Rocas - Abrasividad 2

7
 International Journal of Rock Mechanics & Mining Sciences 43 (2006) 321–327 Technical note The inuence of steel styli hardness on the Cerchar abrasiveness index value T.N. Michalakopoulos , V.G. Anagnostou, M.E. Bassanou, G.N. Panagiotou Laboratory of Excavation Engineering, Department of Mining Engineering, National Technical University of Athens, Zographou Campus, GR-15780 Athens, Greece Accepted 30 June 2005 Available online 12 September 2005 1. Introd uction During the last decades mechanical rock excavation has gained a signicant share in the construction of both civ il and mi nin g eng ine erin g projec ts. The mac hin es use d for mec han ical roc k exc avatio n are in genera l capital intensive and, in most cases, site specic, so that a good und erstand ing of the app lic ation condit ions plays a vital role in maximizing machine performance. A number of models have been developed during the last years to evalu ate mach ine perfo rmance under various application conditions  [1–3]. In al l such mo del s rock abrasiveness is an intact rock property used as a major input parameter  [1,4]. According to Atkinson  [5]  the abrasiveness of a rock ‘‘is the wear or loss of material which the rock produces on another material such as a TBM cutter or drill bit insert. [y] It is a function of mineralogy, especially the quartz content, and the microstructure of the material.’’ Abrasi veness is considered to exp res s ‘‘a behavi oral cha racteristic of the rock rat her tha n a fundamental physical or mechanical property’’. As a consequence, it is di f cult to impl ement a test ing procedure wi th a strong, unambiguous physical basis and a large number of testing procedures have been proposed. A number of dif fere nt roc k abrasiveness tests have been reported [1,5–7]. Of these tests the Cerchar test has gained populari ty as a rel ati vely convenie nt and ine xpe nsi ve met hod of mea sur ing and compar ing the abrasiveness of rocks  [1–5,8–11]. The resulting Cerchar Abr asi ven ess Index (CAI) val ue is use d as an inp ut parameter by many of the above-mentioned models for estimating mechanical excavators performance. However, in spite of its popularity, there are some ambiguities in the description of the test setup in the various references, especially regarding the hardness of the steel styli used. In this paper the inuence of the steel styli hardness on the CAI value is examined. 2. Testing p rocedu re The Cerchar test has been proposed by the Labora toire du Cen tre d’Etud es et Rec her ches des Cha rbo nnag es (Cerchar) de France  [12]. According to the original test specication, West  [13]  prepared a testing device, which is shown in  Fig. 1. The testing device mainly features a vice, 1, holding the rock sample, and a steel stylus, 4, tting into a holder, 5. On the stylus a dead weight of 70 N is appl ied , 6. The rock sampl e vi ce can be move d under the steel stylus through a handwheel, 2, that drives a scre wth read of pit ch 1 mm/ rev. To determine the CAI value the rock is slowly displaced by 10 mm with a vel oci ty of app rox ima tel y 1 mm/ s. The abrasiveness of the rock is then obtained by measuring the resulting wear at on the tip of the steel stylus. The CAI value is calculated using the following formula  [14]: CAI ¼ 10 2 d , (1) where d  is the wear at diameter of the stylus tip in mm. From the above description, the Cerchar test can be classied as an  abrasive wear with pressure test [15]. AR TIC LE IN PR ESS www.elsevier.com/locate/ijrmms 136 5-16 09/ $ - see front matte r r 2005 Elsevier Ltd. All rights reserved. doi:10.1016/j.ijrmms.2005.06.009 Cor resp ond ing author. Tel.: +30210 7722208; fax: +30210 7722191. E-mail address:  [email protected] (T.N. Michalakopoulos).

description

ROCAS 2

Transcript of Rocas - Abrasividad 2

  • International Journal of Rock Mechanics & Mi

    ical

    li hs i

    osto

    ining

    GR-1

    30 Ju

    e 12 S

    is the wear or loss of material which the rock produces

    However, in spite of its popularity, there are some

    (Cerchar) de France [12]. According to the original test

    is shown in Fig. 1. The testing device mainly features a

    where d is the wear at diameter of the stylus tip in mm.

    ARTICLE IN PRESS

    Corresponding author. Tel.: +30210 772 2208;

    From the above description, the Cerchar test can be

    classied as an abrasive wear with pressure test [15].

