Sample Prep System - GPC Cleanupgpccleanup.com/pdf/PrepLincSystemCatalog.pdfSample Prep System J2...

1901 Pennsylvania Drive Suite CColumbia, MO 65202(573) 214-0472 (866) 292-0472 Fax: (573) 214-0474www.j2scientific.com sales @j2scientific.com

Sample Prep System

J2 Scientific introduces the ultimate flexibility and automation for the sample prep lab. The PrepLinc™ Platform Automated Sample Preparation System offers the ability to combine common sample prep process inline on one system. With modules available for automating Solid Phase Extraction, Gel Permeation Chromatography Cleanup and Concentration, there are a multitude of configuration possibilities. Combine SPE with Concentration, combine GPC Cleanup with SPE, even concentrate a sample between two processes.

The combination of these technologies gives the user flexibility and options to signifi-cantly decrease sample handling while increasing data quality and productivity. High powered software utilizes the features of each module to make the PrepLinc™ a complete sample prep solution,

Autosampler - Create unique mat with your choice of tray sizes - Create user-defined trays in the software - Septum piercing is standard

SPE - Use up to 15 mL columns; not limited to one manufacturer - Multi-column methods - Positive pressure with programmable flow rates - Forward and reverse flow on any position - Large volume pump option for a variety of water methods

AccuVap - Only FULLY automated concentration system - Concentrate samples from SPE & GPC or from vial - Collect multiple fraction in chamber for combined concentration - Quantitate in chamber; transfer to GC vial ready for analysis - Take sample completely to dryness or adjustable endpoint - Chamber options based on final volume

GPC Cleanup - Direct Inject; inject entire sample onto column - Use traditional and high pressure columns up to 5500 psi - Integrate with AccuVap or SPE

Hardware Configurations SPE Single Column * SPE Multi-Column * GPC Cleanup * Stand Alone Concentration ** GPC Cleanup with Inline SPE Multi-Column*

GPC Cleanup with Inline SPE Single Column* * Mode can be combined with optional AccuVap Concentration system ** Requires optional AccuVap FLX System

Programming Multi-Module Methods with Linc EditorThe Linc Editor makes it possible to “linc” methods from different modules together to process a sample in one pro-cess. The easy drag-and-drop editor is a breeze to use and it really completes the PrepLinc™ group of products.

Autosampler Mat Editor & Capacity

GPC with Evaporation – 216 Samples• GPC Only Mode – 84 Samples• GPC with SPE Mode -- 45 Samples • SPE Single Column Mode – 45 Samples• SPE 2 Column Mode – 18 Samples • SPE 3 Column Mode – 9 Samples• SPE w/ Evap. Single Column – 45 Samples• SPE w/ Evaporation 2 Column – 18 Samples • SPE w/ Evaporation 3 Column – 9 Samples•

PrepLinc™ Sequence Editor

Sequences are not limited to one method, one module or one “Linc” method• User can customize sequence as laboratory flow dictates• Choose sample and collect tray and location for first sample; sequentially copies for additional sam-• ples, but can be edited for unique situationsChoose priority samples• Re-arrange, add and delete unprocessed samples after run has begun•

Change method and tray information for unprocessed samples after run has begun•

1901 Pennsylvania Drive Suite C1901 Pennsylvania Drive Suite CColumbia, MO 65202Columbia, MO 65202

(573) 214-0472 (866) 292-0472 (573) 214-0472 (866) 292-0472 Fax: (573) 214-0474Fax: (573) 214-0474

www.j2scientific.com sales @j2scientific.comwww.j2scientific.com sales @j2scientific.com

To request a quote or locate your nearest dealer, contact Customer Care

toll-free in the US at1-866-292-0472

or 1-573-214-0472

The flexible autosampler mat editor and tray editor provide for a variety of sample and collect tray configurations.

