Revised Phase II Environmental Investigation
Transcript of Revised Phase II Environmental Investigation
Prepared by:
BUREAU VERITAS NORTH AMERICA, INC. Health, Safety, and Environmental Services
841 Bishop Street, Suite 1100 Honolulu, Hawaii 96813
(808) 531-6708 www.us.bureauveritas.com
Revised Phase II Environmental Investigation
1025 Waimanu Street(TMK Number: [1] 2-3-003: Parcel 040)
Honolulu, Oahu, Hawaii
May 29, 2014
Project No. 17012-012090.00
Prepared for:
URBAN WORKS, INC.831 Pohukaina Street, Suite E-1
Honolulu, Hawaii 96813
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CONTENTS Section Page List of Acronyms ........................................................................................................................................ iv Executive Summary .................................................................................................................................... v
1.0 INTRODUCTION, BACKGROUND, AND PURPOSE ....................................................................... 1 1.1 BACKGROUND ................................................................................................................................... 1 1.2 PURPOSE ........................................................................................................................................... 1
2.0 SITE DESCRIPTION ........................................................................................................................... 2 2.1 PHYSICAL SETTING .......................................................................................................................... 2 2.1.1 Soils/Geology ................................................................................................................................... 2 2.1.2 Groundwater .................................................................................................................................... 2 2.1.3 Surface water ................................................................................................................................... 3 2.2 HISTORICAL LAND USE .................................................................................................................... 3 2.3 CURRENT LAND USE ........................................................................................................................ 4
3.0 APPLICABLE ACTION LEVELS ....................................................................................................... 4
4.0 DESCRIPTION OF FIELD ACTIVITIES ............................................................................................. 4 4.1 UTILITY SURVEY ............................................................................................................................... 4 4.2 SOIL SAMPLING ................................................................................................................................. 5 4.2.1 Soil Sample Collection Procedure ................................................................................................... 5 4.2.2 Soil Sample Collection and Observations ........................................................................................ 6 4.2.3 Sub-Sampling for Laboratory Analysis ............................................................................................ 7 4.3 GROUNDWATER SAMPLING ............................................................................................................ 7 4.4 CHAIN-OF-CUSTODY ........................................................................................................................ 8 4.5 DECONTAMINATION PROCEDURES............................................................................................... 8 4.6 SITE RESTORATION ......................................................................................................................... 9
5.0 LABORATORY ANALYTICAL RESULTS ......................................................................................... 9 5.1 SOIL ANALYTICAL RESULTS ........................................................................................................... 9 5.2 GROUNDWATER ANALYTICAL RESULTS .................................................................................... 11 5.3 LABORATORY QUALITY CONTROL ............................................................................................... 12
6.0 SUMMARY AND CONCLUSIONS ................................................................................................... 13
7.0 RECOMMENDATIONS ..................................................................................................................... 14
8.0 LIMITATIONS ................................................................................................................................... 14 References Figures
1 Site Location Map 2 Site Vicinity Map
CONTENTS (Continued)
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3 Borehole Sample Location 4 Concentrations Exceeding Tier 1 EALs (Based on Screening-Level Investigation) Tables
1 Summary of Preliminary Soil Analytical Results from Shallow Decision Unit and Boreholes MW-1 and MW-2
2 Summary of Preliminary Soil Analytical Results from Borehole MW-3 and MW-4 3 Summary of Preliminary Groundwater Analytical Results from Wells MW-1 and MW-2 4 Summary of Preliminary Groundwater Analytical Results from Wells MW-3 and MW-4 Appendices
A Borehole Logs B Groundwater Sampling Logs C Analytical Laboratory Report and Chain-of-Custody Forms
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List of Acronyms bgs Below ground surface Bureau Veritas Bureau Veritas North America, Inc. C-EHMP Construction Environmental Hazard Management Plan DPP Department of Planning and Permitting DU Decision unit EAL Environmental Action Level EHE Environmental Hazard Evaluation EPA Environmental Protection Agency ESA Environmental Site Assessment GPR Ground penetrating radar HDOH State OF Hawaii Department of Health HEER Office Office of Hazard Evaluation and Emergency Response LCS Laboratory control sample LCSD Laboratory control sample duplicate mg/kg Milligram per kilogram mg/L Milligram per liter MS Matrix spike MSD Matrix spike duplicate PAH Polynuclear aromatic hydrocarbons ppmv Parts per million by volume PID Photoionization Detector REC Recognized environmental condition RSL Regional Screening Level TMK Tax Map Key TGM Technical Guidance Manual TPH Total petroleum hydrocarbons TPH-DRO Total petroleum hydrocarbons as diesel range organics TPH-GRO Total petroleum hydrocarbons as gasoline range organics TPH-RRO Total petroleum hydrocarbons as residual range organics µg/L Micrograms per liter UIC Underground Injection Control USGS United States Geological Survey VOC Volatile organic compound
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Executive Summary Urban Works, Inc. retained Bureau Veritas North America, Inc. (Bureau Veritas) to conduct a Phase II Environmental Investigation of the Artspace project site located at 1025 Waimanu Street (Tax Map Key [TMK] Number: [1] 2-3-003: Parcel 040), Honolulu, Oahu, Hawaii (hereafter referred to as the “site”). The site consists of a 30,000 square foot rectangular parcel of land that is located within the “Kakaako Commercial Development District.” The purpose of the Phase II environmental assessment was to assess the presence or absence of impacts from historical releases that may have occurred on or around the site. On July 10, 2012, a direct push drilling rig was used to (1) advance 16 boreholes for the collection of shallow multi-increment soil samples, and (2) advance four boreholes for the collection of multi-increment soil samples and groundwater grab samples (from temporary monitoring wells set within the four boreholes). Two decision units (DU) were established on the site to investigate the shallow soils for impacts related to the on-site contractor storage yard. The area of each DU measured approximately 15,000 square feet in size. One of DU areas was established on the northwestern half of the site and the soil sample was designated as sample number UW MI-1. A second DU area was established on the southeastern half of the site and a soil sample was designated as sample number UW MI-2. Samples UW MI-1 and UW MI-2 were multi-increment soil samples that were collected from the 0.5 to 3.0 feet below ground surface (bgs) interval from eight shallow boreholes collected from within each of the established DU areas. No staining or odors were observed within any of soils retrieved two DU areas. Two boreholes with temporary groundwater monitoring wells (MW-1 and MW-2) were positioned along the northwest side of the site to assess potential impacts from the former off-site auto body and paint area. Two boreholes with temporary groundwater monitoring wells (MW-3 and MW-4) were positioned along the southeast of the site to assess potential impacts from the former off-site chemical and fertilizer warehouse and off-site dry cleaning facility. No staining or odors were observed within any of the soil boreholes. Six multi-increment soil samples were collected from select soil intervals within the four boreholes. Temporary well casings were installed in the four soil boreholes to facilitate the collection of a groundwater grab sample from each borehole. Boreholes BH-1, BH-2, BH-3, and BH-4 were converted to groundwater monitoring wells MW-1, MW-2, MW-3, and MW-4, respectively. The soil and groundwater data were compared to the State of Hawaii Department of Health (HDOH) unrestricted Tier 1 Environmental Action Levels (EAL) for sites where groundwater is not a current or potential drinking water resource and a surface water body is not located within 150 meters of the site. Multi-Increment Samples - Shallow Soils in DU1 and DU2 Soil samples UW MI-1 and UW MI-2 were multi-increment samples from the shallow soils of the two DUs established at the site (i.e., 0.5 to 3.0 feet bgs). The analyte, total petroleum hydrocarbons as residual range organics (TPH-RRO), was detected at concentrations of 490 milligrams per kilogram (mg/kg) and 610 mg/kg. The TPH-RRO concentration of 610 mg/kg detected in soil sample UW MI-2 (i.e., southeastern side of site) exceeded the HDOH Tier 1 EAL of 500 mg/kg for TPH-RRO which is based on gross contamination hazards (nuisance concerns) at residential sites (HDOH, 2012). The United States Environmental Protection Agency (EPA) has not established a Regional Screening Level (RSL) for TPH-RRO (EPA, 2012).
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Total petroleum hydrocarbons as diesel range organics (TPH-DRO), total lead, and several polynuclear aromatic hydrocarbons (PAH) analytes were detected; however, the concentrations were below the applicable HDOH Tier 1 EALs. Concentrations of total petroleum hydrocarbons as gasoline range organics (TPH -GRO), total cadmium and volatile organic compounds (VOC) were not detected at concentrations above the laboratory reporting limits in either of the samples. The source of the TPH-RRO impacted soil identified in soil sample UW MI-2, which was collected from the southeastern side of site at a depth of 0.5 to 3.0 feet bgs, is potentially the result of shallow soil impacts related to the former on-site contractor storage yard or possibly resulting from fill material that was brought in from the adjacent Pacifica Honolulu Condominium property. Boreholes BH-1 and BH-2 (Soil and Groundwater) Four multi-increment soil samples collected from select soil intervals (i.e., UW BH1 1’, UW BH1 6’, UW BH2 1’, and UW BH2 7’) were collected from boreholes BH-1 and BH-2, which were positioned along the northwest side of the site to assess potential impacts from the former off-site auto body and paint area. TPH-RRO was detected at concentrations ranging from not detectable up to 1,900 mg/kg. Only the TPH-RRO concentration of 1,900 mg/kg, which was detected in soil sample UW BH1-1’, exceeded the HDOH Tier 1 EAL of 500 mg/kg for TPH-RRO. The HDOH Tier 1 EAL for TPH-RRO is based on gross contamination hazards (nuisance concerns) at residential sites (HDOH, 2012). The EPA has not established a RSL for TPH-RRO (EPA, 2012). TPH-DRO, total lead, and several PAH analytes were detected; however, the concentrations were below the applicable HDOH Tier 1 EALs. Concentrations of TPH-GRO, total cadmium, and VOCs were not detected at concentrations above the laboratory reporting limits in the samples. Boreholes BH-1 and BH-2 were converted to temporary groundwater monitoring wells MW-1 and MW-2, respectively. Two groundwater grab samples (i.e., UW MW-1 and UW MW-2) were collected from these two temporary monitoring wells. TPH-RRO was detected at a concentration of 1,400 micrograms per liter (µg/L) in groundwater sample UW MW-1, which was below the HDOH Tier 1 EAL of 2,500 µg/L for TPH-RRO. Concentrations of TPH-GRO, TPH-DRO, total cadmium, total lead, and VOCs were not detected at concentrations above the laboratory reporting limit in either of the samples. Two of the PAH analytes were reported at concentrations that exceeded the HDOH Tier 1 EALs in sample UW MW-1. The PAH analyte indeno[1,2,3-cd]pyrene was detected at a concentration of 0.38 µg/L, which exceeds the HDOH Tier 1 EAL of 0.095 µg/L. The PAH analyte benzo[g,h,i]perylene was detected at a concentration of 0.34 µg/L, which exceeds the HDOH Tier 1 EAL of 0.13 µg/L. The HDOH Tier 1 EALs for both indeno[1,2,3-cd]pyrene and benzo[g,h,i]perylene are based on gross contamination hazards (nuisance concerns: HDOH, 2012). The EPA has not established RSLs for contaminants in groundwater and, therefore, RSLs for indeno[1,2,3-cd]pyrene and benzo(g,h,i)perylene in groundwater are unavailable for comparison. The EPA has established a RSL for indeno[1,2,3-cd]pyrene for tap water of 0.029 µg/L (EPA, 2012), which the indeno[1,2,3-cd]pyrene concentration of 0.38 µg/L in groundwater at MW-1 exceeds; however, the groundwater beneath the site is not a source of drinking water. The source of the TPH-RRO impacted soil identified in borehole BH-1 at a depth of 0.5 to 2.5 feet bgs and the PAH impacted groundwater discovered in temporary well MW-1 is likely the result of off-site impacts associated with the former auto body and paint shop that was present on the adjacent property from at least 1962 through 1977.
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Boreholes BH-3 and BH-4 (Soil and Groundwater) Two multi-increment soil samples collected from selected soil intervals (i.e., UW BH3 7’ and UW BH4 6’) were collected from boreholes BH-3 and BH-4, which were positioned along the southeast of the site to assess potential impacts from the former off-site chemical and fertilizer warehouse and off-site dry cleaning facility. TPH-RRO, TPH-DRO, several PAH analytes, and two of the organochlorine pesticide analytes were detected; however, the concentrations were below the applicable HDOH unrestricted Tier 1 EALs, or the HDOH has not established a Tier 1 EAL. Concentrations of total arsenic, VOCs, and pesticide screen analytes were not detected in either of the samples at levels of that exceeded the laboratory reporting limits. Boreholes BH-3 and BH-4 were converted to temporary groundwater monitoring wells MW-3 and MW-4, respectively. Two groundwater grab samples (i.e., UW MW-3 and UW MW-4) were collected from these two temporary monitoring wells. TPH-RRO was reported at concentrations of not detectable and 980 µg/L; however, these concentrations were below the HDOH Tier 1 EAL of 2,500 µg/L for TPH-RRO. Concentrations of TPH-DRO, total arsenic, PAHs, VOCs, organochlorine pesticide analytes, and pesticide screen analytes were not detected at concentrations above the laboratory reporting limits in either of the samples. In summary, the investigation has identified the following:
TPH-RRO impacted soil, having a concentration of 610 mg/kg, was identified in the shallow soils (i.e. 0.5 to 3.0 feet bgs) at the DU located on the southeastern half of the site.
TPH-RRO impacted soil, having a concentration of 1,900 mg/kg, was identified in a shallow soil sample (i.e. 0.5 to 2.5 feet bgs collected from BH-1/MW-1).
The PAH analytes indeno[1,2,3-cd]pyrene and benzo[g,h,i]perylene were detected at concentrations that exceed the HDOH Tier 1 EALs in the groundwater sample collected from well MW-1.
TPH-RRO concentrations in soil and indeno[1,2,3-cd]pyrene and benzo(g,h,i)perylene concentrations in groundwater exceed their respective HDOH Tier 1 EALs. However, the soil and groundwater concentrations of these three analytes do not exceed the EPA Region 9 RSLs. The EPA has not established a RSL in soil for TPH-RRO nor has it established any RSLs for contaminants in groundwater. It should be noted these conclusions are based on preliminary samples, not a full site characterization. Phase II samples were collected to determine presence or absence and did not fully characterize or delineate the contamination at the site. Bureau Veritas recommends the following:
1. Conduct an Environmental Hazard Evaluation (EHE) to evaluate potential environmental hazards associated with the identified soil and groundwater impacts, including the potential use of the unrestricted Tier 1 EALs for sites located less than 150 meters of surface water (i.e., to evaluate the potential for groundwater and storm drain water comingling).
2. Prepare a Construction Environmental Hazard Management Plan (C-EHMP) to guide the
handling and management of the impacted soil and groundwater during future construction activities.
