SPECTRUM ANALYTICAL, INC. HANIBAL TECHNOLOGY … · 2011. 12. 15. · Sample Identification S52-VMP...

Laboratory Report

Report Date: 16-Oct-08 14:43

Final Report

Revised Report

Re-Issued Report

Chesapeake GeoSciences, Inc.

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ü

SPECTRUM ANALYTICAL, INC.Featuring

HANIBAL TECHNOLOGY

Project:

Project

Riggs Park VIS-NE Washington, DC

CG-07-0282

Laboratory ID Client Sample ID Matrix Date Sampled Date ReceivedContainer

15-Sep-08 15:3010-Sep-08 09:15AirSA84560-01 S52-VMP Summa canister

15-Sep-08 15:3010-Sep-08 09:32AirSA84560-02 S395-GMP Summa canister

15-Sep-08 15:3010-Sep-08 09:41AirSA84560-03 S389-GMPRR Summa canister




15-Sep-08 15:3010-Sep-08 11:12AirSA84560-07 S354-GMPR Summa canister



15-Sep-08 15:3010-Sep-08 13:14AirSA84560-10 S130-GMPR2 Summa canister

15-Sep-08 15:3010-Sep-08 13:24AirSA84560-11 S130-VMP1 Summa canister












15-Sep-08 15:3012-Sep-08 10:02AirSA84560-23 S373-INA Summa canister



15-Sep-08 15:3012-Sep-08 10:26AirSA84560-26 S373-AOA Summa canister










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Case Narrative:

In order to report data to the Method Detection Limit (MDL) the format of the report has replaced data presented in the Result Units

column with alternative data when the target analyte is not present above the Reportable Detection Limit (RDL). If the target analyte is

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* Reportable Detection Limit BRL = Below Reporting Limit of 97

Sample IdentificationS52-VMP

Matrix10-Sep-08 09:15

Collection Date/Time Received15-Sep-08

Client Project #CG-07-0282 Air

SA84560-01

Analyte(s) Result Units *RDL AnalyzedMethod Ref. Cert.Batch*RDLResult ug/m³CAS No. Flag

Air Quality Analyses

APH Targets ppbv Prepared 16-Sep-08

Naphthalene Modified MA APH 16-Sep-08 8091255< 5.24 12.60< 1.00 2.4091-20-3 U

EPA TO-15 SIM ppbv Prepared 16-Sep-08

Propene EPA TO-15 " "< 0.10 0.17< 0.056395 0.10000115-07-1 U

Dichlorodifluoromethane (Freon12) " " "2.62 0.490.53000 0.1000075-71-8

Chloromethane " " "< 0.15 0.21< 0.072377 0.1000074-87-3 U X

1,2-Dichlorotetrafluoroethane (Freon 114) " " "< 0.38 0.70< 0.053850 0.1000076-14-2 U

Vinyl chloride " " "< 0.08 0.26< 0.031300 0.1000075-01-4 U X

1,3-Butadiene " " "< 0.10 0.22< 0.046885 0.10000106-99-0 U X

Bromomethane " " "< 0.23 0.39< 0.059621 0.1000074-83-9 U X

Chloroethane " " "< 0.11 0.26< 0.042158 0.1000075-00-3 U X

Acetone " " "5.28 1.192.2200 0.5000067-64-1

Trichlorofluoromethane (Freon 11) " " "2.19 0.560.39000 0.1000075-69-4

Ethanol " " "< 0.20 0.94< 0.10462 0.5000064-17-5 U

1,1-Dichloroethene " " "< 0.11 0.40< 0.028198 0.1000075-35-4 U X

Acrylonitrile " " "< 0.03 0.59< 0.014000 0.27300107-13-1 U

Methylene chloride " " "< 0.10 0.35< 0.028198 0.1000075-09-2 U X

1,1,2-Trichlorotrifluoroethane (Freon 113) " " "0.61 0.770.080000 0.1000076-13-1 J

Carbon disulfide " " "< 0.09 1.56< 0.029810 0.5000075-15-0 U X

trans-1,2-Dichloroethene " " "< 0.07 0.40< 0.016752 0.10000156-60-5 U X

1,1-Dichloroethane " " "< 0.10 0.40< 0.023691 0.1000075-34-3 U X

Methyl tert-butyl ether " " "< 0.15 0.36< 0.042158 0.100001634-04-4 U X

Isopropyl alcohol " " "< 0.21 1.23< 0.084869 0.5000067-63-0 U

2-Butanone (MEK) " " "2.71 0.290.92000 0.1000078-93-3 X

cis-1,2-Dichloroethene " " "< 0.09 0.40< 0.021627 0.10000156-59-2 U X

Hexane " " "< 0.06 0.35< 0.016752 0.10000110-54-3 U X

Ethyl acetate " " "< 0.17 0.36< 0.045877 0.10000141-78-6 U

Chloroform " " "0.78 0.490.16000 0.1000067-66-3 X

Tetrahydrofuran " " "< 0.17 0.29< 0.056395 0.10000109-99-9 U


1,1,1-Trichloroethane " " "< 0.14 0.55< 0.025589 0.1000071-55-6 U

Benzene " " "0.32 0.320.10000 0.1000071-43-2 X

Carbon tetrachloride " " "1.01 0.630.16000 0.1000056-23-5 X

Cyclohexane " " "< 0.08 0.34< 0.024658 0.10000110-82-7 U

1,2-Dichloropropane " " "< 0.18 0.46< 0.039287 0.1000078-87-5 U X

Bromodichloromethane " " "< 0.18 0.67< 0.026200 0.1000075-27-4 U

Trichloroethene " " "< 0.16 0.54< 0.029810 0.1000079-01-6 U X

1,4-Dioxane " " "< 1.25 1.25< 0.34600 0.34600123-91-1 U

n-Heptane " " "< 0.17 0.41< 0.042158 0.10000142-82-5 U

4-Methyl-2-pentanone (MIBK) " " "< 0.34 0.41< 0.083760 0.10000108-10-1 U X

cis-1,3-Dichloropropene " " "< 0.14 0.45< 0.031300 0.1000010061-01-5 U X

trans-1,3-Dichloropropene " " "< 0.08 0.45< 0.017200 0.1000010061-02-6 U X

1,1,2-Trichloroethane " " "< 0.19 0.55< 0.035536 0.1000079-00-5 U X

Toluene " " "1.13 0.380.30000 0.10000108-88-3 X

2-Hexanone (MBK) " " "0.78 0.410.19000 0.10000591-78-6

Dibromochloromethane " " "< 0.20 0.85< 0.023691 0.10000124-48-1 U

1,2-Dibromoethane (EDB) " " "< 0.20 0.77< 0.026200 0.10000106-93-4 U X

Tetrachloroethene " " "4.00 0.680.59000 0.10000127-18-4 X

Chlorobenzene " " "< 0.22 0.46< 0.046885 0.10000108-90-7 U X

Ethylbenzene " " "< 0.29 0.43< 0.067702 0.10000100-41-4 U X

1,1,1,2-Tetrachloroethane " " "< 0.12 1.46< 0.017000 0.21200630-20-6 U

m,p-Xylene " " "0.69 0.430.16000 0.10000179601-23-1 X







SA84560-01




Bromoform EPA TO-15 16-Sep-08 8091255< 0.14 1.03< 0.014000 0.1000075-25-2 U X

Styrene " " "< 0.30 0.43< 0.069408 0.10000100-42-5 U X

o-Xylene " " "< 0.32 0.43< 0.073340 0.1000095-47-6 U X

1,1,2,2-Tetrachloroethane " " "< 0.12 0.69< 0.017200 0.1000079-34-5 U X

1,3,5-Trimethylbenzene " " "< 0.43 0.49< 0.086507 0.10000108-67-8 U

4-Ethyltoluene " " "< 0.44 0.49< 0.088643 0.10000622-96-8 U

1,2,4-Trimethylbenzene " " "0.44 0.490.090000 0.1000095-63-6 J

Isopropylbenzene " " "< 0.13 0.74< 0.026000 0.1500098-82-8 U

1,3-Dichlorobenzene " " "< 0.42 0.60< 0.070078 0.10000541-73-1 U X

Benzyl chloride " " "< 0.40 0.52< 0.078574 0.10000100-44-7 U X



1,2,4-Trichlorobenzene " " "< 0.71 0.74< 0.095501 0.10000120-82-1 U X

Hexachlorobutadiene " " "< 0.81 1.07< 0.075539 0.1000087-68-3 U X

sec-Butylbenzene " " "< 0.14 0.80< 0.026000 0.14500135-98-8 U

4-Isopropyltoluene " " "< 0.09 0.65< 0.017000 0.1210099-87-6 U

n-Butylbenzene " " "< 0.14 0.68< 0.026000 0.12300104-51-8 U

Surrogate recoveries:

70-130 %984-Bromofluorobenzene " " "460-00-4

Total Volatile Hydrocarbons C5-C12 ppmv Prepared 16-Sep-08

Total Volatile Hydrocarbons C5-C12 Mod. EPA TO-15 " "0.0254





Sample IdentificationS395-GMP




SA84560-02





EPA TO-15 ppbv Prepared 17-Sep-08

Propene EPA TO-15 " "3.94 0.862.29 0.500115-07-1

Dichlorodifluoromethane (Freon12) " " "2.23 2.470.450 0.50075-71-8 J




1,3-Butadiene " " "< 0.41 1.10< 0.186 0.500106-99-0 U X

Bromomethane " " "< 0.58 1.94< 0.149 0.50074-83-9 U X

Chloroethane " " "< 0.42 1.32< 0.158 0.50075-00-3 U X

Acetone " " "385.00 1.19162 0.50067-64-1 E

Trichlorofluoromethane (Freon 11) " " "1.46 2.810.260 0.50075-69-4 J

Ethanol " " "12.40 0.946.57 0.50064-17-5

Acrylonitrile " " "< 0.59 1.08< 0.273 0.500107-13-1 U



1,1,2-Trichlorotrifluoroethane (Freon 113) " " "< 1.33 3.83< 0.174 0.50076-13-1 U

