 ('foC) Purge Method: f?~ ~M,pc_ /~4/J~ LengthofWaterColumn(ft.):(=) PurgeStmtTime: /3 ,~z? Z flo~f' Volume/Ft.(based on dia): (x) Sampling Method: cJ tf~e- .J I£~ One Volume (gal.): (=) Sampling Start Time: 3/' 5 {) I ~ 1 '1 F~:J Sample Type: Grab K Composite ___ _ In-line Filter: Y ~ (j /

I ~~~~------------ f, ~ Collected I# of Vials Collected I# of Jars I/ , <;ollected I # of Jars

Sample Type/Bottles: __£___ VOA _!j_ _l_sVOA/Pest/PCB_T_ _6_ Metals/Cyanide ;2 t 2. r-(J fl-tJc ifll!J]2 I /'3. ·c..;§ I J 3 :s-o I I Well Vol.fFt. I

I ' Vol. Removed I Vol. I I Vol. 2 I Vol. 3 I Vol. 4 Vol. 5 I I Dia. Cin.) I gal/ft. I

~c._, t ( &:> : I ,, a : I e I I :

0.75 I 0.023 I

t Temperature t J, I

,/'?l!fli I 7 1

I ~I OJJ41 v

I ~-;H I I

~~I I I ~ I o.o64 1

r. { I 1 1.s 1 o.092 1

co;;AfJr;;_vj! - I I -+ L 1 2.0 1 o.I63

-.sa -1

\!;,?; .5;1, sL I Others: V = 0.041 x ( d)2 x h '>. I

I V = volume (gal.)

~tr;~a#~) ~ U¥r 3;o 1 3a=f ~ ·) d = diameter (in.) h = hieght (ft.)

Location. 'Reference Features: Landmark# 1: Direction: Distance: _____ _ ------------------------ ----------Landmark #2: Direction: Distance:. _____ _

Sketch:

~------~--~----------------~~ -2 b ....___,)

() T!Avw 2

Photos: & Time of photo: ll-i ~.(#/Location: V Direction ofphoto:--'tJ'----_Photographer: {fi ,Q Remarks:___!.P,~~~___J.,~_:___Jtt::.~~c.:....:::::::......::..=::~~--l-~~--~:::::s.:::::~~L.::3-..JL.L:a-.::~Jo....!c_:::..:k)y_ .

~~~~~--~~~~~~~~~~~~LL~~~~~~~~~~~--~~(J\~V~I~~W~•

Page 66: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

GROUNDWATER SAMPLING DATA SHEET

Site: C&FiTMIARACKOPERATIONS MID# MJN000510835 Date: II ~ 05-1 L_

Field Personnel: ~ 11-Q Data Sheet Logger: ~11t) Well Number: 7/u W~ CJ3-" _ m s/ll!.sj)

Aquifer Type: @>;Bedrock Weather: Or ~c 4' st= ~as-/corresponding Boring: s.Btf) 5

I ll r ./JJ//1 /t:::J/'

Type of Well (Casing): _ V <--- Stick-up (Ground to TOC (ft.)): 6., 1 o .~ ., '/Jt!C ;o- S/td-

Screen Type & Length: ~ .. / ~ .....-,......., Top of Casing Elevation( ft.): _ ___ _ __ _

Depth of Well (ft.): /.2. S / (rt)c ) Ground Elevation (ft.): ________ _

Static Water Level (ft.): (-) fJ-..o'J (!~}urge Method: 'f1iufc46c £~ Gf Q~o5~Si7 Length of Water Column (ft.):(=) Purge Start Time:___._/ _5 _,_.2_;9,___ ______ _

Volume/Ft.(based on dia): (x) Sampling Method: S~ -0; 1)) One Volume (gal.): (=) _____ Sampling Start Time: ~.,~~~ ~ / /Cj Sample Type: Grab X Composite ___ _ In-line Filter:-'1!!4'-llii~tii::€::::Pl~::..__------

Collected I # of6 1ls Collected I # of Jars Sample Type/Bottles: ~ VOA

--17~12 Vol. Removed

o.023 I Temperature oe.__ 0.041 :::p

0.064 1

o.092 1

____________ Direction: _____ Distance: ____ _ Direction: ---- --- ----- -----

~a! 1-.evk -----

) c

' fJ 7111 tU-3 Photos: ~ Time of photo:/ /o,lf5;/Location:_Z_oirection of photo: {AJ Photographer: Tt/lJ Remarks: Pfu& ~ /j);;tf;.._, d't4AJJ1 {IJdf~or~ ,..-,

~.£ ~a1• (JW 12/9/09)

Page 67: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

GROUNDWATER SAMPLING DATA SHEET

~ t -ob Site: C&H TAMARACK OPERATIONS MID# MIN000510835 Date: _ _ r1 _____ -; z_

_

Field Personnel: Tf1-D Data Sheet Logger: Tfr72 Well Number: TfVLU)- OS . 'F

Aquifer Typ~ Bedrock Weather: 0 f/Wcas/=;:;}-3/ Corresponding Boring: IV//j-Type ofWell (Casing): ) l' PV (!_ Stick-up (Ground to TOC (ft.)): {)es> 6 ~

c;J,..J...~;''IJllc ,;o._.s;~r Screen Type & Lengtj' ==o.C / ~"'' 1 _/ Top of Casing Elevation(ft.):

Depth of Well (ft.): (Toe) ;.. 3~ B.5 Ground Elevation (ft.): ________ _

Static Water Level (ft.): 6c0 ,20, 78 ~ Purge Method:P.e,o:S-&f.Hc. ~~ Jds,a~ Length of Water Column (ft.):(=) Purge Start Time: __ CJ____.!,Cf_,-~.' /~3c..__ ____ _

Volume/Ft.(based on dia): (x) ______ Sampling Method: S~

One Volume (gal.): (=) Sampling Stat1 Time: (tJ 1t 0D

Sample Type: Grab )( 7

Composite In-line Filter :_~~/ -?-'N'---:::::oo.-L-------Collected I# of Vials

-/l -lollected I # of Jars ~.ollected I # of Jars

.J.± J

Sample Type/Bottles: ..6_ VOA ~ SVOA/Pest/PCB __Z-~Metals/Cyanide

-ri 1/Ylt;;' CJ,'oo 1 1 Well Vol./Ft. 1 Vol. Removed Vol. 3 I I Dia. (in.) gal/ft. I

(. I I I 0.75 o.023 I Temperature\ ~C.) 1-l _L..:.._F>J- _.!:....._./J..---1--Cf....t...::....:, S=---1 <J:::TO 0.041 D

I b I I (oi./:

1.25 0.064 I pH ,-- I I I 1.5 0.092 I W5 -ll',d") 1 2.0 1 0.163 1

Others: V = 0.04 I x (di x h V = voltune (gal.) d =diameter (in.) h = hieght (ft.)

Direction: _____ Distance: ____ _ Direction: _____ Distance: ____ _

Page 68: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL BORING SAMPLE DATA SHEET Page I of2

Site: C& H TAMARACK OPERATIONS Date: __ .wllw_::_j.;_-'----'c"' / --;; -, .. ~----

EPA ID#: MIN000510835 Sample Location:_,S"'Be__··_··----

Operators: _______ ____,['-'!'-'~'-'· __________ Corresponding Well: TMW · 5

Samplers:'-------~-'"'[~) _________ Data Sheet Logger:_---'-'N'-''{)"---------

Soil Cover ,·~· ,~j / tl:rCWt (sand, grass, staining, etc.) Weather (\\)frc tr~ f ~)- < y -j'-

Location Reference Features: Landmark #1 _____________ Direction _____ Distance----=-----Landmark #2 Direction ,---Distance·-_-_· -t----

Sketch: 1 ~~-I il_&,~_, A)/ :

Sampling Method: Grab:_______ Composite: _________ _ (Check all Hand Auger:_____ Geoprobe Macrocore: _____ _ that apply) GP Small Discrete: ___ GP Large Discrete: ______ _

Other (explain): _________________ _

SOIL BORING LOG WITH SAMPLE DESCRIPTION ON PAGE 2

Photos: YIN Photographer ______ #/Location Time ____ Direction, ____ _

Remarks: -------------------------------

Well Installation Infmmation: Aquifer Type: Drift or Bedrock (circle one)

Type of Well Casing: I I' r I

15 '

"'I· Depth of Well: 2:3. rfi l (below ground level)

Static Water Level: --"'7"-'(L')'-''-LJLI,__ ' ____ (bgl)

(JW !2/9/09)

Page 69: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

SOIL BORING SAMPLE DATA SHEET Page 2 of2 v'l~ <~

Site: C& H TAMARACK OPERATIONS Boring/Well ID:____,S"-"B"-----'"J.'-fJ---'-/-"-T"'-M'-'W"----~-"--) _

1Sampling Time (MT): ~} t'\ VOA Sample Interval:---"y-;u,J1 _ ___,_:==

# of Samples/Boring: N A Remaining Sample Interval:_-+---'-""'"'-Collected I # of Vials Collected I# of Jars Collected I# of Jars

Sample Type/Bottles: __ VOA __ SVOA/Pest/PCB __ Metals/Cyanide

Lithological Description

Comments

c Unit Description

C.,, ' 1~1 ~1St, brOVI]~ :':Mtl

~~~

0 0 00-

I > 1

IJ1o '

'r\•0 I

0 ,

~ ,,

--0-00

000o 0~

JZ \

-

L} ,. f t iP

\ 10

Grain size chart *-Lithological description must include: Gravel coarse 314 in. to 3 in.

-Moisture content- (d1y, moist, very moist, or wet) fme 3116 in. to 314 in. -Color- (black, gray, brown, tan, etc., others as necessary) Sand coarse 2 1mn. to 4.75 mm. -Grain size- (clay, silt, sand, gravel, etc., see table to right) med. 0.425 mm. to 2 mm. -Other materials -(debris (type), organics, etc.) fme 0.074 mrn. to 0.425 mm. -Special characteristics- (staining, streaking, etc.) Silt/Clay < 0.074 nnn. (use plasticity)

(JW 1219/09)

Page 70: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

Parcels FIGURE 2

APPROXIMATE PARCEL BOUNDARY SITE FEATURES D OSCEOLA TOWNSHIP

illJiillTI] ~m...-~._, Remains of former TORCH LAKE AREA SEWAGE AUTHORITY IJii<., •• , ·.o~ Ahmeek stamp mill

• N

. W . E

s

=-=-=- Topographic contour

e Former stack or chimney (from Sanborn maps)

......., Route from Houghton (to Hendrickson property)

- Stream

r--~---- Former lakeshore (1946 topographic map)

·++·-+ Former Mineral Range Railroad (1 U46 topographic map)

[~~--~~j Site boundary I:::::J::J::J::J=i1 ~::J::J::J::JJJ 2002 Tamarack City Stamp Mill BFRA (MDEQ)

CJ C & H Tai·narack Operations Site subarea

k~~~H Former s1·amp mill (from Sanborn maps)

Sources: Feature layers from Michigan Geographic Data Library website; 2009 aerial photograph from Michigan Imagery Solution website; historical features from Sanborn fire insurance maps and historical aerial photographs; site specific information from MDEQ files and local governments.

SITE INSPECTION WORK PLAN C & H Tamarack Operations 0 200 400 600 800 1 ,000 Feet Compiled by: John E. Spielberg, 9/7/2012

@8~ Michigan Department of Environmental Quality L----L----L----L----~~ (rev. 10/19/2012, JES)

. : Division - Projected Coordi System: ~ Remediation Superfund Section nate Michigan GeoRef, NAD-83, meters

Site Assessment and Site Management Unit Done in ESRI ArcMap 10.0

Page 71: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

'~<l-t ~

FIGURE 3 GROUNDWATER SAMPLE LOCATIONS

N

W~E -~

s

<., ·, ·. .f:t . • b 200 400 Fe ~ :1 ~- . ~

. I I

Legend

Temporary monitoring we ll 01

Sources: Feature layers from Michigan Geographic Data Library website; site specific 0 Co-located soil boring information-from MDEQ files

Topographic contour SITE INSPECTION WORK PLAN

[Ditl C & H Tamarack Operations Compiled by: John E. Spielberg, 10/12

Michigan Department of Environmental Quality Projected Coordinate System: Michigan GeoRef, NAD-83, meters Remediation Division - Superfund Section Done in ESRI ArcMap 10.1

Site Assessment and Site Management Unit

Page 72: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

FIGURE 4 SOIL/WASTE SAMPLE LOCATIONS

Legend

SS-01 Surficial Soil 01

SB-01 0 Soil Boring 01

..

0 .; - 200 400 Feet I J 1 · I I

Sources: Feature layers from Michigan Geographic Data Library; site specific information from MDEQ files

SITE INSPECTION WORK PLAN C & H Tamarack Operations Compiled by: John E . Spielberg, 10/12

Michigan Department of Environmental Quality Projected Coordinate System: Michigan GeoRef, NAD-83, meters

Remediation Division - Superfund Section Done in ESRI ArcMap 10.1 Site Assessment and Site Management Unit

Page 73: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

Appendix E

Chemical Analysis Data of

Site Inspection Collected Samples

Page 74: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Division: RRD

Report to: JOHN SPIELBERG Lab Work Order # : 21100087

MDEQ-RRD-LANSING Work Site ID : LB041244

CONSTITUTION HALL Site Name : C & H TAMARACK OPERATIONS

525 W. ALLEGAN, LANSING, MI 48909 Received: 11/13/2012

Reported: 12/18/2012

Total: $5,410.00 Collected By: JOHN SPIELBERG

Samples Received :

No: Sample ID Sample Description Matrix: Collection Date

01 AC08207 SS-01 SEDIMENT 11/06/2012

02 AC08208 SS-02 SEDIMENT 11/05/2012

03 AC08209 SS-02 D SEDIMENT 11/05/2012

04 AC08210 SS-03 SEDIMENT 11/05/2012

05 AC08211 SS-03 MS SEDIMENT 11/05/2012

06 AC08212 SS-03 MSD SEDIMENT 11/05/2012

07 AC08213 SS-04 SEDIMENT 11/05/2012

08 AC08214 SS-05 SEDIMENT 11/05/2012

09 AC08215 SS-06 SEDIMENT 11/06/2012

10 AC08216 SS-07 SEDIMENT 11/06/2012

11 AC08217 SS-08 SEDIMENT 11/06/2012

12 AC08218 SS-09 SEDIMENT 11/06/2012

13 AC08219 SS-10 SEDIMENT 11/06/2012

14 AC08220 SS-11 SEDIMENT 11/06/2012

15 AC08221 SS-12 SEDIMENT 11/06/2012

16 AC08222 SS-12 D SEDIMENT 11/06/2012

17 AC08223 SS-13 SEDIMENT 11/06/2012

18 AC08224 SS-14 SEDIMENT 11/06/2012

19 AC08225 SB-01 SEDIMENT 11/05/2012

20 AC08226 SB-02 SEDIMENT 11/05/2012

21 AC08227 SB-02 D SEDIMENT 11/05/2012

22 AC08228 SB-03 SEDIMENT 11/06/2012

23 AC08229 SB-03 MS SEDIMENT 11/06/2012

24 AC08230 SB-03 MSD SEDIMENT 11/06/2012

25 AC08231 SB-04 SEDIMENT 11/06/2012

26 AC08232 SB-05 SEDIMENT 11/05/2012

27 AC08233 SB-06 SEDIMENT 11/05/2012

28 AC08234 SB-08 SEDIMENT 11/06/2012

29 AC08235 SB-09 SEDIMENT 11/06/2012

30 AC08236 SB-10 SEDIMENT 11/05/2012

31 AC08237 SB-11 SEDIMENT 11/06/2012

32 AC08238 SB-12 SEDIMENT 11/06/2012

33 AC08239 W-1 SEDIMENT 11/05/2012

34 AC08240 W-2 SEDIMENT 11/05/2012

Lab Work Order #: 21100087 Page 1 of 106

Page 75: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

I certify that the analysis performed by the MDEQ Environmental Laboratory are accurate and that the laboratory

tests were conducted by methods approved by the U.S. Environmental Protection Agency and other appropriate

regulatory agencies.

