Semtvolatile HSL Compounds (Pagel) Case No: 3SQ>7~- … · 2020-02-20 · ^B G o T 5i1 ^ ^ » c E a...
143
Initial Calibration Data Semtvolatile HSL Compounds (Pagel) Case No: 3SQ>7~-_________ Instrument tD; Contractor: gMCOTT&C-___________ Calibration Date: 3./M-/&S" Contract No: 6&-g»3-"feWf_______ Minimum RF forSPCC is 0*050 Maximum % RSD forCCC is 30% Hesponw Factor (subcchpt is th« amount of nanogramt) SPCC -Syswm P«r*ormance Check Compound* (e.j RF -Avtrae« Retoonsa Factor , t -not d«tectataf« at20 ng %RSD -Parcam Relative Standard Daviation CCC -Cal.brat.on Chack Compound.M " - FormVI 4/84
Transcript of Semtvolatile HSL Compounds (Pagel) Case No: 3SQ>7~- … · 2020-02-20 · ^B G o T 5i1 ^ ^ » c E a...
Initial Calibration DataSemtvolatile HSL Compounds
(Pagel)Case No: 3SQ>7~-_________ Instrument tD;Contractor: gMCOTT&C-___________ Calibration Date: 3./M-/&S"Contract No: 6&-g»3-"feWf_______
Minimum RF for SPCC is 0*050 Maximum % RSD for CCC is 30%
Hesponw Factor (subcchpt is th« amount of nanogramt) SPCC -Syswm P«r*ormance Check Compound* (e.jRF -Avtrae« Retoonsa Factor , t -not d«tectataf« at 20 ng%RSD -Parcam Relative Standard DaviationCCC -Cal.brat.on Chack Compound. M
" -FormVI4/84
Initial Calibration DataSemivolatile HSL Compounds
(Page 2)Case No: -33O1—_____' Instrument ID:Contractor: COTEC, _________ ___. Calibration Date- 3-/2~:L/&S"
Contract No:
Minimum RF for SPCC is 0.050 Maximum % RSD for CCC is 30%
Laboratory ID ita. i'2.-B.3-
Compound RF120 «F160 RF %RSDCCC-SPCC
2. 4-Dinitrotoiuent2. 6-Pinitfototuene_____ &.'&Diethylphthalate
0.3ZV
4 - Chlor ophenyl -phanytetherFluorene ^ »•4-Nitroaniiine ii>. :L-S|
w. )°ilo/zet
4. 6-Dmttro-2-MethytphenolN-Nitrosodiphenylamine (1 )4 - Bromophenyl -pheny let herHexachlorobenzene o.l&lPentachiorophanol O.tOf /3PhenanthreneAnthracene 6Dt-N-ButylphthalateFluorantheneBenzidme 7®PyreneButylbenzylphthalate 2-33. S'-Dichlorobenzidme O.6ST SiBenzofa fcAnthrace ne .S6C. Abis<2-£thylhe*vl|Phthalaie 0.899 3? --Chrysene LSI JDi-n-Octyl PhthalateBenzo(b)Fiuoranthene /.Z-30 /&Benzo( k |F luora nthene i.J-S* /aBenzoiajPyrene o.eeoIndenoO. 2. 3-cd}Pyrene . 5 S 5Dioenz(a. hlAnthraeene
h. t}Perylene O-foS"? /s
Response Factor {subscript is the amount of nanograms) SPCC -System Performance Check Compounds (••)RF .Average Response Factor t -not dttectable at 20 ng%RSD -Percent Relative Standard Deviation 0) 'Cannot be separated from dtphenylamineCCC -Calibration Check Compounds (•)
FormVt
ARIQ'03304/B4
uonunuing uaiioration CheekSemivolatiie HSL Compound*
(Pagel)
Case No:Contractor: &V >7&C _______ Time:Contract No: && -&*-&-&¥ Laboratory ID:instrument ID: _____ &&L ________ Initial Calibration Date:
Minimum RF for SPCC is 0.050 Maximum %D for CCC is 25%
Compound %D CCC SPCCN • Nit rosodimethyta mine APhenolAniline AO/O ryt*-* Ebut • 2 -ChloroeihyljE th«r2-ChlofOpheno*
1. 4-OtchtorobenzeneBenzyl Alcohol 0,3/2- Mo » os i *h if2-Oichlorobanz«ne2 • Methylphenolbi&(2 -chloroi£Qprocyl}£lher4-MerhylphenolN-Nrtroso-Di-n-Propyiamine 0.2.3CHe xachlor oethane HNitrooenzene mIsophof one ,2-Nnrophenof £3-7,3?2,
0,1V*]-• 2 -CnlocoeihoxyJMethane
2. 4-Dichlorophenol O-T-BQ1 2 4-TnchlofObenzene O-30/Naphthalene4.ChloroanilmeHexachtorobuiadiene4 Cnloro-3-Methyiphenoi
Hexachlofocyclcpentadiene 0,3/2- 2-S2. 4, B-TrtchJoropheno* 0-3&5"2, 4, S'Tnchlorcpheno!2 • Cnioronaptithalene2 -Nirroarwlme Z2-Otmethyl PhthalateAcenaphthyfene3-MtiroanihneAcenaphthene A302. A/332 4-Diniuophenot Q.t+l4>Nitropr>enoJ 2.3Dibenzofuran A
RP50 H*«»"** acior *rom daily standard file at concentration %0 -Percent Differenceindicated CCC -Calibration Check Compounds (.}
RT Average Response Factor from initial calibration FermV) SPCC -System Performance Check Compounds {••)
Form VII 4/84
Continuing Calibration Check. Semivolatlle HSL Compounds
(Page 2)
Case No: 3603____________ Calibration Date:Contractor: &JCz>T&C~_________ Time: ______Contract No: G& -Vlrdfo _____ Uboratory ID:Instrument ID: - ______ ; ____ initial Calibration Date:
Minimum RF for SPCC is 0.050 Maximum %D for CCC is 25%
Compound2, 4-OinrtrotoiiMfW2, C-OinrtrotoiuaneDiethylphthjlate4.Chtoroph«nyi-phenyl«th*fFiuoren*4-Nitroaniline4, 6-Dinitro-2-Methyfph*nolN-Nitro*odiph«nyiamine (1 14-Bromoph*nyt-phenyietherHexach lorobonzenePentachlorophenolPhenanthren*AnthraceneDi-N-BulylphthalattfFluor ant heneBenndintPyreneButylbenzylphtha late3, 3'-Dtchlorobenzidin«BenzofalAnthracanebis{2-EthylheKyf)PhthaiateChryseneOt-n-Octyl Phthalate8enzo(b)FluorantheneBenzofk^luorantheneB«ruo<»)Pvf9netndeno(1 . 2. 3-cd)Pvren«Dibenfla, h AnthraceneBenzofg. h, i)Perylene
Iff
o.3"?-r0,32 2-/.31&O.LSS"/.33S"CU2-»^cx/6?0- f?O,^SX-G.f&lo./o//,0&O.1/3/./Vfo.*wgO.*f73
• 2*0<?f*l.t+lo.*f-ie/.V3*-Q.B?*/.&J-!J'3-7-*?AZ-3OA/O^A0-6600.&S9O.&OQn.c,S?
RF80O-3300, *7"?"/./990.5&SJ.I&S0./?30.15*1o.(* OA0- /.ST5o.f(*o0. OSZ-0-9SOO.&OI/.ti4~0.&3G
•*•/.py/A/3/O,3O#/.zsg0.1Wl*3(p®A¥*^0.7WA 06^O,"76?.SS6»
D.59J5"0, ?-
SD
/2-6
\<Z>ti-llWZ) -ia>is-13i-z~/a1.1I7<*?**/7——
/0/5Iff&/2~3/•£j(-/3///0
CCC
-Ni5ir\«&i-tvJ^V*
*
*
*
*
SPCC
0
• *
RFtn -Response Factor from daily standard tile ai concentration CCC -Calibration Check Compounds {•)indicated SPCC -System Performance Chech Compounds
RT -Average Response Factor from initial calibration Form VI (1) -Cannot be separated from diphenylamme°»D Percent Difference . _
Form VII
WI00332 4'84
Continuing Calibration CheckSemivolatile HSL Compounds
(Page!)
Case No: 3&03____________ Calibration Data:Contractor: /CQ-TgC._________ Time: _______ll:Zg>Contract No: - - - - ______ Laboratory ID:Instrument ID: (25GSL. _________ - Initial Calibration Date:
Minimum RF for SPCC is 0.050 Maximum %D (or CCC is 25%
Compound RF %D CCC SPCCN • Nitrosodimethylamine A 7/3 75"PhenolAniline 14t»t(-2-CMoro*thyl)Eth«r 2-.2 •Chloropbenoi1 , 3 Dtchiorobcnzene 1.ST&
7 33Beruryl Alcohol f.cxfi2-Methylphenol /.sen*bis(2-cftioroi*opfopYl)Elh*r4. MethylphenolN-Nitroto-Cfc-n-PTOpytamine 23 * *HexachioroethaneNitrobenzeneisophorone2-Nitrophenol2, 4-Dimathylphenol 7-0Benzoic Actdbis{ • 2 -ChloroeihoiyJMetriane2. 4-Dichlorophenoi £>.*-«??1 2, 4 TnchlorobemeneNaphtnaiene4-Cnlorosndinr &.2&CHe xachlor obutadiene4 - Chloro-3-Methyipheno!2 • MethylnaphinaleneMexdchior ocyclopentadjene -2 4, 6-Tr»chiorophenol /o24 5-Tr»chIorophenol2-Chloronaphihftlene2'NitroamtineDimethyl PhthatateAcenaphthylene3 NiuoanihneAcenapnthene2, 4-Dmitrophenol4-NitrophenoiDrbenzofuran
P*cio* from daily standard file at concentration %D -Percent Differenceindicated CCC -Calibration Check Compounds (.)
ST Average Response Factor from initial calibration Form VI SPCC -Sv*«W Bertormance Check Compounds (• 0*« Iff§333Form VII ^wv
Continuing Calibration Ctwck ._,S«mivolatile HSL Compounds
(Page 2) lr
Case No: 3&03___________ Calibration Date:Contractor: &SC&7T£C~ ______ Time:Contract No: —J^ ______ Laboratory ID:Instrument ID: ____ - |nitiai Calibration Date:
Minimum RF for SPCC i> 0.050 Maximum %D for CCC is 25%
Compound RF %D CCC SPCC2, 4-Diniiroto*i>ene Z-fc2, o-Dmrtrotolueoe 2-3Dtethyiphthalata4-Chlwophenyf-phenytather 2.0Ftuoren*4-Nitroaniltne4. 6-Dinitro-2-Methylph«nol O./ft?N'NitrosodiphcnyUrnin* (1 )4'Bromoph*nyt-pnftnyl0th*rH«xachk>rob«nrene O.i&l Z-2-Pentachlorophenol o. ftPhenanthraneAnthraceneDi -N -Butyl PhthalateFluoranthene /sBenzidin*Pyreon 2-0Butylbenrylphthalata A / /
"$£&'zo
3, S'-DtchJorobenzHJine itBenjotaiAnthraconebi s(2 -Chrysene i.Di-n-Octyl Phthaiata A6enzo(b)Fiuoranthen« AZJOBenzotk)F| uoranthene /3Benxo(a)PyTtneIndanofl . 2. 3-cd)PveneDibenz(a, h)Anihric*n* iBenzo(g. h. i)Perytan«
RFgQ -Response Factor from daily standard t*te at concentration CCC -Calibration Check Compounds (•)indicated SPCC -System Performance Chech Compounds {* •)
HT -Average Response Factor from initial calibration Form Vt (1) -Cannot be separated Irom diphenylamineDoD Percent Difference •
••—T-Form Vt)
4/84
Case -o. __*Contract No. .Date of Analj
EVALUATIONLABORATORY
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D+caf kjorotrlph«nylpho*ph!n«t (DFTPP)Contract No.
-- " - • * • • • iRsd)Contractor tt1*sQ\ £d———————, Contract No. ittS-iJl- £
tnitrgmfm ID Qffl Dm ———=^— / —————————— Tin*
mto ION ABUNDANCE CRITERIA %RELATIVE ABUNDANCE61
at00
70
t27
197
1M
1»
275
366
441
442
443
30.0 ' OOM ol man 190
Im then 2.0% of n»» 9
m*M 00 rtiative tbundtnct
1m ttien 2 J* of mm 69
40.0 • O0.» of me» 198
IMS tfwt 1 J% of miu 199
bM» pt«kr 100% rttHhrt ebundeACi
6.0 - 9JQ* ol mm 191
10.0 -30.0% of m«» 198
pMt* then 1,00% Of m*u 19§
prtwnt. but *ttt lh»n mnu 443
fleeter lhan 40.0% of mt» 198
17.0- 23.0% of mi«i442
¥-3.7- \O Co.V6.7® «zj;
Vo-o<2>
/00
6,76/«,.<?A3S"?.«£rS*C0
/B.C, W.&1V«iut tn perenthMJi is % m» 60'Value in pertnthetii i| % maw 442.THIS f£KFORMANCE TUNE APftlES TO THE FOLLOWINGSAMPLES. BLANKS AND STANDARDS.
SAMf LI ID LAtID DATE OF ANALYtlS TIME OF ANALYSIS
1.7.
13
ftR!D0338
DtcafJuorotrlphtnylphotphin* (OFTPP)Cm No. ,. 3603 f y*Sg> con a, —&SCCT&C—————— Contract No.
Inttrumtm ID - *~ D-f - .j-Pg/frST
ID
m/. |OM ABtmOANCC CRITERIA KRELATIVE ABUNDANCESI
*89
70
T27
197
199
198
27S
306
441
447
443
30J)-8fXO%af MHT98
** thin 2.0% of mutOO
im» 89 rtUttvt abcvidanc*
.t j.oxo/~-«r40.0 * 804)% o* mo* f 98
IwthMlA^MalM
UM peek, 100% rtiitirt abundmci
M.fJUrfmMUW
J00.3aO»of««i«8
gr««tor ttiM 1J30% of mm 198
prntftt. but tea thjn mw» 443
oruttr than 4QJJ% of mew 108
t7.0-23.0%ef n»«W
S.S<2> ( )f
5Sf0 (<2)'i,7<5
/00
75/w*» ^
/ jL- %••* /O
//.V- fA<3J*V*H* in portnthtti* It % R»» 88. 2?2V«lut In ptrtnthttfe Is % flmt 442. XITHIS PERFORMANCE TUNE APPLIES TO THE FOLLOWING CDSAMPLES, BLANKS AND STANDARDS. CD
SAMPLE ID LAB 10 DATE OF ANALYSIS TIME OF ANALYSIS
tRt
CALIBRATION
Dtcafluorotriphenylphosphine (DFTPP)No. contractor
Instrument ID w~ Date ~'"("=_________ Time
Lab in **** r rl.5 J- Data Retgase Authorized By: _
m/t ION ABUNDANCE CRITERIA %RELATIVE ABUNDANCE51
68
69
70
t27
197 .
198
199
275
365
441
442
443
30.0- 60.0% of mass 198
less than 2.0% of mass 69
man 69 relative abundance
less than 2.0% of man 69
40.0 - 60,0% of mass 198
ieu than 1.0% of mass 198
bast peak, 100% relative abundance
5.0 -9.0% of mass 198
10.0 -30.0% of mass 198
greater than 1.00% of mass 198
present, but less than mass 443 •
greater than 40.0% of mass 198
17.0 -23.0% of mass 442
0* J5
C C^>'
11.7c f ° Jy/,J~r
• o/£>& .C
iv.'ic,S.K
/,z19.*J
bV. 90U.*4 (/? )2
Value in parenthesis is % man 69.'Value in parenthesis is % mass 442. CDTHIS PERFORMANCE TUNE APPLIES TO THE FOLLOWING -3"SAMPLES. BLANKS AND STANDARDS.
