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Method: METALES ENVI Page 1 Date: 28/12/2015 02:22:11 p.m.

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Reprocessing BegunLogged In Analyst: Administrator Technique: ICP Continuous

Results Data Set (original): validacion STD 90%Results Library (original): C:\Users\Public\PerkinElmer\ICP\Data\Results\Results.mdbResults Data Set (reprocessed):Results Library (reprocessed):

====================================================================================================Method LoadedMethod Name: METALES ENVI Method Last Saved: 28/12/2015 10:33:41 a.m.IEC File: MSF File:Method Description: Metales en Aguas Completo

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Sequence No.: 1 Autosampler Location: 14Sample ID: Blanco de Calibracion Date Collected: 28/12/2015 09:52:29 a.m.Analyst: Data Type: Reprocessed on 28/12/2015 02:21:32 p.m.Logged In Analyst (Original) : AdministratorInitial Sample Wt: Initial Sample Vol:Dilution: Sample Prep Vol:Wash Time:

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Mean Data: Blanco de CalibracionMean Corrected Calib

Analyte Intensity Std.Dev. RSD Conc. UnitsMn 257.610 39.6 7.33 18.53% [0.00] mg/L

Be 313.107 -2015.0 15.59 0.77% [0.00] mg/L

Cd 228.802 147.0 2.53 1.72% [0.00] mg/L

Pb 220.353 -137.3 17.97 13.09% [0.00] mg/L

Se 196.026 -47.7 10.94 22.93% [0.00] mg/L

Zn 206.200 -14.7 11.31 76.89% [0.00] mg/L

Ba 233.527 -78.3 8.43 10.77% [0.00] mg/L

Cu 327.393 1628.0 56.64 3.48% [0.00] mg/L

Fe 238.204 -62.1 26.06 41.99% [0.00] mg/L

V 290.880 95.3 17.25 18.10% [0.00] mg/L

Co 228.616 -92.4 1.99 2.15% [0.00] mg/LAs 188.979 -31.3 6.01 19.21% [0.00] mg/L

Mo 202.031 137.6 4.59 3.34% [0.00] mg/L

Sr 407.771 272.9 36.91 13.52% [0.00] mg/L

Li 670.784 1026.7 226.38 22.05% [0.00] mg/L

Sn 189.927 32.7 13.04 39.94% [0.00] mg/L

Ti 334.940 188.6 15.14 8.03% [0.00] mg/L

Ca 317.933 101.0 10.58 10.47% [0.00] mg/L

Na 589.592 922.2 97.62 10.59% [0.00] mg/L

K 766.490 1308.4 36.78 2.81% [0.00] mg/L

Cr 267.716 275.8 14.28 5.18% [0.00] mg/L

Ni 231.604 1026.8 40.52 3.95% [0.00] mg/L

Al 396.153 161.4 7.58 4.70% [0.00] mg/L

Mg 285.213 -50.0 28.63 57.28% [0.00] mg/L

Ag 328.068 -1807.9 102.06 5.65% [0.00] mg/L

B 249.677 48290.7 142.39 0.29% [0.00] mg/LSb 206.836 30.8 3.36 10.91% [0.00] mg/L

Tl 190.801 -76.7 14.26 18.59% [0.00] mg/L

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Sequence No.: 2 Autosampler Location: 15Sample ID: MIX 1-1 Date Collected: 28/12/2015 09:54:32 a.m.Analyst: Data Type: Reprocessed on 28/12/2015 02:21:32 p.m.Logged In Analyst (Original) : AdministratorInitial Sample Wt: Initial Sample Vol:Dilution: Sample Prep Vol:Wash Time:

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Mean Data: MIX 1-1Mean Corrected CalibAnalyte Intensity Std.Dev. RSD Conc. UnitsMn 257.610 3536.8 17.99 0.51% [0.05] mg/L

Be 313.107 20886.4 197.86 0.95% [0.05] mg/L

Cd 228.802 1625.2 16.85 1.04% [0.05] mg/L

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Pb 220.353 285.8 24.74 8.66% [0.05] mg/L

Se 196.026 82.6 13.33 16.14% [0.05] mg/L

Zn 206.200 289.8 21.70 7.49% [0.05] mg/L

Ag 328.068 8846.8 42.88 0.48% [0.05] mg/L

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Sequence No.: 3 Autosampler Location: 16Sample ID: MIX 1-2 Date Collected: 28/12/2015 09:56:44 a.m.Analyst: Data Type: Reprocessed on 28/12/2015 02:21:32 p.m.Logged In Analyst (Original) : Administrator

Initial Sample Wt: Initial Sample Vol:Dilution: Sample Prep Vol:Wash Time:

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Mean Data: MIX 1-2Mean Corrected Calib

Analyte Intensity Std.Dev. RSD Conc. UnitsMn 257.610 6886.1 26.35 0.38% [0.1] mg/L

Be 313.107 40957.0 342.32 0.84% [0.1] mg/L

Cd 228.802 3118.4 24.45 0.78% [0.1] mg/L

Pb 220.353 557.7 19.59 3.51% [0.1] mg/L

Se 196.026 127.8 15.88 12.43% [0.1] mg/L

Zn 206.200 522.2 11.75 2.25% [0.1] mg/L

Ag 328.068 44457.7 113.80 0.26% [0.25] mg/L

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Analyte Intensity Std.Dev. RSD Conc. Units

Mn 257.610 68571.5 243.15 0.35% [1] mg/LBe 313.107 417243.0 2259.96 0.54% [1] mg/L

Cd 228.802 31259.2 117.07 0.37% [1] mg/L

Pb 220.353 5800.6 56.77 0.98% [1] mg/L

Se 196.026 1353.5 9.52 0.70% [1] mg/L

Zn 206.200 5238.9 30.20 0.58% [1] mg/L

Ag 328.068 180166.6 798.42 0.44% [1] mg/L

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Sequence No.: 5 Autosampler Location: 18Sample ID: MIX 1-4 Date Collected: 28/12/2015 10:00:49 a.m.Analyst: Data Type: Reprocessed on 28/12/2015 02:21:33 p.m.Logged In Analyst (Original) : AdministratorInitial Sample Wt: Initial Sample Vol:Dilution: Sample Prep Vol:

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Analyte Intensity Std.Dev. RSD Conc. UnitsMn 257.610 333956.3 412.19 0.12% [5] mg/L

Be 313.107 2109629.5 18073.96 0.86% [5] mg/L

Cd 228.802 154788.1 1094.73 0.71% [5] mg/L

Pb 220.353 29041.8 139.49 0.48% [5] mg/L

Se 196.026 6920.3 16.53 0.24% [5] mg/L

Zn 206.200 25940.6 117.39 0.45% [5] mg/L

Ag 328.068 353581.4 2473.64 0.70% [2] mg/L

====================================================================================================Sequence No.: 6 Autosampler Location: 19Sample ID: MIX 2-1 Date Collected: 28/12/2015 10:02:44 a.m.Analyst: Data Type: Reprocessed on 28/12/2015 02:21:33 p.m.Logged In Analyst (Original) : AdministratorInitial Sample Wt: Initial Sample Vol:

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Dilution: Sample Prep Vol:Wash Time:

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Analyte Intensity Std.Dev. RSD Conc. UnitsBa 233.527 437.7 12.81 2.93% [0.05] mg/L

Cu 327.393 6725.6 65.05 0.97% [0.05] mg/L

Fe 238.204 769.6 12.39 1.61% [0.1] mg/L

V 290.880 586.4 9.50 1.62% [0.05] mg/LCo 228.616 1247.9 16.83 1.35% [0.05] mg/L

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Analyte Intensity Std.Dev. RSD Conc. UnitsBa 233.527 8333.5 42.08 0.50% [1] mg/L

Cu 327.393 133444.9 225.03 0.17% [1] mg/L

Fe 238.204 13907.5 133.58 0.96% [2] mg/L

V 290.880 12104.9 82.22 0.68% [1] mg/L

Co 228.616 24588.3 120.66 0.49% [1] mg/L

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Sequence No.: 8 Autosampler Location: 21Sample ID: MIX 2-3 Date Collected: 28/12/2015 10:06:02 a.m.Analyst: Data Type: Reprocessed on 28/12/2015 02:21:33 p.m.Logged In Analyst (Original) : AdministratorInitial Sample Wt: Initial Sample Vol:Dilution: Sample Prep Vol:

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Analyte Intensity Std.Dev. RSD Conc. UnitsBa 233.527 21302.7 12.12 0.06% [2.5] mg/L

Cu 327.393 331773.7 1474.34 0.44% [2.5] mg/L

Fe 238.204 35239.9 97.44 0.28% [5] mg/L

V 290.880 31110.7 82.51 0.27% [2.5] mg/L

Co 228.616 61242.6 336.30 0.55% [2.5] mg/L

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Sequence No.: 9 Autosampler Location: 22Sample ID: MIX 2-4 Date Collected: 28/12/2015 10:07:31 a.m.

Analyst: Data Type: Reprocessed on 28/12/2015 02:21:33 p.m.Logged In Analyst (Original) : AdministratorInitial Sample Wt: Initial Sample Vol:Dilution: Sample Prep Vol:Wash Time:

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Analyte Intensity Std.Dev. RSD Conc. UnitsBa 233.527 42145.4 398.26 0.94% [5] mg/L

Cu 327.393 654260.9 7428.34 1.14% [5] mg/L

Fe 238.204 69401.4 757.03 1.09% [10] mg/L

V 290.880 61436.9 743.69 1.21% [5] mg/L

Co 228.616 121211.5 1559.62 1.29% [5] mg/L

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Sequence No.: 10 Autosampler Location: 23Sample ID: MIX 3-1 Date Collected: 28/12/2015 10:09:01 a.m.Analyst: Data Type: Reprocessed on 28/12/2015 02:21:33 p.m.

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Analyte Intensity Std.Dev. RSD Conc. UnitsAs 188.979 63.8 5.97 9.36% [0.05] mg/L

Mo 202.031 676.0 5.49 0.81% [0.05] mg/LSr 407.771 108698.1 692.80 0.64% [0.05] mg/L

Li 670.784 7274.5 98.40 1.35% [0.05] mg/L

Sn 189.927 268.3 19.47 7.26% [0.05] mg/L

Ti 334.940 4295.9 56.88 1.32% [0.05] mg/L

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Analyte Intensity Std.Dev. RSD Conc. UnitsAs 188.979 1117.9 4.44 0.40% [1] mg/L

Mo 202.031 13138.9 92.48 0.70% [1] mg/L

Sr 407.771 2140432.6 10858.89 0.51% [1] mg/L

Li 670.784 143329.2 1174.13 0.82% [1] mg/L

Sn 189.927 5274.3 34.77 0.66% [1] mg/L

Ti 334.940 82538.0 686.98 0.83% [1] mg/L

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Analyte Intensity Std.Dev. RSD Conc. UnitsAs 188.979 2774.5 31.23 1.13% [2.5] mg/L

Mo 202.031 32139.8 179.90 0.56% [2.5] mg/L

Sr 407.771 5319704.8 7627.14 0.14% [2.5] mg/L

Li 670.784 353821.8 2497.01 0.71% [2.5] mg/L

Sn 189.927 13156.4 64.14 0.49% [2.5] mg/L

Ti 334.940 202000.6 1364.07 0.68% [2.5] mg/L

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Analyte Intensity Std.Dev. RSD Conc. UnitsAs 188.979 5606.8 47.35 0.84% [5] mg/LMo 202.031 64300.9 303.21 0.47% [5] mg/L

Sr 407.771 10622714.9 46129.13 0.43% [5] mg/L

Li 670.784 703775.8 3161.99 0.45% [5] mg/L

Sn 189.927 26335.2 169.15 0.64% [5] mg/L

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Ti 334.940 409324.0 2184.97 0.53% [5] mg/L

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Analyte Intensity Std.Dev. RSD Conc. UnitsCa 317.933 15977.9 43.11 0.27% [0.5] mg/L

Na 589.592 20954.0 132.42 0.63% [0.5] mg/L

K 766.490 1832.3 177.87 9.71% [0.5] mg/L

Cr 267.716 82867.6 741.25 0.89% [0.1] mg/L

Ni 231.604 4068.1 78.07 1.92% [0.1] mg/L

Al 396.153 3893.2 98.64 2.53% [0.5] mg/L

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Analyte Intensity Std.Dev. RSD Conc. UnitsCa 317.933 67075.2 409.06 0.61% [2.5] mg/L

Na 589.592 39264.8 175.26 0.45% [2.5] mg/L

K 766.490 8532.6 29.40 0.34% [2.5] mg/L

Cr 267.716 203222.1 2504.96 1.23% [0.25] mg/L

Ni 231.604 9903.0 142.67 1.44% [0.25] mg/LAl 396.153 19454.6 126.18 0.65% [2.5] mg/L

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Analyte Intensity Std.Dev. RSD Conc. UnitsCa 317.933 258540.4 1830.41 0.71% [10] mg/L

Na 589.592 147910.7 1042.80 0.71% [10] mg/L

K 766.490 33367.6 242.80 0.73% [10] mg/L

Cr 267.716 792324.1 925.77 0.12% [1] mg/L

Ni 231.604 37716.3 175.74 0.47% [1] mg/L

Al 396.153 76782.3 488.96 0.64% [10] mg/L

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Sequence No.: 17 Autosampler Location: 30Sample ID: MIX 4-4 Date Collected: 28/12/2015 10:20:37 a.m.Analyst: Data Type: Reprocessed on 28/12/2015 02:21:34 p.m.Logged In Analyst (Original) : AdministratorInitial Sample Wt: Initial Sample Vol:


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Analyte Intensity Std.Dev. RSD Conc. UnitsCa 317.933 1265213.9 4533.76 0.36% [50] mg/L

Na 589.592 719957.8 1486.14 0.21% [50] mg/L

K 766.490 166625.2 415.55 0.25% [50] mg/L

Cr 267.716 3768004.3 26810.92 0.71% [5] mg/L

Ni 231.604 180261.0 514.51 0.29% [5] mg/L

Al 396.153 378741.0 1017.40 0.27% [50] mg/L

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Sequence No.: 18 Autosampler Location: 31

Sample ID: MIX 5-1 Date Collected: 28/12/2015 10:22:13 a.m.Analyst: Data Type: Reprocessed on 28/12/2015 02:21:34 p.m.Logged In Analyst (Original) : AdministratorInitial Sample Wt: Initial Sample Vol:Dilution: Sample Prep Vol:Wash Time:

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Analyte Intensity Std.Dev. RSD Conc. UnitsMg 285.213 13700.5 143.04 1.04% [0.5] mg/L

B 249.677 25758.5 675.23 2.62% [0.5] mg/L

Sb 206.836 247.5 18.86 7.62% [0.1] mg/L

Tl 190.801 208.5 7.88 3.78% [0.1] mg/L

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Analyte Intensity Std.Dev. RSD Conc. Units

Mg 285.213 59132.9 324.77 0.55% [2.5] mg/LB 249.677 110241.5 806.82 0.73% [2.5] mg/L

Sb 206.836 621.6 22.57 3.63% [0.25] mg/L

Tl 190.801 520.1 4.32 0.83% [0.25] mg/L

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Analyte Intensity Std.Dev. RSD Conc. UnitsMg 285.213 237193.1 1296.31 0.55% [10] mg/L

B 249.677 435713.1 1653.57 0.38% [10] mg/L

Sb 206.836 2534.8 15.18 0.60% [1] mg/L

Tl 190.801 2103.1 14.50 0.69% [1] mg/L

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Sequence No.: 21 Autosampler Location: 34Sample ID: MIX 5-4 Date Collected: 28/12/2015 10:27:25 a.m.Analyst: Data Type: Reprocessed on 28/12/2015 02:21:34 p.m.Logged In Analyst (Original) : AdministratorInitial Sample Wt: Initial Sample Vol:


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Analyte Intensity Std.Dev. RSD Conc. UnitsMg 285.213 1154214.0 11317.88 0.98% [50] mg/L

B 249.677 2080172.5 16211.21 0.78% [50] mg/L

Sb 206.836 12594.1 75.56 0.60% [5] mg/L

Tl 190.801 10154.8 65.06 0.64% [5] mg/L

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Calibration Summary

Analyte Stds. Equation Intercept Slope Curvature Corr. Coef. Reslope

Mn 257.610 4 Lin, Calc Int 495.3 66740 0.00000 0.999986Be 313.107 4 Lin, Calc Int -1407.1 422100 0.00000 0.999998

Cd 228.802 4 Lin, Calc Int 92.7 30950 0.00000 0.999998

Pb 220.353 4 Lin, Calc Int -9.3 5810 0.00000 1.000000

Se 196.026 4 Lin, Calc Int -5.8 1384 0.00000 0.999985

Zn 206.200 4 Lin, Calc Int 20.3 5185 0.00000 0.999998

Ba 233.527 4 Lin, Calc Int 8.5 8442 0.00000 0.999978

Cu 327.393 4 Lin, Calc Int 1336.1 130900 0.00000 0.999972

Fe 238.204 4 Lin, Calc Int 101.1 6948 0.00000 0.999969

V 290.880 4 Lin, Calc Int -10.8 12310 0.00000 0.999969

Co 228.616 4 Lin, Calc Int 184.5 24250 0.00000 0.999985

As 188.979 4 Lin, Calc Int -1.7 1119 0.00000 0.999984

Mo 202.031 4 Lin, Calc Int 85.6 12850 0.00000 0.999990

Sr 407.771 4 Lin, Calc Int 6194.0 2124000 0.00000 0.999999

Li 670.784 4 Lin, Calc Int 1016.1 140700 0.00000 0.999992

Sn 189.927 4 Lin, Calc Int 2.3 5266 0.00000 1.000000

Ti 334.940 4 Lin, Calc Int -74.2 81700 0.00000 0.999973

Ca 317.933 4 Lin, Calc Int 3174.4 25250 0.00000 0.999992

Na 589.592 4 Lin, Calc Int 5645.1 14280 0.00000 0.999860

K 766.490 4 Lin, Calc Int 110.8 3330 0.00000 0.999999

Cr 267.716 4 Lin, Calc Int 14633.6 751700 0.00000 0.999953

Ni 231.604 4 Lin, Calc Int 737.3 35950 0.00000 0.999962

Al 396.153 4 Lin, Calc Int 395.4 7570 0.00000 0.999996

Mg 285.213 4 Lin, Calc Int 2382.3 23050 0.00000 0.999987

Ag 328.068 4 Lin, Calc Int 491.6 177100 0.00000 0.999953

B 249.677 4 Lin, Calc Int 7383.8 41510 0.00000 0.999961

Sb 206.836 4 Lin, Calc Int 0.1 2519 0.00000 0.999999

Tl 190.801 4 Lin, Calc Int 20.7 2029 0.00000 0.999975

====================================================================================================Sequence No.: 22 Autosampler Location: 35Sample ID: Blanco Reactivo Date Collected: 28/12/2015 10:33:48 a.m.Analyst: Data Type: Reprocessed on 28/12/2015 02:21:34 p.m.Logged In Analyst (Original) : AdministratorInitial Sample Wt: Initial Sample Vol:Dilution: Sample Prep Vol:Wash Time:

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Mean Data: Blanco ReactivoMean Corrected Calib. Sample

Analyte Intensity Conc. Units Std.Dev. Conc. Units Std.Dev. RSDMn 257.610 -1.9 -0.007 mg/L 0.0003 -0.007 mg/L 0.0003 3.78%

Be 313.107 -11.4 0.003 mg/L 0.0001 0.003 mg/L 0.0001 4.52%

Cd 228.802 23.4 -0.002 mg/L 0.0001 -0.002 mg/L 0.0001 6.28%Pb 220.353 -36.1 -0.005 mg/L 0.0076 -0.005 mg/L 0.0076 166.03%

Se 196.026 12.8 0.013 mg/L 0.0150 0.013 mg/L 0.0150 111.90%

Zn 206.200 2.0 -0.004 mg/L 0.0002 -0.004 mg/L 0.0002 5.83%

Ba 233.527 -5.4 -0.002 mg/L 0.0021 -0.002 mg/L 0.0021 125.95%

Cu 327.393 -91.3 -0.011 mg/L 0.0004 -0.011 mg/L 0.0004 3.26%

Fe 238.204 2.8 -0.014 mg/L 0.0009 -0.014 mg/L 0.0009 6.36%

V 290.880 -24.2 -0.001 mg/L 0.0026 -0.001 mg/L 0.0026 236.08%

Co 228.616 -8.8 -0.008 mg/L 0.0005 -0.008 mg/L 0.0005 6.61%

As 188.979 3.1 0.004 mg/L 0.0080 0.004 mg/L 0.0080 188.95%

Mo 202.031 -7.1 -0.007 mg/L 0.0007 -0.007 mg/L 0.0007 9.45%

Sr 407.771 -81.1 -0.003 mg/L 0.0000 -0.003 mg/L 0.0000 0.77%

Li 670.784 -228.9 -0.009 mg/L 0.0009 -0.009 mg/L 0.0009 10.26%

Sn 189.927 3.0 0.000 mg/L 0.0008 0.000 mg/L 0.0008 659.06%

Ti 334.940 43.8 0.001 mg/L 0.0004 0.001 mg/L 0.0004 29.80%Ca 317.933 -8.1 -0.126 mg/L 0.0003 -0.126 mg/L 0.0003 0.20%

Na 589.592 -156.3 -0.406 mg/L 0.0095 -0.406 mg/L 0.0095 2.33%

K 766.490 -112.1 -0.067 mg/L 0.0058 -0.067 mg/L 0.0058 8.64%

Cr 267.716 -10.1 -0.019 mg/L 0.0000 -0.019 mg/L 0.0000 0.14%

Ni 231.604 1.8 -0.020 mg/L 0.0005 -0.020 mg/L 0.0005 2.33%

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Al 396.153 -101.7 -0.066 mg/L 0.0108 -0.066 mg/L 0.0108 16.48%

Mg 285.213 34.2 -0.102 mg/L 0.0001 -0.102 mg/L 0.0001 0.13%

Ag 328.068 37.4 -0.003 mg/L 0.0001 -0.003 mg/L 0.0001 4.06%

B 249.677 -10507.8 -0.431 mg/L 0.0062 -0.431 mg/L 0.0062 1.43%

Sb 206.836 0.4 0.000 mg/L 0.0033 0.000 mg/L 0.0033 >999.9%

Tl 190.801 5.1 -0.008 mg/L 0.0027 -0.008 mg/L 0.0027 35.24%

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Sequence No.: 23 Autosampler Location: 17Sample ID: QC 1-3 Date Collected: 28/12/2015 10:36:05 a.m.


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Mean Data: QC 1-3Mean Corrected Calib. Sample

Analyte Intensity Conc. Units Std.Dev. Conc. Units Std.Dev. RSDMn 257.610 68809.6 1.024 mg/L 0.0038 1.024 mg/L 0.0038 0.37%

QC value within limits for Mn 257.610 Recovery = 102.35%

Be 313.107 417718.0 0.993 mg/L 0.0018 0.993 mg/L 0.0018 0.18%

QC value within limits for Be 313.107 Recovery = 99.30%

Cd 228.802 31491.1 1.015 mg/L 0.0063 1.015 mg/L 0.0063 0.62%

QC value within limits for Cd 228.802 Recovery = 101.46%

Pb 220.353 5810.9 1.002 mg/L 0.0079 1.002 mg/L 0.0079 0.78%

QC value within limits for Pb 220.353 Recovery = 100.17%

Se 196.026 1351.8 0.981 mg/L 0.0111 0.981 mg/L 0.0111 1.13%

QC value within limits for Se 196.026 Recovery = 98.07%

Zn 206.200 5257.7 1.010 mg/L 0.0020 1.010 mg/L 0.0020 0.20%

QC value within limits for Zn 206.200 Recovery = 101.00%

Ba 233.527 -0.9 -0.001 mg/L 0.0008 -0.001 mg/L 0.0008 70.03%

Cu 327.393 110.9 -0.009 mg/L 0.0006 -0.009 mg/L 0.0006 6.47%

Fe 238.204 47.3 -0.008 mg/L 0.0006 -0.008 mg/L 0.0006 7.44%

V 290.880 -18.7 -0.001 mg/L 0.0010 -0.001 mg/L 0.0010 151.43%

Co 228.616 0.4 -0.008 mg/L 0.0009 -0.008 mg/L 0.0009 11.83%

As 188.979 4.0 0.005 mg/L 0.0037 0.005 mg/L 0.0037 72.03%

Mo 202.031 5.3 -0.006 mg/L 0.0010 -0.006 mg/L 0.0010 16.50%

Sr 407.771 264.3 -0.003 mg/L 0.0000 -0.003 mg/L 0.0000 1.05%Li 670.784 -248.5 -0.009 mg/L 0.0003 -0.009 mg/L 0.0003 3.73%

Sn 189.927 0.9 -0.000 mg/L 0.0018 -0.000 mg/L 0.0018 689.08%

Ti 334.940 61.8 0.002 mg/L 0.0004 0.002 mg/L 0.0004 24.58%

Ca 317.933 2293.4 -0.035 mg/L 0.0002 -0.035 mg/L 0.0002 0.47%

Na 589.592 3248.8 -0.168 mg/L 0.0087 -0.168 mg/L 0.0087 5.18%

K 766.490 434.8 0.097 mg/L 0.0100 0.097 mg/L 0.0100 10.27%

Cr 267.716 -28.4 -0.020 mg/L 0.0001 -0.020 mg/L 0.0001 0.33%

Ni 231.604 83.0 -0.018 mg/L 0.0006 -0.018 mg/L 0.0006 3.27%

Al 396.153 -11.7 -0.054 mg/L 0.0083 -0.054 mg/L 0.0083 15.38%

Mg 285.213 214.7 -0.094 mg/L 0.0007 -0.094 mg/L 0.0007 0.78%

Ag 328.068 180747.3 1.018 mg/L 0.0075 1.018 mg/L 0.0075 0.74%

QC value within limits for Ag 328.068 Recovery = 101.75%

B 249.677 1582.6 -0.140 mg/L 0.0102 -0.140 mg/L 0.0102 7.28%

Sb 206.836 12.1 0.005 mg/L 0.0090 0.005 mg/L 0.0090 188.68%

Tl 190.801 -13.3 -0.017 mg/L 0.0035 -0.017 mg/L 0.0035 20.69%All analyte(s) passed QC.

