Rock - SRMEG · Rock Klima, Schubert Texture-Coefficient (Howarth & Rowlands 1987) Considers: Grain...

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1 1 Short Course Singapore 2011 Rock Klima, Schubert Rock 2 Short Course Singapore 2011 Rock Klima, Schubert The Rock Cycle drawing: USCS http://3dparks.wr.usgs.gov/nyc/images/fig6.jpg

Transcript of Rock - SRMEG · Rock Klima, Schubert Texture-Coefficient (Howarth & Rowlands 1987) Considers: Grain...

Page 1: Rock - SRMEG · Rock Klima, Schubert Texture-Coefficient (Howarth & Rowlands 1987) Considers: Grain Shape Grain Orientation Grain Interlocking AW Weighting factor for packing density

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Rock

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Rock

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The Rock Cycle

drawing: USCShttp://3dparks.wr.usgs.gov/nyc/images/fig6.jpg

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Graph: USCShttp://3dparks.wr.usgs.gov/nyc/images/fig6.jpg

The Rock Cycle

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GraniteIgneous (magamatic) rock, plutonic rock

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BasaltIgneous (magamatic) rock, vulcanic rock

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Sediments(“soil”) over consolidated silt / clay

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Sandstonesedimentary rock

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Limestonesedimentary rock

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Metamorphic RocksMineral Assemblage Change: Shale to Schist

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Slate very low grade metamorphic rock

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Phyllitelow grade metamorphic rock

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Dolomite – marblemedium grade metamorphic rock / carbonatic rock

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Mica Shistmedium grade metamorphic rock

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Gneishigh grade metamorphic rock

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How to name rocks

• Mineral constituents

• Chemical composition (magmatic rocks)

• Texture / structure / microtexture

• Grain size (sedimentary rocks)

• Geological position (magmatic rocks: plutonite– vulcanite)

• Genesis of rocks Recommendations by the IUGS Subcommissions on the

Systematics of Igneous Rocks and Metamorphic Rocks

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How to name rocks

• main constituent: constituent (mineral) present in modal content ≥50%.

• major mineral constituents: constituent (mineral) present in modal content ≥5%.

• minor constituents: constituent (mineral) present in modal content <5%.

• essential constituent: constituent (mineral) that must be present in a rock in a certain minimum amount to satisfy the definition of a rock

• critical constituent: constituent (mineral) indicating by its presence or absence distinctive conditions for the formation of a rock and/or a distinctive chemical composition of a rock.

• Recommendations by the IUGS Subcommission on the Systematics of Metamorphic Rocks: Web version 01/02/07

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Composition

Fabric

Origin

XRD analysis, optical microscopic scanning, chemical analysis

Optical macro – microscopical inspection, XR texture analysis, microspicalautomated interactive image analysis

Fabric elements, mineral paragenesis, geological considerations

A proper rock name is derived from:

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Microscope

Thin Section

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X-RAY Diffractometer

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Principle of X-Ray Diffraction

Bragg's LawThe layers of a crystal act like weak reflecting mirrors for the X-

rays. Only if the path difference of the reflected X-rays is a whole number of wavelengths does constructive interference occur. This is described by Bragg's Law:

nλ = 2dsinθ

λ: wavelength of the X-raysd : the spacing of the layersθ: the incident angle of the photons

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Principle of X-Ray Diffraction

XRD Pattern of a mixture of Minerals

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Properties appointed by:

• mineral composition

• texture / structure / microtexture

• history of origin / genesis

• condition / weathering / alteration

ROCK (Intact rock)

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Example: Serpentinite

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Rock Fabric:Texture and Structure

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Fabric:The complete spatial and geometrical configuration

of all components (penetrative fabric elements, scale dependent) that make up a rock

Texture:Geometrical aspects of the

component particles of a rock, including size, shape and

arrangement;

Also:

Degree of crystallographic lattice-(or shape-) preferred orientation of

components

Structure:The presence of compositional

layering, folds, foliation, fractures, lineation . .

(scale dependent!)

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Rock (Micro-) Fabric:Elements, Terms Symmetry

different types of voids (microcracks, pores), their size, orientation and distribution

disturbance of crystallites (free space in the solid matrix)

voids

vector data (shape preferred orientation); scalar data (grain shape, grain size)

geometry (morphology) of crystallites (related to the solid matrix)

microstructure

crystallographic preferred orientation (e.g., quartz c-axes etc.)

preferred orientation of lattice of crystallites (related to the solid matrix)

texture

ExampleAspect of materialElements of rock fabric

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Rock Section displayingcomposition and microfabric elements of thematerial

(Shape, Size, Interlocking, arrangement of grains)

Original Photograph

Line Drawing

ExplodedDiagram

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Scope O: outlines of porphyroclasts and ribbons

Scope I: elongate parent grains, transgranular and grain-boundary microcracks

Scope II: recrystallised grain mosaique, subgrain boundaries and complete microcrack pattern

Example „scopes“ of fabrics:

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Some Microstructural Indices