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1.0 INTRODUCTION, BACKGROUND, AND PURPOSE Urban Works, Inc. retained Bureau Veritas North America, Inc. (Bureau Veritas) to conduct a Phase II Environmental Investigation of the Artspace project site (Tax Map Key [TMK] Number: [1] 2-3-003: Parcel 040), located at 1025 Waimanu Street, Honolulu, Oahu, Hawaii (hereafter referred to as the “site”). A Site Location Map showing the general location of the site is presented on Figure 1. 1.1 BACKGROUND Bureau Veritas previously prepared a Phase I Environmental Site Assessment (ESA) at the site for Hawaii Community Development Program. The Phase I ESA identified one Recognized Environmental Condition (REC) that was related to historical use of the site, which was located on the site, and a potential REC related to potential impacts from historical uses at an adjacent and nearby properties in the vicinity of the site (Bureau Veritas, 2010). The Phase I ESA revealed the following evidence of RECs, as defined by ASTM, in connection with the site:
Historical research indicated that the site was previously used as a contractor’s storage yard from at least 1955 until 2008. The storage yard was unpaved and aerial photographs indicated heavy equipment was stored on site. Historical usage as a contractor’s storage yard indicates the potential use and storage of petroleum products and other hazardous materials. Additionally, vicinity properties identified in fire insurance maps included a drycleaner, chemical and fertilizer warehouse, and auto body and paint shop. These types of facilities are typically associated with the storage and/or usage of hazardous chemicals and materials, with the potential for releases of such materials.
These findings were considered a REC because the site and vicinity properties indicate previous storage and potential usage of hazardous materials, chemicals, and/or petroleum products. Therefore, Bureau Veritas recommended conducting a subsurface investigation to assess the presence or absence of impacts from potential releases associated with these findings. 1.2 PURPOSE The purpose of the Phase II environmental assessment was to assess the presence or absence of impacts from historical releases that may have occurred on or around the site. This Phase II investigation consisted of the following primary activities:
Two multi-incremental soil samples were collected from the shallow soils of the two Decision Units (DUs) defined at the site to assess potential impacts from the former on-site contractor storage yard.
Two boreholes positioned along the northwest of the site to assess potential impacts from the former off-site auto body and paint area. Multi-increment soil samples were collected from select soil intervals. Groundwater grab samples were collected from the temporary groundwater monitoring wells (MW-1 and MW-2) established in the boreholes.
Two boreholes positioned along the southeast of the site to assess potential impacts from the former off-site chemical and fertilizer warehouse and off-site dry cleaning facility. Multi-increment soil samples were collected from select soil intervals. Groundwater grab samples were collected from the temporary groundwater monitoring wells (MW-3 and MW-4) established in the boreholes.
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2.0 SITE DESCRIPTION The site consists of a 30,000 square foot rectangular parcel of land located at 1025 Waimanu Street, in Honolulu, Oahu, Hawaii, in an industrial business district (Figures 1 and 2, Figures Tab). The site is further described as the parcel of land designated as TMK Number: (1) 2-3-003: Parcel 040. According to the City and County of Honolulu Department of Planning and Permitting (DPP), the site is located within the “Kakaako Commercial Development District”. 2.1 PHYSICAL SETTING The site lies in the western portion of the Honolulu Plain physiographic division, on the central southern coast of the island of Oahu. The approximate latitude and longitude of the site are 21° 17’ 45.86”N and 157° 51’ 06.12” W, respectively. According to the United States Geological Survey (USGS) 7.5-Minute Honolulu, Oahu, Topographic Quadrangle Map (1998), the elevation at the site is between 5 and 10 feet above mean sea level. The general topography of the site and surrounding region slopes down to the south, toward Kewalo Basin and the Pacific Ocean. 2.1.1 Soils/Geology According to the United States Department of Agriculture’s (USDA) report entitled “Soil Survey of Islands of Kauai, Oahu, Maui, Molokai, and Lanai” (Foote, D.E. et. al., 1972) the soil type beneath the site is classified as Fill Land soil. Fill Land soil (mapping unit F) consists of material dredged from the ocean or hauled from nearby areas, garbage, and general material from other sources. This land type is used for developments including airports, housing areas, and industrial facilities. During drilling and sampling activities conducted at the site, the soil encountered immediately beneath the surface consisted of silty clay with varying percentages of basalt and coral gravel clasts, and coral and coral sand. Beneath the silty clay, near the groundwater table a one to two foot thick layer of grey saturated silty clay was observed. Groundwater was present at a depth of approximately 6.5 to 7.5 feet below ground surface (bgs). A hard coral shelf was encountered at approximately one to two feet below the water table. 2.1.2 Groundwater Bureau Veritas reviewed the Aquifer Identification and Classification for Oahu: Groundwater Protection Strategy for Hawaii, Technical Report No. 179, (Mink, J.F. and Lau, L.S. 1990), published by the Water Resources Research Center at the University of Hawaii, for information on groundwater conditions below the site. The report describes two aquifers below the site as part of the Nuuanu aquifer system of the Honolulu sector on the island of Oahu. The upper aquifer is an unconfined basal aquifer of the sedimentary type, occurring in nonvolcanic lithology. The status is described as a replaceable, moderate salinity water supply, not used for drinking water or of ecological importance, which has a potential for use. This aquifer has a high vulnerability to contamination. The lower aquifer is a confined basal aquifer of the flank type, occurring in horizontally extensive lavas. Its status is described as an irreplaceable, fresh drinking water supply that is currently in use. This aquifer has a low vulnerability to contamination.
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The site is located below the State of Hawaii Department of Health (HDOH) defined Underground Injection Control (UIC) line. Areas above the UIC line denote potential underground drinking water aquifers. Areas below the UIC line generally denote groundwater that is unsuitable for drinking water purposes. Consequently, the groundwater below the site is considered non-drinking water. The regional groundwater flow direction is inferred to the southwest toward the Pacific Ocean, based on the surface topography. However, topography is not always a reliable basis for predicting groundwater flow direction. The local gradient and flow direction under the site may be influenced naturally by tidal fluctuations, zones of higher or lower permeability, or artificially by nearby pumping or recharge, and may deviate from the regional trend. According to the 1983 U.S. Department of the Interior Geological Survey 7.5 Minute Topographic Map of the Honolulu Quadrangle with the Hawaii Department of Land and Natural Resources Division of Water and Land Development Underground Injection Well Overlay, no drinking water wells or other commercial or municipal wells lie with ¼ mile of the site. (USGS, 1983). Groundwater at the site is located at a depth of approximately 6.5 to 7.5 feet bgs. It is unknown if groundwater is infiltrating into the City and County of Honolulu storm drain system. 2.1.3 Surface water The nearest surface water body is the Kewalo Basin harbor, approximately 1,500 feet to the southwest of the site. The Kewalo Basin is connected to the Pacific Ocean near Honolulu Harbor. The storm water runoff from the site flows via sheet flow both northeast towards Waimanu Street and southwest towards Kawaiahao Street. The storm water then discharges into the City and County of Honolulu storm drain system. 2.2 HISTORICAL LAND USE According to the Bureau Veritas Phase I ESA report (Bureau Veritas 2010), Sanborn Fire Insurance maps indicated the site was previously used as a contractor’s storage yard from at least 1955 until 2008. The contractor storage yard was unpaved and aerial photographs indicated heavy equipment was stored on site. Historical usage as a contractor’s storage yard indicates the potential use and storage of petroleum products and other hazardous materials. From 2008 to the present, the site has been a paved parking lot. Reportedly, prior to paving in 2008, fill material was brought onto the site to increase the slope of site and help control surface runoff. The fill material was reportedly brought in from the adjacent Pacifica Condominium site, which is located across Waimanu Street (TMK [1] 2-3-003: Parcel 105). The fill material appears to have been used to increase the grade in the central portion of the site (in the northwest to southeast direction). The site slopes downward from the central area toward Waimanu Street on the northeast and toward Kawaiahao Street on the southwest. It should be noted that the fill material is believed to have been brought onto the site, prior to paving in 2008, when the site was owned by Evershine X. Hawaii Community Development Authority purchased the property on or about May 20, 2010 according to the City and County of Honolulu DPP’s website.
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The Sanborn Fire Insurance maps also indicate the indicated the following historical uses on several nearby properties:
The property (TMK [1] 2-3-003: Parcel 043) located adjacent and northwest of the site was labeled as auto body and paint facility and also showed a paint booth on the 1962, 1972 and 1977 maps.
The property (TMK [1] 2-3-003: Parcel 037) located southeast of the site was labeled in the 1962 map as a chemical and fertilizer warehouse.
The property (TMK [1] 2-3-003: Parcel 059) located south-southeast of the site was labeled Honolulu Laundry and had a dry cleaning facility in the 1955, 1962, 1972, 1977, and 1986 maps. The 1991 and 1993 maps did not show the presence of the laundry, although the dry cleaning facility remained.
2.3 CURRENT LAND USE The site is currently owned by Hawaii Community Development Authority and is currently paved with asphalt demarcated with parking spaces. The site is enclosed by a chain-link fence and gates, and is currently used for public parking. The site is the proposed, future location of a residential condominium building with first floor retail space. Specifically, the site is the proposed, future location of a nine level mixed use property that will include commercial, residential, parking, and community use areas. This mixed-use development project is intended to serve the broader Hawaiian Community by developing a traditional Hawaiian Cultural Center with classroom space, space for teaching and performing Hula, music, and other traditional practices, as well as 72 units of affordable multi-ethnic artist housing for Hawaiian artists and their families. 3.0 APPLICABLE ACTION LEVELS The analytical results were compared to the HDOH Tier 1 Environmental Action Levels (EAL) that are presented in the Evaluation of Environmental Hazards at Sites with Contaminated Soil and Groundwater (HDOH, 2012). The Tier 1 EALs are published by the HDOH’s Office of Hazard Evaluation and Emergency Response (HEER Office). The EALs used in this report are the unrestricted Tier 1 EALs where groundwater is not a current or potential source of drinking water and the nearest surface water body is greater than 150 meters from the site (HDOH, 2012). It is unknown if the groundwater at the site, located at approximately 6.5 to 7.5 feet bgs, is infiltrating into the City and County of Honolulu storm drain system. If the groundwater is connected to the storm drain system, it may be appropriate to compare to the unrestricted Tier 1 EALs where groundwater is not a current or potential source of drinking water and the nearest surface water body is less than 150 meters from the site. Bureau Veritas recommends evaluating the use of these Tier 1 EALs within the Environmental Hazard Evaluation (EHE). 4.0 DESCRIPTION OF FIELD ACTIVITIES 4.1 UTILITY SURVEY On July 10, 2012, a utility survey was conducted to assess the potential presence of subsurface structures such as water, sewer, or electrical lines. A utility survey, consisting of magnetic toning and a ground penetrating radar (GPR) survey, was conducted in the area of the proposed borehole locations.
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The utility survey operator marked the ground surface with paint in the vicinity of detected utilities or subsurface anomalies. 4.2 SOIL SAMPLING On July 10, 2012, a direct push drilling rig was used to (1) advance boreholes for the collection of shallow multi-increment soil samples, and (2) advance the four boreholes that were converted to temporary monitoring wells. To investigate the historical unpaved contractor storage yard, Bureau Veritas followed guidance issued by the State of Hawaii Department of Health (HDOH) that recommends the use of multi-increment sampling techniques to sample large areas, or decision units. The HDOH defines the term decision unit (DU) as "a well-defined area of a site where a decision is to be made regarding the extent and magnitude of contaminants identified within the unit, as well as the potential environmental hazards posed by the contaminants." Two DU areas were established on the site to investigate the shallow soils for impacts related to the on-site contractor storage yard. The areas of the two DUs are shown on Figure 3 and each measure approximately 15,000 square feet in size. The first DU area was established on the northwestern half of the site and the soil sample was designated as sample number UW MI-1. A second DU area was established on the southeastern half of the site and a soil sample was designated as sample number UW MI-2. Sixteen boreholes were advanced into the shallow subsurface (eight in each DU) to collect multi-increment samples from the 0.5 to 3.0 feet bgs depth interval. Two multi-increment soil samples, UW MI-1 and UW MI-2, were collected from the two DUs (each representing the eight boreholes drilled in each DU). The location of the boreholes and MI samples are shown on Figure 3. No staining or odors were observed within any of soils retrieved two DU areas. Two boreholes with temporary groundwater monitoring wells (MW-1 and MW-2) were positioned along the northwest side of the site to assess potential impacts from the former off-site auto body and paint area. Two boreholes with temporary groundwater monitoring wells (MW-3 and MW-4) were positioned along the southeast of the site to assess potential impacts from the former off-site chemical and fertilizer warehouse and off-site dry cleaning facility. The locations of temporary wells MW-1, MW-2, MW-3 and MW-4 are shown on Figure 3. No staining or odors were observed within any of the soil boreholes. Six multi-increment soil samples were collected from select soil intervals within the boreholes. Four multi-increment soil samples were collected from MW-1 and MW-2. Two multi-increment soil samples were collected from MW-3 and MW-4. 4.2.1 Soil Sample Collection Procedure A total of eight soil samples were collected. Six of the eight soil samples were multi-increment samples collected from select soil intervals within the four boreholes (i.e., boreholes BH-1 through BH-4). Two of the eight soil samples were multi-increment samples collected from the shallow soils of the site by collecting soil increments from 16 shallow boreholes (i.e., eight shallow boreholes in each of the two DUs). Each of the eight soil samples was given a unique sample identification number. The soil samples were collected using a 4 feet long open-barrel sampler, with an outside diameter of 2 inches. The open-barrel sampler was fitted with a disposable acrylic liner. The open-barrel samplers were advanced into the subsurface by the direct push sampling rig. After retrieval of the acrylic lined open-barrel sampler, soil samples for laboratory analyses were collected using multi-increment sampling techniques.
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For the six multi-increment soil samples collected from the four boreholes, soil increments were collected from specific 2-foot soil intervals. The soil increments for volatile analyses [i.e., total petroleum hydrocarbons as gasoline range organics (TPH-GRO) and volatile organic compounds (VOCs)] were collected from the 2-foot soil core first by collecting ten 5-gram subsamples with disposable Lock N’ Load™ syringes and placed in a pre-weighed glass jar containing methanol preservative. The soil increments for non-volatile analyses [i.e., total petroleum hydrocarbons as diesel range organics (TPH-DRO), total petroleum hydrocarbons as residual range organics (TPH-RRO), polynuclear aromatic hydrocarbons (PAH), pesticides, and total metals] were collected next by collecting 30 soil increments from the remaining 2-foot soil core. However, because the remaining soil was nearly the volume of 30 soil increments, the entire remaining 2-foot soil core was collected as the sample and placed in a self-sealing plastic bag. For the two multi-increment shallow soil samples collected from eight shallow boreholes in each DU, soil increments were collected and combined from the target soil interval (i.e., 0.5 to 3 feet bgs). The soil increments for volatile analyses were collected by collecting five 5-gram subsamples with disposable Lock N’Load TM syringes from each of the eight shallow boreholes in each DU and placing the subsamples in a pre-weighted glass jar containing methanol preservative. A total of 40 5-gram subsamples were collected and combined for the sample to be analyzed for volatiles (i.e., five subsamples from each of the eight boreholes within each DU). The remainders of eight soil cores were combined to form the sample for non-volatiles. The sampling equipment was cleaned between each of the collection of samples from each of the deeper boreholes and between surface soil sampling areas. The equipment cleaning process involved brushing or scraping off excess soil particles, washing in a non-phosphate detergent solution, and rinsing with steam distilled water. Once collected, the samples were labeled (including sample identification, and date/time of sample collection) and immediately placed in a cooler containing frozen gel ice for transport to the analytical laboratory. Following the collection of soil samples, a small portion of soil from each sample was subjected to field analysis using a photoionization detector (PID). The field analysis consisted of placing a small portion of soil from the sample into a self-sealing plastic bag and sealed. The vapor within the bag was allowed to equilibrate for a minimum of five minutes prior to inserting the tip of the PID probe into the side of the plastic bag. Following soil sample collection, the soil from the soil borehole was described and classified by the field geologist using the Unified Soil Classification System. The soil descriptions are presented on the borehole logs in Appendix A. 4.2.2 Soil Sample Collection and Observations The table below provides a summary of sample collection information including the depth of sample collection and the PID reading recorded.