George L. Krisztian,

Laboratory Director

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 2 of 106

Page 76: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08207 SS-01

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/17/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

##Weight of sample(grams) 11.26

SURROGATE #Bromofluorobenzene# 116

SURROGATE #Dibromofluoromethane# 136

SURROGATE #Toluene-d8# 127

630-20-6 1,1,1,2-Tetrachloroethane Not Detected 59 50

71-55-6 1,1,1-Trichloroethane Not Detected 59 50

79-34-5 1,1,2,2-Tetrachloroethane Not Detected 59 50

79-00-5 1,1,2-Trichloroethane Not Detected 59 50

75-34-3 1,1-Dichloroethane Not Detected 59 50

75-35-4 1,1-Dichloroethylene Not Detected 59 50

87-61-6 1,2,3-Trichlorobenzene Not Detected 300 7 50

96-18-4 1,2,3-Trichloropropane Not Detected 59 50

526-73-8 1,2,3-Trimethylbenzene Not Detected 59 50

120-82-1 1,2,4-Trichlorobenzene Not Detected 300 7 50

95-63-6 1,2,4-Trimethylbenzene Not Detected 59 50

96-12-8 1,2-Dibromo-3-chloropropane Not Detected 300 50

106-93-4 1,2-Dibromoethane Not Detected 59 Z 50

95-50-1 1,2-Dichlorobenzene Not Detected 59 50

107-06-2 1,2-Dichloroethane Not Detected 59 50

78-87-5 1,2-Dichloropropane Not Detected 59 50

108-67-8 1,3,5-Trimethylbenzene Not Detected 59 50

541-73-1 1,3-Dichlorobenzene Not Detected 59 50

106-46-7 1,4-Dichlorobenzene Not Detected 59 50

78-93-3 2-Butanone (MEK) Not Detected 300 50

591-78-6 2-Hexanone Not Detected 300 50

91-57-6 2-Methylnaphthalene Not Detected 300 X 50

67-64-1 2-Propanone (acetone) Not Detected 1200 5 7 50

108-10-1 4-Methyl-2-pentanone (MIBK) Not Detected 300 50

107-13-1 Acrylonitrile Not Detected 300 Z 50

71-43-2 Benzene Not Detected 59 50

108-86-1 Bromobenzene Not Detected 59 50

74-97-5 Bromochloromethane Not Detected 59 50

75-27-4 Bromodichloromethane Not Detected 59 50

75-25-2 Bromoform Not Detected 59 50

74-83-9 Bromomethane Not Detected 240 50

75-15-0 Carbon disulfide Not Detected 59 50

56-23-5 Carbon tetrachloride Not Detected 59 50

108-90-7 Chlorobenzene Not Detected 59 50

75-00-3 Chloroethane Not Detected 300 50

67-66-3 Chloroform Not Detected 59 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 3 of 106

Page 77: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08207 SS-01

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/17/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

74-87-3 Chloromethane Not Detected 300 50

156-59-2 cis-1,2-Dichloroethylene Not Detected 59 50

10061-01-5 cis-1,3-Dichloropropylene Not Detected 59 50

110-82-7 Cyclohexane Not Detected 300 50

124-48-1 Dibromochloromethane Not Detected 59 50

74-95-3 Dibromomethane Not Detected 59 50

75-71-8 Dichlorodifluoromethane Not Detected 300 50

60-29-7 Diethyl ether Not Detected 240 50

108-20-3 Diisopropyl Ether Not Detected 300 50

100-41-4 Ethylbenzene Not Detected 59 50

637-92-3 Ethyltertiarybutylether Not Detected 300 50

67-72-1 Hexachloroethane Not Detected 300 50

98-82-8 Isopropylbenzene Not Detected 59 50

108383,106423 m & p - Xylene Not Detected 120 50

74-88-4 Methyl iodide Not Detected 59 50

75-09-2 Methylene chloride Not Detected 120 50

1634-04-4 Methyltertiarybutylether Not Detected 59 50

91-20-3 Naphthalene Not Detected 300 X 7 50

104-51-8 n-Butylbenzene Not Detected 59 50

103-65-1 n-Propylbenzene Not Detected 59 50

95-47-6 o-Xylene Not Detected 59 50

99-87-6 p-Isopropyl toluene Not Detected 59 50

135-98-8 sec-Butylbenzene Not Detected 59 50

100-42-5 Styrene Not Detected 59 50

98-06-6 tert-Butylbenzene Not Detected 59 50

75-65-0 tertiary Butyl Alcohol Not Detected 3000 50

994-05-8 tertiaryAmylmethylether Not Detected 300 50

127-18-4 Tetrachloroethylene Not Detected 59 50

109-99-9 Tetrahydrofuran Not Detected 300 50

108-88-3 Toluene Not Detected 59 50

156-60-5 trans-1,2-Dichloroethylene Not Detected 59 50

10061-02-6 trans-1,3-Dichloropropylene Not Detected 59 50

110-57-6 trans-1,4-Dichloro-2-butene Not Detected 300 Z 50

79-01-6 Trichloroethylene Not Detected 59 50

75-69-4 Trichlorofluoromethane Not Detected 59 50

75-01-4 Vinyl chloride Not Detected 59 Z 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 4 of 106

Page 78: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08207 SS-01

CAS# Analyte Name Result Unit RL Qualifier Date Tested Method Analyst

% Total Solids 90.4 % 0.1 11/19/2012 2540B SM JW

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 5 of 106

Page 79: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08208 SS-02

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/16/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

##Weight of sample(grams) 11.44

SURROGATE #Bromofluorobenzene# 143

SURROGATE #Dibromofluoromethane# 189

SURROGATE #Toluene-d8# 169

630-20-6 1,1,1,2-Tetrachloroethane Not Detected 55 50

71-55-6 1,1,1-Trichloroethane Not Detected 55 50

79-34-5 1,1,2,2-Tetrachloroethane Not Detected 55 50

79-00-5 1,1,2-Trichloroethane Not Detected 55 50

75-34-3 1,1-Dichloroethane Not Detected 55 50

75-35-4 1,1-Dichloroethylene Not Detected 55 50

87-61-6 1,2,3-Trichlorobenzene Not Detected 280 7 50

96-18-4 1,2,3-Trichloropropane Not Detected 55 50

526-73-8 1,2,3-Trimethylbenzene 79 55 50

120-82-1 1,2,4-Trichlorobenzene Not Detected 280 7 50

95-63-6 1,2,4-Trimethylbenzene 150 55 50

96-12-8 1,2-Dibromo-3-chloropropane Not Detected 280 50

106-93-4 1,2-Dibromoethane Not Detected 55 Z 50

95-50-1 1,2-Dichlorobenzene Not Detected 55 50

107-06-2 1,2-Dichloroethane Not Detected 55 50

78-87-5 1,2-Dichloropropane Not Detected 55 50

108-67-8 1,3,5-Trimethylbenzene Not Detected 55 50

541-73-1 1,3-Dichlorobenzene Not Detected 55 50

106-46-7 1,4-Dichlorobenzene Not Detected 55 50

78-93-3 2-Butanone (MEK) Not Detected 280 50

591-78-6 2-Hexanone Not Detected 280 50

91-57-6 2-Methylnaphthalene Not Detected 280 X 7 50

67-64-1 2-Propanone (acetone) Not Detected 1100 5 50

108-10-1 4-Methyl-2-pentanone (MIBK) Not Detected 280 50

107-13-1 Acrylonitrile Not Detected 280 Z 50

71-43-2 Benzene Not Detected 55 50

108-86-1 Bromobenzene Not Detected 55 50

74-97-5 Bromochloromethane Not Detected 55 50

75-27-4 Bromodichloromethane Not Detected 55 50

75-25-2 Bromoform Not Detected 55 50

74-83-9 Bromomethane Not Detected 220 50

75-15-0 Carbon disulfide Not Detected 55 50

56-23-5 Carbon tetrachloride Not Detected 55 50

108-90-7 Chlorobenzene Not Detected 55 50

75-00-3 Chloroethane Not Detected 280 50

67-66-3 Chloroform Not Detected 55 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 6 of 106

Page 80: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08208 SS-02

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/16/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

74-87-3 Chloromethane Not Detected 280 50

156-59-2 cis-1,2-Dichloroethylene Not Detected 55 50

10061-01-5 cis-1,3-Dichloropropylene Not Detected 55 50

110-82-7 Cyclohexane Not Detected 280 50

124-48-1 Dibromochloromethane Not Detected 55 50

74-95-3 Dibromomethane Not Detected 55 50

75-71-8 Dichlorodifluoromethane Not Detected 280 50

60-29-7 Diethyl ether Not Detected 220 50

108-20-3 Diisopropyl Ether Not Detected 280 50

100-41-4 Ethylbenzene Not Detected 55 50

637-92-3 Ethyltertiarybutylether Not Detected 280 50

67-72-1 Hexachloroethane Not Detected 280 50

98-82-8 Isopropylbenzene Not Detected 55 50

108383,106423 m & p - Xylene 240 110 50

74-88-4 Methyl iodide Not Detected 55 50

75-09-2 Methylene chloride Not Detected 110 50

1634-04-4 Methyltertiarybutylether Not Detected 55 50

91-20-3 Naphthalene Not Detected 280 X 5 7 50

104-51-8 n-Butylbenzene Not Detected 55 50

103-65-1 n-Propylbenzene Not Detected 55 50

95-47-6 o-Xylene 180 55 50

99-87-6 p-Isopropyl toluene Not Detected 55 50

135-98-8 sec-Butylbenzene Not Detected 55 50

100-42-5 Styrene Not Detected 55 50

98-06-6 tert-Butylbenzene Not Detected 55 50

75-65-0 tertiary Butyl Alcohol Not Detected 2800 50

994-05-8 tertiaryAmylmethylether Not Detected 280 50

127-18-4 Tetrachloroethylene Not Detected 55 50

109-99-9 Tetrahydrofuran Not Detected 280 50

108-88-3 Toluene 170 55 50

156-60-5 trans-1,2-Dichloroethylene Not Detected 55 50

10061-02-6 trans-1,3-Dichloropropylene Not Detected 55 50

110-57-6 trans-1,4-Dichloro-2-butene Not Detected 280 Z 50

79-01-6 Trichloroethylene Not Detected 55 50

75-69-4 Trichlorofluoromethane Not Detected 55 50

75-01-4 Vinyl chloride Not Detected 55 Z 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 7 of 106

Page 81: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08208 SS-02

CAS# Analyte Name Result Unit RL Qualifier Date Tested Method Analyst

% Total Solids 93.0 % 0.1 11/19/2012 2540B SM JW

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 8 of 106

Page 82: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08209 SS-02 D

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/16/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

##Weight of sample(grams) 11.19

SURROGATE #Bromofluorobenzene# 140

SURROGATE #Dibromofluoromethane# 171

SURROGATE #Toluene-d8# 160

630-20-6 1,1,1,2-Tetrachloroethane Not Detected 56 50

71-55-6 1,1,1-Trichloroethane Not Detected 56 50

79-34-5 1,1,2,2-Tetrachloroethane Not Detected 56 50

79-00-5 1,1,2-Trichloroethane Not Detected 56 50

75-34-3 1,1-Dichloroethane Not Detected 56 50

75-35-4 1,1-Dichloroethylene Not Detected 56 50

87-61-6 1,2,3-Trichlorobenzene Not Detected 280 7 50

96-18-4 1,2,3-Trichloropropane Not Detected 56 50

526-73-8 1,2,3-Trimethylbenzene 78 56 50

120-82-1 1,2,4-Trichlorobenzene Not Detected 280 7 50

95-63-6 1,2,4-Trimethylbenzene 180 56 50

96-12-8 1,2-Dibromo-3-chloropropane Not Detected 280 50

106-93-4 1,2-Dibromoethane Not Detected 56 Z 50

95-50-1 1,2-Dichlorobenzene Not Detected 56 50

107-06-2 1,2-Dichloroethane Not Detected 56 50

78-87-5 1,2-Dichloropropane Not Detected 56 50

108-67-8 1,3,5-Trimethylbenzene Not Detected 56 50

541-73-1 1,3-Dichlorobenzene Not Detected 56 50

106-46-7 1,4-Dichlorobenzene Not Detected 56 50

78-93-3 2-Butanone (MEK) Not Detected 280 50

591-78-6 2-Hexanone Not Detected 280 50

91-57-6 2-Methylnaphthalene 520 280 X 7 50

67-64-1 2-Propanone (acetone) Not Detected 1100 5 50

108-10-1 4-Methyl-2-pentanone (MIBK) Not Detected 280 50

107-13-1 Acrylonitrile Not Detected 280 Z 50

71-43-2 Benzene Not Detected 56 50

108-86-1 Bromobenzene Not Detected 56 50

74-97-5 Bromochloromethane Not Detected 56 50

75-27-4 Bromodichloromethane Not Detected 56 50

75-25-2 Bromoform Not Detected 56 50

74-83-9 Bromomethane Not Detected 220 50

75-15-0 Carbon disulfide Not Detected 56 50

56-23-5 Carbon tetrachloride Not Detected 56 50

108-90-7 Chlorobenzene Not Detected 56 50

75-00-3 Chloroethane Not Detected 280 50

67-66-3 Chloroform Not Detected 56 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 9 of 106