====================================================================================================

Sequence No.: 24 Autosampler Location: 21Sample ID: QC 2-3 Date Collected: 28/12/2015 10:38:03 a.m.Analyst: Data Type: Reprocessed on 28/12/2015 02:21:35 p.m.Logged In Analyst (Original) : AdministratorInitial Sample Wt: Initial Sample Vol:Dilution: Sample Prep Vol:Wash Time:

----------------------------------------------------------------------------------------------------

Mean Data: QC 2-3

Mean Corrected Calib. SampleAnalyte Intensity Conc. Units Std.Dev. Conc. Units Std.Dev. RSDMn 257.610 -16.0 -0.008 mg/L 0.0001 -0.008 mg/L 0.0001 0.73%

Be 313.107 -125.0 0.003 mg/L 0.0001 0.003 mg/L 0.0001 3.48%

Cd 228.802 -554.0 -0.021 mg/L 0.0003 -0.021 mg/L 0.0003 1.50%

Pb 220.353 -4.8 0.001 mg/L 0.0018 0.001 mg/L 0.0018 235.61%

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Se 196.026 -102.9 -0.070 mg/L 0.0106 -0.070 mg/L 0.0106 15.10%

Zn 206.200 24.0 0.001 mg/L 0.0013 0.001 mg/L 0.0013 182.84%

Ba 233.527 21001.5 2.487 mg/L 0.0081 2.487 mg/L 0.0081 0.33%

QC value within limits for Ba 233.527 Recovery = 99.47%

Cu 327.393 324907.0 2.471 mg/L 0.0031 2.471 mg/L 0.0031 0.13%

QC value within limits for Cu 327.393 Recovery = 98.85%

Fe 238.204 34628.3 4.969 mg/L 0.0170 4.969 mg/L 0.0170 0.34%

QC value within limits for Fe 238.204 Recovery = 99.39%

V 290.880 30724.8 2.496 mg/L 0.0034 2.496 mg/L 0.0034 0.14%

QC value within limits for V 290.880 Recovery = 99.83%

Co 228.616 60454.4 2.485 mg/L 0.0016 2.485 mg/L 0.0016 0.06% QC value within limits for Co 228.616 Recovery = 99.40%

As 188.979 -3.0 -0.001 mg/L 0.0069 -0.001 mg/L 0.0069 603.80%

Mo 202.031 6.9 -0.006 mg/L 0.0015 -0.006 mg/L 0.0015 25.20%

Sr 407.771 294.0 -0.003 mg/L 0.0000 -0.003 mg/L 0.0000 1.09%

Li 670.784 -314.5 -0.009 mg/L 0.0008 -0.009 mg/L 0.0008 8.64%

Sn 189.927 8.2 0.001 mg/L 0.0013 0.001 mg/L 0.0013 116.33%

Ti 334.940 61.1 0.002 mg/L 0.0002 0.002 mg/L 0.0002 11.51%

Ca 317.933 2291.4 -0.035 mg/L 0.0028 -0.035 mg/L 0.0028 8.01%

Na 589.592 2676.2 -0.208 mg/L 0.0041 -0.208 mg/L 0.0041 1.96%

K 766.490 285.6 0.052 mg/L 0.0505 0.052 mg/L 0.0505 96.21%

Cr 267.716 -355.1 -0.020 mg/L 0.0001 -0.020 mg/L 0.0001 0.54%

Ni 231.604 267.4 -0.013 mg/L 0.0004 -0.013 mg/L 0.0004 2.81%

Al 396.153 12.0 -0.051 mg/L 0.0106 -0.051 mg/L 0.0106 20.90%

Mg 285.213 5.6 -0.103 mg/L 0.0007 -0.103 mg/L 0.0007 0.72%

Ag 328.068 -6251.0 -0.038 mg/L 0.0001 -0.038 mg/L 0.0001 0.39%

B 249.677 2509.3 -0.117 mg/L 0.0019 -0.117 mg/L 0.0019 1.62%

Sb 206.836 -26.3 -0.010 mg/L 0.0018 -0.010 mg/L 0.0018 17.08%

Tl 190.801 -54.1 -0.037 mg/L 0.0009 -0.037 mg/L 0.0009 2.45%

All analyte(s) passed QC.

====================================================================================================


----------------------------------------------------------------------------------------------------


Analyte Intensity Conc. Units Std.Dev. Conc. Units Std.Dev. RSDMn 257.610 5.4 -0.007 mg/L 0.0002 -0.007 mg/L 0.0002 3.24%

Be 313.107 -1781.1 -0.001 mg/L 0.0001 -0.001 mg/L 0.0001 10.73%

Cd 228.802 2158.5 0.067 mg/L 0.0007 0.067 mg/L 0.0007 1.01%

Pb 220.353 -52.3 -0.007 mg/L 0.0054 -0.007 mg/L 0.0054 72.93%

Se 196.026 3.2 0.007 mg/L 0.0146 0.007 mg/L 0.0146 223.88%

Zn 206.200 13.3 -0.001 mg/L 0.0006 -0.001 mg/L 0.0006 44.77%

Ba 233.527 -85.8 -0.011 mg/L 0.0004 -0.011 mg/L 0.0004 4.01%

Cu 327.393 -1064.5 -0.018 mg/L 0.0005 -0.018 mg/L 0.0005 2.67%

Fe 238.204 113.8 0.002 mg/L 0.0010 0.002 mg/L 0.0010 53.19%

V 290.880 -1165.4 -0.094 mg/L 0.0013 -0.094 mg/L 0.0013 1.35%

Co 228.616 11.7 -0.007 mg/L 0.0008 -0.007 mg/L 0.0008 10.90%As 188.979 2764.6 2.471 mg/L 0.0294 2.471 mg/L 0.0294 1.19%

QC value within limits for As 188.979 Recovery = 98.84%

Mo 202.031 32341.4 2.511 mg/L 0.0063 2.511 mg/L 0.0063 0.25%

QC value within limits for Mo 202.031 Recovery = 100.44%

Sr 407.771 5287023.5 2.486 mg/L 0.0191 2.486 mg/L 0.0191 0.77%

QC value within limits for Sr 407.771 Recovery = 99.45%

Li 670.784 349836.1 2.479 mg/L 0.0134 2.479 mg/L 0.0134 0.54%

QC value within limits for Li 670.784 Recovery = 99.16%

Sn 189.927 13055.6 2.479 mg/L 0.0109 2.479 mg/L 0.0109 0.44%

QC value within limits for Sn 189.927 Recovery = 99.16%

Ti 334.940 201291.4 2.465 mg/L 0.0169 2.465 mg/L 0.0169 0.68%

QC value within limits for Ti 334.940 Recovery = 98.59%

Ca 317.933 2412.0 -0.030 mg/L 0.0008 -0.030 mg/L 0.0008 2.73%

Na 589.592 5485.6 -0.011 mg/L 0.0116 -0.011 mg/L 0.0116 104.11%K 766.490 274.7 0.049 mg/L 0.0336 0.049 mg/L 0.0336 68.25%

Cr 267.716 39.2 -0.019 mg/L 0.0000 -0.019 mg/L 0.0000 0.19%

Ni 231.604 -192.4 -0.026 mg/L 0.0008 -0.026 mg/L 0.0008 3.16%

Al 396.153 1080.6 0.091 mg/L 0.0043 0.091 mg/L 0.0043 4.78%

Mg 285.213 226.0 -0.094 mg/L 0.0012 -0.094 mg/L 0.0012 1.32%

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Ag 328.068 141.8 -0.002 mg/L 0.0008 -0.002 mg/L 0.0008 39.74%

B 249.677 11127.2 0.090 mg/L 0.0058 0.090 mg/L 0.0058 6.49%

Sb 206.836 -37.4 -0.015 mg/L 0.0042 -0.015 mg/L 0.0042 28.32%

Tl 190.801 -237.1 -0.127 mg/L 0.0022 -0.127 mg/L 0.0022 1.74%


====================================================================================================

Sequence No.: 26 Autosampler Location: 29Sample ID: QC 4-3 Date Collected: 28/12/2015 10:42:28 a.m.Analyst: Data Type: Reprocessed on 28/12/2015 02:21:36 p.m.


----------------------------------------------------------------------------------------------------



Be 313.107 -535.7 0.002 mg/L 0.0000 0.002 mg/L 0.0000 0.41%

Cd 228.802 35.8 -0.002 mg/L 0.0006 -0.002 mg/L 0.0006 33.35%

Pb 220.353 -272.0 -0.045 mg/L 0.0064 -0.045 mg/L 0.0064 14.08%

Se 196.026 5.3 0.008 mg/L 0.0132 0.008 mg/L 0.0132 165.23%

Zn 206.200 -450.5 -0.091 mg/L 0.0033 -0.091 mg/L 0.0033 3.69%

Ba 233.527 -420.0 -0.051 mg/L 0.0003 -0.051 mg/L 0.0003 0.66%

Cu 327.393 78.2 -0.010 mg/L 0.0002 -0.010 mg/L 0.0002 2.50%

Fe 238.204 113.2 0.002 mg/L 0.0005 0.002 mg/L 0.0005 27.66%

V 290.880 55.2 0.005 mg/L 0.0032 0.005 mg/L 0.0032 58.85%

Co 228.616 79.9 -0.004 mg/L 0.0004 -0.004 mg/L 0.0004 9.12%

As 188.979 -34.8 -0.030 mg/L 0.0166 -0.030 mg/L 0.0166 56.38%

Mo 202.031 134.5 0.004 mg/L 0.0010 0.004 mg/L 0.0010 26.81%

Sr 407.771 5257.9 -0.000 mg/L 0.0001 -0.000 mg/L 0.0001 12.79%

Li 670.784 600.6 -0.003 mg/L 0.0004 -0.003 mg/L 0.0004 12.80%

Sn 189.927 -65.4 -0.013 mg/L 0.0015 -0.013 mg/L 0.0015 11.97%

Ti 334.940 352.6 0.005 mg/L 0.0004 0.005 mg/L 0.0004 8.27%

Ca 317.933 257688.9 10.08 mg/L 0.055 10.08 mg/L 0.055 0.54%

QC value within limits for Ca 317.933 Recovery = 100.79%

Na 589.592 147130.3 9.905 mg/L 0.0456 9.905 mg/L 0.0456 0.46%

QC value within limits for Na 589.592 Recovery = 99.05%K 766.490 33309.0 9.969 mg/L 0.0277 9.969 mg/L 0.0277 0.28%

QC value within limits for K 766.490 Recovery = 99.69%

Cr 267.716 783974.0 1.023 mg/L 0.0074 1.023 mg/L 0.0074 0.72%

QC value within limits for Cr 267.716 Recovery = 102.35%

Ni 231.604 37551.4 1.024 mg/L 0.0058 1.024 mg/L 0.0058 0.57%

QC value within limits for Ni 231.604 Recovery = 102.41%

Al 396.153 76432.6 10.04 mg/L 0.031 10.04 mg/L 0.031 0.31%

QC value within limits for Al 396.153 Recovery = 100.45%

Mg 285.213 500.8 -0.082 mg/L 0.0012 -0.082 mg/L 0.0012 1.48%

Ag 328.068 -52.9 -0.003 mg/L 0.0007 -0.003 mg/L 0.0007 23.24%

B 249.677 7555.6 0.004 mg/L 0.0044 0.004 mg/L 0.0044 107.42%

Sb 206.836 416.1 0.165 mg/L 0.0027 0.165 mg/L 0.0027 1.66%

Tl 190.801 7.2 -0.007 mg/L 0.0041 -0.007 mg/L 0.0041 62.30%


====================================================================================================


----------------------------------------------------------------------------------------------------


Analyte Intensity Conc. Units Std.Dev. Conc. Units Std.Dev. RSD

Mn 257.610 21.9 -0.007 mg/L 0.0001 -0.007 mg/L 0.0001 1.13%Be 313.107 -102.2 0.003 mg/L 0.0001 0.003 mg/L 0.0001 2.31%

Cd 228.802 37.3 -0.002 mg/L 0.0003 -0.002 mg/L 0.0003 17.41%

Pb 220.353 -13.6 -0.001 mg/L 0.0011 -0.001 mg/L 0.0011 157.19%

Se 196.026 2.3 0.006 mg/L 0.0119 0.006 mg/L 0.0119 204.48%

Zn 206.200 29.9 0.002 mg/L 0.0017 0.002 mg/L 0.0017 93.67%

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Ba 233.527 -3.5 -0.001 mg/L 0.0016 -0.001 mg/L 0.0016 114.55%

Cu 327.393 122.6 -0.009 mg/L 0.0009 -0.009 mg/L 0.0009 9.88%

Fe 238.204 50.7 -0.007 mg/L 0.0015 -0.007 mg/L 0.0015 20.51%

V 290.880 28.9 0.003 mg/L 0.0009 0.003 mg/L 0.0009 29.37%

Co 228.616 -18.3 -0.008 mg/L 0.0007 -0.008 mg/L 0.0007 7.82%

As 188.979 -3.8 -0.002 mg/L 0.0107 -0.002 mg/L 0.0107 571.84%

Mo 202.031 49.9 -0.003 mg/L 0.0012 -0.003 mg/L 0.0012 42.18%

Sr 407.771 776.9 -0.003 mg/L 0.0000 -0.003 mg/L 0.0000 0.44%

Li 670.784 -132.3 -0.008 mg/L 0.0011 -0.008 mg/L 0.0011 13.85%

Sn 189.927 2.3 -0.000 mg/L 0.0015 -0.000 mg/L 0.0015 >999.9%

Ti 334.940 71.4 0.002 mg/L 0.0003 0.002 mg/L 0.0003 17.46%Ca 317.933 3590.1 0.016 mg/L 0.0021 0.016 mg/L 0.0021 12.91%