Carbon disulfide " " "2.68 1.560.860 0.50075-15-0 X




Isopropyl alcohol " " "1.60 1.230.650 0.50067-63-0

2-Butanone (MEK) " " "23.10 1.477.85 0.50078-93-3 X


Hexane " " "< 0.33 1.76< 0.0923 0.500110-54-3 U X

Ethyl acetate " " "64.90 1.8018.0 0.500141-78-6

Chloroform " " "6.38 2.431.31 0.50067-66-3 X




Benzene " " "< 0.40 1.60< 0.124 0.50071-43-2 U X

Carbon tetrachloride " " "< 1.39 3.15< 0.221 0.50056-23-5 U X

Cyclohexane " " "< 0.39 1.72< 0.113 0.500110-82-7 U




1,4-Dioxane " " "< 1.25 1.80< 0.346 0.500123-91-1 U

n-Heptane " " "< 0.45 2.05< 0.111 0.500142-82-5 U





Toluene " " "2.82 1.880.750 0.500108-88-3 X

2-Hexanone (MBK) " " "4.71 2.051.15 0.500591-78-6



Tetrachloroethene " " "< 0.97 3.39< 0.143 0.500127-18-4 U X



Ethylbenzene " " "< 0.61 2.17< 0.141 0.500100-41-4 U X

m,p-Xylene " " "1.34 4.340.310 1.00179601-23-1 J X







SA84560-02





Styrene " " "< 0.68 2.13< 0.159 0.500100-42-5 U X

o-Xylene " " "< 0.50 2.17< 0.116 0.50095-47-6 U X




4-Ethyltoluene " " "< 0.58 2.46< 0.117 0.500622-96-8 U




1,4-Dichlorobenzene " " "1.98 3.010.330 0.500106-46-7 J X




n-Butylbenzene " " "< 0.68 2.74< 0.123 0.500104-51-8 U











Sample IdentificationS389-GMPRR




SA84560-03






Propene EPA TO-15 " "6.95 0.864.04 0.500115-07-1





1,3-Butadiene " " "< 0.41 1.10< 0.186 0.500106-99-0 U X

Bromomethane " " "< 0.58 1.94< 0.149 0.50074-83-9 U X

Chloroethane " " "< 0.42 1.32< 0.158 0.50075-00-3 U X

Acetone " " "288.00 1.19121 0.50067-64-1 E


Ethanol " " "14.70 0.947.80 0.50064-17-5

Acrylonitrile " " "< 0.59 1.08< 0.273 0.500107-13-1 U









2-Butanone (MEK) " " "18.00 1.476.10 0.50078-93-3 X


Hexane " " "0.88 1.760.250 0.500110-54-3 J X

Ethyl acetate " " "57.30 1.8015.9 0.500141-78-6

Chloroform " " "3.99 2.430.820 0.50067-66-3 X




Benzene " " "< 0.40 1.60< 0.124 0.50071-43-2 U X


Cyclohexane " " "< 0.39 1.72< 0.113 0.500110-82-7 U




1,4-Dioxane " " "< 1.25 1.80< 0.346 0.500123-91-1 U

n-Heptane " " "< 0.45 2.05< 0.111 0.500142-82-5 U




1,1,2-Trichloroethane " " "4.15 2.730.760 0.50079-00-5 X

Toluene " " "2.52 1.880.670 0.500108-88-3 X

2-Hexanone (MBK) " " "3.28 2.050.800 0.500591-78-6






Ethylbenzene " " "< 0.61 2.17< 0.141 0.500100-41-4 U X

m,p-Xylene " " "1.47 4.340.340 1.00179601-23-1 J X







SA84560-03





Styrene " " "< 0.68 2.13< 0.159 0.500100-42-5 U X

o-Xylene " " "1.73 2.170.400 0.50095-47-6 J X



1,3,5-Trimethylbenzene " " "4.97 2.461.01 0.500108-67-8

4-Ethyltoluene " " "19.80 2.464.03 0.500622-96-8





sec-Butylbenzene " " "4.01 2.740.730 0.500135-98-8

4-Isopropyltoluene " " "5.80 2.681.08 0.50099-87-6


n-Butylbenzene " " "< 0.68 2.74< 0.123 0.500104-51-8 U















SA84560-04






Propene EPA TO-15 " "16.50 1.729.56 1.00115-07-1

Dichlorodifluoromethane (Freon12) " " "< 1.07 4.94< 0.216 1.0075-71-8 U




1,3-Butadiene " " "< 0.82 2.21< 0.372 1.00106-99-0 U X

Bromomethane " " "< 1.16 3.88< 0.298 1.0074-83-9 U X

Chloroethane " " "< 0.83 2.64< 0.316 1.0075-00-3 U X

Acetone " " "787.00 2.38331 1.0067-64-1 E

Trichlorofluoromethane (Freon 11) " " "< 2.21 5.62< 0.394 1.0075-69-4 U

Ethanol " " "26.40 1.8914.0 1.0064-17-5

Acrylonitrile " " "< 1.18 2.17< 0.546 1.00107-13-1 U









2-Butanone (MEK) " " "33.60 2.9511.4 1.0078-93-3 X


Hexane " " "< 0.65 3.53< 0.185 1.00110-54-3 U X

Ethyl acetate " " "59.10 3.6016.4 1.00141-78-6

Chloroform " " "3.02 4.870.620 1.0067-66-3 J X




Benzene " " "< 0.79 3.19< 0.248 1.0071-43-2 U X


Cyclohexane " " "< 0.78 3.44< 0.226 1.00110-82-7 U




1,4-Dioxane " " "< 2.49 3.60< 0.692 1.00123-91-1 U

n-Heptane " " "4.51 4.101.10 1.00142-82-5





Toluene " " "4.52 3.761.20 1.00108-88-3 X

2-Hexanone (MBK) " " "5.49 4.101.34 1.00591-78-6






Ethylbenzene " " "< 1.22 4.34< 0.282 1.00100-41-4 U X

m,p-Xylene " " "< 2.13 8.67< 0.492 2.00179601-23-1 U X







SA84560-04





Styrene " " "< 1.35 4.25< 0.318 1.00100-42-5 U X

o-Xylene " " "< 1.01 4.34< 0.232 1.0095-47-6 U X




4-Ethyltoluene " " "9.34 4.921.90 1.00622-96-8








n-Butylbenzene " " "< 1.35 5.49< 0.246 1.00104-51-8 U















SA84560-05






Propene EPA TO-15 " "0.60 0.860.350 0.500115-07-1 J





1,3-Butadiene " " "< 0.41 1.10< 0.186 0.500106-99-0 U X

Bromomethane " " "< 0.58 1.94< 0.149 0.50074-83-9 U X

Chloroethane " " "< 0.42 1.32< 0.158 0.50075-00-3 U X

Acetone " " "15.40 1.196.46 0.50067-64-1


Ethanol " " "7.77 0.944.12 0.50064-17-5

Acrylonitrile " " "0.69 1.080.320 0.500107-13-1 J









2-Butanone (MEK) " " "3.13 1.471.06 0.50078-93-3 X


Hexane " " "< 0.33 1.76< 0.0923 0.500110-54-3 U X

Ethyl acetate " " "1.44 1.800.400 0.500141-78-6 J

Chloroform " " "1.36 2.430.280 0.50067-66-3 J X




Benzene " " "< 0.40 1.60< 0.124 0.50071-43-2 U X


Cyclohexane " " "< 0.39 1.72< 0.113 0.500110-82-7 U



Trichloroethene " " "3.44 2.690.640 0.50079-01-6 X

1,4-Dioxane " " "< 1.25 1.80< 0.346 0.500123-91-1 U

n-Heptane " " "< 0.45 2.05< 0.111 0.500142-82-5 U


cis-1,3-Dichloropropene " " "1.50 2.270.330 0.50010061-01-5 J X

trans-1,3-Dichloropropene " " "2.63 2.270.580 0.50010061-02-6 X


Toluene " " "1.99 1.880.530 0.500108-88-3 X

2-Hexanone (MBK) " " "2.70 2.050.660 0.500591-78-6


1,2-Dibromoethane (EDB) " " "4.46 3.840.580 0.500106-93-4 X


Chlorobenzene " " "2.44 2.300.530 0.500108-90-7 X


Ethylbenzene " " "1.08 2.170.250 0.500100-41-4 J X

m,p-Xylene " " "3.47 4.340.800 1.00179601-23-1 J X







SA84560-05





Styrene " " "3.36 2.130.790 0.500100-42-5 X

o-Xylene " " "< 0.50 2.17< 0.116 0.50095-47-6 U X




4-Ethyltoluene " " "< 0.58 2.46< 0.117 0.500622-96-8 U


1,3-Dichlorobenzene " " "5.59 3.010.930 0.500541-73-1 X




4-Isopropyltoluene " " "1.77 2.680.330 0.50099-87-6 J

1,2-Dichlorobenzene " " "3.49 3.010.580 0.50095-50-1 Z-2 X

n-Butylbenzene " " "4.88 2.740.890 0.500104-51-8

1,2,4-Trichlorobenzene " " "6.53 3.710.880 0.500120-82-1 Z-2 X














SA84560-06






Propene EPA TO-15 " "< 0.10 0.17< 0.056395 0.10000115-07-1 U





1,3-Butadiene " " "< 0.10 0.22< 0.046885 0.10000106-99-0 U X

Bromomethane " " "< 0.23 0.39< 0.059621 0.1000074-83-9 U X

Chloroethane " " "< 0.11 0.26< 0.042158 0.1000075-00-3 U X

Acetone " " "30.30 1.1912.760 0.5000067-64-1 E


Ethanol " " "8.43 0.944.4700 0.5000064-17-5


Acrylonitrile " " "< 0.03 0.59< 0.014000 0.27300107-13-1 U








2-Butanone (MEK) " " "1.89 0.290.64000 0.1000078-93-3 X


Hexane " " "< 0.06 0.35< 0.016752 0.10000110-54-3 U X

Ethyl acetate " " "< 0.17 0.36< 0.045877 0.10000141-78-6 U

Chloroform " " "3.84 0.490.79000 0.1000067-66-3 X




Benzene " " "< 0.05 0.32< 0.016752 0.1000071-43-2 U X


Cyclohexane " " "< 0.08 0.34< 0.024658 0.10000110-82-7 U




1,4-Dioxane " " "< 1.25 1.25< 0.34600 0.34600123-91-1 U

n-Heptane " " "< 0.17 0.41< 0.042158 0.10000142-82-5 U





Toluene " " "0.56 0.380.15000 0.10000108-88-3 X

2-Hexanone (MBK) " " "< 0.37 0.41< 0.089952 0.10000591-78-6 U





Ethylbenzene " " "< 0.29 0.43< 0.067702 0.10000100-41-4 U X


m,p-Xylene " " "< 0.29 0.43< 0.067356 0.10000179601-23-1 U X







SA84560-06





Styrene " " "< 0.30 0.43< 0.069408 0.10000100-42-5 U X

o-Xylene " " "< 0.32 0.43< 0.073340 0.1000095-47-6 U X



4-Ethyltoluene " " "< 0.44 0.49< 0.088643 0.10000622-96-8 U











n-Butylbenzene " " "< 0.14 0.68< 0.026000 0.12300104-51-8 U









Sample IdentificationS354-GMPR




SA84560-07






Propene EPA TO-15 " "1.70 0.860.990 0.500115-07-1





1,3-Butadiene " " "< 0.41 1.10< 0.186 0.500106-99-0 U X

Bromomethane " " "< 0.58 1.94< 0.149 0.50074-83-9 U X

Chloroethane " " "< 0.42 1.32< 0.158 0.50075-00-3 U X

Acetone " " "132.00 1.1955.6 0.50067-64-1


Ethanol " " "6.66 0.943.53 0.50064-17-5

Acrylonitrile " " "< 0.59 1.08< 0.273 0.500107-13-1 U









2-Butanone (MEK) " " "3.63 1.471.23 0.50078-93-3 X


Hexane " " "< 0.33 1.76< 0.0923 0.500110-54-3 U X

Ethyl acetate " " "< 0.55 1.80< 0.154 0.500141-78-6 U

Chloroform " " "1.22 2.430.250 0.50067-66-3 J X




Benzene " " "< 0.40 1.60< 0.124 0.50071-43-2 U X


Cyclohexane " " "< 0.39 1.72< 0.113 0.500110-82-7 U




1,4-Dioxane " " "< 1.25 1.80< 0.346 0.500123-91-1 U

n-Heptane " " "< 0.45 2.05< 0.111 0.500142-82-5 U





Toluene " " "< 0.46 1.88< 0.122 0.500108-88-3 U X

2-Hexanone (MBK) " " "< 1.18 2.05< 0.289 0.500591-78-6 U






Ethylbenzene " " "< 0.61 2.17< 0.141 0.500100-41-4 U X

m,p-Xylene " " "< 1.07 4.34< 0.246 1.00179601-23-1 U X







SA84560-07





Styrene " " "< 0.68 2.13< 0.159 0.500100-42-5 U X

o-Xylene " " "< 0.50 2.17< 0.116 0.50095-47-6 U X




4-Ethyltoluene " " "< 0.58 2.46< 0.117 0.500622-96-8 U








n-Butylbenzene " " "< 0.68 2.74< 0.123 0.500104-51-8 U















SA84560-08






Propene EPA TO-15 " "< 0.10 0.17< 0.056395 0.10000115-07-1 U





1,3-Butadiene " " "< 0.10 0.22< 0.046885 0.10000106-99-0 U X

Bromomethane " " "< 0.23 0.39< 0.059621 0.1000074-83-9 U X

Chloroethane " " "< 0.11 0.26< 0.042158 0.1000075-00-3 U X

Acetone " " "7.32 1.193.0800 0.5000067-64-1


Ethanol " " "11.00 0.945.8500 0.5000064-17-5


Acrylonitrile " " "< 0.03 0.59< 0.014000 0.27300107-13-1 U



Carbon disulfide " " "0.28 1.560.090000 0.5000075-15-0 J X





2-Butanone (MEK) " " "4.22 0.291.4300 0.1000078-93-3 X


Hexane " " "1.20 0.350.34000 0.10000110-54-3 X

Ethyl acetate " " "< 0.17 0.36< 0.045877 0.10000141-78-6 U

Chloroform " " "1.51 0.490.31000 0.1000067-66-3 X




Benzene " " "0.32 0.320.10000 0.1000071-43-2 X


Cyclohexane " " "1.17 0.340.34000 0.10000110-82-7




1,4-Dioxane " " "< 1.25 1.25< 0.34600 0.34600123-91-1 U

n-Heptane " " "6.43 0.411.5700 0.10000142-82-5





Toluene " " "9.18 0.382.4400 0.10000108-88-3 X

2-Hexanone (MBK) " " "< 0.37 0.41< 0.089952 0.10000591-78-6 U





Ethylbenzene " " "< 0.29 0.43< 0.067702 0.10000100-41-4 U X


m,p-Xylene " " "0.48 0.430.11000 0.10000179601-23-1 X







SA84560-08





Styrene " " "< 0.30 0.43< 0.069408 0.10000100-42-5 U X

o-Xylene " " "< 0.32 0.43< 0.073340 0.1000095-47-6 U X



4-Ethyltoluene " " "< 0.44 0.49< 0.088643 0.10000622-96-8 U











n-Butylbenzene " " "< 0.14 0.68< 0.026000 0.12300104-51-8 U













SA84560-09






Propene EPA TO-15 " "< 0.10 0.17< 0.056395 0.10000115-07-1 U





1,3-Butadiene " " "< 0.10 0.22< 0.046885 0.10000106-99-0 U X

Bromomethane " " "< 0.23 0.39< 0.059621 0.1000074-83-9 U X

Chloroethane " " "< 0.11 0.26< 0.042158 0.1000075-00-3 U X

Acetone " " "3.68 1.191.5500 0.5000067-64-1


Ethanol " " "< 0.20 0.94< 0.10462 0.5000064-17-5 U


Acrylonitrile " " "< 0.03 0.59< 0.014000 0.27300107-13-1 U








2-Butanone (MEK) " " "1.24 0.290.42000 0.1000078-93-3 X


Hexane " " "< 0.06 0.35< 0.016752 0.10000110-54-3 U X

Ethyl acetate " " "< 0.17 0.36< 0.045877 0.10000141-78-6 U

Chloroform " " "0.78 0.490.16000 0.1000067-66-3 X




Benzene " " "< 0.05 0.32< 0.016752 0.1000071-43-2 U X


Cyclohexane " " "< 0.08 0.34< 0.024658 0.10000110-82-7 U




1,4-Dioxane " " "< 1.25 1.25< 0.34600 0.34600123-91-1 U

n-Heptane " " "0.37 0.410.090000 0.10000142-82-5 J





Toluene " " "1.13 0.380.30000 0.10000108-88-3 X

2-Hexanone (MBK) " " "< 0.37 0.41< 0.089952 0.10000591-78-6 U





Ethylbenzene " " "< 0.29 0.43< 0.067702 0.10000100-41-4 U X


m,p-Xylene " " "0.61 0.430.14000 0.10000179601-23-1 X







SA84560-09





Styrene " " "< 0.30 0.43< 0.069408 0.10000100-42-5 U X

o-Xylene " " "< 0.32 0.43< 0.073340 0.1000095-47-6 U X