Page 83: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08209 SS-02 D

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/16/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

74-87-3 Chloromethane Not Detected 280 50

156-59-2 cis-1,2-Dichloroethylene Not Detected 56 50

10061-01-5 cis-1,3-Dichloropropylene Not Detected 56 50

110-82-7 Cyclohexane Not Detected 280 50

124-48-1 Dibromochloromethane Not Detected 56 50

74-95-3 Dibromomethane Not Detected 56 50

75-71-8 Dichlorodifluoromethane Not Detected 280 50

60-29-7 Diethyl ether Not Detected 220 50

108-20-3 Diisopropyl Ether Not Detected 280 50

100-41-4 Ethylbenzene Not Detected 56 50

637-92-3 Ethyltertiarybutylether Not Detected 280 50

67-72-1 Hexachloroethane Not Detected 280 50

98-82-8 Isopropylbenzene Not Detected 56 50

108383,106423 m & p - Xylene 290 110 50

74-88-4 Methyl iodide Not Detected 56 50

75-09-2 Methylene chloride Not Detected 110 50

1634-04-4 Methyltertiarybutylether Not Detected 56 50

91-20-3 Naphthalene 300 280 X 5 7 50

104-51-8 n-Butylbenzene Not Detected 56 50

103-65-1 n-Propylbenzene Not Detected 56 50

95-47-6 o-Xylene 200 56 50

99-87-6 p-Isopropyl toluene Not Detected 56 50

135-98-8 sec-Butylbenzene Not Detected 56 50

100-42-5 Styrene Not Detected 56 50

98-06-6 tert-Butylbenzene Not Detected 56 50

75-65-0 tertiary Butyl Alcohol Not Detected 2800 50

994-05-8 tertiaryAmylmethylether Not Detected 280 50

127-18-4 Tetrachloroethylene Not Detected 56 50

109-99-9 Tetrahydrofuran Not Detected 280 50

108-88-3 Toluene 240 56 50

156-60-5 trans-1,2-Dichloroethylene Not Detected 56 50

10061-02-6 trans-1,3-Dichloropropylene Not Detected 56 50

110-57-6 trans-1,4-Dichloro-2-butene Not Detected 280 Z 50

79-01-6 Trichloroethylene Not Detected 56 50

75-69-4 Trichlorofluoromethane Not Detected 56 50

75-01-4 Vinyl chloride Not Detected 56 Z 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 10 of 106

Page 84: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08209 SS-02 D

CAS# Analyte Name Result Unit RL Qualifier Date Tested Method Analyst

% Total Solids 93.9 % 0.1 11/19/2012 2540B SM JW

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 11 of 106

Page 85: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08210 SS-03

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/17/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier: P

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

##Weight of sample(grams) 11.06

SURROGATE #Bromofluorobenzene# 178 9

SURROGATE #Dibromofluoromethane# 237 9

SURROGATE #Toluene-d8# 209 9

630-20-6 1,1,1,2-Tetrachloroethane Not Detected 150 50

71-55-6 1,1,1-Trichloroethane Not Detected 150 50

79-34-5 1,1,2,2-Tetrachloroethane Not Detected 150 50

79-00-5 1,1,2-Trichloroethane Not Detected 150 50

75-34-3 1,1-Dichloroethane Not Detected 150 50

75-35-4 1,1-Dichloroethylene Not Detected 150 50

87-61-6 1,2,3-Trichlorobenzene Not Detected 740 7 50

96-18-4 1,2,3-Trichloropropane Not Detected 150 50

526-73-8 1,2,3-Trimethylbenzene Not Detected 150 50

120-82-1 1,2,4-Trichlorobenzene Not Detected 740 7 50

95-63-6 1,2,4-Trimethylbenzene Not Detected 150 50

96-12-8 1,2-Dibromo-3-chloropropane Not Detected 740 50

106-93-4 1,2-Dibromoethane Not Detected 150 Z 50

95-50-1 1,2-Dichlorobenzene Not Detected 150 50

107-06-2 1,2-Dichloroethane Not Detected 150 50

78-87-5 1,2-Dichloropropane Not Detected 150 50

108-67-8 1,3,5-Trimethylbenzene Not Detected 150 50

541-73-1 1,3-Dichlorobenzene Not Detected 150 50

106-46-7 1,4-Dichlorobenzene Not Detected 150 50

78-93-3 2-Butanone (MEK) Not Detected 740 50

591-78-6 2-Hexanone Not Detected 740 50

91-57-6 2-Methylnaphthalene Not Detected 740 X 7 50

67-64-1 2-Propanone (acetone) Not Detected 2900 5 50

108-10-1 4-Methyl-2-pentanone (MIBK) Not Detected 740 50

107-13-1 Acrylonitrile Not Detected 740 Z 50

71-43-2 Benzene Not Detected 150 50

108-86-1 Bromobenzene Not Detected 150 50

74-97-5 Bromochloromethane Not Detected 150 50

75-27-4 Bromodichloromethane Not Detected 150 50

75-25-2 Bromoform Not Detected 150 50

74-83-9 Bromomethane Not Detected 590 50

75-15-0 Carbon disulfide Not Detected 150 50

56-23-5 Carbon tetrachloride Not Detected 150 50

108-90-7 Chlorobenzene Not Detected 150 50

75-00-3 Chloroethane Not Detected 740 50

67-66-3 Chloroform Not Detected 150 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 12 of 106

Page 86: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08210 SS-03

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/17/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier: P

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

74-87-3 Chloromethane Not Detected 740 50

156-59-2 cis-1,2-Dichloroethylene Not Detected 150 50

10061-01-5 cis-1,3-Dichloropropylene Not Detected 150 50

110-82-7 Cyclohexane Not Detected 740 50

124-48-1 Dibromochloromethane Not Detected 150 50

74-95-3 Dibromomethane Not Detected 150 50

75-71-8 Dichlorodifluoromethane Not Detected 740 50

60-29-7 Diethyl ether Not Detected 590 50

108-20-3 Diisopropyl Ether Not Detected 740 50

100-41-4 Ethylbenzene Not Detected 150 50

637-92-3 Ethyltertiarybutylether Not Detected 740 50

67-72-1 Hexachloroethane Not Detected 740 50

98-82-8 Isopropylbenzene Not Detected 150 50

108383,106423 m & p - Xylene Not Detected 290 50

74-88-4 Methyl iodide Not Detected 150 50

75-09-2 Methylene chloride Not Detected 290 50

1634-04-4 Methyltertiarybutylether Not Detected 150 50

91-20-3 Naphthalene Not Detected 740 X 5 7 50

104-51-8 n-Butylbenzene Not Detected 150 50

103-65-1 n-Propylbenzene Not Detected 150 50

95-47-6 o-Xylene Not Detected 150 50

99-87-6 p-Isopropyl toluene Not Detected 150 50

135-98-8 sec-Butylbenzene Not Detected 150 50

100-42-5 Styrene Not Detected 150 50

98-06-6 tert-Butylbenzene Not Detected 150 50

75-65-0 tertiary Butyl Alcohol Not Detected 7400 50

994-05-8 tertiaryAmylmethylether Not Detected 740 50

127-18-4 Tetrachloroethylene Not Detected 150 50

109-99-9 Tetrahydrofuran Not Detected 740 50

108-88-3 Toluene Not Detected 150 50

156-60-5 trans-1,2-Dichloroethylene Not Detected 150 50

10061-02-6 trans-1,3-Dichloropropylene Not Detected 150 50

110-57-6 trans-1,4-Dichloro-2-butene Not Detected 740 Z 50

79-01-6 Trichloroethylene Not Detected 150 50

75-69-4 Trichlorofluoromethane Not Detected 150 50

75-01-4 Vinyl chloride Not Detected 150 Z 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 13 of 106

Page 87: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08210 SS-03

CAS# Analyte Name Result Unit RL Qualifier Date Tested Method Analyst

% Total Solids 50.6 % 0.1 11/19/2012 2540B SM JW

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 14 of 106

Page 88: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08211 SS-03 MS

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/17/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier: P

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

##Weight of sample(grams) 11.06

SURROGATE #Bromofluorobenzene# 169

SURROGATE #Dibromofluoromethane# 223 9

SURROGATE #Toluene-d8# 213 9

630-20-6 1,1,1,2-Tetrachloroethane 7900 150 50

71-55-6 1,1,1-Trichloroethane 7400 150 50

79-34-5 1,1,2,2-Tetrachloroethane 7300 150 50

79-00-5 1,1,2-Trichloroethane 7400 150 50

75-34-3 1,1-Dichloroethane 7100 150 50

75-35-4 1,1-Dichloroethylene 8600 150 50

87-61-6 1,2,3-Trichlorobenzene 7000 740 7 50

96-18-4 1,2,3-Trichloropropane 7800 150 50

526-73-8 1,2,3-Trimethylbenzene 6800 150 50

120-82-1 1,2,4-Trichlorobenzene 6500 740 7 50

95-63-6 1,2,4-Trimethylbenzene 7100 150 50

96-12-8 1,2-Dibromo-3-chloropropane 7200 740 50

106-93-4 1,2-Dibromoethane 7200 150 Z 50

95-50-1 1,2-Dichlorobenzene 6900 150 50

107-06-2 1,2-Dichloroethane 7500 150 50

78-87-5 1,2-Dichloropropane 6900 150 50

108-67-8 1,3,5-Trimethylbenzene 6900 150 50

541-73-1 1,3-Dichlorobenzene 6800 150 50

106-46-7 1,4-Dichlorobenzene 6900 150 50

78-93-3 2-Butanone (MEK) 5700 740 50

591-78-6 2-Hexanone 6600 740 50

91-57-6 2-Methylnaphthalene 6700 740 X 6 7 50

67-64-1 2-Propanone (acetone) 6500 2900 5 50

108-10-1 4-Methyl-2-pentanone (MIBK) 7400 740 50

107-13-1 Acrylonitrile 7300 740 Z 50

71-43-2 Benzene 7000 150 50

108-86-1 Bromobenzene 7000 150 50

74-97-5 Bromochloromethane 7900 150 50

75-27-4 Bromodichloromethane 7200 150 50

75-25-2 Bromoform 7400 150 50

74-83-9 Bromomethane 7700 590 50

75-15-0 Carbon disulfide 8900 150 4 50

56-23-5 Carbon tetrachloride 7200 150 50

108-90-7 Chlorobenzene 7400 150 50

75-00-3 Chloroethane 7900 740 50

67-66-3 Chloroform 7200 150 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 15 of 106

Page 89: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08211 SS-03 MS

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/17/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier: P

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

74-87-3 Chloromethane 6600 740 50

156-59-2 cis-1,2-Dichloroethylene 7100 150 50

10061-01-5 cis-1,3-Dichloropropylene 7000 150 50

110-82-7 Cyclohexane 6600 740 50

124-48-1 Dibromochloromethane 8000 150 50

74-95-3 Dibromomethane 7700 150 50

75-71-8 Dichlorodifluoromethane 5500 740 50

60-29-7 Diethyl ether 7000 590 50

108-20-3 Diisopropyl Ether 6900 740 50

100-41-4 Ethylbenzene 7400 150 50

637-92-3 Ethyltertiarybutylether 7000 740 50

67-72-1 Hexachloroethane 6700 740 50

98-82-8 Isopropylbenzene 7000 150 50

108383,106423 m & p - Xylene 15000 290 50

74-88-4 Methyl iodide 8400 150 50

75-09-2 Methylene chloride 6900 290 50

1634-04-4 Methyltertiarybutylether 7300 150 50

91-20-3 Naphthalene 5300 740 X 5 7 50

104-51-8 n-Butylbenzene 7100 150 50

103-65-1 n-Propylbenzene 6900 150 50

95-47-6 o-Xylene 7400 150 50

99-87-6 p-Isopropyl toluene 7100 150 50

135-98-8 sec-Butylbenzene 7000 150 50

100-42-5 Styrene 7600 150 50

98-06-6 tert-Butylbenzene 7100 150 50

75-65-0 tertiary Butyl Alcohol 31000 7400 50

994-05-8 tertiaryAmylmethylether 7200 740 50

127-18-4 Tetrachloroethylene 7700 150 50

109-99-9 Tetrahydrofuran 6700 740 50

108-88-3 Toluene 7100 150 50

156-60-5 trans-1,2-Dichloroethylene 6900 150 50

10061-02-6 trans-1,3-Dichloropropylene 7100 150 50

110-57-6 trans-1,4-Dichloro-2-butene 5900 740 Z 50

79-01-6 Trichloroethylene 7200 150 50

75-69-4 Trichlorofluoromethane 7600 150 50

75-01-4 Vinyl chloride 6400 150 Z 50

Results are estimated due to high surrogate recovery. Sample is a matrix spike.

Compounds spiked at 7350 ug/Kg, except tertiary butyl alcohol spiked at 36800 ug/Kg & m&p-xylene spiked at 14700 ug/Kg.