Summary of Soil Sample Collection Information
Borehole or DU Area
Sample Number
Depth of Sample (feet bgs)
PID Reading (ppmv)
Comment
MW-1 UW BH1-1’ 0.5 to 2.5 0.0 No staining or odors UW BH1-6’ 5 to 7 0.0 No staining or odors
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Borehole or DU Area
Sample Number
Depth of Sample (feet bgs)
PID Reading (ppmv)
Comment
MW-2 UW BH2-1’ 0.5 to 2.5 0.0 No staining or odors UW BH2-7’ 6.5 to 8.5 0.0 No staining or odors
MW-3 UW BH3-7’ 6 to 8 0.0 No staining or odors MW-4 UW BH4-6’ 5 to 7 0.0 No staining or odors
NW Side of Site UW MI-1 0.5 to 3.0 0.0 No staining or odors SE Side of Site UW MI-2 0.5 to 3.0 0.0 No staining or odors
Notes: bgs: Below ground surface ppmv: Parts per million by volume NW Northwest SE Southeast
4.2.3 Sub-Sampling for Laboratory Analysis A sub-sampling technique was used by the analytical laboratory to reduce the bulk sample collected in the field through multi-increment approaches to a laboratory analysis quantity, the analytical sample. The entire bulk sample was dried and then passed through a 2-millimeter (mm) (No. 10) sieve to remove larger debris. The portion that passes through the sieve was referred to as the “total soil sample”. The total soil sample was spread out on a clean flat surface, by slowly pouring the sample out and then spreading it to a thin (about ¼ inch) even layer. The spread-out soil was incrementally sampled using a stratified-random pattern by collecting approximately 30 small increments to make up a 10-gram sample for analysis (e.g. approximately 30 increments of approximately 0.333 grams). The 10-gram sub-sample was then analyzed. 4.3 GROUNDWATER SAMPLING Temporary well casings were installed in the four boreholes to facilitate the collection of a groundwater sample from each borehole. Boreholes BH-1, BH-2, BH-3, and BH-4 were converted to groundwater monitoring wells MW-1, MW-2, MW-3, and MW-4, respectively. A sand filter pack was installed around the PVC casing from approximately 3 feet bgs to the bottom of the borehole. The depth to groundwater was measured in each well before sampling to calculate the height of the water column and casing volume. Groundwater purging and sampling was performed using a low-flow sampling technique (EPA, 1996). This technique uses a peristaltic pump with new polyethylene tubing, dedicated to each well, to purge the wells and to collect groundwater samples. To purge the well and collect the groundwater sample, the intake end of the tubing was positioned near the bottom of the screened interval. The flow rate was limited to approximately 0.5 liters per minute, or less, during purging and sampling, to minimize drawdown. The well was purged until at least three casing volumes were removed and/or the water quality parameters (turbidity, temperature, pH, and electrical conductivity) were monitored until the water reached equilibrium. Field parameters were measured and recorded on a field groundwater sampling log at regular intervals during the purge process. The groundwater sampling log is included in this report in Appendix B.
Project No. 17012-012090.00 8
Upon completion of purging, groundwater samples for TPH-DRO, TPH-RRO, PAH and pesticides analyses were collected by pumping groundwater into 1-liter amber glass containers with Teflon™ lined caps. Samples for the metals (i.e., arsenic, cadmium, or lead) analyses were collected by pumping the groundwater through a 0.45 micron inline filter into preserved 500-milliliter polyethylene bottles. Samples for volatile constituents [i.e., TPH-GRO and VOCs] were collected from the well using a dedicated disposable polyethylene bailer and transferring the sample into 40-milliliter glass sample containers containing a hydrochloric acid preservative, and sealed with no headspace. The groundwater samples were collected from temporary monitoring wells on the same day as they were developed. As such, the groundwater samples were considered grab samples.
Summary of Groundwater Sample Collection Information
Borehole or DU Area
Sample Number
Depth to Water (feet bgs):
Total Well Depth (feet bgs)
Comment
MW-1 UW MW-1 6.35 9.65 No odor or sheen MW-2 UW MW-2 7.42 11.50 No odor or sheen MW-3 UW MW-3 7.18 11.44 No odor or sheen MW-4 UW MW-4 6.00 10.86 No odor or sheen
Note: bgs: Below ground surface
4.4 CHAIN-OF-CUSTODY Each sample was logged on a chain-of-custody form upon collection. The chain-of-custody form listed the project name, project manager, sampler, the designated laboratory, addresses and telephone numbers, the sample identification, number of containers per sample, sampling date and time, and the required analyses. The chain-of-custody forms accompanied the samples from the field to the laboratory. Whenever the samples changed hands, the custodian of the samples signed the “relinquished by” section and the receiving person signed the “received by” section. The soil and groundwater samples were delivered by hand under standard chain-of-custody procedures to TestAmerica Analytical Laboratory, located in Honolulu, Hawaii. 4.5 DECONTAMINATION PROCEDURES Drilling equipment in contact with subsurface soil in each borehole was washed in a non-phosphate detergent and water solution and triple rinsed with tap water between drilling at each borehole location. New disposable gloves were worn by the sampler during the soil sample collection activities. The gloves were disposed of following the collection of a soil sample and new gloves were donned prior to the collection or handling of the following soil sample. Equipment used for groundwater sampling at each monitoring well was dedicated and disposable to prevent cross contamination between monitoring points. The dedicated, disposable sampling equipment included the peristaltic pump tubing and in-line filters. New disposable gloves were worn by the sampler during the groundwater sample collection activities. The gloves were disposed of following the collection of a groundwater sample and new gloves were donned prior to the collection of the following groundwater sample.
Project No. 17012-012090.00 9
4.6 SITE RESTORATION Following the collection of the soil and groundwater samples, the temporary monitoring well casings were removed from the boreholes, and the boreholes were abandoned. The remaining soil not collected as part of the laboratory sample was returned to the borehole. The remaining open space in the borehole was filled with bentonite granules to approximately 0.5 feet bgs. The remainder of the borehole was filled with concrete containing black dye to generally match the original asphalt parking lot surface. 5.0 LABORATORY ANALYTICAL RESULTS A total of eight multi-increment soil samples and four groundwater grab samples were collected and submitted to TestAmerica Analytical laboratory located in Honolulu, Hawaii for analysis. The soil and groundwater analytical results were compared to the unrestricted Tier 1 EALs for sites where groundwater is not a current or potential drinking water resource and a surface water body is not located within 150 meters of the site. Copies of the Analytical Laboratory Report and Chain of Custody Documentation are presented in Appendix C. Figure 4 presents a summary of results which shows the contaminants that were identified at concentrations exceeding the HDOH Tier 1 EALs. 5.1 SOIL ANALYTICAL RESULTS The soil samples were selectively analyzed for the constituents as listed in the table below:
Analytical Testing of Soil Samples
Sample Number
TPH-GRO
TPH-DRO
TPH-RRO
VOC PAH Total Pb&Cd
Total As
Organ. Pest.
Pest. Screen
UW MI-1 UW MI-2
UW BH1 1’ UW BH1 6’ UW BH2 1’ UW BH2 7’ UW BH3 7’ UW BH4 6’
Notes: TPH-GRO Total petroleum hydrocarbons as gasoline range organics (TPH-GRO) using
Environmental Protection Agency (EPA) Method 8015 Modified TPH-DRO Total petroleum hydrocarbons as diesel range organics (TPH-DRO) using EPA Method
8015 Modified TPH-RRO Total petroleum hydrocarbons as residual range organics (TPH-RRO) using EPA Method
8015 Modified VOC Volatile organic compounds (VOCs) using EPA Method 8260B PAH Polynuclear aromatic hydrocarbons (PAHs) using EPA Method 8270SIM Total Pb&Cd Total metals cadmium and lead using EPA Method 6010 Total As Total metals arsenic using EPA Method 6010 Organ. Pest. Organochlorine pesticides using EPA Method 8081 Pest. Screen Modified pesticide screen using EPA Method 8270
Project No. 17012-012090.00 10
Table 1, located behind the Tables tab, presents a summary of the analytical results for the following eight soil samples: UW MI-1, UW MI-2, UW BH1 1’, UW BH1 6’, UW BH2 1’, and UW BH2 7’. Table 2 presents a summary of the analytical results for the following two soil samples: UW BH3 7’ and UW BH4 6’. Multi-Increment Samples - Shallow Soils in DU1 and DU2 Soil samples UW MI-1 and UW MI-2 were multi-increment samples from the shallow soils of the two DUs established at the site (i.e., 0.5 to 3.0 feet bgs). TPH-RRO was detected at concentrations of 490 mg/kg and 610 mg/kg. The TPH-RRO concentration of 610 mg/kg detected in soil sample UW MI-2 (i.e., southeastern side of site) exceeded the HDOH Tier 1 EAL of 500 mg/kg for TPH-RRO, which is based on gross contamination hazards (nuisance concerns) at residential sites (HDOH, 2012). The United States Environmental Protection Agency (EPA) has not established a Regional Screening Level (RSL) for TPH-RRO (EPA, 2012). TPH-DRO was detected at concentrations of 57 mg/kg and 85 mg/kg; however, these concentrations are below the HDOH Tier 1 EAL of 500 mg/kg for TPH-DRO. Total lead was detected at concentrations of 93 mg/kg and 130 mg/kg; however, these concentrations are below the HDOH Tier 1 EAL of 200 mg/kg for total lead. The majority of the PAH analytes were reported at detectable concentrations; however, these concentrations were below the HDOH Tier 1 EALs. Concentrations of TPH-GRO, total cadmium and VOCs were not detected at concentrations above the laboratory reporting limits in either of the samples. The source of the TPH-RRO impacted soil identified in soil sample UW MI-2, which was collected from the southeastern side of site at a depth of 0.5 to 3.0 feet bgs is potentially the result of shallow soil impacts related to the former on-site contractor storage yard or possibly resulting from fill material that was brought in from the adjacent Pacifica Honolulu Condominium property. Boreholes BH-1 and BH-2 Two boreholes (i.e., boreholes BH-1 and BH-2) were positioned along the northwest side of the site to assess potential impacts from the former off-site auto body and paint area. Four multi-increment soil samples (i.e., UW BH1 1’, UW BH1 6’, UW BH2 1’, and UW BH2 7) were collected from select depth intervals within these two boreholes. TPH-RRO was reported at concentrations ranging from not detectable up to 1,900 mg/kg. Only the TPH-RRO concentration of 1,900 mg/kg, which was detected in soil sample UW BH1-1’ (i.e., from BH-1 on the northwest side of site), exceeded the HDOH Tier 1 EAL of 500 mg/kg for TPH-RRO. The HDOH Tier 1 EAL for TPH-RRO is based on gross contamination hazards (nuisance concerns) at residential sites (HDOH, 2012). The EPA has not established a RSL for TPH-RRO (EPA, 2012). TPH-DRO was detected at concentrations ranging from not detectable up to 160 mg/kg; however, these concentrations are below the HDOH Tier 1 EAL of 500 mg/kg for TPH-DRO. Total lead was detected at concentrations ranging from not detectable up to 79 mg/kg; however, these concentrations are below the HDOH Tier 1 EAL of 200 mg/kg for total lead. The majority of the PAH analytes were reported at detectable concentrations in the two shallow soils samples (samples UW BH1 1’ and UW BH2 1’); however, these concentrations were below the HDOH Tier 1 EALs. Only three of the PAH analytes were reported at detectable concentrations in samples UW BH1 6’ and UW BH2 6’, which are the two deeper soil samples; however, these concentrations were below the HDOH Tier 1 EALs. Concentrations of TPH-GRO, total cadmium, and VOCs were not detected at concentrations above the laboratory reporting limits in either of the samples.
Project No. 17012-012090.00 11
The source of the TPH-RRO impacted soil identified in borehole BH-1 at a depth of 0.5 to 2.5 feet is likely the result of off-site impacts associated with the former auto body and paint shop that was present on the adjacent property from at least 1962 through 1977 or from the imported fill material. Boreholes BH-3 and BH-4 Two boreholes (i.e., boreholes BH-3 and BH-4) were positioned along the southeast of the site to assess potential impacts from the former off-site chemical and fertilizer warehouse and off-site dry cleaning facility. Two multi-increment soil samples (i.e., UW BH3 7’ and UW BH4 6’) were collected from these two boreholes. TPH-RRO was reported at concentrations of not detectable and 11 mg/kg; however, these concentrations are below the HDOH Tier 1 EAL of 500 mg/kg for TPH-RRO. TPH-DRO was detected at concentrations of not detectable and 86 mg/kg; however, these concentrations are below the HDOH Tier 1 EAL of 500 mg/kg for TPH-DRO. Many of the PAH analytes were reported at concentrations below the laboratory reporting limits. A number of the PAH analytes were present at detectable concentrations; however, these concentrations were below the respective HDOH Tier 1 EALs. Two of the 21 organochlorine pesticide analytes (i.e., alpha-Chlordane and gamma-Chlordane) were reported at detectable concentrations in sample UW BH3 7’; however, the HDOH has not established a Tier 1 EAL for these analytes. None of the organochlorine pesticide analytes were reported in sample UW BH4 6’ at detectable concentrations. Concentrations of total arsenic, VOCs, and pesticide screen analytes were not detected in either of the samples at levels that exceeded the laboratory reporting limits. 5.2 GROUNDWATER ANALYTICAL RESULTS Boreholes BH-1, BH-2, BH-3, and BH-4 were converted to temporary groundwater monitoring wells MW-1, MW-2, MW-3, and MW-4, respectively. The groundwater grab samples from each well were selectively analyzed for the constituents as listed in the table below:
Analytical Testing of Groundwater Samples
Sample Number
TPH-GRO
TPH-DRO
TPH-RRO
VOC PAH Total Pb&Cd
Total As
Organ. Pest.