4-Ethyltoluene " " "< 0.44 0.49< 0.088643 0.10000622-96-8 U











n-Butylbenzene " " "< 0.14 0.68< 0.026000 0.12300104-51-8 U









Sample IdentificationS130-GMPR2




SA84560-10






Propene EPA TO-15 " "0.89 0.860.520 0.500115-07-1





1,3-Butadiene " " "< 0.41 1.10< 0.186 0.500106-99-0 U X

Bromomethane " " "< 0.58 1.94< 0.149 0.50074-83-9 U X

Chloroethane " " "< 0.42 1.32< 0.158 0.50075-00-3 U X

Acetone " " "79.80 1.1933.6 0.50067-64-1


Ethanol " " "3.22 0.941.71 0.50064-17-5

Acrylonitrile " " "< 0.59 1.08< 0.273 0.500107-13-1 U









2-Butanone (MEK) " " "1.98 1.470.670 0.50078-93-3 X


Hexane " " "< 0.33 1.76< 0.0923 0.500110-54-3 U X

Ethyl acetate " " "< 0.55 1.80< 0.154 0.500141-78-6 U

Chloroform " " "< 1.08 2.43< 0.221 0.50067-66-3 U X




Benzene " " "< 0.40 1.60< 0.124 0.50071-43-2 U X


Cyclohexane " " "< 0.39 1.72< 0.113 0.500110-82-7 U




1,4-Dioxane " " "< 1.25 1.80< 0.346 0.500123-91-1 U

n-Heptane " " "< 0.45 2.05< 0.111 0.500142-82-5 U





Toluene " " "< 0.46 1.88< 0.122 0.500108-88-3 U X

2-Hexanone (MBK) " " "< 1.18 2.05< 0.289 0.500591-78-6 U






Ethylbenzene " " "< 0.61 2.17< 0.141 0.500100-41-4 U X

m,p-Xylene " " "< 1.07 4.34< 0.246 1.00179601-23-1 U X



Sample IdentificationS130-GMPR2




SA84560-10





Styrene " " "< 0.68 2.13< 0.159 0.500100-42-5 U X

o-Xylene " " "< 0.50 2.17< 0.116 0.50095-47-6 U X




4-Ethyltoluene " " "< 0.58 2.46< 0.117 0.500622-96-8 U








n-Butylbenzene " " "< 0.68 2.74< 0.123 0.500104-51-8 U











Sample IdentificationS130-VMP1




SA84560-11






Propene EPA TO-15 " "< 0.10 0.17< 0.056395 0.10000115-07-1 U



1,2-Dichlorotetrafluoroethane (Freon 114) " " "2.38 0.700.34000 0.1000076-14-2


1,3-Butadiene " " "< 0.10 0.22< 0.046885 0.10000106-99-0 U X

Bromomethane " " "< 0.23 0.39< 0.059621 0.1000074-83-9 U X

Chloroethane " " "< 0.11 0.26< 0.042158 0.1000075-00-3 U X

Acetone " " "13.30 1.195.6000 0.5000067-64-1


Ethanol " " "8.07 0.944.2800 0.5000064-17-5


Acrylonitrile " " "< 0.03 0.59< 0.014000 0.27300107-13-1 U







Isopropyl alcohol " " "0.81 1.230.33000 0.5000067-63-0 J

2-Butanone (MEK) " " "3.83 0.291.3000 0.1000078-93-3 X


Hexane " " "< 0.06 0.35< 0.016752 0.10000110-54-3 U X

Ethyl acetate " " "< 0.17 0.36< 0.045877 0.10000141-78-6 U

Chloroform " " "< 0.15 0.49< 0.029810 0.1000067-66-3 U X



1,1,1-Trichloroethane " " "0.93 0.550.17000 0.1000071-55-6

Benzene " " "0.32 0.320.10000 0.1000071-43-2 X


Cyclohexane " " "< 0.08 0.34< 0.024658 0.10000110-82-7 U




1,4-Dioxane " " "13.70 1.253.8000 0.34600123-91-1

n-Heptane " " "< 0.17 0.41< 0.042158 0.10000142-82-5 U





Toluene " " "0.87 0.380.23000 0.10000108-88-3 X

2-Hexanone (MBK) " " "0.90 0.410.22000 0.10000591-78-6





Ethylbenzene " " "< 0.29 0.43< 0.067702 0.10000100-41-4 U X


m,p-Xylene " " "< 0.29 0.43< 0.067356 0.10000179601-23-1 U X







SA84560-11





Styrene " " "< 0.30 0.43< 0.069408 0.10000100-42-5 U X

o-Xylene " " "< 0.32 0.43< 0.073340 0.1000095-47-6 U X



4-Ethyltoluene " " "< 0.44 0.49< 0.088643 0.10000622-96-8 U











n-Butylbenzene " " "< 0.14 0.68< 0.026000 0.12300104-51-8 U













SA84560-12






Propene EPA TO-15 " "< 0.10 0.17< 0.056395 0.10000115-07-1 U



1,2-Dichlorotetrafluoroethane (Freon 114) " " "1.68 0.700.24000 0.1000076-14-2


1,3-Butadiene " " "< 0.10 0.22< 0.046885 0.10000106-99-0 U X

Bromomethane " " "< 0.23 0.39< 0.059621 0.1000074-83-9 U X

Chloroethane " " "< 0.11 0.26< 0.042158 0.1000075-00-3 U X

Acetone " " "4.61 1.191.9400 0.5000067-64-1


Ethanol " " "1.00 0.940.53000 0.5000064-17-5


Acrylonitrile " " "< 0.03 0.59< 0.014000 0.27300107-13-1 U








2-Butanone (MEK) " " "1.47 0.290.50000 0.1000078-93-3 X


Hexane " " "< 0.06 0.35< 0.016752 0.10000110-54-3 U X

Ethyl acetate " " "0.47 0.360.13000 0.10000141-78-6

Chloroform " " "< 0.15 0.49< 0.029810 0.1000067-66-3 U X




Benzene " " "0.29 0.320.090000 0.1000071-43-2 J X


Cyclohexane " " "< 0.08 0.34< 0.024658 0.10000110-82-7 U




1,4-Dioxane " " "< 1.25 1.25< 0.34600 0.34600123-91-1 U

n-Heptane " " "< 0.17 0.41< 0.042158 0.10000142-82-5 U





Toluene " " "1.47 0.380.39000 0.10000108-88-3 X

2-Hexanone (MBK) " " "< 0.37 0.41< 0.089952 0.10000591-78-6 U





Ethylbenzene " " "< 0.29 0.43< 0.067702 0.10000100-41-4 U X


m,p-Xylene " " "0.74 0.430.17000 0.10000179601-23-1 X







SA84560-12





Styrene " " "< 0.30 0.43< 0.069408 0.10000100-42-5 U X

o-Xylene " " "< 0.32 0.43< 0.073340 0.1000095-47-6 U X



4-Ethyltoluene " " "< 0.44 0.49< 0.088643 0.10000622-96-8 U











n-Butylbenzene " " "< 0.14 0.68< 0.026000 0.12300104-51-8 U













SA84560-13






Propene EPA TO-15 " "3.77 0.862.19 0.500115-07-1





1,3-Butadiene " " "< 0.41 1.10< 0.186 0.500106-99-0 U X

Bromomethane " " "< 0.58 1.94< 0.149 0.50074-83-9 U X

Chloroethane " " "< 0.42 1.32< 0.158 0.50075-00-3 U X

Acetone " " "304.00 1.19128 0.50067-64-1 E


Ethanol " " "5.20 0.942.76 0.50064-17-5

Acrylonitrile " " "< 0.59 1.08< 0.273 0.500107-13-1 U









2-Butanone (MEK) " " "6.43 1.472.18 0.50078-93-3 X


Hexane " " "< 0.33 1.76< 0.0923 0.500110-54-3 U X

Ethyl acetate " " "< 0.55 1.80< 0.154 0.500141-78-6 U

Chloroform " " "8.13 2.431.67 0.50067-66-3 X




Benzene " " "< 0.40 1.60< 0.124 0.50071-43-2 U X


Cyclohexane " " "< 0.39 1.72< 0.113 0.500110-82-7 U




1,4-Dioxane " " "< 1.25 1.80< 0.346 0.500123-91-1 U

n-Heptane " " "< 0.45 2.05< 0.111 0.500142-82-5 U




1,1,2-Trichloroethane " " "1.42 2.730.260 0.50079-00-5 J X

Toluene " " "< 0.46 1.88< 0.122 0.500108-88-3 U X

2-Hexanone (MBK) " " "< 1.18 2.05< 0.289 0.500591-78-6 U



Tetrachloroethene " " "2.03 3.390.300 0.500127-18-4 J X



Ethylbenzene " " "< 0.61 2.17< 0.141 0.500100-41-4 U X

m,p-Xylene " " "< 1.07 4.34< 0.246 1.00179601-23-1 U X







SA84560-13





Styrene " " "< 0.68 2.13< 0.159 0.500100-42-5 U X

o-Xylene " " "< 0.50 2.17< 0.116 0.50095-47-6 U X




4-Ethyltoluene " " "< 0.58 2.46< 0.117 0.500622-96-8 U








n-Butylbenzene " " "< 0.68 2.74< 0.123 0.500104-51-8 U















SA84560-14






Propene EPA TO-15 " "5.65 1.723.28 1.00115-07-1





1,3-Butadiene " " "< 0.82 2.21< 0.372 1.00106-99-0 U X

Bromomethane " " "< 1.16 3.88< 0.298 1.0074-83-9 U X

Chloroethane " " "< 0.83 2.64< 0.316 1.0075-00-3 U X

Acetone " " "152.00 2.3863.9 1.0067-64-1


Ethanol " " "< 0.66 1.89< 0.352 1.0064-17-5 U

Acrylonitrile " " "< 1.18 2.17< 0.546 1.00107-13-1 U









2-Butanone (MEK) " " "7.79 2.952.64 1.0078-93-3 X


Hexane " " "< 0.65 3.53< 0.185 1.00110-54-3 U X

Ethyl acetate " " "< 1.11 3.60< 0.308 1.00141-78-6 U

Chloroform " " "< 2.15 4.87< 0.442 1.0067-66-3 U X




Benzene " " "< 0.79 3.19< 0.248 1.0071-43-2 U X


Cyclohexane " " "< 0.78 3.44< 0.226 1.00110-82-7 U




1,4-Dioxane " " "< 2.49 3.60< 0.692 1.00123-91-1 U

n-Heptane " " "< 0.91 4.10< 0.222 1.00142-82-5 U





Toluene " " "< 0.92 3.76< 0.244 1.00108-88-3 U X

2-Hexanone (MBK) " " "< 2.37 4.10< 0.578 1.00591-78-6 U






Ethylbenzene " " "< 1.22 4.34< 0.282 1.00100-41-4 U X

m,p-Xylene " " "< 2.13 8.67< 0.492 2.00179601-23-1 U X







SA84560-14





Styrene " " "< 1.35 4.25< 0.318 1.00100-42-5 U X

o-Xylene " " "< 1.01 4.34< 0.232 1.0095-47-6 U X




4-Ethyltoluene " " "12.60 4.922.56 1.00622-96-8








n-Butylbenzene " " "< 1.35 5.49< 0.246 1.00104-51-8 U















SA84560-15






Propene EPA TO-15 " "3.30 3.441.92 2.00115-07-1 J





1,3-Butadiene " " "< 1.64 4.42< 0.744 2.00106-99-0 U X

Bromomethane " " "< 2.31 7.76< 0.596 2.0074-83-9 U X

Chloroethane " " "< 1.67 5.28< 0.632 2.0075-00-3 U X

Acetone " " "154.00 4.7564.6 2.0067-64-1


Ethanol " " "10.90 3.775.80 2.0064-17-5

Acrylonitrile " " "< 2.36 4.34< 1.09 2.00107-13-1 U









2-Butanone (MEK) " " "8.26 5.902.80 2.0078-93-3 X


Hexane " " "< 1.30 7.05< 0.369 2.00110-54-3 U X

Ethyl acetate " " "< 2.22 7.21< 0.616 2.00141-78-6 U

Chloroform " " "< 4.30 9.70< 0.884 2.0067-66-3 U X




Benzene " " "< 1.58 6.38< 0.496 2.0071-43-2 U X


Cyclohexane " " "< 1.56 6.88< 0.452 2.00110-82-7 U




1,4-Dioxane " " "< 4.97 7.20< 1.38 2.00123-91-1 U

n-Heptane " " "< 1.82 8.20< 0.444 2.00142-82-5 U





Toluene " " "< 1.84 7.53< 0.488 2.00108-88-3 U X

2-Hexanone (MBK) " " "< 4.75 8.20< 1.16 2.00591-78-6 U






Ethylbenzene " " "< 2.45 8.67< 0.564 2.00100-41-4 U X

m,p-Xylene " " "< 4.27 17.30< 0.984 4.00179601-23-1 U X







SA84560-15





Styrene " " "< 2.71 8.51< 0.636 2.00100-42-5 U X

o-Xylene " " "< 2.01 8.67< 0.464 2.0095-47-6 U X




4-Ethyltoluene " " "5.70 9.801.16 2.00622-96-8 J








n-Butylbenzene " " "< 2.70 11.00< 0.492 2.00104-51-8 U















SA84560-16






Propene EPA TO-15 " "< 0.10 0.17< 0.056395 0.10000115-07-1 U





1,3-Butadiene " " "< 0.10 0.22< 0.046885 0.10000106-99-0 U X

Bromomethane " " "< 0.23 0.39< 0.059621 0.1000074-83-9 U X

Chloroethane " " "< 0.11 0.26< 0.042158 0.1000075-00-3 U X

Acetone " " "7.13 1.193.0000 0.5000067-64-1


Ethanol " " "15.70 0.948.3400 0.5000064-17-5


Acrylonitrile " " "< 0.03 0.59< 0.014000 0.27300107-13-1 U

Methylene chloride " " "4.55 0.351.3100 0.1000075-09-2 X







2-Butanone (MEK) " " "1.71 0.290.58000 0.1000078-93-3 X


Hexane " " "1.90 0.350.54000 0.10000110-54-3 X

Ethyl acetate " " "< 0.17 0.36< 0.045877 0.10000141-78-6 U

Chloroform " " "0.68 0.490.14000 0.1000067-66-3 X




Benzene " " "0.26 0.320.080000 0.1000071-43-2 J X


Cyclohexane " " "0.45 0.340.13000 0.10000110-82-7




1,4-Dioxane " " "< 1.25 1.25< 0.34600 0.34600123-91-1 U

n-Heptane " " "2.05 0.410.50000 0.10000142-82-5





Toluene " " "3.24 0.380.86000 0.10000108-88-3 X

2-Hexanone (MBK) " " "< 0.37 0.41< 0.089952 0.10000591-78-6 U





Ethylbenzene " " "< 0.29 0.43< 0.067702 0.10000100-41-4 U X


m,p-Xylene " " "0.43 0.430.10000 0.10000179601-23-1 X







SA84560-16





Styrene " " "< 0.30 0.43< 0.069408 0.10000100-42-5 U X

o-Xylene " " "< 0.32 0.43< 0.073340 0.1000095-47-6 U X



4-Ethyltoluene " " "< 0.44 0.49< 0.088643 0.10000622-96-8 U











n-Butylbenzene " " "< 0.14 0.68< 0.026000 0.12300104-51-8 U













SA84560-17






Tetrachloroethene EPA TO-15 19-Sep-08 8091570542.00 3.3979.9 0.500127-18-4 X




Propene " 18-Sep-08 8091468< 0.10 0.17< 0.056395 0.10000115-07-1 U





1,3-Butadiene " " "< 0.10 0.22< 0.046885 0.10000106-99-0 U X

Bromomethane " " "< 0.23 0.39< 0.059621 0.1000074-83-9 U X

Chloroethane " " "< 0.11 0.26< 0.042158 0.1000075-00-3 U X

Acetone " " "1.40 1.190.59000 0.5000067-64-1


Ethanol " " "< 0.20 0.94< 0.10462 0.5000064-17-5 U


Acrylonitrile " " "< 0.03 0.59< 0.014000 0.27300107-13-1 U








2-Butanone (MEK) " " "1.00 0.290.34000 0.1000078-93-3 X


Hexane " " "0.49 0.350.14000 0.10000110-54-3 X

Ethyl acetate " " "6.59 0.361.8300 0.10000141-78-6

Chloroform " " "< 0.15 0.49< 0.029810 0.1000067-66-3 U X




Benzene " " "< 0.05 0.32< 0.016752 0.1000071-43-2 U X


Cyclohexane " " "< 0.08 0.34< 0.024658 0.10000110-82-7 U




1,4-Dioxane " " "< 1.25 1.25< 0.34600 0.34600123-91-1 U

n-Heptane " " "0.45 0.410.11000 0.10000142-82-5





Toluene " " "1.24 0.380.33000 0.10000108-88-3 X

2-Hexanone (MBK) " " "< 0.37 0.41< 0.089952 0.10000591-78-6 U



Tetrachloroethene " " "300.00 0.6844.310 0.10000127-18-4 E X







SA84560-17




Chlorobenzene EPA TO-15 18-Sep-08 8091468< 0.22 0.46< 0.046885 0.10000108-90-7 U X

