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Subsurface Soil, Groundwater, and Vapor Intrusion Investigation Report
CVS Pharmacy Property
3425 West Sixteenth Street Indianapolis, Indiana
Prepared for:
Mr. Robert McCormack 3425 Partners, LLC
10734 Sky Prairie Street Fishers, Indiana 46037
and Mr. Blake Sanderson
Americana Bank 6653 West Broadway
McCordsville, Indiana 46055
Prepared by:
Kerr Environmental Services, Inc. 709 Main Street
Ellettsville, Indiana 47429 (812) 935-5377
(812) 876-3307 FAX
December 2, 2014
Project Number 14012
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Kerr Environmental Services, Inc. Page i
Table of Contents LETTER OF TRANSMITTAL Enclosed TABLE OF CONTENTS i 1.0 EXECUTIVE SUMMARY 1 2.0 OBJECTIVE AND SCOPE 3 3.0. SITE DESCRIPTION 3 4.0 SUBSURFACE SOIL AND GROUNDWATER INVESTIGATION 4 5.0 VAPOR INTRUSION INVESTIGATION 5 6.0 ANALYTICAL RESULTS 5 6.1 Comparative Action Levels 5 6.2 Laboratory Results 6 7.0 CONCLUSIONS AND RECOMMENDATIONS 7
TABLES
Table 1 Subsurface Soil Analytical Results Table 2 Groundwater Analytical Results Table 3 Indoor Air and Sub Slab Analytical Results
FIGURES
Figure 1 Project Location Map (U.S.G.S. Quad Map) Figure 2 Site Map
APPENDIX Laboratory Data Sheets and Chain of Custody Documentation
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Kerr Environmental Services, Inc. 1
1.0 Executive Summary
Kerr Environmental Services, Inc. performed the subsurface soil, groundwater, and vapor
intrusion investigation at the CVS Pharmacy Property (hereinafter referred to as the "project
site") located at 3425 West Sixteenth Street in Indianapolis, Indiana, at the request of Mr. Robert
McCormack, 3425 Partners, LLC, with reliance on this report extended to Americana Bank of
McCordsville, Indiana.
The project site consists of a commercial building of approximately 10,852 square feet situated
on approximately 1.09 acres. The remainder of the project site is parking lots, drives, and
landscaped areas. The project site is bounded by West Sixteenth Street to the north with an
access drive to Tibbs Avenue to the east. Surrounding properties include commercial properties
to the north, a car wash and residential properties to the west, a church to the south, and a Burger
King to the east with a gasoline station and residential properties across Tibbs Avenue.
Recognized environmental concerns were discovered during the performance of a Phase I
Environmental Site Assessment (ESA) of the project site. The Phase I ESA was placed on hold
pending the outcome of this investigation. The recognized environmental concerns identified
included the presence of former underground petroleum storage tanks located on properties
immediately east and west of the project site. The adjacent Burger King was formerly a gasoline
service station. The adjacent car wash formerly utilized a fuel tank located within a few feet of
the project site. In addition, there are other existing or former gasoline service stations located
within close proximity to the project site.
To investigate these environmental concerns at the project site, Kerr Environmental Services,
Inc. conducted a subsurface soil and groundwater investigation. A total of six subsurface soil
samples and five groundwater samples were collected. The analytical results revealed
subsurface soil contamination at a depth of 27 to 28 feet below ground surface in sample GP-5D
collected immediately adjacent to the car wash on the west side of the project site. This sample
contained 1-methylnaphthalene, 2-methylnaphthalene, naphthalene, 1,2,4-trimethylbenzene,
xylenes above residential migration to groundwater screening levels and 1,2,4-trimethylbenzene
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was also above residential direct contact screening levels. These compounds are associated with
coal, crude oil, naphthalene solvents, and other petroleum products.
The analytical results of groundwater samples showed the presence of trichloroethene (TCE), a
solvent, above residential vapor intrusion screening levels and residential tap water (drinking
water standards) screening levels. Three samples were also above the commercial/industrial
vapor screening levels.
Due to the TCE concentrations in the groundwater, Kerr Environmental Services, Inc. conducted
a vapor intrusion investigation at the project site, consisting of the collection of indoor air and
sub slab air samples. Analytical results revealed the presence of benzene in the indoor air.
However, the benzene was present well below residential and commercial/industrial action
levels. Two sub-slab samples also contained benzene as well, but also below screening levels.
One of these two samples, collected near the northeastern corner of the building, also contained
TCE and tetrachloroethene (also known as perchloroethene or PCE). PCE was detected below
screening levels. TCE was detected above both residential and commercial/industrial screening
levels. The indoor air samples were collected immediately adjacent to each of the sub-slab
samples and did not contain a detectable concentration of TCE or PCE.
In conclusion, the subsurface soil has been impacted by an apparent release at the adjacent car
wash. Groundwater has been impacted with TCE. Sub-slab air samples revealed the presence of
TCE. However, the air samples in the CVS Pharmacy building were below action levels and are
not believed to be a concern. The vapor intrusion investigation was taken during a worst-case
scenario, during cold weather, which would indicate that levels would be lower during other
times of the year.
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2.0 Objective and Scope
The objective of this subsurface soil, groundwater, and vapor intrusion investigation was to
determine the presence or absence and relative concentrations of contaminants at the project site.
This investigation is not a guarantee or certification that the project site is free of contamination
or hazardous materials, but rather it is an opinion of the potential for contamination to exist
based on the scope of this investigation.
The scope of this investigation included the collection of subsurface soil and groundwater
samples, collection of sub slab and indoor air samples, laboratory analyses of compounds or
chemicals of concern, and the preparation of this Subsurface Soil, Groundwater, and Vapor
Intrusion Investigation Report. Certain information presented herein has been provided by
regulatory agencies and interviews. That information is assumed to be correct and Kerr
Environmental Services, Inc. makes no representation or warranties regarding such information.
Kerr Environmental Services' opinions stated herein are based on generally accepted
environmental site assessment methodologies and procedures with respect to due care customary
in the environmental field at the time of this assessment. Kerr Environmental Services' opinions
are not to be construed as legal advice. Legal counsel should be consulted when deemed
necessary by the reader.
This Vapor Intrusion Investigation Report was prepared at the request of Mr. Robert
McCormack, 3425 Partners, LLC, with reliance on this report extended to Americana Bank of
McCordsville, Indiana. Kerr Environmental Services, Inc. assumes no obligation to any other
party for reliance upon this report.
3.0 Site Description
The project site is the CVS Pharmacy property located at 3425 West Sixteenth Street in
Indianapolis, Indiana. The project site is located in the Northeast Quarter of the Southeast
Quarter of Section 32, Township 16 North, Range 3 East, in Wayne Township, Marion County.
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Kerr Environmental Services, Inc. 4
The project site is located less than a mile west of the White River and less than a mile east of
the Indianapolis Motor Speedway. The project site is bounded by West Sixteenth Street to the
north with an access drive to Tibbs Avenue to the east. See Figure 1, Project Location Map, and
Figure 2, Site Map.
The project site consists of a commercial building of approximately 10,852 square feet situated
on approximately 1.09 acres. The remainder of the project site is parking lots, drives, and
landscaped areas. Surrounding properties include commercial properties to the north, a car wash
and residential properties to the west, a church to the south, and a Burger King to the east with a
gasoline station and residential properties across Tibbs Avenue.
The project site lies within the Tipton Till Plain physiographic province of the Central Till Plain
Region. The Tipton Till Plain is a till plain of low relief with extensive areas of ice
disintegration features. Bedrock in the area of the project site is dolomite and limestone of the
Muscatatuck Group of Devonian Age. The bedrock is overlain with undifferentiated outwash.
The depth of the unconsolidated deposits is over 100 feet. The depth to groundwater is likely
seasonal to some extent and was encountered at approximately 27 feet below the ground surface.
Soils on the project site consist of Urban Land Fox Complex (UfA). These soils are dominantly
Fox loam soils that have been altered by site development. The slope in the area is 0-2 percent.
These soils are well drained and found on terraces of the till plains.
4.0 Subsurface Soil and Groundwater Investigation
On October 27, 2014, Kerr Environmental Services, Inc. collected six subsurface soil samples
and five groundwater samples from the project site. These samples were collected utilizing a
Geoprobe, a track-mounted hydraulic sampling device. The sample locations were strategically
placed adjacent to properties that have, or have had, underground storage tanks (USTs). Three
sample locations were immediately adjacent to the Burger King property to the east of the
project site and two sample locations were immediately adjacent to the car wash property to the
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Kerr Environmental Services, Inc. 5
west of the project site. The subsurface soil samples were taken directly from soil core sleeves.
The groundwater samples were collected by utilizing new tubing with a decontaminated check
valve and peristaltic pump through the hollow stem rods of the Geoprobe. All samples were
placed in containers supplied by the laboratory, labeled with appropriate identifying information,
and placed in an iced cooler for delivery to the laboratory under strict chain of custody protocol.
The sample locations are shown on Figure 2.
5.0 Vapor Intrusion Investigation
On November 13 and 14, 2014, Kerr Environmental Services, Inc. collected ten air samples at
the project site to evaluate the potential for vapor intrusion. Five samples of the air beneath the
slab foundation were collected, as well as five samples of the indoor air. The air and sub slab
samples were collected at the same location. The indoor air samples were collected with Suma
canisters with a vacuum and regulated valve. The sub slab samples were collected in the same
way except that the regulated valve was connected to a tube that was affixed through the
concrete floor. The indoor air samples were collected during normal operations of the facility.
All samples were placed in packaging supplied by the laboratory, labeled with appropriate
identifying information, and delivered to the laboratory under strict chain of custody protocol.
The sample locations are shown on Figure 2.
6.0 Analytical Results
6.1 Comparative Action Levels
Comparative action levels were selected from the Indiana Department of Environmental
Management’s (IDEM’s) Remediation Closure Guide, updated in 2014. The residential and
industrial screening levels were both utilized.
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6.2 Laboratory Results
The subsurface soil and groundwater samples were delivered to ENVision Laboratories, Inc. of
Indianapolis, Indiana for laboratory analyses. The air samples were delivered to EnvisionAir of
Indianapolis, Indiana for laboratory analyses.
The analytical results revealed subsurface soil contamination at a depth of 27 to 28 feet below
ground surface in sample GP-5D collected immediately adjacent to the car wash on the west side
of the project site. This sample contained 1-methylnaphthalene, 2-methylnaphthalene,
naphthalene, 1,2,4-trimethylbenzene, xylenes above residential migration to groundwater
screening levels and 1,2,4-trimethylbenzene was also above residential direct contact screening
levels. These compounds are associated with coal, crude oil, naphthalene solvents, and other
petroleum products. The subsurface soil analytical results are summarized on Table 1.
The analytical results of groundwater samples showed the presence of TCE, a solvent, above
residential vapor intrusion screening levels and residential tap water (drinking water standards)
screening levels. Three samples were also above the commercial/industrial vapor screening
levels. The groundwater analytical results are summarized on Table 2.
Analytical results revealed the presence of benzene in the indoor air. However, the benzene was
present well below residential and commercial/industrial action levels. Two sub-slab samples
also contained benzene as well, but also below screening levels. One of these two samples,
collected near the northeastern corner of the building, also contained TCE and PCE. PCE was
detected below screening levels. TCE was detected above both residential and
commercial/industrial screening levels. The indoor air samples were collected immediately
adjacent to each of the sub-slab samples and did not contain a detectable concentration of TCE or
PCE.
The indoor air and sub slab sample analytical data is summarized on Table 3. Laboratory data
sheets and chain of custody documentation can be found in the Appendix.
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TABLES
Table 1 Subsurface Soil Analytical Results Table 2 Groundwater Analytical Results Table 3 Indoor Air and Sub Slab Analytical Results
Reference 67 Page 10
Sample ID GP-1 GP-2 GP-3 GP-4 GP-5 GP-5D Com/IndDepth 10.5-11.5' 19-20' 19-20' 19-20' 19-20' 27-28' MTG DC DC
VOCs Detected (mg/kg):n-Butylbenzene <0.005 <0.005 <0.005 <0.005 <0.005 4.49 50 110 110sec-Butylbenzene <0.005 <0.005 <0.005 <0.005 <0.005 2.64 94 150 150Ethylbenzene <0.005 <0.005 <0.005 <0.005 <0.005 5.14 16 76 270Isopropylbenzene (Cumene) <0.005 <0.005 <0.005 <0.005 <0.005 2.76 13 270 270p-Isopropyltoluene <0.005 <0.005 <0.005 <0.005 <0.005 3.42 None None None1-Methylnaphthalene <0.005 <0.005 <0.005 <0.005 <0.005 4.06 1 220 5302-Methylnaphthalene <0.005 <0.005 <0.005 <0.005 <0.005 4.78 2.8 320 2,200n-Propylbenzene <0.005 <0.005 <0.005 <0.005 <0.005 10.2 20 260 2601,2,4-Trimethylbenzene <0.005 <0.005 <0.005 <0.005 <0.005 109 0.44 87 2201,3,5-Trimethylbenzene <0.005 <0.005 <0.005 <0.005 <0.005 29.6 33 3,100 27,000Xylene, M&P <0.005 <0.005 <0.005 <0.005 <0.005 5.72 3.7 390 390Xylene, Total <0.011 <0.011 <0.010 <0.011 <0.011 5.72 200 260 260SVOCs Detected (mg/kg):Naphthalene <0.073 <0.071 <0.070 <0.071 <0.073 3.87 0.092 50 180
Underlined typeface indicates result above residential migration to groundwater screening levels.Italic typeface indicates result above residential direct contact screening levels.
Residential
Table 1Subsurface Soil Analytical Results
CVS Pharmacy Property3425 West Sixteenth Street
Indianapolis, Indiana
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Sample ID Com/IndParameter Tap Vapor Exp Vapor ExpVOCs Detected (ug/L):cis-1,2-Dichloroethene <5 <5 <5 6.24 29.1 70 None NoneTrichloroethene (TCE) 86.8 50.4 27.4 55.7 18.8 5 9.1 381,2,4-Trimethylbenzene <5 <5 <5 <5 9.34 15 None NoneSVOCs Detected (ug/L): None None None None None
Underlined typeface indicates result above residential tap water screening levels.Italic typeface indicates result above residential vapor exposure screening levels.Bold typeface indicates result above commercial/industrial vapor exposure screening levels.
ResidentialGP-1W GP-2W GP-3W GP-4W GP-5W
Table 2Groundwater Analytical Results
CVS Pharmacy Property3425 West Sixteenth Street
Indianapolis, Indiana
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Sample ID Benzene Tetrachloroethene TrichloroetheneIA-1 <1.60 <3.19 <1.07IA-2 <1.60 <3.19 <1.07IA-3 <1.60 <3.19 <1.07IA-4 1.76 <3.19 <1.07IA-5 <1.60 <3.19 <1.07Residential 24 42 2.1Com/Ind 120 180 8.8
Sample ID Benzene Tetrachloroethene TrichloroetheneSS-1 30.0 384 139SS-2 26.5 <31.9 <10.7SS-3 23.0 <31.9 <10.7SS-4 21.4 <31.9 <10.7SS-5 20.1 <31.9 <10.7Residential 240 420 21Com/Ind 1,200 1,800 88
Underlined typeface indicates result above residential screening levels.Bold typeface indicates result above commercial/industrial screening levels.
Sub-Slab
Table 3Indoor Air and Sub-Slab Analytical Results
CVS Pharmacy Property3425 West Sixteenth Street
Indianapolis, Indiana
Indoor Air
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FIGURES
Figure 1 Project Location Map Figure 2 Site Map
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Figure 1: Project Location MapCVS Pharmacy Property
3425 West Sixteenth StreetIndianapolis, Indiana
Kerr Environmental Services, Inc.
709 Main StreetEllettsville, Indiana 47429(812) 935-5377 / 876-3307 FAX
Base Taken FromU.S.G.S. Topographic Map
Indianapolis West, Ind. Quadrangle
Project Site
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Figure : Site Map2CVS Pharmacy Property
3425 West Sixteenth StreetIndianapolis, Indiana
Kerr Environmental Services, Inc.
709 Main StreetEllettsville, Indiana 47429(812) 935-5377 / 876-3307 FAX
Base Taken From 2014 Aerial Photographs.