CDCD
SAMPLE ID LAB ID DATE OF ANALYSIS TIME OF ANALYStS3^
*H
WC/aVIS TUNING AND MASS CALIBRATION ,dfBromofluorobanzen* (BFB)
C.«NQ. contractor OontfKfl*,tn
Ub ID Data Rtlei$t Authorteed fly:
m/e ION ABUNDANCE CRITERIA %RELATIVE ABUNDANCE
50
75
95
96
173
174
17S
T7S
177
75.0 . 40.0% of Iht fca» peak
3OO • 80)% of tht bnt p«k
Saw p«*k, 100% relative abundanct
E.O - B.0% of tht bast paafc
Ltu than 7.0% of the bat* peak
Greater than 50.0% of th« bast peak
S.O- 9*0% of ma» T74
Greater than SS.0%, but late than 101.0% of mail 174
5.0 • 9,0% of man 176
za. s~zs.7
/<Z><2>
T-0
7L.I#<? C )'
"73.3 CW-s) '4 C )2
V*Jo» in porcnthtsli it % man 774.in parvmhtsfs is % mau 275.
THIS PERFORMANCE TUNE APPLIES TO THE FOLLOWINGSAMPLES, BLANKS AND STANDARDS.
SAMPLE LAB ID DATE OF ANALYSIS TIME Of ANALYSIS
C-7302.
PR03ECT NAME; SouM/JljiU? Sajpflla- EPA SITE NO.: Vfl |2 1TDD NOs F ftO-Oftloft l « ' "T REGION;
QUALITY ASSURANCE REVIEW OFINORGAFllC ANALYTICAL DATA PACKAGE
Case No.: <3 Co O D ______________ _ Applicable Sample No's.:Contract No.; /o8-n/r-kft§2 ________ . _ WY^tt3OfrnC4?3f; Wf 43-32,Contract Laboratory: .VEfiSAft. . WV^rvP^!) Vng4l1-l;Applicable IFB No.: _______ „Reviewer: ~Review Date: S5 ____________ WTfa W^RZ.
The inorganic analytical data for this case has been reviewed. The quality assurance evaluation issummarized in the following table:
Reviewer's Evaluation*
AcceptableAcceptable with except onis.juestionaWeJnacceptabie
FractionTASK 1
ICPor AAMETALS
/£\ f*3
TASK 11FURNACE AAMETALS
y , *3
TASK IICOLD VAPOR A AMERCURY
/43
TASK IIICYANIDE
v/
* Definitions of the evaluation score categories are listed on next page.
This evaluation was based upon an analysis of .the review items indicated below:
• DATA COMPLETENESS • INITIAL CALIBRATION VERIFICATION• BLANK ANALYSIS RESULTS • CONTINUING CALIBRATION VERIFICATION• MATRIX SPIKE RESULTS • INTERFERENCE QC RESULTS• DUPLICATE ANALYSIS RESULTS • DETECTION LIMITS RESULTS• STANDARD ADDITIONS RESULTS • INSTRUMENT SENSITIVITY REPORTS
± • QUANTITATIVE CALCULATIONS
Data review forms are attached for. each of the review items indicated above.No errors noted, no form attached.Q Spot C heck perf orm ed.
Comments: H lpOjv /Luu (vlxwK On Jyp 1/1 rLkCMr*4 a&tr£>
ARiOOSlf
DATA EVALUATION SCORE- CATEGORIES
ACCEPTABIE: Data, is within established control limits, orthe data which is outside established controllimits does not affect the validity of theanalytical results.
AOCEPgABJJE WISH EXCEPTIONCS ) .• Data is not completely withinestablished control limits. The deficiences areidentified and specific data is still valid,given certain qualifications which are listed below
E: Data is not within established control limits.The deficiences bring the validity of the entiredata set into question. However, the data validityis neither proved nor disproved by the availableinformation«
UKAOCEPTA3I£: Data is not within established control limits.The deficiences imply the results are not meaningful.
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DATACOMPLETENESS
FIELD QC
TASK 1 ;1 WM ~ v n MM.METALS
TASK II :FURNACEAA:METALS
TASK 11 :COLD VAPORAA:- .MERCURY
TASK Mi:CYANIDE
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COMMENTS:(I) RESULT REPORTED BY LABORATORY AND CONFIRMED BY REVIEWER.____________________________________
(2) RESULT INFERRED FROM QUANTITAT10N LIST, DIASNOST1CS, CHROMATQGRAM AND/OR SPECTRA.
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BLANKS
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XKZTZAL AND CONTINUING CALIBRATION VEEIrtCATtON3
LAB HAKE VgrsJW- Tv\c • CASE NO.SOW HO. "1 t
n*TC \-S^-€^ nxitsInitial C*llb.*_________Continuing Ctlibneion2
H«alsk:1. AluilSUX
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B - S
Form II c- "Q. C. Eeport No. I lu
INITIAL AND CONTINUING CALIBRATION VERIFICATIOS3
LAB NAME Vl. bft'T , Tn c , CASE NO.SOU NO.
DATE __\ - 07- "&S UNITSCompound
, ' j ?Initial Calib.1 Continuing Calibration14
H*tal«S
1. Alumimia2. Antinonr3 . Arsenic4. B*riuBS. Berjllina
t * C QS UA
7. Calcium8. ChroaiuQ9. Cobalt10. Cop?*r11. Iron12. Lead13 . Magnvaium1 4. M4n£«no*«15. Mercury •16. HidMl17 . Potasiiua18. S«l»niua19, Silver20. Sodium21. Thallium22. Tin__23. Vanadium24. ZincOther:
Cyanide
True Value found I& True Value
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B - 3
fiR100366
Form IIQ. C. Eeport No.
INITIAL ANB CONTINUING CALISSAIION VERIFICATION3
LA3 HAKE j .rsfl/- s T>>f . CASE NO.SOW NO.
DATE ) -2-2-g^ ________ ' UNITSCompound, ____lai tlal_Calib._*__________Continuing Calibration2lietais:1. Aluminum2. Antimony3. Arsenic4. BariusS. Beryllium6. Cadmium7. CalciumS. Chromium9. Cobalt '10. Casper11. Iroa_ _12. Lead13. HaxBecium14. Maairaaeee15 . Mercury •16. Hiefcel17. Foeaszinm18. SeleniumIf. Silver20. Sodium21. Thallium22. Tin23. Vanadium2 4. ZincOther:
Cyanide
True Value
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B - 8
form II G?Q. C. Report No. | "?S
INITIAL AND CONTINUING CALIBRATION VERIFICATION3
us SAKE U?.r-sAr-. L»\s. CASE NO.SOW NO.
CompoundHetalsk:1. Aluminum2. Antimony3. Arsenic4. Barium3. Beryllium6. Cadmium7. Calcium8. Chromium9. Cobalt10. Copper11. Iron12. Lead13. Magnesium1 4.. Manganese15 . Mercury •16. Nickel17 . Potassium13. Selenium19. Silver20. Sodium21. Thallium22. Tin23. Vanadium24. ZincOther:
Cyanide
InitijTrue Value
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B - 8
;-&
Fora IIQ. C. Report No.
INITIAL AND CONTINUING CALIBRATION VERIFICATION3
LAB SAME V|g_rt>Ar- ] XA* . CASE NO.SOW NO.
vaz-e^_____ OSITS'Camggund ____Initial ._e*jHb. *_________Continuing Calibration2HccalsS1. Aluminum2. Antimony3. Arsenic4. Barium5. Berylliumt. Cadmium7. CalciumS. Chromiumf. .Cobalt10. CopperU. Iron12. Lead12. Magnesium14, Kanyaneee15. ercurj16. Sickel17. Potassium18. SeleniumIf. Silver20. Sodium21. Thallium22. Tin23. Vanadium24. ZiacOther:
Cyanide
True Value
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B -
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APPENDIX G
AJU 00372
V f r< r.
grwronmtnMl Protection Agency. CLPSampJe Management Qtfict,P, 0, Box 818. Afffunana. Virprnra 22313 703/557-2490
Organic* Analysis Data Sheet(Page 1)
Laboratory Name: Gu££ South Research Institute Case No; . 3& 0Lab Sample /D No; r4 lp O /_____________ QC Report No;
Sample Number
Samnfa Mam* i.A M-TC ^ .- —r-J_____xi Contract No; 66-01-Data Re/ease Authorized By: - FX ^ ^ Date Sample Received;
VofatiJftjCompoundcConcentration: (Low J Medium (Circle One)
Date An •l««rf."1/ /> /?*/ f '
C0nf?/pif Pftao*" „ ' ' nH Iff ' f *^
CAS
74-87-374.S3-975-01-475-OO-37S-09-267-64-17S-1S-075-35-475-34-3156-60-567-66-3107-06-27S-93.371-SS-656-23-5103-05-475-27-4
PercentPercent
<CrUoromemaneBromomeman*Vinyl CnlorideChlorofltnaneManftvf»n« Cntoride - .AcetoneCarbon OtsulfideT, 1 -D/chloroatnene1, 1 -Dich(oro«tn»neTranj-1, 2-DtchioroetheneCn/QToform1, 2-OjchforoernanB2-Suianone /51 j1, 1. 7-Tricnfonwman*Carbon TerracftlondsVirtyj AcerateSromodfcnforametnane
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79-34-578-87-510061-02-679-01-6124-48-179-00-571 -43-210051-01-5110-75-875-25-2531-78-6108-10-1127-18-4108-88-3108-90-7100-41-4100-42-5
1. 1.2. 2-Tetraeriloreemane1, 2-DtcNoroprooaneTrans-1. 3-0>cnioroorooeneTnehforoethene0)6romoen(oromerh»nc1. 1 2-TncrMoroeirtaneBenzeneci5-1,3-rJrcnJoroDroo«ne2-Chforo«tnvfv(nviernerSromoform2-HeKanone4.M«Tnvt-2-PenianoneTetracnforoetheneTolueneChlorooenjeneEthv/twnzeneSlyrcnffTora' Xvfertss
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Organics Analysis Data Sheet(Page 2)
SermveJatile CompoundsConcentration: f.Low/ Medium (Circle One)
Sample Number
hfDate AnalvConc/Dil F
CAS (Number62-75-9108-95-262-53-3111-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-73963S-32-9106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-965-85-0111-91-1120-83-2120-82-191-20-3106-47-887-68-3S9-50-791-57-677-47-488-06-295-95-491-58-788-74-4131-11-3208-96-899-09-2 -~
N-NitrosodirnetnvlarninePhenolAnilinebis(-2-ChioroethvltEiher2-ChloroDhenol1. 3-Dtchlorooenzene1 . 4-DichlorobenzeneBenzvl Alcohol1. 2-Dichlorobenzene2-Methvlpnenolbis(2-chloroisopropyl)Eiher4-MetnvionenolN-Nitroso-Di-n-PropylammeHexachloroema neNitrobenzeneIsophorone2-Nitroonenoi2. 4-OimethylDnenolBenzoic Acidbis(- 2-Ch loroethoxyjMethane2. 4-Dicnloropnenol1 . 2, A-TnchlorobenzeneNaphthalene4-ChforoaniitneHexachloroouiaaiene4-Chloro-3-Metrtyiphenoi2-MethytnaphthaieneHexacniorocvclopemaaiene2. 4. 6-Tnchloroonenot2, 4. 5-Trichloroohenoi2-Chloronaomnalene2-NitroanilmeDimetnvl PhthalateAcenapnthvlene3-Nitroantline
7frt- ft-nT- | £yartnr" ^ 0 O
' ug/jjarug/Kg CAS (*~ circl* On»j Number
to io/O (tn L<-fO tu-fO i*-1C W_/C iw/n LW;o tc/C tc/O U-;n i —;0 M-/D tCfD lw/O fcLr n t^/ D (LTO w-10 /O twIO U10 K-,/O iv/Ot.i!O (,-;o t\-tn tciO n.
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83-32-951-28-5100-02-7132-64-9121-14-2606-20-284-66-27005-72-386-73-7100-01-6534-52-186-3O-6101-55-3118-74-187-86-585-01-8120-12-784-74-2206-44-092-87-5129-00-085-68-791-94-156-55-3117-81-7218-01-91 1 7-84-0205-99-2207-08-950-32-8193-39-553-70-3191-24-2
Acenapnthene2. 4-Dmitropnenol4-NitroohenolOibenzofuran2. 4-Dinitrotoluene2. 6-DinitrotolueneDiethyiohthatate4.CntoroDhenvl-oheny|etherFluorene4-Nitroanitme4. 6-Dinnro-2-M«thylpnenolN-Nitrosodtphenylamine (114-BromoDhenyl-phenytemerHexachlorobenzenePentachlorophenoi ,3-Dc C1PhenanthreneAnthraceneOi-n-ButylphthalateF luoranrhene /^\ J^BcnzidmePvrene / O TButvlbenzyiphthaiate3, 3'-OichtoroaenziameBenzoo (AnThracenebis(2-Ethvihexvi)PhmaiateChrvseneDi-n-Octyl PhthalateBenzcKDiFluorantheneBenzo<"i(tFiuorantheneBenzo<a)Pvrenelnaen« 1 . 2. 3-cd)PvreneDtbenzta. htAntnraceneBenzwg. h. i)Pervl«ne
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V,
Organrcs Analysis Data Sheet
Sample Number
f(Page 3) L Jt,- 0
Pesticide/PCBsConcentration: (LOW /Medium, {Circle One)Date Extracted/Prepared:Date Analyzed: _JJ
/Conc/Dil Factor: ^ &CAS ,—• Lug/lp/ug/KgNumber . . ——TCircl* One)319-84-63T9-8S-7319-85-858-89-976-44-8309-00-21024-57-3959-98-86O-57-172-55-972-20-833213-65-972-54-87421-93-4.1031-07-8SO-29-372«J3-553494-7Q-557-74-98001-35-212674.11-211104-28-211141-16-553469-21-912672-29-611O97-69-111096-82-5
Aipna-SHCBeta-BHCDelta -BHCGamma-BMC (Lmoane)HeotacniorAldnnHffotachfor EnoxiaeEndosuifan IDieiorin4. 4--DDEEndnnEnOosuifan II4, 4'-DDDEndrm AidehvoeEndosuifan Suffate4. 4%DOTMethoxvchlorEndrrn KetoneChlordaneToxaoneneArocior-1016Arocfor-1221Arocior-1232Aroclor-1242Aroclor-1248Arocior-t25dAroctor-1260
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Laboratory N
Sample MatrData Release
CASNumb* i174-87-374-83-975-01 -475-00-375-09-267-64-175-15-075-35-475-34-3156-60-567-66-3107-06-278-93-371-55-656-23-5103-05-475-27-4
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ConcentrDate £xttDate AnaConc/DtPercent PPercent f
ChloromernaneBromometfianeVinyl ChlorideChloroernaneMethylBne Chloride ;QAcetoneCarbon Disufftde1. 1 -Drchlorofltnene1, l-DichloroetnaneTrans-1, 2-DichtoroerheneChloroform1. 2-Dichloro«tnane2-Butanone '- ^1,1. 1-TrrchloroetnaneCaroon TetracntondeVmy[ AcetateBromoOichlorometnane
Volatilfl-iation: [Low
V— *•acted/Preparev*"ri> ' A
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Sample Number
(\ - o? ys Data Sheet1}Case No: 30 0QC Report NcContract No:Date Sample
soundsdium (Circ* h m
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1. 1. 2. 2-TerracnioroeTnane1. 2-DtcnioroprooaneTrans-1. 3-DicnioroorooeneTricnioroetncne «5 TD ibrom ocn (orometha ne1.1. 2-TrtchloroetnaneBenzenecrs-1. 3-Dich(oroorooene2-Chloro«invfvinvletherBromoform2-Hcxanone4-Metnyl-2'PentanoneTetrachioroetneneTolueneChlorobenzcneEthytbenzeneStyreneTotal Xvt*n«
— ug^orug/Kg" Circle One!