Ethylbenzene " " "< 0.29 0.43< 0.067702 0.10000100-41-4 U X


m,p-Xylene " " "< 0.29 0.43< 0.067356 0.10000179601-23-1 U X

Bromoform " " "< 0.14 1.03< 0.014000 0.1000075-25-2 U X

Styrene " " "< 0.30 0.43< 0.069408 0.10000100-42-5 U X

o-Xylene " " "< 0.32 0.43< 0.073340 0.1000095-47-6 U X



4-Ethyltoluene " " "< 0.44 0.49< 0.088643 0.10000622-96-8 U











n-Butylbenzene " " "< 0.14 0.68< 0.026000 0.12300104-51-8 U













SA84560-18






Tetrachloroethene EPA TO-15 19-Sep-08 8091570207.00 3.3930.5 0.500127-18-4 X




Propene " 18-Sep-08 8091468< 0.10 0.17< 0.056395 0.10000115-07-1 U





1,3-Butadiene " " "< 0.10 0.22< 0.046885 0.10000106-99-0 U X

Bromomethane " " "< 0.23 0.39< 0.059621 0.1000074-83-9 U X

Chloroethane " " "< 0.11 0.26< 0.042158 0.1000075-00-3 U X

Acetone " " "6.11 1.192.5700 0.5000067-64-1


Ethanol " " "< 0.20 0.94< 0.10462 0.5000064-17-5 U


Acrylonitrile " " "< 0.03 0.59< 0.014000 0.27300107-13-1 U








2-Butanone (MEK) " " "1.03 0.290.35000 0.1000078-93-3 X


Hexane " " "< 0.06 0.35< 0.016752 0.10000110-54-3 U X

Ethyl acetate " " "6.49 0.361.8000 0.10000141-78-6

Chloroform " " "< 0.15 0.49< 0.029810 0.1000067-66-3 U X




Benzene " " "< 0.05 0.32< 0.016752 0.1000071-43-2 U X


Cyclohexane " " "< 0.08 0.34< 0.024658 0.10000110-82-7 U




1,4-Dioxane " " "< 1.25 1.25< 0.34600 0.34600123-91-1 U

n-Heptane " " "< 0.17 0.41< 0.042158 0.10000142-82-5 U





Toluene " " "0.71 0.380.19000 0.10000108-88-3 X

2-Hexanone (MBK) " " "0.37 0.410.090000 0.10000591-78-6 J



Tetrachloroethene " " "181.00 0.6826.630 0.10000127-18-4 E X







SA84560-18





Ethylbenzene " " "< 0.29 0.43< 0.067702 0.10000100-41-4 U X


m,p-Xylene " " "< 0.29 0.43< 0.067356 0.10000179601-23-1 U X

Bromoform " " "< 0.14 1.03< 0.014000 0.1000075-25-2 U X

Styrene " " "< 0.30 0.43< 0.069408 0.10000100-42-5 U X

o-Xylene " " "< 0.32 0.43< 0.073340 0.1000095-47-6 U X



4-Ethyltoluene " " "< 0.44 0.49< 0.088643 0.10000622-96-8 U











n-Butylbenzene " " "< 0.14 0.68< 0.026000 0.12300104-51-8 U













SA84560-19






Propene EPA TO-15 " "< 0.10 0.17< 0.056395 0.10000115-07-1 U





1,3-Butadiene " " "< 0.10 0.22< 0.046885 0.10000106-99-0 U X

Bromomethane " " "< 0.23 0.39< 0.059621 0.1000074-83-9 U X

Chloroethane " " "< 0.11 0.26< 0.042158 0.1000075-00-3 U X

Acetone " " "2.02 1.190.85000 0.5000067-64-1


Ethanol " " "< 0.20 0.94< 0.10462 0.5000064-17-5 U


Acrylonitrile " " "< 0.03 0.59< 0.014000 0.27300107-13-1 U








2-Butanone (MEK) " " "1.00 0.290.34000 0.1000078-93-3 X


Hexane " " "< 0.06 0.35< 0.016752 0.10000110-54-3 U X

Ethyl acetate " " "8.07 0.362.2400 0.10000141-78-6

Chloroform " " "< 0.15 0.49< 0.029810 0.1000067-66-3 U X




Benzene " " "< 0.05 0.32< 0.016752 0.1000071-43-2 U X


Cyclohexane " " "< 0.08 0.34< 0.024658 0.10000110-82-7 U




1,4-Dioxane " " "< 1.25 1.25< 0.34600 0.34600123-91-1 U

n-Heptane " " "< 0.17 0.41< 0.042158 0.10000142-82-5 U





Toluene " " "0.83 0.380.22000 0.10000108-88-3 X

2-Hexanone (MBK) " " "< 0.37 0.41< 0.089952 0.10000591-78-6 U





Ethylbenzene " " "< 0.29 0.43< 0.067702 0.10000100-41-4 U X


m,p-Xylene " " "< 0.29 0.43< 0.067356 0.10000179601-23-1 U X







SA84560-19





Styrene " " "< 0.30 0.43< 0.069408 0.10000100-42-5 U X

o-Xylene " " "< 0.32 0.43< 0.073340 0.1000095-47-6 U X



4-Ethyltoluene " " "< 0.44 0.49< 0.088643 0.10000622-96-8 U











n-Butylbenzene " " "< 0.14 0.68< 0.026000 0.12300104-51-8 U













SA84560-20






Methylene chloride EPA TO-15 20-Sep-08 809157085.80 1.7424.7 0.50075-09-2 X




Propene " 19-Sep-08 8091468< 0.10 0.17< 0.056395 0.10000115-07-1 U


Chloromethane " " "0.64 0.210.31000 0.1000074-87-3 X



1,3-Butadiene " " "< 0.10 0.22< 0.046885 0.10000106-99-0 U X

Bromomethane " " "< 0.23 0.39< 0.059621 0.1000074-83-9 U X

Chloroethane " " "< 0.11 0.26< 0.042158 0.1000075-00-3 U X

Acetone " " "1.12 1.190.47000 0.5000067-64-1 J


Ethanol " " "< 0.20 0.94< 0.10462 0.5000064-17-5 U


Acrylonitrile " " "< 0.03 0.59< 0.014000 0.27300107-13-1 U

Methylene chloride " " "159.00 0.3545.650 0.1000075-09-2 E X

1,1,2-Trichlorotrifluoroethane (Freon 113) " " "0.84 0.770.11000 0.1000076-13-1






2-Butanone (MEK) " " "0.80 0.290.27000 0.1000078-93-3 X


Hexane " " "3.74 0.351.0600 0.10000110-54-3 X

Ethyl acetate " " "0.40 0.360.11000 0.10000141-78-6

Chloroform " " "0.88 0.490.18000 0.1000067-66-3 X




Benzene " " "0.26 0.320.080000 0.1000071-43-2 J X

Carbon tetrachloride " " "0.50 0.630.080000 0.1000056-23-5 J X

Cyclohexane " " "0.45 0.340.13000 0.10000110-82-7




1,4-Dioxane " " "< 1.25 1.25< 0.34600 0.34600123-91-1 U

n-Heptane " " "0.74 0.410.18000 0.10000142-82-5





Toluene " " "3.42 0.380.91000 0.10000108-88-3 X

2-Hexanone (MBK) " " "< 0.37 0.41< 0.089952 0.10000591-78-6 U










SA84560-20





Ethylbenzene " " "< 0.29 0.43< 0.067702 0.10000100-41-4 U X


m,p-Xylene " " "0.65 0.430.15000 0.10000179601-23-1 X

Bromoform " " "< 0.14 1.03< 0.014000 0.1000075-25-2 U X

Styrene " " "< 0.30 0.43< 0.069408 0.10000100-42-5 U X

o-Xylene " " "< 0.32 0.43< 0.073340 0.1000095-47-6 U X



4-Ethyltoluene " " "< 0.44 0.49< 0.088643 0.10000622-96-8 U











n-Butylbenzene " " "< 0.14 0.68< 0.026000 0.12300104-51-8 U













SA84560-21






Propene EPA TO-15 " "2.91 0.861.69 0.500115-07-1





1,3-Butadiene " " "< 0.41 1.10< 0.186 0.500106-99-0 U X

Bromomethane " " "< 0.58 1.94< 0.149 0.50074-83-9 U X

Chloroethane " " "< 0.42 1.32< 0.158 0.50075-00-3 U X

Acetone " " "378.00 1.19159 0.50067-64-1 E


Ethanol " " "5.75 0.943.05 0.50064-17-5

Acrylonitrile " " "< 0.59 1.08< 0.273 0.500107-13-1 U







Methyl tert-butyl ether " " "1.19 1.800.330 0.5001634-04-4 J X


2-Butanone (MEK) " " "17.00 1.475.75 0.50078-93-3 X


Hexane " " "< 0.33 1.76< 0.0923 0.500110-54-3 U X

Ethyl acetate " " "< 0.55 1.80< 0.154 0.500141-78-6 U

Chloroform " " "1.41 2.430.290 0.50067-66-3 J X




Benzene " " "< 0.40 1.60< 0.124 0.50071-43-2 U X


Cyclohexane " " "< 0.39 1.72< 0.113 0.500110-82-7 U




1,4-Dioxane " " "< 1.25 1.80< 0.346 0.500123-91-1 U

n-Heptane " " "< 0.45 2.05< 0.111 0.500142-82-5 U





Toluene " " "< 0.46 1.88< 0.122 0.500108-88-3 U X

2-Hexanone (MBK) " " "3.57 2.050.870 0.500591-78-6






Ethylbenzene " " "< 0.61 2.17< 0.141 0.500100-41-4 U X

m,p-Xylene " " "< 1.07 4.34< 0.246 1.00179601-23-1 U X







SA84560-21





Styrene " " "< 0.68 2.13< 0.159 0.500100-42-5 U X

o-Xylene " " "< 0.50 2.17< 0.116 0.50095-47-6 U X




4-Ethyltoluene " " "< 0.58 2.46< 0.117 0.500622-96-8 U








n-Butylbenzene " " "< 0.68 2.74< 0.123 0.500104-51-8 U















SA84560-22






Propene EPA TO-15 " "43.00 0.8625.0 0.500115-07-1





1,3-Butadiene " " "< 0.41 1.10< 0.186 0.500106-99-0 U X

Bromomethane " " "< 0.58 1.94< 0.149 0.50074-83-9 U X

Chloroethane " " "< 0.42 1.32< 0.158 0.50075-00-3 U X

Acetone " " "461.00 1.19194 0.50067-64-1 E


Ethanol " " "28.50 0.9415.1 0.50064-17-5

Acrylonitrile " " "< 0.59 1.08< 0.273 0.500107-13-1 U







Methyl tert-butyl ether " " "44.70 1.8012.4 0.5001634-04-4 X


2-Butanone (MEK) " " "150.00 1.4750.8 0.50078-93-3 X


Hexane " " "1.66 1.760.470 0.500110-54-3 J X

Ethyl acetate " " "< 0.55 1.80< 0.154 0.500141-78-6 U

Chloroform " " "60.80 2.4312.5 0.50067-66-3 X




Benzene " " "< 0.40 1.60< 0.124 0.50071-43-2 U X


Cyclohexane " " "< 0.39 1.72< 0.113 0.500110-82-7 U




1,4-Dioxane " " "< 1.25 1.80< 0.346 0.500123-91-1 U

n-Heptane " " "1.11 2.050.270 0.500142-82-5 J





Toluene " " "< 0.46 1.88< 0.122 0.500108-88-3 U X

2-Hexanone (MBK) " " "30.50 2.057.45 0.500591-78-6






Ethylbenzene " " "< 0.61 2.17< 0.141 0.500100-41-4 U X

m,p-Xylene " " "< 1.07 4.34< 0.246 1.00179601-23-1 U X







SA84560-22





Styrene " " "< 0.68 2.13< 0.159 0.500100-42-5 U X

o-Xylene " " "< 0.50 2.17< 0.116 0.50095-47-6 U X




4-Ethyltoluene " " "< 0.58 2.46< 0.117 0.500622-96-8 U








n-Butylbenzene " " "< 0.68 2.74< 0.123 0.500104-51-8 U











Sample IdentificationS373-INA




SA84560-23




Naphthalene Modified MA APH 19-Sep-08 809156319.20 12.603.67 2.4091-20-3


Propene EPA TO-15 " "< 0.10 0.17< 0.056395 0.10000115-07-1 U


Chloromethane " " "1.20 0.210.58000 0.1000074-87-3 X



1,3-Butadiene " " "< 0.10 0.22< 0.046885 0.10000106-99-0 U X

Bromomethane " " "< 0.23 0.39< 0.059621 0.1000074-83-9 U X

Chloroethane " " "< 0.11 0.26< 0.042158 0.1000075-00-3 U X

Acetone " " "7.87 1.193.3100 0.5000067-64-1


Ethanol " " "< 0.20 0.94< 0.10462 0.5000064-17-5 U


Acrylonitrile " " "< 0.03 0.59< 0.014000 0.27300107-13-1 U








2-Butanone (MEK) " " "1.21 0.290.41000 0.1000078-93-3 X

cis-1,2-Dichloroethene " " "0.63 0.400.16000 0.10000156-59-2 X

Hexane " " "1.45 0.350.41000 0.10000110-54-3 X

Ethyl acetate " " "1.51 0.360.42000 0.10000141-78-6