Na 589.592 6313.5 0.047 mg/L 0.0058 0.047 mg/L 0.0058 12.29%

K 766.490 5.4 -0.032 mg/L 0.0394 -0.032 mg/L 0.0394 124.31%

Cr 267.716 108.0 -0.019 mg/L 0.0001 -0.019 mg/L 0.0001 0.27%

Ni 231.604 107.9 -0.018 mg/L 0.0005 -0.018 mg/L 0.0005 3.00%

Al 396.153 49.5 -0.046 mg/L 0.0059 -0.046 mg/L 0.0059 12.96%

Mg 285.213 231916.3 9.957 mg/L 0.0048 9.957 mg/L 0.0048 0.05%

QC value within limits for Mg 285.213 Recovery = 99.57%

Ag 328.068 5599.7 0.029 mg/L 0.0035 0.029 mg/L 0.0035 11.99%

B 249.677 432711.8 10.25 mg/L 0.050 10.25 mg/L 0.050 0.48%

QC value within limits for B 249.677 Recovery = 102.47%

Sb 206.836 2470.9 0.981 mg/L 0.0020 0.981 mg/L 0.0020 0.21%

QC value within limits for Sb 206.836 Recovery = 98.08%

Tl 190.801 2071.6 1.011 mg/L 0.0088 1.011 mg/L 0.0088 0.87%

QC value within limits for Tl 190.801 Recovery = 101.09%


====================================================================================================

Sequence No.: 28 Autosampler Location: 36Sample ID: lavado Date Collected: 28/12/2015 10:46:27 a.m.Analyst: Data Type: Reprocessed on 28/12/2015 02:21:37 p.m.Logged In Analyst (Original) : AdministratorInitial Sample Wt: Initial Sample Vol:Dilution: Sample Prep Vol:Wash Time:

----------------------------------------------------------------------------------------------------

Mean Data: lavado

Mean Corrected Calib. SampleAnalyte Intensity Conc. Units Std.Dev. Conc. Units Std.Dev. RSDMn 257.610 16.1 0.000 mg/L 0.0003 0.000 mg/L 0.0003 96.54%

Be 313.107 -75.0 -0.000 mg/L 0.0000 -0.000 mg/L 0.0000 28.16%

Cd 228.802 41.8 0.001 mg/L 0.0003 0.001 mg/L 0.0003 45.90%

Pb 220.353 -22.5 0.002 mg/L 0.0040 0.002 mg/L 0.0040 170.42%

Se 196.026 14.0 0.001 mg/L 0.0053 0.001 mg/L 0.0053 603.25%

Zn 206.200 1.0 -0.000 mg/L 0.0020 -0.000 mg/L 0.0020 >999.9%

Ba 233.527 -7.1 -0.000 mg/L 0.0007 -0.000 mg/L 0.0007 322.38%

Cu 327.393 -23.2 0.001 mg/L 0.0003 0.001 mg/L 0.0003 66.79%

Fe 238.204 7.1 0.001 mg/L 0.0011 0.001 mg/L 0.0011 182.90%

V 290.880 -34.0 -0.001 mg/L 0.0023 -0.001 mg/L 0.0023 294.22%

Co 228.616 13.5 0.001 mg/L 0.0005 0.001 mg/L 0.0005 56.25%

As 188.979 3.6 0.000 mg/L 0.0040 0.000 mg/L 0.0040 883.70%

Mo 202.031 35.0 0.003 mg/L 0.0002 0.003 mg/L 0.0002 6.81%

Sr 407.771 104.6 0.000 mg/L 0.0001 0.000 mg/L 0.0001 64.24%Li 670.784 -458.9 -0.002 mg/L 0.0008 -0.002 mg/L 0.0008 46.79%

Sn 189.927 10.0 0.001 mg/L 0.0006 0.001 mg/L 0.0006 48.09%

Ti 334.940 18.5 -0.000 mg/L 0.0002 -0.000 mg/L 0.0002 73.07%

Ca 317.933 17.9 0.001 mg/L 0.0010 0.001 mg/L 0.0010 100.99%

Na 589.592 -50.3 0.007 mg/L 0.0066 0.007 mg/L 0.0066 88.37%

K 766.490 -41.2 0.021 mg/L 0.0095 0.021 mg/L 0.0095 44.46%

Cr 267.716 -20.4 -0.000 mg/L 0.0000 -0.000 mg/L 0.0000 114.28%

Ni 231.604 55.8 0.002 mg/L 0.0009 0.002 mg/L 0.0009 58.26%

Al 396.153 -4.1 0.013 mg/L 0.0071 0.013 mg/L 0.0071 54.90%

Mg 285.213 51.1 0.001 mg/L 0.0007 0.001 mg/L 0.0007 89.23%

Ag 328.068 -13.8 -0.000 mg/L 0.0007 -0.000 mg/L 0.0007 227.05%

B 249.677 -1715.7 0.212 mg/L 0.0063 0.212 mg/L 0.0063 2.97%

Sb 206.836 15.8 0.006 mg/L 0.0059 0.006 mg/L 0.0059 96.34%

Tl 190.801 3.2 -0.001 mg/L 0.0046 -0.001 mg/L 0.0046 496.76%

====================================================================================================

Sequence No.: 29 Autosampler Location: 36Sample ID: lavado Date Collected: 28/12/2015 10:48:27 a.m.Analyst: Data Type: Reprocessed on 28/12/2015 02:21:37 p.m.

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----------------------------------------------------------------------------------------------------

Mean Data: lavadoMean Corrected Calib. Sample


Be 313.107 -65.5 -0.000 mg/L 0.0000 -0.000 mg/L 0.0000 1.84%Cd 228.802 35.4 0.000 mg/L 0.0006 0.000 mg/L 0.0006 154.33%

Pb 220.353 -16.3 0.003 mg/L 0.0034 0.003 mg/L 0.0034 100.48%

Se 196.026 12.0 -0.001 mg/L 0.0096 -0.001 mg/L 0.0096 >999.9%

Zn 206.200 0.1 -0.000 mg/L 0.0003 -0.000 mg/L 0.0003 84.22%

Ba 233.527 -0.4 0.001 mg/L 0.0001 0.001 mg/L 0.0001 14.55%

Cu 327.393 -29.6 0.000 mg/L 0.0013 0.000 mg/L 0.0013 277.94%

Fe 238.204 -3.9 -0.001 mg/L 0.0007 -0.001 mg/L 0.0007 74.11%

V 290.880 -20.1 0.000 mg/L 0.0010 0.000 mg/L 0.0010 303.30%

Co 228.616 7.8 0.001 mg/L 0.0001 0.001 mg/L 0.0001 21.19%

As 188.979 -2.7 -0.005 mg/L 0.0064 -0.005 mg/L 0.0064 123.28%

Mo 202.031 21.9 0.002 mg/L 0.0006 0.002 mg/L 0.0006 24.46%

Sr 407.771 5.8 0.000 mg/L 0.0000 0.000 mg/L 0.0000 39.98%

Li 670.784 -355.7 -0.001 mg/L 0.0016 -0.001 mg/L 0.0016 179.05%

Sn 189.927 17.0 0.003 mg/L 0.0015 0.003 mg/L 0.0015 57.21%

Ti 334.940 58.8 0.000 mg/L 0.0004 0.000 mg/L 0.0004 238.19%

Ca 317.933 76.2 0.003 mg/L 0.0006 0.003 mg/L 0.0006 18.60%

Na 589.592 22.5 0.013 mg/L 0.0068 0.013 mg/L 0.0068 54.04%

K 766.490 -74.2 0.011 mg/L 0.0262 0.011 mg/L 0.0262 230.04%

Cr 267.716 11.2 0.000 mg/L 0.0000 0.000 mg/L 0.0000 90.48%

Ni 231.604 77.1 0.002 mg/L 0.0002 0.002 mg/L 0.0002 9.27%

Al 396.153 -56.9 0.006 mg/L 0.0070 0.006 mg/L 0.0070 117.52%

Mg 285.213 26.8 -0.000 mg/L 0.0013 -0.000 mg/L 0.0013 389.00%

Ag 328.068 -58.3 -0.001 mg/L 0.0005 -0.001 mg/L 0.0005 83.48%

B 249.677 -4452.0 0.146 mg/L 0.0068 0.146 mg/L 0.0068 4.66%

Sb 206.836 11.3 0.004 mg/L 0.0039 0.004 mg/L 0.0039 90.76%

Tl 190.801 -0.9 -0.003 mg/L 0.0021 -0.003 mg/L 0.0021 70.41%

====================================================================================================

Sequence No.: 30 Autosampler Location: 37Sample ID: STD 90% MIX 1 Date Collected: 28/12/2015 10:50:28 a.m.Analyst: Data Type: Reprocessed on 28/12/2015 02:21:38 p.m.Logged In Analyst (Original) : AdministratorInitial Sample Wt: Initial Sample Vol:Dilution: Sample Prep Vol:Wash Time:

----------------------------------------------------------------------------------------------------

Mean Data: STD 90% MIX 1Mean Corrected Calib. Sample


Be 313.107 1895660.5 4.491 mg/L 0.0202 4.491 mg/L 0.0202 0.45%

Cd 228.802 139562.9 4.509 mg/L 0.0047 4.509 mg/L 0.0047 0.10%

Pb 220.353 26156.0 4.508 mg/L 0.0035 4.508 mg/L 0.0035 0.08%Se 196.026 6125.0 4.416 mg/L 0.0334 4.416 mg/L 0.0334 0.76%

Zn 206.200 23400.0 4.512 mg/L 0.0120 4.512 mg/L 0.0120 0.27%

Ba 233.527 13.4 0.002 mg/L 0.0010 0.002 mg/L 0.0010 42.93%

Cu 327.393 40.9 0.001 mg/L 0.0007 0.001 mg/L 0.0007 70.08%

Fe 238.204 48.2 0.007 mg/L 0.0012 0.007 mg/L 0.0012 18.26%

V 290.880 -10.2 0.001 mg/L 0.0016 0.001 mg/L 0.0016 139.97%

Co 228.616 9.8 0.001 mg/L 0.0004 0.001 mg/L 0.0004 56.82%

As 188.979 -7.0 -0.009 mg/L 0.0088 -0.009 mg/L 0.0088 98.57%

Mo 202.031 15.5 0.002 mg/L 0.0018 0.002 mg/L 0.0018 103.00%

Sr 407.771 988.4 0.001 mg/L 0.0000 0.001 mg/L 0.0000 6.10%

Li 670.784 -311.5 -0.001 mg/L 0.0005 -0.001 mg/L 0.0005 89.94%

Sn 189.927 -3.0 -0.001 mg/L 0.0015 -0.001 mg/L 0.0015 131.39%

Ti 334.940 84.0 0.000 mg/L 0.0003 0.000 mg/L 0.0003 53.77%

Ca 317.933 2660.6 0.106 mg/L 0.0025 0.106 mg/L 0.0025 2.39%Na 589.592 5402.3 0.389 mg/L 0.0074 0.389 mg/L 0.0074 1.91%

K 766.490 257.9 0.111 mg/L 0.0072 0.111 mg/L 0.0072 6.47%

Cr 267.716 -84.0 -0.000 mg/L 0.0000 -0.000 mg/L 0.0000 0.72%

Ni 231.604 102.6 0.003 mg/L 0.0003 0.003 mg/L 0.0003 10.00%

Al 396.153 -2.2 0.013 mg/L 0.0025 0.013 mg/L 0.0025 19.23%

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Mg 285.213 385.3 0.015 mg/L 0.0013 0.015 mg/L 0.0013 8.42%

Ag 328.068 317593.3 1.793 mg/L 0.0034 1.793 mg/L 0.0034 0.19%

B 249.677 -2214.8 0.200 mg/L 0.0049 0.200 mg/L 0.0049 2.45%

Sb 206.836 21.3 0.008 mg/L 0.0021 0.008 mg/L 0.0021 24.79%

Tl 190.801 -59.3 -0.032 mg/L 0.0014 -0.032 mg/L 0.0014 4.39%

====================================================================================================

Sequence No.: 31 Autosampler Location: 37Sample ID: STD 90% MIX 1 Date Collected: 28/12/2015 10:52:35 a.m.Analyst: Data Type: Reprocessed on 28/12/2015 02:21:38 p.m.