    1365-1609/$ - see front matter r 2005 Elsevier Ltd. All rights reserved.

    doi:10.1016/j.ijrmms.2005.06.009

    fax: +30210 772 2191.

    E-mail address: [email protected] (T.N. Michalakopoulos).quartz content, and the microstructure of the material.Abrasiveness is considered to express a behavioralcharacteristic of the rock rather than a fundamentalphysical or mechanical property. As a consequence, itis difcult to implement a testing procedure with astrong, unambiguous physical basis and a large numberof testing procedures have been proposed.A number of different rock abrasiveness tests have

    been reported [1,57]. Of these tests the Cerchar test hasgained popularity as a relatively convenient andinexpensive method of measuring and comparing the

    vice, 1, holding the rock sample, and a steel stylus, 4,tting into a holder, 5. On the stylus a dead weight of70N is applied, 6. The rock sample vice can be movedunder the steel stylus through a handwheel, 2, that drivesa screwthread of pitch 1mm/rev.To determine the CAI value the rock is slowly displaced

    by 10mm with a velocity of approximately 1mm/s. Theabrasiveness of the rock is then obtained by measuring theresulting wear at on the tip of the steel stylus. The CAIvalue is calculated using the following formula [14]:

    CAI 102d, (1)insert. [y] It is a function of mineralogy, especially the

    on another material such as a TBM cutter or drill bit specication, West [13] prepared a testing device, whichTechn

    The inuence of steel styabrasivenes

    T.N. Michalakopoulos, V.G. Anagn

    Laboratory of Excavation Engineering, Department of M

    Zographou Campus,

    Accepted

    Available onlin

    1. Introduction

    During the last decades mechanical rock excavationhas gained a signicant share in the construction of bothcivil and mining engineering projects. The machinesused for mechanical rock excavation are in generalcapital intensive and, in most cases, site specic, so thata good understanding of the application conditionsplays a vital role in maximizing machine performance. Anumber of models have been developed during the lastyears to evaluate machine performance under variousapplication conditions [13]. In all such models rockabrasiveness is an intact rock property used as a majorinput parameter [1,4].According to Atkinson [5] the abrasiveness of a rockambiguities in the description of the test setup in thevarious references, especially regarding the hardness ofthe steel styli used. In this paper the inuence of the steelstyli hardness on the CAI value is examined.

    2. Testing procedure

    The Cerchar test has been proposed by the Laboratoiredu Centre dEtudes et Recherches des Charbonnagesning Sciences 43 (2006) 321327

    note

    ardness on the Cercharndex value

    u, M.E. Bassanou, G.N. Panagiotou

    Engineering, National Technical University of Athens,

    5780 Athens, Greece

    ne 2005

    eptember 2005

    abrasiveness of rocks [15,811]. The resulting CercharAbrasiveness Index (CAI) value is used as an inputparameter by many of the above-mentioned models forestimating mechanical excavators performance.

    www.elsevier.com/locate/ijrmms

  • A formal description of the testing procedure isprovided in the French standard NF P 94-430-1 [14],which, to the authors knowledge, is the only formalstandard.Al-Ameen and Waller [16] and Plinninger et al. [17]

    provide signicant details about the testing conditionsand their inuence on the CAI value.

    3. Steel styli specications

    According to the French standard NF P 94-430-1 thetip of the steel stylus applied to the rock sample isformed as a sharp conical point of cone angle equal to901731 and 1mm length. The overall length of the steelstylus should be greater than 15mm.The recommended steel styli geometry is generally the

    same in the various references. However, this does notapply regarding the hardness of the steel styli. It is

    obvious that any change in the hardness of the steelstyli alters signicantly the testing conditions, thusproviding incomparable CAI values. This has beendemonstrated by Al-Ameen and Waller [16], whenthey modied the test specications, in order to enablethe determination of the CAI value of certain coalsamples.In the original test setup description [12], Valantin

    recommended styli made from steel of 2000MPa tensilestrength. No recommendation was made for the stylihardness.Suana and Peters [18] recommend steel styli of

    ARTICLE IN PRESS

    Reference Tensile strength (MPa)

    T.N. Michalakopoulos et al. / International Journal of Rock Mechanics & Mining Sciences 43 (2006) 321327322Valantin [12] 2000

    Suana and Peters [18] 2000

    Atkinson et al. [8,9]

    West [13] 2000

    Atkinson [5] 2000

    Al-Ameen and Waller [16]

    AFNOR [14]

    Plinninger et al. [17] 2000Fig. 1. The West testing device for determining the Cerchar

    abrasiveness index (reproduced from [13]).