Standout Features:

Automated Solid Phase Extraction

The PrepLinc™ SPEi from J2 Scientific ac-centuates our line of full-featured auto-mated sample preparation instruments. The SPEi system uses positive pressure for consistent flow sample to sample and run to run. The intuitive software and range of parameters make method de-velopment easy. Converting any manual SPE method to automated takes no time.

Use the SPEi as a stand-alone automated SPE system or integrate with other PrepLinc™ modules, like the AccuVap™ Evaporation module or GPC Cleanup module for a completely automated sample prep system.

Use cartridges from 1mL - 15mL plus many specialty and flash chromatography columnsUse cartridges from 1mL - 15mL plus many specialty and flash chromatography columns• • Perform multi-column procedures; up to 5 columns inlinePerform multi-column procedures; up to 5 columns inline• • Flow Inject Module for water/aqueous samples *Coming SoonFlow Inject Module for water/aqueous samples *Coming Soon• • Concentrate eluate to final volume or concentrate between prep processes with our Accu-Concentrate eluate to final volume or concentrate between prep processes with our Accu-• • VapVapAbility to perform forward and reverse elution through cartridgesAbility to perform forward and reverse elution through cartridges• • Program up to 12 different solvents in a methodProgram up to 12 different solvents in a method• • Programmable flow rates to 65 mLs/minProgrammable flow rates to 65 mLs/min• • Positive Pressure Elution for Sample and SolventsPositive Pressure Elution for Sample and Solvents• • Nitrogen Drying Nitrogen Drying • • Select from 12 Solvents for processing (3 standard)Select from 12 Solvents for processing (3 standard)• • Closed System with Pressure MonitoringClosed System with Pressure Monitoring• •

SPE for Environmental, Water, Food, Pharma and Forensics samplesAutomate a manual SPE method in minutesAdapt to any cartridge style from 1mL to 15mL

Configuration OptionsAdd up to 5 SPEi column modules •

- Capacity of 45 samples - Flow from one module to any other module

Add column modules as need • increasesSolvent selector valve for selection •

of up to 12 solvents

1901 Pennsylvania Drive Suite CColumbia, MO 65202(573) 214-0472 (866) 292-0472 Fax: (573) 214-0474www.j2scientific.com sales @j2scientific.com

SPE Method EditorCreate simple, single-column or complex, multi-column methods through the same intuitive method editor.

Configuration Options

The method screen shown at left is an example of typical single column SPE method. There is one condition step, the sample is introduced to the column, a wash step, the sample is dried and then the sample is eluted.

This example method is more complicated and shows the real flexibility of the PrepLinc software. Three SPE columns are used for this example. Condition and wash steps are performed to move the sample through all three columns. A reverse elution is performed on one of the columns for the final collection. Both elutions are evaporated using the optional AccuVap and can be collected in separate vials.

PL GPC Cleanup Module

AccuVap Inline or FLX modules - Inline offers GPC + Evap mode - FLX offers GPC + Evap mode and Evap Only mode

SPE CartridgesThe SPEi system will adapt to most manufacturers cartridges.J2 Scientific offers a selection of cartridges, adapters and plungers.

PrepLinc ModulesAdd these modules to your PrepLinc system for increased flexibility and automation.

Standout Features: Enclosed evaporation chamber• Three heating zones with user defined heat & vacuum for each • zoneVacuum control from 100-760 torr• Two endpoint settings: dryness or adjustable endpoint (1-5 • mL)Manage use of up to three solvents for sample exchange, final • solvent and rinsingAdd a pre-evaporation spike• Add a keeper solution• Perform multiple solvent exchanges• Heated rinse cycle with choice of solvent ensures no carry-over• Transfer concentrated sample into GC vial or other storage vial•

Adding an AccuVap™ Concentration Module to the PrepLinc™ System eliminates the need for a separate bulk evaporation step when combined with processes like SPE or GPC Cleanup. Choose from two models: AccuVap™ Inline or AccuVap™ FLX. Both offer concentration of sol-vent directly from another process (GPC or SPE), but the FLX also allows offline concentration.