Chloroform " " "< 0.15 0.49< 0.029810 0.1000067-66-3 U X


1,2-Dichloroethane " " "0.40 0.400.10000 0.10000107-06-2 X


Benzene " " "0.61 0.320.19000 0.1000071-43-2 X


Cyclohexane " " "< 0.08 0.34< 0.024658 0.10000110-82-7 U




1,4-Dioxane " " "< 1.25 1.25< 0.34600 0.34600123-91-1 U

n-Heptane " " "0.78 0.410.19000 0.10000142-82-5





Toluene " " "3.39 0.380.90000 0.10000108-88-3 X

2-Hexanone (MBK) " " "< 0.37 0.41< 0.089952 0.10000591-78-6 U





Ethylbenzene " " "0.48 0.430.11000 0.10000100-41-4 X


m,p-Xylene " " "1.34 0.430.31000 0.10000179601-23-1 X



Sample IdentificationS373-INA




SA84560-23





Styrene " " "0.64 0.430.15000 0.10000100-42-5 X

o-Xylene " " "0.52 0.430.12000 0.1000095-47-6 X



4-Ethyltoluene " " "< 0.44 0.49< 0.088643 0.10000622-96-8 U











n-Butylbenzene " " "< 0.14 0.68< 0.026000 0.12300104-51-8 U













SA84560-24






Propene EPA TO-15 " "< 0.10 0.17< 0.056395 0.10000115-07-1 U





1,3-Butadiene " " "< 0.10 0.22< 0.046885 0.10000106-99-0 U X

Bromomethane " " "< 0.23 0.39< 0.059621 0.1000074-83-9 U X

Chloroethane " " "< 0.11 0.26< 0.042158 0.1000075-00-3 U X

Acetone " " "< 0.16 1.19< 0.067702 0.5000067-64-1 U


Ethanol " " "< 0.20 0.94< 0.10462 0.5000064-17-5 U


Acrylonitrile " " "< 0.03 0.59< 0.014000 0.27300107-13-1 U








2-Butanone (MEK) " " "1.59 0.290.54000 0.1000078-93-3 X


Hexane " " "< 0.06 0.35< 0.016752 0.10000110-54-3 U X

Ethyl acetate " " "< 0.17 0.36< 0.045877 0.10000141-78-6 U

Chloroform " " "1.22 0.490.25000 0.1000067-66-3 X




Benzene " " "0.32 0.320.10000 0.1000071-43-2 X


Cyclohexane " " "< 0.08 0.34< 0.024658 0.10000110-82-7 U




1,4-Dioxane " " "< 1.25 1.25< 0.34600 0.34600123-91-1 U

n-Heptane " " "< 0.17 0.41< 0.042158 0.10000142-82-5 U





Toluene " " "0.98 0.380.26000 0.10000108-88-3 X

2-Hexanone (MBK) " " "< 0.37 0.41< 0.089952 0.10000591-78-6 U





Ethylbenzene " " "< 0.29 0.43< 0.067702 0.10000100-41-4 U X


m,p-Xylene " " "< 0.29 0.43< 0.067356 0.10000179601-23-1 U X







SA84560-24





Styrene " " "< 0.30 0.43< 0.069408 0.10000100-42-5 U X

o-Xylene " " "< 0.32 0.43< 0.073340 0.1000095-47-6 U X



4-Ethyltoluene " " "< 0.44 0.49< 0.088643 0.10000622-96-8 U











n-Butylbenzene " " "< 0.14 0.68< 0.026000 0.12300104-51-8 U













SA84560-25






Propene EPA TO-15 " "5.47 0.863.18 0.500115-07-1





1,3-Butadiene " " "< 0.41 1.10< 0.186 0.500106-99-0 U X

Bromomethane " " "< 0.58 1.94< 0.149 0.50074-83-9 U X

Chloroethane " " "< 0.42 1.32< 0.158 0.50075-00-3 U X

Acetone " " "501.00 1.19211 0.50067-64-1 E


Ethanol " " "8.77 0.944.65 0.50064-17-5

Acrylonitrile " " "< 0.59 1.08< 0.273 0.500107-13-1 U









2-Butanone (MEK) " " "10.20 1.473.47 0.50078-93-3 X


Hexane " " "< 0.33 1.76< 0.0923 0.500110-54-3 U X

Ethyl acetate " " "< 0.55 1.80< 0.154 0.500141-78-6 U

Chloroform " " "8.47 2.431.74 0.50067-66-3 X




Benzene " " "< 0.40 1.60< 0.124 0.50071-43-2 U X


Cyclohexane " " "< 0.39 1.72< 0.113 0.500110-82-7 U




1,4-Dioxane " " "< 1.25 1.80< 0.346 0.500123-91-1 U

n-Heptane " " "< 0.45 2.05< 0.111 0.500142-82-5 U





Toluene " " "< 0.46 1.88< 0.122 0.500108-88-3 U X

2-Hexanone (MBK) " " "1.97 2.050.480 0.500591-78-6 J






Ethylbenzene " " "< 0.61 2.17< 0.141 0.500100-41-4 U X

m,p-Xylene " " "2.99 4.340.690 1.00179601-23-1 J X







SA84560-25





Styrene " " "< 0.68 2.13< 0.159 0.500100-42-5 U X

o-Xylene " " "2.43 2.170.560 0.50095-47-6 X




4-Ethyltoluene " " "< 0.58 2.46< 0.117 0.500622-96-8 U








n-Butylbenzene " " "< 0.68 2.74< 0.123 0.500104-51-8 U











Sample IdentificationS373-AOA




SA84560-26






Propene EPA TO-15 " "< 0.10 0.17< 0.056395 0.10000115-07-1 U


Chloromethane " " "1.14 0.210.55000 0.1000074-87-3 X



1,3-Butadiene " " "< 0.10 0.22< 0.046885 0.10000106-99-0 U X

Bromomethane " " "< 0.23 0.39< 0.059621 0.1000074-83-9 U X

Chloroethane " " "< 0.11 0.26< 0.042158 0.1000075-00-3 U X

Acetone " " "7.75 1.193.2600 0.5000067-64-1


Ethanol " " "8.96 0.944.7500 0.5000064-17-5


Acrylonitrile " " "< 0.03 0.59< 0.014000 0.27300107-13-1 U








2-Butanone (MEK) " " "0.83 0.290.28000 0.1000078-93-3 X


Hexane " " "1.30 0.350.37000 0.10000110-54-3 X

Ethyl acetate " " "< 0.17 0.36< 0.045877 0.10000141-78-6 U

Chloroform " " "< 0.15 0.49< 0.029810 0.1000067-66-3 U X




Benzene " " "0.32 0.320.10000 0.1000071-43-2 X


Cyclohexane " " "< 0.08 0.34< 0.024658 0.10000110-82-7 U




1,4-Dioxane " " "< 1.25 1.25< 0.34600 0.34600123-91-1 U

n-Heptane " " "0.37 0.410.090000 0.10000142-82-5 J





Toluene " " "1.47 0.380.39000 0.10000108-88-3 X

2-Hexanone (MBK) " " "< 0.37 0.41< 0.089952 0.10000591-78-6 U





Ethylbenzene " " "< 0.29 0.43< 0.067702 0.10000100-41-4 U X


m,p-Xylene " " "0.56 0.430.13000 0.10000179601-23-1 X



Sample IdentificationS373-AOA




SA84560-26





Styrene " " "< 0.30 0.43< 0.069408 0.10000100-42-5 U X

o-Xylene " " "< 0.32 0.43< 0.073340 0.1000095-47-6 U X



4-Ethyltoluene " " "< 0.44 0.49< 0.088643 0.10000622-96-8 U











n-Butylbenzene " " "< 0.14 0.68< 0.026000 0.12300104-51-8 U













SA84560-27






Propene EPA TO-15 " "< 0.10 0.17< 0.056395 0.10000115-07-1 U





1,3-Butadiene " " "< 0.10 0.22< 0.046885 0.10000106-99-0 U X

Bromomethane " " "< 0.23 0.39< 0.059621 0.1000074-83-9 U X

Chloroethane " " "< 0.11 0.26< 0.042158 0.1000075-00-3 U X

Acetone " " "1.62 1.190.68000 0.5000067-64-1


Ethanol " " "< 0.20 0.94< 0.10462 0.5000064-17-5 U


Acrylonitrile " " "< 0.03 0.59< 0.014000 0.27300107-13-1 U








2-Butanone (MEK) " " "0.94 0.290.32000 0.1000078-93-3 X


Hexane " " "< 0.06 0.35< 0.016752 0.10000110-54-3 U X

Ethyl acetate " " "0.32 0.360.090000 0.10000141-78-6 J

Chloroform " " "0.88 0.490.18000 0.1000067-66-3 X

Tetrahydrofuran " " "2.09 0.290.71000 0.10000109-99-9



Benzene " " "< 0.05 0.32< 0.016752 0.1000071-43-2 U X


Cyclohexane " " "< 0.08 0.34< 0.024658 0.10000110-82-7 U




1,4-Dioxane " " "< 1.25 1.25< 0.34600 0.34600123-91-1 U

n-Heptane " " "< 0.17 0.41< 0.042158 0.10000142-82-5 U





Toluene " " "0.75 0.380.20000 0.10000108-88-3 X

2-Hexanone (MBK) " " "0.41 0.410.10000 0.10000591-78-6





Ethylbenzene " " "< 0.29 0.43< 0.067702 0.10000100-41-4 U X


m,p-Xylene " " "< 0.29 0.43< 0.067356 0.10000179601-23-1 U X







SA84560-27





Styrene " " "< 0.30 0.43< 0.069408 0.10000100-42-5 U X

o-Xylene " " "< 0.32 0.43< 0.073340 0.1000095-47-6 U X



4-Ethyltoluene " " "< 0.44 0.49< 0.088643 0.10000622-96-8 U











n-Butylbenzene " " "< 0.14 0.68< 0.026000 0.12300104-51-8 U













SA84560-28






Propene EPA TO-15 " "< 0.10 0.17< 0.056395 0.10000115-07-1 U





1,3-Butadiene " " "< 0.10 0.22< 0.046885 0.10000106-99-0 U X

Bromomethane " " "< 0.23 0.39< 0.059621 0.1000074-83-9 U X

Chloroethane " " "< 0.11 0.26< 0.042158 0.1000075-00-3 U X

Acetone " " "1.78 1.190.75000 0.5000067-64-1


Ethanol " " "< 0.20 0.94< 0.10462 0.5000064-17-5 U


Acrylonitrile " " "< 0.03 0.59< 0.014000 0.27300107-13-1 U








2-Butanone (MEK) " " "0.77 0.290.26000 0.1000078-93-3 X


Hexane " " "< 0.06 0.35< 0.016752 0.10000110-54-3 U X

Ethyl acetate " " "0.32 0.360.090000 0.10000141-78-6 J

Chloroform " " "< 0.15 0.49< 0.029810 0.1000067-66-3 U X




Benzene " " "< 0.05 0.32< 0.016752 0.1000071-43-2 U X


Cyclohexane " " "< 0.08 0.34< 0.024658 0.10000110-82-7 U




1,4-Dioxane " " "< 1.25 1.25< 0.34600 0.34600123-91-1 U

n-Heptane " " "< 0.17 0.41< 0.042158 0.10000142-82-5 U





Toluene " " "0.71 0.380.19000 0.10000108-88-3 X

2-Hexanone (MBK) " " "< 0.37 0.41< 0.089952 0.10000591-78-6 U





Ethylbenzene " " "< 0.29 0.43< 0.067702 0.10000100-41-4 U X


m,p-Xylene " " "< 0.29 0.43< 0.067356 0.10000179601-23-1 U X







SA84560-28





Styrene " " "< 0.30 0.43< 0.069408 0.10000100-42-5 U X

o-Xylene " " "< 0.32 0.43< 0.073340 0.1000095-47-6 U X



4-Ethyltoluene " " "< 0.44 0.49< 0.088643 0.10000622-96-8 U











n-Butylbenzene " " "< 0.14 0.68< 0.026000 0.12300104-51-8 U













SA84560-29






Propene EPA TO-15 " "20.30 3.4411.8 2.00115-07-1





1,3-Butadiene " " "< 1.64 4.42< 0.744 2.00106-99-0 U X

Bromomethane " " "< 2.31 7.76< 0.596 2.0074-83-9 U X

Chloroethane " " "< 1.67 5.28< 0.632 2.0075-00-3 U X

Acetone " " "554.00 4.75233 2.0067-64-1


Ethanol " " "28.50 3.7715.1 2.0064-17-5

Acrylonitrile " " "< 2.36 4.34< 1.09 2.00107-13-1 U









2-Butanone (MEK) " " "51.00 5.9017.3 2.0078-93-3 X


Hexane " " "< 1.30 7.05< 0.369 2.00110-54-3 U X

Ethyl acetate " " "< 2.22 7.21< 0.616 2.00141-78-6 U

Chloroform " " "5.84 9.701.20 2.0067-66-3 J X




Benzene " " "< 1.58 6.38< 0.496 2.0071-43-2 U X


Cyclohexane " " "< 1.56 6.88< 0.452 2.00110-82-7 U




1,4-Dioxane " " "< 4.97 7.20< 1.38 2.00123-91-1 U

n-Heptane " " "< 1.82 8.20< 0.444 2.00142-82-5 U





Toluene " " "< 1.84 7.53< 0.488 2.00108-88-3 U X