    Table 1

    Recommended steel styli specicationsRockwell Hardness HRC 5456 and 2000MPa tensilestrength.Atkinson et al. [8,9] recommend styli made of EN24

    or EN25 steel, heat treated to 610 Vickers Hardness(HRC 56).West [13] also recommends styli made of EN24 steel

    with a tensile strength of 2000MPa, but heat treated toHRC 40.Atkinson [5] does not provide any recommendation

    on steel type, but recommends steel of 2000MPa tensilestrength and HRC 5456.Al-Ameen and Waller [16] follow the recommenda-

    tion of Atkinson et al. with styli made of EN24steel, heat treated to 610 Vickers Hardness, butalso provide a recommendation for modied styli madeof EN3 steel heat treated to 225 Vickers Hardness(HRC 19).AFNOR [14], which provides the only formal test

    description, species that the styli must be made of steelheat treated to HRC 5456.Plinninger et al. [17] suggest the use of 115CrV4 steel

    hardened to HRC 55 with a tensile strength of about2000MPa.The various recommendations can be seen in Table 1.From the authors experience, although it is clear

    from the above that there is a general consensus for stylimade from steel heat treated to HRC 5456, severalequipment manufacturers, planners and contractorsrequest CAI values determined with steel styli of HRC40, as is recommended by West.

    Hardness Steel type

    HRC 5456

    HRC 56 (HV 610) EN24 or EN25

    HRC 40 EN24

    HRC 5456

    HRC 56 (HV 610) EN24

    HRC 19 (HV 225) EN3

    HRC 5456

    HRC 55 115CrV4

  • 4. Test setup and results

    The objective of this study has been to investigate theinuence of steel styli hardness on the CAI valueobtained. To accomplish this objective the CAI valueof 73 rock samples has been determined for twodifferent steel styli types. Of the 73 samples, 5 wereeither extremely fragmented/weathered or too hard totest, thus results for a total of 68 samples were obtained.The samples were of 6 different rock types, which can beseen in Table 2.Each sample has been subjected to 5 individual tests

    with each steel styli type, and the mean CAI value andstandard deviation of the mean corresponding to eachstyli type have been computed.The specications of the utilized steel types can be

    seen in Table 3. Styli of hardness HRC 55 were usedbecause this is the hardness specied in the formal testdescription, and of HRC 40 because this is therecommendation by West, which is more frequentlyused in routine Cerchar testing.The CAI values obtained can be seen in Table 4,

    where CAI55 stands for CAI values obtained with steelstyli of HRC 55, and respectively CAI40 for HRC 40. InTable 5 the absolute frequency of the obtained CAI

    used. Moreover, it is observed that the CAI40 values aredistributed over a wider range.

    Finally, Eq. (2) has been used to relate the CAI55 andCAI40 value classication shown in Table 8.

    ARTICLE IN PRESST.N. Michalakopoulos et al. / International Journal of Rocvalues for each steel styli type can be seen. Fig. 2 showsthe corresponding bar chart.As expected, the CAI40 value was greater than the

    CAI55 value for all rock samples, demonstrating the

    Table 2

    Sample description

    Sample type Sample nos.

    (i) Gabbro 13

    (ii) Pyroxenite-Gabbro 4

    (iii) Mylonite 516

    (iv) Recrystalized massive limestone 1724

    (v) Serpentinized peridotite 2552

    (vi) Limestone 5368

    Table 3

    Utilized steel styli nominal specications [19,20]

    CAI55 CAI40

    Steel type CALMAX EN24 (BS970-817M40)

    HRC 55 40

    C % 0.60 0.40

    Ni % 1.80

    Cr % 4.50 0.80

    Mn % 0.80 0.70

    Mo % 0.50 0.25

    Si % 0.35

    V % 0.20 6. Conclusions

    The Cerchar test has gained popularity as a relativelyconvenient and inexpensive method of measuring and5. Regression analysis