Pest. Screen
UW MW-1 UW MW-2 UW MW-3 UW MW-4
Notes: TPH-GRO 8260B Total Petroleum Hydrocarbons (TPH) as Gasoline Range Organics (GRO) using
Environmental Protection Agency (EPA) Method 8260B TPH-DRO 8015M TPH as Diesel Range Organics (DRO) using EPA Method 8015 Modified TPH-RRO 8015M TPH as Residual Range Organics (RRO) using EPA Method 8015 Modified VOC 8260B Volatile Organic Compounds (VOCs) using EPA Method 8260B PAH 8270 SIM Polynuclear Aromatic Hydrocarbons (PAHs) using EPA Method 8270SIM Total Pb&Cd 6010 Total metals cadmium and lead using EPA Method 6010 Total As 6010 Total metals arsenic using EPA Method 6010 Organ. Pest. 8081 Organochlorine pesticides using EPA Method 8081 Pest. Screen 8081 Modified pesticide screen using EPA Method 8270
Table 3 present a summary of the analytical results for groundwater samples UW MW-1 and UW MW-2. The summary of the analytical results for groundwater samples UW MW-3 and UW MW-4 are present in Table 4.
Project No. 17012-012090.00 12
Wells MW-1 and MW-2 Boreholes BH-1 and BH-2 were converted to temporary groundwater monitoring wells MW-1 and MW-2, respectively. These two wells were positioned along the northwest side of the site to assess potential impacts from the former off-site auto body and paint area. Two groundwater grab samples (i.e., UW MW-1 and UW MW-2) were collected from these two temporary monitoring wells. TPH-RRO was reported at concentrations of not detectable and 1,400 micrograms per liter (µg/L); however, these concentrations were below the HDOH Tier 1 EAL of 2,500 µg/L for TPH-RRO. The majority of the PAH analytes were reported at detectable concentrations in the groundwater sample UW MW-1; however, these concentrations were below the HDOH Tier 1 EALs except for two of the PAH analytes. Indeno[1,2,3-cd]pyrene was detected at a concentration of 0.38 µg/L, which exceeds the HDOH Tier 1 EAL of 0.095 µg/L for indeno[1,2,3-cd]pyrene. Benzo[g,h,i]perylene was detected at a concentration of 0.34 µg/L, which exceeds the HDOH Tier 1 EAL of 0.13 µg/L for benzo[g,h,i]perylene. The HDOH Tier 1 EALs for both indeno[1,2,3-cd]pyrene and benzo[g,h,i]perylene are based on gross contamination hazards (nuisance concerns: HDOH, 2012). The EPA has not established RSLs for contaminants in groundwater and, therefore, RSLs for indeno[1,2,3-cd]pyrene and benzo(g,h,i)perylene in groundwater are unavailable for comparison. The EPA has established a RSL for indeno[1,2,3-cd]pyrene for tap water of 0.029 µg/L (EPA, 2012), which the indeno[1,2,3-cd]pyrene concentration of 0.38 µg/L in groundwater at MW-1 exceeds; however, the groundwater beneath the site is not a source of drinking water. Concentrations of PAHs were not detected at concentrations above the laboratory reporting limit in groundwater sample UW MW-2. Concentrations of TPH-GRO, TPH-DRO, total cadmium, total lead, and VOCs were not detected at concentrations above the laboratory reporting limit in either of the samples. The source of the PAH impacted groundwater discovered in temporary well MW-1 is likely the result of off-site impacts associated with the former auto body and paint shop that was present on the adjacent property. Wells MW-3 and MW-4 Boreholes BH-3 and BH-4 were converted to temporary groundwater monitoring wells MW-3 and MW-4, respectively. These two wells were positioned along the southeast of the site to assess potential impacts from the former off-site chemical and fertilizer warehouse and the off-site dry cleaning facility. Two groundwater grab samples (i.e., UW MW-3 and UW MW-4) were collected from these two temporary monitoring wells. TPH-RRO was reported at concentrations of not detectable and 980 µg/L; however, these concentrations were below the HDOH Tier 1 EAL of 2,500 µg/L for TPH-RRO. Concentrations of TPH-DRO, total arsenic, PAHs, VOCs, organochlorine pesticide analytes, and pesticide screen analytes were not detected at concentrations above the laboratory reporting limit in either of the samples. 5.3 LABORATORY QUALITY CONTROL The laboratory report indicated that the reported results were within the laboratory’s quality control/quality assurance criteria and that no data qualifier flags were reported except for the following. For the four groundwater grab samples, the laboratory control sample (LCS) and/or the laboratory control sample duplicate (LCSD) for the batch recovered low for the following analytes: naphthalene,
Project No. 17012-012090.00 13
benzo(b)fluoranthene, benzo(k)fluoranthene and fluorene. Re-extraction and/or re-analysis were performed outside of holding time with acceptable results. Both sets of data have been reported in the laboratory report. The Pesticide Screen analysis for the groundwater grab samples UW MW-3 and UW MW-4 was performed outside of holding time. It should be noted that Pesticide Screen analysis conducted on the soils samples from these locations reported no detectable concentrations in either of the soil samples at levels of that exceeded the laboratory reporting limit. Therefore resampling and analysis of the groundwater is not recommended. For one of the soil samples, UW BH 1 1’, not enough multi-increment sample was available to perform the matrix spike/matrix spike duplicate (MS/MSD) for the organic prep method (EPA Method 3550b). The TPH-DRO, TPH-RRO, and the PAH results have the potential to be affected. However, the LCS/LCSD results were used as proxy values and the laboratory reported the results. Overall, the laboratory results are deemed acceptable for the intended purposes of this investigation. 6.0 SUMMARY AND CONCLUSIONS On July 10, 2012, a direct push drilling rig was used to (1) advance 16 boreholes for the collection of shallow multi-increment soil samples, and (2) advance four boreholes for the collection of multi-increment soil samples and groundwater grab samples (from temporary monitoring wells set within the four boreholes). This Phase II investigation consisted of the following primary activities:
Two multi-incremental soil samples were collected from the shallow soils of the two DUs defined at the site to assess potential impacts from the former on-site contractor storage yard.
Two boreholes positioned along the northwest of the site to assess potential impacts from the former off-site auto body and paint area. Multi-increment soil samples were collected from select soil intervals. Groundwater grab samples were collected from the temporary groundwater monitoring wells (MW-1 and MW-2) established in the boreholes.
Two boreholes positioned along the southeast of the site to assess potential impacts from the former off-site chemical and fertilizer warehouse and off-site dry cleaning facility. Multi-increment soil samples were collected from select soil intervals. Groundwater grab samples were collected from the temporary groundwater monitoring wells (MW-3 and MW-4) established in the boreholes.
The soil and groundwater results were compared to the unrestricted Tier 1 EALs for sites where groundwater is not a current or potential drinking water resource and a surface water body is not located within 150 meters of the site. In summary, the investigation has identified the following issues:
TPH-RRO impacted soil, having a concentration of 610 mg/kg, was identified in the shallow soils (i.e. 0.5 to 3.0 feet bgs) at the Decision Unit located on the southeastern half of the site.
TPH-RRO impacted soil, having a concentration of 1,900 mg/kg, was identified in a shallow soil sample (i.e. 0.5 to 2.5 feet bgs collected from BH-1/MW-1.
The PAH analytes indeno[1,2,3-cd]pyrene and benzo[g,h,i]perylene were detected at concentrations that exceed the HDOH Tier 1 EALs in the groundwater sample collected from well MW-1.
Project No. 17012-012090.00 14
TPH-RRO concentrations in soil and indeno[1,2,3-cd]pyrene and benzo(g,h,i)perylene concentrations in groundwater exceed their respective HDOH Tier 1 EALs. However, the soil and groundwater concentrations of these three analytes do not exceed the EPA Region 9 RSLs. The EPA has not established a RSL in soil for TPH-RRO nor has it established any RSLs for contaminants in groundwater. It should be noted these conclusions are based on preliminary samples, not a full site characterization. Phase II samples were collected to determine presence or absence and did not fully characterize or delineate the contamination at the site. 7.0 RECOMMENDATIONS Bureau Veritas recommends the following:
1. Conduct an Environmental Hazard Evaluation (EHE) to evaluate potential environmental hazards associated with the identified soil and groundwater impacts, including the potential use of the unrestricted Tier 1 EALs for sites located less than 150 meters of surface water (i.e., to evaluate the potential for groundwater and storm drain water comingling).
2. Prepare a Construction Environmental Hazard Management Plan (C-EHMP) to guide the
handling and management of the impacted soil and groundwater during future construction activities.
8.0 LIMITATIONS This report is for the exclusive use of Urban Works, Inc. and no other party shall have any right to rely on any service provided by Bureau Veritas without prior written consent. The information and opinions expressed in this report are given in response to a limited assignment and should be considered and implemented only in light of that assignment. The services provided by Bureau Veritas in completing this project were consistent with normal standards of the profession. No other warranty, expressed or implied, is made. Bureau Veritas will not distribute or publish this report without consent except as required by law or court order. This report prepared by: John P. Rau, P.G. Senior Geologist/Manager Health, Safety, and Environmental Services This report reviewed by: Daniel P. Ford, P.G Regional Vice President Health, Safety, and Environmental Services
REFERENCES
Project No. 17012-012090.00
REFERENCES Bureau Veritas North America, Inc. (Bureau Veritas), 2010. Phase I Environmental Site Assessment of the Property Located at 1025 Waimanu Street (Tax Map Key [TMK] Number: [1] 2-3-003: Parcel 040), Honolulu, Oahu, Hawaii. Prepared for Hawaii Community Development Authority. Bureau Veritas Project No. 17009-009188.00 February 15. Hawaii State Department of Health (HDOH), 2011. Evaluation of Environmental Hazards at Sites with Contaminated Soil and Groundwater, Volumes I and II. Prepared by the Hazard Evaluation & Emergency Response Office. Fall 2011. (Updated February 2012). Foote, D.E., et al., 1972. United States Department of Agriculture Soil Conservation Service in cooperation with the University of Hawaii Agricultural Experiment Station. Soil Survey of the Islands of Kauai, Oahu, Maui, Molokai, and Lanai, State of Hawaii. Hawaii State Department of Health (HDOH), 2012. Evaluation of Environmental Hazards at Sites with Contaminated Soil and Groundwater, Volumes I and II, prepared by the Hazard Evaluation & Emergency Response (HEER) Office. Fall 2011 (Revised January 2012). HDOH, 2009b. Technical Guidance Manual for the Implementation of the Hawaii State Contingency Plan (Interim Final), prepared by the HEER Office. June 21. Hawaii State Department of Land and Natural Resources (HDLNR), 2006. Ground Water Index and Summary. Prepared by the Division of Water Resource Management. Mink, J.F. and L.S. Lau, 1990. Aquifer Identification and Classification for Oahu: Groundwater Protection Strategy for Hawaii. Technical Report No. 179. Honolulu: Water Resources Research Center, University of Hawaii at Manoa. United States Environmental Protection Agency (EPA), 1996. Low-Flow (Minimal Drawdown) Ground-Water Sampling Procedures. Prepared by Office of Solid Waste and Emergency Response. EPA 540/S-95/540. April. United States Environmental Protection Agency (EPA), 2012. Regional Screening Levels, Region 9 (Pacific Southwest). Available on line at http://www.epa.gov/region9/superfund/prg/. April. United States Department of the Interior Geological Survey (USGS). 1998. 7.5 Minute Topographic Map, Honolulu Quadrangle. United States Department of the Interior Geological Survey (USGS). 1983. 7.5 Minute Topographic Map, Honolulu Quadrangle with Hawaii Department of Land and Natural Resources, Division of Water and Land Development Underground Injection Well Overlay (1983). University of Hawaii (UH), 1983. Atlas of Hawaii (Second Edition). UH Department of Geography, University of Hawaii Press, Honolulu, Hawaii.