West Sixteenth StreetK
opetS
ky’s
Car
Wash
Burger King
Church
Residential
ProjectSite
GP-1
GP-2
GP-2GP-4
GP-5
Air 1
Air 2
Air 3
Air 4
Air 5
Geopro
be
Sam
ple
Location
IndoorA
ir/S
ub-S
lab
Sam
ple
Location
To Tibbs Avenue
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APPENDIX
LABORATORY DATA SHEETS AND CHAIN OF CUSTODY DOCUMENTATION
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Mr. Dana Kerr Kerr Environmental Services, Inc. 709 Main Street Ellettsville, IN 47429 October 30, 2014 ENVision Project Number: 2014-3153 Client Project Name: CVS Dear Mr. Kerr, Please find the attached analytical report for the samples received October 27, 2014. All test methods performed were fully compliant with local, state, and federal EPA methods unless otherwise noted. The project was analyzed as requested on the enclosed chain of custody record. Please review the comments section for additional information about your results or Quality Control data. The reference for the preservation technique utilized by ENVision Laboratories for Volatile Organics in soil may be found on Table A.1 (p. 42) of Method 5035A: Closed-System Purge-and-Trap and Extraction for Volatile Organics in Soil and Waste Samples, July 2002, Draft Revision 1. All soils collected via Method 5035A are frozen at the laboratory upon receipt. Feel free to contact me if you have any questions or comments regarding your analytical report or service. Thank you for your business. ENVision Laboratories looks forward to working with you on your next project. Yours Sincerely, David Norris Client Services Manager ENVision Laboratories, Inc. PA DEP Lab Code: 68-04846 NELAP Cert:004
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
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Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Analytical Method: EPA 8260Prep Method: EPA 5035AAnalytical Batch: 103014VS
Client Sample ID: GP-1 Sample Collection Date/Time: 10/27/14 9:50Envision Sample Number: 14-24289 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: soil
Acetone < 0.109 0.109Acrolein < 0.00018 0.001 1Acrylonitrile < 0.002 0.002Benzene < 0.005 0.005Bromobenzene < 0.005 0.005Bromochloromethane < 0.005 0.005Bromodichloromethane < 0.005 0.005Bromoform < 0.005 0.005Bromomethane < 0.005 0.005n-Butanol < 0.054 0.0542-Butanone (MEK) < 0.011 0.011n-Butylbenzene < 0.005 0.005sec-Butylbenzene < 0.005 0.005tert-Butylbenzene < 0.005 0.005Carbon Disulfide < 0.005 0.005Carbon Tetrachloride < 0.005 0.005Chlorobenzene < 0.005 0.005Chloroethane < 0.005 0.0052-Chloroethylvinylether < 0.054 0.054Chloroform < 0.005 0.005Chloromethane < 0.005 0.0052-Chlorotoluene < 0.005 0.0054-Chlorotoluene < 0.005 0.0051,2-Dibromo-3-chloropropane < 0.0018 0.0018Dibromochloromethane < 0.005 0.0051,2-Dibromoethane (EDB) < 0.00030 0.001 1Dibromomethane < 0.005 0.0051,2-Dichlorobenzene < 0.005 0.0051,3-Dichlorobenzene < 0.005 0.0051,4-Dichlorobenzene < 0.005 0.005trans-1,4-Dichloro-2-butene < 0.005 0.005Dichlorodifluoromethane < 0.005 0.0051,1-Dichloroethane < 0.005 0.0051,2-Dichloroethane < 0.005 0.0051,1-Dichloroethene < 0.005 0.005
Compounds Sample Results (mg/kg) Rep. Limit (mg/kg) Flags
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 19
Analytical Report
8260 continued…
cis-1,2-Dichloroethene < 0.005 0.005trans-1,2-Dichloroethene < 0.005 0.0051,2-Dichloropropane < 0.005 0.0051,3-Dichloropropane < 0.005 0.0052,2-Dichloropropane < 0.005 0.0051,1-Dichloropropene < 0.005 0.0051,3-Dichloropropene < 0.005 0.005Ethylbenzene < 0.005 0.005Ethyl methacrylate < 0.109 0.109Hexachloro-1,3-butadiene < 0.005 0.005n-Hexane < 0.011 0.0112-Hexanone < 0.011 0.011Iodomethane < 0.011 0.011Isopropylbenzene (Cumene) < 0.005 0.005p-Isopropyltoluene < 0.005 0.005Methylene chloride < 0.022 0.0224-Methyl-2-pentanone (MIBK) < 0.011 0.011Methyl-tert-butyl-ether < 0.005 0.0051-Methylnaphthalene < 0.005 0.0052-Methylnaphthalene < 0.005 0.005n-Propylbenzene < 0.005 0.005Styrene < 0.005 0.0051,1,1,2-Tetrachloroethane < 0.005 0.0051,1,2,2-Tetrachloroethane < 0.005 0.005Tetrachloroethene < 0.005 0.005Toluene < 0.005 0.0051,2,3-Trichlorobenzene < 0.005 0.0051,2,4-Trichlorobenzene < 0.005 0.0051,1,1-Trichloroethane < 0.005 0.0051,1,2-Trichloroethane < 0.005 0.005Trichloroethene < 0.005 0.005Trichlorofluoromethane < 0.005 0.0051,2,3-Trichloropropane < 0.005 0.0051,2,4-Trimethylbenzene < 0.005 0.0051,3,5-Trimethylbenzene < 0.005 0.005Vinyl acetate < 0.011 0.011Vinyl chloride < 0.002 0.002Xylene, M&P < 0.005 0.005Xylene, 0rtho < 0.005 0.005Xylene, Total < 0.011 0.011Dibromofluoromethane (surrogate) 99%1,2-Dichloroethane-d4 (surrogate) 90%Toluene-d8 (surrogate) 104%4-bromofluorobenzene (surrogate) 97%Analysis Date/Time: 10-30-14/11:19Analyst Initials tjg
Percent Solids: 92%All results reported on dry weight basis.
Compounds Sample Results (mg/kg) Rep. Limit (mg/kg) Flags
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 20
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Analytical Method: EPA 8270 CPAHPrep Method: EPA 3550CAnalytical Batch: 102914PS
Client Sample ID: GP-1 Sample Collection Date/Time: 10/27/14 9:50Envision Sample Number: 14-24289 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: soil
Benzo(a)anthracene < 0.36 0.36Benzo(a)pyrene < 0.073 0.073Benzo(b)fluoranthene < 0.36 0.36Benzo(k)fluoranthene < 0.36 0.36Chrysene < 0.36 0.36Dibenzo(a,h)anthracene < 0.073 0.073Indeno(1,2,3-cd)pyrene < 0.36 0.36Naphthalene < 0.073 0.073Nitrobenzene-d14 (surrogate) 55%2-Fluorobiphenyl (surrogate) 63%p-Terphenyl-d14 (surrogate) 101%Analysis Date/Time: 10-29-14/17:57Analyst Initials: ajgDate Extracted: 10/29/2014Initial Sample Weight: 30 gFinal Volume: 1.0 mL
Percent Solids 92%
All results reported on dry weight basis.
Compounds Sample Results (mg/kg) Rep. Limit (mg/kg) Flags
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 21
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Client Sample ID: GP-1 Sample Collection Date/Time: 10/27/14 9:50Envision Sample Number: 14-24289 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: soil
Analyte Sample Results Flags Method Percent Moisture 8.0% EPA 1684Percent Solids 92.0% EPA 1684Analysis Date: 10/29/14Analyst Initials ajg
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 22
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Analytical Method: EPA 8260Prep Method: EPA 5035AAnalytical Batch: 103014VW
Client Sample ID: GP-2 Sample Collection Date/Time: 10/27/14 11:25Envision Sample Number: 14-24290 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: soil
Acetone < 0.105 0.105Acrolein < 0.00018 0.001 1Acrylonitrile < 0.002 0.002Benzene < 0.005 0.005Bromobenzene < 0.005 0.005Bromochloromethane < 0.005 0.005Bromodichloromethane < 0.005 0.005Bromoform < 0.005 0.005Bromomethane < 0.005 0.005n-Butanol < 0.053 0.0532-Butanone (MEK) < 0.011 0.011n-Butylbenzene < 0.005 0.005sec-Butylbenzene < 0.005 0.005tert-Butylbenzene < 0.005 0.005Carbon Disulfide < 0.005 0.005Carbon Tetrachloride < 0.005 0.005Chlorobenzene < 0.005 0.005Chloroethane < 0.005 0.0052-Chloroethylvinylether < 0.053 0.053Chloroform < 0.005 0.005Chloromethane < 0.005 0.0052-Chlorotoluene < 0.005 0.0054-Chlorotoluene < 0.005 0.0051,2-Dibromo-3-chloropropane < 0.0018 0.0018Dibromochloromethane < 0.005 0.0051,2-Dibromoethane (EDB) < 0.00029 0.001 1Dibromomethane < 0.005 0.0051,2-Dichlorobenzene < 0.005 0.0051,3-Dichlorobenzene < 0.005 0.0051,4-Dichlorobenzene < 0.005 0.005trans-1,4-Dichloro-2-butene < 0.005 0.005Dichlorodifluoromethane < 0.005 0.0051,1-Dichloroethane < 0.005 0.0051,2-Dichloroethane < 0.005 0.0051,1-Dichloroethene < 0.005 0.005
Compounds Sample Results (mg/kg) Rep. Limit (mg/kg) Flags
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 23
Analytical Report
8260 continued…
cis-1,2-Dichloroethene < 0.005 0.005trans-1,2-Dichloroethene < 0.005 0.0051,2-Dichloropropane < 0.005 0.0051,3-Dichloropropane < 0.005 0.0052,2-Dichloropropane < 0.005 0.0051,1-Dichloropropene < 0.005 0.0051,3-Dichloropropene < 0.005 0.005Ethylbenzene < 0.005 0.005Ethyl methacrylate < 0.105 0.105Hexachloro-1,3-butadiene < 0.005 0.005n-Hexane < 0.011 0.0112-Hexanone < 0.011 0.011Iodomethane < 0.011 0.011Isopropylbenzene (Cumene) < 0.005 0.005p-Isopropyltoluene < 0.005 0.005Methylene chloride < 0.021 0.0214-Methyl-2-pentanone (MIBK) < 0.011 0.011Methyl-tert-butyl-ether < 0.005 0.0051-Methylnaphthalene < 0.005 0.0052-Methylnaphthalene < 0.005 0.005n-Propylbenzene < 0.005 0.005Styrene < 0.005 0.0051,1,1,2-Tetrachloroethane < 0.005 0.0051,1,2,2-Tetrachloroethane < 0.005 0.005Tetrachloroethene < 0.005 0.005Toluene < 0.005 0.0051,2,3-Trichlorobenzene < 0.005 0.0051,2,4-Trichlorobenzene < 0.005 0.0051,1,1-Trichloroethane < 0.005 0.0051,1,2-Trichloroethane < 0.005 0.005Trichloroethene 0.00922 0.005Trichlorofluoromethane < 0.005 0.0051,2,3-Trichloropropane < 0.005 0.0051,2,4-Trimethylbenzene < 0.005 0.0051,3,5-Trimethylbenzene < 0.005 0.005Vinyl acetate < 0.011 0.011Vinyl chloride < 0.002 0.002Xylene, M&P < 0.005 0.005Xylene, 0rtho < 0.005 0.005Xylene, Total < 0.011 0.011Dibromofluoromethane (surrogate) 97%1,2-Dichloroethane-d4 (surrogate) 93%Toluene-d8 (surrogate) 102%4-bromofluorobenzene (surrogate) 97%Analysis Date/Time: 10-30-14/11:37Analyst Initials tjg
Percent Solids: 95%All results reported on dry weight basis.
Compounds Sample Results (mg/kg) Rep. Limit (mg/kg) Flags
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 24
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Analytical Method: EPA 8270 CPAHPrep Method: EPA 3550CAnalytical Batch: 102914PS
Client Sample ID: GP-2 Sample Collection Date/Time: 10/27/14 11:25Envision Sample Number: 14-24290 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: soil
Benzo(a)anthracene < 0.35 0.35Benzo(a)pyrene < 0.071 0.071Benzo(b)fluoranthene < 0.35 0.35Benzo(k)fluoranthene < 0.35 0.35Chrysene < 0.35 0.35Dibenzo(a,h)anthracene < 0.071 0.071Indeno(1,2,3-cd)pyrene < 0.35 0.35Naphthalene < 0.071 0.071Nitrobenzene-d14 (surrogate) 42%2-Fluorobiphenyl (surrogate) 51%p-Terphenyl-d14 (surrogate) 91%Analysis Date/Time: 10-29-14/18:24Analyst Initials: ajgDate Extracted: 10/29/2014Initial Sample Weight: 30 gFinal Volume: 1.0 mL
Percent Solids 95%
All results reported on dry weight basis.
Compounds Sample Results (mg/kg) Rep. Limit (mg/kg) Flags
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 25
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Client Sample ID: GP-2 Sample Collection Date/Time: 10/27/14 11:25Envision Sample Number: 14-24290 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: soil
Analyte Sample Results Flags Method Percent Moisture 5.0% EPA 1684Percent Solids 95.0% EPA 1684Analysis Date: 10/29/14Analyst Initials ajg
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 26
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Analytical Method: EPA 8260Prep Method: EPA 5035AAnalytical Batch: 103014VS
Client Sample ID: GP-3 Sample Collection Date/Time: 10/27/14 13:25Envision Sample Number: 14-24291 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: soil
Acetone < 0.104 0.104Acrolein < 0.00018 0.001 1Acrylonitrile < 0.002 0.002Benzene < 0.005 0.005Bromobenzene < 0.005 0.005Bromochloromethane < 0.005 0.005Bromodichloromethane < 0.005 0.005Bromoform < 0.005 0.005Bromomethane < 0.005 0.005n-Butanol < 0.052 0.0522-Butanone (MEK) < 0.010 0.010n-Butylbenzene < 0.005 0.005sec-Butylbenzene < 0.005 0.005tert-Butylbenzene < 0.005 0.005Carbon Disulfide < 0.005 0.005Carbon Tetrachloride < 0.005 0.005Chlorobenzene < 0.005 0.005Chloroethane < 0.005 0.0052-Chloroethylvinylether < 0.052 0.052Chloroform < 0.005 0.005Chloromethane < 0.005 0.0052-Chlorotoluene < 0.005 0.0054-Chlorotoluene < 0.005 0.0051,2-Dibromo-3-chloropropane < 0.0018 0.0018Dibromochloromethane < 0.005 0.0051,2-Dibromoethane (EDB) < 0.00029 0.001 1Dibromomethane < 0.005 0.0051,2-Dichlorobenzene < 0.005 0.0051,3-Dichlorobenzene < 0.005 0.0051,4-Dichlorobenzene < 0.005 0.005trans-1,4-Dichloro-2-butene < 0.005 0.005Dichlorodifluoromethane < 0.005 0.0051,1-Dichloroethane < 0.005 0.0051,2-Dichloroethane < 0.005 0.0051,1-Dichloroethene < 0.005 0.005
Compounds Sample Results (mg/kg) Rep. Limit (mg/kg) Flags
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 27
Analytical Report
8260 continued…
cis-1,2-Dichloroethene < 0.005 0.005trans-1,2-Dichloroethene < 0.005 0.0051,2-Dichloropropane < 0.005 0.0051,3-Dichloropropane < 0.005 0.0052,2-Dichloropropane < 0.005 0.0051,1-Dichloropropene < 0.005 0.0051,3-Dichloropropene < 0.005 0.005Ethylbenzene < 0.005 0.005Ethyl methacrylate < 0.104 0.104Hexachloro-1,3-butadiene < 0.005 0.005n-Hexane < 0.010 0.0102-Hexanone < 0.010 0.010Iodomethane < 0.010 0.010Isopropylbenzene (Cumene) < 0.005 0.005p-Isopropyltoluene < 0.005 0.005Methylene chloride < 0.021 0.0214-Methyl-2-pentanone (MIBK) < 0.010 0.010Methyl-tert-butyl-ether < 0.005 0.0051-Methylnaphthalene < 0.005 0.0052-Methylnaphthalene < 0.005 0.005n-Propylbenzene < 0.005 0.005Styrene < 0.005 0.0051,1,1,2-Tetrachloroethane < 0.005 0.0051,1,2,2-Tetrachloroethane < 0.005 0.005Tetrachloroethene < 0.005 0.005Toluene < 0.005 0.0051,2,3-Trichlorobenzene < 0.005 0.0051,2,4-Trichlorobenzene < 0.005 0.0051,1,1-Trichloroethane < 0.005 0.0051,1,2-Trichloroethane < 0.005 0.005Trichloroethene < 0.005 0.005Trichlorofluoromethane < 0.005 0.0051,2,3-Trichloropropane < 0.005 0.0051,2,4-Trimethylbenzene < 0.005 0.0051,3,5-Trimethylbenzene < 0.005 0.005Vinyl acetate < 0.010 0.010Vinyl chloride < 0.002 0.002Xylene, M&P < 0.005 0.005Xylene, 0rtho < 0.005 0.005Xylene, Total < 0.010 0.010Dibromofluoromethane (surrogate) 95%1,2-Dichloroethane-d4 (surrogate) 86%Toluene-d8 (surrogate) 102%4-bromofluorobenzene (surrogate) 94%Analysis Date/Time: 10-30-14/11:56Analyst Initials tjg
Percent Solids: 96%All results reported on dry weight basis.
Compounds Sample Results (mg/kg) Rep. Limit (mg/kg) Flags
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 28
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Analytical Method: EPA 8270 CPAHPrep Method: EPA 3550CAnalytical Batch: 102914PS
Client Sample ID: GP-3 Sample Collection Date/Time: 10/27/14 13:25Envision Sample Number: 14-24291 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: soil
Benzo(a)anthracene < 0.34 0.34Benzo(a)pyrene < 0.070 0.070Benzo(b)fluoranthene < 0.34 0.34Benzo(k)fluoranthene < 0.34 0.34Chrysene < 0.34 0.34Dibenzo(a,h)anthracene < 0.070 0.070Indeno(1,2,3-cd)pyrene < 0.34 0.34Naphthalene < 0.070 0.070Nitrobenzene-d14 (surrogate) 42%2-Fluorobiphenyl (surrogate) 47%p-Terphenyl-d14 (surrogate) 85%Analysis Date/Time: 10-29-14/18:50Analyst Initials: ajgDate Extracted: 10/29/2014Initial Sample Weight: 30 gFinal Volume: 1.0 mL
Percent Solids 96%
All results reported on dry weight basis.