----------------------------------------------------------------------------------------------------



Be 313.107 1886394.5 4.469 mg/L 0.0126 4.469 mg/L 0.0126 0.28%

Cd 228.802 139613.0 4.511 mg/L 0.0347 4.511 mg/L 0.0347 0.77%

Pb 220.353 26100.9 4.498 mg/L 0.0444 4.498 mg/L 0.0444 0.99%

Se 196.026 6143.1 4.429 mg/L 0.0083 4.429 mg/L 0.0083 0.19%

Zn 206.200 23375.2 4.508 mg/L 0.0055 4.508 mg/L 0.0055 0.12%

Ba 233.527 3.0 0.001 mg/L 0.0003 0.001 mg/L 0.0003 34.70%

Cu 327.393 59.6 0.001 mg/L 0.0003 0.001 mg/L 0.0003 21.89%

Fe 238.204 45.8 0.006 mg/L 0.0005 0.006 mg/L 0.0005 8.22%

V 290.880 10.4 0.003 mg/L 0.0009 0.003 mg/L 0.0009 33.15%

Co 228.616 1.9 0.000 mg/L 0.0007 0.000 mg/L 0.0007 162.84%

As 188.979 1.1 -0.002 mg/L 0.0085 -0.002 mg/L 0.0085 474.31%

Mo 202.031 24.3 0.002 mg/L 0.0004 0.002 mg/L 0.0004 16.95%

Sr 407.771 1034.2 0.001 mg/L 0.0001 0.001 mg/L 0.0001 12.97%

Li 670.784 -45.7 0.001 mg/L 0.0014 0.001 mg/L 0.0014 110.36%

Sn 189.927 7.8 0.001 mg/L 0.0029 0.001 mg/L 0.0029 320.28%

Ti 334.940 126.9 0.001 mg/L 0.0006 0.001 mg/L 0.0006 63.09%

Ca 317.933 2645.9 0.105 mg/L 0.0005 0.105 mg/L 0.0005 0.44%

Na 589.592 5412.9 0.390 mg/L 0.0111 0.390 mg/L 0.0111 2.84%

K 766.490 240.3 0.106 mg/L 0.0213 0.106 mg/L 0.0213 20.10%

Cr 267.716 -107.7 -0.000 mg/L 0.0001 -0.000 mg/L 0.0001 41.35%Ni 231.604 90.0 0.002 mg/L 0.0004 0.002 mg/L 0.0004 15.89%

Al 396.153 -58.5 0.006 mg/L 0.0143 0.006 mg/L 0.0143 251.14%

Mg 285.213 404.3 0.016 mg/L 0.0014 0.016 mg/L 0.0014 8.65%

Ag 328.068 317230.3 1.791 mg/L 0.0119 1.791 mg/L 0.0119 0.67%

B 249.677 -1900.3 0.207 mg/L 0.0041 0.207 mg/L 0.0041 1.96%

Sb 206.836 17.7 0.007 mg/L 0.0048 0.007 mg/L 0.0048 69.85%

Tl 190.801 -63.0 -0.034 mg/L 0.0046 -0.034 mg/L 0.0046 13.59%

====================================================================================================

Sequence No.: 32 Autosampler Location: 37Sample ID: STD 90% MIX 1 Date Collected: 28/12/2015 10:54:46 a.m.Analyst: Data Type: Reprocessed on 28/12/2015 02:21:38 p.m.Logged In Analyst (Original) : AdministratorInitial Sample Wt: Initial Sample Vol:


----------------------------------------------------------------------------------------------------



Be 313.107 1877818.0 4.449 mg/L 0.0370 4.449 mg/L 0.0370 0.83%

Cd 228.802 139212.3 4.498 mg/L 0.0407 4.498 mg/L 0.0407 0.90%

Pb 220.353 26020.4 4.485 mg/L 0.0389 4.485 mg/L 0.0389 0.87%

Se 196.026 6164.2 4.444 mg/L 0.0040 4.444 mg/L 0.0040 0.09%

Zn 206.200 23354.3 4.504 mg/L 0.0723 4.504 mg/L 0.0723 1.61%

Ba 233.527 12.5 0.002 mg/L 0.0026 0.002 mg/L 0.0026 121.38%

Cu 327.393 132.0 0.002 mg/L 0.0005 0.002 mg/L 0.0005 27.36%Fe 238.204 53.7 0.007 mg/L 0.0010 0.007 mg/L 0.0010 14.28%

V 290.880 -5.4 0.002 mg/L 0.0006 0.002 mg/L 0.0006 40.69%

Co 228.616 4.9 0.001 mg/L 0.0002 0.001 mg/L 0.0002 30.10%

As 188.979 -2.7 -0.005 mg/L 0.0008 -0.005 mg/L 0.0008 14.63%

Mo 202.031 9.7 0.001 mg/L 0.0009 0.001 mg/L 0.0009 65.51%

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Sr 407.771 885.6 0.000 mg/L 0.0000 0.000 mg/L 0.0000 5.64%

Li 670.784 -216.2 0.000 mg/L 0.0006 0.000 mg/L 0.0006 635.70%

Sn 189.927 7.3 0.001 mg/L 0.0004 0.001 mg/L 0.0004 53.63%

Ti 334.940 91.5 0.001 mg/L 0.0006 0.001 mg/L 0.0006 109.61%

Ca 317.933 2685.7 0.107 mg/L 0.0007 0.107 mg/L 0.0007 0.68%

Na 589.592 5660.8 0.407 mg/L 0.0032 0.407 mg/L 0.0032 0.78%

K 766.490 233.1 0.104 mg/L 0.0280 0.104 mg/L 0.0280 27.03%

Cr 267.716 -98.5 -0.000 mg/L 0.0000 -0.000 mg/L 0.0000 42.20%

Ni 231.604 64.2 0.002 mg/L 0.0003 0.002 mg/L 0.0003 16.40%

Al 396.153 39.9 0.019 mg/L 0.0155 0.019 mg/L 0.0155 82.88%

Mg 285.213 416.6 0.017 mg/L 0.0010 0.017 mg/L 0.0010 6.26%Ag 328.068 316446.3 1.786 mg/L 0.0144 1.786 mg/L 0.0144 0.80%

B 249.677 -2914.4 0.183 mg/L 0.0086 0.183 mg/L 0.0086 4.70%

Sb 206.836 6.6 0.002 mg/L 0.0033 0.002 mg/L 0.0033 136.30%

Tl 190.801 -66.4 -0.035 mg/L 0.0065 -0.035 mg/L 0.0065 18.45%

====================================================================================================


----------------------------------------------------------------------------------------------------



Be 313.107 1882813.6 4.461 mg/L 0.0314 4.461 mg/L 0.0314 0.70%

Cd 228.802 138714.8 4.482 mg/L 0.0426 4.482 mg/L 0.0426 0.95%

Pb 220.353 25964.1 4.475 mg/L 0.0489 4.475 mg/L 0.0489 1.09%

Se 196.026 6121.8 4.413 mg/L 0.0117 4.413 mg/L 0.0117 0.27%

Zn 206.200 23262.9 4.486 mg/L 0.0612 4.486 mg/L 0.0612 1.36%

Ba 233.527 17.9 0.003 mg/L 0.0005 0.003 mg/L 0.0005 18.27%

Cu 327.393 159.3 0.002 mg/L 0.0001 0.002 mg/L 0.0001 3.32%

Fe 238.204 45.5 0.006 mg/L 0.0023 0.006 mg/L 0.0023 37.70%

V 290.880 -15.6 0.001 mg/L 0.0029 0.001 mg/L 0.0029 409.38%

Co 228.616 10.5 0.001 mg/L 0.0005 0.001 mg/L 0.0005 67.50%As 188.979 -6.3 -0.008 mg/L 0.0096 -0.008 mg/L 0.0096 114.95%

Mo 202.031 14.4 0.002 mg/L 0.0012 0.002 mg/L 0.0012 73.54%

Sr 407.771 1005.8 0.001 mg/L 0.0000 0.001 mg/L 0.0000 5.32%

Li 670.784 -316.2 -0.001 mg/L 0.0014 -0.001 mg/L 0.0014 218.04%

Sn 189.927 9.9 0.001 mg/L 0.0023 0.001 mg/L 0.0023 177.63%

Ti 334.940 86.8 0.001 mg/L 0.0003 0.001 mg/L 0.0003 60.20%

Ca 317.933 2716.3 0.108 mg/L 0.0028 0.108 mg/L 0.0028 2.61%

Na 589.592 5816.2 0.418 mg/L 0.0103 0.418 mg/L 0.0103 2.47%

K 766.490 197.0 0.093 mg/L 0.0077 0.093 mg/L 0.0077 8.25%

Cr 267.716 -102.4 -0.000 mg/L 0.0001 -0.000 mg/L 0.0001 41.36%

Ni 231.604 98.4 0.003 mg/L 0.0007 0.003 mg/L 0.0007 25.09%

Al 396.153 -10.0 0.012 mg/L 0.0085 0.012 mg/L 0.0085 69.98%

Mg 285.213 400.2 0.016 mg/L 0.0012 0.016 mg/L 0.0012 7.65%

Ag 328.068 315285.3 1.780 mg/L 0.0168 1.780 mg/L 0.0168 0.94%

B 249.677 -3753.6 0.163 mg/L 0.0084 0.163 mg/L 0.0084 5.14%Sb 206.836 3.0 0.001 mg/L 0.0018 0.001 mg/L 0.0018 177.22%

Tl 190.801 -84.8 -0.044 mg/L 0.0058 -0.044 mg/L 0.0058 13.12%

====================================================================================================


----------------------------------------------------------------------------------------------------

Mean Data: STD 90% MIX 1Mean Corrected Calib. SampleAnalyte Intensity Conc. Units Std.Dev. Conc. Units Std.Dev. RSDMn 257.610 301007.6 4.510 mg/L 0.0296 4.510 mg/L 0.0296 0.66%

Be 313.107 1880152.0 4.455 mg/L 0.0369 4.455 mg/L 0.0369 0.83%

Cd 228.802 140052.7 4.525 mg/L 0.0247 4.525 mg/L 0.0247 0.55%

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Pb 220.353 26217.8 4.519 mg/L 0.0169 4.519 mg/L 0.0169 0.37%

Se 196.026 6130.0 4.419 mg/L 0.0416 4.419 mg/L 0.0416 0.94%

Zn 206.200 23437.3 4.520 mg/L 0.0388 4.520 mg/L 0.0388 0.86%

Ba 233.527 -2.7 0.000 mg/L 0.0006 0.000 mg/L 0.0006 202.41%

Cu 327.393 37.6 0.001 mg/L 0.0003 0.001 mg/L 0.0003 31.36%

Fe 238.204 49.7 0.007 mg/L 0.0014 0.007 mg/L 0.0014 21.42%

V 290.880 -5.5 0.002 mg/L 0.0008 0.002 mg/L 0.0008 50.99%

Co 228.616 -0.4 0.000 mg/L 0.0014 0.000 mg/L 0.0014 403.97%

As 188.979 2.7 -0.000 mg/L 0.0068 -0.000 mg/L 0.0068 >999.9%

Mo 202.031 12.0 0.001 mg/L 0.0004 0.001 mg/L 0.0004 25.82%

Sr 407.771 825.4 0.000 mg/L 0.0000 0.000 mg/L 0.0000 8.85%Li 670.784 -397.7 -0.001 mg/L 0.0010 -0.001 mg/L 0.0010 81.19%

Sn 189.927 12.7 0.002 mg/L 0.0006 0.002 mg/L 0.0006 32.28%

Ti 334.940 85.4 0.001 mg/L 0.0006 0.001 mg/L 0.0006 127.74%

Ca 317.933 2644.1 0.105 mg/L 0.0022 0.105 mg/L 0.0022 2.06%

Na 589.592 3636.6 0.266 mg/L 0.0155 0.266 mg/L 0.0155 5.83%

K 766.490 251.9 0.109 mg/L 0.0350 0.109 mg/L 0.0350 32.01%

Cr 267.716 -72.8 -0.000 mg/L 0.0000 -0.000 mg/L 0.0000 40.76%

Ni 231.604 91.2 0.002 mg/L 0.0002 0.002 mg/L 0.0002 8.22%

Al 396.153 -26.5 0.010 mg/L 0.0023 0.010 mg/L 0.0023 23.37%

Mg 285.213 402.3 0.016 mg/L 0.0024 0.016 mg/L 0.0024 14.84%

Ag 328.068 317902.6 1.794 mg/L 0.0086 1.794 mg/L 0.0086 0.48%

B 249.677 -4221.0 0.151 mg/L 0.0008 0.151 mg/L 0.0008 0.53%

Sb 206.836 0.0 -0.000 mg/L 0.0020 -0.000 mg/L 0.0020 >999.9%

Tl 190.801 -66.8 -0.035 mg/L 0.0040 -0.035 mg/L 0.0040 11.24%

====================================================================================================


----------------------------------------------------------------------------------------------------


Analyte Intensity Conc. Units Std.Dev. Conc. Units Std.Dev. RSD

Mn 257.610 298815.4 4.477 mg/L 0.0658 4.477 mg/L 0.0658 1.47%Be 313.107 1886736.6 4.470 mg/L 0.0258 4.470 mg/L 0.0258 0.58%

Cd 228.802 139138.6 4.495 mg/L 0.0264 4.495 mg/L 0.0264 0.59%

Pb 220.353 26058.5 4.491 mg/L 0.0273 4.491 mg/L 0.0273 0.61%

Se 196.026 6198.9 4.469 mg/L 0.0245 4.469 mg/L 0.0245 0.55%

Zn 206.200 23359.8 4.505 mg/L 0.0731 4.505 mg/L 0.0731 1.62%

Ba 233.527 7.7 0.002 mg/L 0.0003 0.002 mg/L 0.0003 16.94%

Cu 327.393 80.3 0.001 mg/L 0.0001 0.001 mg/L 0.0001 4.47%

Fe 238.204 55.6 0.008 mg/L 0.0014 0.008 mg/L 0.0014 18.98%

V 290.880 3.7 0.002 mg/L 0.0023 0.002 mg/L 0.0023 103.50%

Co 228.616 13.4 0.001 mg/L 0.0004 0.001 mg/L 0.0004 39.23%

As 188.979 -3.4 -0.006 mg/L 0.0125 -0.006 mg/L 0.0125 215.48%

Mo 202.031 21.2 0.002 mg/L 0.0004 0.002 mg/L 0.0004 17.68%

Sr 407.771 940.5 0.000 mg/L 0.0000 0.000 mg/L 0.0000 7.55%

Li 670.784 -167.3 0.000 mg/L 0.0011 0.000 mg/L 0.0011 244.67%

Sn 189.927 3.2 0.000 mg/L 0.0009 0.000 mg/L 0.0009 >999.9%Ti 334.940 45.5 0.000 mg/L 0.0003 0.000 mg/L 0.0003 >999.9%