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 16 of 106

Page 90: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08211 SS-03 MS

CAS# Analyte Name Result Unit RL Qualifier Date Tested Method Analyst

% Total Solids 50.6 % 0.1 11/19/2012 2540B SM JW

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 17 of 106

Page 91: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08212 SS-03 MSD

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/17/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier: P

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

##Weight of sample(grams) 11.06

SURROGATE #Bromofluorobenzene# 165

SURROGATE #Dibromofluoromethane# 204 9

SURROGATE #Toluene-d8# 198 9

630-20-6 1,1,1,2-Tetrachloroethane 7900 150 50

71-55-6 1,1,1-Trichloroethane 7300 150 50

79-34-5 1,1,2,2-Tetrachloroethane 7900 150 50

79-00-5 1,1,2-Trichloroethane 7700 150 50

75-34-3 1,1-Dichloroethane 7300 150 50

75-35-4 1,1-Dichloroethylene 8900 150 4 50

87-61-6 1,2,3-Trichlorobenzene 8700 740 7 50

96-18-4 1,2,3-Trichloropropane 8400 150 50

526-73-8 1,2,3-Trimethylbenzene 7600 150 50

120-82-1 1,2,4-Trichlorobenzene 8000 740 7 50

95-63-6 1,2,4-Trimethylbenzene 7700 150 50

96-12-8 1,2-Dibromo-3-chloropropane 8100 740 50

106-93-4 1,2-Dibromoethane 8000 150 Z 50

95-50-1 1,2-Dichlorobenzene 7800 150 50

107-06-2 1,2-Dichloroethane 7800 150 50

78-87-5 1,2-Dichloropropane 7000 150 50

108-67-8 1,3,5-Trimethylbenzene 7600 150 50

541-73-1 1,3-Dichlorobenzene 7400 150 50

106-46-7 1,4-Dichlorobenzene 7500 150 50

78-93-3 2-Butanone (MEK) 5800 740 50

591-78-6 2-Hexanone 7200 740 50

91-57-6 2-Methylnaphthalene 9200 740 X 6 7 50

67-64-1 2-Propanone (acetone) 7000 2900 5 50

108-10-1 4-Methyl-2-pentanone (MIBK) 7600 740 50

107-13-1 Acrylonitrile 7600 740 Z 50

71-43-2 Benzene 7200 150 50

108-86-1 Bromobenzene 7400 150 50

74-97-5 Bromochloromethane 7800 150 50

75-27-4 Bromodichloromethane 7700 150 50

75-25-2 Bromoform 7500 150 50

74-83-9 Bromomethane 7800 590 50

75-15-0 Carbon disulfide 9000 150 4 50

56-23-5 Carbon tetrachloride 7100 150 50

108-90-7 Chlorobenzene 7600 150 50

75-00-3 Chloroethane 8400 740 50

67-66-3 Chloroform 7400 150 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 18 of 106

Page 92: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08212 SS-03 MSD

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/17/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier: P

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

74-87-3 Chloromethane 6800 740 50

156-59-2 cis-1,2-Dichloroethylene 7300 150 50

10061-01-5 cis-1,3-Dichloropropylene 7400 150 50

110-82-7 Cyclohexane 6700 740 50

124-48-1 Dibromochloromethane 8200 150 50

74-95-3 Dibromomethane 8000 150 50

75-71-8 Dichlorodifluoromethane 6200 740 50

60-29-7 Diethyl ether 7300 590 50

108-20-3 Diisopropyl Ether 7100 740 50

100-41-4 Ethylbenzene 7500 150 50

637-92-3 Ethyltertiarybutylether 7400 740 50

67-72-1 Hexachloroethane 7300 740 50

98-82-8 Isopropylbenzene 7500 150 50

108383,106423 m & p - Xylene 15000 290 50

74-88-4 Methyl iodide 8500 150 50

75-09-2 Methylene chloride 7200 290 50

1634-04-4 Methyltertiarybutylether 7500 150 50

91-20-3 Naphthalene 7100 740 X 5 7 50

104-51-8 n-Butylbenzene 7800 150 50

103-65-1 n-Propylbenzene 7400 150 50

95-47-6 o-Xylene 7500 150 50

99-87-6 p-Isopropyl toluene 7700 150 50

135-98-8 sec-Butylbenzene 7500 150 50

100-42-5 Styrene 7700 150 50

98-06-6 tert-Butylbenzene 7600 150 50

75-65-0 tertiary Butyl Alcohol 30000 7400 50

994-05-8 tertiaryAmylmethylether 7900 740 50

127-18-4 Tetrachloroethylene 7600 150 50

109-99-9 Tetrahydrofuran 7000 740 50

108-88-3 Toluene 7300 150 50

156-60-5 trans-1,2-Dichloroethylene 7000 150 50

10061-02-6 trans-1,3-Dichloropropylene 7600 150 50

110-57-6 trans-1,4-Dichloro-2-butene 6500 740 Z 50

79-01-6 Trichloroethylene 7600 150 50

75-69-4 Trichlorofluoromethane 7500 150 50

75-01-4 Vinyl chloride 6900 150 Z 50

Results are estimated due to high surrogate recovery. Sample is a matrix spike duplicate.

Compounds spiked at 7350 ug/Kg, except tertiary butyl alcohol spiked at 36800 ug/Kg & m&p-xylene spiked at 14700 ug/Kg.

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 19 of 106

Page 93: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08212 SS-03 MSD

CAS# Analyte Name Result Unit RL Qualifier Date Tested Method Analyst

% Total Solids 50.6 % 0.1 11/19/2012 2540B SM JW

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 20 of 106

Page 94: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08213 SS-04

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/16/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

##Weight of sample(grams) 10.70

SURROGATE #Bromofluorobenzene# 108

SURROGATE #Dibromofluoromethane# 132

SURROGATE #Toluene-d8# 114

630-20-6 1,1,1,2-Tetrachloroethane Not Detected 65 50

71-55-6 1,1,1-Trichloroethane Not Detected 65 50

79-34-5 1,1,2,2-Tetrachloroethane Not Detected 65 50

79-00-5 1,1,2-Trichloroethane Not Detected 65 50

75-34-3 1,1-Dichloroethane Not Detected 65 50

75-35-4 1,1-Dichloroethylene Not Detected 65 50

87-61-6 1,2,3-Trichlorobenzene Not Detected 320 7 50

96-18-4 1,2,3-Trichloropropane Not Detected 65 50

526-73-8 1,2,3-Trimethylbenzene Not Detected 65 50

120-82-1 1,2,4-Trichlorobenzene Not Detected 320 7 50

95-63-6 1,2,4-Trimethylbenzene Not Detected 65 50

96-12-8 1,2-Dibromo-3-chloropropane Not Detected 320 50

106-93-4 1,2-Dibromoethane Not Detected 65 Z 50

95-50-1 1,2-Dichlorobenzene Not Detected 65 50

107-06-2 1,2-Dichloroethane Not Detected 65 50

78-87-5 1,2-Dichloropropane Not Detected 65 50

108-67-8 1,3,5-Trimethylbenzene Not Detected 65 50

541-73-1 1,3-Dichlorobenzene Not Detected 65 50

106-46-7 1,4-Dichlorobenzene Not Detected 65 50

78-93-3 2-Butanone (MEK) Not Detected 320 50

591-78-6 2-Hexanone Not Detected 320 50

91-57-6 2-Methylnaphthalene Not Detected 320 X 7 50

67-64-1 2-Propanone (acetone) Not Detected 1300 5 50

108-10-1 4-Methyl-2-pentanone (MIBK) Not Detected 320 50

107-13-1 Acrylonitrile Not Detected 320 Z 50

71-43-2 Benzene Not Detected 65 50

108-86-1 Bromobenzene Not Detected 65 50

74-97-5 Bromochloromethane Not Detected 65 50

75-27-4 Bromodichloromethane Not Detected 65 50

75-25-2 Bromoform Not Detected 65 50

74-83-9 Bromomethane Not Detected 260 50

75-15-0 Carbon disulfide Not Detected 65 50

56-23-5 Carbon tetrachloride Not Detected 65 50

108-90-7 Chlorobenzene Not Detected 65 50

75-00-3 Chloroethane Not Detected 320 50

67-66-3 Chloroform Not Detected 65 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 21 of 106

Page 95: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08213 SS-04

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/16/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

74-87-3 Chloromethane Not Detected 320 50

156-59-2 cis-1,2-Dichloroethylene Not Detected 65 50

10061-01-5 cis-1,3-Dichloropropylene Not Detected 65 50

110-82-7 Cyclohexane Not Detected 320 50

124-48-1 Dibromochloromethane Not Detected 65 50

74-95-3 Dibromomethane Not Detected 65 50

75-71-8 Dichlorodifluoromethane Not Detected 320 50

60-29-7 Diethyl ether Not Detected 260 50

108-20-3 Diisopropyl Ether Not Detected 320 50

100-41-4 Ethylbenzene Not Detected 65 50

637-92-3 Ethyltertiarybutylether Not Detected 320 50

67-72-1 Hexachloroethane Not Detected 320 50

98-82-8 Isopropylbenzene Not Detected 65 50

108383,106423 m & p - Xylene Not Detected 130 50

74-88-4 Methyl iodide Not Detected 65 50

75-09-2 Methylene chloride Not Detected 130 50

1634-04-4 Methyltertiarybutylether Not Detected 65 50

91-20-3 Naphthalene Not Detected 320 X 5 7 50

104-51-8 n-Butylbenzene Not Detected 65 50

103-65-1 n-Propylbenzene Not Detected 65 50

95-47-6 o-Xylene Not Detected 65 50

99-87-6 p-Isopropyl toluene Not Detected 65 50

135-98-8 sec-Butylbenzene Not Detected 65 50

100-42-5 Styrene Not Detected 65 50

98-06-6 tert-Butylbenzene Not Detected 65 50

75-65-0 tertiary Butyl Alcohol Not Detected 3200 50

994-05-8 tertiaryAmylmethylether Not Detected 320 50

127-18-4 Tetrachloroethylene Not Detected 65 50

109-99-9 Tetrahydrofuran Not Detected 320 50

108-88-3 Toluene Not Detected 65 50

156-60-5 trans-1,2-Dichloroethylene Not Detected 65 50

10061-02-6 trans-1,3-Dichloropropylene Not Detected 65 50

110-57-6 trans-1,4-Dichloro-2-butene Not Detected 320 Z 50

79-01-6 Trichloroethylene Not Detected 65 50

75-69-4 Trichlorofluoromethane Not Detected 65 50

75-01-4 Vinyl chloride Not Detected 65 Z 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 22 of 106

Page 96: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08213 SS-04

CAS# Analyte Name Result Unit RL Qualifier Date Tested Method Analyst

% Total Solids 88.3 % 0.1 11/19/2012 2540B SM JW

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 23 of 106

Page 97: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08214 SS-05

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/16/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

##Weight of sample(grams) 11.14

SURROGATE #Bromofluorobenzene# 105

SURROGATE #Dibromofluoromethane# 128

SURROGATE #Toluene-d8# 114

630-20-6 1,1,1,2-Tetrachloroethane Not Detected 59 50

71-55-6 1,1,1-Trichloroethane Not Detected 59 50

79-34-5 1,1,2,2-Tetrachloroethane Not Detected 59 50

79-00-5 1,1,2-Trichloroethane Not Detected 59 50

75-34-3 1,1-Dichloroethane Not Detected 59 50

75-35-4 1,1-Dichloroethylene Not Detected 59 50

87-61-6 1,2,3-Trichlorobenzene Not Detected 300 7 50

96-18-4 1,2,3-Trichloropropane Not Detected 59 50

526-73-8 1,2,3-Trimethylbenzene Not Detected 59 50

120-82-1 1,2,4-Trichlorobenzene Not Detected 300 7 50

95-63-6 1,2,4-Trimethylbenzene Not Detected 59 50

96-12-8 1,2-Dibromo-3-chloropropane Not Detected 300 50

106-93-4 1,2-Dibromoethane Not Detected 59 Z 50

95-50-1 1,2-Dichlorobenzene Not Detected 59 50

107-06-2 1,2-Dichloroethane Not Detected 59 50

78-87-5 1,2-Dichloropropane Not Detected 59 50

108-67-8 1,3,5-Trimethylbenzene Not Detected 59 50

541-73-1 1,3-Dichlorobenzene Not Detected 59 50

106-46-7 1,4-Dichlorobenzene Not Detected 59 50

78-93-3 2-Butanone (MEK) Not Detected 300 50

591-78-6 2-Hexanone Not Detected 300 50

91-57-6 2-Methylnaphthalene 300 300 X 6 7 50

67-64-1 2-Propanone (acetone) Not Detected 1200 5 50

108-10-1 4-Methyl-2-pentanone (MIBK) Not Detected 300 50

107-13-1 Acrylonitrile Not Detected 300 Z 50

71-43-2 Benzene Not Detected 59 50

108-86-1 Bromobenzene Not Detected 59 50

74-97-5 Bromochloromethane Not Detected 59 50

75-27-4 Bromodichloromethane Not Detected 59 50

75-25-2 Bromoform Not Detected 59 50

74-83-9 Bromomethane Not Detected 240 50

75-15-0 Carbon disulfide Not Detected 59 50

56-23-5 Carbon tetrachloride Not Detected 59 50

108-90-7 Chlorobenzene Not Detected 59 50

75-00-3 Chloroethane Not Detected 300 50

67-66-3 Chloroform Not Detected 59 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 24 of 106

Page 98: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08214 SS-05

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/16/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

74-87-3 Chloromethane Not Detected 300 50

156-59-2 cis-1,2-Dichloroethylene Not Detected 59 50

10061-01-5 cis-1,3-Dichloropropylene Not Detected 59 50

110-82-7 Cyclohexane Not Detected 300 50

124-48-1 Dibromochloromethane Not Detected 59 50

74-95-3 Dibromomethane Not Detected 59 50

75-71-8 Dichlorodifluoromethane Not Detected 300 50

60-29-7 Diethyl ether Not Detected 240 50

108-20-3 Diisopropyl Ether Not Detected 300 50

100-41-4 Ethylbenzene Not Detected 59 50

637-92-3 Ethyltertiarybutylether Not Detected 300 50

67-72-1 Hexachloroethane Not Detected 300 50

98-82-8 Isopropylbenzene Not Detected 59 50

108383,106423 m & p - Xylene Not Detected 120 50

74-88-4 Methyl iodide Not Detected 59 50

75-09-2 Methylene chloride Not Detected 120 50

1634-04-4 Methyltertiarybutylether Not Detected 59 50

91-20-3 Naphthalene Not Detected 300 X 5 7 50

104-51-8 n-Butylbenzene Not Detected 59 50

103-65-1 n-Propylbenzene Not Detected 59 50

95-47-6 o-Xylene Not Detected 59 50

99-87-6 p-Isopropyl toluene Not Detected 59 50

135-98-8 sec-Butylbenzene Not Detected 59 50

100-42-5 Styrene Not Detected 59 50

98-06-6 tert-Butylbenzene Not Detected 59 50

75-65-0 tertiary Butyl Alcohol Not Detected 3000 50

994-05-8 tertiaryAmylmethylether Not Detected 300 50

127-18-4 Tetrachloroethylene Not Detected 59 50

109-99-9 Tetrahydrofuran Not Detected 300 50

108-88-3 Toluene Not Detected 59 50

156-60-5 trans-1,2-Dichloroethylene Not Detected 59 50

10061-02-6 trans-1,3-Dichloropropylene Not Detected 59 50

110-57-6 trans-1,4-Dichloro-2-butene Not Detected 300 Z 50

79-01-6 Trichloroethylene Not Detected 59 50

75-69-4 Trichlorofluoromethane Not Detected 59 50

75-01-4 Vinyl chloride Not Detected 59 Z 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 25 of 106

Page 99: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08214 SS-05

CAS# Analyte Name Result Unit RL Qualifier Date Tested Method Analyst

% Total Solids 91.1 % 0.1 11/19/2012 2540B SM JW

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 26 of 106

Page 100: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08215 SS-06

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/16/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