Compounds Sample Results (mg/kg) Rep. Limit (mg/kg) Flags
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 29
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Client Sample ID: GP-3 Sample Collection Date/Time: 10/27/14 13:25Envision Sample Number: 14-24291 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: soil
Analyte Sample Results Flags Method Percent Moisture 4.0% EPA 1684Percent Solids 96.0% EPA 1684Analysis Date: 10/29/14Analyst Initials ajg
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 30
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Analytical Method: EPA 8260Prep Method: EPA 5035AAnalytical Batch: 103014VS
Client Sample ID: GP-4 Sample Collection Date/Time: 10/27/14 15:00Envision Sample Number: 14-24292 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: soil
Acetone < 0.105 0.105Acrolein < 0.00018 0.001 1Acrylonitrile < 0.002 0.002Benzene < 0.005 0.005Bromobenzene < 0.005 0.005Bromochloromethane < 0.005 0.005Bromodichloromethane < 0.005 0.005Bromoform < 0.005 0.005Bromomethane < 0.005 0.005n-Butanol < 0.053 0.0532-Butanone (MEK) < 0.011 0.011n-Butylbenzene < 0.005 0.005sec-Butylbenzene < 0.005 0.005tert-Butylbenzene < 0.005 0.005Carbon Disulfide < 0.005 0.005Carbon Tetrachloride < 0.005 0.005Chlorobenzene < 0.005 0.005Chloroethane < 0.005 0.0052-Chloroethylvinylether < 0.053 0.053Chloroform < 0.005 0.005Chloromethane < 0.005 0.0052-Chlorotoluene < 0.005 0.0054-Chlorotoluene < 0.005 0.0051,2-Dibromo-3-chloropropane < 0.0018 0.0018Dibromochloromethane < 0.005 0.0051,2-Dibromoethane (EDB) < 0.00029 0.001 1Dibromomethane < 0.005 0.0051,2-Dichlorobenzene < 0.005 0.0051,3-Dichlorobenzene < 0.005 0.0051,4-Dichlorobenzene < 0.005 0.005trans-1,4-Dichloro-2-butene < 0.005 0.005Dichlorodifluoromethane < 0.005 0.0051,1-Dichloroethane < 0.005 0.0051,2-Dichloroethane < 0.005 0.0051,1-Dichloroethene < 0.005 0.005
Compounds Sample Results (mg/kg) Rep. Limit (mg/kg) Flags
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 31
Analytical Report
8260 continued…
cis-1,2-Dichloroethene < 0.005 0.005trans-1,2-Dichloroethene < 0.005 0.0051,2-Dichloropropane < 0.005 0.0051,3-Dichloropropane < 0.005 0.0052,2-Dichloropropane < 0.005 0.0051,1-Dichloropropene < 0.005 0.0051,3-Dichloropropene < 0.005 0.005Ethylbenzene < 0.005 0.005Ethyl methacrylate < 0.105 0.105Hexachloro-1,3-butadiene < 0.005 0.005n-Hexane < 0.011 0.0112-Hexanone < 0.011 0.011Iodomethane < 0.011 0.011Isopropylbenzene (Cumene) < 0.005 0.005p-Isopropyltoluene < 0.005 0.005Methylene chloride < 0.021 0.0214-Methyl-2-pentanone (MIBK) < 0.011 0.011Methyl-tert-butyl-ether < 0.005 0.0051-Methylnaphthalene < 0.005 0.0052-Methylnaphthalene < 0.005 0.005n-Propylbenzene < 0.005 0.005Styrene < 0.005 0.0051,1,1,2-Tetrachloroethane < 0.005 0.0051,1,2,2-Tetrachloroethane < 0.005 0.005Tetrachloroethene < 0.005 0.005Toluene < 0.005 0.0051,2,3-Trichlorobenzene < 0.005 0.0051,2,4-Trichlorobenzene < 0.005 0.0051,1,1-Trichloroethane < 0.005 0.0051,1,2-Trichloroethane < 0.005 0.005Trichloroethene < 0.005 0.005Trichlorofluoromethane < 0.005 0.0051,2,3-Trichloropropane < 0.005 0.0051,2,4-Trimethylbenzene < 0.005 0.0051,3,5-Trimethylbenzene < 0.005 0.005Vinyl acetate < 0.011 0.011Vinyl chloride < 0.002 0.002Xylene, M&P < 0.005 0.005Xylene, 0rtho < 0.005 0.005Xylene, Total < 0.011 0.011Dibromofluoromethane (surrogate) 98%1,2-Dichloroethane-d4 (surrogate) 82%Toluene-d8 (surrogate) 103%4-bromofluorobenzene (surrogate) 98%Analysis Date/Time: 10-30-14/12:13Analyst Initials tjg
Percent Solids: 95%All results reported on dry weight basis.
Compounds Sample Results (mg/kg) Rep. Limit (mg/kg) Flags
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 32
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Analytical Method: EPA 8270 CPAHPrep Method: EPA 3550CAnalytical Batch: 102914PS
Client Sample ID: GP-4 Sample Collection Date/Time: 10/27/14 15:00Envision Sample Number: 14-24292 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: soil
Benzo(a)anthracene < 0.35 0.35Benzo(a)pyrene < 0.071 0.071Benzo(b)fluoranthene < 0.35 0.35Benzo(k)fluoranthene < 0.35 0.35Chrysene < 0.35 0.35Dibenzo(a,h)anthracene < 0.071 0.071Indeno(1,2,3-cd)pyrene < 0.35 0.35Naphthalene < 0.071 0.071Nitrobenzene-d14 (surrogate) 41%2-Fluorobiphenyl (surrogate) 47%p-Terphenyl-d14 (surrogate) 80%Analysis Date/Time: 10-29-14/19:17Analyst Initials: ajgDate Extracted: 10/29/2014Initial Sample Weight: 30 gFinal Volume: 1.0 mL
Percent Solids 95%
All results reported on dry weight basis.
Compounds Sample Results (mg/kg) Rep. Limit (mg/kg) Flags
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 33
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Client Sample ID: GP-4 Sample Collection Date/Time: 10/27/14 15:00Envision Sample Number: 14-24292 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: soil
Analyte Sample Results Flags Method Percent Moisture 5.0% EPA 1684Percent Solids 95.0% EPA 1684Analysis Date: 10/29/14Analyst Initials ajg
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 34
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Analytical Method: EPA 8260Prep Method: EPA 5035AAnalytical Batch: 103014VS
Client Sample ID: GP-5 Sample Collection Date/Time: 10/27/14 16:10Envision Sample Number: 14-24293 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: soil
Acetone < 0.109 0.109Acrolein < 0.00018 0.001 1Acrylonitrile < 0.002 0.002Benzene < 0.005 0.005Bromobenzene < 0.005 0.005Bromochloromethane < 0.005 0.005Bromodichloromethane < 0.005 0.005Bromoform < 0.005 0.005Bromomethane < 0.005 0.005n-Butanol < 0.054 0.0542-Butanone (MEK) < 0.011 0.011n-Butylbenzene < 0.005 0.005sec-Butylbenzene < 0.005 0.005tert-Butylbenzene < 0.005 0.005Carbon Disulfide < 0.005 0.005Carbon Tetrachloride < 0.005 0.005Chlorobenzene < 0.005 0.005Chloroethane < 0.005 0.0052-Chloroethylvinylether < 0.054 0.054Chloroform < 0.005 0.005Chloromethane < 0.005 0.0052-Chlorotoluene < 0.005 0.0054-Chlorotoluene < 0.005 0.0051,2-Dibromo-3-chloropropane < 0.0018 0.0018Dibromochloromethane < 0.005 0.0051,2-Dibromoethane (EDB) < 0.00030 0.001 1Dibromomethane < 0.005 0.0051,2-Dichlorobenzene < 0.005 0.0051,3-Dichlorobenzene < 0.005 0.0051,4-Dichlorobenzene < 0.005 0.005trans-1,4-Dichloro-2-butene < 0.005 0.005Dichlorodifluoromethane < 0.005 0.0051,1-Dichloroethane < 0.005 0.0051,2-Dichloroethane < 0.005 0.0051,1-Dichloroethene < 0.005 0.005
Compounds Sample Results (mg/kg) Rep. Limit (mg/kg) Flags
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 35
Analytical Report
8260 continued…
cis-1,2-Dichloroethene < 0.005 0.005trans-1,2-Dichloroethene < 0.005 0.0051,2-Dichloropropane < 0.005 0.0051,3-Dichloropropane < 0.005 0.0052,2-Dichloropropane < 0.005 0.0051,1-Dichloropropene < 0.005 0.0051,3-Dichloropropene < 0.005 0.005Ethylbenzene < 0.005 0.005Ethyl methacrylate < 0.109 0.109Hexachloro-1,3-butadiene < 0.005 0.005n-Hexane < 0.011 0.0112-Hexanone < 0.011 0.011Iodomethane < 0.011 0.011Isopropylbenzene (Cumene) < 0.005 0.005p-Isopropyltoluene < 0.005 0.005Methylene chloride < 0.022 0.0224-Methyl-2-pentanone (MIBK) < 0.011 0.011Methyl-tert-butyl-ether < 0.005 0.0051-Methylnaphthalene < 0.005 0.0052-Methylnaphthalene < 0.005 0.005n-Propylbenzene < 0.005 0.005Styrene < 0.005 0.0051,1,1,2-Tetrachloroethane < 0.005 0.0051,1,2,2-Tetrachloroethane < 0.005 0.005Tetrachloroethene < 0.005 0.005Toluene < 0.005 0.0051,2,3-Trichlorobenzene < 0.005 0.0051,2,4-Trichlorobenzene < 0.005 0.0051,1,1-Trichloroethane < 0.005 0.0051,1,2-Trichloroethane < 0.005 0.005Trichloroethene < 0.005 0.005Trichlorofluoromethane < 0.005 0.0051,2,3-Trichloropropane < 0.005 0.0051,2,4-Trimethylbenzene < 0.005 0.0051,3,5-Trimethylbenzene < 0.005 0.005Vinyl acetate < 0.011 0.011Vinyl chloride < 0.002 0.002Xylene, M&P < 0.005 0.005Xylene, 0rtho < 0.005 0.005Xylene, Total < 0.011 0.011Dibromofluoromethane (surrogate) 98%1,2-Dichloroethane-d4 (surrogate) 90%Toluene-d8 (surrogate) 103%4-bromofluorobenzene (surrogate) 100%Analysis Date/Time: 10-30-14/12:31Analyst Initials tjg
Percent Solids: 92%All results reported on dry weight basis.
Compounds Sample Results (mg/kg) Rep. Limit (mg/kg) Flags
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 36
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Analytical Method: EPA 8270 CPAHPrep Method: EPA 3550CAnalytical Batch: 102914PS
Client Sample ID: GP-5 Sample Collection Date/Time: 10/27/14 16:10Envision Sample Number: 14-24293 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: soil
Benzo(a)anthracene < 0.36 0.36Benzo(a)pyrene < 0.073 0.073Benzo(b)fluoranthene < 0.36 0.36Benzo(k)fluoranthene < 0.36 0.36Chrysene < 0.36 0.36Dibenzo(a,h)anthracene < 0.073 0.073Indeno(1,2,3-cd)pyrene < 0.36 0.36Naphthalene < 0.073 0.073Nitrobenzene-d14 (surrogate) 42%2-Fluorobiphenyl (surrogate) 47%p-Terphenyl-d14 (surrogate) 79%Analysis Date/Time: 10-29-14/19:44Analyst Initials: ajgDate Extracted: 10/29/2014Initial Sample Weight: 30 gFinal Volume: 1.0 mL
Percent Solids 92%
All results reported on dry weight basis.
Compounds Sample Results (mg/kg) Rep. Limit (mg/kg) Flags
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 37
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Client Sample ID: GP-5 Sample Collection Date/Time: 10/27/14 16:10Envision Sample Number: 14-24293 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: soil
Analyte Sample Results Flags Method Percent Moisture 8.0% EPA 1684Percent Solids 92.0% EPA 1684Analysis Date: 10/29/14Analyst Initials ajg
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 38
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Analytical Method: EPA 8260Prep Method: EPA 5030BAnalytical Batch: 102914VW
Client Sample ID: GP-1W Sample Collection Date/Time: 10/27/14 10:15Envision Sample Number: 14-24294 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: water
Compounds Sample Results (ug/L) Reporting Limit (ug/L) FlagsAcetone < 100 100Acrolein < 1 1 Acrylonitrile < 0.45 1 1Benzene < 5 5Bromobenzene < 5 5Bromochloromethane < 5 5Bromodichloromethane < 5 5Bromoform < 5 5Bromomethane < 5 5n-Butanol < 50 502-Butanone (MEK) < 10 10n-Butylbenzene < 5 5sec-Butylbenzene < 5 5tert-Butylbenzene < 5 5Carbon Disulfide < 5 5Carbon Tetrachloride < 5 5Chlorobenzene < 5 5Chloroethane < 5 52-Chloroethylvinylether < 50 50Chloroform < 5 5Chloromethane < 5 52-Chlorotoluene < 5 54-Chlorotoluene < 5 51,2-Dibromo-3-chloropropane < 1 1Dibromochloromethane < 5 51,2-Dibromoethane (EDB) < 1 1Dibromomethane < 5 51,2-Dichlorobenzene < 5 51,3-Dichlorobenzene < 5 51,4-Dichlorobenzene < 5 5trans-1,4-Dichloro-2-butene < 1 1Dichlorodifluoromethane < 5 5
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
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ENVISION
Reference 67 Page 39
Analytical Report
8260 continued…Compounds Sample Results (ug/L) Reporting Limit (ug/L) Flags
1,1-Dichloroethane < 5 51,2-Dichloroethane < 5 51,1-Dichloroethene < 5 5cis-1,2-Dichloroethene < 5 5trans-1,2-Dichloroethene < 5 51,2-Dichloropropane < 5 51,3-Dichloropropane < 5 52,2-Dichloropropane < 5 51,1-Dichloropropene < 5 51,3-Dichloropropene < 4.1 4.1Ethylbenzene < 5 5Ethyl methacrylate < 100 100Hexachloro-1,3-butadiene < 2.6 2.6n-Hexane < 10 102-Hexanone < 10 10Iodomethane < 10 10Isopropylbenzene (Cumene) < 5 5p-Isopropyltoluene < 5 5Methylene chloride < 5 54-Methyl-2-pentanone (MIBK) < 10 10Methyl-tert-butyl-ether < 5 51-Methylnaphthalene < 5 52-Methylnaphthalene < 5 5n-Propylbenzene < 5 5Styrene < 5 51,1,1,2-Tetrachloroethane < 5 51,1,2,2-Tetrachloroethane < 0.66 1 1Tetrachloroethene < 5 5Toluene < 5 51,2,3-Trichlorobenzene < 5 51,2,4-Trichlorobenzene < 5 51,1,1-Trichloroethane < 5 51,1,2-Trichloroethane < 5 5Trichloroethene 86.8 5Trichlorofluoromethane < 5 51,2,3-Trichloropropane < 1 11,2,4-Trimethylbenzene < 5 51,3,5-Trimethylbenzene < 5 5Vinyl acetate < 10 10Vinyl chloride < 2 2Xylene, M&P < 5 5Xylene, 0rtho < 5 5Xylene (Total) < 10 10Dibromofluoromethane (surrogate) 103%1,2-Dichloroethane-d4 (surrogate) 99%Toluene-d8 (surrogate) 101%4-bromofluorobenzene (surrogate) 99%Analysis Date/Time: 10-29-14/10:50Analyst Initials tjg
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
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Your Projects. Our Passion.
ENVISION
Reference 67 Page 40
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Analytical Method: EPA 8270SIMPrep Method: EPA 3511Analytical Batch: 102914PW
Client Sample ID: GP-1W Sample Collection Date/Time: 10/27/14 10:15Envision Sample Number: 14-24294 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: water
Compounds Sample Results (ug/L) Reporting Limit (ug/L) FlagsBenzo(a)anthracene < 0.10 0.10Benzo(a)pyrene < 0.10 0.10Benzo(b)fluoranthene < 0.10 0.10Benzo(k)fluoranthene < 0.10 0.10Chrysene < 0.10 0.10Dibenzo(a,h)anthracene < 0.029 0.029Indeno(1,2,3-cd)pyrene < 0.022 0.022Naphthalene < 1.0 1.0
Nitrobenzene-d5 (surrogate) 22%2-Fluorobiphenyl (surrogate) 18%p-Terphenyl-d14 (surrogate) 22%Analysis Date/Time: 10-29-14/16:00Analyst Initials ajgDate Extracted 10/28/2014Initial Sample Volume 40mlFinal Volume 2.0ml
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
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Your Projects. Our Passion.