Ca 317.933 2705.9 0.107 mg/L 0.0004 0.107 mg/L 0.0004 0.37%

Na 589.592 3547.9 0.259 mg/L 0.0065 0.259 mg/L 0.0065 2.50%

K 766.490 -40.6 0.021 mg/L 0.0261 0.021 mg/L 0.0261 121.54%

Cr 267.716 -71.3 -0.000 mg/L 0.0000 -0.000 mg/L 0.0000 54.09%

Ni 231.604 82.4 0.002 mg/L 0.0013 0.002 mg/L 0.0013 59.40%

Al 396.153 -21.3 0.011 mg/L 0.0044 0.011 mg/L 0.0044 41.19%

Mg 285.213 377.0 0.015 mg/L 0.0017 0.015 mg/L 0.0017 11.20%

Ag 328.068 315968.5 1.783 mg/L 0.0097 1.783 mg/L 0.0097 0.54%

B 249.677 -5219.9 0.127 mg/L 0.0021 0.127 mg/L 0.0021 1.66%

Sb 206.836 2.5 0.001 mg/L 0.0015 0.001 mg/L 0.0015 186.16%

Tl 190.801 -56.1 -0.030 mg/L 0.0048 -0.030 mg/L 0.0048 15.80%

====================================================================================================Sequence No.: 36 Autosampler Location: 38Sample ID: STD 90% MIX 1 Date Collected: 28/12/2015 11:03:13 a.m.Analyst: Data Type: Reprocessed on 28/12/2015 02:21:40 p.m.Logged In Analyst (Original) : AdministratorInitial Sample Wt: Initial Sample Vol:

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Be 313.107 1880248.8 4.455 mg/L 0.0269 4.455 mg/L 0.0269 0.60%

Cd 228.802 140455.4 4.538 mg/L 0.0382 4.538 mg/L 0.0382 0.84%

Pb 220.353 26412.3 4.552 mg/L 0.0458 4.552 mg/L 0.0458 1.01%Se 196.026 6171.1 4.449 mg/L 0.0212 4.449 mg/L 0.0212 0.48%

Zn 206.200 23475.1 4.527 mg/L 0.0128 4.527 mg/L 0.0128 0.28%

Ba 233.527 -8.3 -0.000 mg/L 0.0011 -0.000 mg/L 0.0011 324.27%

Cu 327.393 95.0 0.001 mg/L 0.0011 0.001 mg/L 0.0011 76.67%

Fe 238.204 61.6 0.008 mg/L 0.0017 0.008 mg/L 0.0017 19.95%

V 290.880 1.8 0.002 mg/L 0.0024 0.002 mg/L 0.0024 112.19%

Co 228.616 1.6 0.000 mg/L 0.0004 0.000 mg/L 0.0004 100.22%

As 188.979 -11.7 -0.013 mg/L 0.0058 -0.013 mg/L 0.0058 44.19%

Mo 202.031 8.3 0.001 mg/L 0.0007 0.001 mg/L 0.0007 59.43%

Sr 407.771 1001.0 0.001 mg/L 0.0000 0.001 mg/L 0.0000 2.96%

Li 670.784 -299.6 -0.001 mg/L 0.0009 -0.001 mg/L 0.0009 176.56%

Sn 189.927 -6.8 -0.002 mg/L 0.0020 -0.002 mg/L 0.0020 106.14%

Ti 334.940 123.7 0.001 mg/L 0.0006 0.001 mg/L 0.0006 56.53%

Ca 317.933 2685.9 0.107 mg/L 0.0013 0.107 mg/L 0.0013 1.20%

Na 589.592 3801.6 0.277 mg/L 0.0054 0.277 mg/L 0.0054 1.96%

K 766.490 204.4 0.095 mg/L 0.0441 0.095 mg/L 0.0441 46.45%

Cr 267.716 -110.8 -0.000 mg/L 0.0001 -0.000 mg/L 0.0001 52.15%

Ni 231.604 72.3 0.002 mg/L 0.0004 0.002 mg/L 0.0004 20.22%

Al 396.153 74.4 0.023 mg/L 0.0087 0.023 mg/L 0.0087 37.54%

Mg 285.213 369.6 0.015 mg/L 0.0020 0.015 mg/L 0.0020 13.52%

Ag 328.068 319062.6 1.801 mg/L 0.0138 1.801 mg/L 0.0138 0.77%

B 249.677 -4968.5 0.133 mg/L 0.0070 0.133 mg/L 0.0070 5.21%

Sb 206.836 -3.4 -0.002 mg/L 0.0012 -0.002 mg/L 0.0012 76.24%

Tl 190.801 -61.7 -0.033 mg/L 0.0017 -0.033 mg/L 0.0017 5.26%

====================================================================================================

Sequence No.: 37 Autosampler Location: 38Sample ID: STD 90% MIX 1 Date Collected: 28/12/2015 11:05:20 a.m.


----------------------------------------------------------------------------------------------------



Be 313.107 1887701.4 4.472 mg/L 0.0281 4.472 mg/L 0.0281 0.63%

Cd 228.802 139863.8 4.519 mg/L 0.0277 4.519 mg/L 0.0277 0.61%

Pb 220.353 26148.9 4.507 mg/L 0.0235 4.507 mg/L 0.0235 0.52%

Se 196.026 6151.0 4.434 mg/L 0.0512 4.434 mg/L 0.0512 1.15%

Zn 206.200 23388.9 4.510 mg/L 0.0140 4.510 mg/L 0.0140 0.31%Ba 233.527 -2.0 0.000 mg/L 0.0014 0.000 mg/L 0.0014 348.31%

Cu 327.393 89.5 0.001 mg/L 0.0006 0.001 mg/L 0.0006 45.84%

Fe 238.204 41.4 0.006 mg/L 0.0020 0.006 mg/L 0.0020 35.73%

V 290.880 6.6 0.003 mg/L 0.0014 0.003 mg/L 0.0014 56.84%

Co 228.616 3.5 0.001 mg/L 0.0002 0.001 mg/L 0.0002 31.13%

As 188.979 2.1 -0.001 mg/L 0.0099 -0.001 mg/L 0.0099 >999.9%

Mo 202.031 16.0 0.002 mg/L 0.0011 0.002 mg/L 0.0011 63.70%

Sr 407.771 1050.4 0.001 mg/L 0.0000 0.001 mg/L 0.0000 6.29%

Li 670.784 -153.2 0.001 mg/L 0.0016 0.001 mg/L 0.0016 298.49%

Sn 189.927 0.9 -0.000 mg/L 0.0024 -0.000 mg/L 0.0024 632.60%

Ti 334.940 119.9 0.001 mg/L 0.0003 0.001 mg/L 0.0003 33.14%

Ca 317.933 2639.4 0.105 mg/L 0.0008 0.105 mg/L 0.0008 0.79%

Na 589.592 3690.2 0.269 mg/L 0.0089 0.269 mg/L 0.0089 3.32%

K 766.490 135.4 0.074 mg/L 0.0344 0.074 mg/L 0.0344 46.30%Cr 267.716 -80.0 -0.000 mg/L 0.0000 -0.000 mg/L 0.0000 28.03%

Ni 231.604 86.4 0.002 mg/L 0.0006 0.002 mg/L 0.0006 24.12%

Al 396.153 8.4 0.015 mg/L 0.0086 0.015 mg/L 0.0086 59.10%

Mg 285.213 377.7 0.015 mg/L 0.0004 0.015 mg/L 0.0004 2.97%

Ag 328.068 316928.6 1.789 mg/L 0.0108 1.789 mg/L 0.0108 0.60%

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B 249.677 -5484.1 0.121 mg/L 0.0015 0.121 mg/L 0.0015 1.28%

Sb 206.836 1.5 0.000 mg/L 0.0049 0.000 mg/L 0.0049 >999.9%

Tl 190.801 -57.7 -0.031 mg/L 0.0050 -0.031 mg/L 0.0050 16.11%

====================================================================================================

Sequence No.: 38 Autosampler Location: 39Sample ID: STD 90% MIX 1 Date Collected: 28/12/2015 11:07:25 a.m.Analyst: Data Type: Reprocessed on 28/12/2015 02:21:41 p.m.Logged In Analyst (Original) : AdministratorInitial Sample Wt: Initial Sample Vol:


----------------------------------------------------------------------------------------------------



Be 313.107 1894321.4 4.488 mg/L 0.0320 4.488 mg/L 0.0320 0.71%

Cd 228.802 141073.3 4.558 mg/L 0.0108 4.558 mg/L 0.0108 0.24%

Pb 220.353 26542.7 4.575 mg/L 0.0054 4.575 mg/L 0.0054 0.12%

Se 196.026 6212.4 4.479 mg/L 0.0151 4.479 mg/L 0.0151 0.34%

Zn 206.200 23506.0 4.533 mg/L 0.0451 4.533 mg/L 0.0451 1.00%

Ba 233.527 -4.6 0.000 mg/L 0.0006 0.000 mg/L 0.0006 627.99%

Cu 327.393 268.6 0.003 mg/L 0.0007 0.003 mg/L 0.0007 24.95%

Fe 238.204 79.4 0.011 mg/L 0.0076 0.011 mg/L 0.0076 68.91%

V 290.880 -8.4 0.001 mg/L 0.0011 0.001 mg/L 0.0011 83.01%

Co 228.616 -0.5 0.000 mg/L 0.0002 0.000 mg/L 0.0002 55.65%

As 188.979 -2.4 -0.005 mg/L 0.0043 -0.005 mg/L 0.0043 88.66%

Mo 202.031 6.6 0.001 mg/L 0.0013 0.001 mg/L 0.0013 123.40%

Sr 407.771 986.6 0.001 mg/L 0.0000 0.001 mg/L 0.0000 6.90%

Li 670.784 -205.7 0.000 mg/L 0.0006 0.000 mg/L 0.0006 387.22%

Sn 189.927 2.4 -0.000 mg/L 0.0031 -0.000 mg/L 0.0031 >999.9%

Ti 334.940 115.2 0.001 mg/L 0.0005 0.001 mg/L 0.0005 61.55%

Ca 317.933 2782.6 0.111 mg/L 0.0016 0.111 mg/L 0.0016 1.49%

Na 589.592 3373.9 0.247 mg/L 0.0105 0.247 mg/L 0.0105 4.27%

K 766.490 197.1 0.093 mg/L 0.0277 0.093 mg/L 0.0277 29.82%

Cr 267.716 -96.8 -0.000 mg/L 0.0001 -0.000 mg/L 0.0001 44.92%

Ni 231.604 80.8 0.002 mg/L 0.0009 0.002 mg/L 0.0009 42.71%

Al 396.153 60.1 0.021 mg/L 0.0070 0.021 mg/L 0.0070 32.81%Mg 285.213 365.7 0.014 mg/L 0.0008 0.014 mg/L 0.0008 5.40%

Ag 328.068 320000.3 1.806 mg/L 0.0039 1.806 mg/L 0.0039 0.22%

B 249.677 -5513.1 0.120 mg/L 0.0044 0.120 mg/L 0.0044 3.69%

Sb 206.836 4.9 0.002 mg/L 0.0040 0.002 mg/L 0.0040 224.39%

Tl 190.801 -66.1 -0.035 mg/L 0.0072 -0.035 mg/L 0.0072 20.43%

====================================================================================================


----------------------------------------------------------------------------------------------------



Be 313.107 1877963.6 4.449 mg/L 0.0088 4.449 mg/L 0.0088 0.20%

Cd 228.802 140047.8 4.525 mg/L 0.0380 4.525 mg/L 0.0380 0.84%

Pb 220.353 26294.7 4.532 mg/L 0.0605 4.532 mg/L 0.0605 1.33%

Se 196.026 6186.0 4.460 mg/L 0.0243 4.460 mg/L 0.0243 0.54%

Zn 206.200 23523.7 4.536 mg/L 0.0231 4.536 mg/L 0.0231 0.51%

Ba 233.527 5.0 0.001 mg/L 0.0012 0.001 mg/L 0.0012 94.47%

Cu 327.393 132.3 0.002 mg/L 0.0002 0.002 mg/L 0.0002 13.99%

Fe 238.204 57.7 0.008 mg/L 0.0036 0.008 mg/L 0.0036 44.99%

V 290.880 -16.7 0.001 mg/L 0.0010 0.001 mg/L 0.0010 168.41%Co 228.616 3.2 0.000 mg/L 0.0008 0.000 mg/L 0.0008 159.58%

As 188.979 5.4 0.002 mg/L 0.0090 0.002 mg/L 0.0090 433.59%

Mo 202.031 4.0 0.001 mg/L 0.0007 0.001 mg/L 0.0007 80.72%

Sr 407.771 891.4 0.000 mg/L 0.0000 0.000 mg/L 0.0000 3.99%

Li 670.784 -109.8 0.001 mg/L 0.0016 0.001 mg/L 0.0016 190.91%

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Sn 189.927 -3.9 -0.001 mg/L 0.0028 -0.001 mg/L 0.0028 215.95%