##Weight of sample(grams) 11.36

SURROGATE #Bromofluorobenzene# 141

SURROGATE #Dibromofluoromethane# 165

SURROGATE #Toluene-d8# 150

630-20-6 1,1,1,2-Tetrachloroethane Not Detected 74 50

71-55-6 1,1,1-Trichloroethane Not Detected 74 50

79-34-5 1,1,2,2-Tetrachloroethane Not Detected 74 50

79-00-5 1,1,2-Trichloroethane Not Detected 74 50

75-34-3 1,1-Dichloroethane Not Detected 74 50

75-35-4 1,1-Dichloroethylene Not Detected 74 50

87-61-6 1,2,3-Trichlorobenzene Not Detected 370 7 50

96-18-4 1,2,3-Trichloropropane Not Detected 74 50

526-73-8 1,2,3-Trimethylbenzene Not Detected 74 50

120-82-1 1,2,4-Trichlorobenzene Not Detected 370 7 50

95-63-6 1,2,4-Trimethylbenzene Not Detected 74 50

96-12-8 1,2-Dibromo-3-chloropropane Not Detected 370 50

106-93-4 1,2-Dibromoethane Not Detected 74 Z 50

95-50-1 1,2-Dichlorobenzene Not Detected 74 50

107-06-2 1,2-Dichloroethane Not Detected 74 50

78-87-5 1,2-Dichloropropane Not Detected 74 50

108-67-8 1,3,5-Trimethylbenzene Not Detected 74 50

541-73-1 1,3-Dichlorobenzene Not Detected 74 50

106-46-7 1,4-Dichlorobenzene Not Detected 74 50

78-93-3 2-Butanone (MEK) Not Detected 370 50

591-78-6 2-Hexanone Not Detected 370 50

91-57-6 2-Methylnaphthalene Not Detected 370 X 7 50

67-64-1 2-Propanone (acetone) Not Detected 1500 5 50

108-10-1 4-Methyl-2-pentanone (MIBK) Not Detected 370 50

107-13-1 Acrylonitrile Not Detected 370 Z 50

71-43-2 Benzene Not Detected 74 50

108-86-1 Bromobenzene Not Detected 74 50

74-97-5 Bromochloromethane Not Detected 74 50

75-27-4 Bromodichloromethane Not Detected 74 50

75-25-2 Bromoform Not Detected 74 50

74-83-9 Bromomethane Not Detected 300 50

75-15-0 Carbon disulfide Not Detected 74 50

56-23-5 Carbon tetrachloride Not Detected 74 50

108-90-7 Chlorobenzene Not Detected 74 50

75-00-3 Chloroethane Not Detected 370 50

67-66-3 Chloroform Not Detected 74 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 27 of 106

Page 101: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08215 SS-06

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/16/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

74-87-3 Chloromethane Not Detected 370 50

156-59-2 cis-1,2-Dichloroethylene Not Detected 74 50

10061-01-5 cis-1,3-Dichloropropylene Not Detected 74 50

110-82-7 Cyclohexane Not Detected 370 50

124-48-1 Dibromochloromethane Not Detected 74 50

74-95-3 Dibromomethane Not Detected 74 50

75-71-8 Dichlorodifluoromethane Not Detected 370 50

60-29-7 Diethyl ether Not Detected 300 50

108-20-3 Diisopropyl Ether Not Detected 370 50

100-41-4 Ethylbenzene Not Detected 74 50

637-92-3 Ethyltertiarybutylether Not Detected 370 50

67-72-1 Hexachloroethane Not Detected 370 50

98-82-8 Isopropylbenzene Not Detected 74 50

108383,106423 m & p - Xylene Not Detected 150 50

74-88-4 Methyl iodide Not Detected 74 50

75-09-2 Methylene chloride Not Detected 150 50

1634-04-4 Methyltertiarybutylether Not Detected 74 50

91-20-3 Naphthalene Not Detected 370 X 5 7 50

104-51-8 n-Butylbenzene Not Detected 74 50

103-65-1 n-Propylbenzene Not Detected 74 50

95-47-6 o-Xylene Not Detected 74 50

99-87-6 p-Isopropyl toluene Not Detected 74 50

135-98-8 sec-Butylbenzene Not Detected 74 50

100-42-5 Styrene Not Detected 74 50

98-06-6 tert-Butylbenzene Not Detected 74 50

75-65-0 tertiary Butyl Alcohol Not Detected 3700 50

994-05-8 tertiaryAmylmethylether Not Detected 370 50

127-18-4 Tetrachloroethylene Not Detected 74 50

109-99-9 Tetrahydrofuran Not Detected 370 50

108-88-3 Toluene Not Detected 74 50

156-60-5 trans-1,2-Dichloroethylene Not Detected 74 50

10061-02-6 trans-1,3-Dichloropropylene Not Detected 74 50

110-57-6 trans-1,4-Dichloro-2-butene Not Detected 370 Z 50

79-01-6 Trichloroethylene Not Detected 74 50

75-69-4 Trichlorofluoromethane Not Detected 74 50

75-01-4 Vinyl chloride Not Detected 74 Z 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 28 of 106

Page 102: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08215 SS-06

CAS# Analyte Name Result Unit RL Qualifier Date Tested Method Analyst

% Total Solids 79.5 % 0.1 11/19/2012 2540B SM JW

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 29 of 106

Page 103: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08216 SS-07

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/16/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

##Weight of sample(grams) 11.04

SURROGATE #Bromofluorobenzene# 112

SURROGATE #Dibromofluoromethane# 132

SURROGATE #Toluene-d8# 120

630-20-6 1,1,1,2-Tetrachloroethane Not Detected 68 50

71-55-6 1,1,1-Trichloroethane Not Detected 68 50

79-34-5 1,1,2,2-Tetrachloroethane Not Detected 68 50

79-00-5 1,1,2-Trichloroethane Not Detected 68 50

75-34-3 1,1-Dichloroethane Not Detected 68 50

75-35-4 1,1-Dichloroethylene Not Detected 68 50

87-61-6 1,2,3-Trichlorobenzene Not Detected 340 7 50

96-18-4 1,2,3-Trichloropropane Not Detected 68 50

526-73-8 1,2,3-Trimethylbenzene Not Detected 68 50

120-82-1 1,2,4-Trichlorobenzene Not Detected 340 7 50

95-63-6 1,2,4-Trimethylbenzene Not Detected 68 50

96-12-8 1,2-Dibromo-3-chloropropane Not Detected 340 50

106-93-4 1,2-Dibromoethane Not Detected 68 Z 50

95-50-1 1,2-Dichlorobenzene Not Detected 68 50

107-06-2 1,2-Dichloroethane Not Detected 68 50

78-87-5 1,2-Dichloropropane Not Detected 68 50

108-67-8 1,3,5-Trimethylbenzene Not Detected 68 50

541-73-1 1,3-Dichlorobenzene Not Detected 68 50

106-46-7 1,4-Dichlorobenzene Not Detected 68 50

78-93-3 2-Butanone (MEK) Not Detected 340 50

591-78-6 2-Hexanone Not Detected 340 50

91-57-6 2-Methylnaphthalene Not Detected 340 X 7 50

67-64-1 2-Propanone (acetone) Not Detected 1400 5 50

108-10-1 4-Methyl-2-pentanone (MIBK) Not Detected 340 50

107-13-1 Acrylonitrile Not Detected 340 Z 50

71-43-2 Benzene Not Detected 68 50

108-86-1 Bromobenzene Not Detected 68 50

74-97-5 Bromochloromethane Not Detected 68 50

75-27-4 Bromodichloromethane Not Detected 68 50

75-25-2 Bromoform Not Detected 68 50

74-83-9 Bromomethane Not Detected 270 50

75-15-0 Carbon disulfide Not Detected 68 50

56-23-5 Carbon tetrachloride Not Detected 68 50

108-90-7 Chlorobenzene Not Detected 68 50

75-00-3 Chloroethane Not Detected 340 50

67-66-3 Chloroform Not Detected 68 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 30 of 106

Page 104: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08216 SS-07

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/16/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

74-87-3 Chloromethane Not Detected 340 50

156-59-2 cis-1,2-Dichloroethylene Not Detected 68 50

10061-01-5 cis-1,3-Dichloropropylene Not Detected 68 50

110-82-7 Cyclohexane Not Detected 340 50

124-48-1 Dibromochloromethane Not Detected 68 50

74-95-3 Dibromomethane Not Detected 68 50

75-71-8 Dichlorodifluoromethane Not Detected 340 50

60-29-7 Diethyl ether Not Detected 270 50

108-20-3 Diisopropyl Ether Not Detected 340 50

100-41-4 Ethylbenzene Not Detected 68 50

637-92-3 Ethyltertiarybutylether Not Detected 340 50

67-72-1 Hexachloroethane Not Detected 340 50

98-82-8 Isopropylbenzene Not Detected 68 50

108383,106423 m & p - Xylene Not Detected 140 50

74-88-4 Methyl iodide Not Detected 68 50

75-09-2 Methylene chloride Not Detected 140 50

1634-04-4 Methyltertiarybutylether Not Detected 68 50

91-20-3 Naphthalene Not Detected 340 X 5 7 50

104-51-8 n-Butylbenzene Not Detected 68 50

103-65-1 n-Propylbenzene Not Detected 68 50

95-47-6 o-Xylene Not Detected 68 50

99-87-6 p-Isopropyl toluene Not Detected 68 50

135-98-8 sec-Butylbenzene Not Detected 68 50

100-42-5 Styrene Not Detected 68 50

98-06-6 tert-Butylbenzene Not Detected 68 50

75-65-0 tertiary Butyl Alcohol Not Detected 3400 50

994-05-8 tertiaryAmylmethylether Not Detected 340 50

127-18-4 Tetrachloroethylene Not Detected 68 50

109-99-9 Tetrahydrofuran Not Detected 340 50

108-88-3 Toluene Not Detected 68 50

156-60-5 trans-1,2-Dichloroethylene Not Detected 68 50

10061-02-6 trans-1,3-Dichloropropylene Not Detected 68 50

110-57-6 trans-1,4-Dichloro-2-butene Not Detected 340 Z 50

79-01-6 Trichloroethylene Not Detected 68 50

75-69-4 Trichlorofluoromethane Not Detected 68 50

75-01-4 Vinyl chloride Not Detected 68 Z 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 31 of 106

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MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08216 SS-07

CAS# Analyte Name Result Unit RL Qualifier Date Tested Method Analyst

% Total Solids 84.5 % 0.1 11/19/2012 2540B SM JW

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 32 of 106

Page 106: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08217 SS-08

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/17/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

##Weight of sample(grams) 10.42

SURROGATE #Bromofluorobenzene# 116

SURROGATE #Dibromofluoromethane# 140

SURROGATE #Toluene-d8# 129

630-20-6 1,1,1,2-Tetrachloroethane Not Detected 81 50

71-55-6 1,1,1-Trichloroethane Not Detected 81 50

79-34-5 1,1,2,2-Tetrachloroethane Not Detected 81 50

79-00-5 1,1,2-Trichloroethane Not Detected 81 50

75-34-3 1,1-Dichloroethane Not Detected 81 50

75-35-4 1,1-Dichloroethylene Not Detected 81 50

87-61-6 1,2,3-Trichlorobenzene Not Detected 400 7 50

96-18-4 1,2,3-Trichloropropane Not Detected 81 50

526-73-8 1,2,3-Trimethylbenzene Not Detected 81 50

120-82-1 1,2,4-Trichlorobenzene Not Detected 400 7 50

95-63-6 1,2,4-Trimethylbenzene Not Detected 81 50

96-12-8 1,2-Dibromo-3-chloropropane Not Detected 400 50

106-93-4 1,2-Dibromoethane Not Detected 81 Z 50

95-50-1 1,2-Dichlorobenzene Not Detected 81 50

107-06-2 1,2-Dichloroethane Not Detected 81 50

78-87-5 1,2-Dichloropropane Not Detected 81 50

108-67-8 1,3,5-Trimethylbenzene Not Detected 81 50

541-73-1 1,3-Dichlorobenzene Not Detected 81 50

106-46-7 1,4-Dichlorobenzene Not Detected 81 50

78-93-3 2-Butanone (MEK) Not Detected 400 50

591-78-6 2-Hexanone Not Detected 400 50

91-57-6 2-Methylnaphthalene Not Detected 400 X 50

67-64-1 2-Propanone (acetone) Not Detected 1600 5 7 50

108-10-1 4-Methyl-2-pentanone (MIBK) Not Detected 400 50

107-13-1 Acrylonitrile Not Detected 400 Z 50

71-43-2 Benzene Not Detected 81 50

108-86-1 Bromobenzene Not Detected 81 50

74-97-5 Bromochloromethane Not Detected 81 50

75-27-4 Bromodichloromethane Not Detected 81 50

75-25-2 Bromoform Not Detected 81 50

74-83-9 Bromomethane Not Detected 320 50

75-15-0 Carbon disulfide Not Detected 81 50

56-23-5 Carbon tetrachloride Not Detected 81 50

108-90-7 Chlorobenzene Not Detected 81 50

75-00-3 Chloroethane Not Detected 400 50

67-66-3 Chloroform Not Detected 81 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 33 of 106

Page 107: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08217 SS-08

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/17/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

74-87-3 Chloromethane Not Detected 400 50

156-59-2 cis-1,2-Dichloroethylene Not Detected 81 50

10061-01-5 cis-1,3-Dichloropropylene Not Detected 81 50

110-82-7 Cyclohexane Not Detected 400 50

124-48-1 Dibromochloromethane Not Detected 81 50

74-95-3 Dibromomethane Not Detected 81 50

75-71-8 Dichlorodifluoromethane Not Detected 400 50

60-29-7 Diethyl ether Not Detected 320 50

108-20-3 Diisopropyl Ether Not Detected 400 50

100-41-4 Ethylbenzene Not Detected 81 50

637-92-3 Ethyltertiarybutylether Not Detected 400 50

67-72-1 Hexachloroethane Not Detected 400 50

98-82-8 Isopropylbenzene Not Detected 81 50

108383,106423 m & p - Xylene Not Detected 160 50

74-88-4 Methyl iodide Not Detected 81 50

75-09-2 Methylene chloride Not Detected 160 50

1634-04-4 Methyltertiarybutylether Not Detected 81 50

91-20-3 Naphthalene Not Detected 400 X 7 50

104-51-8 n-Butylbenzene Not Detected 81 50

103-65-1 n-Propylbenzene Not Detected 81 50

95-47-6 o-Xylene Not Detected 81 50

99-87-6 p-Isopropyl toluene Not Detected 81 50

135-98-8 sec-Butylbenzene Not Detected 81 50

100-42-5 Styrene Not Detected 81 50

98-06-6 tert-Butylbenzene Not Detected 81 50

75-65-0 tertiary Butyl Alcohol Not Detected 4000 50

994-05-8 tertiaryAmylmethylether Not Detected 400 50

127-18-4 Tetrachloroethylene Not Detected 81 50

109-99-9 Tetrahydrofuran Not Detected 400 50

108-88-3 Toluene Not Detected 81 50

156-60-5 trans-1,2-Dichloroethylene Not Detected 81 50

10061-02-6 trans-1,3-Dichloropropylene Not Detected 81 50

110-57-6 trans-1,4-Dichloro-2-butene Not Detected 400 Z 50

79-01-6 Trichloroethylene Not Detected 81 50

75-69-4 Trichlorofluoromethane Not Detected 81 50

75-01-4 Vinyl chloride Not Detected 81 Z 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 34 of 106