ENVISION
Reference 67 Page 41
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Analytical Method: EPA 8260Prep Method: EPA 5030BAnalytical Batch: 102914VW
Client Sample ID: GP-2W Sample Collection Date/Time: 10/27/14 12:00Envision Sample Number: 14-24295 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: water
Compounds Sample Results (ug/L) Reporting Limit (ug/L) FlagsAcetone < 100 100Acrolein < 1 1 Acrylonitrile < 0.45 1 1Benzene < 5 5Bromobenzene < 5 5Bromochloromethane < 5 5Bromodichloromethane < 5 5Bromoform < 5 5Bromomethane < 5 5n-Butanol < 50 502-Butanone (MEK) < 10 10n-Butylbenzene < 5 5sec-Butylbenzene < 5 5tert-Butylbenzene < 5 5Carbon Disulfide < 5 5Carbon Tetrachloride < 5 5Chlorobenzene < 5 5Chloroethane < 5 52-Chloroethylvinylether < 50 50Chloroform < 5 5Chloromethane < 5 52-Chlorotoluene < 5 54-Chlorotoluene < 5 51,2-Dibromo-3-chloropropane < 1 1Dibromochloromethane < 5 51,2-Dibromoethane (EDB) < 1 1Dibromomethane < 5 51,2-Dichlorobenzene < 5 51,3-Dichlorobenzene < 5 51,4-Dichlorobenzene < 5 5trans-1,4-Dichloro-2-butene < 1 1Dichlorodifluoromethane < 5 5
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
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ENVISION
Reference 67 Page 42
Analytical Report
8260 continued…Compounds Sample Results (ug/L) Reporting Limit (ug/L) Flags
1,1-Dichloroethane < 5 51,2-Dichloroethane < 5 51,1-Dichloroethene < 5 5cis-1,2-Dichloroethene < 5 5trans-1,2-Dichloroethene < 5 51,2-Dichloropropane < 5 51,3-Dichloropropane < 5 52,2-Dichloropropane < 5 51,1-Dichloropropene < 5 51,3-Dichloropropene < 4.1 4.1Ethylbenzene < 5 5Ethyl methacrylate < 100 100Hexachloro-1,3-butadiene < 2.6 2.6n-Hexane < 10 102-Hexanone < 10 10Iodomethane < 10 10Isopropylbenzene (Cumene) < 5 5p-Isopropyltoluene < 5 5Methylene chloride < 5 54-Methyl-2-pentanone (MIBK) < 10 10Methyl-tert-butyl-ether < 5 51-Methylnaphthalene < 5 52-Methylnaphthalene < 5 5n-Propylbenzene < 5 5Styrene < 5 51,1,1,2-Tetrachloroethane < 5 51,1,2,2-Tetrachloroethane < 0.66 1 1Tetrachloroethene < 5 5Toluene < 5 51,2,3-Trichlorobenzene < 5 51,2,4-Trichlorobenzene < 5 51,1,1-Trichloroethane < 5 51,1,2-Trichloroethane < 5 5Trichloroethene 50.4 5Trichlorofluoromethane < 5 51,2,3-Trichloropropane < 1 11,2,4-Trimethylbenzene < 5 51,3,5-Trimethylbenzene < 5 5Vinyl acetate < 10 10Vinyl chloride < 2 2Xylene, M&P < 5 5Xylene, 0rtho < 5 5Xylene (Total) < 10 10Dibromofluoromethane (surrogate) 103%1,2-Dichloroethane-d4 (surrogate) 100%Toluene-d8 (surrogate) 103%4-bromofluorobenzene (surrogate) 98%Analysis Date/Time: 10-29-14/11:09Analyst Initials tjg
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
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Your Projects. Our Passion.
ENVISION
Reference 67 Page 43
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Analytical Method: EPA 8270SIMPrep Method: EPA 3511Analytical Batch: 102914PW
Client Sample ID: GP-2W Sample Collection Date/Time: 10/27/14 12:00Envision Sample Number: 14-24295 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: water
Compounds Sample Results (ug/L) Reporting Limit (ug/L) FlagsBenzo(a)anthracene < 0.10 0.10Benzo(a)pyrene < 0.10 0.10Benzo(b)fluoranthene < 0.10 0.10Benzo(k)fluoranthene < 0.10 0.10Chrysene < 0.10 0.10Dibenzo(a,h)anthracene < 0.029 0.029Indeno(1,2,3-cd)pyrene < 0.022 0.022Naphthalene < 1.0 1.0
Nitrobenzene-d5 (surrogate) 35%2-Fluorobiphenyl (surrogate) 29%p-Terphenyl-d14 (surrogate) 24%Analysis Date/Time: 10-29-14/16:25Analyst Initials ajgDate Extracted 10/28/2014Initial Sample Volume 40mlFinal Volume 2.0ml
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 44
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Analytical Method: EPA 8260Prep Method: EPA 5030BAnalytical Batch: 102914VW
Client Sample ID: GP-3W Sample Collection Date/Time: 10/27/14 14:00Envision Sample Number: 14-24296 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: water
Compounds Sample Results (ug/L) Reporting Limit (ug/L) FlagsAcetone < 100 100Acrolein < 1 1 Acrylonitrile < 0.45 1 1Benzene < 5 5Bromobenzene < 5 5Bromochloromethane < 5 5Bromodichloromethane < 5 5Bromoform < 5 5Bromomethane < 5 5n-Butanol < 50 502-Butanone (MEK) < 10 10n-Butylbenzene < 5 5sec-Butylbenzene < 5 5tert-Butylbenzene < 5 5Carbon Disulfide < 5 5Carbon Tetrachloride < 5 5Chlorobenzene < 5 5Chloroethane < 5 52-Chloroethylvinylether < 50 50Chloroform < 5 5Chloromethane < 5 52-Chlorotoluene < 5 54-Chlorotoluene < 5 51,2-Dibromo-3-chloropropane < 1 1Dibromochloromethane < 5 51,2-Dibromoethane (EDB) < 1 1Dibromomethane < 5 51,2-Dichlorobenzene < 5 51,3-Dichlorobenzene < 5 51,4-Dichlorobenzene < 5 5trans-1,4-Dichloro-2-butene < 1 1Dichlorodifluoromethane < 5 5
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 45
Analytical Report
8260 continued…Compounds Sample Results (ug/L) Reporting Limit (ug/L) Flags
1,1-Dichloroethane < 5 51,2-Dichloroethane < 5 51,1-Dichloroethene < 5 5cis-1,2-Dichloroethene < 5 5trans-1,2-Dichloroethene < 5 51,2-Dichloropropane < 5 51,3-Dichloropropane < 5 52,2-Dichloropropane < 5 51,1-Dichloropropene < 5 51,3-Dichloropropene < 4.1 4.1Ethylbenzene < 5 5Ethyl methacrylate < 100 100Hexachloro-1,3-butadiene < 2.6 2.6n-Hexane < 10 102-Hexanone < 10 10Iodomethane < 10 10Isopropylbenzene (Cumene) < 5 5p-Isopropyltoluene < 5 5Methylene chloride < 5 54-Methyl-2-pentanone (MIBK) < 10 10Methyl-tert-butyl-ether < 5 51-Methylnaphthalene < 5 52-Methylnaphthalene < 5 5n-Propylbenzene < 5 5Styrene < 5 51,1,1,2-Tetrachloroethane < 5 51,1,2,2-Tetrachloroethane < 0.66 1 1Tetrachloroethene < 5 5Toluene < 5 51,2,3-Trichlorobenzene < 5 51,2,4-Trichlorobenzene < 5 51,1,1-Trichloroethane < 5 51,1,2-Trichloroethane < 5 5Trichloroethene 27.4 5Trichlorofluoromethane < 5 51,2,3-Trichloropropane < 1 11,2,4-Trimethylbenzene < 5 51,3,5-Trimethylbenzene < 5 5Vinyl acetate < 10 10Vinyl chloride < 2 2Xylene, M&P < 5 5Xylene, 0rtho < 5 5Xylene (Total) < 10 10Dibromofluoromethane (surrogate) 100%1,2-Dichloroethane-d4 (surrogate) 100%Toluene-d8 (surrogate) 101%4-bromofluorobenzene (surrogate) 97%Analysis Date/Time: 10-29-14/11:28Analyst Initials tjg
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 46
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Analytical Method: EPA 8270SIMPrep Method: EPA 3511Analytical Batch: 102914PW
Client Sample ID: GP-3W Sample Collection Date/Time: 10/27/14 14:00Envision Sample Number: 14-24296 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: water
Compounds Sample Results (ug/L) Reporting Limit (ug/L) FlagsBenzo(a)anthracene < 0.10 0.10Benzo(a)pyrene < 0.10 0.10Benzo(b)fluoranthene < 0.10 0.10Benzo(k)fluoranthene < 0.10 0.10Chrysene < 0.10 0.10Dibenzo(a,h)anthracene < 0.029 0.029Indeno(1,2,3-cd)pyrene < 0.022 0.022Naphthalene < 1.0 1.0
Nitrobenzene-d5 (surrogate) 44%2-Fluorobiphenyl (surrogate) 35%p-Terphenyl-d14 (surrogate) 30%Analysis Date/Time: 10-29-14/16:50Analyst Initials ajgDate Extracted 10/28/2014Initial Sample Volume 40mlFinal Volume 2.0ml
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 47
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Analytical Method: EPA 8260Prep Method: EPA 5030BAnalytical Batch: 102914VW
Client Sample ID: GP-4W Sample Collection Date/Time: 10/27/14 15:20Envision Sample Number: 14-24297 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: water
Compounds Sample Results (ug/L) Reporting Limit (ug/L) FlagsAcetone < 100 100Acrolein < 1 1 Acrylonitrile < 0.45 1 1Benzene < 5 5Bromobenzene < 5 5Bromochloromethane < 5 5Bromodichloromethane < 5 5Bromoform < 5 5Bromomethane < 5 5n-Butanol < 50 502-Butanone (MEK) < 10 10n-Butylbenzene < 5 5sec-Butylbenzene < 5 5tert-Butylbenzene < 5 5Carbon Disulfide < 5 5Carbon Tetrachloride < 5 5Chlorobenzene < 5 5Chloroethane < 5 52-Chloroethylvinylether < 50 50Chloroform < 5 5Chloromethane < 5 52-Chlorotoluene < 5 54-Chlorotoluene < 5 51,2-Dibromo-3-chloropropane < 1 1Dibromochloromethane < 5 51,2-Dibromoethane (EDB) < 1 1Dibromomethane < 5 51,2-Dichlorobenzene < 5 51,3-Dichlorobenzene < 5 51,4-Dichlorobenzene < 5 5trans-1,4-Dichloro-2-butene < 1 1Dichlorodifluoromethane < 5 5
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 48
Analytical Report
8260 continued…Compounds Sample Results (ug/L) Reporting Limit (ug/L) Flags
1,1-Dichloroethane < 5 51,2-Dichloroethane < 5 51,1-Dichloroethene < 5 5cis-1,2-Dichloroethene 6.24 5trans-1,2-Dichloroethene < 5 51,2-Dichloropropane < 5 51,3-Dichloropropane < 5 52,2-Dichloropropane < 5 51,1-Dichloropropene < 5 51,3-Dichloropropene < 4.1 4.1Ethylbenzene < 5 5Ethyl methacrylate < 100 100Hexachloro-1,3-butadiene < 2.6 2.6n-Hexane < 10 102-Hexanone < 10 10Iodomethane < 10 10Isopropylbenzene (Cumene) < 5 5p-Isopropyltoluene < 5 5Methylene chloride < 5 54-Methyl-2-pentanone (MIBK) < 10 10Methyl-tert-butyl-ether < 5 51-Methylnaphthalene < 5 52-Methylnaphthalene < 5 5n-Propylbenzene < 5 5Styrene < 5 51,1,1,2-Tetrachloroethane < 5 51,1,2,2-Tetrachloroethane < 0.66 1 1Tetrachloroethene < 5 5Toluene < 5 51,2,3-Trichlorobenzene < 5 51,2,4-Trichlorobenzene < 5 51,1,1-Trichloroethane < 5 51,1,2-Trichloroethane < 5 5Trichloroethene 55.7 5Trichlorofluoromethane < 5 51,2,3-Trichloropropane < 1 11,2,4-Trimethylbenzene < 5 51,3,5-Trimethylbenzene < 5 5Vinyl acetate < 10 10Vinyl chloride < 2 2Xylene, M&P < 5 5Xylene, 0rtho < 5 5Xylene (Total) < 10 10Dibromofluoromethane (surrogate) 103%1,2-Dichloroethane-d4 (surrogate) 100%Toluene-d8 (surrogate) 99%4-bromofluorobenzene (surrogate) 98%Analysis Date/Time: 10-29-14/11:46Analyst Initials tjg
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 49
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Analytical Method: EPA 8270SIMPrep Method: EPA 3511Analytical Batch: 102914PW
Client Sample ID: GP-4W Sample Collection Date/Time: 10/27/14 15:20Envision Sample Number: 14-24297 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: water
Compounds Sample Results (ug/L) Reporting Limit (ug/L) FlagsBenzo(a)anthracene < 0.10 0.10Benzo(a)pyrene < 0.10 0.10Benzo(b)fluoranthene < 0.10 0.10Benzo(k)fluoranthene < 0.10 0.10Chrysene < 0.10 0.10Dibenzo(a,h)anthracene < 0.029 0.029Indeno(1,2,3-cd)pyrene < 0.022 0.022Naphthalene < 1.0 1.0
Nitrobenzene-d5 (surrogate) 41%2-Fluorobiphenyl (surrogate) 34%p-Terphenyl-d14 (surrogate) 29%Analysis Date/Time: 10-29-14/17:15Analyst Initials ajgDate Extracted 10/28/2014Initial Sample Volume 40mlFinal Volume 2.0ml
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 50
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Analytical Method: EPA 8260Prep Method: EPA 5030BAnalytical Batch: 102914VW
Client Sample ID: GP-5W Sample Collection Date/Time: 10/27/14 16:30Envision Sample Number: 14-24298 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: water
Compounds Sample Results (ug/L) Reporting Limit (ug/L) FlagsAcetone < 100 100Acrolein < 1 1 Acrylonitrile < 0.45 1 1Benzene < 5 5Bromobenzene < 5 5Bromochloromethane < 5 5Bromodichloromethane < 5 5Bromoform < 5 5Bromomethane < 5 5n-Butanol < 50 502-Butanone (MEK) < 10 10n-Butylbenzene < 5 5sec-Butylbenzene < 5 5tert-Butylbenzene < 5 5Carbon Disulfide < 5 5Carbon Tetrachloride < 5 5Chlorobenzene < 5 5Chloroethane < 5 52-Chloroethylvinylether < 50 50Chloroform < 5 5Chloromethane < 5 52-Chlorotoluene < 5 54-Chlorotoluene < 5 51,2-Dibromo-3-chloropropane < 1 1Dibromochloromethane < 5 51,2-Dibromoethane (EDB) < 1 1Dibromomethane < 5 51,2-Dichlorobenzene < 5 51,3-Dichlorobenzene < 5 51,4-Dichlorobenzene < 5 5trans-1,4-Dichloro-2-butene < 1 1Dichlorodifluoromethane < 5 5
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 51
Analytical Report
8260 continued…Compounds Sample Results (ug/L) Reporting Limit (ug/L) Flags
1,1-Dichloroethane < 5 51,2-Dichloroethane < 5 51,1-Dichloroethene < 5 5cis-1,2-Dichloroethene 29.1 5trans-1,2-Dichloroethene < 5 51,2-Dichloropropane < 5 51,3-Dichloropropane < 5 52,2-Dichloropropane < 5 51,1-Dichloropropene < 5 51,3-Dichloropropene < 4.1 4.1Ethylbenzene < 5 5Ethyl methacrylate < 100 100Hexachloro-1,3-butadiene < 2.6 2.6n-Hexane < 10 102-Hexanone < 10 10Iodomethane < 10 10Isopropylbenzene (Cumene) < 5 5p-Isopropyltoluene < 5 5Methylene chloride < 5 54-Methyl-2-pentanone (MIBK) < 10 10Methyl-tert-butyl-ether < 5 51-Methylnaphthalene < 5 52-Methylnaphthalene < 5 5n-Propylbenzene < 5 5Styrene < 5 51,1,1,2-Tetrachloroethane < 5 51,1,2,2-Tetrachloroethane < 0.66 1 1Tetrachloroethene < 5 5Toluene < 5 51,2,3-Trichlorobenzene < 5 51,2,4-Trichlorobenzene < 5 51,1,1-Trichloroethane < 5 51,1,2-Trichloroethane < 5 5Trichloroethene 18.8 5Trichlorofluoromethane < 5 51,2,3-Trichloropropane < 1 11,2,4-Trimethylbenzene 9.34 51,3,5-Trimethylbenzene < 5 5Vinyl acetate < 10 10Vinyl chloride < 2 2Xylene, M&P < 5 5Xylene, 0rtho < 5 5Xylene (Total) < 10 10Dibromofluoromethane (surrogate) 100%1,2-Dichloroethane-d4 (surrogate) 102%Toluene-d8 (surrogate) 102%4-bromofluorobenzene (surrogate) 97%Analysis Date/Time: 10-29-14/12:05Analyst Initials tjg
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 52
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Analytical Method: EPA 8270SIMPrep Method: EPA 3511Analytical Batch: 102914PW
Client Sample ID: GP-5W Sample Collection Date/Time: 10/27/14 16:30Envision Sample Number: 14-24298 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: water
Compounds Sample Results (ug/L) Reporting Limit (ug/L) FlagsBenzo(a)anthracene < 0.10 0.10Benzo(a)pyrene < 0.10 0.10Benzo(b)fluoranthene < 0.10 0.10Benzo(k)fluoranthene < 0.10 0.10Chrysene < 0.10 0.10Dibenzo(a,h)anthracene < 0.029 0.029Indeno(1,2,3-cd)pyrene < 0.022 0.022Naphthalene < 1.0 1.0
Nitrobenzene-d5 (surrogate) 51%2-Fluorobiphenyl (surrogate) 42%p-Terphenyl-d14 (surrogate) 36%Analysis Date/Time: 10-29-14/17:40Analyst Initials ajgDate Extracted 10/28/2014Initial Sample Volume 40mlFinal Volume 2.0ml
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 53
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Analytical Method: EPA 8260Prep Method: EPA 5030BAnalytical Batch: 102914VW
Client Sample ID: TRIP BLANK Sample Collection Date/Time: 10/27/14Envision Sample Number: 14-24299 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: water