2-Hexanone (MBK) " " "7.21 8.201.76 2.00591-78-6 J






Ethylbenzene " " "< 2.45 8.67< 0.564 2.00100-41-4 U X

m,p-Xylene " " "< 4.27 17.30< 0.984 4.00179601-23-1 U X







SA84560-29





Styrene " " "< 2.71 8.51< 0.636 2.00100-42-5 U X

o-Xylene " " "< 2.01 8.67< 0.464 2.0095-47-6 U X




4-Ethyltoluene " " "6.10 9.801.24 2.00622-96-8 J








n-Butylbenzene " " "< 2.70 11.00< 0.492 2.00104-51-8 U















SA84560-30




Naphthalene Modified MA APH 18-Sep-08 809132821.80 50.304.16 9.6091-20-3 J


Propene EPA TO-15 " "46.30 3.4426.9 2.00115-07-1


Chloromethane " " "2.97 4.131.44 2.0074-87-3 J X



1,3-Butadiene " " "< 1.64 4.42< 0.744 2.00106-99-0 U X

Bromomethane " " "< 2.31 7.76< 0.596 2.0074-83-9 U X

Chloroethane " " "< 1.67 5.28< 0.632 2.0075-00-3 U X

Acetone " " "1690.00 4.75713 2.0067-64-1 E


Ethanol " " "73.50 3.7739.0 2.0064-17-5

Acrylonitrile " " "< 2.36 4.34< 1.09 2.00107-13-1 U









2-Butanone (MEK) " " "112.00 5.9037.9 2.0078-93-3 X


Hexane " " "4.51 7.051.28 2.00110-54-3 J X

Ethyl acetate " " "< 2.22 7.21< 0.616 2.00141-78-6 U

Chloroform " " "40.10 9.708.24 2.0067-66-3 X




Benzene " " "< 1.58 6.38< 0.496 2.0071-43-2 U X


Cyclohexane " " "< 1.56 6.88< 0.452 2.00110-82-7 U




1,4-Dioxane " " "< 4.97 7.20< 1.38 2.00123-91-1 U

n-Heptane " " "5.90 8.201.44 2.00142-82-5 J





Toluene " " "4.06 7.531.08 2.00108-88-3 J X

2-Hexanone (MBK) " " "16.10 8.203.92 2.00591-78-6






Ethylbenzene " " "< 2.45 8.67< 0.564 2.00100-41-4 U X

m,p-Xylene " " "< 4.27 17.30< 0.984 4.00179601-23-1 U X







SA84560-30





Styrene " " "< 2.71 8.51< 0.636 2.00100-42-5 U X

o-Xylene " " "< 2.01 8.67< 0.464 2.0095-47-6 U X




4-Ethyltoluene " " "30.70 9.806.24 2.00622-96-8






4-Isopropyltoluene " " "7.94 10.701.48 2.0099-87-6 J


n-Butylbenzene " " "< 2.70 11.00< 0.492 2.00104-51-8 U















SA84560-31






Propene EPA TO-15 " "17.60 3.4410.2 2.00115-07-1





1,3-Butadiene " " "< 1.64 4.42< 0.744 2.00106-99-0 U X

Bromomethane " " "< 2.31 7.76< 0.596 2.0074-83-9 U X

Chloroethane " " "< 1.67 5.28< 0.632 2.0075-00-3 U X

Acetone " " "898.00 4.75378 2.0067-64-1


Ethanol " " "42.40 3.7722.5 2.0064-17-5

Acrylonitrile " " "< 2.36 4.34< 1.09 2.00107-13-1 U









2-Butanone (MEK) " " "30.70 5.9010.4 2.0078-93-3 X


Hexane " " "< 1.30 7.05< 0.369 2.00110-54-3 U X

Ethyl acetate " " "< 2.22 7.21< 0.616 2.00141-78-6 U

Chloroform " " "< 4.30 9.70< 0.884 2.0067-66-3 U X




Benzene " " "< 1.58 6.38< 0.496 2.0071-43-2 U X


Cyclohexane " " "< 1.56 6.88< 0.452 2.00110-82-7 U




1,4-Dioxane " " "< 4.97 7.20< 1.38 2.00123-91-1 U

n-Heptane " " "8.36 8.202.04 2.00142-82-5




1,1,2-Trichloroethane " " "8.95 10.901.64 2.0079-00-5 J X

Toluene " " "7.38 7.531.96 2.00108-88-3 J X

2-Hexanone (MBK) " " "< 4.75 8.20< 1.16 2.00591-78-6 U






Ethylbenzene " " "< 2.45 8.67< 0.564 2.00100-41-4 U X

m,p-Xylene " " "< 4.27 17.30< 0.984 4.00179601-23-1 U X







SA84560-31





Styrene " " "< 2.71 8.51< 0.636 2.00100-42-5 U X

o-Xylene " " "< 2.01 8.67< 0.464 2.0095-47-6 U X




4-Ethyltoluene " " "5.70 9.801.16 2.00622-96-8 J








n-Butylbenzene " " "< 2.70 11.00< 0.492 2.00104-51-8 U















SA84560-32






Propene EPA TO-15 " "< 0.10 0.17< 0.056395 0.10000115-07-1 U





1,3-Butadiene " " "< 0.10 0.22< 0.046885 0.10000106-99-0 U X

Bromomethane " " "< 0.23 0.39< 0.059621 0.1000074-83-9 U X

Chloroethane " " "< 0.11 0.26< 0.042158 0.1000075-00-3 U X

Acetone " " "1.97 1.190.83000 0.5000067-64-1


Ethanol " " "< 0.20 0.94< 0.10462 0.5000064-17-5 U


Acrylonitrile " " "< 0.03 0.59< 0.014000 0.27300107-13-1 U








2-Butanone (MEK) " " "1.21 0.290.41000 0.1000078-93-3 X


Hexane " " "0.28 0.350.080000 0.10000110-54-3 J X

Ethyl acetate " " "< 0.17 0.36< 0.045877 0.10000141-78-6 U

Chloroform " " "0.97 0.490.20000 0.1000067-66-3 X




Benzene " " "0.29 0.320.090000 0.1000071-43-2 J X


Cyclohexane " " "< 0.08 0.34< 0.024658 0.10000110-82-7 U




1,4-Dioxane " " "< 1.25 1.25< 0.34600 0.34600123-91-1 U

n-Heptane " " "0.49 0.410.12000 0.10000142-82-5





Toluene " " "1.62 0.380.43000 0.10000108-88-3 X

2-Hexanone (MBK) " " "0.57 0.410.14000 0.10000591-78-6





Ethylbenzene " " "< 0.29 0.43< 0.067702 0.10000100-41-4 U X


m,p-Xylene " " "0.56 0.430.13000 0.10000179601-23-1 X







SA84560-32





Styrene " " "< 0.30 0.43< 0.069408 0.10000100-42-5 U X

o-Xylene " " "< 0.32 0.43< 0.073340 0.1000095-47-6 U X



4-Ethyltoluene " " "< 0.44 0.49< 0.088643 0.10000622-96-8 U


Isopropylbenzene " " "1.43 0.740.29000 0.1500098-82-8









n-Butylbenzene " " "< 0.14 0.68< 0.026000 0.12300104-51-8 U













SA84560-33






Propene EPA TO-15 " "18.90 0.8611.0 0.500115-07-1





1,3-Butadiene " " "< 0.41 1.10< 0.186 0.500106-99-0 U X

Bromomethane " " "< 0.58 1.94< 0.149 0.50074-83-9 U X

Chloroethane " " "< 0.42 1.32< 0.158 0.50075-00-3 U X

Acetone " " "6.44 1.192.71 0.50067-64-1


Ethanol " " "5.52 0.942.93 0.50064-17-5

Acrylonitrile " " "< 0.59 1.08< 0.273 0.500107-13-1 U









2-Butanone (MEK) " " "1.30 1.470.440 0.50078-93-3 J X


Hexane " " "< 0.33 1.76< 0.0923 0.500110-54-3 U X

Ethyl acetate " " "< 0.55 1.80< 0.154 0.500141-78-6 U

Chloroform " " "2.73 2.430.560 0.50067-66-3 X




Benzene " " "< 0.40 1.60< 0.124 0.50071-43-2 U X


Cyclohexane " " "< 0.39 1.72< 0.113 0.500110-82-7 U




1,4-Dioxane " " "< 1.25 1.80< 0.346 0.500123-91-1 U

n-Heptane " " "< 0.45 2.05< 0.111 0.500142-82-5 U





Toluene " " "1.35 1.880.360 0.500108-88-3 J X

2-Hexanone (MBK) " " "< 1.18 2.05< 0.289 0.500591-78-6 U






Ethylbenzene " " "< 0.61 2.17< 0.141 0.500100-41-4 U X

m,p-Xylene " " "< 1.07 4.34< 0.246 1.00179601-23-1 U X







SA84560-33





Styrene " " "< 0.68 2.13< 0.159 0.500100-42-5 U X

o-Xylene " " "< 0.50 2.17< 0.116 0.50095-47-6 U X




4-Ethyltoluene " " "< 0.58 2.46< 0.117 0.500622-96-8 U








n-Butylbenzene " " "< 0.68 2.74< 0.123 0.500104-51-8 U















SA84560-34






Propene EPA TO-15 " "8.61 3.445.00 2.00115-07-1





1,3-Butadiene " " "< 1.64 4.42< 0.744 2.00106-99-0 U X

Bromomethane " " "< 2.31 7.76< 0.596 2.0074-83-9 U X

Chloroethane " " "< 1.67 5.28< 0.632 2.0075-00-3 U X

Acetone " " "858.00 4.75361 2.0067-64-1


Ethanol " " "12.10 3.776.40 2.0064-17-5

Acrylonitrile " " "< 2.36 4.34< 1.09 2.00107-13-1 U









2-Butanone (MEK) " " "16.40 5.905.56 2.0078-93-3 X

cis-1,2-Dichloroethene " " "32.50 7.938.20 2.00156-59-2 X

Hexane " " "< 1.30 7.05< 0.369 2.00110-54-3 U X

Ethyl acetate " " "< 2.22 7.21< 0.616 2.00141-78-6 U

Chloroform " " "< 4.30 9.70< 0.884 2.0067-66-3 U X




Benzene " " "< 1.58 6.38< 0.496 2.0071-43-2 U X


Cyclohexane " " "< 1.56 6.88< 0.452 2.00110-82-7 U




1,4-Dioxane " " "< 4.97 7.20< 1.38 2.00123-91-1 U

n-Heptane " " "4.43 8.201.08 2.00142-82-5 J





Toluene " " "4.97 7.531.32 2.00108-88-3 J X

2-Hexanone (MBK) " " "< 4.75 8.20< 1.16 2.00591-78-6 U






Ethylbenzene " " "< 2.45 8.67< 0.564 2.00100-41-4 U X

m,p-Xylene " " "< 4.27 17.30< 0.984 4.00179601-23-1 U X







SA84560-34





Styrene " " "< 2.71 8.51< 0.636 2.00100-42-5 U X

o-Xylene " " "< 2.01 8.67< 0.464 2.0095-47-6 U X




4-Ethyltoluene " " "< 2.30 9.80< 0.468 2.00622-96-8 U








n-Butylbenzene " " "< 2.70 11.00< 0.492 2.00104-51-8 U















SA84560-35






Propene EPA TO-15 " "< 0.10 0.17< 0.056395 0.10000115-07-1 U


Chloromethane " " "0.99 0.210.48000 0.1000074-87-3 X



1,3-Butadiene " " "< 0.10 0.22< 0.046885 0.10000106-99-0 U X

Bromomethane " " "< 0.23 0.39< 0.059621 0.1000074-83-9 U X

Chloroethane " " "< 0.11 0.26< 0.042158 0.1000075-00-3 U X

Acetone " " "9.80 1.194.1100 0.5000067-64-1


Ethanol " " "26.50 0.9414.080 0.5000064-17-5 E


Acrylonitrile " " "< 0.03 0.59< 0.014000 0.27300107-13-1 U








2-Butanone (MEK) " " "1.12 0.290.38000 0.1000078-93-3 X


Hexane " " "2.50 0.350.71000 0.10000110-54-3 X

Ethyl acetate " " "0.50 0.360.14000 0.10000141-78-6

Chloroform " " "0.44 0.490.090000 0.1000067-66-3 J X




Benzene " " "< 0.05 0.32< 0.016752 0.1000071-43-2 U X


Cyclohexane " " "< 0.08 0.34< 0.024658 0.10000110-82-7 U




1,4-Dioxane " " "< 1.25 1.25< 0.34600 0.34600123-91-1 U

n-Heptane " " "0.49 0.410.12000 0.10000142-82-5





Toluene " " "1.77 0.380.47000 0.10000108-88-3 X

2-Hexanone (MBK) " " "< 0.37 0.41< 0.089952 0.10000591-78-6 U





Ethylbenzene " " "< 0.29 0.43< 0.067702 0.10000100-41-4 U X


m,p-Xylene " " "< 0.29 0.43< 0.067356 0.10000179601-23-1 U X







SA84560-35





Styrene " " "< 0.30 0.43< 0.069408 0.10000100-42-5 U X

o-Xylene " " "< 0.32 0.43< 0.073340 0.1000095-47-6 U X



4-Ethyltoluene " " "< 0.44 0.49< 0.088643 0.10000622-96-8 U











n-Butylbenzene " " "< 0.14 0.68< 0.026000 0.12300104-51-8 U









Result *RDL Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Flag Analyte(s)