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MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08217 SS-08

CAS# Analyte Name Result Unit RL Qualifier Date Tested Method Analyst

% Total Solids 75.0 % 0.1 11/19/2012 2540B SM JW

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 35 of 106

Page 109: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08218 SS-09

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/16/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

##Weight of sample(grams) 11.54

SURROGATE #Bromofluorobenzene# 106

SURROGATE #Dibromofluoromethane# 129

SURROGATE #Toluene-d8# 114

630-20-6 1,1,1,2-Tetrachloroethane Not Detected 55 50

71-55-6 1,1,1-Trichloroethane Not Detected 55 50

79-34-5 1,1,2,2-Tetrachloroethane Not Detected 55 50

79-00-5 1,1,2-Trichloroethane Not Detected 55 50

75-34-3 1,1-Dichloroethane Not Detected 55 50

75-35-4 1,1-Dichloroethylene Not Detected 55 50

87-61-6 1,2,3-Trichlorobenzene Not Detected 270 7 50

96-18-4 1,2,3-Trichloropropane Not Detected 55 50

526-73-8 1,2,3-Trimethylbenzene Not Detected 55 50

120-82-1 1,2,4-Trichlorobenzene Not Detected 270 7 50

95-63-6 1,2,4-Trimethylbenzene Not Detected 55 50

96-12-8 1,2-Dibromo-3-chloropropane Not Detected 270 50

106-93-4 1,2-Dibromoethane Not Detected 55 Z 50

95-50-1 1,2-Dichlorobenzene Not Detected 55 50

107-06-2 1,2-Dichloroethane Not Detected 55 50

78-87-5 1,2-Dichloropropane Not Detected 55 50

108-67-8 1,3,5-Trimethylbenzene Not Detected 55 50

541-73-1 1,3-Dichlorobenzene Not Detected 55 50

106-46-7 1,4-Dichlorobenzene Not Detected 55 50

78-93-3 2-Butanone (MEK) Not Detected 270 50

591-78-6 2-Hexanone Not Detected 270 50

91-57-6 2-Methylnaphthalene Not Detected 270 X 7 50

67-64-1 2-Propanone (acetone) Not Detected 1100 5 50

108-10-1 4-Methyl-2-pentanone (MIBK) Not Detected 270 50

107-13-1 Acrylonitrile Not Detected 270 Z 50

71-43-2 Benzene Not Detected 55 50

108-86-1 Bromobenzene Not Detected 55 50

74-97-5 Bromochloromethane Not Detected 55 50

75-27-4 Bromodichloromethane Not Detected 55 50

75-25-2 Bromoform Not Detected 55 50

74-83-9 Bromomethane Not Detected 220 50

75-15-0 Carbon disulfide Not Detected 55 50

56-23-5 Carbon tetrachloride Not Detected 55 50

108-90-7 Chlorobenzene Not Detected 55 50

75-00-3 Chloroethane Not Detected 270 50

67-66-3 Chloroform Not Detected 55 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 36 of 106

Page 110: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08218 SS-09

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/16/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

74-87-3 Chloromethane Not Detected 270 50

156-59-2 cis-1,2-Dichloroethylene Not Detected 55 50

10061-01-5 cis-1,3-Dichloropropylene Not Detected 55 50

110-82-7 Cyclohexane Not Detected 270 50

124-48-1 Dibromochloromethane Not Detected 55 50

74-95-3 Dibromomethane Not Detected 55 50

75-71-8 Dichlorodifluoromethane Not Detected 270 50

60-29-7 Diethyl ether Not Detected 220 50

108-20-3 Diisopropyl Ether Not Detected 270 50

100-41-4 Ethylbenzene Not Detected 55 50

637-92-3 Ethyltertiarybutylether Not Detected 270 50

67-72-1 Hexachloroethane Not Detected 270 50

98-82-8 Isopropylbenzene Not Detected 55 50

108383,106423 m & p - Xylene Not Detected 110 50

74-88-4 Methyl iodide Not Detected 55 50

75-09-2 Methylene chloride Not Detected 110 50

1634-04-4 Methyltertiarybutylether Not Detected 55 50

91-20-3 Naphthalene Not Detected 270 X 5 7 50

104-51-8 n-Butylbenzene Not Detected 55 50

103-65-1 n-Propylbenzene Not Detected 55 50

95-47-6 o-Xylene Not Detected 55 50

99-87-6 p-Isopropyl toluene Not Detected 55 50

135-98-8 sec-Butylbenzene Not Detected 55 50

100-42-5 Styrene Not Detected 55 50

98-06-6 tert-Butylbenzene Not Detected 55 50

75-65-0 tertiary Butyl Alcohol Not Detected 2700 50

994-05-8 tertiaryAmylmethylether Not Detected 270 50

127-18-4 Tetrachloroethylene Not Detected 55 50

109-99-9 Tetrahydrofuran Not Detected 270 50

108-88-3 Toluene Not Detected 55 50

156-60-5 trans-1,2-Dichloroethylene Not Detected 55 50

10061-02-6 trans-1,3-Dichloropropylene Not Detected 55 50

110-57-6 trans-1,4-Dichloro-2-butene Not Detected 270 Z 50

79-01-6 Trichloroethylene Not Detected 55 50

75-69-4 Trichlorofluoromethane Not Detected 55 50

75-01-4 Vinyl chloride Not Detected 55 Z 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 37 of 106

Page 111: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08218 SS-09

CAS# Analyte Name Result Unit RL Qualifier Date Tested Method Analyst

% Total Solids 97.6 % 0.1 11/19/2012 2540B SM JW

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 38 of 106

Page 112: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08219 SS-10

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/17/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

##Weight of sample(grams) 10.97

SURROGATE #Bromofluorobenzene# 121

SURROGATE #Dibromofluoromethane# 146

SURROGATE #Toluene-d8# 128

630-20-6 1,1,1,2-Tetrachloroethane Not Detected 99 50

71-55-6 1,1,1-Trichloroethane Not Detected 99 50

79-34-5 1,1,2,2-Tetrachloroethane Not Detected 99 50

79-00-5 1,1,2-Trichloroethane Not Detected 99 50

75-34-3 1,1-Dichloroethane Not Detected 99 50

75-35-4 1,1-Dichloroethylene Not Detected 99 50

87-61-6 1,2,3-Trichlorobenzene Not Detected 500 7 50

96-18-4 1,2,3-Trichloropropane Not Detected 99 50

526-73-8 1,2,3-Trimethylbenzene Not Detected 99 50

120-82-1 1,2,4-Trichlorobenzene Not Detected 500 7 50

95-63-6 1,2,4-Trimethylbenzene Not Detected 99 50

96-12-8 1,2-Dibromo-3-chloropropane Not Detected 500 50

106-93-4 1,2-Dibromoethane Not Detected 99 Z 50

95-50-1 1,2-Dichlorobenzene Not Detected 99 50

107-06-2 1,2-Dichloroethane Not Detected 99 50

78-87-5 1,2-Dichloropropane Not Detected 99 50

108-67-8 1,3,5-Trimethylbenzene Not Detected 99 50

541-73-1 1,3-Dichlorobenzene Not Detected 99 50

106-46-7 1,4-Dichlorobenzene Not Detected 99 50

78-93-3 2-Butanone (MEK) Not Detected 500 50

591-78-6 2-Hexanone Not Detected 500 50

91-57-6 2-Methylnaphthalene Not Detected 500 X 50

67-64-1 2-Propanone (acetone) Not Detected 2000 5 7 50

108-10-1 4-Methyl-2-pentanone (MIBK) Not Detected 500 50

107-13-1 Acrylonitrile Not Detected 500 Z 50

71-43-2 Benzene Not Detected 99 50

108-86-1 Bromobenzene Not Detected 99 50

74-97-5 Bromochloromethane Not Detected 99 50

75-27-4 Bromodichloromethane Not Detected 99 50

75-25-2 Bromoform Not Detected 99 50

74-83-9 Bromomethane Not Detected 400 50

75-15-0 Carbon disulfide Not Detected 99 50

56-23-5 Carbon tetrachloride Not Detected 99 50

108-90-7 Chlorobenzene Not Detected 99 50

75-00-3 Chloroethane Not Detected 500 50

67-66-3 Chloroform Not Detected 99 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 39 of 106

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MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08219 SS-10

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/17/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

74-87-3 Chloromethane Not Detected 500 50

156-59-2 cis-1,2-Dichloroethylene Not Detected 99 50

10061-01-5 cis-1,3-Dichloropropylene Not Detected 99 50

110-82-7 Cyclohexane Not Detected 500 50

124-48-1 Dibromochloromethane Not Detected 99 50

74-95-3 Dibromomethane Not Detected 99 50

75-71-8 Dichlorodifluoromethane Not Detected 500 50

60-29-7 Diethyl ether Not Detected 400 50

108-20-3 Diisopropyl Ether Not Detected 500 50

100-41-4 Ethylbenzene Not Detected 99 50

637-92-3 Ethyltertiarybutylether Not Detected 500 50

67-72-1 Hexachloroethane Not Detected 500 50

98-82-8 Isopropylbenzene Not Detected 99 50

108383,106423 m & p - Xylene Not Detected 200 50

74-88-4 Methyl iodide Not Detected 99 50

75-09-2 Methylene chloride Not Detected 200 50

1634-04-4 Methyltertiarybutylether Not Detected 99 50

91-20-3 Naphthalene Not Detected 500 X 7 50

104-51-8 n-Butylbenzene Not Detected 99 50

103-65-1 n-Propylbenzene Not Detected 99 50

95-47-6 o-Xylene Not Detected 99 50

99-87-6 p-Isopropyl toluene Not Detected 99 50

135-98-8 sec-Butylbenzene Not Detected 99 50

100-42-5 Styrene Not Detected 99 50

98-06-6 tert-Butylbenzene Not Detected 99 50

75-65-0 tertiary Butyl Alcohol Not Detected 5000 50

994-05-8 tertiaryAmylmethylether Not Detected 500 50

127-18-4 Tetrachloroethylene Not Detected 99 50

109-99-9 Tetrahydrofuran Not Detected 500 50

108-88-3 Toluene Not Detected 99 50

156-60-5 trans-1,2-Dichloroethylene Not Detected 99 50

10061-02-6 trans-1,3-Dichloropropylene Not Detected 99 50

110-57-6 trans-1,4-Dichloro-2-butene Not Detected 500 Z 50

79-01-6 Trichloroethylene Not Detected 99 50

75-69-4 Trichlorofluoromethane Not Detected 99 50

75-01-4 Vinyl chloride Not Detected 99 Z 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 40 of 106

Page 114: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08219 SS-10

CAS# Analyte Name Result Unit RL Qualifier Date Tested Method Analyst

% Total Solids 67.1 % 0.1 11/19/2012 2540B SM JW

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 41 of 106

Page 115: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08220 SS-11

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/17/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

##Weight of sample(grams) 11.38

SURROGATE #Bromofluorobenzene# 129

SURROGATE #Dibromofluoromethane# 159

SURROGATE #Toluene-d8# 141

630-20-6 1,1,1,2-Tetrachloroethane Not Detected 64 50

71-55-6 1,1,1-Trichloroethane Not Detected 64 50

79-34-5 1,1,2,2-Tetrachloroethane Not Detected 64 50

79-00-5 1,1,2-Trichloroethane Not Detected 64 50

75-34-3 1,1-Dichloroethane Not Detected 64 50

75-35-4 1,1-Dichloroethylene Not Detected 64 50

87-61-6 1,2,3-Trichlorobenzene Not Detected 320 7 50

96-18-4 1,2,3-Trichloropropane Not Detected 64 50

526-73-8 1,2,3-Trimethylbenzene Not Detected 64 50

120-82-1 1,2,4-Trichlorobenzene Not Detected 320 7 50

95-63-6 1,2,4-Trimethylbenzene Not Detected 64 50

96-12-8 1,2-Dibromo-3-chloropropane Not Detected 320 50

106-93-4 1,2-Dibromoethane Not Detected 64 Z 50

95-50-1 1,2-Dichlorobenzene Not Detected 64 50

107-06-2 1,2-Dichloroethane Not Detected 64 50

78-87-5 1,2-Dichloropropane Not Detected 64 50

108-67-8 1,3,5-Trimethylbenzene Not Detected 64 50

541-73-1 1,3-Dichlorobenzene Not Detected 64 50

106-46-7 1,4-Dichlorobenzene Not Detected 64 50

78-93-3 2-Butanone (MEK) Not Detected 320 50

591-78-6 2-Hexanone Not Detected 320 50

91-57-6 2-Methylnaphthalene Not Detected 320 X 50

67-64-1 2-Propanone (acetone) Not Detected 1300 5 7 50

108-10-1 4-Methyl-2-pentanone (MIBK) Not Detected 320 50

107-13-1 Acrylonitrile Not Detected 320 Z 50

71-43-2 Benzene Not Detected 64 50

108-86-1 Bromobenzene Not Detected 64 50

74-97-5 Bromochloromethane Not Detected 64 50

75-27-4 Bromodichloromethane Not Detected 64 50

75-25-2 Bromoform Not Detected 64 50

74-83-9 Bromomethane Not Detected 260 50

75-15-0 Carbon disulfide Not Detected 64 50

56-23-5 Carbon tetrachloride Not Detected 64 50

108-90-7 Chlorobenzene Not Detected 64 50

75-00-3 Chloroethane Not Detected 320 50

67-66-3 Chloroform Not Detected 64 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 42 of 106

Page 116: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08220 SS-11

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/17/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