Compounds Sample Results (ug/L) Reporting Limit (ug/L) FlagsAcetone < 100 100Acrolein < 1 1 Acrylonitrile < 0.45 1 1Benzene < 5 5Bromobenzene < 5 5Bromochloromethane < 5 5Bromodichloromethane < 5 5Bromoform < 5 5Bromomethane < 5 5n-Butanol < 50 502-Butanone (MEK) < 10 10n-Butylbenzene < 5 5sec-Butylbenzene < 5 5tert-Butylbenzene < 5 5Carbon Disulfide < 5 5Carbon Tetrachloride < 5 5Chlorobenzene < 5 5Chloroethane < 5 52-Chloroethylvinylether < 50 50Chloroform < 5 5Chloromethane < 5 52-Chlorotoluene < 5 54-Chlorotoluene < 5 51,2-Dibromo-3-chloropropane < 1 1Dibromochloromethane < 5 51,2-Dibromoethane (EDB) < 1 1Dibromomethane < 5 51,2-Dichlorobenzene < 5 51,3-Dichlorobenzene < 5 51,4-Dichlorobenzene < 5 5trans-1,4-Dichloro-2-butene < 1 1Dichlorodifluoromethane < 5 5
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Reference 67 Page 54
Analytical Report
8260 continued…Compounds Sample Results (ug/L) Reporting Limit (ug/L) Flags
1,1-Dichloroethane < 5 51,2-Dichloroethane < 5 51,1-Dichloroethene < 5 5cis-1,2-Dichloroethene < 5 5trans-1,2-Dichloroethene < 5 51,2-Dichloropropane < 5 51,3-Dichloropropane < 5 52,2-Dichloropropane < 5 51,1-Dichloropropene < 5 51,3-Dichloropropene < 4.1 4.1Ethylbenzene < 5 5Ethyl methacrylate < 100 100Hexachloro-1,3-butadiene < 2.6 2.6n-Hexane < 10 102-Hexanone < 10 10Iodomethane < 10 10Isopropylbenzene (Cumene) < 5 5p-Isopropyltoluene < 5 5Methylene chloride < 5 54-Methyl-2-pentanone (MIBK) < 10 10Methyl-tert-butyl-ether < 5 51-Methylnaphthalene < 5 52-Methylnaphthalene < 5 5Naphthalene < 1.4 1.4n-Propylbenzene < 5 5Styrene < 5 51,1,1,2-Tetrachloroethane < 5 51,1,2,2-Tetrachloroethane < 0.66 1 1Tetrachloroethene < 5 5Toluene < 5 51,2,3-Trichlorobenzene < 5 51,2,4-Trichlorobenzene < 5 51,1,1-Trichloroethane < 5 51,1,2-Trichloroethane < 5 5Trichloroethene < 5 5Trichlorofluoromethane < 5 51,2,3-Trichloropropane < 1 11,2,4-Trimethylbenzene < 5 51,3,5-Trimethylbenzene < 5 5Vinyl acetate < 10 10Vinyl chloride < 2 2Xylene, M&P < 5 5Xylene, 0rtho < 5 5Xylene (Total) < 10 10Dibromofluoromethane (surrogate) 100%1,2-Dichloroethane-d4 (surrogate) 98%Toluene-d8 (surrogate) 99%4-bromofluorobenzene (surrogate) 99%Analysis Date/Time: 10-29-14/12:24Analyst Initials tjg
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Reference 67 Page 55
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Analytical Method: EPA 8260Prep Method: EPA 5035AAnalytical Batch: 103014VS
Client Sample ID: GP-5D Sample Collection Date/Time: 10/27/14 17:15Envision Sample Number: 14-24300 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: soil
Acetone < 5.56 5.56 2Acrolein < 0.00944 0.056 1,2Acrylonitrile < 0.111 0.111 2Benzene < 0.034 0.278 1,2Bromobenzene < 0.278 0.278 2Bromochloromethane < 0.278 0.278 2Bromodichloromethane < 0.278 0.278 2Bromoform < 0.278 0.278 2Bromomethane < 0.278 0.278 2n-Butanol < 2.78 2.78 22-Butanone (MEK) < 0.556 0.556 2n-Butylbenzene 4.49 0.278 2sec-Butylbenzene 2.64 0.278 2tert-Butylbenzene < 0.278 0.278 2Carbon Disulfide < 0.278 0.278 2Carbon Tetrachloride < 0.278 0.278 2Chlorobenzene < 0.278 0.278 2Chloroethane < 0.278 0.278 22-Chloroethylvinylether < 2.78 2.78 2Chloroform < 0.278 0.278 2Chloromethane < 0.278 0.278 22-Chlorotoluene < 0.278 0.278 24-Chlorotoluene < 0.278 0.278 21,2-Dibromo-3-chloropropane < 0.0944 0.0944 2Dibromochloromethane < 0.278 0.278 21,2-Dibromoethane (EDB) < 0.0156 0.056 1,2Dibromomethane < 0.278 0.278 21,2-Dichlorobenzene < 0.278 0.278 21,3-Dichlorobenzene < 0.278 0.278 21,4-Dichlorobenzene < 0.278 0.278 2trans-1,4-Dichloro-2-butene < 0.278 0.278 2Dichlorodifluoromethane < 0.278 0.278 21,1-Dichloroethane < 0.278 0.278 21,2-Dichloroethane < 0.278 0.278 21,1-Dichloroethene < 0.278 0.278 2
Compounds Sample Results (mg/kg) Rep. Limit (mg/kg) Flags
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Reference 67 Page 56
Analytical Report
8260 continued…
cis-1,2-Dichloroethene < 0.278 0.278 2trans-1,2-Dichloroethene < 0.278 0.278 21,2-Dichloropropane < 0.278 0.278 21,3-Dichloropropane < 0.278 0.278 22,2-Dichloropropane < 0.278 0.278 21,1-Dichloropropene < 0.278 0.278 21,3-Dichloropropene < 0.278 0.278 2Ethylbenzene 5.14 0.278 2Ethyl methacrylate < 5.56 5.56 2Hexachloro-1,3-butadiene < 0.278 0.278 2n-Hexane < 0.556 0.556 22-Hexanone < 0.556 0.556 2Iodomethane < 0.556 0.556 2Isopropylbenzene (Cumene) 2.76 0.278 2p-Isopropyltoluene 3.42 0.278 2Methylene chloride < 1.11 1.11 24-Methyl-2-pentanone (MIBK) < 0.556 0.556 2Methyl-tert-butyl-ether < 0.180 0.278 1,21-Methylnaphthalene 4.06 0.278 22-Methylnaphthalene 4.78 0.278 2n-Propylbenzene 10.2 0.278 2Styrene < 0.278 0.278 21,1,1,2-Tetrachloroethane < 0.278 0.278 21,1,2,2-Tetrachloroethane < 0.278 0.278 2Tetrachloroethene < 0.278 0.278 2Toluene < 0.278 0.278 21,2,3-Trichlorobenzene < 0.278 0.278 21,2,4-Trichlorobenzene < 0.278 0.278 21,1,1-Trichloroethane < 0.278 0.278 21,1,2-Trichloroethane < 0.278 0.278 2Trichloroethene < 0.278 0.278 2Trichlorofluoromethane < 0.278 0.278 21,2,3-Trichloropropane < 0.278 0.278 21,2,4-Trimethylbenzene 109 2.78 31,3,5-Trimethylbenzene 29.6 2.78 3Vinyl acetate < 0.556 0.556 2Vinyl chloride < 0.111 0.111 2Xylene, M&P 5.72 0.278 2Xylene, 0rtho < 0.278 0.278 2Xylene, Total 5.72 0.556 2Dibromofluoromethane (surrogate) 88%1,2-Dichloroethane-d4 (surrogate) 106%Toluene-d8 (surrogate) 96%4-bromofluorobenzene (surrogate) 96%Analysis Date/Time: 10-30-14/12:49Analyst Initials tjg
Percent Solids: 90%All results reported on dry weight basis.
Compounds Sample Results (mg/kg) Rep. Limit (mg/kg) Flags
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Reference 67 Page 57
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Analytical Method: EPA 8270 CPAHPrep Method: EPA 3550CAnalytical Batch: 102914PS
Client Sample ID: GP-5D Sample Collection Date/Time: 10/27/14 17:15Envision Sample Number: 14-24300 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: soil
Benzo(a)anthracene < 0.37 0.37Benzo(a)pyrene < 0.074 0.074Benzo(b)fluoranthene < 0.37 0.37Benzo(k)fluoranthene < 0.37 0.37Chrysene < 0.37 0.37Dibenzo(a,h)anthracene < 0.074 0.074Indeno(1,2,3-cd)pyrene < 0.37 0.37Naphthalene 3.87 0.074Nitrobenzene-d14 (surrogate) 48%2-Fluorobiphenyl (surrogate) 53%p-Terphenyl-d14 (surrogate) 87%Analysis Date/Time: 10-29-14/20:11Analyst Initials: ajgDate Extracted: 10/29/2014Initial Sample Weight: 30 gFinal Volume: 1.0 mL
Percent Solids 90%
All results reported on dry weight basis.
Compounds Sample Results (mg/kg) Rep. Limit (mg/kg) Flags
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Reference 67 Page 58
Analytical Report
Client Name: KERR ENVIRONMENTAL SERVICES, INC
Project ID: CVS
Client Project Manager: DANA KERR
ENVision Project Number: 2014-3153
Client Sample ID: GP-5D Sample Collection Date/Time: 10/27/14 17:15Envision Sample Number: 14-24300 Sample Received Date/Time: 10/27/14 17:29Sample Matrix: soil
Analyte Sample Results Flags Method Percent Moisture 10.0% EPA 1684Percent Solids 90.0% EPA 1684Analysis Date: 10/29/14Analyst Initials ajg
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Reference 67 Page 59
EPA 8260 Quality Control Data
ENVision Batch Number: 103014VS
Method Blank (MB): MB Results (ug/kg) Rep Lim (ug/kg) Flag
Acetone < 100 100
Acrolein < 0.17 1 1
Acrylonitrile < 2 2
Benzene < 5 5
Bromobenzene < 5 5
Bromochloromethane < 5 5
Bromodichloromethane < 5 5
Bromoform < 5 5
Bromomethane < 5 5
n-Butanol < 50 50
2-Butanone (MEK) < 10 10
n-Butylbenzene < 5 5
sec-Butylbenzene < 5 5
tert-Butylbenzene < 5 5
Carbon Disulfide < 5 5
Carbon Tetrachloride < 5 5
Chlorobenzene < 5 5
Chloroethane < 5 5
2-Chloroethylvinylether < 50 50
Chloroform < 5 5
Chloromethane < 5 5
2-Chlorotoluene < 5 5
4-Chlorotoluene < 5 5
1,2-Dibromo-3-chloropropane < 1.7 1.7
Dibromochloromethane < 5 5
1,2-Dibromoethane (EDB) < 0.28 1 1
Dibromomethane < 5 5
1,2-Dichlorobenzene < 5 5
1,3-Dichlorobenzene < 5 5
1,4-Dichlorobenzene < 5 5
trans-1,4-Dichloro-2-butene < 5 5
Dichlorodifluoromethane < 5 5
1,1-Dichloroethane < 5 5
1,2-Dichloroethane < 5 5
1,1-Dichloroethene < 5 5
cis-1,2-Dichloroethene < 5 5
trans-1,2-Dichloroethene < 5 5
1,2-Dichloropropane < 5 5
1,3-Dichloropropane < 5 5
2,2-Dichloropropane < 5 5
1,1-Dichloropropene < 5 5
1,3-Dichloropropene < 5 5
Ethylbenzene < 5 5
Ethyl methacrylate < 100 100
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Reference 67 Page 60
8260 QC Continued…
Method Blank (MB): MB Results (ug/kg) Rep Lim (ug/kg) Flag
Hexachloro-1,3-butadiene < 5 5
2-Hexanone < 10 10
n-Hexane < 10 10
Iodomethane < 10 10
Isopropylbenzene (Cumene) < 5 5
p-Isopropyltoluene < 5 5
Methylene chloride < 20 20
4-Methyl-2-pentanone (MIBK) < 10 10
Methyl-tert-butyl-ether < 5 5
1-Methylnaphthalene < 5 5
2-Methylnaphthalene < 5 5
Naphthalene < 5 5
n-Propylbenzene < 5 5
Styrene < 5 5
1,1,1,2-Tetrachloroethane < 5 5
1,1,2,2-Tetrachloroethane < 5 5
Tetrachloroethene < 5 5
Toluene < 5 5
1,2,3-Trichlorobenzene < 5 5
1,2,4-Trichlorobenzene < 5 5
1,1,1-Trichloroethane < 5 5
1,1,2-Trichloroethane < 5 5
Trichloroethene < 5 5
Trichlorofluoromethane < 5 5
1,2,3-Trichloropropane < 5 5
1,2,4-Trimethylbenzene < 5 5
1,3,5-Trimethylbenzene < 5 5
Vinyl acetate < 10 10
Vinyl chloride < 2 2
Xylene, M&P < 5 5
Xylene, 0rtho < 5 5
Xylenes, Total < 10 10
Dibromofluoromethane (surrogate) 103%
1,2-Dichloroethane-d4 (surrogate) 105%
Toluene-d8 (surrogate) 104%
4-bromofluorobenzene (surrogate) 100%
Analysis Date/Time: 10-30-14/11:01
Analyst Initials tjg
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
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Reference 67 Page 61
8260 QC Continued…
LCS/LCSD LCS Results (ug/kg)LCS/LCSD Conc.
(ug/kg)LCSD Result
(ug/kg) LCS Rec.LCSD Rec. % D Flag
Vinyl Chloride 46.6 50 50.1 93% 100% 7.2
1,1-Dichloroethene 46.2 50 49.3 92% 99% 6.5
trans-1,2-Dichloroethene 50.2 50 52.2 100% 104% 3.9
Methyl-tert-butyl ether 51.8 50 55.1 104% 110% 6.2
1,1-dichloroethane 46.4 50 48.9 93% 98% 5.2
cis-1,2-Dichloroethene 47.2 50 50.7 94% 101% 7.2
Chloroform 47.0 50 51.3 94% 103% 8.7
1,1,1-Trichloroethane 48.2 50 50.4 96% 101% 4.5
Benzene 48.5 50 50.3 97% 101% 3.6
Trichloroethene 48.3 50 51.9 97% 104% 7.2
Toluene 49.4 50 52.0 99% 104% 5.1
1,1,1,2-Tetrachloroethane 50.4 50 50.4 101% 101% 0.0
Chlorobenzene 51.2 50 51.1 102% 102% 0.2
Ethylbenzene 49.9 50 49.4 100% 99% 1.0
o-Xylene 48.7 50 50.0 97% 100% 2.6
n-Propylbenzene 50.0 50 50.9 100% 102% 1.8
Dibromofluoromethane (surrogate) 98% 102%
1,2-Dichloroethane-d4 (surrogate) 109% 94%
Toluene-d8 (surrogate) 101% 99%
4-bromofluorobenzene (surrogate) 103% 100%
Analysis Date/Time: 10-30-14/10:25 10-30-14/10:43
Analyst Initials tjg tjg
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
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Reference 67 Page 62
EPA 8270 cPAH Quality Control Data
ENVision Batch Number: 102914PS1
Method Blank (MB):Method Blank
Results (mg/kg)Reporting Limit
(mg/kg) Flag
Benzo(a)anthracene < 0.33 0.33
Benzo(a)pyrene < 0.33 0.33
Benzo(b)fluoranthene < 0.33 0.33
Benzo(k)fluoranthene < 0.33 0.33
Chrysene < 0.33 0.33
Dibenzo(a,h)anthracene < 0.33 0.33
Indeno(1,2,3-cd)pyrene < 0.33 0.33
Naphthalene < 0.33 0.33
Nitrobenzene-d5 (surrogate) 52%
2-Fluorobiphenyl (surrogate) 58%
p-Terphenyl-d14 (surrogate) 99%
Analysis Date/Time 10-29-14/16:36
Analyst Initials ajg
Date Extracted 10/29/2014
Initial Sample Weight: 30 g
Final Volume 1.0 mL
LCS/LCSD LCS Results LCS
Concentration LCSD ResultsLCS
RecoveryLCSD
Recovery RPD Flag
Benzo(a)anthracene 31.65 50 30.55 63.3% 61.1% 3.5%
Benzo(a)pyrene 32.07 50 31.31 64.1% 62.6% 2.4%
Benzo(b)fluoranthene 33.12 50 33.91 66.2% 67.8% 2.4%
Benzo(k)fluoranthene 34.81 50 31.89 69.6% 63.8% 8.8%
Chrysene 33.39 50 32.45 66.8% 64.9% 2.9%
Dibenzo(a,h)anthracene 31.54 50 30.29 63.1% 60.6% 4.0%
Indeno(1,2,3-cd)pyrene 30.96 50 29.69 61.9% 59.4% 4.2%
Naphthalene 25.69 50 24.98 51.4% 50.0% 2.8%Nitrobenzene-d5 (surrogate) 49% 54%2-Fluorobiphenyl (surrogate) 58% 61%p-Terphenyl-d14 (surrogate) 87% 97%
Analysis Date/Time: 10-29-14/17:03 10-29-14/17:30Analyst Initials: ajg ajgDate Extracted: 10/29/2014 10/29/2014
Initial Sample Weight: 30 g 30 gFinal Volume: 1.0 mL 1.0 mL
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Reference 67 Page 63
EPA 8260 Quality Control Data
ENVision Batch Number: 102914VW
Method Blank (MB): MB Results (ug/L) Rep Lim (ug/L) Flag
Acetone < 100 100
Acrolein < 1 1
Acrylonitrile < 0.45 1 1
Benzene < 5 5
Bromobenzene < 5 5
Bromochloromethane < 5 5
Bromodichloromethane < 5 5
Bromoform < 5 5
Bromomethane < 5 5
n-Butanol < 50 50
2-Butanone (MEK) < 10 10
n-Butylbenzene < 5 5
sec-Butylbenzene < 5 5
tert-Butylbenzene < 5 5
Carbon Disulfide < 5 5
Carbon Tetrachloride < 5 5
Chlorobenzene < 5 5
Chloroethane < 5 5
2-Chloroethylvinylether < 50 50
Chloroform < 5 5
Chloromethane < 5 5
2-Chlorotoluene < 5 5
4-Chlorotoluene < 5 5
1,2-Dibromo-3-chloropropane < 1 1
Dibromochloromethane < 5 5
1,2-Dibromoethane (EDB) < 1 1
Dibromomethane < 5 5
1,2-Dichlorobenzene < 5 5
1,3-Dichlorobenzene < 5 5
1,4-Dichlorobenzene < 5 5
trans-1,4-Dichloro-2-butene < 1 1
Dichlorodifluoromethane < 5 5
1,1-Dichloroethane < 5 5
1,2-Dichloroethane < 5 5
1,1-Dichloroethene < 5 5
cis-1,2-Dichloroethene < 5 5
trans-1,2-Dichloroethene < 5 5
1,2-Dichloropropane < 5 5
1,3-Dichloropropane < 5 5
2,2-Dichloropropane < 5 5
1,1-Dichloropropene < 5 5
1,3-Dichloropropene < 4.1 4.1
Ethylbenzene < 5 5
Ethyl methacrylate < 100 100
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Reference 67 Page 64
8260 QC Continued…
Method Blank (MB): MB Results (ug/L) Rep Lim (ug/L) Flag
Hexachloro-1,3-butadiene < 2.6 2.6
2-Hexanone < 10 10
n-Hexane < 10 10
Iodomethane < 10 10
Isopropylbenzene (Cumene) < 5 5
p-Isopropyltoluene < 5 5
Methylene chloride < 5 5
4-Methyl-2-pentanone (MIBK) < 10 10
Methyl-tert-butyl-ether < 5 5
1-Methylnaphthalene < 5 5
2-Methylnaphthalene < 5 5
Naphthalene < 1.4 1.4
n-Propylbenzene < 5 5
Styrene < 5 5
1,1,1,2-Tetrachloroethane < 5 5
1,1,2,2-Tetrachloroethane < 0.66 1 1
Tetrachloroethene < 5 5
Toluene < 5 5
1,2,3-Trichlorobenzene < 5 5
1,2,4-Trichlorobenzene < 5 5
1,1,1-Trichloroethane < 5 5
1,1,2-Trichloroethane < 5 5
Trichloroethene < 5 5
Trichlorofluoromethane < 5 5
1,2,3-Trichloropropane < 1 1
1,2,4-Trimethylbenzene < 5 5
1,3,5-Trimethylbenzene < 5 5
Vinyl acetate < 10 10
Vinyl chloride < 2 2
Xylene, M&P < 5 5
Xylene, 0rtho < 5 5
Xylene (total) < 10 10
Dibromofluoromethane (surrogate) 97%
1,2-Dichloroethane-d4 (surrogate) 90%
Toluene-d8 (surrogate) 95%
4-bromofluorobenzene (surrogate) 96%
Analysis Date/Time: 10-29-14/10:12
Analyst Initials tjg
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639
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ENVISION
Reference 67 Page 65
8260 QC Continued…
LCS/LCSD LCS Results (ug/L)
LCS/LCSD Conc. (ug/L)
LCSD Result (ug/L) LCS Rec.