Unlike other semi-automated evaporation systems, the AccuVap™ will automatically solvent exchange and quantitatively transfer your sample to a GC vial ready for analysis. Powerful software controls heat and vacuum at every stage of the process to protect analyte recoveries. Programmable heated rinses eliminate carryover.

Save time and improve results. Free up lab technicians and decrease sample handling. Adding the AccuVap™ to your PrepLinc™ system will really automate your world!

AccuVap™ Method EditorThe PrepLinc™ AccuVap™ Method Editor is • full-featured, yet intuitive. Parameters for each stage of the concentra-• tion process are clearly separated. Solvents are programmed at software setup • for easy recall when programming methods. Heating rates and vacuum settings are adjust-• able on the fly for quick method develop-ment.Knowledgeable applications staff are avail-• able to optimize method parameters for matrix, solvent and analytes of interest.

AccuVap™ Options

Inline or FLX ModelChoose your AccuVap model based on intended uses. Consult the lists below to determine the model best suited for your lab.

AccuVap™ Inline - GPC with Evaporation* - SPE with Evaporation*

AccuVap™ FLX - GPC with Evaporation* - SPE with Evaporation* - Evaporation Only

* Requires additional PL options

Solvent Recovery Module & ChillerCollects and condenses solvent vapor from concentration process for disposal or recycling

SRM Condenser ModuleCondenses solvent vapor and drains to vessel for disposal or recycling.Collects up to 95% of solvent vapors

Immersion ChillerChiller options for SRM module.140 W at -30oC

Evaporation Chamber OptionsChoose an evaporation chamber based on the desired final volume.

AV081 - StandardFor final volumes from 1 mL to 10 mL

AV082 - 5mL TipFor final volumes from 0.5 mL to 5 mL

AV083 - 10 mL TipFor final volumes from 0.5 mL to 5 mLFor small volume and single addition concentrations


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or 1-573-214-0472

Optional PL GPC Cleanup Module

Optional PL SPEi Starter Kit

(can add 4 more column modules)

Standout Features:

The GPC Cleanup Module for PrepLinc™ performs clean-up of a wide range of sample matrices including foods, tissues, grains, plants and environmental samples such as soil, sludge, and hazardous waste for EPA (SW-846 Method 3640A), CLP, FDA, USDA and USDI analysis.

Using our experience with GPC Cleanup, J2 Scientific has perfected it on this new platform. All the unique features of previous models are combined with high-powered software and the ability for further automation by combining GPC with other prep processes on the PrepLinc™.

The PrepLinc™ GPC Cleanup Module provides another level of functionality to the PrepLinc™ system. The abil-ity to combine GPC Cleanup with Automated Concen-tration and/or SPE on the PrepLinc™ system, completes the sample prep package.

Direct Inject - inject the entire sample onto the column• Septum piercing standard for sample & collect vials• Probe tracking & user-defined rinses• 2- or 5-column selector valve• UPS Power Watchdog• Sample Dilution• Multiple Injections• Specialized calibration & reporting software features for GPC• Create methods directly from the column calibration file• Use with low-pressure glass or high pressure columns• Integrate with PrepLinc SPE and AccuVap modules•

GPC Method EditorUse the defined method templates for standard GPC Cleanup and Column calibration or create a specialized method with multiple collect or dump fractions using the simple method builder.

Programmable dilution prior to • injectionDifferent flow rate during equili-• brationUser defined rinses• Collect fraction flow directed to • SPE column*Collect fration flow directed to • AccuVap*Program multiple collect • fractions; direct each to vial, SPE • or AccuVap individually**requires optional modules

GPC Cleanup Reports

Configuration Options

Autosampler OptionsChoose the autosampler size based on desired batch capacity and level of integration with other PrepLinc modules. Choose Model 3300 autosampler for capacities up to 72 samples per batch and in-getration with up to two SPEi column modules. Choose Model AS4 autosampler for capacities up to 200 and full SPEi integration.

with Model 3300 with Model AS4

PrepLinc Module OptionsThe following PrepLinc modules can be added for integration with the GPC Cleanup module.