FIGURES
TABLES
Sample ID: HDOH Depth (feet bgs): Tier 1
Portion of the site: EALAnalyte Unit: (mg/kg)Total Petroleum Hydrocarbon (TPH) / EPA Method 8260BTPH-GRO ND< 17 ND< 16 ND< 2.1 ND< 1.6 ND< 5.2 ND< 6.1 100Total Petroleum Hydrocarbon / EPA Method 8015-ModifiedTPH-DRO ND< 8.2 ND< 8.4 500TPH-RRO ND< 17 500Total metals/EPA Method 6010Cadmium ND< 0.95 ND< 0.98 ND< 0.99 ND< 1.0 ND< 0.98 ND< 1.0 14Lead ND< 2.9 ND< 3.1 200Polynuclear Aromatic Hydrocarbons (PAHs) / EPA Method 8270SIMNaphthalene ND< 0.0016 ND< 0.0017 ND< 0.0018 4.52-Methylnaphthalene ND< 0.0016 ND< 0.0017 ND< 0.0018 ND< 0.0017 281-Methylnaphthalene ND< 0.0016 ND< 0.0017 ND< 0.0018 ND< 0.0017 26Acenaphthylene ND< 0.0016 ND< 0.0018 130Acenaphthene ND< 0.0016 ND< 0.0017 ND< 0.0018 120Fluorene ND< 0.0016 ND< 0.0016 ND< 0.0017 ND< 0.0018 100Phenanthrene ND< 0.0016 ND< 0.0018 440Anthracene ND< 0.0016 ND< 0.0018 4.3Fluoranthene ND< 0.0016 ND< 0.0018 460Pyrene ND< 0.0016 ND< 0.0018 44Benzo[a]anthracene ND< 0.0016 ND< 0.0018 1.5Chrysene ND< 0.0016 ND< 0.0018 30Benzo[b]fluoranthene 1.5Benzo[k]fluoranthene ND< 0.0016 ND< 0.0018 15Notes on page 4
Urban Works Phase II InvestigationSummary of Soil Analytical Results
Table 1
Sampling Date: July 10, 2012Project No. 17012-012090.00
1025 Waimanu Street, Honolulu, Oahu, Hawaii
UW MI-1
(mg/kg)
6 to 8UW BH 2 7'
Site Surface0.5 to 3.0UW MI-2
(mg/kg)
5 to 7UW BH 1 6'
(mg/kg)
0.5 to 2.5UW BH 1 1'
Northwest Side of Site(mg/kg)
0.5 to 2.5
(mg/kg)
0.0077
0.590.38
0.0068
(mg/kg)
0.220.11
0.011
UW BH 2 1'
0.12
0.5 to 3.0
0.0390.11
57490
93
0.003
0.00660.042
0.0046
0.140.440.430.380.720.46
0.0049
26
0.0036
380
0.120.150.11
0.004
0.0018
0.026
0.290.30.3
0.0038
42
0.0037
85610*
130
0.050.12
0.150.12
0.054 0.0370.13
1601,900*
79
0.260.15
0.0210.039
0.0020.0059
23
0.0019
0.00180.00170.0022
Page 1 of 4
Sample ID: HDOH Depth (feet bgs): Tier 1
Portion of the site: EALAnalyte Unit: (mg/kg)PAHs / EPA Method 8270SIM (continued)Benzo[a]pyrene ND< 0.0016 ND< 0.0018 0.15Indeno[1,2,3-cd]pyrene ND< 0.0016 1.5Dibenz[a,h]anthracene ND< 0.0016 ND< 0.0018 0.15Benzo[g,h,i]perylene ND< 0.0018 35Volatile Organic Compounds (VOCs) / EPA Method 5035/8260BDichlorodifluoromethane ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 NSChloromethane ND< 1.7 ND< 1.6 ND< 0.21 ND< 0.16 ND< 0.52 ND< 0.61 0.29Vinyl chloride ND< 0.034 ND< 0.033 ND< 0.0043 ND< 0.0033 ND< 0.01 ND< 0.012 0.072Bromomethane ND< 0.59 ND< 0.57 ND< 0.075 ND< 0.058 ND< 0.18 ND< 0.21 0.22Chloroethane ND< 1.7 ND< 1.6 ND< 0.21 ND< 0.16 ND< 0.52 ND< 0.61 11Trichlorofluoromethane ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 NS1,1-Dichloroethene ND< 0.085 ND< 0.081 ND< 0.011 ND< 0.0082 ND< 0.026 ND< 0.031 8.90Methylene Chloride ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 1.10trans-1,2-Dichloroethene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 2.71,1-Dichloroethane ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 0.330002,2-Dichloropropane ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 NScis-1,2-Dichloroethene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 0.31Chlorobromomethane ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 NSChloroform ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 0.0231,1,1-Trichloroethane ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 220Carbon tetrachloride ND< 0.085 ND< 0.081 ND< 0.011 ND< 0.0082 ND< 0.026 ND< 0.031 0.0871,1-Dichloropropene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 NSBenzene ND< 0.068 ND< 0.065 ND< 0.0086 ND< 0.0066 ND< 0.021 ND< 0.024 0.671,2-Dichloroethane ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 0.02Trichloroethene ND< 0.068 ND< 0.065 ND< 0.0086 ND< 0.0066 ND< 0.021 ND< 0.024 0.261,2-Dichloropropane ND< 0.051 ND< 0.049 ND< 0.0064 ND< 0.0049 ND< 0.016 ND< 0.018 0.052Dibromomethane ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 NSNotes on page 4
0.120.0360.140.22
Site Surface
0.310.053
0.20.017
0.002 0.0580.016
Northwest Side of Site0.5 to 2.5 5 to 7 0.5 to 2.5
(mg/kg) (mg/kg) (mg/kg)
0.0710.097 0.088
0.0022
Table 1 (continued)
UW BH 1 1' UW BH 1 6' UW BH 2 1'6 to 8
UW BH 2 7' UW MI-1 UW MI-20.5 to 3.0 0.5 to 3.0
0.210.0470.21
(mg/kg) (mg/kg) (mg/kg)
Page 2 of 4
Sample ID: HDOH Depth (feet bgs): Tier 1
Portion of the site: EALAnalyte Unit: (mg/kg)VOCs / EPA Method 5035/8260B (continued)Dichlorobromomethane ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 NScis-1,3-Dichloropropene ND< 0.068 ND< 0.065 ND< 0.0086 ND< 0.0066 ND< 0.021 ND< 0.024 NSToluene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 32trans-1,3-Dichloropropene ND< 0.068 ND< 0.065 ND< 0.0086 ND< 0.0066 ND< 0.021 ND< 0.024 NS1,1,2-Trichloroethane ND< 0.051 ND< 0.049 ND< 0.0064 ND< 0.0049 ND< 0.016 ND< 0.018 0.0089Tetrachloroethene ND< 0.085 ND< 0.081 ND< 0.011 ND< 0.0082 ND< 0.026 ND< 0.031 0.0881,3-Dichloropropane ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 NSChlorodibromomethane ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 NSEthylene Dibromide ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 NSChlorobenzene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 2.2Ethylbenzene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 211,1,1,2-Tetrachloroethane ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 1.901,1,2,2-Tetrachloroethane ND< 0.042 ND< 0.041 ND< 0.0054 ND< 0.0041 ND< 0.013 ND< 0.015 0.009m-Xylene & p-Xylene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 45o-Xylene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 45Styrene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 2.9Bromoform ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 44Isopropylbenzene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 NSBromobenzene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 NSN-Propylbenzene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 NS1,2,3-Trichloropropane ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 0.00132-Chlorotoluene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 NS1,3,5-Trimethylbenzene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 NS4-Chlorotoluene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 NStert-Butylbenzene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 NS1,2,4-Trimethylbenzene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 NSsec-Butylbenzene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 NS1,3-Dichlorobenzene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 42Notes on page 4
0.5 to 2.5 5 to 7 0.5 to 2.5UW MI-2
(mg/kg)
Table 1 (continued)
UW BH 1 1' UW BH 1 6' UW BH 2 1' UW BH 2 7' UW MI-1
(mg/kg)
6 to 8 0.5 to 3.0 0.5 to 3.0Northwest Side of Site Site Surface
(mg/kg) (mg/kg) (mg/kg) (mg/kg)
Page 3 of 4
Sample ID: HDOH Depth (feet bgs): Tier 1
Portion of the site: EALAnalyte Unit: (mg/kg)Volatile Organic Compounds (VOCs) / EPA Method 5035/8260B (continued)4-Isopropyltoluene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 NS1,4-Dichlorobenzene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 0.047n-Butylbenzene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 NS1,2-Dichlorobenzene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 7.51,2-Dibromo-3-Chloropropane ND< 0.85 ND< 0.81 ND< 0.11 ND< 0.082 ND< 0.26 ND< 0.31 0.00091,2,4-Trichlorobenzene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 0.0981,2,3-Trichlorobenzene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 NSHexachlorobutadiene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 2.2Naphthalene ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 4.5Methyl tert-butyl ether ND< 0.17 ND< 0.16 ND< 0.021 ND< 0.016 ND< 0.052 ND< 0.061 2.0Notes:bgs Below ground surface.HDOH Tier 1 EAL
italic Analytes laboratory Reporting Limit (RL) is greater than the HDOH Tier 1 EAL.mg/kg Milligrams per kilogram.ND< Analyte not detected. The value after the '<' is the laboratory Method Reporting Limit (MRL).NS No standard is currently established by the HDOH for this analyte.TPH-DRO Total Petroleum Hydrocarbon as Diesel Range Organics.TPH-GRO Total Petroleum Hydrocarbon as Gasoline Range Organics.TPH-RRO Total Petroleum Hydrocarbon as Residual Range Organics.* Concentration greater than or equal to the HDOH Tier 1 EAL.
State of Hawaii Department of Health (HDOH) Tier 1 Environmental Action Levels (EAL) at sites where groundwater is NOT a current or potential drinking water resource and a surface water body is NOT located within 150 meters of the site (HDOH, 2012).
Table 1 (continued)
(mg/kg)
0.5 to 3.0UW MI-2
(mg/kg)
0.5 to 3.0UW MI-1
Site Surface(mg/kg)
UW BH 2 7'
Northwest Side of Site
UW BH 1 1'
(mg/kg)
0.5 to 2.5UW BH 2 1'
(mg/kg)
0.5 to 2.5
(mg/kg)
6 to 8UW BH 1 6'
5 to 7
Page 4 of 4
Sample ID: HDOH Depth (feet bgs): Tier 1
Portion of the site: EALAnalyte Unit: (mg/kg)Total Petroleum Hydrocarbon / EPA Method 8015-ModifiedTPH-DRO ND< 8.3 500TPH-RRO ND< 17 500Total metals/EPA Method 6010Arsenic ND< 5.9 ND< 6.0 24Polynuclear Aromatic Hydrocarbons (PAHs) / EPA Method 8270SIMNaphthalene ND< 0.0016 ND< 0.0017 4.52-Methylnaphthalene ND< 0.0016 ND< 0.0017 281-Methylnaphthalene ND< 0.0016 ND< 0.0017 26Acenaphthylene ND< 0.0016 ND< 0.0017 130Acenaphthene ND< 0.0016 ND< 0.0017 120Fluorene ND< 0.0016 ND< 0.0017 100Phenanthrene ND< 0.0016 440Anthracene ND< 0.0016 ND< 0.0017 4.3Fluoranthene ND< 0.0016 460Pyrene ND< 0.0016 44Benzo[a]anthracene ND< 0.0016 1.5Chrysene ND< 0.0016 30Benzo[b]fluoranthene ND< 0.0016 1.5Benzo[k]fluoranthene ND< 0.0016 ND< 0.0017 15Benzo[a]pyrene ND< 0.0016 0.15Indeno[1,2,3-cd]pyrene 1.5Dibenz[a,h]anthracene ND< 0.0016 ND< 0.0017 0.15Benzo[g,h,i]perylene ND< 0.0016 35Volatile Organic Compounds (VOCs) / EPA Method 5035/8260BDichlorodifluoromethane ND< 0.015 ND< 0.013 NSChloromethane ND< 0.15 ND< 0.13 0.29Vinyl chloride ND< 0.0029 ND< 0.0026 0.072Bromomethane ND< 0.051 ND< 0.046 0.22Chloroethane ND< 0.15 ND< 0.13 11Trichlorofluoromethane ND< 0.015 ND< 0.013 NS1,1-Dichloroethene ND< 0.0073 ND< 0.0066 8.90Methylene Chloride ND< 0.015 ND< 0.013 1.10trans-1,2-Dichloroethene ND< 0.015 ND< 0.013 2.71,1-Dichloroethane ND< 0.015 ND< 0.013 0.330002,2-Dichloropropane ND< 0.015 ND< 0.013 NSNotes on page 5
Summary of Soil Analytical Results
5 to 7Southeast side of Site
(mg/kg)
1025 Waimanu Street, Honolulu, Oahu, Hawaii
(mg/kg)
Urban Works Phase II Investigation
Project No. 17012-012090.00
0.0068
0.0068
1186
Table 2
0.0019
UW BH 3 7'6 to 8
UW BH 4 6'
0.00510.0041
Sampling Date: July 10, 2012
0.0063
0.0039
0.0057
0.00730.0024
1 of 5
Sample ID: HDOH Depth (feet bgs): Tier 1
Portion of the site: EALAnalyte Unit: (mg/kg)VOCs / EPA Method 5035/8260B (continued)cis-1,2-Dichloroethene ND< 0.015 ND< 0.013 0.31Chlorobromomethane ND< 0.015 ND< 0.013 NSChloroform ND< 0.015 ND< 0.013 0.0231,1,1-Trichloroethane ND< 0.015 ND< 0.013 220Carbon tetrachloride ND< 0.0073 ND< 0.0066 0.0871,1-Dichloropropene ND< 0.015 ND< 0.013 NSBenzene ND< 0.0058 ND< 0.0053 0.671,2-Dichloroethane ND< 0.015 ND< 0.013 0.02Trichloroethene ND< 0.0058 ND< 0.0053 0.261,2-Dichloropropane ND< 0.0044 ND< 0.0039 0.052Dibromomethane ND< 0.015 ND< 0.013 NSDichlorobromomethane ND< 0.015 ND< 0.013 NScis-1,3-Dichloropropene ND< 0.0058 ND< 0.0053 NSToluene ND< 0.015 ND< 0.013 32trans-1,3-Dichloropropene ND< 0.0058 ND< 0.0053 NS1,1,2-Trichloroethane ND< 0.0044 ND< 0.0039 0.0089Tetrachloroethene ND< 0.0073 ND< 0.0066 0.0881,3-Dichloropropane ND< 0.015 ND< 0.013 NSChlorodibromomethane ND< 0.015 ND< 0.013 NSEthylene Dibromide ND< 0.015 ND< 0.013 NSChlorobenzene ND< 0.015 ND< 0.013 2.2Ethylbenzene ND< 0.015 ND< 0.013 211,1,1,2-Tetrachloroethane ND< 0.015 ND< 0.013 1.901,1,2,2-Tetrachloroethane ND< 0.0036 ND< 0.0033 0.009m-Xylene & p-Xylene ND< 0.015 ND< 0.013 45o-Xylene ND< 0.015 ND< 0.013 45Styrene ND< 0.015 ND< 0.013 2.9Bromoform ND< 0.015 ND< 0.013 44Isopropylbenzene ND< 0.015 ND< 0.013 NSBromobenzene ND< 0.015 ND< 0.013 NSN-Propylbenzene ND< 0.015 ND< 0.013 NS1,2,3-Trichloropropane ND< 0.015 ND< 0.013 0.00132-Chlorotoluene ND< 0.015 ND< 0.013 NS1,3,5-Trimethylbenzene ND< 0.015 ND< 0.013 NS4-Chlorotoluene ND< 0.015 ND< 0.013 NStert-Butylbenzene ND< 0.015 ND< 0.013 NS1,2,4-Trimethylbenzene ND< 0.015 ND< 0.013 NSsec-Butylbenzene ND< 0.015 ND< 0.013 NS1,3-Dichlorobenzene ND< 0.015 ND< 0.013 424-Isopropyltoluene ND< 0.015 ND< 0.013 NS1,4-Dichlorobenzene ND< 0.015 ND< 0.013 0.047Notes on page 5
Table 2 (continued)
UW BH 3 7' UW BH 4 6'
(mg/kg) (mg/kg)
6 to 8Southeast side of Site
5 to 7
2 of 5
Sample ID: HDOH Depth (feet bgs): Tier 1
Portion of the site: EALAnalyte Unit: (mg/kg)VOCs / EPA Method 5035/8260B (continued)n-Butylbenzene ND< 0.015 ND< 0.013 NS1,2-Dichlorobenzene ND< 0.015 ND< 0.013 7.51,2-Dibromo-3-Chloropropane ND< 0.073 ND< 0.066 0.00091,2,4-Trichlorobenzene ND< 0.015 ND< 0.013 0.0981,2,3-Trichlorobenzene ND< 0.015 ND< 0.013 NSHexachlorobutadiene ND< 0.015 ND< 0.013 2.2Naphthalene ND< 0.015 ND< 0.013 4.5Methyl tert-butyl ether ND< 0.015 ND< 0.013 2.0
Aldrin ND< 0.00033 ND< 0.0033 0.92alpha-BHC ND< 0.00033 ND< 0.0033 NSbeta-BHC ND< 0.00033 ND< 0.0033 NSdelta-BHC ND< 0.00033 ND< 0.0033 NSgamma-BHC (Lindane) ND< 0.00033 ND< 0.0033 0.0754,4'-DDD ND< 0.00066 ND< 0.0066 2.04,4'-DDE ND< 0.00066 ND< 0.0066 1.44,4'-DDT ND< 0.00066 ND< 0.0066 1.7Dieldrin ND< 0.00066 ND< 0.0066 1.5Endosulfan I ND< 0.00033 ND< 0.0033 18Endosulfan II ND< 0.00066 ND< 0.0066 18Endosulfan Sulfate ND< 0.00066 ND< 0.0066 NSEndrin ND< 0.00066 ND< 0.0066 3.7Endrin aldehyde ND< 0.00066 ND< 0.0066 NSHeptachlor ND< 0.00066 ND< 0.0066 0.11Heptachlor epoxide ND< 0.00033 ND< 0.0033 0.053Methoxychlor ND< 0.0033 ND< 0.033 16Endrin ketone ND< 0.00066 ND< 0.0066 NSToxaphene ND< 0.033 ND< 0.33 0.44alpha-Chlordane ND< 0.0033 NSgamma-Chlordane ND< 0.0033 NS
2,3,4,6-Tetrachlorophenol ND< 0.1 ND< 0.1 4.9Ametryne ND< 0.1 ND< 0.1 11Atraton ND< 0.1 ND< 0.1 NSAtrazine ND< 0.1 ND< 0.1 2.1Azinphos-methyl ND< 0.1 ND< 0.1 NSBolstar ND< 0.1 ND< 0.1 NSBromacil ND< 0.1 ND< 0.1 NSCarbophenothion ND< 0.1 ND< 0.1 NSChlorpyrifos ND< 0.1 ND< 0.1 NSCoumaphos ND< 0.1 ND< 0.1 NSNotes on page 5
0.00160.002
Table 2 (continued)
Pesticide Screen / EPA Method 8270
UW BH 3 7' UW BH 4 6'6 to 8 5 to 7
Southeast side of Site(mg/kg) (mg/kg)
Organochlorine Pesticides / EPA Method 8081A
3 of 5
Sample ID: HDOH Depth (feet bgs): Tier 1
Portion of the site: EALAnalyte Unit: (mg/kg)
Demeton ND< 0.1 ND< 0.1 NSDiazinon ND< 0.1 ND< 0.1 NSDichlorvos ND< 0.1 ND< 0.1 NSDimethenamid ND< 0.1 ND< 0.1 NSDimethoate ND< 0.1 ND< 0.1 NSDisulfoton ND< 0.1 ND< 0.1 NSEPN ND< 0.1 ND< 0.1 NSEthoprop ND< 0.1 ND< 0.1 NSEthyl parathion ND< 0.1 ND< 0.1 NSFensulfothion ND< 0.1 ND< 0.1 NSFenthion ND< 0.1 ND< 0.1 NSHexachlorphene ND< 0.1 ND< 0.1 NSHexazinone ND< 0.1 ND< 0.1 400Malathion ND< 0.1 ND< 0.1 NSMerphos ND< 0.1 ND< 0.1 NSMethyl parathion ND< 0.1 ND< 0.1 NSMevinphos ND< 0.1 ND< 0.1 NSNaled ND< 0.1 ND< 0.1 NSPentachlorophenol ND< 0.1 ND< 0.1 0.89Phorate ND< 0.1 ND< 0.1 NSPhosmet ND< 0.1 ND< 0.1 NSPrometon ND< 0.1 ND< 0.1 NSPrometryn ND< 0.1 ND< 0.1 NSPropazine ND< 0.1 ND< 0.1 NSRonnel ND< 0.1 ND< 0.1 NSSecbumeton ND< 0.1 ND< 0.1 NSSimazine ND< 0.1 ND< 0.1 0.24Simetryn ND< 0.1 ND< 0.1 NSStirophos ND< 0.1 ND< 0.1 NSSulfotep ND< 0.1 ND< 0.1 NSTerbuthylazine ND< 0.1 ND< 0.1 NSTerbutryn ND< 0.1 ND< 0.1 NSTokuthion ND< 0.1 ND< 0.1 NSTrichloronate ND< 0.1 ND< 0.1 NSTrifluralin ND< 0.1 ND< 0.1 54Notes on page 5
Southeast side of Site
Table 2 (continued)
UW BH 3 7' UW BH 4 6'6 to 8 5 to 7
(mg/kg)Pesticide Screen / EPA Method 8270 (continued)
(mg/kg)
4 of 5
Notes:bgs Below ground surface.HDOH Tier 1 EAL
italic Analytes laboratory Reporting Limit (RL) is greater than the HDOH Tier 1 EAL.mg/kg Milligrams per kilogram.ND<
NS No standard is currently established by the HDOH for this analyte.TPH-DRO Total Petroleum Hydrocarbon as Diesel Range Organics.TPH-RRO Total Petroleum Hydrocarbon as Residual Range Organics.