Ti 334.940 99.4 0.001 mg/L 0.0004 0.001 mg/L 0.0004 54.82%

Ca 317.933 2741.9 0.109 mg/L 0.0003 0.109 mg/L 0.0003 0.25%

Na 589.592 3376.5 0.247 mg/L 0.0038 0.247 mg/L 0.0038 1.55%

K 766.490 259.9 0.112 mg/L 0.0294 0.112 mg/L 0.0294 26.29%

Cr 267.716 -87.8 -0.000 mg/L 0.0000 -0.000 mg/L 0.0000 13.74%

Ni 231.604 93.3 0.003 mg/L 0.0005 0.003 mg/L 0.0005 20.13%

Al 396.153 37.6 0.018 mg/L 0.0164 0.018 mg/L 0.0164 89.11%

Mg 285.213 367.0 0.014 mg/L 0.0016 0.014 mg/L 0.0016 11.20%

Ag 328.068 317767.8 1.794 mg/L 0.0135 1.794 mg/L 0.0135 0.75%

B 249.677 -6248.3 0.103 mg/L 0.0073 0.103 mg/L 0.0073 7.15%Sb 206.836 9.2 0.003 mg/L 0.0078 0.003 mg/L 0.0078 225.51%

Tl 190.801 -57.0 -0.031 mg/L 0.0032 -0.031 mg/L 0.0032 10.31%

====================================================================================================


----------------------------------------------------------------------------------------------------

Mean Data: STD 90% MIX 1

Mean Corrected Calib. SampleAnalyte Intensity Conc. Units Std.Dev. Conc. Units Std.Dev. RSDMn 257.610 300804.1 4.507 mg/L 0.0223 4.507 mg/L 0.0223 0.50%

Be 313.107 1894088.4 4.488 mg/L 0.0278 4.488 mg/L 0.0278 0.62%

Cd 228.802 139868.6 4.519 mg/L 0.0299 4.519 mg/L 0.0299 0.66%

Pb 220.353 26221.9 4.519 mg/L 0.0296 4.519 mg/L 0.0296 0.66%

Se 196.026 6158.8 4.440 mg/L 0.0386 4.440 mg/L 0.0386 0.87%

Zn 206.200 23535.4 4.538 mg/L 0.0269 4.538 mg/L 0.0269 0.59%

Ba 233.527 -3.6 0.000 mg/L 0.0017 0.000 mg/L 0.0017 798.26%

Cu 327.393 232.9 0.002 mg/L 0.0008 0.002 mg/L 0.0008 30.84%

Fe 238.204 59.6 0.008 mg/L 0.0022 0.008 mg/L 0.0022 26.29%

V 290.880 -16.5 0.001 mg/L 0.0008 0.001 mg/L 0.0008 128.67%

Co 228.616 -3.4 0.000 mg/L 0.0011 0.000 mg/L 0.0011 476.27%

As 188.979 -0.5 -0.003 mg/L 0.0124 -0.003 mg/L 0.0124 387.77%

Mo 202.031 6.6 0.001 mg/L 0.0013 0.001 mg/L 0.0013 124.63%Sr 407.771 933.3 0.000 mg/L 0.0000 0.000 mg/L 0.0000 2.49%

Li 670.784 -162.2 0.000 mg/L 0.0011 0.000 mg/L 0.0011 229.73%

Sn 189.927 -1.4 -0.001 mg/L 0.0013 -0.001 mg/L 0.0013 162.21%

Ti 334.940 90.1 0.001 mg/L 0.0003 0.001 mg/L 0.0003 51.92%

Ca 317.933 2780.5 0.110 mg/L 0.0005 0.110 mg/L 0.0005 0.41%

Na 589.592 3524.2 0.258 mg/L 0.0048 0.258 mg/L 0.0048 1.85%

K 766.490 232.4 0.103 mg/L 0.0037 0.103 mg/L 0.0037 3.60%

Cr 267.716 -90.5 -0.000 mg/L 0.0000 -0.000 mg/L 0.0000 31.20%

Ni 231.604 88.5 0.002 mg/L 0.0003 0.002 mg/L 0.0003 12.99%

Al 396.153 -6.7 0.013 mg/L 0.0220 0.013 mg/L 0.0220 175.03%

Mg 285.213 382.3 0.015 mg/L 0.0009 0.015 mg/L 0.0009 6.09%

Ag 328.068 317416.3 1.792 mg/L 0.0118 1.792 mg/L 0.0118 0.66%

B 249.677 -6471.2 0.097 mg/L 0.0051 0.097 mg/L 0.0051 5.25%

Sb 206.836 1.5 0.000 mg/L 0.0042 0.000 mg/L 0.0042 995.74%

Tl 190.801 -66.0 -0.035 mg/L 0.0059 -0.035 mg/L 0.0059 16.94%

====================================================================================================


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Analyte Intensity Conc. Units Std.Dev. Conc. Units Std.Dev. RSDMn 257.610 301302.4 4.514 mg/L 0.0229 4.514 mg/L 0.0229 0.51%Be 313.107 1901331.6 4.505 mg/L 0.0440 4.505 mg/L 0.0440 0.98%

Cd 228.802 141474.7 4.571 mg/L 0.0167 4.571 mg/L 0.0167 0.37%

Pb 220.353 26680.5 4.598 mg/L 0.0211 4.598 mg/L 0.0211 0.46%

Se 196.026 6224.2 4.487 mg/L 0.0075 4.487 mg/L 0.0075 0.17%

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Zn 206.200 23577.7 4.547 mg/L 0.0262 4.547 mg/L 0.0262 0.58%

Ba 233.527 -2.8 0.000 mg/L 0.0002 0.000 mg/L 0.0002 78.22%

Cu 327.393 163.5 0.002 mg/L 0.0008 0.002 mg/L 0.0008 42.22%

Fe 238.204 68.8 0.010 mg/L 0.0043 0.010 mg/L 0.0043 45.68%

V 290.880 8.7 0.003 mg/L 0.0010 0.003 mg/L 0.0010 39.16%

Co 228.616 15.4 0.001 mg/L 0.0011 0.001 mg/L 0.0011 105.14%

As 188.979 7.5 0.004 mg/L 0.0074 0.004 mg/L 0.0074 188.00%

Mo 202.031 2.5 0.001 mg/L 0.0011 0.001 mg/L 0.0011 148.63%

Sr 407.771 993.1 0.001 mg/L 0.0001 0.001 mg/L 0.0001 12.24%

Li 670.784 -249.1 -0.000 mg/L 0.0006 -0.000 mg/L 0.0006 417.50%

Sn 189.927 -3.3 -0.001 mg/L 0.0029 -0.001 mg/L 0.0029 243.98%Ti 334.940 313.6 0.003 mg/L 0.0027 0.003 mg/L 0.0027 81.14%

Ca 317.933 2726.5 0.108 mg/L 0.0011 0.108 mg/L 0.0011 0.98%

Na 589.592 3520.4 0.257 mg/L 0.0096 0.257 mg/L 0.0096 3.75%

K 766.490 151.8 0.079 mg/L 0.0164 0.079 mg/L 0.0164 20.74%

Cr 267.716 -81.2 -0.000 mg/L 0.0000 -0.000 mg/L 0.0000 29.54%

Ni 231.604 112.2 0.003 mg/L 0.0002 0.003 mg/L 0.0002 7.59%

Al 396.153 8.4 0.015 mg/L 0.0018 0.015 mg/L 0.0018 12.14%

Mg 285.213 393.5 0.016 mg/L 0.0017 0.016 mg/L 0.0017 10.86%

Ag 328.068 320257.2 1.808 mg/L 0.0082 1.808 mg/L 0.0082 0.45%

B 249.677 -6812.0 0.089 mg/L 0.0085 0.089 mg/L 0.0085 9.57%

Sb 206.836 2.5 0.001 mg/L 0.0065 0.001 mg/L 0.0065 806.64%

Tl 190.801 -64.9 -0.035 mg/L 0.0045 -0.035 mg/L 0.0045 13.00%

====================================================================================================


----------------------------------------------------------------------------------------------------



Be 313.107 1898748.6 4.499 mg/L 0.0385 4.499 mg/L 0.0385 0.86%

Cd 228.802 139934.1 4.521 mg/L 0.0269 4.521 mg/L 0.0269 0.60%Pb 220.353 26240.0 4.522 mg/L 0.0306 4.522 mg/L 0.0306 0.68%

Se 196.026 6181.7 4.457 mg/L 0.0169 4.457 mg/L 0.0169 0.38%

Zn 206.200 23960.8 4.620 mg/L 0.0076 4.620 mg/L 0.0076 0.16%

Ba 233.527 -6.6 -0.000 mg/L 0.0018 -0.000 mg/L 0.0018 >999.9%

Cu 327.393 114.6 0.002 mg/L 0.0004 0.002 mg/L 0.0004 27.98%

Fe 238.204 75.3 0.010 mg/L 0.0019 0.010 mg/L 0.0019 18.23%

V 290.880 9.6 0.003 mg/L 0.0010 0.003 mg/L 0.0010 35.90%

Co 228.616 -0.3 0.000 mg/L 0.0010 0.000 mg/L 0.0010 294.91%

As 188.979 -6.5 -0.009 mg/L 0.0023 -0.009 mg/L 0.0023 26.97%

Mo 202.031 18.2 0.002 mg/L 0.0015 0.002 mg/L 0.0015 75.48%

Sr 407.771 854.3 0.000 mg/L 0.0001 0.000 mg/L 0.0001 11.70%

Li 670.784 -286.6 -0.000 mg/L 0.0004 -0.000 mg/L 0.0004 97.43%

Sn 189.927 -6.1 -0.002 mg/L 0.0025 -0.002 mg/L 0.0025 146.02%

Ti 334.940 91.8 0.001 mg/L 0.0004 0.001 mg/L 0.0004 67.29%

Ca 317.933 2670.1 0.106 mg/L 0.0010 0.106 mg/L 0.0010 0.90%Na 589.592 3417.1 0.250 mg/L 0.0144 0.250 mg/L 0.0144 5.75%

K 766.490 111.0 0.067 mg/L 0.0278 0.067 mg/L 0.0278 41.56%

Cr 267.716 -76.0 -0.000 mg/L 0.0000 -0.000 mg/L 0.0000 28.91%

Ni 231.604 112.5 0.003 mg/L 0.0007 0.003 mg/L 0.0007 23.01%

Al 396.153 -12.3 0.012 mg/L 0.0061 0.012 mg/L 0.0061 51.98%

Mg 285.213 376.5 0.015 mg/L 0.0002 0.015 mg/L 0.0002 1.65%

Ag 328.068 317099.0 1.790 mg/L 0.0097 1.790 mg/L 0.0097 0.54%

B 249.677 -6746.8 0.091 mg/L 0.0041 0.091 mg/L 0.0041 4.58%

Sb 206.836 17.3 0.007 mg/L 0.0022 0.007 mg/L 0.0022 33.36%

Tl 190.801 -66.0 -0.035 mg/L 0.0039 -0.035 mg/L 0.0039 11.11%

====================================================================================================

Sequence No.: 43 Autosampler Location: 40

Sample ID: STD 90% MIX 1 Date Collected: 28/12/2015 11:18:15 a.m.Analyst: Data Type: Reprocessed on 28/12/2015 02:21:43 p.m.Logged In Analyst (Original) : AdministratorInitial Sample Wt: Initial Sample Vol:Dilution: Sample Prep Vol:Wash Time:

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Be 313.107 1893722.5 4.487 mg/L 0.0303 4.487 mg/L 0.0303 0.67%

Cd 228.802 139023.2 4.491 mg/L 0.0267 4.491 mg/L 0.0267 0.59%

Pb 220.353 26082.1 4.495 mg/L 0.0216 4.495 mg/L 0.0216 0.48%

Se 196.026 6177.7 4.454 mg/L 0.0267 4.454 mg/L 0.0267 0.60%

Zn 206.200 23448.1 4.522 mg/L 0.0293 4.522 mg/L 0.0293 0.65%Ba 233.527 0.2 0.001 mg/L 0.0012 0.001 mg/L 0.0012 186.05%