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Organics Analysis Data Sheet(Page 2)
Sermv0Jajile CompoundsConcentration:/ Low/ Medium (Circle One)^ --- . - / . i ~ r
Sample Number
Date ExtraDate AnalvCone/Oil F
CAS (Number62-75-9108-95-262-53-31 1 1 .44-4
95-57-8541.73-1106-46-7100-51-693-50-19S-4S-73963S-32-9106-44-5621-64-767-72-198-95-378-59-183-75-5105-67-965-85-0m-91-i120-83-2120-82-191-20-3106-4,7-307-68-359-50-791-57-677-47-488-05-295-95-491-53-788-74.4131.11-3203-96-899-09-2
N-NurosodtmetnvfaminePhenolAnilinebis<-2-ChIoroemvnEmer2 -Chloroonenoi1 3-Dicfilorooenzene1 '4-DicnioroDenzeneBenjvl Alcohol1 2-Dicnlorobenzene2-Merhvtohenolb(s[2-chloroisooroDvii£theri-MerhyfonenorN-Nitroso-Di-n-ProfJviammeHexachioroetnaneNitrobenzeneIsoonorone2-Nirrobnenol2. 4-DimetnvlDnenolBenzoic Acidbisi-2-ChtoroernoxviMethane2. 4-DiChloroonenol1 2. 4-TncriforobenzeneNaonmaiene4-QiioroanmneHcxacn lorobutao iene4-Chloro-3-MetnylDnenol2 -MethvinaontnaieneHexacniorocvciooentaaiene2. 4 6-Tncnioroonenol2, 4. 5-Tricnioroonenoi2 .Chloronsontnaiene2-Nitroaniun*Dimethyl PhtngiateAcenaonmviene3-Nitroaniime
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fo i*~/O (in L<~/n Ltc i>~1C M_/c i*~;p tu.in ti-tc t-c10 U-in j ./O W_/O tu/n fw/O M.f n t^/O (Lro w-io L -IO t>-/o u/O |A_
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Acenaonthene2. 4-Dimtroohenoi4-NitroonenoiDibcnzofuran2. 4-Oinr:rotoluene2. 6-OmitrotOlueneDietnylDhthalate4-ChtorODnenvi-onenvietnerFluorene4-Nirroanrlme4. 6-Omrtro-2-Metnyloheno(N-NiirosooionenvJamine ( 1 J4-BromoDhenyf-ohenvietnerHexacntorobenzenePentachioroonenoi *3£)3~PhenanthreneAnthraceneDi-n-8uryiphinai3tePluorantnene /C3~BenzidmePyrene /Q "JButvibenzyiDhtnaiate3. 3'-DicniorooenzidtneBenzaaiAnrnracenebis(2-EthvthexvilPhrnaiateChrvseneDi-n-Octyl PhtnatateBenzcxQjFluoranmerieSenzwtclFluoranfneneBenzo<a)PvreneIndenoil, 2. 3-cdiPvreneDibenzra. niAnthraceneBenzwg, h iiPerviene
/O **-..5*O.S"o*iL/O Lto t/Q i^ M1C V*-J/C (.*-/e uuCD *-.'O t-A-/n &~IQ /*-/C f.<-• G — * -/C <X_/O 6U/C CL-f? — few-er n-_ ,( * —/C 6Co C *,/c
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Environmental Protection Agencv. CLPSamo'e Management O 'CB.P. O. Box 8ia. Alexandria, Virgmta 22313 703/557-2490
Organics Analysis Data Sheet(Page 3)
Pesticide/PCBs 'Concentration: ( Low /Mediurn (Circle One)
' / -^ /. / p'//Date Extracted/Prepared: —/ ^ / u f AT"'____
Date Analyzed: / . i -.Conc/Dil Factor: ___
Sample Number
CAS j^ ug/Mpf ug / KgNumber TETircle One)319-84-6319-85-7319-86-858-89-9 =- =76-4A-8309-00-2 -1024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-8 .7421-93-41031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-32-5
Aiona-BHC8eta-8HCDeita-BHC.Gamma-BHC (lincaneiHeotacniorAldrmHeatacnior EooxtaeEndosuifan 1Dieidrtn4. 4--DDEEndnnEndosuifan ll4. 4--ODDEndnn AldehydeEndosuffan Sulfate" "4. 4'-DDTMethoxvchlorEndnn KetoneChiordaneToxaoneneAroclor'1016Aroclor-1221Aroctor-1232Aroclor-1242Aroclor-1248Arocior-1254Aroclor-1250 -
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Ve ... iw w —_____ orW /W / \______ V / U , U ^ .,S ———————— w s t f—————————.^——— V(
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Environment*! PP.O. Box SI I.
Laboratory NLab Sample iSample Ma irData Release
CASNumber74-87-374-83-97S-O1-475-00-375-O9-267-64-175-15-075-35-475-34-315S-60-567*66-3T 07-06-27S-S3-371-S5-656-23-5103-05-475-27-4
_=——— — — — ^
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Organics Analysis Data She(Paget)
2im«- £ulf South Research Institute Cas No- CON*- H CH D
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ConcentrDate ExtDate An;Conc/DiPsrcent fPercent F
<CTtloromerriancBromomerhaneVinyl ChlorideChloroetnaneM*Thyf«ne Chlonae /AceroneCarbon Oisuifide7, 1 -Dichloroerhene1. 1-DichloroetnaneTran*-l, 2-DichloroerheneChloroform1. 2-Dichloroeihane2-But»none o?6J. 1, 1-7ncnloro«trTineCaroon Terracnionfi*Vinyl AcetateBromoCich/orometnane
VolatjlflJation: (LowV— -acted/Prepare
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pound*rdium (Cir
(i F '.f/!--.--l1. '
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603f f t
68-01- (jflS ilR. iu . /t /«//§'/ '
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pjsture (Decanted)ug/£pT tig/Kg
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A/ ACAS (Numbwr Vi79-34-S78-87-510061-02-679-01-6 J1 24-48- 179-00-571-43-210OS1-01-5110-75-875-25-25S1-78-6108-1O-1127-18-4103-88-3108-90-7100-41-4100-42-5
1 T. 2. 2-Tetrachloroethane1. 2'DtchloroorooaneTrans-1. 3-DichioroorooeneTnenioroerheneDibromochforomethane1.1. 2-Trtcnioro«rh»neSenreneCtS-1, 3-DtchforoDroo«ne2-ChforoflthvlvmvtetherBrornoform2-Hexanone4-Metnvl-2-PentanoneTetrachioroetneneToluene S tT "ChlorobenzeneEthvlbenzeneStyreneTotal Xvlenes
11
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Organics Analysis Data Sheet(Page 2}
Semiveia ile CompoundsConcentration: f Low./ Medium (Circle One)x*——** i i _ f
Sample Number
Date Anal>Conc/Dil F
CAS CNumber62-75-9108-95-262-53-31 1 1 .44-4
95-57-8541-73-1106-46-7100-51-695-50-195-48-739638-32-9106-44-5621 -64-767-72-198-95-378-59-188-75-5105-67-965-85-0111-91-1120-83-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47-488-06-2 "95-95-491-58-788-74-4131-11-3208-96-899-09-2
N-Nitroso<JimetnvlarmnePhenolAnihnebisf-2-ChloroetnvnEiher2-CMoronhenoJ.1 . 3-Dichiorobenzene.1, 4-Oichlorobenzene . ,.Benzvl Alcohol1. 2-Dichlorobenzene2-Methvlohenolb«(2 -chloroisopropyl lEther4-MetnyiphenolN-Nitroso-Di-n-ProovlammeHexacnioroetnaneNitrobenzeneIsophorone2-Nitrophenoi2, 4-OimettiylohenolBenzoic Acidbisl-2-Chloroethbxv)Methane2. 4-Dicnloropnenol1 . 2. 4-TrichlQrob.enzeneNaomnaiene4-ChioroaniimeHexacniorobutaOiene4-Chloro-3-Methvtohenot2-MethylnapntnaleneHexacniorocvciopentadiene2. 4, 6-Trichiorophenol2. 4, 5-TnchloroDhenoi2-Chlorbnaonthalene2-NnroanihneDimethyl PhthalateAcenapnthviene3-Nitroaniline
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Acenaonthene2. 4-Oimtrophenot4-NitroohenotDibenzofuran,2. 4-Dinrtrotoiuen«2. 6-DinitrotolueneDiethylphthalate ,4-Ch lorophenvl-phenyietherFluorened-Nitroanitme4. 6-Dinrtro-2-MethylpnenolN-Nitrosodiohenylamme (1 }4-Bromophenyl-phenvletherHexachiorobenzenePentachlorophenol \£QPhenanthreneAnthraceneDt-n-SurylphthalateFluorantnene /O 3"SenzidmePyrene f T"Butvibenzyiohtnaiate3. 3'-picniorooenz!dtneBenzof a iAnthracenebis<2-EtnvihexvMPhtnaiaieChrvseneOi-n-Octvl PhthalateSenzobtFluoranthene8enzo<k)Fluorantnene8enzo<atPvreneIndeno* 1 . 2, 3-ccJ)PvreneDibenzta. hiAmnraceneBenz«q. n oPerviene
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Ermnmwral Projection Agency. CLP Samole Management OfficeP, O, Sax SIB. Alexandra, v.rgtma 22313 703/557-2490
Organics Analysis Data Sheet(Page 3)
p£Sticid e / P C B sConcentration: (LOW /Medium (Circje One}Date Extracted/Prepared: ; /^ /
Sample Number
P. . , . \ s.i -y*t t \ tf tDate Analyzed:Conc/Dil Factor: /OQ
58-89-976-44.-S
959-98-8
72-55-972-20-833213-65-972-54-87421-93-41031-07-850-29-372- 3-553494-70-557-74-98001-35-212674-11-21 H04-28-21M41-16-S53469-21-912672-29-611097-69-111096-82-5
Aiona-BHCSeta-BHC
Gamma-BHC tLinaanetHeotacnior
Heotacnior EsoxioeEnaosuifan lDieiorm4. 4--QDE.SndrmEnaosuifan n
rndosulfan Sulfate4. 4--DDT^ethoxvchfor:ndnn Ketone.hlordaneoxapheneAroclor-1016Aroctor-1221ArecJor- 1 232Aroclor-1242Aroctor-1248Arocior-1254Aroclor-1260
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s = Wetght of sample extracted (g)
t = Volume of total extract (ul)
vs ——^,\r _____ Orws
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Laboratory NLab Sample 1Sample MatrData Release
CASNumb*r74-87-374-83-975-01-475-OO-375-09-267-64-175-15-075-35-475-34-31 56-60-567-66-3107-O6-278-93-371-55-656-23-5108-05-475-27-4
roteciwn Ao«nev. CLPSample Management Office,Alexandra. Viroimt 22313 703 /S 57 -2490
Organics Analysis Data She(Page!)
Ftm.fr Gulf South Research Institute Case NO- „
nun- H '3». f \Arcf~Atithor'?f»fl By" £fc£ &?,., / "- •
ConcentrDate ExtDate An*Conc/DiPercent fPercent f
ChloromeinaneBromomethaneVinvl ChlorideChtoroetnaneMethyiflne Chloride c ft,AcetoneCarbon Oisulfide1, 1-Dichloroetnene1, 1-DichloroethanflTrans-1, 2-DichloroetheneChloroform1, 2-Dichforoethane2-Butanone1.1, 1-TrichtoroethaneCaitx>n TetrachlondeVtnvt AcetateBromodichforom etnane
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undsum fCirc
Sample Number
8t
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68-01- (jflSR*r*iw*H- / '/'/j/Sr,
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CAS ^Wumfcwr ^79-34-578-87-510061-02-679-01-6124-48-179-00-571-43-21 006 T -01 -5110-75-875-25-2591-78-6108-10-1127-18-4108-88-3108-9O-7100-41-4100-42-5
1, 1.2. 2-Tetracntoroetnane1, 2-OichforooroDaneTrans-1. 3-OiChioroorooeneTnchloroeiheneOibromochforomethgne1.1. 2-TnchloroernaneBenzenects-1. 3-Oichloroorooene2-ChloroethylvmyietnerBromoform2-Henanone4-M(smvl-2.PentanoneTetrachloroetheneTolueneChlorobenzeneEthylbenreneStvreneTotal Xvienes
ugjOjOr ug/Kg• Icireta Onel
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Environmental Protection Agency. CLP Sample Management Office.P. 0 8os SIS. Alexandria. Virgin* 22313 703/557-2490
Organics Analysis Data Sheet(Page 2)
Sermve4o,tj)0 CompoundsConcentration: [ low./ Medium (Circle One)—- / j .. r
Sample Number
Date Anal1,Conc/Dil F
CAS (Number62-75-9103-95-262-S3-31 1 1 .44-495-57-8541-73-1106-46-7100-51-©95-50-195-48-739638-32-9106-44-5€21-64-767-72-19S-95-378-59-188- 75 -5105-67-965- 85-0111.91-1120-83-2120-32-191-20-3106-47-887-68-359-50-791-S7-677-47-488-O6-295-95-4S1-S3-788-74.4131-11-3208-96-899-09-2
N-NitrosodimeinvlammePhenolAnilinebtsf-2-ChloroethvnEther2-ChioroDhenot1 . 3-Otch!orooenz8ne1 4-Dictiforooenzene9*nn Alcohol1 , 2-Dichlorofaenzene2-Methvlphenolbtj£(2 -chloroisopropvUEiher4-MamvlDhenolN-Nitroso-Di-n-ProoviammeHexachioroetnaneNitrobenzeneJsQohorone2-Niiroonenol2. 4-DimethyionenolSenzoic Acidbisl- 2 -ChloroethoxvlM ethane2. 4-Oicn!orooheno(1, 2. 4-TnchlorobenreneNapninalene4-ChloroanilrneHexacniorobutadiene4-Ch!oro-3-Metnytphenol2 -MethytnaDhtna leneHexacniorocycfopentadtene2. 4. 6-TnchiOf oohenoi2, 4. 5-TnchioroDhenot2 -Chloronapmhaiene
Acenapnthvfene3-Nttroanitine
«H- 12/ISr/Sf'artnrr ^ O C)
"""ug/I^Tug/Kg CAS ("" Circle On») Number
/"o t*—tO re/O l<-iO 60/C i(C M—/C i^_/r> LWin to-fC M-/O U-;o i •_;0 W_/O W-fO l^/O «_(0 M> 0 (.LfrO t-t-)O IA_
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83-32-951-28-5100-02-7132-64-9121-14-2606-20-284-66-27005-72-386-73-7100-01-6534-52 -186-30-6101-55-3118-74-187-86-585-01 -S120-12-784-74-2206-44.-092-87-5129-00-085-68-791-94-156-55-3117-81-7218-O1-9117-84-0205-99-2207-O8-950-32-8193-39-553-70-3191-24-2
Acenaonthene2, 4-Omitrophenol4-NitroohenolDibenrofuran2. 4-Ointtroioluene2. 6-DinitrotolueneDiethylphthatate4-ChloroDhenyl-ohenviemerFluorene4-Nitroanihne4. 6-Dinitro-2-MethylphenolN-Nitrosodiphenvlamine (1 )4-8romophenyl-ohenyterherHexachlorobenzenePentachlorophenoi t 2CPhenanthreneAnthraceneDi-n-ButylphthalateFluorantheneSenzidtnePyren*Butylbenzylpntnatate3. 3"-DicnlorobenzidincBenzotajAnihracenebis(2-6thvlnexvuPhtnaiateChrvseneDi-n-Octyl PhthalateSenrotbjFluorantneneBenzo<k)FluorantheneBenzoojPyreneInaencn 1 . 2. 3-cd)PyrcneDibenzia, niAnmraceneBenzag. h OPerytene
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Environmental Protection Agency. CLP Sample M» nagemant Office.P. O. Box B1 S. Alexandria. Virginia 22313 703/557-2490
Organics Analysis Data Sheet(Page 3}
Pesiicide/PCBsConcentration: _ (LOW /Mediurrj {Circfe One)Date Extracted/Prepared:Date Analyzed:
Sample Number
../ *r
' /Conc/Dil Factor: ____'„