LCSD Rec. % D Flag
Vinyl Chloride 52.4 50 52.4 105% 105% 0.0
1,1-Dichloroethene 58.5 50 56.1 117% 112% 4.2
trans-1,2-Dichloroethene 51.4 50 51.0 103% 102% 0.8
Methyl-tert-butyl-ether 57.0 50 51.5 114% 103% 10.1
1,1-Dichloroethane 56.3 50 55.5 113% 111% 1.4
cis-1,2-Dichloroethene 57.0 50 54.5 114% 109% 4.5
Chloroform 54.8 50 53.6 110% 107% 2.2
1,1,1-Trichloroethane 55.0 50 53.1 110% 106% 3.5
Benzene 56.4 50 56.1 113% 112% 0.5
Trichloroethene 53.3 50 52.8 107% 106% 0.9
Toluene 53.4 50 54.7 107% 109% 2.4
1,1,1,2-Tetracholorethane 52.0 50 51.5 104% 103% 1.0
Chlorobenzene 53.4 50 52.7 107% 105% 1.3
Ethylbenzene 57.3 50 56.2 115% 112% 1.9
o-Xylene 53.3 50 53.9 107% 108% 1.1
n-Propylbenzene 59.5 50 58.0 119% 116% 2.6
Dibromofluoromethane (surrogate) 93% 99%
1,2-Dichloroethane-d4 (surrogate) 112% 97%
Toluene-d8 (surrogate) 94% 102%
4-bromofluorobenzene (surrogate) 100% 105%
Analysis Date/Time: 10-29-14/09:15 10-29-14/09:34
Analyst Initials tjg tjg
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
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Reference 67 Page 66
EPA 8270SIM Quality Control Data
ENVision Batch Number: 102814PW3
Method Blank (MB):Method Blank Result (ug/L)
Reporting Limit (ug/L) Flag
Benzo(a)anthracene < 0.10 0.10
Benzo(a)pyrene < 0.10 0.10
Benzo(b)fluoranthene < 0.10 0.10
Benzo(k)fluoranthene < 0.10 0.10
Chrysene < 0.10 0.10
Dibenzo(a,h)anthracene < 0.10 0.10
Indeno(1,2,3-cd)pyrene < 0.022 0.022
Naphthalene < 1.0 1.0
Nitrobenzene-d14 (surrogate) 52%
2-Fluorobiphenyl (surrogate) 42%
p-Terphenyl-d14 (surrogate) 35%
Analysis Date/Time: 10-29-14/09:23
Analyst Initials ajg
Date Extracted 10/28/2014
Initial Sample Volume 40ml
Final Volume 2.0ml
LCS/LCSDLCS Results
(ug/L)LCS/LCSD
Conc. (ug/L)LCSD Results
(ug/L)LCS
RecoveryLCSD
Recovery RPD Flag
Benzo(a)anthracene 1.07 2.0 1.15 53.5% 57.5% 7.2%
Benzo(a)pyrene 1.37 2.0 1.24 68.5% 62.0% 10.0%
Benzo(b)fluoranthene 1.07 2.0 1.45 53.5% 72.5% 30.2%
Benzo(k)fluoranthene 1.15 2.0 1.23 57.5% 61.5% 6.7%
Chrysene 1.13 2.0 1.12 56.5% 56.0% 0.9%
Dibenzo(a,h)anthracene 1.01 2.0 1.09 50.5% 54.5% 7.6%
Indeno(1,2,3-cd)pyrene 1.02 2.0 1.00 51.0% 50.0% 2.0%
Naphthalene 1.57 2.0 1.31 78.5% 65.5% 18.1%Nitrobenzene-d14(surrogate) 111% 81%2-Fluorobiphenyl (surrogate) 92% 68%p-Terphenyl-d14 (surrogate) 52% 49%
Analysis Date/Time: 10-29-14/09:48 10-29-14/10:13Analyst Initials: ajg ajgDate Extracted: 10/28/2014 10/28/2014
Initial Sample Volume: 40ml 40mlFinal Volume: 2.0ml 2.0ml
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
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Your Projects. Our Passion.
ENVISION
Reference 67 Page 67
Flag Number Comments1 Reported value is below the reporting limit but above the MDL.2 Reported value is from a 50x dilution. DAE 10-30-143 Reported value is from a 500x dilution. DAE 10-30-14
ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive
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www.envisionlaboratories.com
Your Projects. Our Passion.
ENVISION
Reference 67 Page 68
Reference 67 Page 69
Reference 67 Page 70
Mr. Dana Kerr Kerr Environmental Services, Inc. 709 Main Street Ellettsville, IN 47429 November 21, 2014 ENVision Project Number: 2014-517 Client Project Name: CVS Dear Mr. Kerr, Please find the attached analytical report for the samples received November 14, 2014. All test methods performed were fully compliant with local, state, and federal EPA methods unless otherwise noted. The project was analyzed as requested on the enclosed chain of custody record. Please review the comments section for additional information about your results or Quality Control data. Feel free to contact me if you have any questions or comments regarding your analytical report or service. Thank you for your business. EnvisionAir looks forward to working with you on your next project. Yours Sincerely, David Norris Client Services Manager EnvisionAir
EnvisionAir 1441 Sadlier Circle West Drive
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Fax: 317-351-0882 www.envision-air.com
Reference 67 Page 71
Client Name: KERR ENVIRONMENTAL
Project ID: CVS
Client Project Manager: DANA KERR
EnvisionAir Project Number: 2014-517
Sample Summary
Canister Pressure / Vacuum
Laboratory Sample Number: Sample Description: Matrix:
START Date
Collected:
START Time
Collected:End Date Collected:
End Time Collected:
Date Received:
Time Received
Initial Field (in. Hg)
Final Field (in. Hg)
Lab Received (in. Hg)
14-2000 SS-1 A 11/13/14 15:21 11/14/14 15:55 -29 -3 -314-2001 SS-2 A 11/13/14 15:38 11/14/14 15:55 -29 0 014-2002 SS-3 A 11/13/14 15:45 11/14/14 15:55 -29 -2 -214-2003 SS-4 A 11/13/14 15:56 11/14/14 15:55 -28 -1 -114-2004 SS-5 A 11/13/14 16:05 11/14/14 15:55 -29 -1.5 -1.514-2005 IA-1 A 11/13/14 15:02 11/14/14 15:02 11/14/14 15:55 -29 0 014-2006 IA-2 A 11/13/14 15:03 11/14/14 15:04 11/14/14 15:55 -29 -1 -114-2007 IA-3 A 11/13/14 15:04 11/14/14 15:06 11/14/14 15:55 -29 -2 -214-2008 IA-4 A 11/13/14 15:05 11/14/14 15:08 11/14/14 15:55 -29 -3.5 -3.514-2009 IA-5 A 11/13/14 15:06 11/14/14 15:10 11/14/14 15:55 -29 -3.5 -3.5
EnvisionAir 1441 Sadlier Circle West Drive
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Fax: 317-351-0882 www.envision-air.com
Reference 67 Page 72
Client Name: KERR ENVIRONMENTAL
Project ID: CVS
Client Project Manager: DANA KERR
EnvisionAir Project Number: 2014-517
Analytical Method: TO-15 Analytical Batch: 111814TAIR
Client Sample ID: SS-1 Sample Collection START Date/Time: 11/13/14 15:21Sample Received Date/Time: 11/14/14 15:55
Envision Sample Number: 14-2000Sample Matrix: AIR
Compounds Sample Results ug/m³ Reporting Limit ug/m³ Flag 4-Ethyltoluene < 4920 4920 2 4-Methyl-2-pentanone (MIBK) < 20500 20500 21,1,1-Trichloroethane < 5460 5460 21,1,2,2-Tetrachloroethane < 3.36 3.36 1,21,1,2-Trichloroethane < 2.10 2.10 1,21,1-Dichloroethane < 40.5 40.5 21,1-Dichloroethene < 1980 1980 21,1-Dichloropropene < 454 454 21,2,4-Trichlorobenzene < 7.42 7.42 21,2,4-Trimethylbenzene < 49.2 49.2 21,2-dibromoethane (EDB) < 0.32 0.32 1,21,2-Dichlorobenzene < 601 601 21,2-Dichloroethane < 4.05 4.05 21,2-Dichloropropane < 4.62 4.62 21,3,5-Trimethylbenzene < 49.2 49.2 21,3-Butadiene < 2.21 2.21 21,3-Dichlorobenzene < 601 601 21,4-Dichlorobenzene < 6.01 6.01 21,4-Dioxane < 18.0 18.0 22-Butanone (MEK) < 29500 29500 22-Hexanone < 205 205 2Acetone < 23800 23800 2Benzene 30.0 16.0 2Benzyl Chloride < 4.14 4.14 1,2Bromodichloromethane < 5.36 5.36 1,2Bromoform < 103 103 2Bromomethane < 38.8 38.8 2Carbon Disulfide < 3110 3110 2Carbon Tetrachloride < 6.29 6.29 2Chlorobenzene < 230 230 2Chloroethane < 132 132 2
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Reference 67 Page 73
Compounds Sample Results ug/m³ Reporting Limit ug/m³ FlagChloroform < 8.30 8.30 2Chloromethane < 206 206 2cis-1,2-Dichloroethene < 198 198 2cis-1,3-Dichloropropene < 45.4 45.4 2Cyclohexane < 55100 55100 2Dibromochloromethane < 8.52 8.52 2Dichlorodifluoromethane < 495 495 2Ethyl Acetate < 18000 18000 2Ethylbenzene < 86.8 86.8 2Hexachloro-1,3-butadiene < 10.7 10.7 2Isooctane < 4670 4670 2m,p-Xylene < 434 434 2Methylene Chloride < 417 417 2Methyl-tert-butyl ether < 361 361 2N-Heptane < 4100 4100 2N-Hexane < 1760 1760 2o-Xylene < 434 434 2Propylene < 1720 1720 2Styrene < 4260 4260 2Tetrachloroethene 384 31.9 2Tetrahydrofuran < 2950 2950 2Toluene < 37700 37700 2trans-1,2-Dichloroethene < 396 396 2trans-1,3-Dichloropropene < 45.4 45.4 2Trichlorethene 139 10.7 2Trichlorofluoromethane < 5620 5620 2Vinyl Acetate < 1760 1760 2Vinyl Bromide < 4.37 4.37 2Vinyl Chloride < 12.8 12.8 24-bromofluorobenzene (surrogate) 91%Analysis Date/Time: 11-19-14/05:48Analyst Initials tjg
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Reference 67 Page 74
Client Name: KERR ENVIRONMENTAL
Project ID: CVS
Client Project Manager: DANA KERR
EnvisionAir Project Number: 2014-517
Analytical Method: TO-15 Analytical Batch: 111814TAIR
Client Sample ID: SS-2 Sample Collection START Date/Time: 11/13/14 15:38Sample Received Date/Time: 11/14/14 15:55
Envision Sample Number: 14-2001Sample Matrix: AIR
Compounds Sample Results ug/m³ Reporting Limit ug/m³ Flag 4-Ethyltoluene < 4920 4920 2 4-Methyl-2-pentanone (MIBK) < 20500 20500 21,1,1-Trichloroethane < 5460 5460 21,1,2,2-Tetrachloroethane < 3.36 3.36 1,21,1,2-Trichloroethane < 2.10 2.10 1,21,1-Dichloroethane < 40.5 40.5 21,1-Dichloroethene < 1980 1980 21,1-Dichloropropene < 454 454 21,2,4-Trichlorobenzene < 7.42 7.42 21,2,4-Trimethylbenzene < 49.2 49.2 21,2-dibromoethane (EDB) < 0.32 0.32 1,21,2-Dichlorobenzene < 601 601 21,2-Dichloroethane < 4.05 4.05 21,2-Dichloropropane < 4.62 4.62 21,3,5-Trimethylbenzene < 49.2 49.2 21,3-Butadiene < 2.21 2.21 21,3-Dichlorobenzene < 601 601 21,4-Dichlorobenzene < 6.01 6.01 21,4-Dioxane < 18.0 18.0 22-Butanone (MEK) < 29500 29500 22-Hexanone < 205 205 2Acetone < 23800 23800 2Benzene 26.5 16.0 2Benzyl Chloride < 4.14 4.14 1,2Bromodichloromethane < 5.36 5.36 1,2Bromoform < 103 103 2Bromomethane < 38.8 38.8 2Carbon Disulfide < 3110 3110 2Carbon Tetrachloride < 6.29 6.29 2Chlorobenzene < 230 230 2Chloroethane < 132 132 2
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Reference 67 Page 75
Compounds Sample Results ug/m³ Reporting Limit ug/m³ FlagChloroform < 8.30 8.30 2Chloromethane < 206 206 2cis-1,2-Dichloroethene < 198 198 2cis-1,3-Dichloropropene < 45.4 45.4 2Cyclohexane < 55100 55100 2Dibromochloromethane < 8.52 8.52 2Dichlorodifluoromethane < 495 495 2Ethyl Acetate < 18000 18000 2Ethylbenzene < 86.8 86.8 2Hexachloro-1,3-butadiene < 10.7 10.7 2Isooctane < 4670 4670 2m,p-Xylene < 434 434 2Methylene Chloride < 417 417 2Methyl-tert-butyl ether < 361 361 2N-Heptane < 4100 4100 2N-Hexane < 1760 1760 2o-Xylene < 434 434 2Propylene < 1720 1720 2Styrene < 4260 4260 2Tetrachloroethene < 31.9 31.9 2Tetrahydrofuran < 2950 2950 2Toluene < 37700 37700 2trans-1,2-Dichloroethene < 396 396 2trans-1,3-Dichloropropene < 45.4 45.4 2Trichlorethene < 10.7 10.7 2Trichlorofluoromethane < 5620 5620 2Vinyl Acetate < 1760 1760 2Vinyl Bromide < 4.37 4.37 2Vinyl Chloride < 12.8 12.8 24-bromofluorobenzene (surrogate) 99%Analysis Date/Time: 11-19-14/06:23Analyst Initials tjg
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Fax: 317-351-0882 www.envision-air.com
Reference 67 Page 76
Client Name: KERR ENVIRONMENTAL
Project ID: CVS
Client Project Manager: DANA KERR
EnvisionAir Project Number: 2014-517
Analytical Method: TO-15 Analytical Batch: 111814TAIR
Client Sample ID: SS-3 Sample Collection START Date/Time: 11/13/14 15:45Sample Received Date/Time: 11/14/14 15:55
Envision Sample Number: 14-2002Sample Matrix: AIR
Compounds Sample Results ug/m³ Reporting Limit ug/m³ Flag 4-Ethyltoluene < 4920 4920 2 4-Methyl-2-pentanone (MIBK) < 20500 20500 21,1,1-Trichloroethane < 5460 5460 21,1,2,2-Tetrachloroethane < 3.36 3.36 1,21,1,2-Trichloroethane < 2.10 2.10 1,21,1-Dichloroethane < 40.5 40.5 21,1-Dichloroethene < 1980 1980 21,1-Dichloropropene < 454 454 21,2,4-Trichlorobenzene < 7.42 7.42 21,2,4-Trimethylbenzene < 49.2 49.2 21,2-dibromoethane (EDB) < 0.32 0.32 1,21,2-Dichlorobenzene < 601 601 21,2-Dichloroethane < 4.05 4.05 21,2-Dichloropropane < 4.62 4.62 21,3,5-Trimethylbenzene < 49.2 49.2 21,3-Butadiene < 2.21 2.21 21,3-Dichlorobenzene < 601 601 21,4-Dichlorobenzene < 6.01 6.01 21,4-Dioxane < 18.0 18.0 22-Butanone (MEK) < 29500 29500 22-Hexanone < 205 205 2Acetone < 23800 23800 2Benzene 23.0 16.0 2Benzyl Chloride < 4.14 4.14 1,2Bromodichloromethane < 5.36 5.36 1,2Bromoform < 103 103 2Bromomethane < 38.8 38.8 2Carbon Disulfide < 3110 3110 2Carbon Tetrachloride < 6.29 6.29 2Chlorobenzene < 230 230 2Chloroethane < 132 132 2
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Reference 67 Page 77