    In Fig. 3 the plot of CAI40 versus CAI55 values ispresented. The relation of the two CAI values has beenexamined and a linear correlation was observed, yieldingthe following equation:

    CAI55 0:110914 0:587356CAI40. (2)The predicted CAI55 values and the corresponding

    residuals for each rock sample are given in Table 4. Thepredicted CAI55 values are plotted versus the observedones in Fig. 4, indicating that no signicant anomaliesare present.The regression analysis is given in Table 6, and the

    analysis of variance in Table 7. Since the p-value inTable 7 is less than 0.01, there is a statistically signicantrelationship between CAI55 and CAI40 at the 99%condence level.The R2 statistic indicates that the model as tted

    explains 73.9251% of the variability in CAI55. Thecorrelation coefcient equals 0.859797, indicating amoderately strong relationship between CAI55 andCAI40. The standard error of the estimate shows thestandard deviation of the residuals to be 0.393807. Thisvalue has been used to construct the 95% prediction andcondence bands presented in Fig. 3.In Fig. 5 the studentized deleted residuals are plotted

    versus the predicted CAI55 values. The randompattern indicates that the selected model describesadequately the observed data. Moreover, the linearityand homoscedasticity of the residuals are veried. Theabsolute studentized deleted residuals of 6 observationsare greater than 2.00 and are identied as potentialoutliers.In Fig. 6 the quantile plot of the standardized

    residuals empirical distribution and the standardnormal distribution can be seen. This plot veries therequired regression assumption of normality.signicant impact of steel styli hardness on the obtainedCAI value. The reasonable general conclusion of thisinvestigation is that the CAI value of a rock sample isdecreased by an increase of the hardness of steel styli

    k Mechanics & Mining Sciences 43 (2006) 321327 323comparing the abrasiveness of rocks. However, there are

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    Table 4

    Analysis of the observed CAI values and the linear model results

    Sample no. Observed CAI40 Observed CAI55 Predicted CAI55 Observed residuals Standardized residuals Studentized

    deleted residuals

    Mean Std deviation

    of the mean

    Mean Std deviation

    of the mean

    1 6.35 0.68 3.58 0.28 3.840620 0.260623 0.666800 0.7189372 4.55 0.28 3.66 0.30 2.783380 0.876618 2.242813 2.359460

    3 2.49 0.28 2.13 0.57 1.573430 0.556570 1.423975 1.436480

    4 4.27 0.39 3.05 0.15 2.618920 0.431077 1.102904 1.118210

    5 1.78 0.53 1.25 0.29 1.156410 0.093593 0.239456 0.239430

    6 2.85 0.49 2.06 0.19 1.784880 0.275122 0.703895 0.701103

    7 0.64 0.12 0.64 0.06 0.486822 0.153178 0.391903 0.401577

    8 3.08 0.49 1.73 0.28 1.919970 0.189969 0.486033 0.4832809 1.35 0.38 1.27 0.17 0.903844 0.366156 0.936804 0.949292

    10 1.35 0.19 1.45 0.11 0.903844 0.546156 1.397331 1.428140

    11 2.87 0.73 1.32 0.29 1.796620 0.476625 1.219437 1.22389012 2.06 0.61 2.44 0.49 1.320870 1.119130 2.863276 3.049710

    13 3.51 0.13 2.67 0.08 2.172530 0.497468 1.272764 1.282000

    14 3.35 0.85 2.62 0.27 2.078560 0.541445 1.385278 1.397030

    15 2.08 0.61 1.30 0.19 1.332610 0.032614 0.083442 0.08311516 5.28 0.29 3.27 0.29 3.212150 0.057848 0.148003 0.152330

    17 2.87 0.14 1.75 0.21 1.796620 0.046625 0.119289 0.11838118 2.54 0.21 1.78 0.16 1.602800 0.177203 0.453371 0.450868

    19 2.74 0.14 1.91 0.13 1.720270 0.189731 0.485424 0.482590

    20 3.63 0.29 2.61 0.24 2.243020 0.366985 0.938925 0.941311

    21 4.29 0.28 1.57 0.15 2.630670 1.060670 2.713707 2.89686022 2.64 0.25 1.52 0.25 1.661530 0.141533 0.362110 0.35978723 2.64 0.22 1.70 0.16 1.661530 0.038467 0.098417 0.097696