PrepLinc SPEi Starter Kit - Add two column modules with M3300 autosampler - Add five column modules with AS4 autosampler

AccuVap Inline or FLX modules - Inline offers GPC + Evap mode - FLX offers GPC + Evap mode and Evap Only mode


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or 1-573-214-0472

The PrepLinc™ software makes keeping track of your column calibration and sample data easy. Create Method and Configuration reports to report sytsem setup. Create Sequence reports with time/date stamps. Create Calibration and Comparison reports in compliance with Method 3640a and CLP guidlines. Quickly determine if a column calibra-tion has met pass/fail requirements and print a report to prove it!

with Model AS4

Standout Features: Enclosed evaporation chamber• Three heating zones with user defined heat & vacuum for each • zoneVacuum control from 100-760 torr• Two endpoint settings: dryness or adjustable endpoint (1-5 mL)• Manage use of up to three solvents for sample exchange, final • solvent and rinsingAdd a pre-evaporation spike• Add a keeper solution• Perform multiple solvent exchanges• Heated rinse cycle with choice of solvent ensures no carry-over• Transfer concentrated sample into GC vial or other storage vial•

A new way to concentrate! The AccuVap EVS™ combines gentle heat and vacuum to concentrate large volumes of solvent. Precise control devices monitor solvent volume, temperature and vacuum to ensure controlled evaporation.

The AccuVap EVS™ Evaporation System is a fully automated way to concentrate offline samples ranging in volume from a few to hundreds of mil-liliters of solvent. The AccuVap EVS™ can replace more manual evaporation methods like kudera-dan-ish, rotary evaporation and other semi-automated techniques.. The AccuVap EVS™ performs solvent exchange and quantitative transfer.

AccuVap EVS™ Method Editor

The PrepLinc™ AccuVap EVS™ Method Editor • is full-featured, yet intuitive. Parameters for each stage of the concentra-• tion process are clearly separated. Solvents are programmed at software setup • for easy recall when programming methods. Heating rates and vacuum settings are adjust-• able on the fly for quick method develop-ment.Knowledgeable applications staff are avail-• able to optimize method parameters for matrix, solvent and analytes of interest.

Concentrate samples after PFE extraction.Full automation for concentrating overnight.Concentrate large volumes after liquid-liquid extraction.Fully automates most other evaporation techniques.

AccuVap EVS™ Options

Autosampler OptionsChoose the autosampler model based on capacity need. The Model 3300 autosampler offers 72. The Model AS4 offers 216.

Solvent Recovery Module & ChillerCollects and condenses solvent vapor from concentration process for disposal or recycling

with Model 3300with Model AS4

SRM Condenser ModuleCondenses solvent vapor and drains to vessel for disposal or recycling.Collects up to 95% of solvent vapors

Immersion ChillerChiller option for SRM module.140 W at -30oC

Evaporation Chamber OptionsChoose an evaporation chamber based on the desired final volume.

AV081 - StandardFor final volumes from 1 mL to 10 mL

AV082 - 5mL TipFor final volumes from 0.5 mL to 5 mL

AV083 - 10 mL TipFor final volumes from 0.5 mL to 5 mLFor small volume and single addition concentrations


(573) 214-0472 (866) 292-0472 (573) 214-0472 (866) 292-0472 Fax: (573) 214-0474Fax: (573) 214-0474




or 1-573-214-0472

with Model AS4with Model 3300

Sample Prep System - GPC Cleanupgpccleanup.com/pdf/PrepLincSystemCatalog.pdfSample Prep System J2...

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