Perimeter LP is the length of all edge pixels outlining an object

Shape Factor SF is an expression of the circularity of an object. SF is calculated as:

A = area of grain

LP = perimeter of grain

SFA

LP

=4

2

π

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Some Microstructural Indices

Compactness is a numeric expression of the shape of an object as it moves from a circle to a line. Compactness is calculated as:

A = area of grain

LP = perimeter of grain

CompactnessLAP=

2

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Some Microstructural Indices

Aspect ratio AR is a numeric expression of grain elipticity. AR is calculated as:

Dmax = major axis length

Dmin = minor axis length

ARDD

= max

min

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Some Microstructural Indices

Index of grain size homogeneity : t (index of “textural”homogeneity introduced by Dreyer 1973. t is calculated as:

Aavg = average grain area

Ai = area of individual grain

[ ]t

A

A A

avg

i avg

=−∑ ( )2

12

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Some Microstructural Indices

Feret’s diameter: Feret's diameter is the greatest distance possible between any two points along

the boundary of a region of interest. Dequiv is calculated as:

A = grain area

DA

equiv =⎛⎝⎜

⎞⎠⎟

412

πminimumFeret‘s diameter

maximumFeret‘s diameter

ΘL, ΘB = angle

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Some Microstructural Indices

Index of interlocking: g (Dreyer1973) calculates the complexity of grain-grain relationships. g is calculated as:

n : number of grain considered

Ai : area of exposed grain section

LPi: portion of the grain perimeter which contacts neighboring grains

gn

=⎛

⎝⎜⎜

⎠⎟⎟∑1

12

L

AP

i

i

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Some Microstructural Indices

Foliation index: F (Tsidzi 1986) is calculated as:

Mi : content of phase i

Si : shape factor (aspect ratio)

F M Si in i

n

=⎛⎝⎜

⎞⎠⎟

=∑1

100

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Texture-Coefficient (Howarth & Rowlands 1987)

Considers:Grain ShapeGrain OrientationGrain Interlocking

AW Weighting factor for packing densityN0 Number of grains with aspect ration <2.0N1 Number of grains with aspect ration >2.0FF0 Mean value of the Form Factors of all grains with aspect ratio <2.0; FF describes the deviation of grains from circular shape and the

roughness of the grain boundary respectivelyAR1 Mean value of all aspect ratios >2.0

AF1 Angle factor, a measure of the degree of constant grain orientation and the deviation of the max Feret’s diameter from a reference direction

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Texture-Coefficient (Howarth & Rowlands 1987)

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Texture-Coefficient (Howarth & Rowlands 1987)

Relationship between texturecoefficient and UCS

Relationship between texture coefficient and TBM performance

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Texture-Coefficient (Howarth & Rowlands 1987)

Texture coefficient of igneous and sedimentary rocks

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Texture-Coefficient (Howarth & Rowlands 1987)

Relationship between texture coefficient and UCS of 9 different metamorphicrock types (50 samples): no correlation for metamorphic rocks!

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Intergranular microcracks

(quartz, Biotite)

Intragranular microcracks

quartz, feldspar, biotite, chlorite

Microcracks

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Disintegration of rock by inter- und intragranular microcracks

QU quartz FSP feldspar

GR garnet BI biotite

CHL chlorite

GR

QU

FSP

BIBI

BI

FSP CHL

QU

Microcracks

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Example thin section photograph, traced grain boundaries and microcrack traces pattern.

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Rock (Micro-) Fabric:Elements, Terms Symmetry

transgranularcrack

intergrain, multigrain crack

multigrain microcrack

transecting one or more grains

intergranularcrack

grain-bounderymicrocrack

grain-bounderymicrocrack

between two grains

intragranularcrack

intragrain, cleavage, transgranularcrack

intragranularmicrocrack

inside one grain

Terms used in fractographicstudies (e.g., Monoto et al., 1981)

Terms used in geological studies (e.g., Richter and Simmons, 1976; Kranz1983)

Proposed termPosition of the microcrack

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Rock

Klima, SchubertX

Y

Z

Schematic Microcrack Orientation and DistributionExample

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in particular the microcrack pattern is responsible for the regular divisibility of apparently massive rock, e. g. marbles for utilization as dimension stones

Microfabric,

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Pore size distribution of gneisses, cummulative [cm3/g]

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Pore size distribution of gneisses, -dV/dlogD [c3/g]

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Characterization of Intact Rock:

Abrasiveness

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Quartz Equivalent Proportion

0,1553Carbonate

31,05total

1,32334Phyllosilicate

5,581831Feldspar

24,0024100Quartz

Example:

Proportion [%]

Rosival-abrasion-hardness

Mineral

Page 26: Rock - SRMEG · Rock Klima, Schubert Texture-Coefficient (Howarth & Rowlands 1987) Considers: Grain Shape Grain Orientation Grain Interlocking AW Weighting factor for packing density

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Abrasiveness of Sedimentary rocks(FSCHIM )

[mm] mean diameter of quartz grains

V [%] Quartz equivalent proportion

[MPa] Brazilian tensile strength

Schimazek & Knatz 1970

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CERCHAR-Abrasiveness-Test

• The abrasiveness of intact rock or rock mass affects the wear behaviour of drilling, cutting and milling tools.