Analyte not detected. The value after the '<' is the laboratory Method Reporting Limit (MRL).
Table 2 (continued)
State of Hawaii Department of Health (HDOH) Tier 1 Environmental Action Levels (EAL) at sites where groundwater is NOT a current or potential drinking water resource and a surface water body is NOT located within 150 meters of the site (HDOH, 2012).
5 of 5
Sample ID: HDOH Tier 1Analyte Unit: EAL (µg/L)Total Petroleum Hydrocarbon / EPA Method 8015BTPH-GRO ND< 50 ND< 50 5,000Total Petroleum Hydrocarbon / EPA Method 8015BTPH-DRO ND< 250 ND< 250 2,500TPH-RRO ND< 500 2,500Total metals/EPA Method 6010BCadmium ND< 10 ND< 10 3.0Lead ND< 30 ND< 30 29Polynuclear Aromatic Hydrocarbons (PAHs) / EPA Method 8270SIMNaphthalene ND< 0.10 2102-Methylnaphthalene ND< 0.13 ND< 0.13 1001-Methylnaphthalene ND< 0.10 ND< 0.10 100Acenaphthylene ND< 0.10 ND< 0.10 300Acenaphthene ND< 0.10 ND< 0.10 200Fluorene ND< 0.10 ND< 0.10 300Phenanthrene ND< 0.10 300Anthracene ND< 0.10 22Fluoranthene ND< 0.10 130Pyrene ND< 0.10 68Benzo[a]anthracene ND< 0.10 4.7Chrysene ND< 0.10 1.0Benzo[b]fluoranthene ND< 0.10 0.75Benzo[k]fluoranthene ND< 0.10 0.4Benzo[a]pyrene ND< 0.20 0.81Indeno[1,2,3-cd]pyrene ND< 0.10 0.095Dibenz[a,h]anthracene ND< 0.10 ND< 0.10 0.52Benzo[g,h,i]perylene ND< 0.10 0.13Volatile Organic Compounds (VOCs) / EPA Method 8260BDichlorodifluoromethane ND< 1.0 ND< 1.0 NSChloromethane ND< 5.0 ND< 5.0 370Vinyl chloride ND< 1.0 ND< 1.0 62Bromomethane ND< 5.0 ND< 5.0 460Chloroethane ND< 5.0 ND< 5.0 160Trichlorofluoromethane ND< 1.0 ND< 1.0 NS1,1-Dichloroethene ND< 1.0 ND< 1.0 3,900Methylene Chloride ND< 3.0 ND< 3.0 3,900trans-1,2-Dichloroethene ND< 1.0 ND< 1.0 2,600Notes on page 3
Summary of Groundwater Analytical ResultsTable 3
1,400
0.34*
0.38*
0.210.43
0.50
Urban Works Phase II Investigation1025 Waimanu Street, Honolulu, Oahu, Hawaii
UW MW-2(µg/L)
UW MW-1
Sampling Date: July 10, 2012Project No. 17012-012090.00
(µg/L)
0.46
0.12
0.870.47
0.151.0
0.49
1 of 3
Sample ID: HDOH Tier 1Analyte Unit: EAL (µg/L)VOCs / EPA Method 8260B (continued)1,1-Dichloroethane ND< 1.0 ND< 1.0 472,2-Dichloropropane ND< 1.0 ND< 1.0 NScis-1,2-Dichloroethene ND< 1.0 ND< 1.0 1,100Chlorobromomethane ND< 1.0 ND< 1.0 NSChloroform ND< 1.0 ND< 1.0 941,1,1-Trichloroethane ND< 1.0 ND< 1.0 6,000Carbon tetrachloride ND< 1.0 ND< 1.0 981,1-Dichloropropene ND< 1.0 ND< 1.0 NSBenzene ND< 1.0 ND< 1.0 1,7001,2-Dichloroethane ND< 1.0 ND< 1.0 160Trichloroethene ND< 1.0 ND< 1.0 6101,2-Dichloropropane ND< 1.0 ND< 1.0 100Dibromomethane ND< 1.0 ND< 1.0 NSDichlorobromomethane ND< 1.0 ND< 1.0 NScis-1,3-Dichloropropene ND< 1.0 ND< 1.0 NSToluene ND< 1.0 ND< 1.0 400trans-1,3-Dichloropropene ND< 1.0 ND< 1.0 NS1,1,2-Trichloroethane ND< 1.0 ND< 1.0 100Tetrachloroethene ND< 1.0 ND< 1.0 1801,3-Dichloropropane ND< 1.0 ND< 1.0 NSChlorodibromomethane ND< 1.0 ND< 1.0 NSEthylene Dibromide ND< 1.0 ND< 1.0 NSChlorobenzene ND< 1.0 ND< 1.0 160Ethylbenzene ND< 1.0 ND< 1.0 3001,1,1,2-Tetrachloroethane ND< 1.0 ND< 1.0 31001,1,2,2-Tetrachloroethane ND< 1.0 ND< 1.0 200m-Xylene & p-Xylene ND< 2.0 ND< 2.0 1,000o-Xylene ND< 1.0 ND< 1.0 1,000Styrene ND< 1.0 ND< 1.0 32Bromoform ND< 1.0 ND< 1.0 5,100Isopropylbenzene ND< 1.0 ND< 1.0 NSBromobenzene ND< 1.0 ND< 1.0 NSN-Propylbenzene ND< 1.0 ND< 1.0 NS1,2,3-Trichloropropane ND< 1.0 ND< 1.0 1402-Chlorotoluene ND< 1.0 ND< 1.0 NS1,3,5-Trimethylbenzene ND< 1.0 ND< 1.0 NS4-Chlorotoluene ND< 1.0 ND< 1.0 NStert-Butylbenzene ND< 1.0 ND< 1.0 NS1,2,4-Trimethylbenzene ND< 1.0 ND< 1.0 NSsec-Butylbenzene ND< 1.0 ND< 1.0 NS1,3-Dichlorobenzene ND< 1.0 ND< 1.0 3704-Isopropyltoluene ND< 1.0 ND< 1.0 NSNotes on page 3
Table 3 (continued)
(µg/L) (µg/L)UW MW-1 UW MW-2
2 of 3
Sample ID: HDOH Tier 1Analyte Unit: EAL (µg/L)VOCs / EPA Method 8260B (continued)1,4-Dichlorobenzene ND< 1.0 ND< 1.0 110n-Butylbenzene ND< 1.0 ND< 1.0 NS1,2-Dichlorobenzene ND< 1.0 ND< 1.0 1001,2-Dibromo-3-Chloropropane ND< 2.0 ND< 2.0 0.041,2,4-Trichlorobenzene ND< 1.0 ND< 1.0 1601,2,3-Trichlorobenzene ND< 1.0 ND< 1.0 NSHexachlorobutadiene ND< 1.0 ND< 1.0 11Naphthalene ND< 1.0 ND< 1.0 210Methyl tert-butyl ether ND< 1.0 ND< 1.0 1800Notes:bgs Below ground surface.
italic Analytes laboratory MRL is greater than the HDOH Tier 1 Action Level.µg/L Microigrams per LiterND<
NS No standard is currently established by the HDOH for this analyte.TPH-DRO Total Petroleum Hydrocarbon as Diesel Range Organics.TPH-GRO Total Petroleum Hydrocarbon as Gasoline Range Organics.TPH-RRO Total Petroleum Hydrocarbon as Residual Range Organics.* Concentration greater than or equal to the HDOH Tier 1 EAL.
Analyte not detected. The value after the '<' is the laboratory Method Reporting Limit (MRL).
UW MW-1 UW MW-2(µg/L) (µg/L)
HDOH Tier 1 EAL State of Hawaii Department of Health (HDOH) Tier 1 Environmental Action Levels (EAL) at sites where groundwater is NOT a current or potential drinking water resource and a surface water body is NOT located within 150 meters of the site (HDOH, 2012).