CAS Lug/lp^ug/KgNumber ("Circle One)319-84-6319-85-7 -319-86-858-89,976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-87421-93-41031-07-850-29-372-43-553494-70-557-74-98001-35-212574-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5
Atpna-BMCBeta-BHCOeita-BHCGamma-BHC (LmdanetHeptacnrorAlarmHeotacnior EpoxrdeEndosuifan 1Oieidrm4. 4--ODEEndnnEndosulfan II4, 4'-ODOEndnn AldehydeEndosuifan Sulfate4. 4'.DDTMethoxychforEndnn KetoneChlordaneToxapheneAroclor-1016Aroclor.1221Aroclor-1232Aroclor-1242Aroclor-1248Arocior-1 254Aroclor-1260
n.cs- ur,r,r ue . L<O.CS" t* _C.cC !A-r .<jfr LIc-os u.r-.G* " L.*~
nit*t ^~K. ,o ioo./e /x.r-ic; u.r.~tv /jun-fu 'v-r <° /AC (O IA.i-.fc- (U.i' '. f C i wC.*ro 6/L O *A-
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Vs = Volume of water extracted (mf)
W£ •= Weight of sample extracted {o)
V. = Volume of total extract tut)
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Environm»ftt4tProt«ciian Agency. fXPS*mple Management Office.P.O.Box 818, Al«xinona. Virgimt 22313 703/557-2490
Organics Analysts Data Sheet(Pagel)
Laboratory Name: Giilf South Research Inscicute Case No: 5Cf 03
Sample Number
Lab Sample ID No; ffj 3.1 t________________ QC Report No:Sample Matrix: J^±kC£l_______________. Contract No: 66-01-—-.Data Release Authorized 3y: <£^g *** / .*&*/&w* Date Sample Received:
CompoundsConcentration: .(Low /Medium (Circle One)
Date AnaConc/DiPercent Percent
CAS (Numb*r ^74-S7-374-83-975-01 -475-00-375-09-267-64-175-15-075*35-475-34-3156-60-567-66-3107-06-278-93-371-55-656-23-5108-05-475-27-4
ChiorometnaneSromomernaneVinyl ChlorideChioroatnaneMemviene Chloride f AcetoneCarbon DisuUide1, 1-DichIoroetnene1. 1 -DichloroetnsneTranj-1. 2-Dichioro«iheneChloroform1, 2-Oichioroethana2-BLrtanone ^ f1,7. 1-TriehioroetnaneCarbon TetracnionotVmvi AcetateBromoaicftioromeTnjn*
ly»d.- /7-/?/$^ lv-- / fS / T Vv
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/uACAS (Numb«r x°l79-34-578-87-510061-02-679-01-6124-48-179-00-571-43-210O6l-Ot-5110-75-875-25-2591-78-6108-10-1127-18-4108-88-3108-90-71 00-41 -4100-42-5
1, 1.2, 2-Tetrachioroemine1 . 2*DichioroprooaneTrans-1. 3-D'ChiorooropeneTncfiioroerheneDibromocftioromethan*1.1, 2-TrichiproethaneBenzenecis-1. 3-OiChforooropene2 -ChioroeihvJvinvietnerSromoform2-Hexanene4-Memvl*2'PentanoneTetrachioroetheneTolueneChloro&enreneEthvibenzeneStyreneTotal Xvienes
ru9/K9"" Circle On«|
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Data Naooning QuihfwtFe* rtsonmg raaulls To EFA tht toiK*nfing ni<utti flualifi«r» ar* u»*dAddnionaJ (lag* or footnotes •xelaimng r*sult« gr» •neouragwc Howwir. tfw•arf incimn of *«cn flag mufi M ««iwicti
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mould M cantirmoa By GC 'MS
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Environmental Protection Agency. CLP Sample Management OHice.P, 0. Box 818, Alexandria. Virginia 22313 703/557-2490
Organics Analysis Data Sheet(Page 2}
Sermve*atile CompoundsConcentration: ( Low/ Medium (Circle One)
Sample Number
CASNumber62-75-9108-95-262-53-31 1 1 .44.4
95-57-8541-73-1106-46-7100-51-695-50-195-48-739638-32-9106-44-5621 -64-767-72-198-95-378-59-188-75-5105-67-965-85-0111-91-1120-83-2120-82-191-20-3106-47-887-68-359-50-791-57-677-4.7-488-06-2 * '95-95-491-58-788-74-4
131-11-3208-96-899-09-2
Date AnalyConc/Dil F
~H- Ml*«nr.- ' '50 aV-.- -- —
- - • - - - - £ - - - - - - -)--V^us^flTug/Kg CAS (
TCircle One) NumberN-NitrosodimetnylaminePhenolAnrlmeb!S(-2-Chloroethvl)Ether2-Chlorooheriol1 , 3-Dichlorobenzene1 , 4-DichlorobenzeneBenzvt Atcohol1 . 2-Drchiorobenzene2-Methvlphenoibis(2 -chloroisopropvt (Ether4-MethviohenolN-Nitroso-Di-n-ProDvlammeHexacnioroetnaneNitrobenzeneIsoohorone2-Nitroorienoi2. 4-DimethviohenotBenzoic Acidbis(-2-ChloroethOKv»Mcthane2. 4-Dichloropnenoi1. 2. 4-TnchlorobenzeneNapntnaiene4-ChtoroanilineHexacniorobutaoiene4-Chloro-3-Metnvtphenof2-MethvtnaphtnaleneHexacnlorocvciooentadiene2. 4. 6-Tnchloroonenol2. 4. 5-Tnchloroonenol2 -Chloronapnthaiene2-NitroanilmeOtmethvl PhthatateAcenaphthvtene3-Nitroaniime
to £<~/O re./n LC./n to/D i1C M_/C U.in u^>r> u_/O u.>QLu/n f_fO W_/n t^-FO Ux/O in t<./ 0 (LTO w-JO iA./O y-iu u/O t^'( ; ;<./c,.<tOL-/o i*~fO_/.LOil.
TG ?.LIO Mo ;.L10 L^o u.SO ;--
83-32-951-28-5100-02-7132-64-9121-14-2606-20-284-66-27005-72-386-73-7100-O1 -6534-52-136-30-6101-55-3118-74-187-86-585-01 -8120-12-784-74-2206-44-092-87-5129-00-085-68-791-94-156-55-3 "117-81-7218-01-91 1 7-84-0205-99-2207 -OS -950-32-8193-39-553-70-3191-24-2
Acenaomnene2. 4-Dmitrophenot4-NttrophenofDibeniofuran2. 4-Ointtroroluene2. 6-DinttrotolueneDiethvtphthaiate4.Chioropnenv(-phenvfetherFluprene4-Nitroamhne4. 6-Dinnro-2-MethvlphenolN-NitrosodiPhenvtaminedl4-Brpmophenvt-phenvletherHexachtoroPenzenePentachloropheno! £ Q 3"PhenanthreneAnthraceneOi-n-ButvlohthatateFluorantnene fO 3BenzidmePvrene fc TButvibenrvipmnaiate3. 3'-Oicnlorooenzioine8enzota)Anthraceneois<2 -Einvthexyi iPhtnaiateChrvseneDi-n-Octvi PhthalateBenzcxoiFluorantneneBenzoiktFluorantneneBenzooiPvrenelnaeno<l. 2. 3-cd)PvreneDibenrta. ntAntnraceneBenzoio. h ilPcrvlene
s* —— ^, ug/lorug/Kg** TCircte One
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Environment*! Protection Agency. CLPSamoi* Management Office.P, 0. So* SIS, Alexandria. Virginia 22313 703/S57-2490
Organics Analysis Data Sheet(Page 3)
Sample Number
Concentration: (Low /Medium, (Circle One)i: ( Low /- .—*Date Extracted/Prepared:Date Analyzed: ——! "J'Zi. I oConc/Dil Factor:CAS , ^_Numbvr x , " "TCirctB One)319-84-6319-85-7319-86-858-89-976-44-8309-00-21024-57-3959-98-8SO-57-172-55-972-20-833213-65-972-54-87421-33-41031-07-850-29-372-43-553494-70-557- 74-98O01-35-212674-11-211104-28-211141-16-553469-21-912672-29-611 097-69- 111096-82-5
Alona-BHCBeta-BHCDetta-BHCGamma-BHC (Lindane)HeotacniorAlarmHeotacntor EpoxiaeEnaosuitan I.Dieldrin4. 4--DDEEndnnEndosutfan il4. 4 '-ODDEndnn AldenvdeEndosuifan Sutfate4, 4-.DDTMerhoxvchlorEnarin KetoneChlordaneToxaoheneAroclpr-1016ArocJor-1221Aroclpr-1232Aroctor-1242Aroclpr-1248Aroctor-1 254Aroclor-1260
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Vs = Volume of water extracted (ml)
W_ = Weight of sample extracted (g)
V. * Volume o^ total extract (ul)
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Concentration: Low / Madiurn (Circle One)Data Ertractad/PraparwfcData Anatyt»d: ———««1Conc/OH Factor: ———LJ.—————CASNumber (Circle One)319-84-6319-85*7319-86-S5S-8S-974-44-8309-00-21024.57.3W9-M-860-57-172-SS-972-20-933213-65-972-54-87421-93-41031-07-850-29-372*43-553494-70-557*74-98001 -35-212674.11-211104-28-211 141- 16-653489-21 -912672-29-811097-68-111094-82-6
Aiphi-BHCBete-BHCDatU-SHCOammft-SHClUftdm)HtptachlorAUrinHepuchtorCpOMCleEndnuKanlOwkJrm4,4'.OOEEndrinEndosutfan t)4, 4--OOOEndiin AkfehyaeEndo*uH*n *utf»»4. 4--DOTMelhoKvchlorEndrto KetoneChtontorwToxapheneArodor-1016AroclOf-1221Arodor.1232Aroclor.1242A/oclOf-1249Aroctor.1254Aroctor.1280
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gnvironm«msl Protection Agency, CLP Samole Management Office.P, O, BaxSli. Alexandria. Virginia 22313 703/557-249Q
Organics Analysis Data Sheet(Page!)
Laboratory Name: Qu-lf Souch Research Institute Case No:
Sample Number
Ub Sample ID No: - n t>f f_______________ QC Report No:Sample Matrix: lAAlTC1_______________ ~ Contract No; 6B-01-Data Release Authorized By: .£'-£ < "L f t 3i_ <•&*** Date Sample
Volatile-Compound*Concentration: (Low ; Medium (Circle One)-*——-*
Date AmConc/DiPercent FPercent P
CAS £Numb«r ^74-87-374-S3-975-01 -475-00-375-09-267-64-175-1S-O75-35-475-34-3156-60-567-66-3107-O6-27§-93-371-55-656.23-51 03-O5-475-27-4
Cn lor orn etna ne§romometnan«Vinv* ChJonde-ChioroatnaneMetnvJ»n« Chlonae 5-AcetoneCarbon Disulfide1. 1-Oicnioroetrtene1, 1 -DicnioroatPianeTranj-1, 2-DichloroetheneChloroform1. 2-Dichloroethane2-8ut»none1, 1. 1-TrtchJoro«trianeCar&on TatracniondeVmvl AcetateSromoaicniorometnane
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1, 1.2. 2-Teiracnloroetnane1. 2-DichloroprooaneTran*-1, 3-DicPilorooroo«neTncnloroetneneDi&romocrHoromethane1.1. 2-Tnchl0roetn8neBenzenecjs-1. 3-DicnlorooroDene2 -ChloroemvlvinvletherSromoform2-Hexanone4-MerhVl-2-PemanoneTetrachloroeineneTolueneChlorobenzeneEthvlbenreneStvreneTorai Xvienes
— >»ug^orug/Kg" circle Onal
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Environmental Protection Agency. CLP Sample Management OHice.P. 0- Box 818. Alexandria. Virginia 22313 703/557-2490
Organics Analysis Data Sheet(Page 2)
SermvoiAtrle CompoundsConcentration: ( Low./ Medium (Circle One)x —- / . j -. r
Sample Number
Date ExtraDate AnalyConc/Dil F
CAS (]Number62-75-9108-95-262-53-31 1 1 .44-4
95-57-8541-73-1106-46-7100-51-695-50-195-48-739638-32-9106-44-5621-64.767-72-198-95-378-59-188-75-5105-67-965-85-0111-91-1120-83-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47-488-06-2'95-95-491-58-788-74-4131-11-3208-96-899-09-2
N-NitrosoatmetnyiammePhenolAnilineb!S(-2-ChloroetnvilEther2-ChloroDhenol1. 3-Dichlorobenzene1 . 4-DichlorobenzeneBenzvl Alcohol _ . . . _ .1, 2-Dicfilorobenzene .2-MethvlohenoltHSl2-chloroisoproovl)Ether4-MetnvionenblN-Nitroso-Di-n-ProDvlammeHexachloroetnaneNitrobenzeneIsoohorone2-Nitroonenoi2. 4-OimethvlonenolBenzoic Acidbis(-2-Chloroethoxv)Methane2. 4-Oichtoropnenol1. 2. 4.-TrtchlorobenzeneNapnthalene4-ChtoroanilmeHexacntorabutadiene4-Chtoro-3-Methv(phenoi2-MethvmaphthaieneHexacniorocvciODentadiene2. 4. 6-TnchloroDnenol2. 4 5-Tnchloropfienbi2-Chlorona0hthalene2-NitroantlmeDimethyl PhthatateAcenaonthvlene3-Nitroantltne
:ted/ Prepares«*«•• /£/
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83-32-951-28-5100-02-7132-64-9121-14-2606-20-284-66-27005-72-386-73-7100-01-6534-52-186-30-6101-55-3118-74-187-86-585-01 -8120-12-784-74-2206-44-092-87-5129-00-085-68-791-94-156-55-3117-81-7218-01-9117-84-0205-99-2207-08-950-32-8193-39-553-70-3191-24-2
Acenaomhene2. 4-Dinitroohenol4-Nnrooh«nolDibenzofuran2.4-Dimtrptoluene2. 6-DinitrotoiueneDiethvlpntnalate4-Chloroonenvl-ohenvietnerFluorene4-Nitroanilme4. 6-Oinitro-2-MethvlpnenolN-Nitrosodtohenvlamme (1)4-BromoDhenvl-DhenvietherHexacntorobenzenePentachiorooheno)PhenanthreneAnthraceneDi-n-ButytphinatateRuoramneneBenzidmePyreneSutvibenzvipntnalate3. 3'-Dicr>iprooenzidmeBenzotajAntnracenebis<2-E:nvinexvitPtimaiateChrvseneDi-n-Octvi PhthalateSenzcxblFluorantheneBenzoiniFluorantheneBenzotajPvreneindencxl. 2. 3-ca)PvreneDibenna, njAntnraceneSenzaq. h nPervlene
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Organics Analysis Data Sheet{Page 3)
icide/PCBs
Sample Number
Concentration: ( Low /Medium, (Circle One)— }-? /i IDare Extracted/Prepared: —/ z / & /
Date Analyzed; J.Conc/Dil Factor;CAS *•••" Lug/lpfug/KgNumber x . {Circle One)319-84-6319-85-7319-85-858-89-976-44.-S309-00-21024-57-3959-98-S60-57-172-55-972-20-833213-65-972-54-87421-93-41031-07-S50-29-372-43-553494-70-557-74-98001-35-212674.11-211104-28-211141-16-553469-21-912672-29-611097-69^111 095-82 -5
Alpna-SHCBeta-BHCDelta -BHCGamma-BHC (LmdanefHeotacniorAldrinHeotacnior EooxideEndosuifan IDieldrm4.4--OOESndrinEndosuJfan ll4. 4'-DDDEndnn AldehvdeEndosuifan Sulfate4. 4--DDTMethoxvchforEndnn KetoneChlordaneToxaorteneAroclor-1016Aroclor-1221Aroclor-1232Aroctor-1242Aroclor-1248Arocior-1254Arocior-1260
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Vj = Volume of extract injected (ul)
V = Volume of water extracted (ml)
W 3 Weight of sample extracted (g)
V. = Volume o' total extract (ul)
Environmental Protection Agencv. CLP Sample Management Office,P. O. BoxSIS, Alexandria. Virginia 22313 703/557-2490
Organics Analysis Data Sheet(Page!)