Cu 327.393 220.7 0.002 mg/L 0.0006 0.002 mg/L 0.0006 26.95%

Fe 238.204 56.2 0.008 mg/L 0.0014 0.008 mg/L 0.0014 17.91%

V 290.880 -35.5 -0.001 mg/L 0.0013 -0.001 mg/L 0.0013 144.59%

Co 228.616 8.5 0.001 mg/L 0.0005 0.001 mg/L 0.0005 67.08%

As 188.979 -1.7 -0.004 mg/L 0.0063 -0.004 mg/L 0.0063 149.34%

Mo 202.031 22.6 0.002 mg/L 0.0014 0.002 mg/L 0.0014 61.35%

Sr 407.771 914.2 0.000 mg/L 0.0000 0.000 mg/L 0.0000 3.60%

Li 670.784 -349.6 -0.001 mg/L 0.0004 -0.001 mg/L 0.0004 42.50%

Sn 189.927 -1.8 -0.001 mg/L 0.0012 -0.001 mg/L 0.0012 134.55%

Ti 334.940 84.3 0.000 mg/L 0.0007 0.000 mg/L 0.0007 148.31%

Ca 317.933 2616.6 0.104 mg/L 0.0003 0.104 mg/L 0.0003 0.29%

Na 589.592 3266.2 0.240 mg/L 0.0074 0.240 mg/L 0.0074 3.10%

K 766.490 168.5 0.084 mg/L 0.0407 0.084 mg/L 0.0407 48.32%

Cr 267.716 -84.1 -0.000 mg/L 0.0001 -0.000 mg/L 0.0001 120.31%

Ni 231.604 105.1 0.003 mg/L 0.0014 0.003 mg/L 0.0014 48.54%

Al 396.153 56.6 0.021 mg/L 0.0044 0.021 mg/L 0.0044 21.27%

Mg 285.213 386.6 0.015 mg/L 0.0016 0.015 mg/L 0.0016 10.21%

Ag 328.068 315966.2 1.783 mg/L 0.0104 1.783 mg/L 0.0104 0.58%

B 249.677 -6862.8 0.088 mg/L 0.0095 0.088 mg/L 0.0095 10.79%

Sb 206.836 9.0 0.003 mg/L 0.0052 0.003 mg/L 0.0052 151.24%

Tl 190.801 -60.1 -0.032 mg/L 0.0104 -0.032 mg/L 0.0104 32.45%

====================================================================================================

Sequence No.: 44 Autosampler Location: 40Sample ID: STD 90% MIX 1 Date Collected: 28/12/2015 11:20:21 a.m.Analyst: Data Type: Reprocessed on 28/12/2015 02:21:43 p.m.Logged In Analyst (Original) : Administrator

Initial Sample Wt: Initial Sample Vol:Dilution: Sample Prep Vol:Wash Time:

----------------------------------------------------------------------------------------------------



Be 313.107 1870064.5 4.431 mg/L 0.0616 4.431 mg/L 0.0616 1.39%

Cd 228.802 138989.0 4.490 mg/L 0.0187 4.490 mg/L 0.0187 0.42%

Pb 220.353 25963.1 4.475 mg/L 0.0151 4.475 mg/L 0.0151 0.34%

Se 196.026 6117.2 4.410 mg/L 0.0169 4.410 mg/L 0.0169 0.38%

Zn 206.200 23444.0 4.521 mg/L 0.0201 4.521 mg/L 0.0201 0.45%

Ba 233.527 1.7 0.001 mg/L 0.0011 0.001 mg/L 0.0011 134.97%

Cu 327.393 84.0 0.001 mg/L 0.0006 0.001 mg/L 0.0006 42.59%Fe 238.204 66.8 0.009 mg/L 0.0044 0.009 mg/L 0.0044 47.47%

V 290.880 5.8 0.002 mg/L 0.0013 0.002 mg/L 0.0013 54.34%

Co 228.616 6.5 0.001 mg/L 0.0002 0.001 mg/L 0.0002 36.08%

As 188.979 -3.2 -0.006 mg/L 0.0175 -0.006 mg/L 0.0175 310.93%

Mo 202.031 15.2 0.002 mg/L 0.0010 0.002 mg/L 0.0010 58.94%

Sr 407.771 975.5 0.000 mg/L 0.0000 0.000 mg/L 0.0000 8.32%

Li 670.784 -176.3 0.000 mg/L 0.0012 0.000 mg/L 0.0012 318.80%

Sn 189.927 10.6 0.001 mg/L 0.0012 0.001 mg/L 0.0012 84.92%

Ti 334.940 87.6 0.001 mg/L 0.0001 0.001 mg/L 0.0001 25.73%

Ca 317.933 2687.6 0.107 mg/L 0.0009 0.107 mg/L 0.0009 0.87%

Na 589.592 3489.8 0.255 mg/L 0.0022 0.255 mg/L 0.0022 0.88%

K 766.490 66.6 0.054 mg/L 0.0308 0.054 mg/L 0.0308 57.45%

Cr 267.716 -111.7 -0.000 mg/L 0.0000 -0.000 mg/L 0.0000 5.77%

Ni 231.604 90.6 0.002 mg/L 0.0001 0.002 mg/L 0.0001 4.90%Al 396.153 55.0 0.021 mg/L 0.0139 0.021 mg/L 0.0139 67.28%

Mg 285.213 398.8 0.016 mg/L 0.0011 0.016 mg/L 0.0011 7.08%

Ag 328.068 315743.4 1.782 mg/L 0.0060 1.782 mg/L 0.0060 0.34%

B 249.677 -6853.6 0.088 mg/L 0.0034 0.088 mg/L 0.0034 3.87%

Sb 206.836 -5.8 -0.002 mg/L 0.0064 -0.002 mg/L 0.0064 255.21%

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Tl 190.801 -59.7 -0.032 mg/L 0.0034 -0.032 mg/L 0.0034 10.50%

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Be 313.107 1875641.7 4.444 mg/L 0.0381 4.444 mg/L 0.0381 0.86%

Cd 228.802 138185.6 4.464 mg/L 0.0090 4.464 mg/L 0.0090 0.20%

Pb 220.353 25797.0 4.446 mg/L 0.0256 4.446 mg/L 0.0256 0.58%

Se 196.026 6115.6 4.409 mg/L 0.0217 4.409 mg/L 0.0217 0.49%

Zn 206.200 23356.9 4.504 mg/L 0.0571 4.504 mg/L 0.0571 1.27%

Ba 233.527 -12.3 -0.001 mg/L 0.0009 -0.001 mg/L 0.0009 109.97%

Cu 327.393 26.9 0.001 mg/L 0.0006 0.001 mg/L 0.0006 71.17%

Fe 238.204 77.4 0.011 mg/L 0.0035 0.011 mg/L 0.0035 32.43%

V 290.880 -0.1 0.002 mg/L 0.0023 0.002 mg/L 0.0023 115.95%

Co 228.616 -10.3 -0.000 mg/L 0.0006 -0.000 mg/L 0.0006 >999.9%

As 188.979 7.9 0.004 mg/L 0.0148 0.004 mg/L 0.0148 344.17%

Mo 202.031 8.4 0.001 mg/L 0.0011 0.001 mg/L 0.0011 94.05%

Sr 407.771 1026.5 0.001 mg/L 0.0000 0.001 mg/L 0.0000 3.90%

Li 670.784 -226.9 0.000 mg/L 0.0005 0.000 mg/L 0.0005 >999.9%

Sn 189.927 15.7 0.002 mg/L 0.0006 0.002 mg/L 0.0006 25.03%

Ti 334.940 140.6 0.001 mg/L 0.0005 0.001 mg/L 0.0005 40.01%

Ca 317.933 2636.3 0.105 mg/L 0.0025 0.105 mg/L 0.0025 2.38%

Na 589.592 3334.4 0.244 mg/L 0.0102 0.244 mg/L 0.0102 4.19%

K 766.490 70.7 0.055 mg/L 0.0261 0.055 mg/L 0.0261 47.58%

Cr 267.716 -118.1 -0.000 mg/L 0.0000 -0.000 mg/L 0.0000 25.35%

Ni 231.604 89.5 0.002 mg/L 0.0002 0.002 mg/L 0.0002 10.01%

Al 396.153 37.5 0.018 mg/L 0.0132 0.018 mg/L 0.0132 71.85%

Mg 285.213 399.0 0.016 mg/L 0.0016 0.016 mg/L 0.0016 10.03%

Ag 328.068 314108.8 1.773 mg/L 0.0049 1.773 mg/L 0.0049 0.27%B 249.677 -7573.8 0.071 mg/L 0.0021 0.071 mg/L 0.0021 3.01%

Sb 206.836 3.8 0.001 mg/L 0.0050 0.001 mg/L 0.0050 369.85%

Tl 190.801 -62.2 -0.033 mg/L 0.0045 -0.033 mg/L 0.0045 13.64%

====================================================================================================

Sequence No.: 46 Autosampler Location: 0Sample ID: lavado Date Collected: 28/12/2015 11:24:34 a.m.Analyst: Data Type: Reprocessed on 28/12/2015 02:21:44 p.m.Logged In Analyst (Original) : AdministratorInitial Sample Wt: Initial Sample Vol:Dilution: Sample Prep Vol:Wash Time:

----------------------------------------------------------------------------------------------------

Mean Data: lavadoMean Corrected Calib. Sample


Be 313.107 4430.4 0.011 mg/L 0.0002 0.011 mg/L 0.0002 2.32%

Cd 228.802 477.6 0.015 mg/L 0.0007 0.015 mg/L 0.0007 4.46%

Pb 220.353 52.8 0.015 mg/L 0.0038 0.015 mg/L 0.0038 25.08%

Se 196.026 41.2 0.021 mg/L 0.0250 0.021 mg/L 0.0250 121.81%

Zn 206.200 56.0 0.010 mg/L 0.0006 0.010 mg/L 0.0006 6.01%

Ba 233.527 9.0 0.002 mg/L 0.0002 0.002 mg/L 0.0002 11.94%

Cu 327.393 106.1 0.002 mg/L 0.0001 0.002 mg/L 0.0001 5.83%

Fe 238.204 19.1 0.002 mg/L 0.0006 0.002 mg/L 0.0006 25.88%

V 290.880 -2.3 0.002 mg/L 0.0010 0.002 mg/L 0.0010 58.84%

Co 228.616 29.1 0.002 mg/L 0.0002 0.002 mg/L 0.0002 14.56%

As 188.979 6.7 0.003 mg/L 0.0045 0.003 mg/L 0.0045 136.29%Mo 202.031 19.2 0.002 mg/L 0.0018 0.002 mg/L 0.0018 88.12%

Sr 407.771 1949.6 0.001 mg/L 0.0000 0.001 mg/L 0.0000 5.15%

Li 670.784 -102.6 0.001 mg/L 0.0007 0.001 mg/L 0.0007 73.27%

Sn 189.927 3.4 0.000 mg/L 0.0015 0.000 mg/L 0.0015 >999.9%

Ti 334.940 105.4 0.001 mg/L 0.0002 0.001 mg/L 0.0002 22.91%

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Ca 317.933 232.7 0.010 mg/L 0.0012 0.010 mg/L 0.0012 12.38%

Na 589.592 111.4 0.019 mg/L 0.0045 0.019 mg/L 0.0045 24.15%

K 766.490 6.1 0.036 mg/L 0.0224 0.036 mg/L 0.0224 63.14%

Cr 267.716 505.9 0.001 mg/L 0.0000 0.001 mg/L 0.0000 2.67%

Ni 231.604 112.6 0.003 mg/L 0.0009 0.003 mg/L 0.0009 29.22%

Al 396.153 -9.7 0.012 mg/L 0.0044 0.012 mg/L 0.0044 36.57%

Mg 285.213 255.3 0.010 mg/L 0.0004 0.010 mg/L 0.0004 4.54%

Ag 328.068 1294.9 0.007 mg/L 0.0001 0.007 mg/L 0.0001 1.95%

B 249.677 -11304.3 -0.019 mg/L 0.0038 -0.019 mg/L 0.0038 20.01%

Sb 206.836 11.6 0.004 mg/L 0.0044 0.004 mg/L 0.0044 99.76%

Tl 190.801 6.8 0.001 mg/L 0.0034 0.001 mg/L 0.0034 386.54%

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Be 313.107 -129.6 -0.000 mg/L 0.0000 -0.000 mg/L 0.0000 5.73%

Cd 228.802 -922.2 -0.031 mg/L 0.0004 -0.031 mg/L 0.0004 1.47%

Pb 220.353 35.9 0.012 mg/L 0.0015 0.012 mg/L 0.0015 12.11%

Se 196.026 -164.5 -0.128 mg/L 0.0131 -0.128 mg/L 0.0131 10.22%

Zn 206.200 36.4 0.007 mg/L 0.0018 0.007 mg/L 0.0018 27.64%

Ba 233.527 37685.5 4.465 mg/L 0.0166 4.465 mg/L 0.0166 0.37%

Cu 327.393 578733.9 4.421 mg/L 0.0553 4.421 mg/L 0.0553 1.25%

Fe 238.204 61808.6 8.895 mg/L 0.0395 8.895 mg/L 0.0395 0.44%

V 290.880 55118.5 4.478 mg/L 0.0113 4.478 mg/L 0.0113 0.25%

Co 228.616 108303.5 4.466 mg/L 0.0653 4.466 mg/L 0.0653 1.46%

As 188.979 -1.2 -0.004 mg/L 0.0034 -0.004 mg/L 0.0034 87.51%

Mo 202.031 -21.4 -0.001 mg/L 0.0004 -0.001 mg/L 0.0004 38.31%

Sr 407.771 1056.9 0.001 mg/L 0.0000 0.001 mg/L 0.0000 2.92%

Li 670.784 -531.0 -0.002 mg/L 0.0013 -0.002 mg/L 0.0013 58.48%Sn 189.927 13.3 0.002 mg/L 0.0017 0.002 mg/L 0.0017 88.20%

Ti 334.940 63.2 0.000 mg/L 0.0005 0.000 mg/L 0.0005 196.41%

Ca 317.933 3184.7 0.126 mg/L 0.0013 0.126 mg/L 0.0013 1.00%

Na 589.592 5393.5 0.389 mg/L 0.0120 0.389 mg/L 0.0120 3.09%

K 766.490 201.7 0.094 mg/L 0.0285 0.094 mg/L 0.0285 30.24%

Cr 267.716 -633.8 -0.001 mg/L 0.0001 -0.001 m

STD 90% parte 1

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Transcript of STD 90% parte 1