Compounds Sample Results ug/m³ Reporting Limit ug/m³ FlagChloroform < 8.30 8.30 2Chloromethane < 206 206 2cis-1,2-Dichloroethene < 198 198 2cis-1,3-Dichloropropene < 45.4 45.4 2Cyclohexane < 55100 55100 2Dibromochloromethane < 8.52 8.52 2Dichlorodifluoromethane < 495 495 2Ethyl Acetate < 18000 18000 2Ethylbenzene < 86.8 86.8 2Hexachloro-1,3-butadiene < 10.7 10.7 2Isooctane < 4670 4670 2m,p-Xylene < 434 434 2Methylene Chloride < 417 417 2Methyl-tert-butyl ether < 361 361 2N-Heptane < 4100 4100 2N-Hexane < 1760 1760 2o-Xylene < 434 434 2Propylene < 1720 1720 2Styrene < 4260 4260 2Tetrachloroethene < 31.9 31.9 2Tetrahydrofuran < 2950 2950 2Toluene < 37700 37700 2trans-1,2-Dichloroethene < 396 396 2trans-1,3-Dichloropropene < 45.4 45.4 2Trichlorethene < 10.7 10.7 2Trichlorofluoromethane < 5620 5620 2Vinyl Acetate < 1760 1760 2Vinyl Bromide < 4.37 4.37 2Vinyl Chloride < 12.8 12.8 24-bromofluorobenzene (surrogate) 101%Analysis Date/Time: 11-19-14/06:58Analyst Initials tjg
EnvisionAir 1441 Sadlier Circle West Drive
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Reference 67 Page 78
Client Name: KERR ENVIRONMENTAL
Project ID: CVS
Client Project Manager: DANA KERR
EnvisionAir Project Number: 2014-517
Analytical Method: TO-15 Analytical Batch: 111814TAIR
Client Sample ID: SS-4 Sample Collection START Date/Time: 11/13/14 15:56Sample Received Date/Time: 11/14/14 15:55
Envision Sample Number: 14-2003Sample Matrix: AIR
Compounds Sample Results ug/m³ Reporting Limit ug/m³ Flag 4-Ethyltoluene < 4920 4920 2 4-Methyl-2-pentanone (MIBK) < 20500 20500 21,1,1-Trichloroethane < 5460 5460 21,1,2,2-Tetrachloroethane < 3.36 3.36 1,21,1,2-Trichloroethane < 2.10 2.10 1,21,1-Dichloroethane < 40.5 40.5 21,1-Dichloroethene < 1980 1980 21,1-Dichloropropene < 454 454 21,2,4-Trichlorobenzene < 7.42 7.42 21,2,4-Trimethylbenzene < 49.2 49.2 21,2-dibromoethane (EDB) < 0.32 0.32 1,21,2-Dichlorobenzene < 601 601 21,2-Dichloroethane < 4.05 4.05 21,2-Dichloropropane < 4.62 4.62 21,3,5-Trimethylbenzene < 49.2 49.2 21,3-Butadiene < 2.21 2.21 21,3-Dichlorobenzene < 601 601 21,4-Dichlorobenzene < 6.01 6.01 21,4-Dioxane < 18.0 18.0 22-Butanone (MEK) < 29500 29500 22-Hexanone < 205 205 2Acetone < 23800 23800 2Benzene 21.4 16.0 2Benzyl Chloride < 4.14 4.14 1,2Bromodichloromethane < 5.36 5.36 1,2Bromoform < 103 103 2Bromomethane < 38.8 38.8 2Carbon Disulfide < 3110 3110 2Carbon Tetrachloride < 6.29 6.29 2Chlorobenzene < 230 230 2Chloroethane < 132 132 2
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Reference 67 Page 79
Compounds Sample Results ug/m³ Reporting Limit ug/m³ FlagChloroform < 8.30 8.30 2Chloromethane < 206 206 2cis-1,2-Dichloroethene < 198 198 2cis-1,3-Dichloropropene < 45.4 45.4 2Cyclohexane < 55100 55100 2Dibromochloromethane < 8.52 8.52 2Dichlorodifluoromethane < 495 495 2Ethyl Acetate < 18000 18000 2Ethylbenzene < 86.8 86.8 2Hexachloro-1,3-butadiene < 10.7 10.7 2Isooctane < 4670 4670 2m,p-Xylene < 434 434 2Methylene Chloride < 417 417 2Methyl-tert-butyl ether < 361 361 2N-Heptane < 4100 4100 2N-Hexane < 1760 1760 2o-Xylene < 434 434 2Propylene < 1720 1720 2Styrene < 4260 4260 2Tetrachloroethene < 31.9 31.9 2Tetrahydrofuran < 2950 2950 2Toluene < 37700 37700 2trans-1,2-Dichloroethene < 396 396 2trans-1,3-Dichloropropene < 45.4 45.4 2Trichlorethene < 10.7 10.7 2Trichlorofluoromethane < 5620 5620 2Vinyl Acetate < 1760 1760 2Vinyl Bromide < 4.37 4.37 2Vinyl Chloride < 12.8 12.8 24-bromofluorobenzene (surrogate) 98%Analysis Date/Time: 11-19-14/07:33Analyst Initials tjg
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Reference 67 Page 80
Client Name: KERR ENVIRONMENTAL
Project ID: CVS
Client Project Manager: DANA KERR
EnvisionAir Project Number: 2014-517
Analytical Method: TO-15 Analytical Batch: 111814TAIR
Client Sample ID: SS-5 Sample Collection START Date/Time: 11/13/14 16:05Sample Received Date/Time: 11/14/14 15:55
Envision Sample Number: 14-2004Sample Matrix: AIR
Compounds Sample Results ug/m³ Reporting Limit ug/m³ Flag 4-Ethyltoluene < 4920 4920 2 4-Methyl-2-pentanone (MIBK) < 20500 20500 21,1,1-Trichloroethane < 5460 5460 21,1,2,2-Tetrachloroethane < 3.36 3.36 1,21,1,2-Trichloroethane < 2.10 2.10 1,21,1-Dichloroethane < 40.5 40.5 21,1-Dichloroethene < 1980 1980 21,1-Dichloropropene < 454 454 21,2,4-Trichlorobenzene < 7.42 7.42 21,2,4-Trimethylbenzene < 49.2 49.2 21,2-dibromoethane (EDB) < 0.32 0.32 1,21,2-Dichlorobenzene < 601 601 21,2-Dichloroethane < 4.05 4.05 21,2-Dichloropropane < 4.62 4.62 21,3,5-Trimethylbenzene < 49.2 49.2 21,3-Butadiene < 2.21 2.21 21,3-Dichlorobenzene < 601 601 21,4-Dichlorobenzene < 6.01 6.01 21,4-Dioxane < 18.0 18.0 22-Butanone (MEK) < 29500 29500 22-Hexanone < 205 205 2Acetone < 23800 23800 2Benzene 20.1 16.0 2Benzyl Chloride < 4.14 4.14 1,2Bromodichloromethane < 5.36 5.36 1,2Bromoform < 103 103 2Bromomethane < 38.8 38.8 2Carbon Disulfide < 3110 3110 2Carbon Tetrachloride < 6.29 6.29 2Chlorobenzene < 230 230 2Chloroethane < 132 132 2
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Reference 67 Page 81
Compounds Sample Results ug/m³ Reporting Limit ug/m³ FlagChloroform < 8.30 8.30 2Chloromethane < 206 206 2cis-1,2-Dichloroethene < 198 198 2cis-1,3-Dichloropropene < 45.4 45.4 2Cyclohexane < 55100 55100 2Dibromochloromethane < 8.52 8.52 2Dichlorodifluoromethane < 495 495 2Ethyl Acetate < 18000 18000 2Ethylbenzene < 86.8 86.8 2Hexachloro-1,3-butadiene < 10.7 10.7 2Isooctane < 4670 4670 2m,p-Xylene < 434 434 2Methylene Chloride < 417 417 2Methyl-tert-butyl ether < 361 361 2N-Heptane < 4100 4100 2N-Hexane < 1760 1760 2o-Xylene < 434 434 2Propylene < 1720 1720 2Styrene < 4260 4260 2Tetrachloroethene < 31.9 31.9 2Tetrahydrofuran < 2950 2950 2Toluene < 37700 37700 2trans-1,2-Dichloroethene < 396 396 2trans-1,3-Dichloropropene < 45.4 45.4 2Trichlorethene < 10.7 10.7 2Trichlorofluoromethane < 5620 5620 2Vinyl Acetate < 1760 1760 2Vinyl Bromide < 4.37 4.37 2Vinyl Chloride < 12.8 12.8 24-bromofluorobenzene (surrogate) 96%Analysis Date/Time: 11-19-14/08:08Analyst Initials tjg
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Reference 67 Page 82
Client Name: KERR ENVIRONMENTAL
Project ID: CVS
Client Project Manager: DANA KERR
EnvisionAir Project Number: 2014-517
Analytical Method: TO-15Analytical Batch: 111814TAIR
Client Sample ID: IA-1 Sample Collection START Date/Time: 11/13/14 15:02Sample Collection END Date/Time: 11/14/14 15:02
Envision Sample Number: 14-2005 Sample Received Date/Time: 11/14/14 15:55Sample Matrix: AIR
Compounds Sample Results ug/m³ Reporting Limit ug/m³ Flag 4-Ethyltoluene < 492 492 4-Methyl-2-pentanone (MIBK) < 2050 20501,1,1-Trichloroethane < 546 5461,1,2,2-Tetrachloroethane < 0.34 0.34 11,1,2-Trichloroethane < 0.21 0.21 11,1-Dichloroethane < 4.05 4.051,1-Dichloroethene < 198 1981,1-Dichloropropene < 45.4 45.41,2,4-Trichlorobenzene < 0.74 0.741,2,4-Trimethylbenzene < 4.92 4.921,2-dibromoethane (EDB) < 0.03 0.03 11,2-Dichlorobenzene < 60.1 60.11,2-Dichloroethane < 0.40 0.401,2-Dichloropropane < 0.46 0.461,3,5-Trimethylbenzene < 4.92 4.921,3-Butadiene < 0.22 0.221,3-Dichlorobenzene < 60.1 60.11,4-Dichlorobenzene < 0.60 0.601,4-Dioxane < 1.80 1.802-Butanone (MEK) < 2950 29502-Hexanone < 20.5 20.5Acetone < 2380 2380Benzene < 1.60 1.60Benzyl Chloride < 0.41 0.41 1Bromodichloromethane < 0.54 0.54 1Bromoform < 10.3 10.3Bromomethane < 3.88 3.88Carbon Disulfide < 311 311Carbon Tetrachloride < 0.63 0.63Chlorobenzene < 23.0 23.0Chloroethane < 13.2 13.2
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Reference 67 Page 83
Compounds Sample Results ug/m³ Reporting Limit ug/m³ FlagChloroform < 0.83 0.83Chloromethane < 20.6 20.6cis-1,2-Dichloroethene < 19.8 19.8cis-1,3-Dichloropropene < 4.54 4.54Cyclohexane < 5510 5510Dibromochloromethane < 0.85 0.85Dichlorodifluoromethane < 49.5 49.5Ethyl Acetate < 1800 1800Ethylbenzene < 8.68 8.68Hexachloro-1,3-butadiene < 1.07 1.07Isooctane < 467 467m,p-Xylene < 43.4 43.4Methylene Chloride < 41.7 41.7Methyl-tert-butyl ether < 36.1 36.1N-Heptane < 410 410N-Hexane < 176 176o-Xylene < 43.4 43.4Propylene < 172 172Styrene < 426 426Tetrachloroethene < 3.19 3.19Tetrahydrofuran < 295 295Toluene < 3770 3770trans-1,2-Dichloroethene < 39.6 39.6trans-1,3-Dichloropropene < 4.54 4.54Trichlorethene < 1.07 1.07Trichlorofluoromethane < 562 562Vinyl Acetate < 176 176Vinyl Bromide < 0.44 0.44Vinyl Chloride < 1.28 1.284-bromofluorobenzene (surrogate) 110%Analysis Date/Time: 11-19-14/15:01Analyst Initials tjg
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Reference 67 Page 84
Client Name: KERR ENVIRONMENTAL
Project ID: CVS
Client Project Manager: DANA KERR
EnvisionAir Project Number: 2014-517
Analytical Method: TO-15Analytical Batch: 111814TAIR
Client Sample ID: IA-2 Sample Collection START Date/Time: 11/13/14 15:03Sample Collection END Date/Time: 11/14/14 15:04
Envision Sample Number: 14-2006 Sample Received Date/Time: 11/14/14 15:55Sample Matrix: AIR
Compounds Sample Results ug/m³ Reporting Limit ug/m³ Flag 4-Ethyltoluene < 492 492 4-Methyl-2-pentanone (MIBK) < 2050 20501,1,1-Trichloroethane < 546 5461,1,2,2-Tetrachloroethane < 0.34 0.34 11,1,2-Trichloroethane < 0.21 0.21 11,1-Dichloroethane < 4.05 4.051,1-Dichloroethene < 198 1981,1-Dichloropropene < 45.4 45.41,2,4-Trichlorobenzene < 0.74 0.741,2,4-Trimethylbenzene < 4.92 4.921,2-dibromoethane (EDB) < 0.03 0.03 11,2-Dichlorobenzene < 60.1 60.11,2-Dichloroethane < 0.40 0.401,2-Dichloropropane < 0.46 0.461,3,5-Trimethylbenzene < 4.92 4.921,3-Butadiene < 0.22 0.221,3-Dichlorobenzene < 60.1 60.11,4-Dichlorobenzene < 0.60 0.601,4-Dioxane < 1.80 1.802-Butanone (MEK) < 2950 29502-Hexanone < 20.5 20.5Acetone < 2380 2380Benzene < 1.60 1.60Benzyl Chloride < 0.41 0.41 1Bromodichloromethane < 0.54 0.54 1Bromoform < 10.3 10.3Bromomethane < 3.88 3.88Carbon Disulfide < 311 311Carbon Tetrachloride < 0.63 0.63Chlorobenzene < 23.0 23.0Chloroethane < 13.2 13.2
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Reference 67 Page 85
Compounds Sample Results ug/m³ Reporting Limit ug/m³ FlagChloroform < 0.83 0.83Chloromethane < 20.6 20.6cis-1,2-Dichloroethene < 19.8 19.8cis-1,3-Dichloropropene < 4.54 4.54Cyclohexane < 5510 5510Dibromochloromethane < 0.85 0.85Dichlorodifluoromethane < 49.5 49.5Ethyl Acetate < 1800 1800Ethylbenzene < 8.68 8.68Hexachloro-1,3-butadiene < 1.07 1.07Isooctane < 467 467m,p-Xylene < 43.4 43.4Methylene Chloride < 41.7 41.7Methyl-tert-butyl ether < 36.1 36.1N-Heptane < 410 410N-Hexane < 176 176o-Xylene < 43.4 43.4Propylene < 172 172Styrene < 426 426Tetrachloroethene < 3.19 3.19Tetrahydrofuran < 295 295Toluene < 3770 3770trans-1,2-Dichloroethene < 39.6 39.6trans-1,3-Dichloropropene < 4.54 4.54Trichlorethene < 1.07 1.07Trichlorofluoromethane < 562 562Vinyl Acetate < 176 176Vinyl Bromide < 0.44 0.44Vinyl Chloride < 1.28 1.284-bromofluorobenzene (surrogate) 112%Analysis Date/Time: 11-19-14/15:35Analyst Initials tjg
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Reference 67 Page 86
Client Name: KERR ENVIRONMENTAL
Project ID: CVS
Client Project Manager: DANA KERR
EnvisionAir Project Number: 2014-517
Analytical Method: TO-15Analytical Batch: 111814TAIR
Client Sample ID: IA-3 Sample Collection START Date/Time: 11/13/14 15:04Sample Collection END Date/Time: 11/14/14 15:06
Envision Sample Number: 14-2007 Sample Received Date/Time: 11/14/14 15:55Sample Matrix: AIR