Laboratory Name: Gulf South Research Institute Case No:
Sample Number
Lab Sample ID No: J^H£______________ OC Report No: (Sample Matrix: t=l________i______^ Contract No: 68-01-Data Release Authorized By: vg r s< •**•" *-t*s**{ Qate Sample Received:
Vo latile-CompoundsConcentration: (Low / Medium . (Circle One}
-"'Date AnaConc/DiPercent fPercent P
CAS CNumber ^74-87-374-83-975-O1 -*75-00-375-09-267-64-175-15-075-35-475-34-3156-60-567-66-3107-O6-278-93-371-55-656-23-5108-05-475-27-4
ChlorometnancBromomethaneVinvl ChlorideChioroethane•Methylene Chloride S"AcetoneCarbon Oisulfide1. 1 -Oichloroflthene1; l-DtchloroernansTrans-1. 2-DtchloroetheneChloroform1. 2-Dichloroetfian*2-8uianone1,1. 1-Trichloro«th8neCarbon TetrachiondeVinvl AcetateBromoflicnioromethan*
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/uA /- CAS {ug/Lt>r ug/KgNumber ^ fCircle One!79-34-578-87-510061-02-679-01-6124-48-179-00-571-43-210061-01-5110-75-875-25-2591-78-6108-10-1127-18-4108-88-3108-90-7100-41-4100-42-5
1.1.2. 2-T«tracnioroethane1 . 2-DichloroorooaneTrans-1. 3-E>ichloroorooeneTnchloro«then* .Dibromochioromethane1.1, 2-TrtchloroetnaneBenzenecis-1. 3-Oichloroorof>ene .2 -ChloroflthvlvmvietherBromoform2-Hexanone4.Methvl-2.PemanoneTetrachioroetheneTolueneChlorobenzeneEthylbenreneStveneTotal Xvlenes
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_ final tnnctinouW b* conlinncd by GC 'MS
U Inacatn compound *«t anaiynd for out nor o»i«ei«Raoort tn* minimum MIMCIKXI umii for ma iamoia ••""m» u (• a 1 OUt 0*aao on rwcauarv eenc»ntr*iifln ' • Tn'« fl*fl •» "«*0 <*«*" "*• »*wMt if totmo m in# oiank
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Environmonta' Protoction Agencv. CLPSamole Management Office.P. O 8ox818. Alexandra. Virginia 22313 703/557-2490
Organics Analysis Data Sheet(Page 2)
Sample Number
¥
ermve4*vtHe CompoundsConcentration; ( Low/ Medium (Circ)e One)
"Date AnalyConc/Dil F
CAS (Number62-75-9108-S5-262-S3-3111-44.4
05-57-8541-73-11O6-46-7100-51-695-SO-195-48-739638-32-9106-44-5621*64-767-72-198-95-378-59-188-75-5105-67-965-85-0111-91-1120-S3-2120-82-191-20-3105-47-887-63-3S9-5Q.791-57-677-A7-488-06-295-95-491-53-788-74-4131-1 1-3208-96-899-09-2
N-NitrosodimetnyiammePhenolAnilinebis^-2-ChloroethvilEther2-Chlorooh.enol1. 3-Dicniorobenzene1 4-DichtorobenzeneBenrvl Alcohol1 2-Dichlorobenzene2-Methviohenoibts(2-chiorotsooroovl l£ther4-Metrivlofieno!N-fJitroso-Di-n-ProDviammeHexacnioroeinaneNitrooenzeneIsoohorone2-NitroonenoJ2. 4-OimetnvlonenolBenzoic Acidbia-2-Chloroethoxv)Methane2. 4-OichIoroDnenoi1 , 2. 4-TncnlorobenzeneNaontnalene4-ChioroanilmeHexaeniorooutaoiene4-Chloro-3-Metnviphenoi2-MeinvinaDhtrtaleneHexachlorocvciooentadiene2. 4 6-Tnchforoonenol2. 4. 5-Tncnloroonenoi2-Chloronaontnaiene2-NitroaniimeDtmethvi PhthalateAcenaontnviene3-NrtroanrJme
«.. (z-y/r/s-/-' 'ar,nr-. ^TO Q
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83-32-951-28-5100-02-7132-64-9121-14-2606-20-284-66-27005-72-386-73-7100-O1 -6534-52-186-30-61O1-55-3118-74-187-86-585-01-8120-12-784-74-2206-44-092-87-S129-00-085-68-791-94-156-55-3117-81-7218-01-9117-84-0205-99-2207-08-950-32-8193-39-553-70-3191-24-2
Acenaomnene2. 4-DmrtroDhenoi4-NitroohenolDibenzofuran2. 4-Dinitrotoluene2. 6-DmitrotOlueneDiethvlohthalate4-Chloroohenvi-DhenvietherPluorene4-Nitroanilme4. 6-Dmitro-2-Methv'DnenoiN-NitrosodtDhenvlamine ( 1 }4-BromoDhenvl-DhenvletnerHexacrtiorobenrenePentacniorophenolPhenanthreneAnthraceneDi-n-Buiv'ohthalateFfuorantneneBenzidinePyreneSutvibenzvlontnaiate3, 3"-DicnlorooenzidineSenzotaiAntnracenebis(2-£thvlhexvi)PhmaiateChrvseneDi-n-Octvl PhthalateBenzcXDiFiuorantneneBenzotkiFluorantheneSanzcKalPvreneindenal. 2. 3-cd)PvreneOibenzia. htAntnraceneBenzwg. h iiPervlene
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Environmental Protection Agency. CLP Same's Management 0#iP. 0. SDK 818. Alexandra. Virginia 22313 703/557-2490
Organics Analysis Data Sheet(Page 3}
Pgsticid e / P C B sConcentration: (Low /'Medium (Circle One)
Date Extracted/Prepared: f"2- f *-t I iv~Date Analyzed: W^ b "_______________
Sample Number
CAS Cug/ip* ug / KgNumber TUircle One)319-84-6319-85-7 .319-86-858-89-976-44-8309-00,2 ...1024-57-3959-98-860-57-172-S5-.972-20-8 .33213-65-972-54-874 21 -93-d1031-07-850-29-3 ,.72-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5
Aiona-BHC8eta-8HCDeita-BHCGamma-8HC ILmaane)HeotacniorAlarmHeotacntor EooxiaeEnoosuifan 1Dieidrin4, A'-DDEEndrrnEndosuifan II4. 4'- ODDEndrrn AldenvdeEndosuifan Sulfate4. 4'-DOTMemoxvchlorEndnn KetoneChlordaneToxaoheneAroclor-1016Aroclor-1221Aroclor-1232Aroclor-1242ArocJor-1248Arocior-1254Aroclor-I2SO
n.cs- &~r,nr o-C.' LLo.r,s" <>\C.r-C /x_r .L*T LIC-O5 U.fn /?~ L>-
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W = Weight of sample extracted (g)
V. = Volume of total extract (ul)
vs
Oryantes Analysis Oats Shaat
Number
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CwNo:QCteportNo:Contract No:
VoMla Compoundf .Conotntration: < £pr Medium (Circte On*}Date Extract*d/Fr«pvKt:
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CAS
79-34-578-87-5tooei-02-479-01*6124-48-179-00-571.43-210061 -O1-51 10-75-875-25-2691-78-6106-10-1127-18-4106-88-3106-90-7100-41-410CM2-5
1, 1, 2. 2-T«trachlofO«han*1.2'DfChloroprooane
Trichteroetheoe .nil >• t - lho tu* wrviCJ i uw oma inanv1.1. 2-TrtchloroethaneBcnnneCtt-1. 3-Oichloroprop9n«2-ChIoro*thyMnylaihtffBromoform2-Heianont
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Ssmlvotsttta CompoundsConc*mrstion: low cJflfijijji? .(CirctoOna)
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Concentration: Low adium? (Circle Onaj)DMData AnatywtCone/Oil Fsoor: ——/..,/CASftfumaa*319*84319-85-731&-M-8SS-89-976-44-8309-00-21024-57-3Hl-96-860-57-172-55-972-20-833213-65-972-64-87421-93-41031-O7-850-29-372-43-553494.70-5S7-74.S8001 -35-212674-11-21 1 104.28-2ni4i-ie-653469-21-912672.29-611097-69-11 1096-62-5
AJph»-BHCBata*BHCDatta-SHCGamrnj-BHC (Lindana)
AJdrtnHaptaeMor Epoudaindoauifan 1DiaUrin4, 4'-DO€EndrinCndoauHan H4, 4--OODEndrin AMahytaEndoautfan SuNata4. 4--DOTMatnoBychtorEno in KatonaChtordanaToxaphanaArocter-1016Aroclor-1221Arador-1232Arador-1242Aroc(or-124SArodor-1254Arador-1260
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(CtrdaOoa) Mumbat____________________<CWeW79-34-576-87-510061-02-679-01-6124-48-179-00-571-43-210061-01-6110-75-875-25-2691-78-6108-10-1127-18-4106-88-3106-90-7100-41*4100-42-5
1,1,2. 2-Tatraehloroathana1,2-DtehloropropanaTrana*1, 3-DtchloroprapanaTriehloroathafta .
1. 1* 2-TrtehtofootbanaSantanact»-1. 3-0*ehlorapropafia2-ChtofoaihyMrtylathafBranoform2-Haxanona4-Mamyt.2*PantanohaT a t r ac nioroafnvnaTotuanaChlorobanianaEthylbanMnaStyranaTotal Xytartat
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Ssmtvolsttts Compound*Coocamntion Loi/ tUadiucn .(CirctaOna.
Numbar {CbeteCAS o9/l«»«gS CAS ' ug/lo<SJ7l?-- - >JK* l" t™ ... ._. ^»» •-
106-95-262-53-3111-44-495 -57-8541-73-1106-49. 7100-51-696-50-195-4S-?39638-32-f106-44.5C2 1-64-767-72-1M-95-378-59-18875-5105-67-9e5-es-o
120-83-2120-82-191-203106-47-6I7-M-359-50-791-i7-677-47-488-06-295-95-491-58-7
131*11-32OS-96-8
H- Nitroaoo>m«thyta minaPhanoiAniima
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H-Nitroao-O* -n-PropytaminaHauchloroathanaNitrobanxan*
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2. 4. S-Tr«hlofoph»not2. 4, 5-TrKhtoroptwnol2 -Chloronaphthalana2-Nitroanilin*Dimethyl Pnthalaia
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Organics Analysis Data Sheat(Page 3)
Patticido/PCBiConcentration: CVl»ow ' Medium (Circle One)Data Enractad/Prapara :Date Analyzed: ——Cone/Oil Factor:CASNumtar CCircta On*)319-84-6319-85-7319-88-8S8-B9-976-44*6309-00-21024-S7-3W9-98-B80-57-172-55-972-20-833213-65-972-54-8 -7421-93-41031 )7-850-29-372-43-553494-7O-557-74-98001 -35-212674-11-211104-28-211141-16-553469*21-912572-29-611097-69-111096-62 -5
Aipha-BHCBata-BHCDotta-BHCGamma-BHC (Undarw)
AkJrmHaptactUor EpoxioaEndoautfan 1Diatdrin4.4'-DD£EndrinEnooauttan H4, 4--DDDEndrin AldahyoaEndoauttan Sutfata4, 4'-OOTMathoxychtorEndrin KatonaDiloroaneToxaphanaAroclor-1016Arochx-1221Aroctor-1232Aroctor-t242Aroclor-1248Aroclor-1254Arocior-1260
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CASNumber74-87-374.83-075-O1 -475-OO-375-O9-267-64-17S-1S-O7S-35-475-34-3156-60-567-66-3107-06-278-93-371-55-6§6-23-5108-05-475-27-4
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(ChlorometMsneBfomomsmaneVinv* Chiof ideCtiloroetnane.Metnvfane Chtorifle *T" ,Ac«ion«Carbon Oisuifide7. 1-Dichforoatnene1. 1-Dtch!oro0ihaneTr»nj-l. 2-Dtehloroeth6neChloroform1.2-Oicntoroethane2-Suianone1.1. 1 -TrieritoroetrianeCaroon TatracniondeVinvf AcetateBromocJiCfilorometnane1
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Sample Number j
1 <~C7
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1. 1.2. 2-Tetracnloroetnane1, 2-DicnJoroorooaneTrans-1, 3-Dicntorooroo«ne"TneMloroetrieneOi bromocn f oromema ne1,1. 2-TncfitoroemaneBenzeneCis-l, 3-DiCrHorooroD«ne2-Chforo«thv(vfnvieiherSromoform2-He*anone4-Metnvl-2-PemanoneTetra en loroetn s n eTolueneChlorobenzeneEthvlbenzeneStvreneTotal Xv'enes
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Organics Analysis Data Sheet(Page 2)
Sernive4ajile CompoundsConcentration: LLow/ Medium (Circle One)
Sample Number
/-\£&&
Date Ana!>Conc/Dit F
CAS (Number62-75-9108-95-2G2-53-31 1 1 .44.4
95-57-8541-73-1106-46-7100-51-695-50-195-48-739638-32-9106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-965-85-0111-91-1120-83-2120-82-191-20-3106-47-887-58-359-50-791-57-677-47-488-06-295-95-491-53-788-74-4131-11-3208-96-899-09-2
N-NiirosodimetnylammePheno*AmJinebisf-2-Chloroetnvi)Ether2-Chlorophenol1. 3-Oictilorobenzene1, 4-DichforobenzeneBenzvl Alcohol1. 2-Oichlorpbenzene2-Methvlphenoibrs(2-chIoroisopropvoEther4-MetrwlpnenolN-Nitroso-Oi-n-ProovlamineMexacnloroemaneNttrooenzeneIsoohorone2-NitroDhenoJ2, 4-DimethvlohenolBenzotc Acidbisf-2-ChloroethoxvtMethane2. 4-Dich(oropnenof1, 2. 4-TnchlorobenzeneNaontnatene4-ChioroanifmeHexacniorobutaaiene4-Chloro-3-Mernviprtenoi2-MethyinapnthaieneHexacnlorocvcfooentaaiene2. 4. 6-Tncnioropnenol2, 4. 5-Tncriloropnenoi2-Chforonaonthalene2-NitroantimeDimethvi PnthaiateAcenapnthytene3-Nitroanilme
. 12-1 IV A 4ypd- 1* MY Jl *T
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/o ioto f^/r> t<-/O to/o*^-;c w/C 4 .»n tu-/O tc/O tcJO (;o i -;0 w./O £A_/n tw/O vU
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83-32-951-28-5100-02-7132-64-9121-14-2606-20-284-66-27005-72-386-73-710O-01 -6534-52-186-30-6101-55-3118-74-187-86-585-01 -8120-12-784-74-2206-44-092-87-5129-00-085-68-791-94-156-55-3117-81-7218-01-9117-84-0205-99-2207-08-950-32-8193-39-5S3-70-3191-24-2
Acenapmnene2. 4-Oinitropnenot4-NitroonenolDibenzofuran2, 4-Dinitroto'uene2, 6-DinitrotolueneDiet hvJpntfia late4-Chloropnenvl-phenytetnerFluorene4-N»troani|ine4. 6-Oinitro-2-MethylDnenoJN-Nitrosodiohenyfamine (1 }4-Bromophenyt-phenyietherHexachlorobenzenePentachJoroohenolPhenanthreneAnthraceneOi-n-ButyiphthalateFiuoramneneSenzidmePyreneButvlbenzvtpntnaiate3. 3'-DicniorooenridineBenztxajAniriracenet)is(2-EthvihexvnPritrtaiateChryseneDi-n--Octvi PhthalateBenzo<D)f:(uoraninene8enzo<K)Pluorantnene .BenzotaiPvreneIndeno* 1 . 2. 3-cd»PvreneDibenzia. njAntnraceneSenrtxg. h, rtPerviene
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Organics Analysis Data Sheet(Page3)
Sample Number
Concentration: ( Low/Mediurrj {Circje One)Date Extracted/Prepared:Date Analyzed: _L.Conc/DH Factor:CAS Lug/Ipf ug/KgNumber """TCireie Onej319-34-6319-85-7319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-87421-93-41031-07-850-29-372-43-S53494-70-557-74-9SCO! -35-212674.- 11-211104-28-211141.16-553469-21 -91 2572 -29-611097-69-111O9S-82-5
Alpna-SHCBeta-BHCDefta-BHCGamma-BMC (LmdaneiHeotacntorAidrtnHeotacntor EpoxrdeEndosuifan 1Dietdrmd. 4--DDEEndnnEndosuifan II4. 4'-DDOEndnn AldehvdeEndosuifan Suffate4. 4--DDTMethoxvcnlorEndrin KetoneChlordaneToxaofteneAroctor-lO16Aroclor-1221Aroctor.1232Aroclor-1242Aroctor-1248Arocior-1254Aroclor-1260
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Vs s Volume of water extracted {mlj
W? = Weight of sample extracted (g)
V s Volume of tptal extract (ul)
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Povtfeida/PCBsConcentration: Low ( ModiumJ {Circle One)DateDaw Anttyatf: -Conc/OU FactorCASNumbof
ftwfipl* Number(T7JO/
319-85-7
S8-S9-976 4-S
1024-57-3
5O-57-172-W-iZ2-20433213-65:972-W-*7*21-93-41031-07-850-29-372-43-5
57.74-98001*35-212674.11-211104.28-211141.16-553469-21-912672-29-611097.69-111096-82-5
Ben-BHCDelu-&HCOammt
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Vj « Volume ol water extracted (ml)
W§ * Weight of tampfe exacted (g)
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CASNumber
1,1,2, 2*Terrachloroetrtan*1. 2-Dtthtorooropane
124 8-179-00-571 3-210061-01-51 10-75*675-25-2591-78-6108-10-1127-18-4108-88-3100-90-7100-41*4100-42-5
Trent-1.3-DtehloropfOpeneTrieMoroetheneDejfomochloromtthene1.1.2-Trichlo»oomaneBecueneCtt.1,3-E>«ch*or ' "
Ofomoteim2-Mexanone*44etn*/f-2-*vmenaneTetrechtoroetheneTolueneChtorobenceneEthyfbemeneStyreneTotal Xytene*
V*v«eaHeei*«>we|f«e<erei«iere«jMelt» * C Thutaf e«**e*iei
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Sample Number
Samlvotettta CompoundsConctntration: Low M J -'. (Drc*a Ona)
ug/lor<ifl7i(Oicte Of
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Organics Analysis Data Shoot(Pago 3)
Ptttfcida/PCBs^^__—--—^< - *Concentration: Low ( Medium } (Circle One)Data Extracted/Prepared:
Sample Number
Cone/W Factor: /..'/CAS
119-84-6319-85-7119-86-858*89-976-444309-00-21024-57-3M9.98-850-57-172-S5-972-20-833213-66-972-54-87421-93-4t 031-07.850-29-372-43-553494-70-557-74-9800t.35-212674- IT -21110* -28 -2M141.1C-553469-21-912672-29-611 097-69- 111096-82-5
Alpne-BHCBeta-SHCDelta -8HC6amma-BMC (Undane) .HeptachlorAtormHeocactitorEonideEndeautfan 1Dioidrm4. 4'-ODEEndrinEndoauHan U4, 4*-DDOEndrin AldehydeEndotulfan Sutfaie4, 4--ODTMethovychtorEndrtnKetoneChlorden*ToxaphenaAroctor-1016Aroclor-1221VocJof-1232Aroclor-1242Aroclor-1248Arockx-1254Anxtor-1260
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V( > Volume of water extracted (ml)
Wft * Weight of Mmpie extracted (0)