Table 3 (continued)
3 of 3
Sample ID:Analyte Unit:Total Petroleum Hydrocarbon / EPA Method 8015BTPH-DRO ND< 250 ND< 250 2,500TPH-RRO ND< 500 2,500Total metals/EPA Method 6010BArsenic ND< 60 ND< 60 69Polynuclear Aromatic Hydrocarbons (PAHs) / EPA Method 8270SIMNaphthalene ND< 0.10 ND< 0.10 2102-Methylnaphthalene ND< 0.13 ND< 0.13 1001-Methylnaphthalene ND< 0.10 ND< 0.10 100Acenaphthylene ND< 0.10 ND< 0.10 300Acenaphthene ND< 0.10 ND< 0.10 200Fluorene ND< 0.10 ND< 0.10 300Phenanthrene ND< 0.10 ND< 0.10 300Anthracene ND< 0.10 ND< 0.10 22Fluoranthene ND< 0.10 ND< 0.10 130Pyrene ND< 0.10 ND< 0.10 68Benzo[a]anthracene ND< 0.10 ND< 0.10 4.7Chrysene ND< 0.10 ND< 0.10 1.0Benzo[b]fluoranthene ND< 0.10 ND< 0.10 0.75Benzo[k]fluoranthene ND< 0.10 ND< 0.10 0.4Benzo[a]pyrene ND< 0.20 ND< 0.20 0.81Indeno[1,2,3-cd]pyrene ND< 0.10 ND< 0.10 0.095Dibenz[a,h]anthracene ND< 0.10 ND< 0.10 0.52Benzo[g,h,i]perylene ND< 0.10 ND< 0.10 0.13Volatile Organic Compounds (VOCs) / EPA Method 8260BDichlorodifluoromethane ND< 1.0 ND< 1.0 NSChloromethane ND< 5.0 ND< 5.0 370Vinyl chloride ND< 1.0 ND< 1.0 62Bromomethane ND< 5.0 ND< 5.0 460Chloroethane ND< 5.0 ND< 5.0 160Trichlorofluoromethane ND< 1.0 ND< 1.0 NS1,1-Dichloroethene ND< 1.0 ND< 1.0 3,900Methylene Chloride ND< 3.0 ND< 3.0 3,900trans-1,2-Dichloroethene ND< 1.0 ND< 1.0 2,6001,1-Dichloroethane ND< 1.0 ND< 1.0 472,2-Dichloropropane ND< 1.0 ND< 1.0 NScis-1,2-Dichloroethene ND< 1.0 ND< 1.0 1,100Chlorobromomethane ND< 1.0 ND< 1.0 NSNotes on page 4
Project No. 17012-012090.00Sampling Date: July 10, 2012
HDOH Tier 1 EAL (µg/L)
980
Table 4Summary of Groundwater Analytical Results
Urban Works Phase II Investigation1025 Waimanu Street, Honolulu, Oahu, Hawaii
UW MW-3 UW MW-4(µg/L) (µg/L)
1 of 4
Sample ID:Analyte Unit:VOCs / EPA Method 8260B (continued)Chloroform ND< 1.0 ND< 1.0 941,1,1-Trichloroethane ND< 1.0 ND< 1.0 6,000Carbon tetrachloride ND< 1.0 ND< 1.0 981,1-Dichloropropene ND< 1.0 ND< 1.0 NSBenzene ND< 1.0 ND< 1.0 1,7001,2-Dichloroethane ND< 1.0 ND< 1.0 160Trichloroethene ND< 1.0 ND< 1.0 6101,2-Dichloropropane ND< 1.0 ND< 1.0 100Dibromomethane ND< 1.0 ND< 1.0 NSDichlorobromomethane ND< 1.0 ND< 1.0 NScis-1,3-Dichloropropene ND< 1.0 ND< 1.0 NSToluene ND< 1.0 ND< 1.0 400trans-1,3-Dichloropropene ND< 1.0 ND< 1.0 NS1,1,2-Trichloroethane ND< 1.0 ND< 1.0 100Tetrachloroethene ND< 1.0 ND< 1.0 1801,3-Dichloropropane ND< 1.0 ND< 1.0 NSChlorodibromomethane ND< 1.0 ND< 1.0 NSEthylene Dibromide ND< 1.0 ND< 1.0 NSChlorobenzene ND< 1.0 ND< 1.0 160Ethylbenzene ND< 1.0 ND< 1.0 3001,1,1,2-Tetrachloroethane ND< 1.0 ND< 1.0 31001,1,2,2-Tetrachloroethane ND< 1.0 ND< 1.0 200m-Xylene & p-Xylene ND< 2.0 ND< 2.0 1,000o-Xylene ND< 1.0 ND< 1.0 1,000Styrene ND< 1.0 ND< 1.0 32Bromoform ND< 1.0 ND< 1.0 5,100Isopropylbenzene ND< 1.0 ND< 1.0 NSBromobenzene ND< 1.0 ND< 1.0 NSN-Propylbenzene ND< 1.0 ND< 1.0 NS1,2,3-Trichloropropane ND< 1.0 ND< 1.0 1402-Chlorotoluene ND< 1.0 ND< 1.0 NS1,3,5-Trimethylbenzene ND< 1.0 ND< 1.0 NS4-Chlorotoluene ND< 1.0 ND< 1.0 NStert-Butylbenzene ND< 1.0 ND< 1.0 NS1,2,4-Trimethylbenzene ND< 1.0 ND< 1.0 NSsec-Butylbenzene ND< 1.0 ND< 1.0 NS1,3-Dichlorobenzene ND< 1.0 ND< 1.0 3704-Isopropyltoluene ND< 1.0 ND< 1.0 NS1,4-Dichlorobenzene ND< 1.0 ND< 1.0 110n-Butylbenzene ND< 1.0 ND< 1.0 NS1,2-Dichlorobenzene ND< 1.0 ND< 1.0 1001,2-Dibromo-3-Chloropropane ND< 2.0 ND< 2.0 0.04Notes on page 4
(µg/L)HDOH Tier 1 EAL (µg/L)
Table 4 (continued)
UW MW-3 UW MW-4(µg/L)
2 of 4
Sample ID:Analyte Unit:VOCs / EPA Method 8260B (continued)1,2,4-Trichlorobenzene ND< 1.0 ND< 1.0 1601,2,3-Trichlorobenzene ND< 1.0 ND< 1.0 NSHexachlorobutadiene ND< 1.0 ND< 1.0 11Naphthalene ND< 1.0 ND< 1.0 210Methyl tert-butyl ether ND< 1.0 ND< 1.0 1800Organochlorine Pesticides / EPA Method 8081A
ND< 0.010 ND< 0.010 0.92ND< 0.010 ND< 0.010 NSND< 0.020 ND< 0.020 NSND< 0.010 ND< 0.010 NSND< 0.010 ND< 0.010 0.075ND< 0.020 ND< 0.020 2.0ND< 0.020 ND< 0.020 1.4ND< 0.020 ND< 0.020 1.7ND< 0.020 ND< 0.020 1.5ND< 0.020 ND< 0.020 18ND< 0.020 ND< 0.020 18ND< 0.020 ND< 0.020 NSND< 0.020 ND< 0.020 3.7ND< 0.050 ND< 0.050 NSND< 0.010 ND< 0.010 0.11ND< 0.010 ND< 0.010 0.053ND< 0.10 ND< 0.10 16ND< 0.020 ND< 0.020 NSND< 1.0 ND< 1.0 0.44ND< 0.010 ND< 0.010 NSND< 0.010 ND< 0.010 NS
Organochlorine Pesticides / EPA Method 8270ND< 0.5 ND< 0.5 10ND< 0.5 ND< 0.5 150ND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 350ND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NS
Notes on page 4
DichlorvosDimethenamidDimethoate
CarbophenothionChlorpyrifosCoumaphosDemeton
MethoxychlorHeptachlor epoxide
Endrin aldehyde
Table 4 (continued)
UW MW-3 UW MW-4(µg/L) (µg/L)
HDOH Tier 1 EAL (µg/L)
4,4'-DDE
gamma-Chlordanealpha-ChlordaneToxapheneEndrin ketone
4,4'-DDT
gamma-BHC (Lindane)delta-BHCbeta-BHCalpha-BHC
4,4'-DDD
Heptachlor
Endosulfan IIEndosulfan IDieldrin
Endrin
Aldrin
Endosulfan Sulfate
2,3,4,6-TetrachlorophenolAmetryneAtratonAtrazineAzinphos-methylBolstarBromacil
Diazinon
3 of 4
Sample ID:Analyte Unit:Organochlorine Pesticides / EPA Method 8270 (continued)
ND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 50,000ND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 13ND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 10ND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 NSND< 0.5 ND< 0.5 20
Notes:bgs Below ground surface.HDOH Tier 1 EAL
italic Analytes laboratory MRL is greater than the HDOH Tier 1 Action Level.µg/L Microigrams per LiterND<
NS No standard is currently established by the HDOH for this analyte.TPH-DRO Total Petroleum Hydrocarbon as Diesel Range Organics.TPH-RRO Total Petroleum Hydrocarbon as Residual Range Organics.
Table 4 (continued)
UW MW-3 UW MW-4 HDOH Tier 1 EAL (µg/L)(µg/L) (µg/L)
TrichloronateTrilfuralin
SimetrynStirophos
TerbutrynTokuthion
SulfotepTerbuthylazine
SecbumetonSimazine
PrometonPrometrynPropazineRonnel
MalathionMerphosMethyl parathionMevinphosNaledPentachlorophenolPhoratePhosmet
DisulfotonEPNEthopropEthyl parathionFensulfothionFenthionHexachlorpheneHexazinone
State of Hawaii Department of Health (HDOH) Tier 1 Environmental Action Levels (EAL) at sites where groundwater is NOT a current or potential drinking water resource and a surface water body is NOT located within 150 meters of the site (HDOH, 2012).
Analyte not detected. The value after the '<' is the laboratory Method Reporting Limit (MRL).
4 of 4
APPENDIX A
BOREHOLE LOGS
UW BH/MW-1
17012-012090.00
Urban Works Phase II
Urban Works, LLC
1025 Waimanu Street, Honolulu
Ground Surface
Asphalt/subgrade gravel
Silty Clay, brown, some sand and fine gravel, damp, no odor/staining.
Grey Gravel stringer
Silty Clay with Sand and Gravel, grey brown, damp, no odor/staining.
Coral and Coral Sand, white/tan, damp to wet.
Increasing grain size with depth.
Coral Sand and Gravel, grey, saturated.
End of Boring
0.0
0.8
3.03.5
4.5
8.0
12.0
16.0
UW BH1-1'
UW BH1-6'
0.0
0.0
Tem
pora
ry 1
" di
a. P
VC
Wel
l Scr
een
Filt
er s
and
ESN, Pacific
Direct push
July 10, 2012
Log of Borehole:
Project No.:
Project:
Client:
Location:
Drilled By:
Drill Method:
Drill Date:
Hole Size:
Datum:
Sheet:
BUREAU VERITASNORTH AMERICA, INC.
970 North Kalaheo AvenueSuite C-316
Kailua, Hawaii 96734
SUBSURFACE PROFILE SAMPLE
Dep
th
0
2
4
6
8
10
12
14
16
Sym
bol Description
Dep
th/
Ele
vatio
n
Num
ber
Typ
e
PID
Wel
l Com
plet
ion
Det
ails
UW BH/MW-2
17012-012090.00
Urban Works Phase II
Urban Works, LLC
1025 Waimanu Street, Honolulu
Ground Surface
Asphalt/subgrade gravel
Silty Clay, very dark greyish brown (10YR 3/2), some sand and fine gravel, damp, no odor/staining.
Coral and Coral Sand, white to tan, damp to saturated, no odor or staining.
Coral Sand and Gravel, grey, saturated.
End of Boring
0.00.5
4.5
9.5
12.0
16.0
UW BH2-1'
UW BH2-7'
0.0
0.0
Tem
pora
ry 1
" di
a. P
VC
Wel
l Scr
een
Filt
er s
and
ESN, Pacific
Direct push
July 10, 2012
Log of Borehole:
Project No.:
Project:
Client:
Location:
Drilled By:
Drill Method:
Drill Date:
Hole Size:
Datum:
Sheet:
BUREAU VERITASNORTH AMERICA, INC.
970 North Kalaheo AvenueSuite C-316
Kailua, Hawaii 96734
SUBSURFACE PROFILE SAMPLE
Dep
th
0
2
4
6
8
10
12
14
16
Sym
bol Description
Dep
th/
Ele
vatio
n
Num
ber
Typ
e
PID
Wel
l Com
plet
ion
Det
ails
UW BH/MW-3
17012-012090.00
Urban Works Phase II
Urban Works, LLC
1025 Waimanu Street, Honolulu
Ground Surface
Asphalt/subgrade gravel
Silty Clay, dusky red (2.5YR 3/3), with stringers of coral and gravel, damp, no odor/staining.
Sand and Coral Gravel, white to tan, moist, no odor/staining.
Coral and Coral Sand, pale red (2.5YR 7/4), wet to saturated, no odor or staining.
Coral Sand and Gravel, grey, saturated.
End of Boring
0.00.5
4.5
6.5
10.0
12.0
16.0
UW BH3-7' 0.0
Tem
pora
ry 1
" di
a. P
VC
Wel
l Scr
een
Filt
er s
and
ESN, Pacific
Direct push
July 10, 2012
Log of Borehole:
Project No.:
Project:
Client:
Location:
Drilled By:
Drill Method:
Drill Date:
Hole Size:
Datum:
Sheet:
BUREAU VERITASNORTH AMERICA, INC.
970 North Kalaheo AvenueSuite C-316
Kailua, Hawaii 96734
SUBSURFACE PROFILE SAMPLE
Dep
th
0
2
4
6
8
10
12
14
16
Sym
bol Description
Dep
th/
Ele
vatio
n
Num
ber
Typ
e
PID
Wel
l Com
plet
ion
Det
ails
UW BH/MW-4
17012-012090.00
Urban Works Phase II
Urban Works, LLC
1025 Waimanu Street, Honolulu
Ground Surface
Asphalt/subgrade gravel
Silty Clay, very dark brown (7.5YR 3/2), with some sand and gravel, damp, no odor/staining.
Coral Sand, light grey (10YR 7/2), with some fine gravel, moist, no odor/staining.
Coral and Coral Sand, grey, wet to saturated, no odor or staining.
Coral Sand and Gravel, grey, saturated.
End of Boring
0.00.5
2.5
6.5
10.0
12.0
16.0
UW BH4-6' 0.0
Tem
pora
ry 1
" di
a. P
VC
Wel
l Scr
een
Filt
er s
and
ESN, Pacific
Direct push
July 10, 2012
Log of Borehole:
Project No.:
Project:
Client:
Location:
Drilled By:
Drill Method:
Drill Date:
Hole Size:
Datum:
Sheet:
BUREAU VERITASNORTH AMERICA, INC.