    24 2.74 0.10 1.62 0.22 1.720270 0.100269 0.256537 0.25470825 1.83 0.25 1.45 0.12 1.185770 0.264225 0.676015 0.677586

    26 1.04 0.17 1.04 0.05 0.721764 0.318236 0.814202 0.829071

    27 2.28 0.46 1.45 0.20 1.450080 0.000085 0.000217 0.00021628 1.58 0.35 1.22 0.08 1.038940 0.181064 0.463249 0.465120

    29 1.55 0.31 1.20 0.10 1.021320 0.178685 0.457163 0.459210

    30 1.73 0.54 1.37 0.18 1.127040 0.242961 0.621612 0.623550

    31 5.67 0.33 3.51 0.22 3.441220 0.068779 0.175971 0.183568

    32 4.67 0.20 3.76 0.24 2.853870 0.906135 2.318332 2.453100

    33 5.05 0.09 3.61 0.34 3.077060 0.532940 1.363518 1.414910

    34 3.91 0.37 2.16 0.32 2.407470 0.247475 0.633161 0.63438435 4.17 0.67 2.69 0.28 2.560190 0.129813 0.332124 0.333268

    36 2.92 0.64 1.75 0.24 1.825990 0.075993 0.194426 0.19298437 2.64 0.16 0.79 0.17 1.661530 0.871533 2.229803 2.30173038 1.93 0.27 1.25 0.23 1.244510 0.005490 0.014045 0.014011

    39 1.70 0.45 0.97 0.24 1.109420 0.139419 0.356701 0.35724940 2.08 0.29 1.12 0.33 1.332610 0.212614 0.543969 0.54303441 1.93 0.28 0.74 0.12 1.244510 0.504510 1.290781 1.30442042 2.90 0.40 1.30 0.15 1.814250 0.514245 1.315687 1.32301043 3.35 0.47 1.83 0.25 2.078560 0.248555 0.635924 0.63385444 1.40 0.31 0.69 0.13 0.933212 0.243212 0.622254 0.62753545 2.13 0.37 1.37 0.12 1.361980 0.008018 0.020515 0.020424

    46 2.26 0.34 1.37 0.36 1.438340 0.068338 0.174841 0.17392147 1.42 0.39 0.64 0.08 0.944959 0.304959 0.780233 0.78793548 3.00 0.53 1.83 0.23 1.872980 0.042981 0.109966 0.10913949 1.52 0.07 0.79 0.17 1.003690 0.213695 0.546735 0.54983950 3.33 0.22 1.57 0.20 2.066810 0.496808 1.271075 1.27868051 2.36 0.14 1.19 0.13 1.497070 0.307073 0.785641 0.78448652 2.67 0.34 1.37 0.26 1.679150 0.309154 0.790965 0.78879653 3.48 0.21 1.32 0.14 2.154910 0.834912 2.136109 2.20226054 3.23 0.14 2.06 0.09 2.008070 0.051927 0.132855 0.131952

    55 2.97 0.13 1.81 0.13 1.855360 0.045360 0.116054 0.11517756 3.71 0.10 2.03 0.09 2.290000 0.260004 0.665216 0.66517557 3.38 0.14 1.83 0.10 2.096180 0.266176 0.681007 0.67922158 2.87 0.10 1.93 0.22 1.796620 0.133375 0.341238 0.338905

    T.N. Michalakopoulos et al. / International Journal of Rock Mechanics & Mining Sciences 43 (2006) 321327324

  • ARTICLE IN PRESS

    ed CA

    f RocTable 4 (continued )

    Sample no. Observed CAI40 Observed CAI55 Predict

    Mean Std deviation

    of the mean

    Mean Std deviation

    of the mean

    T.N. Michalakopoulos et al. / International Journal osome ambiguities regarding the recommended steel stylihardness.In this paper the inuence of steel styli hardness on

    the CAI value has been investigated. Sixty-eight samplesof various rock types have been tested with steel styli ofboth HRC 55 and 40. The relation of the two CAI