V, * Volume of total extract (uO
V. _____________ orW.
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Samp»,M«rte ot ,———.——————— Contact*:DataftolaaaaAuinorindBy: mf f'V rV- Data Sampla ftacafcad:
Votatfta Compounds.Concentration: < \&2 Madiom (Clrda Ona)Data Extracted/Freparad;Data Anaryrad: __
ParcantMoiaturrParcant Moittura (Dacamad):
CAS uo>1o<1g ]Ca c** __Number79-34-578474
79-014
1.1,2. 2>Tetraehlorpethane1 . 2-DfehtofOpf opineTrent-1,3-DieMoropropene
124*48-179-00-57143-210061-01-6110-75476-25-2691*784108-10-1127-18-4108-88-3106-90-7100-41410042-5
TrieMeroetheneDMromochtoroma thane1. 1. 2*TrieMoroaitianeBoftnneen- T. 3-Dichlof oprupene2-CntoroeihvMoyiethefaromotom2-Neunone
TetraenloroatheneTolueneChlorobenienaElhylbanteneStyrenaTotal Xvtenet
tfa
B>«e««*r erfww Vie« even eeewttMM MMC*W« w NW ecu
J\RiOOUI2
r. 0*1*.as»St8. AaMAn.V»fMa 12313 703 674480
Organic* Analysis Data Shoot
ftamfootatila CompoundsConcentration: Low
Data Analynd;Cone/DU Factor
CAS
DibenKa. hVknthraeene
CLP tempi* Me«*f.eflne*«Offie*,ao-tlt, Atoiandna.Vire.Ma 22313 703/567-2490
Organics Analysis Data Shoot(Page 3)
Poatiekto/PCBs/>*?~~~-~~?"SConcentration: Low CMediuniy (Circle One)
Data Extracted/Prepared:Data Anah/zed: ————•
£*mp**
Cone/Oil Factor: —CAS ug/lor/uo/KflNumber319-84431945-731946-858-89-976*444309-00-21024-57.3R59-964BO-57-172-S5-972-20-833213-65472-54-87421-93-41031-07-850-29-372-43-5S3494-70-557-74-98001-35-212674-11-21 1 104-28-211141-16-653469-21-912672-29411097-69-11109642-5
Afehe-BHCSeta-BHCDette-BHCOamma-BHC (Undane)HeptechtorAMrinHeptachler EpcuoOeEndeeuttantOieldrtn4. 4'-OOEEndrinEndoauHan H4, 4--ODOEndrin AldehydeEndosuHan SuHate4, 4--DOTMethevyehferEndrin KetonaChlordaneToxapheneAroclor-1016Arador.1221Ar ockx-1232Arodor.1242Arocfor.1248Aroclor-1254Arodor-1260
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Vft « Volume o* water eitrected (ml.
W$ * Weight of sample ecu-acted (o)
V, « Volume of total astract M)
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gnvironmenwl Protection Apencv, CLPSample Management Office.703/557-2490
COrganics Analysis Data Sheet
(PageT)Laboratory Name: Gulf Souch Research Institute Case No: 36
Sample Number
Lab Sample fD No: ^± _____________ QC Report No:Sampte Matrix: v . T 1 . _____ Contract No: -6 8-0 1-Data Release Authorized By: >VOk-'3£ ' Date Sample Received:
Volatile-CompoundsConcentration: (Low ) Medium (Circle One)
N —- . -. J _ i , /
CASNumber74-17-374-83-97S-01-475-00-375-O9-267-64-175-1 S-07S-35-475-34-3156-60-S67-66-3107-06-278-93-37T-5S45S-23-S1 0S-Q5-475-27-4
Date An;Conc/DiPercentPercent
(CnloromemaneSromomernaneVinv* ChlorideCnianxrtrurneMemyltn* Cnlorta* - *-7AcetoneCaroon DtsuMtdet. 1 -OicfiJoroerrtene1, 1-Dichioro«maneTrans-1, 2-DichioroemeneChloroform1, 2-Oichloroctriane2-SuranoneT. 1, T-TrrcftJoroatnaneCaroon T«rracn(ondffVmvl AcetateSromocficn/oromflrnans
ty9mH. • ,-z,/ /s<y '*J^ /-O pH fo. pWni«f,»«- A/ A
listure f Decanted;og/lpr ug/Kg
te==r.areJ*>On*.|/O Cw
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yyACAS (Number ^79-34-578-87-510061-02-679-01-61 24-48- 179-00-571-43-210061-01-5110-75-875-25-2591-78-6M 08- 10-1127-18-4108-88-3108-90-710O-41-4100-42-5
1 1. 2, 2-TetracrtJoroeinane1, 2-0>ertiorooreoaneTrans-1. 3-DtcnioroorooeneTncrtioroeTheneDibromocnioromerhane1, 1. 2-Tnchloro«trianeBenzenecis-t. S-Dtchforoorooene2 -ChJoro«thv*vf nvJetnerBromoform2-H*xanone4-Metnv(-2-PentanoneTetracnioroetneneTolueneCr)loroO*nzeneEinyJbenreneStyreneTotaf XvJenes
-~>aq/JHpr ug/Kg" circ(*Onal
- tor iwS" Or- it-s' IX-*r EA-C ic.-r **-^c c<-f ^/o <-/c u_?" 6Cr iX.^ A^r* cxS" <u<~ 'A ,
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Sample Number
. COrganics Analysis Data Sheet
(Page 2)
Sermve>4a|iie CompoundsConcentration: ( Low/ Medium (Circle One)s —- i . f _. rDate Extra
Date AnalyCone/Oil F
CAS (Number62-75-9108-95-262-53-31 1 1 .44.495-57-8541-73-1106-46-7100-51-695-50-195-48-739638-32-9106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-965-85-0111-91-1120-83-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47-488-06-295-95-491-58-788-74-4131-11-3208-96-899-09-2
N-NitrosodimetrwlaminePhenolAnilinebisf-2-Chlaroetrwl)Ether2-Chloroohenoi1. 3-Dichlorobenzene1 , 4-DichlorobenzeneBenzyl Alcohol1. 2-Dichtorobenzene2-Methvlohenolbis(2-chlorotsaproDvn£ther4-MethvlohenolN-Nitroso-Oi-n-ProDvlammeHexacnioroe thaneNurooenzeneIsoohorone2-Nitroonenof2, 4.-Dimethyipnen.olBenzotc Acidbis(-2-Chloroethoxv)Methane2, 4-Dichloropnenoi1 , 2. 4-TnchlorooenzeneNapntnaiene4-ChloroanitTneHexacnioroDutaaiene4-Chloro-3-Methvtpnenoi2 -Methyl naphthaleneHexacnlorocvclopentaaiene2. 4. 6-Tnchlor6Dheho(2. 4. 5-Tnchloroonenoi2-Chloronapnthaiene2-NitroanilmeDimethyl PhthaiateAeenaonthytene3-Nitroamhne
ned/ Prepares
zed: |7J ———————————————
- /z-/ S"-6 / IT
artj-v- nO O
X- -
' ——— >ug/ljar ug/Kg CAS (
{Circle One) NumberfO l -to (_ _in i<_ID t\/c t*~)C t,L-tC i^_IP twJO iL.10 t-c'Ou-in t _;0 U-/O (in i\s/D vuin te/ D (LTO M-'0 L.V-/O tw/O Iv/O ix-'(': fv/O,.;1O /:-'O t\-FO /.C!0 i.t.•TO "1 L
' 1C MO ',L(O L1to uSO r-
83-32-951-28-5100-02-7132-64-9121-14-2606-20-284-66-27005-72-386-73-7100-01-6534-52-- 186-30-6101-55-3118-74-1S7-86-585-01 -8120-12-784- 74-2206-44-092-87-5129-00-085-68-791-94-156-55-3117-81-7218-01-91 1 7-84-0205-99-2207-08-950-32-8193-39-553-70-3191-24-2
Acenaohthene2, 4-Dimtrophenol4-NftrotJhenolDibenzofuran2. 4-Dinitrotoluene2. 6-OinitrotolueneDiethylphthalated-ChlorODhenvt-phenvletherFluorene4-Nitroaniline4. 6-Dinitro-2-MethylphenolN-Nitrosodiohenylamine (114-Sromophenvl-DrienvleiherHexachtorobenzenePentachlorophenoi iaOPhenanthreneAnthraceneDi-n-SuivluhthalateFtuoranrhene t OT*BenzidinePyrene IO"Butyibenzylphtnaiate3. 3'-DichloroDenridmeBenzcua (Anthracenebts(2-EthvihexvHPhth3iateChrvseneDi-n-Octvl PhthalateSenzotDiFluoramneneBenzcni()Ffuoran.heneBenzcxafPyreneIndencn 1 . 2. 3-cdlPvreneDibenzta. roAnmraceneBenzotq. h iiPerviene
(1 J-CannoAcpeda.fil.aiJamtdinenytamme
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Environmental Protection Agency. CUPSjmole Management Otfice.P, O. Box SI S. Al.xandria. Virginia 22313 703/557-2 90
Organics Analysts Data Sheet
Sample Number
, .,,(Page 3) 6 . 0
Pesticide/PCBsConcentration: ( Low y'Mediurrj fCircJe One)
^-" — *^ iDate Extracted/Prepared: _L,Date Analyzed: 17. ft
lCone/Oil Factor: ___CASNumber . . ^"" TCircle'One")319-84-6319-85-7319-86-853-39-976-4A-8309OO-21024-57-3959-98-86O-57-172-55-972-20-833213-65-972-54.-S7421-93-4103 1-07 -850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5
Aipna-BHCSeta-BHCDelra-SHCGamma-SHC (LmaanetHeotacniorAidrmHeptacnfor EooxiaeEndosutfan 1Dieidnn4. i'-DDEEndrinEneosuifan tl4. 4'-OODEndrrn AldehvaeEndosuifan Suffate4, 4--DDTMethoxvchiorEndrin KetoneChlordaneToxaoheneAroclor-1016Arocbr-1221Aroclor-1232Aroetor-1242Aroctor-1248Arocior-1254Aroclor-1260
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Vs s Volume of water extracted [ml)
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Laboratory M«na: No:3 o V QCIUporfNo:
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Organic* Analysis Data Shaat
/PCa*Concentration: U>w_ Medium (Circle One)DataEvtractad/Praparad;DataAnalyzad:Conc/Dil Factor:CASlumber (Circlei319-84-6319-85-73 19*Ow*oBB-89-976-444309-00-21024-57.3M9-98-88057-172-55-972-20-833213-65-972-54-87421-93-41031 )7SO-29-372-43-5634W-70-557-74-98001-35-212674-11-211104-28-2tmi-ie-s53489-21-912672-29-611097-69-11 1096-82-5
Alphe-BHCBet*-8HCDetU-ftHCQemme-BHC {Lintfene)HtpteCMOfAtdrinHeetechlor EpondeEndotuHenlOieldrin4. 4'.OOEEndrinEndc*urtanB4. 4'-ODDEndrin AWehydeEndotutfen ftutfate4. 4*-ODTMemoxyeMorEndrin KetoneOOordtntTexapheneAroetor-10164rockx-1221Aroefor-1232Aroclor-1242AroClor-1248Arodor-1254Arocier.t260
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V, « Volume of water exirected (ml)
Wf * Weight of temple attracted (9)
Vt > Volume of tout extrect (u*)
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Laboratory NUP Sample ISample MatrData Release
CASNumber74.07-374-83-97S-01-475-00-375-09-2 _]67-64-175-15-075-35-475-34-3156-60-567.66-3107-06-278 -§3-371-55-656-23-5108 -OS-475-27-4
rotection Agency. CLP Sample Management Otf ice.Alexandria. Virginia 22313 703/S57-249O
Organics Analysis Data She(Pagel)
2emer Gulf. South Research Institute Casp No- —™«- HD3PI*. \Aj4.i&~Authnrfysd By ^ /Vi S < T
ConcentDate ExtDate AmConc/DiPercent 1Percent f
<ChforometftaneSrornometnaneVmv* ChfondeChloroeirijneMetnylene Chlonde *f J3AcetoneCarbon Dtsuifide1. 1-OicnJoroetheneT. l-OichforoerhaneTran«-l, 2-DictttoroemeneChloroform1, 2-Dichioroemana2-3uranone1, 7. 1 -TncftloroetrumeCarbon TetracfifondeVmvi AcetateSromodicfiiorometnane
VolatjIe-J•ation: (LowV- --acted/Prepare
ComJMId:
QC Report NcContract No:Date Sample
poundsidium (Cir"2, /T /y
Sample Number
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68-01- U- 1RArr*iw*H- f / Y /* '
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r jg. n_ i'L> ilw5" LLC LCS" LUV LwC t*.c- u.fb U-r ius~ u_/O u-- ix
/uACAS ^Number ^79-34-S78-87-510061-02-679-01-6124-48-179-OO-S71-43-210061-01-5110-75-875-25-2591-78-6L1 08- 10-1127-18-41OS-B8-3108-90-7100-41100-42-5
1. 1. 2. 2-Tetracrtloroetnane1. 2-Dichiorooro0aneTrans-1, 3-DfCfHoroorooeneTriehloroetrteneDtbromocnioromBthane1, 1 . 2-TncntoroernaneBenzeneCiS-1. 3-Otcnloroorooene2-Chioroethv(vinv(etherBromoform2-H.ntanone4.Methvt-2-PentanoneTetrachloroeiheneTolueneChlorobenzenegtnvlbenzeneStvreneTotal Xvlenes
• TCirele On«l- tt-
c*" O 1*, i
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m«a ov GC 'MSl <n m* final •nrtcr
U !**«.« C*T« *,. >nMlMt ICK M «« «,«« MSffapofl tn* mtrumuffl aiiKlton umir tor trv* MTTOI* wiin9w U (• e . ItXJf Mswi on n«e««a«rv coneeninnon ' • Thi» f(*g it us«d wt>«n m« »n*lyi* >i 'ouna in tn* bla*lut«»n KT«nx fThit u net McMMniy tft* in«mm«m •• *•» tf J umpi* u indcim POWHB** •
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Environmental Protection Agencv. CLP Samole Management Off rce,P.O. Box 818. Alexandria. Virginia 22313 703/557-2490
Organics Analysis Data Sheet(Page 2}
SemivoJ*tiIe CompoundsConcentration: f Low/ Medium (Circle,0ne)
Sample Number
s\Qfltf.