74-87-3 Chloromethane Not Detected 320 50

156-59-2 cis-1,2-Dichloroethylene Not Detected 64 50

10061-01-5 cis-1,3-Dichloropropylene Not Detected 64 50

110-82-7 Cyclohexane Not Detected 320 50

124-48-1 Dibromochloromethane Not Detected 64 50

74-95-3 Dibromomethane Not Detected 64 50

75-71-8 Dichlorodifluoromethane Not Detected 320 50

60-29-7 Diethyl ether Not Detected 260 50

108-20-3 Diisopropyl Ether Not Detected 320 50

100-41-4 Ethylbenzene Not Detected 64 50

637-92-3 Ethyltertiarybutylether Not Detected 320 50

67-72-1 Hexachloroethane Not Detected 320 50

98-82-8 Isopropylbenzene Not Detected 64 50

108383,106423 m & p - Xylene Not Detected 130 50

74-88-4 Methyl iodide Not Detected 64 50

75-09-2 Methylene chloride Not Detected 130 50

1634-04-4 Methyltertiarybutylether Not Detected 64 50

91-20-3 Naphthalene Not Detected 320 X 7 50

104-51-8 n-Butylbenzene Not Detected 64 50

103-65-1 n-Propylbenzene Not Detected 64 50

95-47-6 o-Xylene Not Detected 64 50

99-87-6 p-Isopropyl toluene Not Detected 64 50

135-98-8 sec-Butylbenzene Not Detected 64 50

100-42-5 Styrene Not Detected 64 50

98-06-6 tert-Butylbenzene Not Detected 64 50

75-65-0 tertiary Butyl Alcohol Not Detected 3200 50

994-05-8 tertiaryAmylmethylether Not Detected 320 50

127-18-4 Tetrachloroethylene Not Detected 64 50

109-99-9 Tetrahydrofuran Not Detected 320 50

108-88-3 Toluene Not Detected 64 50

156-60-5 trans-1,2-Dichloroethylene Not Detected 64 50

10061-02-6 trans-1,3-Dichloropropylene Not Detected 64 50

110-57-6 trans-1,4-Dichloro-2-butene Not Detected 320 Z 50

79-01-6 Trichloroethylene Not Detected 64 50

75-69-4 Trichlorofluoromethane Not Detected 64 50

75-01-4 Vinyl chloride Not Detected 64 Z 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 43 of 106

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MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08220 SS-11

CAS# Analyte Name Result Unit RL Qualifier Date Tested Method Analyst

% Total Solids 86.3 % 0.1 11/19/2012 2540B SM JW

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 44 of 106

Page 118: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08221 SS-12

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/17/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

##Weight of sample(grams) 11.04

SURROGATE #Bromofluorobenzene# 105

SURROGATE #Dibromofluoromethane# 130

SURROGATE #Toluene-d8# 111

630-20-6 1,1,1,2-Tetrachloroethane Not Detected 60 50

71-55-6 1,1,1-Trichloroethane Not Detected 60 50

79-34-5 1,1,2,2-Tetrachloroethane Not Detected 60 50

79-00-5 1,1,2-Trichloroethane Not Detected 60 50

75-34-3 1,1-Dichloroethane Not Detected 60 50

75-35-4 1,1-Dichloroethylene Not Detected 60 50

87-61-6 1,2,3-Trichlorobenzene Not Detected 300 7 50

96-18-4 1,2,3-Trichloropropane Not Detected 60 50

526-73-8 1,2,3-Trimethylbenzene Not Detected 60 50

120-82-1 1,2,4-Trichlorobenzene Not Detected 300 7 50

95-63-6 1,2,4-Trimethylbenzene Not Detected 60 50

96-12-8 1,2-Dibromo-3-chloropropane Not Detected 300 50

106-93-4 1,2-Dibromoethane Not Detected 60 Z 50

95-50-1 1,2-Dichlorobenzene Not Detected 60 50

107-06-2 1,2-Dichloroethane Not Detected 60 50

78-87-5 1,2-Dichloropropane Not Detected 60 50

108-67-8 1,3,5-Trimethylbenzene Not Detected 60 50

541-73-1 1,3-Dichlorobenzene Not Detected 60 50

106-46-7 1,4-Dichlorobenzene Not Detected 60 50

78-93-3 2-Butanone (MEK) Not Detected 300 50

591-78-6 2-Hexanone Not Detected 300 50

91-57-6 2-Methylnaphthalene Not Detected 300 X 50

67-64-1 2-Propanone (acetone) Not Detected 1200 5 7 50

108-10-1 4-Methyl-2-pentanone (MIBK) Not Detected 300 50

107-13-1 Acrylonitrile Not Detected 300 Z 50

71-43-2 Benzene Not Detected 60 50

108-86-1 Bromobenzene Not Detected 60 50

74-97-5 Bromochloromethane Not Detected 60 50

75-27-4 Bromodichloromethane Not Detected 60 50

75-25-2 Bromoform Not Detected 60 50

74-83-9 Bromomethane Not Detected 240 50

75-15-0 Carbon disulfide Not Detected 60 50

56-23-5 Carbon tetrachloride Not Detected 60 50

108-90-7 Chlorobenzene Not Detected 60 50

75-00-3 Chloroethane Not Detected 300 50

67-66-3 Chloroform Not Detected 60 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 45 of 106

Page 119: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08221 SS-12

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/17/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

74-87-3 Chloromethane Not Detected 300 50

156-59-2 cis-1,2-Dichloroethylene Not Detected 60 50

10061-01-5 cis-1,3-Dichloropropylene Not Detected 60 50

110-82-7 Cyclohexane Not Detected 300 50

124-48-1 Dibromochloromethane Not Detected 60 50

74-95-3 Dibromomethane Not Detected 60 50

75-71-8 Dichlorodifluoromethane Not Detected 300 50

60-29-7 Diethyl ether Not Detected 240 50

108-20-3 Diisopropyl Ether Not Detected 300 50

100-41-4 Ethylbenzene Not Detected 60 50

637-92-3 Ethyltertiarybutylether Not Detected 300 50

67-72-1 Hexachloroethane Not Detected 300 50

98-82-8 Isopropylbenzene Not Detected 60 50

108383,106423 m & p - Xylene Not Detected 120 50

74-88-4 Methyl iodide Not Detected 60 50

75-09-2 Methylene chloride Not Detected 120 50

1634-04-4 Methyltertiarybutylether Not Detected 60 50

91-20-3 Naphthalene Not Detected 300 X 7 50

104-51-8 n-Butylbenzene Not Detected 60 50

103-65-1 n-Propylbenzene Not Detected 60 50

95-47-6 o-Xylene Not Detected 60 50

99-87-6 p-Isopropyl toluene Not Detected 60 50

135-98-8 sec-Butylbenzene Not Detected 60 50

100-42-5 Styrene Not Detected 60 50

98-06-6 tert-Butylbenzene Not Detected 60 50

75-65-0 tertiary Butyl Alcohol Not Detected 3000 50

994-05-8 tertiaryAmylmethylether Not Detected 300 50

127-18-4 Tetrachloroethylene Not Detected 60 50

109-99-9 Tetrahydrofuran Not Detected 300 50

108-88-3 Toluene Not Detected 60 50

156-60-5 trans-1,2-Dichloroethylene Not Detected 60 50

10061-02-6 trans-1,3-Dichloropropylene Not Detected 60 50

110-57-6 trans-1,4-Dichloro-2-butene Not Detected 300 Z 50

79-01-6 Trichloroethylene Not Detected 60 50

75-69-4 Trichlorofluoromethane Not Detected 60 50

75-01-4 Vinyl chloride Not Detected 60 Z 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 46 of 106

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MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08221 SS-12

CAS# Analyte Name Result Unit RL Qualifier Date Tested Method Analyst

% Total Solids 90.9 % 0.1 11/19/2012 2540B SM JW

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 47 of 106

Page 121: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08222 SS-12 D

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/17/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

##Weight of sample(grams) 11.07

SURROGATE #Bromofluorobenzene# 109

SURROGATE #Dibromofluoromethane# 127

SURROGATE #Toluene-d8# 119

630-20-6 1,1,1,2-Tetrachloroethane Not Detected 57 50

71-55-6 1,1,1-Trichloroethane Not Detected 57 50

79-34-5 1,1,2,2-Tetrachloroethane Not Detected 57 50

79-00-5 1,1,2-Trichloroethane Not Detected 57 50

75-34-3 1,1-Dichloroethane Not Detected 57 50

75-35-4 1,1-Dichloroethylene Not Detected 57 50

87-61-6 1,2,3-Trichlorobenzene Not Detected 280 7 50

96-18-4 1,2,3-Trichloropropane Not Detected 57 50

526-73-8 1,2,3-Trimethylbenzene Not Detected 57 50

120-82-1 1,2,4-Trichlorobenzene Not Detected 280 7 50

95-63-6 1,2,4-Trimethylbenzene Not Detected 57 50

96-12-8 1,2-Dibromo-3-chloropropane Not Detected 280 50

106-93-4 1,2-Dibromoethane Not Detected 57 Z 50

95-50-1 1,2-Dichlorobenzene Not Detected 57 50

107-06-2 1,2-Dichloroethane Not Detected 57 50

78-87-5 1,2-Dichloropropane Not Detected 57 50

108-67-8 1,3,5-Trimethylbenzene Not Detected 57 50

541-73-1 1,3-Dichlorobenzene Not Detected 57 50

106-46-7 1,4-Dichlorobenzene Not Detected 57 50

78-93-3 2-Butanone (MEK) Not Detected 280 50

591-78-6 2-Hexanone Not Detected 280 50

91-57-6 2-Methylnaphthalene Not Detected 280 X 50

67-64-1 2-Propanone (acetone) Not Detected 1100 5 7 50

108-10-1 4-Methyl-2-pentanone (MIBK) Not Detected 280 50

107-13-1 Acrylonitrile Not Detected 280 Z 50

71-43-2 Benzene Not Detected 57 50

108-86-1 Bromobenzene Not Detected 57 50

74-97-5 Bromochloromethane Not Detected 57 50

75-27-4 Bromodichloromethane Not Detected 57 50

75-25-2 Bromoform Not Detected 57 50

74-83-9 Bromomethane Not Detected 230 50

75-15-0 Carbon disulfide Not Detected 57 50

56-23-5 Carbon tetrachloride Not Detected 57 50

108-90-7 Chlorobenzene Not Detected 57 50

75-00-3 Chloroethane Not Detected 280 50

67-66-3 Chloroform Not Detected 57 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 48 of 106

Page 122: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08222 SS-12 D

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/17/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

74-87-3 Chloromethane Not Detected 280 50

156-59-2 cis-1,2-Dichloroethylene Not Detected 57 50

10061-01-5 cis-1,3-Dichloropropylene Not Detected 57 50

110-82-7 Cyclohexane Not Detected 280 50

124-48-1 Dibromochloromethane Not Detected 57 50

74-95-3 Dibromomethane Not Detected 57 50

75-71-8 Dichlorodifluoromethane Not Detected 280 50

60-29-7 Diethyl ether Not Detected 230 50

108-20-3 Diisopropyl Ether Not Detected 280 50

100-41-4 Ethylbenzene Not Detected 57 50

637-92-3 Ethyltertiarybutylether Not Detected 280 50

67-72-1 Hexachloroethane Not Detected 280 50

98-82-8 Isopropylbenzene Not Detected 57 50

108383,106423 m & p - Xylene Not Detected 110 50

74-88-4 Methyl iodide Not Detected 57 50

75-09-2 Methylene chloride Not Detected 110 50

1634-04-4 Methyltertiarybutylether Not Detected 57 50

91-20-3 Naphthalene Not Detected 280 X 7 50

104-51-8 n-Butylbenzene Not Detected 57 50

103-65-1 n-Propylbenzene Not Detected 57 50

95-47-6 o-Xylene Not Detected 57 50

99-87-6 p-Isopropyl toluene Not Detected 57 50

135-98-8 sec-Butylbenzene Not Detected 57 50

100-42-5 Styrene Not Detected 57 50

98-06-6 tert-Butylbenzene Not Detected 57 50

75-65-0 tertiary Butyl Alcohol Not Detected 2800 50

994-05-8 tertiaryAmylmethylether Not Detected 280 50

127-18-4 Tetrachloroethylene Not Detected 57 50

109-99-9 Tetrahydrofuran Not Detected 280 50

108-88-3 Toluene Not Detected 57 50

156-60-5 trans-1,2-Dichloroethylene Not Detected 57 50

10061-02-6 trans-1,3-Dichloropropylene Not Detected 57 50

110-57-6 trans-1,4-Dichloro-2-butene Not Detected 280 Z 50

79-01-6 Trichloroethylene Not Detected 57 50

75-69-4 Trichlorofluoromethane Not Detected 57 50

75-01-4 Vinyl chloride Not Detected 57 Z 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 49 of 106

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MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08222 SS-12 D

CAS# Analyte Name Result Unit RL Qualifier Date Tested Method Analyst

% Total Solids 93.3 % 0.1 11/19/2012 2540B SM JW

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 50 of 106

Page 124: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08223 SS-13

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/17/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

##Weight of sample(grams) 9.97

SURROGATE #Bromofluorobenzene# 191 9

SURROGATE #Dibromofluoromethane# 227 9

SURROGATE #Toluene-d8# 200 9

630-20-6 1,1,1,2-Tetrachloroethane Not Detected 65 50

71-55-6 1,1,1-Trichloroethane Not Detected 65 50

79-34-5 1,1,2,2-Tetrachloroethane Not Detected 65 50

79-00-5 1,1,2-Trichloroethane Not Detected 65 50

75-34-3 1,1-Dichloroethane Not Detected 65 50

75-35-4 1,1-Dichloroethylene Not Detected 65 50

87-61-6 1,2,3-Trichlorobenzene Not Detected 320 7 50

96-18-4 1,2,3-Trichloropropane Not Detected 65 50

526-73-8 1,2,3-Trimethylbenzene Not Detected 65 50

120-82-1 1,2,4-Trichlorobenzene Not Detected 320 7 50

95-63-6 1,2,4-Trimethylbenzene Not Detected 65 50

96-12-8 1,2-Dibromo-3-chloropropane Not Detected 320 50

106-93-4 1,2-Dibromoethane Not Detected 65 Z 50

95-50-1 1,2-Dichlorobenzene Not Detected 65 50

107-06-2 1,2-Dichloroethane Not Detected 65 50

78-87-5 1,2-Dichloropropane Not Detected 65 50

108-67-8 1,3,5-Trimethylbenzene Not Detected 65 50

541-73-1 1,3-Dichlorobenzene Not Detected 65 50

106-46-7 1,4-Dichlorobenzene Not Detected 65 50

78-93-3 2-Butanone (MEK) Not Detected 320 50

591-78-6 2-Hexanone Not Detected 320 50

91-57-6 2-Methylnaphthalene Not Detected 320 X 50

67-64-1 2-Propanone (acetone) Not Detected 1300 5 7 50

108-10-1 4-Methyl-2-pentanone (MIBK) Not Detected 320 50

107-13-1 Acrylonitrile Not Detected 320 Z 50

71-43-2 Benzene Not Detected 65 50

108-86-1 Bromobenzene Not Detected 65 50

74-97-5 Bromochloromethane Not Detected 65 50

75-27-4 Bromodichloromethane Not Detected 65 50

75-25-2 Bromoform Not Detected 65 50

74-83-9 Bromomethane Not Detected 260 50

75-15-0 Carbon disulfide Not Detected 65 50

56-23-5 Carbon tetrachloride Not Detected 65 50

108-90-7 Chlorobenzene Not Detected 65 50

75-00-3 Chloroethane Not Detected 320 50

67-66-3 Chloroform Not Detected 65 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 51 of 106