Compounds Sample Results ug/m³ Reporting Limit ug/m³ Flag 4-Ethyltoluene < 492 492 4-Methyl-2-pentanone (MIBK) < 2050 20501,1,1-Trichloroethane < 546 5461,1,2,2-Tetrachloroethane < 0.34 0.34 11,1,2-Trichloroethane < 0.21 0.21 11,1-Dichloroethane < 4.05 4.051,1-Dichloroethene < 198 1981,1-Dichloropropene < 45.4 45.41,2,4-Trichlorobenzene < 0.74 0.741,2,4-Trimethylbenzene < 4.92 4.921,2-dibromoethane (EDB) < 0.03 0.03 11,2-Dichlorobenzene < 60.1 60.11,2-Dichloroethane < 0.40 0.401,2-Dichloropropane < 0.46 0.461,3,5-Trimethylbenzene < 4.92 4.921,3-Butadiene < 0.22 0.221,3-Dichlorobenzene < 60.1 60.11,4-Dichlorobenzene < 0.60 0.601,4-Dioxane < 1.80 1.802-Butanone (MEK) < 2950 29502-Hexanone < 20.5 20.5Acetone < 2380 2380Benzene < 1.60 1.60Benzyl Chloride < 0.41 0.41 1Bromodichloromethane < 0.54 0.54 1Bromoform < 10.3 10.3Bromomethane < 3.88 3.88Carbon Disulfide < 311 311Carbon Tetrachloride < 0.63 0.63Chlorobenzene < 23.0 23.0Chloroethane < 13.2 13.2
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Reference 67 Page 87
Compounds Sample Results ug/m³ Reporting Limit ug/m³ FlagChloroform < 0.83 0.83Chloromethane < 20.6 20.6cis-1,2-Dichloroethene < 19.8 19.8cis-1,3-Dichloropropene < 4.54 4.54Cyclohexane < 5510 5510Dibromochloromethane < 0.85 0.85Dichlorodifluoromethane < 49.5 49.5Ethyl Acetate < 1800 1800Ethylbenzene < 8.68 8.68Hexachloro-1,3-butadiene < 1.07 1.07Isooctane < 467 467m,p-Xylene < 43.4 43.4Methylene Chloride < 41.7 41.7Methyl-tert-butyl ether < 36.1 36.1N-Heptane < 410 410N-Hexane < 176 176o-Xylene < 43.4 43.4Propylene < 172 172Styrene < 426 426Tetrachloroethene < 3.19 3.19Tetrahydrofuran < 295 295Toluene < 3770 3770trans-1,2-Dichloroethene < 39.6 39.6trans-1,3-Dichloropropene < 4.54 4.54Trichlorethene < 1.07 1.07Trichlorofluoromethane < 562 562Vinyl Acetate < 176 176Vinyl Bromide < 0.44 0.44Vinyl Chloride < 1.28 1.284-bromofluorobenzene (surrogate) 115%Analysis Date/Time: 11-19-14/16:10Analyst Initials tjg
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Reference 67 Page 88
Client Name: KERR ENVIRONMENTAL
Project ID: CVS
Client Project Manager: DANA KERR
EnvisionAir Project Number: 2014-517
Analytical Method: TO-15Analytical Batch: 111814TAIR
Client Sample ID: IA-4 Sample Collection START Date/Time: 11/13/14 15:05Sample Collection END Date/Time: 11/14/14 15:08
Envision Sample Number: 14-2008 Sample Received Date/Time: 11/14/14 15:55Sample Matrix: AIR
Compounds Sample Results ug/m³ Reporting Limit ug/m³ Flag 4-Ethyltoluene < 492 492 4-Methyl-2-pentanone (MIBK) < 2050 20501,1,1-Trichloroethane < 546 5461,1,2,2-Tetrachloroethane < 0.34 0.34 11,1,2-Trichloroethane < 0.21 0.21 11,1-Dichloroethane < 4.05 4.051,1-Dichloroethene < 198 1981,1-Dichloropropene < 45.4 45.41,2,4-Trichlorobenzene < 0.74 0.741,2,4-Trimethylbenzene < 4.92 4.921,2-dibromoethane (EDB) < 0.03 0.03 11,2-Dichlorobenzene < 60.1 60.11,2-Dichloroethane < 0.40 0.401,2-Dichloropropane < 0.46 0.461,3,5-Trimethylbenzene < 4.92 4.921,3-Butadiene < 0.22 0.221,3-Dichlorobenzene < 60.1 60.11,4-Dichlorobenzene < 0.60 0.601,4-Dioxane < 1.80 1.802-Butanone (MEK) < 2950 29502-Hexanone < 20.5 20.5Acetone < 2380 2380Benzene 1.76 1.60Benzyl Chloride < 0.41 0.41 1Bromodichloromethane < 0.54 0.54 1Bromoform < 10.3 10.3Bromomethane < 3.88 3.88Carbon Disulfide < 311 311Carbon Tetrachloride < 0.63 0.63Chlorobenzene < 23.0 23.0Chloroethane < 13.2 13.2
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Reference 67 Page 89
Compounds Sample Results ug/m³ Reporting Limit ug/m³ FlagChloroform < 0.83 0.83Chloromethane < 20.6 20.6cis-1,2-Dichloroethene < 19.8 19.8cis-1,3-Dichloropropene < 4.54 4.54Cyclohexane < 5510 5510Dibromochloromethane < 0.85 0.85Dichlorodifluoromethane < 49.5 49.5Ethyl Acetate < 1800 1800Ethylbenzene < 8.68 8.68Hexachloro-1,3-butadiene < 1.07 1.07Isooctane < 467 467m,p-Xylene < 43.4 43.4Methylene Chloride < 41.7 41.7Methyl-tert-butyl ether < 36.1 36.1N-Heptane < 410 410N-Hexane < 176 176o-Xylene < 43.4 43.4Propylene < 172 172Styrene < 426 426Tetrachloroethene < 3.19 3.19Tetrahydrofuran < 295 295Toluene < 3770 3770trans-1,2-Dichloroethene < 39.6 39.6trans-1,3-Dichloropropene < 4.54 4.54Trichlorethene < 1.07 1.07Trichlorofluoromethane < 562 562Vinyl Acetate < 176 176Vinyl Bromide < 0.44 0.44Vinyl Chloride < 1.28 1.284-bromofluorobenzene (surrogate) 114%Analysis Date/Time: 11-19-14/16:44Analyst Initials tjg
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Reference 67 Page 90
Client Name: KERR ENVIRONMENTAL
Project ID: CVS
Client Project Manager: DANA KERR
EnvisionAir Project Number: 2014-517
Analytical Method: TO-15Analytical Batch: 111814TAIR
Client Sample ID: IA-5 Sample Collection START Date/Time: 11/13/14 15:06Sample Collection END Date/Time: 11/14/14 15:10
Envision Sample Number: 14-2009 Sample Received Date/Time: 11/14/14 15:55Sample Matrix: AIR
Compounds Sample Results ug/m³ Reporting Limit ug/m³ Flag 4-Ethyltoluene < 492 492 4-Methyl-2-pentanone (MIBK) < 2050 20501,1,1-Trichloroethane < 546 5461,1,2,2-Tetrachloroethane < 0.34 0.34 11,1,2-Trichloroethane < 0.21 0.21 11,1-Dichloroethane < 4.05 4.051,1-Dichloroethene < 198 1981,1-Dichloropropene < 45.4 45.41,2,4-Trichlorobenzene < 0.74 0.741,2,4-Trimethylbenzene < 4.92 4.921,2-dibromoethane (EDB) < 0.03 0.03 11,2-Dichlorobenzene < 60.1 60.11,2-Dichloroethane < 0.40 0.401,2-Dichloropropane < 0.46 0.461,3,5-Trimethylbenzene < 4.92 4.921,3-Butadiene < 0.22 0.221,3-Dichlorobenzene < 60.1 60.11,4-Dichlorobenzene < 0.60 0.601,4-Dioxane < 1.80 1.802-Butanone (MEK) < 2950 29502-Hexanone < 20.5 20.5Acetone < 2380 2380Benzene < 1.60 1.60Benzyl Chloride < 0.41 0.41 1Bromodichloromethane < 0.54 0.54 1Bromoform < 10.3 10.3Bromomethane < 3.88 3.88Carbon Disulfide < 311 311Carbon Tetrachloride < 0.63 0.63Chlorobenzene < 23.0 23.0Chloroethane < 13.2 13.2
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Reference 67 Page 91
Compounds Sample Results ug/m³ Reporting Limit ug/m³ FlagChloroform < 0.83 0.83Chloromethane < 20.6 20.6cis-1,2-Dichloroethene < 19.8 19.8cis-1,3-Dichloropropene < 4.54 4.54Cyclohexane < 5510 5510Dibromochloromethane < 0.85 0.85Dichlorodifluoromethane < 49.5 49.5Ethyl Acetate < 1800 1800Ethylbenzene < 8.68 8.68Hexachloro-1,3-butadiene < 1.07 1.07Isooctane < 467 467m,p-Xylene < 43.4 43.4Methylene Chloride < 41.7 41.7Methyl-tert-butyl ether < 36.1 36.1N-Heptane < 410 410N-Hexane < 176 176o-Xylene < 43.4 43.4Propylene < 172 172Styrene < 426 426Tetrachloroethene < 3.19 3.19Tetrahydrofuran < 295 295Toluene < 3770 3770trans-1,2-Dichloroethene < 39.6 39.6trans-1,3-Dichloropropene < 4.54 4.54Trichlorethene < 1.07 1.07Trichlorofluoromethane < 562 562Vinyl Acetate < 176 176Vinyl Bromide < 0.44 0.44Vinyl Chloride < 1.28 1.284-bromofluorobenzene (surrogate) 113%Analysis Date/Time: 11-19-14/17:19Analyst Initials tjg
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Reference 67 Page 92
Analytical Report
TO-15 Quality Control Data
EnvisionAir Batch Number: 111814TAIR
Method Blank (MB): MB Results (ppbv) Reporting Limit (ppbv) Flags 4-Ethyltoluene < 100 100 4-Methyl-2-pentanone (MIBK) < 500 5001,1,1-Trichloroethane < 100 1001,1,2,2-Tetrachloroethane < 0.049 0.049 11,1,2-Trichloroethane < 0.038 0.038 11,1-Dichloroethane < 1 11,1-Dichloroethene < 50 501,1-Dichloropropene < 10 101,2,4-Trichlorobenzene < 0.1 0.11,2,4-Trimethylbenzene < 1 11,2-dibromoethane (EDB) < 0.0041 0.0041 11,2-Dichlorobenzene < 10 101,2-Dichloroethane < 0.1 0.11,2-Dichloropropane < 0.1 0.11,3,5-Trimethylbenzene < 1 11,3-Butadiene < 0.1 0.11,3-Dichlorobenzene < 10 101,4-Dichlorobenzene < 0.1 0.11,4-Dioxane < 0.5 0.52-Butanone (MEK) < 1000 10002-Hexanone < 5 5Acetone < 1000 1000Benzene < 0.5 0.5Benzyl Chloride < 0.08 0.08 1Bromodichloromethane < 0.08 0.08 1Bromoform < 1 1Bromomethane < 1 1Carbon Disulfide < 100 100Carbon Tetrachloride < 0.1 0.1Chlorobenzene < 5 5Chloroethane < 5 5Chloroform < 0.17 0.17Chloromethane < 10 10cis-1,2-Dichloroethene < 5 5cis-1,3-Dichloropropene < 1 1Cyclohexane < 1600 1600Dibromochloromethane < 0.1 0.1Dichlorodifluoromethane < 10 10Ethyl Acetate < 500 500Ethylbenzene < 2 2Hexachloro-1,3-butadiene < 0.1 0.1Isooctane < 100 100m,p-Xylene < 10 10Methylene Chloride < 12 12Methyl-tert-butyl ether < 10 10N-Heptane < 100 100N-Hexane < 50 50o-Xylene < 10 10Propylene < 100 100Styrene < 100 100Tetrachloroethene < 0.47 0.47Tetrahydrofuran < 100 100
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Reference 67 Page 93
Analytical Report
Method Blank (MB): MB Results (ppbv) Reporting Limit (ppbv) FlagsToluene < 1000 1000trans-1,2-Dichloroethene < 10 10trans-1,3-Dichloropropene < 1 1Trichlorethene < 0.2 0.2Trichlorofluoromethane < 100 100Vinyl Acetate < 50 50Vinyl Bromide < 0.1 0.1Vinyl Chloride < 0.5 0.54-bromofluorobenzene (surrogate) 96%Analysis Date/Time: 11-18-14/23:25Analyst Initials tjg
LCS/LCSD LCS Results (ppbv) LCSD Results (ppbv)LCS/D
Conc(ppbv)LCS Rec.
LCSD Rec. RPD Flag
Propylene 8.78 8.96 10 88% 90% 2.0%Dichlorodifluoromethane 9.58 9.16 10 96% 92% 4.5%Chloromethane 9.28 8.91 10 93% 89% 4.1%Vinyl Chloride 9.57 9.59 10 96% 96% 0.2%1,3-Butadiene 9.28 9.35 10 93% 94% 0.8%Bromomethane 9.86 9.63 10 99% 96% 2.4%Chloroethane 9.1 9.41 10 91% 94% 3.3%Vinyl Bromide 9.68 9.66 10 97% 97% 0.2%Trichlorofluoromethane 9.57 9.39 10 96% 94% 1.9%Acetone 9.97 10.3 10 100% 103% 3.3%1,1-Dichloroethene 10.4 10.6 10 104% 106% 1.9%Methylene Chloride 8.94 9.16 10 89% 92% 2.4%Carbon Disulfide 9.48 9.54 10 95% 95% 0.6%trans-1,2-Dichloroethene 10.8 10.8 10 108% 108% 0.0%Methyl-tert-butyl ether 8.93 9.24 10 89% 92% 3.4%1,1-Dichloroethane 9.82 9.7 10 98% 97% 1.2%Vinyl Acetate 11.1 11 10 111% 110% 0.9%N-Hexane 10.9 10.9 10 109% 109% 0.0%2-Butanone (MEK) 11.4 11.6 10 114% 116% 1.7%cis-1,2-Dichloroethene 10.7 10.8 10 107% 108% 0.9%Ethyl Acetate 11.4 11.5 10 114% 115% 0.9%Chloroform 9.77 9.7 10 98% 97% 0.7%Tetrahydrofuran 10.2 11.6 10 102% 116% 12.8%1,2-Dichloroethane 10.1 9.31 10 101% 93% 8.1%1,1,1-Trichloroethane 10 9.35 10 100% 94% 6.7%1,1-Dichloropropene 11 10.3 10 110% 103% 6.6%Carbon Tetrachloride 9.41 8.71 10 94% 87% 7.7%Benzene 11.4 10.4 10 114% 104% 9.2%Cyclohexane 11.9 10.9 10 119% 109% 8.8%1,2-Dichloropropane 10.4 9.88 10 104% 99% 5.1%Trichlorethene 10.8 10.1 10 108% 101% 6.7%Bromodichloromethane 10.3 9.66 10 103% 97% 6.4%1,4-Dioxane 11.5 10.7 10 115% 107% 7.2%Isooctane 10.9 10.1 10 109% 101% 7.6%N-Heptane 10.7 10.2 10 107% 102% 4.8%cis-1,3-Dichloropropene 11.5 10.8 10 115% 108% 6.3% 4-Methyl-2-pentanone (MIBK) 10.6 9.74 10 106% 97% 8.5%trans-1,3-Dichloropropene 11.9 10.9 10 119% 109% 8.8%1,1,2-Trichloroethane 9.8 9.2 10 98% 92% 6.3%Toluene 10.4 11.1 10 104% 111% 6.5%2-Hexanone 10.8 10.5 10 108% 105% 2.8%Dibromochloromethane 9.5 9.33 10 95% 93% 1.8%1,2-dibromoethane (EDB) 10.1 9.62 10 101% 96% 4.9%Tetrachloroethene 10.5 9.78 10 105% 98% 7.1%Chlorobenzene 9.29 9.11 10 93% 91% 2.0%Ethylbenzene 11.9 11 10 119% 110% 7.9%m,p-Xylene 21.8 21.5 20 109% 108% 1.4%Bromoform 10.2 9.99 10 102% 100% 2.1%
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Reference 67 Page 94
Analytical Report
LCS/LCSD LCS Results (ppbv) LCSD Results (ppbv)LCS/D
Conc(ppbv)LCS Rec.
LCSD Rec. RPD Flag
Styrene 11.3 11.3 10 113% 113% 0.0%1,1,2,2-Tetrachloroethane 9.43 9.29 10 94% 93% 1.5%o-Xylene 9.72 9.59 10 97% 96% 1.3% 4-Ethyltoluene 10.7 11.9 10 107% 119% 10.6%1,3,5-Trimethylbenzene 11 10.7 10 110% 107% 2.8%1,2,4-Trimethylbenzene 11.3 10.8 10 113% 108% 4.5%1,3-Dichlorobenzene 10.6 10.4 10 106% 104% 1.9%Benzyl Chloride 11 10.7 10 110% 107% 2.8%1,4-Dichlorobenzene 10.7 10.4 10 107% 104% 2.8%1,2-Dichlorobenzene 9.06 8.81 10 91% 88% 2.8%1,2,4-Trichlorobenzene 8.96 8.48 10 90% 85% 5.5%Hexachloro-1,3-butadiene 8.5 8.57 10 85% 86% 0.8%4-bromofluorobenzene (surrogate) 92% 88%Analysis Date/Time: 11-18-14/21:37 11-18-14/22:15Analyst Initials tjg tjg
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Reference 67 Page 95
Flag Number Comments1 Reporting limit is supported by MDL. TJG2 Reported value is from a 10x dilution. TJG 11-21-14
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Reference 67 Page 96
Reference 67 Page 97
Reference 67 Page 98