Date Anat>Conc/Dil F
CAS (Number62-75-9108-95-262-53-31 1 1 .44-4
95-57-8541-73-1106-46-7100-51-695-50-195-48-739638-32-9106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-965-85-0111-91-1120-83-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47-488-06-295-95-191-58-788-74-4131-11-3208-96-899-09-2
N-NiTrosodimemviammePhenoJAnilinebis(-2-ChloroethvHErher2-Chforonhenol1. 3-Diehlorobenzene1. 4-OicnlorobenzeneBenzvl Alcohol1. 2-DiChlorobenzene2-Methvlpnenolbis(2-chloroisoproDVllEtrier4-MethvtohenoIN-Nuroso-Di-n-ProovlammeHexacntoroernaneNitrobenzeneIsophorone2-Nttroonenol2, 4-DtmethviorienolBenzoic Acidbis(-2-ChloroethoxvtMethane2. 4-Dichloroohenoi1, 2. 4-TnchlorobenzeneNapnthalene4-ChforoaniimeHexacniorobutadiene4-Chloro-3-Metriviprienol2-WetnvinaDnirialcneMexacniorocvciopeniadiene2, 4. 6-Tnchloropnenol2, d. 5-Tncniorophenoi2 -Chloronapnthaiene2-NitroanilmeDimethvl PnrMaiateAcenapntnvlene3-Nitroanthne
«H. VlfrhHartnr- *\C Q
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'u uSO;v
83-32-951-28-510O-02-71 32-64-9121-14-2606-20-284-66-27005-72-386-73-7100-01-6534-52-186-30-6101-55-3118-74-187-85-585-01-8120-12-784-74-2206-44-092-37-5129-OO-085-68-791-94-156-55-3117-81-7218-01-9117-84-0205-99-2207-08-950-32-8193-39-553-70-3191-24-2
Acenaontnene2. 4-Dinttroohenot4-NitroonenolDibenzofuran2. 4-Ointtrototuene2. 6-Oimtrotofuene 'OierhvtoMthalate4-Chloroohenvl-pr.envtetrterFluorene4-NJtroanifme4, 6-Dinitro-2-MethvlphenolN-NitrosoOipnenytamrne (1 )4-8romophenvl-ohenyletrierHexachlorobenzenePentachiorophenolPhenamhreneAnthraceneDi-n-8utvbhthalateFluorantneneBenztdtnePyreneButvibenzviprtrnaiate3. 3'-DicnloroOenziarneBenrcxafAntriracenebisi2-EtnvihexvDPntnaiateChrvseneDi-n-Octvt PhthatateBenzwbtFluoranineneBenzcKkiFluorantneneBenzo<a)Pvreneinoeno.1. 2. 3-cd)PvreneDibenria. niAntnraceneBenztxq. h i)PCrvf»nc
(1 J-C»nnot D« seoerated from dionenylamtne
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Environmental Protection Agency. CLPSamo'eManagement Office.P.O.SoxSlB. Al«x»nana. Virginia 22313 703/557-2*90 /*-__. <r*
Organics Analysis Data Sheet{Page 3)
Pesticide/PC 8sConcentration: lLow /Medium (Circle One)
i-^ /. IDate F*tfart»rf/Pr»pap»rl-. ',!-•!•
Date Analyzed: J. AtT/S T* 11 -, x"Conc/Dil Factor:
Sample Number
CAS C"g/ip* ug/KgNumber ") Circle One)319-84-6319-85-7319-86-853-39-976-44-8309-00-21024-57-3959-93-86O-57-172-55-972-20-S33213-65-972-54-87421-93-41031-07-850-29-372-43-553494-70-557-74-98001 -35-21 2674-: .-211104-28-211141-16-553469-21-912672-29-611O97-69-111096-82-5
Aiona-BHCBeta-SHCDeltl-BHCGamma-BHC (LinoaneiHeptacntorAlarmHeotacnior EooxioeEndosuifan IDjeidnn4. 4--ODEEndnnEndosuifan 114. 4'-ODDEndnn AldehvfleEndosutfan Sutfate4. 4--DDTMethoxvcrtiorEndnn KetoneChlordaneToxaoheneAroctor-1016Aroclor-1221Aroctor-1232Aroclor-1242Arocior-1248Aroctor-1254Aroclor-1260
O.C5" t*-c.c.r uC.JJ<1 LO.C*T M_.C.C.C M_r .o«r LIC J? iA.
r.CT Ln. /d 6ciC.ro tc-O,(O /x»c- 1 <-; CC u /jur\ ' w '^—r- (C IAC fO t^r-5t- ix_,' '. r C £A_C.*5-o trl. O tv-/-, vO tr . o Wo. u 6 -T-Vo lwC.VO Lt,t. o • ;(1-0 KX
Vj = Volume of extract injected {ul)
V = Volume of water extracted (ml)
Wg = Weight of sample extracted (3.
V = Volume of total extract (ul.
r.w.eecet*. Mwm.Wfen*ZUUf - 7 •*/
Organic* Analyst* Data Short
C«*eNo;O 13 I - V ' QC Report W*
,______. Contract No: .C*te S«mp*e Receive*
VoMteCompoundf.Medium (Circle One)
VeeeiB Aekel"" ^ • BV
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Organics Anatytli Data Sh*«t(P»9t 2)
SamtvoUttet CompoundsConcantiaiion: Lew _ Sjym _ • (Orel* One)
Eampie Number
L-3I tt
CA«
Sample Number22313 70J/M7-14IO
, Organics Analysis Data Shaat
Concentration: Low /^Mediuny (CircleOne)Data EKtrectad/Praparad:DataAnatyad:——3'A/-5Vg 5"Cone/Oil factor ——LJ.——————CASNumber (Ctfde11944-631S-9&.7}i»46-aSeVB»'976-444J09-00-21024.57-3W9-9S-8BO-57.172-55-972.20433213-65.972-54-87X21-93-41031-07450-29-372-43-5S3494.7O.S57.7448001.3S-212674-11-2IT 104-28-211141-16-653469.21412672-29411097-69-11109642-5
Alpne-VHCBeta-BNCDelu-BHCOemnw-BHC (Undene)
AWrinHeptachlor EpoaioeEneoewKenlDieUrin4. 4--DDEEndrinEndoeuttenl4. 4'-ODDEndrin AldehydeEndoeuHen SuHate4. 4--DOT
Endrin KetoneChtordeneToxapheneAroelor.1016A/oclor-1221Aroclor-1232Aroc tor- 1242Aroclof-1248Aroctor-1254Aroclor.1260
/rov«51Putic*)2C,L
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Vj * Volume of ettrect infected (ul)
Vf B Volume of water ectrected (ml)
W( « Weight of sample enrected (Q)
V( » Volume of touf eviract (ul)
v. ______
Form! WVI V w *--- 4'B4,
Organics Analysis DataD
27
Environmental Protection Agency. CLP Sample Management Office.P.O. 3ox318. Alexandria, Virginia 22313 703/557-2490
Organics Analysis Data Sheet(Page 2)
Sermvok,tile CompoundsConcentration: ( Low/ Medium (Circle One)^ - - ; . I „.. T
Sample Number
Date AnalyConc/Di[ F
f^ •4o VPlUFT1O0r
62-75-9108-95-262-53-31 1 1 -44-495-57-8541-73-1106-46-7100-51-695-50-195-48-739638-32-9106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-965-85-0111-91.1120-83-2120-82-191-20-3106-47-887-68-359-50-7 ~91-57-677-47.488-06 -'2'95-95-491-58-788-74-4
131-11-3208-96-899-09-2
N-NttrosodirnejnviaminePhenolAnilinebis(-2-Chloroethvl)Ether2-Chloroohenol1 . 3-DichloroOenzene1. 4-DichlorobenzeneBenzvl Alcohol1. 2-Dichlorobenzene2-Metnvlohenolbts(2-chloroisoproDvMEther4-MetnvipnenolN-Nitroso-Di-n-PropvlammeHexacnloroetnaneNitrooenzeneJsopnorone2-Nitropnenof2. 4-OimetnvlonenotBenzoic Aciflbrs(-2-Ch(oroethoxv)Methane2. 4-Oichtorophenot1. 2. 4-TricniorooenzeneNapnthalene4-ChtoroanilmeHexacnioroPuiaaiene4-ChJoro-3-Methyfpnenoi2-Metny) naphthaleneHexacnlorocvclooentadiene2. 4. 6-Tncnloropnenot2, 4. 5-TncnioroDhenof2-Chloronapnthalene2-NitroanitmeOimethvl PhthatateAcenaohthvlene3-Nitroaniltne
_• »"7 / / n r v ^r*mH- t£>-j i ° f X
»Mnr" "lO O
' ——— N.ug/ljrr ug/Kg CAS (""""TCircta One) Number
fO L<~(0 fc/n [,<-/n to/D ;*~1C IX_/C £*_ir> L.)n u-'C l<-'0 Lv-/O f •—JO W-/D U-;O fv/O it
f n w.r/ 0 (L*rO K-10 LV_'O t*-fO Lv./O Lk_'O i/Oil
fO tC./O LL"iO I.L'C KO IL10 IV'0 LVS'O i -
83-32-951-28-5100 -O2 -7132-64-9121-14-2606-20-284-66-27005-72-386-73-7100-01-6534-52-186-30-6101-55-3118-74-187-86-585-01 -8120-12-784-74-2206-44-092-87-5129-00-085-68-791-94-156-55-3117-81-7218-01-9117-84-0205-99-2207-08-950-32-8193-39-553-70-3191-24.2
Acenapnthenc2, 4-Dinttrophenoi4-NitroonenolDibenzofuran2, 4-OinitrorolLt0ne2. 6-DinitrotofueneDiethylpnrhatate4-Chlorppnenyt-phenyietnerFluorane4-NitroanHme4, 6-Dmitro-2-MethytphenolN-Nitrosodtpnenytamine ( 1 .4-8romopnenyl-pheny)emerHexachlorobenzenePeniachlorophenotPhenanthreneAnthraceneDi-n-ButvlphthalateFluorantheneBenzidmePyreneButylPenzvlphthaiate3. 3"-DichJorooenzidmeBenzo<a)Antnracenebis<2-EthvihexvnPhmaiateChryseneDi-n-Octvi PhthalateBenzocblF.uoramrieneSenzwkiFfuorantneneBenzotafPyrenelndeno< 1 . 2. 3-cdtPvreneDibenzia. hlAntnraceneBenzotq. h dPervfene
(1 J-C*nnot be «g|ff!»<«*rfIHa.42efttan.na
S~ ——— Nug/lor ug/Kg
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Environmental Protection Agency. CLFSamole Management Office.P. 0. SoxaiS. Alexandria. Virginia 22313 703/537-2490
Organics Analysts Data Sheet(Page 3)
Pesticide/PC SsConcentration: (tow /Medium (Circle One)Date Extracted/Prepared: . ' ?/ * / °^
i-» /-» /O,L{ LDate Analyzed: _L
Sample Number
Conc/Dil FactorCAS -. • I ug/lj* ug/KgNombeir v . TCircle) On«J319-84-6319-85-7319-86-858-89-976-4A-S309-00-21024-57-39S9-98-860-57-172-55-972-20-833213-65-972-54-87421-93-41031-07-850-29-372-43-553494-70-557-74-98001-35-212674.11-211104-28-211141.16-553469-21-912672-2S-611O97-69-111096-82-5
Afona-BHCSeta-SHCDelta-BHCGamma-BHC (UnoaneiHeptacntorAlarmHeotacnior EooxioeEndosuifan lDieiflnn4. 4--DDEEndnnEnocsutfan n4. 4--DDDEndnn AWehvaeEndosuifan Sulfate4, 4--DDTMethorychlorEndnn KetoneChiordaneToxapheneArocIor-1016Aroclor-1221Aroclor-1232Aroctor-1242AroclOr- 1 248Arocior-1254Aroclor-1260
O.C'S' &-r r,r L*-C.C* iX-D.f.T iu-C.cC /x.r .(J- LIC-C5" u.r.CT (>-
Oi /Cy i- -iC- IO £C-O.fO AUc- 1 o' u.ft- IV AC.n. fo *^r to /AC 'O r *.c-5<- 6c,- ;. r c u.C.*ro i. O tv_/-, VD £A_r.- C WC- u tr.Co toC- *ro t\(.0 tl1 • O" v^
V; 2 Volume of extract injected (ul)
V. = Volume of water extracted (mil
W = Weight of sample extracted (g)
V. = Volume of tPtai extract (ul)
A/A
\ C. 73Organic* Anatysls Data Sh*trt
No.UbS.-g.PH* C73/;^—————— OCfUportN*
SolL~_________—— Counsel Woe -Drti fltlMM ftumoriMdfir ^ JL ^ 0*t« S»rrt?*« R#c v«±
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CAS
gency.0. ftwSlt, AtMMrtnt. VWgMft 22313 703/U7-24SO
Organics Analysis Data Shoat
Sampfe
Concentration: Uw /Ittodiurh (Circle On*)——•".« /x /^,j
O.U Extrwt«l/rV«p.r«d:D«t* An*tY2*d: _——.llConc/DU Factor:CAS
(Ctrcto319-B4-6319-BS-7
58-89-9
309-00-21 024*57-3
W-57-t72-S&-972-20-i
72-S447421-93-4
50-23-372-43-5
57-74-t9001-35-212674-11-211104-28-2
53469-21-912672-29-61 1097-69-11 1096-12-5
Aipha-BHCD«U-BHCIWU-BMC
HeyHCMorAUrinHvptacMor EpOMd*EndotuHint
4, 4'-DD€EndrinEndotuftonl4.4*4)00Endrin AibehyO*Endosutfan Suf at*4.4'-OOTM*thonchlerEndrin Kcton*
Arodor-IOIflAroclof-1221Aroelor-1232Aractof-1242Aroctor-1248Arockw-1254Aredor-1260
7l
2 700 H
V- • Vo(um« o* «0r»ci ini«cttxt (ul)
Vg « Votum* ol water attracted (mil
W, * Weight of umptt •uractod <g)
V > Vottinw o( toal oxtract M>
V, ___________ orW, ——LL———— V, ^.-"i'"-——— V4
Environmental Protection Agencv. CLPSampfe Management OWice.P. O, Bo* 813. Alexandria. Virginia 22313 703/557-2490
Organics Analysis Data Sheet(Page!)