    59 2.92 0.11 1.42 0.18 1.825990

    60 3.15 0.16 1.91 0.21 1.961080

    61 2.57 0.11 1.58 0.09 1.620420

    62 2.85 0.17 1.73 0.15 1.784880

    63 2.89 0.21 1.86 0.10 1.808370

    64 3.12 0.15 1.86 0.15 1.943460

    65 3.13 0.12 2.39 0.18 1.949340

    66 3.20 0.26 1.91 0.18 1.990450

    67 1.93 0.36 0.91 0.07 1.244510

    68 4.67 0.11 2.62 0.20 2.853870

    Table 5

    Absolute frequency of the observed CAI values

    Value range CAI55 CAI40

    0.300.50 0 0

    0.501.00 8 1

    1.002.00 41 15

    2.004.00 19 42

    4.006.00 0 9

    46.00 0 1

    0

    10

    20

    30

    40

    50

    0.3-0.5 0.5-1.0 1.0-2.0 2.0-4.0 4.0-6.0 >6.0CAI value

    Abs

    olut

    e fre

    quen

    cy

    CAI40CAI55

    Fig. 2. Distribution of observed CAI values.I55 Observed residuals Standardized residuals Studentized

    deleted residuals

    k Mechanics & Mining Sciences 43 (2006) 321327 325values has been examined and a linear correlation wasobserved. The yielded equation can be used to convertCAI40 values to CAI55, which are required by the formaldescription of the test.

    0.405993 1.038727 1.0392600.051084 0.130698 0.1297690.040418 0.103409 0.1026740.054878 0.140403 0.1393410.051628 0.132090 0.131088

    0.083464 0.213541 0.2120470.440663 1.127429 1.130130

    0.080452 0.205835 0.2044490.334510 0.855838 0.8586100.233865 0.598340 0.607421

    0.00

    0.50

    1.00

    1.50

    2.00

    2.50

    3.00

    3.50

    4.00

    0.00 0.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00Predicted CAI55

    Obs

    erve

    d CA

    I 55

    Fig. 4. Plot of predicted versus observed CAI55 values.

    0.00

    1.00

    2.00

    3.00

    4.00

    5.00

    0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00

    CAI40

    CAI 5

    5

    Fig. 3. Plot of CAI40 versus CAI55 values.

  • ARTICLE IN PRESS

    Table 6

    Regression analysis

    Linear model: y a bxDependent variable (y): CAI55Independent variable (x): Observed CAI40Data sets: 68

    Parameter Estimate Standard error t statistic p value

    Intercept (a) 0.110914 0.132092 0.839671 0.4041

    Slope (b) 0.587356 0.042938 13.6791 0.0000

    Table 7

    Analysis of variance

    Source Sum of

    squares

    Degrees of

    freedom

    Mean

    square

    F ratio p value

    Model 29.0188 1 29.0188 187.12 0.0000

    Residual 10.2355 66 0.155084

    Total 39.2543 67

    Correlation coefcient 0.859797R2 73:9251%Standard error of estimate 0.393807

    -4.00

    -2.00

    0.00

    2.00

    4.00

    0.00 0.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00Predicted CAI55

    Stud

    entiz

    ed d

    elet

    ed re

    sidua

    ls

    Fig. 5. Plot of predicted CAI55 versus studentized deleted residuals

    values.

    0.00

    0.25

    0.50

    0.75

    1.00

    -3.00 -2.00 -1.00 0.00 1.00 2.00 3.00Standardized residual value

    Cum

    ulat

    ive

    prob

    abili

    ty

    Standardized residualsStandard normal distribution

    Fig. 6. Standardized residuals normality test.

    T.N. Michalakopoulos et al. / International Journal of Rock Mechanics & Mining Sciences 43 (2006) 321327326References

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    Cerchar abrasiveness index (CAI) classication

    Classication CAI55 CAI40a

    Very low abrasiveness 0.300.50 0.320.66

    Low abrasiveness 0.501.00 0.661.51

    Medium abrasiveness 1.002.00 1.513.22

    High abrasiveness 2.004.00 3.226.62

    Extreme abrasiveness 4.006.00 6.6210.03

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    ARTICLE IN PRESST.N. Michalakopoulos et al. / International Journal of Rock Mechanics & Mining Sciences 43 (2006) 321327 327

    The influence of steel styli hardness on the Cerchar abrasiveness index valueIntroductionTesting procedureSteel styli specificationsTest setup and resultsRegression analysisConclusionsReferences