• Abrasiveness of rocks depends on different parameters (e.g. structure and texture, equivalent quartz content, Young’s modulus)

• CERCHAR-Abrasiveness-Test is a common testing procedure for the prediction of tool wear due to the fast measurement process and the cheapness.

• The only formal description of this test is the French Standard AFNOR, NF P94-430-1 (2000)

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CERCHAR-Abrasiveness-Test

„West-Apparatus“(1989) at Graz, University of Technology, Institute of Applied Geosciences, [1] weight, [2] steel pin, [3] vise, [4] rock sample, [5] hand crank

Sample-specimens

steel-styli

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CERCHAR-Abrasiveness-Index (CAI)

Worn steel stylus tip under the microscope (right picture: 90° rotated)

CAI = d*10

d : diameter of worn stylus dip [mm]

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Cerchar-Classification-Scheme(CERCHAR, 1986)

extremely abrasive4,0 - 6,0

very abrasive2,0 - 4,0

medium abrasiveness to abrasive1,0 - 2,0

slightly abrasive0,5 - 1,0

not very abrasive0,3 - 0,5

ClassificationCAI

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CAI of some rocks

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Abrasiveness 0.1 mm

Mohs‘scale

Relation between Mohs‘ hardness grade and steel point abrasiveness test value

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MLPC ABROY Abrasion Meter500 g of crushed rock in the grain size range of 4 - 6.3 mm is placed in the container and the vane is rotated at 4,500 rpm for 5 minutes.The vane suffers abrasion and resulting loss of mass. The quantity of abraded vane metal is then correlated to rock abrasiveness.

French Standard AFNOR, NF P18-579 (1990)

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Qualitatively estimate of the durability of weak rocksSlake Durability Test (ASTM D4644)

Type I: Retained specimen remain virtually unchanged

Type II: Retained specimen consist of large and small fragments.

Type III: Retained specimen is exclusively small fragments.

Calculating the slake durability Index 2nd circle):

B = mass of drum plus oven-dried specimen before 1st circle [g]

WF = mass of drum plus oven-dried specimen retained after the 2nd circle [g]

C = mass of drum [g]

Id(2) = [(WF – C) / (B – C)] x 100

Id(2) = [(WF – C) / (B – C)] x 100

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Qualitatively estimate of the durability of weak

rocks Slake Durability Test (ASTM D4644)

< 30< 60Very Low Durabiliy

30 – 6060 – 85Low Durability

60 – 8585 – 95Medium Durability

85 – 9595 – 98Medium High Durability

95 – 9898 – 99High Durability

> 98> 99Very High Durability

% retainedafter 2 cycles

% retainedafter 1 cycle

Group Name

Gambles´ Slake Durability Classification (Goodman 1980)

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Swelling

Swelling of the ground is a time dependant volume

increase, which is caused by physical-chemical

reactions of rock and water, leading to inward

movement of the tunnel perimeter.

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• Swelling by capillary adsorption

• Swelling by osmosis

• Swelling by hydration of interlayer cations

(swellable clay minerals, e.g., smectite)

• Swelling by formations of new crystal structures

(e.g., anhydrite + water = gypsum)

Stress-Relief - Physico-Chemical Effects Involving Water

Swelling

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• Stress relief leads to a modification of the inter- or

intra-particle stresses which in turn facilitates flow and

ad/absorption of water

• Stress relief causes fissures which in turn facilitate flow

of water

• Water addition causes modification (increase) of inter

(intra) particle distances and this in turn affects the

stresses

Swelling

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• Water content changes increase pore water pressure

from an originally negative to a smaller negative or to a

positive value

• Fissuring or breaking of diagenetic bonds during

shrinkage facilitates flow and modifies original stresses

which in turn facilitates interparticle or intraparticle

addition of water

• Indirect effect: Shearing (e.g. of faults) breaks

diagenetic bonds and increases the exposed surface

areas

Swelling

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Swelling

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Klima, Schubert

Basic Elements of Silicate Structure

Swelling

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67

Short Course Singapore 2011

Rock

Klima, Schubert

Swelling

Crystalline Structure of swellable Smectite

INSTITUTE FOR ROCK MECHANICS AND TUNNELING

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Short Course Singapore 2011

Rock

Klima, Schubert

Huder-Amberg-graph

Swelling

Page 35: Rock - SRMEG · Rock Klima, Schubert Texture-Coefficient (Howarth & Rowlands 1987) Considers: Grain Shape Grain Orientation Grain Interlocking AW Weighting factor for packing density

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Short Course Singapore 2011

Rock

Klima, Schubert

Clay – content [%]

Swelling-pressure[MPa]

Swelling-pressure of clayey anhydrite depending on clay-content, after 600 days

Swelling

INSTITUTE FOR ROCK MECHANICS AND TUNNELING

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Short Course Singapore 2011

Rock

Klima, Schubert

Swelling