Air Quality Analyses - Quality Control

Batch 8091255 - General Air Prep

Blank (8091255-BLK1) Prepared & Analyzed: 16-Sep-08

Propene 0.10000 ppbv UBRL

Dichlorodifluoromethane (Freon12) 0.10000 ppbv UBRL

Chloromethane 0.10000 ppbv UBRL

1,2-Dichlorotetrafluoroethane (Freon 114) 0.10000 ppbv UBRL

Vinyl chloride 0.10000 ppbv UBRL

1,3-Butadiene 0.10000 ppbv UBRL

Bromomethane 0.10000 ppbv UBRL

Chloroethane 0.10000 ppbv UBRL

Acetone 0.50000 ppbv UBRL

Trichlorofluoromethane (Freon 11) 0.10000 ppbv UBRL

Ethanol 0.50000 ppbv UBRL

Acrylonitrile 0.27300 ppbv UBRL

1,1-Dichloroethene 0.10000 ppbv UBRL

Methylene chloride 0.10000 ppbv UBRL

1,1,2-Trichlorotrifluoroethane (Freon 113) 0.10000 ppbv UBRL

Carbon disulfide 0.50000 ppbv UBRL

trans-1,2-Dichloroethene 0.10000 ppbv UBRL

1,1-Dichloroethane 0.10000 ppbv UBRL

Methyl tert-butyl ether 0.10000 ppbv UBRL

Isopropyl alcohol 0.50000 ppbv UBRL

2-Butanone (MEK) 0.10000 ppbv UBRL

cis-1,2-Dichloroethene 0.10000 ppbv UBRL

Hexane 0.10000 ppbv UBRL

Ethyl acetate 0.10000 ppbv UBRL

Chloroform 0.10000 ppbv UBRL

Tetrahydrofuran 0.10000 ppbv UBRL


1,1,1-Trichloroethane 0.10000 ppbv UBRL

Benzene 0.10000 ppbv UBRL

Carbon tetrachloride 0.10000 ppbv UBRL

Cyclohexane 0.10000 ppbv UBRL

1,2-Dichloropropane 0.10000 ppbv UBRL

Bromodichloromethane 0.10000 ppbv UBRL

Trichloroethene 0.10000 ppbv UBRL

n-Heptane 0.10000 ppbv UBRL

1,4-Dioxane 0.34600 ppbv UBRL

4-Methyl-2-pentanone (MIBK) 0.10000 ppbv UBRL

cis-1,3-Dichloropropene 0.10000 ppbv UBRL

trans-1,3-Dichloropropene 0.10000 ppbv UBRL


Toluene 0.10000 ppbv UBRL

2-Hexanone (MBK) 0.10000 ppbv UBRL

Dibromochloromethane 0.10000 ppbv UBRL

1,2-Dibromoethane (EDB) 0.10000 ppbv UBRL

Tetrachloroethene 0.10000 ppbv UBRL

Chlorobenzene 0.10000 ppbv UBRL

Ethylbenzene 0.10000 ppbv UBRL

m,p-Xylene 0.10000 ppbv UBRL

1,1,1,2-Tetrachloroethane 0.21200 ppbv UBRL

Bromoform 0.10000 ppbv UBRL

Styrene 0.10000 ppbv UBRL

o-Xylene 0.10000 ppbv UBRL


1,3,5-Trimethylbenzene 0.10000 ppbv UBRL




Spike

Result

Source

%REC

%REC

Limits RPD

RPD





4-Ethyltoluene 0.10000 ppbv UBRL

Isopropylbenzene 0.15000 ppbv UBRL


1,3-Dichlorobenzene 0.10000 ppbv UBRL

Benzyl chloride 0.10000 ppbv UBRL

Naphthalene 2.40 ppbv UBRL



1,2,4-Trichlorobenzene 0.10000 ppbv UBRL

Hexachlorobutadiene 0.10000 ppbv UBRL

sec-Butylbenzene 0.14500 ppbv UBRL

4-Isopropyltoluene 0.12100 ppbv UBRL

n-Butylbenzene 0.12300 ppbv UBRL

10.0 70-130Surrogate: 4-Bromofluorobenzene 939.2600 ppbv

LCS (8091255-BS1) Prepared & Analyzed: 16-Sep-08

Propene 2.00 70-13094ppbv1.8900

Dichlorodifluoromethane (Freon12) 2.00 70-130114ppbv2.2900

Chloromethane 2.00 70-13094ppbv1.8700

1,2-Dichlorotetrafluoroethane (Freon 114) 2.00 70-13092ppbv1.8400

Vinyl chloride 2.00 70-130103ppbv2.0600

1,3-Butadiene 2.00 70-130102ppbv2.0400

Bromomethane 2.00 70-130110ppbv2.2100

Chloroethane 2.00 70-130110ppbv2.2100

Acetone 2.00 70-13088ppbv1.7700

Trichlorofluoromethane (Freon 11) 2.00 70-130104ppbv2.0900

Ethanol 2.00 70-17884ppbv1.6800

1,1-Dichloroethene 2.00 70-13089ppbv1.7800

Acrylonitrile 2.00 60-16070ppbv1.4000

Methylene chloride 2.00 70-13097ppbv1.9400

1,1,2-Trichlorotrifluoroethane (Freon 113) 2.00 70-13089ppbv1.7800

Carbon disulfide 2.00 70-13096ppbv1.9100

trans-1,2-Dichloroethene 2.00 70-13091ppbv1.8200

1,1-Dichloroethane 2.00 70-13092ppbv1.8300

Methyl tert-butyl ether 2.00 70-130106ppbv2.1100

Isopropyl alcohol 2.00 70-13096ppbv1.9100

2-Butanone (MEK) 2.00 70-13092ppbv1.8500

cis-1,2-Dichloroethene 2.00 70-13096ppbv1.9100

Hexane 2.00 70-130107ppbv2.1400

Ethyl acetate 2.00 70-130104ppbv2.0900

Chloroform 2.00 70-130100ppbv1.9900

Tetrahydrofuran 2.00 70-13096ppbv1.9300


1,1,1-Trichloroethane 2.00 70-13092ppbv1.8500

Benzene 2.00 70-130104ppbv2.0900

Carbon tetrachloride 2.00 70-13096ppbv1.9100

Cyclohexane 2.00 70-130110ppbv2.2000

1,2-Dichloropropane 2.00 70-130101ppbv2.0200

Bromodichloromethane 2.00 70-13098ppbv1.9600

Trichloroethene 2.00 70-130100ppbv1.9900

n-Heptane 2.00 70-130108ppbv2.1700

1,4-Dioxane 2.00 60-160101ppbv2.0200

4-Methyl-2-pentanone (MIBK) 2.00 70-13096ppbv1.9300

cis-1,3-Dichloropropene 2.00 70-13094ppbv1.8900




Spike

Result

Source

%REC

%REC

Limits RPD

RPD





trans-1,3-Dichloropropene 2.00 70-13087ppbv1.7400


Toluene 2.00 70-130104ppbv2.0900

2-Hexanone (MBK) 2.00 70-13090ppbv1.8100

Dibromochloromethane 2.00 70-13097ppbv1.9400

1,2-Dibromoethane (EDB) 2.00 70-13097ppbv1.9400

Tetrachloroethene 2.00 70-130100ppbv1.9900

Chlorobenzene 2.00 70-130102ppbv2.0300

Ethylbenzene 2.00 70-130106ppbv2.1300

1,1,1,2-Tetrachloroethane 2.00 60-16074ppbv1.4700

m,p-Xylene 4.00 70-130109ppbv4.3600

Bromoform 2.00 70-13090ppbv1.7900

Styrene 2.00 70-130102ppbv2.0300

o-Xylene 2.00 70-130110ppbv2.1900


1,3,5-Trimethylbenzene 2.00 70-13089ppbv1.7800

4-Ethyltoluene 2.00 70-130103ppbv2.0600


Isopropylbenzene 2.00 60-160102ppbv2.0400

1,3-Dichlorobenzene 2.00 70-13090ppbv1.7900

Benzyl chloride 2.00 70-13090ppbv1.8000



1,2,4-Trichlorobenzene 2.00 70-13071ppbv1.4200

Hexachlorobutadiene 2.00 70-13072ppbv1.4400

sec-Butylbenzene 2.00 60-160112ppbv2.2400

4-Isopropyltoluene 2.00 60-160124ppbv2.4800

n-Butylbenzene 2.00 60-160107ppbv2.1400





























Spike

Result

Source

%REC

%REC

Limits RPD

RPD




















































Propene 10.0 70-130101ppbv10.1





1,3-Butadiene 10.0 70-13091ppbv9.11




Spike

Result

Source

%REC

%REC

Limits RPD

RPD







Acetone 10.0 70-13087ppbv8.72


Ethanol 10.0 19.7-13280ppbv8.05












Hexane 10.0 70-13090ppbv8.97






Benzene 10.0 70-13083ppbv8.34






1,4-Dioxane 10.0 60-16073ppbv7.29

n-Heptane 10.0 70-13090ppbv8.98





Toluene 10.0 70-13085ppbv8.46








m,p-Xylene 20.0 70-13083ppbv16.6

Bromoform 10.0 70-13078ppbv7.84

Styrene 10.0 70-13079ppbv7.90

o-Xylene 10.0 70-13084ppbv8.39







Benzyl chloride 10.0 70-13069ppbv QC26.93





Spike

Result

Source

%REC

%REC

Limits RPD

RPD







1,2-Dichlorobenzene 10.0 70-13069ppbv QC16.87


1,2,4-Trichlorobenzene 10.0 70-13054ppbv QC15.39

Hexachlorobutadiene 10.0 70-13055ppbv QC25.49


Duplicate (8091328-DUP1) Prepared & Analyzed: 17-Sep-08Source: SA84551-07

Propene 0.500 30ppbv UBRLBRL

Dichlorodifluoromethane (Freon12) 0.500 3011ppbv J0.4600.410

Chloromethane 0.500 30ppbv UBRLBRL

1,2-Dichlorotetrafluoroethane (Freon 114) 0.500 30ppbv UBRLBRL

Vinyl chloride 0.500 30ppbv UBRLBRL

1,3-Butadiene 0.500 30ppbv UBRLBRL

Bromomethane 0.500 30ppbv UBRLBRL

Chloroethane 0.500 30ppbv UBRLBRL

Acetone 0.500 3012ppbv 9.278.24

Trichlorofluoromethane (Freon 11) 0.500 30ppbv UBRLBRL

Ethanol 0.500 3010ppbv 7.236.54

Acrylonitrile 0.500 30ppbv UBRLBRL

1,1-Dichloroethene 0.500 30ppbv UBRLBRL

Methylene chloride 0.500 30ppbv UBRLBRL

1,1,2-Trichlorotrifluoroethane (Freon 113) 0.500 30ppbv UBRLBRL

Carbon disulfide 0.500 30ppbv UBRLBRL

trans-1,2-Dichloroethene 0.500 30ppbv UBRLBRL

1,1-Dichloroethane 0.500 30ppbv UBRLBRL

Methyl tert-butyl ether 0.500 30ppbv UBRLBRL

Isopropyl alcohol 0.500 3011ppbv 1.000.900

2-Butanone (MEK) 0.500 3014ppbv 2.822.45

cis-1,2-Dichloroethene 0.500 30ppbv UBRLBRL

Hexane 0.500 3011ppbv J0.5000.450

Ethyl acetate 0.500 30ppbv UBRLBRL

Chloroform 0.500 30ppbv UBRLBRL

Tetrahydrofuran 0.500 3016ppbv 4.333.68


1,1,1-Trichloroethane 0.500 30ppbv UBRLBRL

Benzene 0.500 30ppbv UBRLBRL

Carbon tetrachloride 0.500 30ppbv UBRLBRL

Cyclohexane 0.500 30ppbv UBRLBRL

1,2-Dichloropropane 0.500 30ppbv UBRLBRL

Bromodichloromethane 0.500 30ppbv UBRLBRL

Trichloroethene 0.500 30ppbv UBRLBRL

1,4-Dioxane 0.500 30ppbv UBRLBRL

n-Heptane 0.500 3012ppbv 0.9000.800

4-Methyl-2-pentanone (MIBK) 0.500 30ppbv UBRLBRL

cis-1,3-Dichloropropene 0.500 30ppbv UBRLBRL

trans-1,3-Dichloropropene 0.500 30ppbv UBRLBRL


Toluene 0.500 3011ppbv 1.731.55

2-Hexanone (MBK) 0.500 30ppbv UBRLBRL

Dibromochloromethane 0.500 30ppbv UBRLBRL

1,2-Dibromoethane (EDB) 0.500 30ppbv UBRLBRL

Tetrachloroethene 0.500 3012ppbv 2.752.45




Spike

Result

Source

%REC

%REC

Limits RPD

RPD





Chlorobenzene 0.500 30ppbv UBRLBRL

1,1,1,2-Tetrachloroethane 0.500 30ppbv UBRLBRL

Ethylbenzene 0.500 30ppbv UBRLBRL

m,p-Xylene 1.00 3011ppbv J0.3800.340

Bromoform 0.500 30ppbv UBRLBRL

Styrene 0.500 30ppbv UBRLBRL

o-Xylene 0.500 30ppbv UBRLBRL


Isopropylbenzene 0.500 30ppbv UBRLBRL

1,3,5-Trimethylbenzene 0.500 30ppbv UBRLBRL

4-Ethyltoluene 0.500 30ppbv UBRLBRL


1,3-Dichlorobenzene 0.500 30ppbv UBRLBRL

Benzyl chloride 0.500 30ppbv UBRLBRL


sec-Butylbenzene 0.500 30ppbv UBRLBRL

4-Isopropyltoluene 0.500 30ppbv UBRLBRL


n-Butylbenzene 0.500 30ppbv UBRLBRL

1,2,4-Trichlorobenzene 0.500 30ppbv UBRLBRL

Hexachlorobutadiene 0.500 30ppbv UBRLBRL




































Spike

Result

Source

%REC

%REC

Limits RPD

RPD













































Propene 10.0 70-13097ppbv9.69