Laboratory Name: Gulf South Research Institute Case No; Ou
Sampia Number
tab Sample fSample MatrData Release
CASNumber74-87-374-83-375-01-*75-00-375-09-267-64-175-15-075-35-475-34-3156-60-567-66-3107-06-278-93-371-55-656-23-5108-05-475-27-4
awn- T^D 31-*• FAJ .TC "AMthnrf«rt By 7&&>.S&~'&&4
ConcentrDate ExtiDate AnaConc/DiPercent fPercent f
<ChforometnaneSromometnaneVinvi ChlorideCftiorwrnaneMernviend Chlonae . S". Acetone;Car&an Otsulfidet. l-DiCfiloroemene1. l-OichloroetnaneTrans-1. 2-DichioroetneneChloroform1. 2-DichIoroemane2-Butanone1, 1. 1-TncnJoroethaneC*r&on TerracfiiondeVmvf AcetateSromodicnioromatnanff
Volatileation: (lowacted/Prepare
QCD
pmp(jMedi
tffti«tiir»- ,, /y,WtsUire (Decanted)^ug/lyrug/Kp
0 L*-/O tJ;ri 0_/r_J i*-
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r * *-68-01-' U fH«.i«*H. / /V/?/
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^ )t*4/ = r)pH U •1,PC-
/J ACAS fNumb«r ^79-34-578-87-510061-02-679-01-6124-48-179-00-571-43-210061-01-5110-75-875-25-2591-78-6103-10-1127-18-4108-88-3108-90-71 00-4 1-410O-42-S
1 1,2. 2-Tetracnioroemane1. 2-DicrtloroprgoaneTrans-1. 3-DtchloroofooeneTnchloroerneneDibromocnioromethane1.1, 2-Trtcnforo«inan*Benzenecis-1. 3-Oichiorooroo«ne2-ChloroetnvivinvtetherBromoform2-Hexanone4.Wctrivl-2-PentanoneTetrachtoroetheneTolueneChlorobenzeneEthvlbenzeneStvreneTotal Xvlenes
•—•ug or ug/Kg""Tcirel« One I
<p u~5" i5^ *A—r —
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Data AetKWT'ng Qualifier*for reooning reiutifl to E*A. tl%« following raiulti gualifiarf arc ua*d *Additional f1ig» Of 'oomores enrtaming remits ara encouraged Homvwr. tn* CO•Winnion oTeacn flag mutt a* • solicit ..*.
Value IT tt%* reiutt is * wlu* gr*aivr man or equal to tnt C Thit (lag >DOli*t to oatHCiO* Mrametar* wn«r* .n« <— -,SMectton ttmtt. reeon tn* va'u* iO*nnfic*tion nat ee*n eonfirm«a BV GC 'MS Smgi*
comoon*ni o*«ttc«*«« *!0 ng 'ul m trie hnaJ extract
ftmort rn* mifttmum detection limit for tna tamine *»>tntrw u (• 5. TOUl datatf on n»e»sa*rv esncaniration' a Thit flag it u&*d wnen in« analyi* >• found m tn* etana•iiution actions (Th* ta net n*c*«»aniy in* innrumaw at «*n ti a tamoia n md«ai*« pe««»t*acwemn bmic J Th* faoirxjt* cnouid r*afl U- 6'"n« contamination ana w*m* trw data u»*fCema mS «•• anaiwatf *or *ot net MtaetM Tr» a«xeonate action
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Environmema I Protection Agency. CLP Sample Management Office,P.O. Box 318. Alexandria. Virginia 22313 703/557-2490
Organics Analysis Data Sheet(Page 2)
Sernive**vtile CompoundsConcentration: r Low/ Medium (Circle One)
Sample Number
Date Extracted/Preparec_ 1 ~2,D^te Analyred- L
i- _LZ-/S--£I /Y¥-L/iJH '
Conc/Dil Fartnr- ^O O
CAS (Number62-75-9108-95-262-53-31 1 1 -AA-A
95-57-8541-73-11O6-46-7100-51-695-50-195-48-739638-32-9106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-965-85-0111-91-1120-83-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47-488-06-295-95-4'91-58-7 '88-74.4131-11-3208-96-899-09-2
N-NitrosodtmethyiaminePhenolAnilinebisf-2-ChloroemvliEther2-Ctilorophenol1. 3-Dichtor_obenzene1. 4-DichtorobenzeheBenzvl Alcohol1. 2-Dichlorobenzene2-Methvlohenol•brsQ-chlororsooroDvMEther4-MethylDhenotN-Nitroso-Di-n-PropylamineHexachtoroetnaneNitrobenzeneIsophorone2-Nttroonenol2, 4-DimethvipnenolBenzoic Acidbrs{-2-Chloroethoxv)Methane2. 4-Dichloro0henoi1 . 2. 4-TnchlorbbenzeneNapntnatene4-ChloroantdneHexacniorooutadiene4-Chloro-3-Methylohenol2-MethvtnaqhthaleneHexacnlorocyciooentadiene2. 4. 6-Tnchloropnenot2. 4. 5-TnchtoroDhenoi2-Chloronapnthaiene2-NitroamlmeDimethyl PhthalateAcenaohthvlene3-Nitroantlme
ug/tflT og/Kg CAS (' {Circle One) Number
fO ioto f^in L<~/n LL,10 ^fC M_/C U.in u^in u./C u..'0 Lir\ t _0 U./n LfO to/O *cin t^/O |.L5~0 w-iO u-/O t,IO L/O LO'(') iC.'0,_V10 L>~/O 'X.10 /,CfO IL
~\ \_) 'LIO Micnclo L^10 aSO ;
83-32-951-28-5100-02-7132-64-9121-14-2606-20-284-66-27005-72-386-73-7100-01-6534-52-186-30-6101-55-3118-74-187-86-585-01-8120-12-784-74-2206-44 -O92-87-5129-00-085-68-79 1-94-156-55-3117-81-7218-01-9117-84-0205-99-2207-08-950-32-8193-39-553-70-3191-24-2
Acenaonthene2. 4-Dmitrophenol4-NitroohenolDibenzofuran2. 4-Dmitrotofuene2. 6-DintfrotolueneDiethytphthalaie4-Chloroohenvl -ohenvietherFluorene4-Nitroanriine4. 6*Dinitro-2-MethyiphenolN-NitrosoOiphenvlamme (1 )4-Bromophenyl -phenyletherHexachtorobenzenePemachtorophenoiPhenanthreneAnthraceneDi-n-ButylphthalateFluorantheneBenzidmePvreneButvtbenzvlphthaiate3, 3"-Dicntorot)enzidineBenzaaiAnthracenebia2-EtnvihexvMPhtnaiateChrvseneDi-n-Octyi PhthalateBenzofb)FiuorantheneBenzaitiFluoramheneBenzotatPyreneIndenw 1 . 2. 3-cd)PvreneDibenzia. htAnrhraceneBenzwq. n dPervlene
(1 .-Cannot be 0£rate<3Jramj4iqM*vtamine
S~ —— *. ug/ or ug/Kg"*"• '("Circle Onal
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Organics Analysis Data Sheet3)
Samp.e Number
Pesticide/PCBsConcentration: (LOW /Medium JCircle One)Dare Extracted/Prepared: / / / °'j_ y jDate Analyzed: I7-/20Conc/DN Factor ___
319-S4-6319-85-7313-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-87421-93-41031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-271141-16-553469-21-912672-29-611097-69-111096-82-5
Aiona-BHCBtra-BHCDefta-BHCGamma-BHC (Linda neiHeotacniorAlarmHeotacntor EooxideEndosuifan lDieiann4, 4--ODEEndnnEndosutfan lj4. 4'- ODDEndnn AldehydeEndosulfan Sulfate4. 4--DDTMethoxvehlorEndnn KetoneChlordaneToxaoheneAroc(or-1016Aroclor-1221Arocior- 1 232Arocior-1242Arcxrlor- 1 248Arocior-1254Aroctor-1260
O.c - ex.c.cr 6c-e t<_O.C.S" ix_.c.cC xr.ccr uC-C5" /xr.G?" L-, 0 /Xr:- (O toO.fO /X( -IU iCr</u /xfiJO S,r (C fAc. tO i.*~r..5C r -. r c L^C.*5"0 iI. O i\~/ .vO £xr.<0 UO-Tu 6^ 'r..Cc5 i."~C- O iv_i-o nJ-O tw
Vj = Volume of extract injected (ul)
Vs = Volume of water extracted (ml)
ws = Weight of sample extracted (3)
Vt s Volume of total extract (u!)
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Organics Analysis Data ShMt(Page 3}
S*mpto Number
Concentration: Lgfltx Medium (Circle One)D*ttExtract*d/Pr«p»r*d:DawAnah/wt ———— ;4Conc/DU Factor:CASNumber319-84-6319.85-7319-66-85S-89-976-44-S309-00-21024-57-3959-90-8BO-57-172-55-972-20-833213-65-972-54-87421-93-41031-07-850-29-372-43-553494-70-557-74-98001 -35-212674-11-211104-28-211141-16-553469-21-912672-29-61 1097-69-11 1096-82-S
Alpha-SHCBeta-aHCDefta-BHCCUmma-aHClUndane) s
AWrinHaptacntor EpexidaEndoauHan 1DiekJrin4. 4--DOEEndrinEndoautfah i4, 4'-000Endrin Aldahydt-EndotuHan Surtate4. 4'-ODTMet noii rworEndrin KetoneChlordanaTonphenaAroclor-1016Aroctor-1221Aroelor-t232Areclor.1242Arodor.1248Aroclor-1254Arodor-1260
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V$ « Votwme o* wtter extracted (ml|
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V, > Volume of total extract (ul)
orWs
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IMLJSCORPORATION
332 OLD EAGLE'seHaai- R'bAOTSuiTe's'i B"WAYNE. PENNSYLVANIA 1 9OS7 " '215-BS7-S51O . . . '" -^ ----:;
March 20, 1986R-585-8-5,.3068-01-6699
Mr. Harold ByerU.S. Environmental Protection Agency841 Chestnut BuildingNinth and Chestnut StreetsPhiladelphia, PA 19107
Subject: Peer Review CommentsTDD No. F3-8408-08Saunders SupplyChuckatuck, Virginia
Dear Mr. Byer:
Submitted herewith are the responses to the peer review comments for the subjectproject. The following changes and clarifications have been made within thereport: " " '" ' ------—- - - -
o Typographical errors have been corrected, and grammatical changes havebeen made where appropriate.
o . proper technical reference to dioxin sampling was inserted in regard tosection 1.2.
o Hazard Ranking System (HRS) (reference no. 4) information has been addedto section 2.4.
o In regard to section 2.6, information concerning permit issue and testingwere added to this section.
o Pond and intake distances from the facility were included in section 3.1.Additionally, a statement clarifying that Godwins Mill pond is also knownas Crumps Mill pond was added.
o Section 3.7 has been rewritten to agree with the HRS.
o HRS (reference no. 4) information dealing with waste quantity producedhas been added to section 4.0.
o Proper technical reference to dioxin sampling was inserted into section 5.1.
A Halliburton c°m*w &B . G 0 U 6 U
Mr. Harold ByerU.S. Environmental Protection AgencyMarch 20, 1986 - Page 2Saunders Supply Company Peer Review Comments Letter
o The appropriate changes have been made to the Site Inspection Form.
If you have any further questions, please contact me.
Respectfully submitted, Reviewed by,
Martin Howe Richard Cromer Garth GlennHydrogeologist Assistant Manager Jftanager, FIT III
MH/kf
NUS CORPORATION
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY- - REGION III841 Chestnut Building-IWj Philadelphia, Pennsylvania 19107
SUBJECT:Request Assistance from FIT Office 7~ ~ /DATE: 7. (1
FROM: Darius Ostrauskas, Environmental ScientistSite Investigation & Support Section (3HW23)
TO: Butch Byer, FIT Regional Project OfficerSite Investigation and Support Section (3HW23)
I. SITE NAME:
II. LOCATION:
HI. WORK ASSIGNMENT:
Slt"!nKectlon - ————— Qualltl *"«•»« "-lew of DataHar«d£S%«, ————— Re-Sampling/Full Field Investigation
7ToxicolovToxicology Assessment ....__. other (See VI below)Enforcement Support —————
IV. PRIORITY
High (*) ,: .. _. Medium
T7 ,V. Preferred Deadline
EXPLANATION OF TASK (* To include justification for high priority):
\y s*
VII. To be completed by FIT RPO only:.
Task complete date by FIT:
Hours allocated:...
t, 2 I
G
„ ^ +~V *^ '
>«r.s-t-c fj~t -S",7"
p-d
o
- &&&*.--?. S .oo
frOctober 10, 1984 ™
To: FILE
From: Darius Ostrauskas
Subject: Saunders Supply Company
Yesterday, I inspected the above site and spoke with Mr. F.D. Howell, Jr.,Vice President of the facility. He stated the following at that tiae:
- vood was f ••••••£ with pentachlorophenol (PCP) on-site between 1964and 1974
- between 1964 and 1974, 1000 gallons of PCP sludge were generatedper year and all of the sludge was disposed of on-site
* disposal consisted of burning the sludge along with wood scraps ina pit on. site
— in 1974, the facility began treating wood with chromated copperarsenate solution and started to slowly phase out the use of PCP
- from 1974 to 1984, all PCP sludge was disposed of off-*ite byJ & L Industries of Newport News, VA
- frost 1964 to 1974, liquids separated from the PCP sludge were dis-charged into an on-site wastewater pond (during the inspectionthis pond was observed by D*0. to have a discharge pipe leading to anintermittent stream adjacent to the site)
- sludge was separated from liquid on-site in at least 2 tanks- one tank had a capacity of 1000 gallons and was filled with whatwas identified as PCP sludge if the time of the inspection)
NUSCORPORATION
332 OLD EAGLE SCHOOL ROAD. SU'lTE 31 B'WAYNE. PENNSYLVANIA 1 gd@7 " '" " ''215-GB7-S51O -. -. '- -=:~ '.W .'":">-4-=
March 20, 19S6R-5S5-S-5-3Q68-01-6699
Mr. Harold ByerU.S. Environmental Protection Agency8*1 Chestnut BuildingNinth and Chestnut StreetsPhiladelphia, PA 19107
Subject: Final ReportTDD No. F3-8W8-08Saunders. SupplyChuckatuck, Virginia
Dear Mr. Byer:
Submitted herewith is a final Site Inspection report for the subject project.
Based on our review of available data, we have concluded that EPA should considerthe following: • ...
o A program of continued monitoring of Godwins Mill Pond Reservoir fororganic and inorganic compounds should be implemented.
o A program of continued monitoring of "the Keliey well and monitoring wellsystem should also be implemented. . _ . .
o Runoff from both the process area and the hardware store area should becontrolled.
o Air sampling for particulates (i.e., chromium and dioxins) should beconducted. •• - -
o Remaining waste sludge and dioxin-contaminated soil should be removedand disposed and/or isolated.
Saunders Supply Company is an active facility which began treating wood withpentachlorophenol (PQP) in 1964. :In 1970, they began also using chromated-copper-arsenate (CCA), and have been using CCA exclusively since 1984. Wastechemicals consisting of PCP, CCA, and no. 2 fuel oil were burned in a shallowsurface pit as a means of disposal. In 1981, Ronald Keliey, of the neighboringKelley's Nursery, complained to health officials that he was finding an oil liquid inpost holes on his property. The Virginia State Health Department and VirginiaState Water Control Board (VA SWCB) began an investigation which led them toconclude that the burn pit was the source of most of the contamination.Subsequently, Saunders had a monitoring well and recovery system installed, inaddition to removing the noticeably contaminated soil from the burn pit.
A Halliburton Company
Mr. Harold ByerU.S. Environmental Protection AgencyMarch 20, 19S6-Page2Saunders Supply Final Site Inspection Report
FIT III conducted a sampling of soil from auger holes adjacent to the burn pit.These samples were analyzed for all isomers of dioxin. The FIT also conducted aroutine environmental sampling of the site, the surrounding area, Godwins MillPond Reservoir, and a monitoring well system for the burn pit. The results of theseanalyses can be found in appendix E and section 6.0, respectively.
A release of contamination from the site to the groundwater has been establishedby the sample results. A release to the surface water is strongly suggested,although no substantiation for PCP found in the upstream sample has beendetermined. This, however, indicates that runoff from the Saunders SupplyHardware Store area may be carrying chemicals from the wood products to thetributary. Further investigation in this regard may be warranted.
A toxicologicai evaluation of the site identifies numerous potential health threatsto local residents and to those who consume water from Godwins Mill Pond. Acomplete review of .the toxicologicai impact of the site may be found in section7.0.
Presently, there are small quantities of waste sludges being held on the site intanks and drums. It appears from the auger samples that additional soil, extentunknown, is contaminated with dioxin compounds outside the burn pit. Soilexcavated from the pit by Saunders was taken to the John C. Holland Landfill (VA-177) for disposal and should be screened for dioxin compounds.
NUS has submitted a Hazard Ranking System (HRS) model to EPA for this site witha score-of 45*95. NUS is presently conducting a dioxin extent of contaminationstudy*
If you have any further questions, please contact me.
Respectfully submitted, Reviewed by, Approved b
Martin Howe Richard Cromer Garth GlennHydrogeologist Assistant Manager Wlanager, FIT III
MH/kf
NUS CORPORATJOIM