Page 125: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08223 SS-13

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/17/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

74-87-3 Chloromethane Not Detected 320 50

156-59-2 cis-1,2-Dichloroethylene Not Detected 65 50

10061-01-5 cis-1,3-Dichloropropylene Not Detected 65 50

110-82-7 Cyclohexane Not Detected 320 50

124-48-1 Dibromochloromethane Not Detected 65 50

74-95-3 Dibromomethane Not Detected 65 50

75-71-8 Dichlorodifluoromethane Not Detected 320 50

60-29-7 Diethyl ether Not Detected 260 50

108-20-3 Diisopropyl Ether Not Detected 320 50

100-41-4 Ethylbenzene Not Detected 65 50

637-92-3 Ethyltertiarybutylether Not Detected 320 50

67-72-1 Hexachloroethane Not Detected 320 50

98-82-8 Isopropylbenzene Not Detected 65 50

108383,106423 m & p - Xylene Not Detected 130 50

74-88-4 Methyl iodide Not Detected 65 50

75-09-2 Methylene chloride Not Detected 130 50

1634-04-4 Methyltertiarybutylether Not Detected 65 50

91-20-3 Naphthalene Not Detected 320 X 7 50

104-51-8 n-Butylbenzene Not Detected 65 50

103-65-1 n-Propylbenzene Not Detected 65 50

95-47-6 o-Xylene Not Detected 65 50

99-87-6 p-Isopropyl toluene Not Detected 65 50

135-98-8 sec-Butylbenzene Not Detected 65 50

100-42-5 Styrene Not Detected 65 50

98-06-6 tert-Butylbenzene Not Detected 65 50

75-65-0 tertiary Butyl Alcohol Not Detected 3200 50

994-05-8 tertiaryAmylmethylether Not Detected 320 50

127-18-4 Tetrachloroethylene Not Detected 65 50

109-99-9 Tetrahydrofuran Not Detected 320 50

108-88-3 Toluene 90 65 2 50

156-60-5 trans-1,2-Dichloroethylene Not Detected 65 50

10061-02-6 trans-1,3-Dichloropropylene Not Detected 65 50

110-57-6 trans-1,4-Dichloro-2-butene Not Detected 320 Z 50

79-01-6 Trichloroethylene Not Detected 65 50

75-69-4 Trichlorofluoromethane Not Detected 65 50

75-01-4 Vinyl chloride Not Detected 65 Z 50

Methanol spilled out of vial during extraction, results and reporting limits are estimated.

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 52 of 106

Page 126: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08223 SS-13

CAS# Analyte Name Result Unit RL Qualifier Date Tested Method Analyst

% Total Solids 87.1 % 0.1 11/19/2012 2540B SM JW

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 53 of 106

Page 127: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08224 SS-14

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/17/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

##Weight of sample(grams) 10.33

SURROGATE #Bromofluorobenzene# 151

SURROGATE #Dibromofluoromethane# 176

SURROGATE #Toluene-d8# 160

630-20-6 1,1,1,2-Tetrachloroethane Not Detected 88 50

71-55-6 1,1,1-Trichloroethane Not Detected 88 50

79-34-5 1,1,2,2-Tetrachloroethane Not Detected 88 50

79-00-5 1,1,2-Trichloroethane Not Detected 88 50

75-34-3 1,1-Dichloroethane Not Detected 88 50

75-35-4 1,1-Dichloroethylene Not Detected 88 50

87-61-6 1,2,3-Trichlorobenzene Not Detected 440 7 50

96-18-4 1,2,3-Trichloropropane Not Detected 88 50

526-73-8 1,2,3-Trimethylbenzene Not Detected 88 50

120-82-1 1,2,4-Trichlorobenzene Not Detected 440 7 50

95-63-6 1,2,4-Trimethylbenzene Not Detected 88 50

96-12-8 1,2-Dibromo-3-chloropropane Not Detected 440 50

106-93-4 1,2-Dibromoethane Not Detected 88 Z 50

95-50-1 1,2-Dichlorobenzene Not Detected 88 50

107-06-2 1,2-Dichloroethane Not Detected 88 50

78-87-5 1,2-Dichloropropane Not Detected 88 50

108-67-8 1,3,5-Trimethylbenzene Not Detected 88 50

541-73-1 1,3-Dichlorobenzene Not Detected 88 50

106-46-7 1,4-Dichlorobenzene Not Detected 88 50

78-93-3 2-Butanone (MEK) Not Detected 440 50

591-78-6 2-Hexanone Not Detected 440 50

91-57-6 2-Methylnaphthalene Not Detected 440 X 50

67-64-1 2-Propanone (acetone) Not Detected 1800 5 7 50

108-10-1 4-Methyl-2-pentanone (MIBK) Not Detected 440 50

107-13-1 Acrylonitrile Not Detected 440 Z 50

71-43-2 Benzene Not Detected 88 50

108-86-1 Bromobenzene Not Detected 88 50

74-97-5 Bromochloromethane Not Detected 88 50

75-27-4 Bromodichloromethane Not Detected 88 50

75-25-2 Bromoform Not Detected 88 50

74-83-9 Bromomethane Not Detected 350 50

75-15-0 Carbon disulfide Not Detected 88 50

56-23-5 Carbon tetrachloride Not Detected 88 50

108-90-7 Chlorobenzene Not Detected 88 50

75-00-3 Chloroethane Not Detected 440 50

67-66-3 Chloroform Not Detected 88 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 54 of 106

Page 128: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08224 SS-14

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/17/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

74-87-3 Chloromethane Not Detected 440 50

156-59-2 cis-1,2-Dichloroethylene Not Detected 88 50

10061-01-5 cis-1,3-Dichloropropylene Not Detected 88 50

110-82-7 Cyclohexane Not Detected 440 50

124-48-1 Dibromochloromethane Not Detected 88 50

74-95-3 Dibromomethane Not Detected 88 50

75-71-8 Dichlorodifluoromethane Not Detected 440 50

60-29-7 Diethyl ether Not Detected 350 50

108-20-3 Diisopropyl Ether Not Detected 440 50

100-41-4 Ethylbenzene Not Detected 88 50

637-92-3 Ethyltertiarybutylether Not Detected 440 50

67-72-1 Hexachloroethane Not Detected 440 50

98-82-8 Isopropylbenzene Not Detected 88 50

108383,106423 m & p - Xylene 340 180 50

74-88-4 Methyl iodide Not Detected 88 50

75-09-2 Methylene chloride Not Detected 180 50

1634-04-4 Methyltertiarybutylether Not Detected 88 50

91-20-3 Naphthalene Not Detected 440 X 7 50

104-51-8 n-Butylbenzene Not Detected 88 50

103-65-1 n-Propylbenzene Not Detected 88 50

95-47-6 o-Xylene 160 88 50

99-87-6 p-Isopropyl toluene Not Detected 88 50

135-98-8 sec-Butylbenzene Not Detected 88 50

100-42-5 Styrene Not Detected 88 50

98-06-6 tert-Butylbenzene Not Detected 88 50

75-65-0 tertiary Butyl Alcohol Not Detected 4400 50

994-05-8 tertiaryAmylmethylether Not Detected 440 50

127-18-4 Tetrachloroethylene Not Detected 88 50

109-99-9 Tetrahydrofuran Not Detected 440 50

108-88-3 Toluene 430 88 50

156-60-5 trans-1,2-Dichloroethylene Not Detected 88 50

10061-02-6 trans-1,3-Dichloropropylene Not Detected 88 50

110-57-6 trans-1,4-Dichloro-2-butene Not Detected 440 Z 50

79-01-6 Trichloroethylene Not Detected 88 50

75-69-4 Trichlorofluoromethane Not Detected 88 50

75-01-4 Vinyl chloride Not Detected 88 Z 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 55 of 106

Page 129: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08224 SS-14

CAS# Analyte Name Result Unit RL Qualifier Date Tested Method Analyst

% Total Solids 71.4 % 0.1 11/19/2012 2540B SM JW

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 56 of 106

Page 130: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08225 SB-01

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/16/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

##Weight of sample(grams) 10.81

SURROGATE #Bromofluorobenzene# 120

SURROGATE #Dibromofluoromethane# 141

SURROGATE #Toluene-d8# 129

630-20-6 1,1,1,2-Tetrachloroethane Not Detected 74 50

71-55-6 1,1,1-Trichloroethane Not Detected 74 50

79-34-5 1,1,2,2-Tetrachloroethane Not Detected 74 50

79-00-5 1,1,2-Trichloroethane Not Detected 74 50

75-34-3 1,1-Dichloroethane Not Detected 74 50

75-35-4 1,1-Dichloroethylene Not Detected 74 50

87-61-6 1,2,3-Trichlorobenzene Not Detected 370 7 50

96-18-4 1,2,3-Trichloropropane Not Detected 74 50

526-73-8 1,2,3-Trimethylbenzene Not Detected 74 50

120-82-1 1,2,4-Trichlorobenzene Not Detected 370 7 50

95-63-6 1,2,4-Trimethylbenzene Not Detected 74 50

96-12-8 1,2-Dibromo-3-chloropropane Not Detected 370 50

106-93-4 1,2-Dibromoethane Not Detected 74 Z 50

95-50-1 1,2-Dichlorobenzene Not Detected 74 50

107-06-2 1,2-Dichloroethane Not Detected 74 50

78-87-5 1,2-Dichloropropane Not Detected 74 50

108-67-8 1,3,5-Trimethylbenzene Not Detected 74 50

541-73-1 1,3-Dichlorobenzene Not Detected 74 50

106-46-7 1,4-Dichlorobenzene Not Detected 74 50

78-93-3 2-Butanone (MEK) Not Detected 370 50

591-78-6 2-Hexanone Not Detected 370 50

91-57-6 2-Methylnaphthalene Not Detected 370 X 7 50

67-64-1 2-Propanone (acetone) Not Detected 1500 5 50

108-10-1 4-Methyl-2-pentanone (MIBK) Not Detected 370 50

107-13-1 Acrylonitrile Not Detected 370 Z 50

71-43-2 Benzene Not Detected 74 50

108-86-1 Bromobenzene Not Detected 74 50

74-97-5 Bromochloromethane Not Detected 74 50

75-27-4 Bromodichloromethane Not Detected 74 50

75-25-2 Bromoform Not Detected 74 50

74-83-9 Bromomethane Not Detected 290 50

75-15-0 Carbon disulfide Not Detected 74 50

56-23-5 Carbon tetrachloride Not Detected 74 50

108-90-7 Chlorobenzene Not Detected 74 50

75-00-3 Chloroethane Not Detected 370 50

67-66-3 Chloroform Not Detected 74 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 57 of 106

Page 131: Tamarack Part 3 - Michigan · r ' ·~· ·--}L -, 11 Jx}-,_ t-·~' 0--

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORYP.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

Sample Number: AC08225 SB-01

Volatile Compounds

Analytical Method: 8260 Date Tested: 11/16/2012 Analyst: SJR

Extraction Method: 5035 Extraction Date: 11/15/2012 Qualifier:

CAS # Compound Result ug/Kg dry RL Qualifier Dilution Factor

74-87-3 Chloromethane Not Detected 370 50

156-59-2 cis-1,2-Dichloroethylene Not Detected 74 50

10061-01-5 cis-1,3-Dichloropropylene Not Detected 74 50

110-82-7 Cyclohexane Not Detected 370 50

124-48-1 Dibromochloromethane Not Detected 74 50

74-95-3 Dibromomethane Not Detected 74 50

75-71-8 Dichlorodifluoromethane Not Detected 370 50

60-29-7 Diethyl ether Not Detected 290 50

108-20-3 Diisopropyl Ether Not Detected 370 50

100-41-4 Ethylbenzene Not Detected 74 50

637-92-3 Ethyltertiarybutylether Not Detected 370 50

67-72-1 Hexachloroethane Not Detected 370 50

98-82-8 Isopropylbenzene Not Detected 74 50

108383,106423 m & p - Xylene Not Detected 150 50

74-88-4 Methyl iodide Not Detected 74 50

75-09-2 Methylene chloride Not Detected 150 50

1634-04-4 Methyltertiarybutylether Not Detected 74 50

91-20-3 Naphthalene Not Detected 370 X 5 7 50

104-51-8 n-Butylbenzene Not Detected 74 50

103-65-1 n-Propylbenzene Not Detected 74 50

95-47-6 o-Xylene Not Detected 74 50

99-87-6 p-Isopropyl toluene Not Detected 74 50

135-98-8 sec-Butylbenzene Not Detected 74 50

100-42-5 Styrene Not Detected 74 50

98-06-6 tert-Butylbenzene Not Detected 74 50

75-65-0 tertiary Butyl Alcohol Not Detected 3700 50

994-05-8 tertiaryAmylmethylether Not Detected 370 50

127-18-4 Tetrachloroethylene Not Detected 74 50

109-99-9 Tetrahydrofuran Not Detected 370 50

108-88-3 Toluene Not Detected 74 50

156-60-5 trans-1,2-Dichloroethylene Not Detected 74 50

10061-02-6 trans-1,3-Dichloropropylene Not Detected 74 50

110-57-6 trans-1,4-Dichloro-2-butene Not Detected 370 Z 50

79-01-6 Trichloroethylene Not Detected 74 50

75-69-4 Trichlorofluoromethane Not Detected 74 50

75-01-4 Vinyl chloride Not Detected 74 Z 50

CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts

RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane

ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian

Lab Work Order #: 21100087 Page 58 of 106