1,3-Butadiene 10.0 70-13089ppbv8.86



Acetone 10.0 70-13086ppbv8.65


Ethanol 10.0 19.7-13279ppbv7.94






Spike

Result

Source

%REC

%REC

Limits RPD

RPD














Hexane 10.0 70-13089ppbv8.91






Benzene 10.0 70-13083ppbv8.34






1,4-Dioxane 10.0 60-16079ppbv7.86

n-Heptane 10.0 70-13088ppbv8.81





Toluene 10.0 70-13084ppbv8.36








m,p-Xylene 20.0 70-13082ppbv16.4


Styrene 10.0 70-13077ppbv7.73

o-Xylene 10.0 70-13083ppbv8.34







Benzyl chloride 10.0 70-13068ppbv QC26.80












Spike

Result

Source

%REC

%REC

Limits RPD

RPD





Propene 0.500 302ppbv 3.183.26

Dichlorodifluoromethane (Freon12) 0.500 300ppbv 0.7000.700







Acetone 0.500 300.5ppbv E211210

Trichlorofluoromethane (Freon 11) 0.500 300ppbv 0.6000.600

Ethanol 0.500 303ppbv 4.654.52





Carbon disulfide 0.500 305ppbv 2.222.12







Hexane 0.500 30ppbv UBRLBRL


Chloroform 0.500 300.6ppbv 1.741.75

Tetrahydrofuran 0.500 30ppbv UBRLBRL










n-Heptane 0.500 30ppbv UBRLBRL





Toluene 0.500 30ppbv UBRLBRL

2-Hexanone (MBK) 0.500 304ppbv 0.4800.500



Tetrachloroethene 0.500 300ppbv J0.4600.460




m,p-Xylene 1.00 303ppbv J0.6900.710



o-Xylene 0.500 304ppbv 0.5600.580






Spike

Result

Source

%REC

%REC

Limits RPD

RPD





1,3,5-Trimethylbenzene 0.500 30ppbv JBRL0.300


1,2,4-Trimethylbenzene 0.500 303ppbv J0.3100.320






















































Spike

Result

Source

%REC

%REC

Limits RPD

RPD




































Propene 2.00 70-13088ppbv1.7600





1,3-Butadiene 2.00 70-130101ppbv2.0200



Acetone 2.00 70-13088ppbv1.7500


Ethanol 2.00 70-17889ppbv1.7800















Spike

Result

Source

%REC

%REC

Limits RPD

RPD





Hexane 2.00 70-130102ppbv2.0500






Benzene 2.00 70-130104ppbv2.0700






n-Heptane 2.00 70-130102ppbv2.0500

1,4-Dioxane 2.00 60-16076ppbv1.5100





Toluene 2.00 70-130102ppbv2.0400








m,p-Xylene 4.00 70-130111ppbv4.4400

Bromoform 2.00 70-13091ppbv1.8200

Styrene 2.00 70-130102ppbv2.0300

o-Xylene 2.00 70-130108ppbv2.1700



























Spike

Result

Source

%REC

%REC

Limits RPD

RPD






























































Spike

Result

Source

%REC

%REC

Limits RPD

RPD














Propene 10.0 70-13087ppbv8.73





1,3-Butadiene 10.0 70-13093ppbv9.31



Acetone 10.0 70-13078ppbv7.76


Ethanol 10.0 19.7-13282ppbv8.25












Hexane 10.0 70-13094ppbv9.36






Benzene 10.0 70-13089ppbv8.92






1,4-Dioxane 10.0 60-16086ppbv8.59

n-Heptane 10.0 70-13094ppbv9.45





Toluene 10.0 70-13091ppbv9.07







Spike

Result

Source

%REC

%REC

Limits RPD

RPD









m,p-Xylene 20.0 70-13091ppbv18.2


Styrene 10.0 70-13086ppbv8.60

o-Xylene 10.0 70-13091ppbv9.07


















Dichlorodifluoromethane (Freon12) 0.500 3027ppbv 0.8100.620

Chloromethane 0.500 3029ppbv J0.4400.330






Acetone 0.500 3029ppbv 19.114.3

Trichlorofluoromethane (Freon 11) 0.500 3026ppbv J0.4300.330

Ethanol 0.500 3028ppbv 341257



Methylene chloride 0.500 3031ppbv QR511.38.33









Hexane 0.500 3024ppbv 0.8000.630



Tetrahydrofuran 0.500 3029ppbv 0.9200.690

1,2-Dichloroethane 0.500 3024ppbv J0.5500.430


Benzene 0.500 3026ppbv J0.4300.330




Spike

Result

Source

%REC

%REC

Limits RPD

RPD






Cyclohexane 0.500 3029ppbv J0.4800.360





n-Heptane 0.500 3012ppbv 1.771.57

4-Methyl-2-pentanone (MIBK) 0.500 3014ppbv J0.5500.480




Toluene 0.500 3012ppbv 23.620.9




Tetrachloroethene 0.500 30ppbv UBRLBRL



Ethylbenzene 0.500 303ppbv J0.3500.360

m,p-Xylene 1.00 302ppbv 1.141.16



o-Xylene 0.500 303ppbv J0.3400.330








1,4-Dichlorobenzene 0.500 302ppbv 1.111.13


























Spike

Result

Source

%REC

%REC

Limits RPD

RPD






























































Spike

Result

Source

%REC

%REC

Limits RPD

RPD







Propene 2.00 70-13094ppbv1.8800





1,3-Butadiene 2.00 70-130102ppbv2.0300



Acetone 2.00 70-13085ppbv1.7000


Ethanol 2.00 70-17884ppbv1.6900












Hexane 2.00 70-13095ppbv1.9000






Benzene 2.00 70-13094ppbv1.8800






1,4-Dioxane 2.00 60-16096ppbv1.9100

n-Heptane 2.00 70-13096ppbv1.9200





Toluene 2.00 70-13094ppbv1.8700







m,p-Xylene 4.00 70-13094ppbv3.7700


Bromoform 2.00 70-13084ppbv1.6900

Styrene 2.00 70-13094ppbv1.8800




Spike

Result

Source

%REC

%REC

Limits RPD

RPD





o-Xylene 2.00 70-13094ppbv1.8800
























































Spike

Result

Source

%REC

%REC

Limits RPD

RPD






































Propene 10.0 70-13097ppbv9.73





1,3-Butadiene 10.0 70-13088ppbv8.82



Acetone 10.0 70-13084ppbv8.43


Ethanol 10.0 19.7-13279ppbv7.94













Spike

Result

Source

%REC

%REC

Limits RPD

RPD







Hexane 10.0 70-13088ppbv8.79






Benzene 10.0 70-13081ppbv8.14






1,4-Dioxane 10.0 60-16069ppbv6.94

n-Heptane 10.0 70-13088ppbv8.83





Toluene 10.0 70-13082ppbv8.21








m,p-Xylene 20.0 70-13081ppbv16.1


Styrene 10.0 70-13077ppbv7.67

o-Xylene 10.0 70-13082ppbv8.25


















Dichlorodifluoromethane (Freon12) 5.00 30ppbv UBRLBRL







Spike

Result

Source

%REC

%REC

Limits RPD

RPD








Acetone 5.00 302ppbv 16.016.4

Trichlorofluoromethane (Freon 11) 5.00 30ppbv UBRLBRL

Ethanol 5.00 301ppbv 693684










2-Butanone (MEK) 5.00 30ppbv UBRLBRL


Hexane 5.00 30ppbv UBRLBRL



Tetrahydrofuran 5.00 30ppbv UBRLBRL










n-Heptane 5.00 30ppbv UBRLBRL





Toluene 5.00 305ppbv 8.708.30




Tetrachloroethene 5.00 30ppbv UBRLBRL




m,p-Xylene 10.0 300ppbv J2.502.50



o-Xylene 5.00 30ppbv UBRLBRL











Spike

Result

Source

%REC

%REC

Limits RPD

RPD















Notes and Definitions

Analyte may be biased low based on QC recovery. Passed in CCC.Z-2

Analyte included in the analysis, but not detectedU

RPD out of acceptance range.QR5

Analyte out of acceptance range in QC spike but no reportable concentration present in sample.QC2

Analyte out of acceptance range.QC1

Detected above the Method Detection Limit but below the Reporting Limit; therefore, result is an estimated

concentration (CLP J-Flag).

J

The concentration indicated for this analyte is an estimated value. This value is considered an estimate (CLP E-flag).E

RPD Relative Percent Difference

dry Sample results reported on a dry weight basis

BRL Below Reporting Limit - Analyte NOT DETECTED at or above the reporting limit

NR Not Reported

A plus sign (+) in the Method Reference column indicates the method is not accredited by NELAC.

Laboratory Control Sample (LCS): A known matrix spiked with compound(s) representative of the target analytes, which is used to

document laboratory performance.

Matrix Duplicate: An intra-laboratory split sample which is used to document the precision of a method in a given sample matrix.

Matrix Spike: An aliquot of a sample spiked with a known concentration of target analyte(s). The spiking occurs prior to sample

preparation and analysis. A matrix spike is used to document the bias of a method in a given sample matrix.

Method Blank: An analyte-free matrix to which all reagents are added in the same volumes or proportions as used in sample

processing. The method blank should be carried through the complete sample preparation and analytical procedure. The method

blank is used to document contamination resulting from the analytical process.

Method Detection Limit (MDL): The minimum concentration of a substance that can be measured and reported with 99%

confidence that the analyte concentration is greater than zero and is determined from analysis of a sample in a given matrix type

containing the analyte.

Reportable Detection Limit (RDL): The lowest concentration that can be reliably achieved within specified limits of precision and

accuracy during routine laboratory operating conditions. For many analytes the RDL analyte concentration is selected as the lowest

non-zero standard in the calibration curve. While the RDL is approximately 5 to 10 times the MDL, the RDL for each sample takes

into account the sample volume/weight, extract/digestate volume, cleanup procedures and, if applicable, dry weight correction.

Sample RDLs are highly matrix-dependent.

Surrogate: An organic compound which is similar to the target analyte(s) in chemical composition and behavior in the analytical

process, but which is not normally found in environmental samples. These compounds are spiked into all blanks, standards, and

samples prior to analysis. Percent recoveries are calculated for each surrogate.

Validated by:

Hanibal C. Tayeh, Ph.D.

Nicole Leja

Rebecca Merz



SPECTRUM ANALYTICAL, INC. HANIBAL TECHNOLOGY … · 2011. 12. 15. · Sample Identification S52-VMP...

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Transcript of SPECTRUM ANALYTICAL, INC. HANIBAL TECHNOLOGY … · 2011. 12. 15. · Sample Identification S52-VMP...