970 North Kalaheo AvenueSuite C-316
Kailua, Hawaii 96734
SUBSURFACE PROFILE SAMPLE
Dep
th
0
2
4
6
8
10
12
14
16
Sym
bol Description
Dep
th/
Ele
vatio
n
Num
ber
Typ
e
PID
Wel
l Com
plet
ion
Det
ails
APPENDIX B
GROUNDWATER SAMPLING LOGS
Project: Urban Works Phase II Site: 1025 Waimanu Street, Honolulu
Project No.: 17012-012090.00 Well ID: UW BH/MW-1
Field Crew: Ken GomesSampling Date:
7/10/2012
Screened Interval (ft): 0.0 to Climatic Conditions: Sunny, partly cloudy ~ 80s°F
Well Diameter (in.): 1 inch 0.041 gal/ft Purge Method: Peristaltic Pump
PID Reading (ppm): N/A ppm Pump Placement (ft): ft
Water Level Indicator: Water level indicator Pump Rate (gal/min): 0.00 gal/min
Total Well Depth (ft): 9.65 ft 3.3
Depth to Water (ft): 6.35 ft
Depth to Product (ft): N/A ft Casing Volume (gal): 0.14 gallons
x 3: 0.41 gallons
TimeDepth to Water (ft)
Purge Rate (gpm)
Gallons Removed pH
Cond. (S/cm) Turbidity
D.O. (mg/L)
Temp (deg C)
Salinity (%) ORP (mV) Comments
1504 Start 7.86 1.97 999 -- 27 0.09
1506 0.2 7.18 2.44 999 -- 28.4 0.11
1508 0.4 7.09 2.35 999 -- 28.2 0.11
1510 0.6 7.05 2.27 999 -- 28.3 0.11
1512 0.8 7.04 2.30 999 -- 28.5 0.11
1514 1.0 7.02 2.22 999 -- 28.4 0.11
1516 1.2 7.04 2.25 999 -- 28.4 0.11
Color: grey brown
Odor: none
Turbidity: turbid to cloudy
Laboratory Analysis: x VOCs 8260B
x TPH-DRO 8015M
x TPH-RRO 8015M
SVOCs 8270C
xPAH 8270SIM
PCBs 8082
X
X Other: TPH-GRO Org Chlor Pest (8081) Mod Pest Screen (8270)
Sample ID: UW MW-1 Total No. of Bottles: 12
Sample Date & Time: 7/10/2012 1518
Notes: DO failed auto calibration
Analytical Laboratory: TestAmerica Transported via: Hand
Signature
Capacity of Casing (gal/linear feet): 1"=0.041; 2"=0.16; 4"=0.65; 6"=1.47; 8"=2.61; 10"=4.08
Lead and Cadmium 6010(Field Filtered? Y )
Groundwater Sampling/Development Log
Field Parameters
Sample or Purge Information
ftLength of Saturated Zone (ft):
Arsenic 6010 (Field Filtered? Y)
Project: Urban Works Phase II Site: 1025 Waimanu Street, Honolulu
Project No.: 17012-012090.00 Well ID: UW BH/MW-2
Field Crew: Ken GomesSampling Date:
7/10/2012
Screened Interval (ft): 0.0 to Climatic Conditions: Sunny, partly cloudy ~ 80s°F
Well Diameter (in.): 1 inch 0.041 gal/ft Purge Method: Peristaltic Pump
PID Reading (ppm): N/A ppm Pump Placement (ft): ft
Water Level Indicator: Water level indicator Pump Rate (gal/min): 0.00 gal/min
Total Well Depth (ft): 11.50 ft 4.1
Depth to Water (ft): 7.42 ft
Depth to Product (ft): N/A ft Casing Volume (gal): 0.17 gallons
x 3: 0.50 gallons
TimeDepth to Water (ft)
Purge Rate (gpm)
Gallons Removed pH
Cond. (S/cm) Turbidity
D.O. (mg/L)
Temp (deg C)
Salinity (%) ORP (mV) Comments
1410 Start 7.12 2.16 999 -- 28.6 0.1
1412 0.2 7.04 2.12 999 -- 28.5 0.10
1414 0.4 7.02 2.07 999 -- 28.4 0.09
1416 0.8 7.06 2.00 999 -- 28.3 0.09
1418 1.0 7.05 1.97 999 -- 28.3 0.09
1420 1.2 7.04 1.95 999 -- 28.3 0.09
Color: grey brown
Odor: none
Turbidity: turbid to cloudy
Laboratory Analysis: x VOCs 8260B
x TPH-DRO 8015M
x TPH-RRO 8015M
SVOCs 8270C
xPAH 8270SIM
PCBs 8082
X
X Other: TPH-GRO Org Chlor Pest (8081) Mod Pest Screen (8270)
Sample ID: UW MW-2 Total No. of Bottles: 12
Sample Date & Time: 7/10/2012 1422
Notes: DO failed auto calibration
Analytical Laboratory: TestAmerica Transported via: Hand
Signature
Capacity of Casing (gal/linear feet): 1"=0.041; 2"=0.16; 4"=0.65; 6"=1.47; 8"=2.61; 10"=4.08
Lead and Cadmium 6010(Field Filtered? Y )
Groundwater Sampling/Development Log
Field Parameters
Sample or Purge Information
ftLength of Saturated Zone (ft):
Arsenic 6010 (Field Filtered? Y)
Project: Urban Works Phase II Site: 1025 Waimanu Street, Honolulu
Project No.: 17012-012090.00 Well ID: UW BH/MW-3
Field Crew: Ken GomesSampling Date:
7/10/2012
Screened Interval (ft): 0.0 to Climatic Conditions: Sunny, partly cloudy ~ 80s°F
Well Diameter (in.): 1 inch 0.041 gal/ft Purge Method: Peristaltic Pump
PID Reading (ppm): N/A ppm Pump Placement (ft): ft
Water Level Indicator: Water level indicator Pump Rate (gal/min): 0.00 gal/min
Total Well Depth (ft): 11.44 ft 4.3
Depth to Water (ft): 7.18 ft
Depth to Product (ft): N/A ft Casing Volume (gal): 0.17 gallons
x 3: 0.52 gallons
TimeDepth to Water (ft)
Purge Rate (gpm)
Gallons Removed pH
Cond. (S/cm) Turbidity
D.O. (mg/L)
Temp (deg C)
Salinity (%) ORP (mV) Comments
1010 Start 6.14 1.21 999 -- 28.9 0.05
1012 0.2 6.61 1.05 999 -- 29.0 0.04
1014 0.4 6.64 0.94 999 -- 28.9 0.04
1016 0.6 6.63 0.94 999 -- 29.2 0.04
1018 0.8 6.64 0.92 999 -- 29.1 0.04
1020 1.0 6.62 0.92 999 -- 29.0 0.04
1022 1.2 6.77 0.834 999 -- 28.8 0.03
1024 1.4 6.72 0.841 999 -- 28.8 0.03
Color: grey brown
Odor: none
Turbidity: turbid to cloudy
Laboratory Analysis: x VOCs 8260B
x TPH-DRO 8015M
x TPH-RRO 8015M
X
SVOCs 8270C
xPAH 8270SIM
PCBs 8082
Other: TPH-GRO X Org Chlor Pest (8081) X Mod Pest Screen (8270)
Sample ID: UW MW-3 Total No. of Bottles: 12
Sample Date & Time: 7/10/2012 1030
Notes: DO failed auto calibration
Analytical Laboratory: TestAmerica Transported via: Hand
Signature
Capacity of Casing (gal/linear feet): 1"=0.041; 2"=0.16; 4"=0.65; 6"=1.47; 8"=2.61; 10"=4.08
Lead and Cadmium 6010(Field Filtered? Y )
Groundwater Sampling/Development Log
Field Parameters
Sample or Purge Information
ftLength of Saturated Zone (ft):
Arsenic 6010 (Field Filtered? Y)
Project: Urban Works Phase II Site: 1025 Waimanu Street, Honolulu
Project No.: 17012-012090.00 Well ID: UW BH/MW-4
Field Crew: Ken GomesSampling Date:
7/10/2012
Screened Interval (ft): 0.0 to Climatic Conditions: Sunny, partly cloudy ~ 80s°F
Well Diameter (in.): 1 inch 0.041 gal/ft Purge Method: Peristaltic Pump
PID Reading (ppm): N/A ppm Pump Placement (ft): ft
Water Level Indicator: Water level indicator Pump Rate (gal/min): 0.00 gal/min
Total Well Depth (ft): 10.86 ft 4.9
Depth to Water (ft): 6.00 ft
Depth to Product (ft): N/A ft Casing Volume (gal): 0.20 gallons
x 3: 0.60 gallons
TimeDepth to Water (ft)
Purge Rate (gpm)
Gallons Removed pH
Cond. (S/cm) Turbidity
D.O. (mg/L)
Temp (deg C)
Salinity (%) ORP (mV) Comments
1200 Start 7.15 6.1 999 -- 28.2 0.32
1202 0.2 7.14 6.940 999 -- 27.9 0.37
1204 0.4 7.13 6.840 999 -- 28.1 0.36
1206 0.6 7.11 6.760 999 -- 28.3 0.36
1208 0.8 7.10 6.720 999 -- 28.1 0.36
1210 1.0 7.12 6.780 999 -- 28.0 0.36
1212 1.2 7.15 6.630 999 -- 28.1 0.35
Color: grey brown
Odor: none
Turbidity: turbid to cloudy
Laboratory Analysis: x VOCs 8260B
x TPH-DRO 8015M
x TPH-RRO 8015M
X
SVOCs 8270C
xPAH 8270SIM
PCBs 8082
Other: TPH-GRO X Org Chlor Pest (8081) X Mod Pest Screen (8270)
Sample ID: UW MW-4 Total No. of Bottles: 12
Sample Date & Time: 7/10/2012 1220
Notes: DO failed auto calibration
Analytical Laboratory: TestAmerica Transported via: Hand
Signature
Capacity of Casing (gal/linear feet): 1"=0.041; 2"=0.16; 4"=0.65; 6"=1.47; 8"=2.61; 10"=4.08
Lead and Cadmium 6010(Field Filtered? Y )
Groundwater Sampling/Development Log
Field Parameters
Sample or Purge Information
ftLength of Saturated Zone (ft):
Arsenic 6010 (Field Filtered? Y)
APPENDIX C
ANALYTICAL REPORTS AND
CHAIN-OF-CUSTODY FORMS
ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Seattle5755 8th Street EastTacoma, WA 98424Tel: (253)922-2310
TestAmerica Job ID: 580-33932-1Client Project/Site: Urban Works Phase II
For:Bureau Veritas North America, Inc.970 North Kalaheo AvenueSuite C-316Kailua, Hawaii 96734
Attn: Patrick Casey
Authorized for release by:8/9/2012 2:34:29 PM
Pam JohnsonProject Manager [email protected]
This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Bureau Veritas North America, Inc.Project/Site: Urban Works Phase II
TestAmerica Job ID: 580-33932-1
Page 2 of 60TestAmerica Seattle
8/9/2012
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47
Subcontract Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 60
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Case NarrativeClient: Bureau Veritas North America, Inc. TestAmerica Job ID: 580-33932-1
Project/Site: Urban Works Phase II
Job ID: 580-33932-1
Laboratory: TestAmerica Seattle
Narrative
Comments
No additional comments.
Receipt
The samples were received on 7/13/2012 10:00 AM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperature of the cooler at receipt was 10.5º C.
Except:
The following samples were received at the laboratory, with melted ice, outside the required temperature criteria: UW BH 1 1'
(580-33932-1), UW BH 1 6' (580-33932-2), UW BH 2 1' (580-33932-3), UW BH 2 7' (580-33932-4), UW BH 3 7' (580-33932-5), UW BH 4 6'
(580-33932-6), UW MI-1 (580-33932-7), UW MI-2 (580-33932-8). The recorded temperature was 10.5/10.1 C; the samples were logged in.
GC/MS VOA - Method 8260B
The laboratory control sample (LCS) and laboratory control sample duplicate (LCSD) for analytical batch 115678 exceeded control limits
for the following analyte: 1,2-Dichloropropane. This analyte was biased high in the LCS and LCSD but was not detected in the associated
samples; therefore, the data have been reported.
Samples UW MI-1 (580-33932-7) and UW MI-2 (580-33932-8) were reanalyzed in analytical batch 115886 due to an auto sampler
programming error which caused the original analyses to be analyzed outside of the 12 hour tune shift.
No other analytical or quality issues were noted.
GC/MS Semi VOA
No analytical or quality issues were noted.
GC Semi VOA - Method 8015B
In analytical batch 116168, for the following samples UW BH 1 1' (580-33932-1), UW BH 2 1' (580-33932-3), UW BH 4 6' (580-33932-6),
UW MI-1 (580-33932-7), UW MI-2 (580-33932-8) from preparation batch 115815.
In samples UW BH 1 1' (580-33932-1) and UW BH 4 6' (580-33932-6), the results in the #2 Diesel C12-C24 range are due to what most
closely resembles overlap from the C24-C32 range.
In sample UW BH 2 1' (580-33932-3), the results in the #2 Diesel (C10-C24) and Motor Oil (>C24-C36) ranges are due to what most
closely resembles a complex mixture of motor oil and heavier oil product.
In samples UW MI-1 (580-33932-7) and UW MI-2 (580-33932-8), the results in the #2 Diesel (C10-C24) and Motor Oil (>C24-C36) ranges
are due to what most closely resembles a complex mixture of motor oil and possible biogenic interference; method 3630 silica gel
cleanup procedure is recommended.
The affected analyte ranges are qualified "Y" and have been reported.
GC Semi VOA - Method 8081A
Surrogate recovery for the following sample UW BH 4 6' (580-33932-6) was outside control limits. Evidence of matrix interference is
present; therefore, re-extraction and/or re-analysis was not performed.
The following sample UW BH 4 6' (580-33932-6) was diluted due to the nature of the sample matrix. Elevated reporting limits (RLs) are
provided.
No other analytical or quality issues were noted.
Metals
No analytical or quality issues were noted.
General Chemistry
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Case NarrativeClient: Bureau Veritas North America, Inc. TestAmerica Job ID: 580-33932-1
Project/Site: Urban Works Phase II
Job ID: 580-33932-1 (Continued)
Laboratory: TestAmerica Seattle (Continued)
No analytical or quality issues were noted.
Subcontract Work
Method 8270 - Modified Pesticide Screen: This method was subcontracted to Anatek Labs Inc - Moscow Idaho. The subcontract
certification is different from those listed on the TestAmerica cover page of this final report.
Organic Prep - Method 3550B
A deviation from the Standard Operating Procedure (SOP) occurred. Details are as follows: Not enough multi-incremental samples were
provided to do an MS/MSD. Instead LCS/LCSD was used. UW BH 1 1' (580-33932-1)
No other analytical or quality issues were noted.
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Definitions/GlossaryTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Qualifiers
GC/MS VOA
Qualifier Description
* LCS or LCSD exceeds the control limits
Qualifier
GC Semi VOA
Qualifier Description
Y The chromatographic response resembles a typical fuel pattern.
Qualifier
X Surrogate is outside control limits
Glossary
These commonly used abbreviations may or may not be present in this report.
☼ Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CNF Contains no Free Liquid
DL, RA, RE, IN Indicates a Dilution, Reanalysis, Re-extraction, or additional Initial metals/anion analysis of the sample
EDL Estimated Detection Limit
EPA United States Environmental Protection Agency
MDL Method Detection Limit
ML Minimum Level (Dioxin)
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RL Reporting Limit
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33932-1Client Sample ID: UW BH 1 1'Matrix: SolidDate Collected: 07/10/12 11:40
Percent Solids: 97.1Date Received: 07/13/12 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Dichlorodifluoromethane ND 170 ug/Kg ☼ 07/17/12 11:46 07/19/12 18:44 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1700 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Chloromethane ND
34 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Vinyl chloride ND
590 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Bromomethane ND
1700 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Chloroethane ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Trichlorofluoromethane ND
85 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼1,1-Dichloroethene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Methylene Chloride ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼trans-1,2-Dichloroethene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼1,1-Dichloroethane ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼2,2-Dichloropropane ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼cis-1,2-Dichloroethene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Chlorobromomethane ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Chloroform ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼1,1,1-Trichloroethane ND
85 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Carbon tetrachloride ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼1,1-Dichloropropene ND
68 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Benzene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼1,2-Dichloroethane ND
68 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Trichloroethene ND
51 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼1,2-Dichloropropane ND *
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Dibromomethane ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Dichlorobromomethane ND
68 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼cis-1,3-Dichloropropene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Toluene ND
68 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼trans-1,3-Dichloropropene ND
51 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼1,1,2-Trichloroethane ND
85 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Tetrachloroethene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼1,3-Dichloropropane ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Chlorodibromomethane ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Ethylene Dibromide ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Chlorobenzene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Ethylbenzene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼1,1,1,2-Tetrachloroethane ND
42 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼1,1,2,2-Tetrachloroethane ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼m-Xylene & p-Xylene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼o-Xylene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Styrene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Bromoform ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Isopropylbenzene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Bromobenzene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼N-Propylbenzene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼1,2,3-Trichloropropane ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼2-Chlorotoluene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼1,3,5-Trimethylbenzene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼4-Chlorotoluene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼tert-Butylbenzene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼1,2,4-Trimethylbenzene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼sec-Butylbenzene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼1,3-Dichlorobenzene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼4-Isopropyltoluene ND
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Client Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33932-1Client Sample ID: UW BH 1 1'Matrix: SolidDate Collected: 07/10/12 11:40
Percent Solids: 97.1Date Received: 07/13/12 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)RL MDL
1,4-Dichlorobenzene ND 170 ug/Kg ☼ 07/17/12 11:46 07/19/12 18:44 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼n-Butylbenzene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼1,2-Dichlorobenzene ND
850 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼1,2-Dibromo-3-Chloropropane ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼1,2,4-Trichlorobenzene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼1,2,3-Trichlorobenzene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Hexachlorobutadiene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Naphthalene ND
170 ug/Kg 07/17/12 11:46 07/19/12 18:44 1☼Methyl tert-butyl ether ND
Fluorobenzene (Surr) 98 80 - 120 07/17/12 11:46 07/19/12 18:44 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Toluene-d8 (Surr) 98 07/17/12 11:46 07/19/12 18:44 180 - 120
Ethylbenzene-d10 96 07/17/12 11:46 07/19/12 18:44 170 - 120
4-Bromofluorobenzene (Surr) 92 07/17/12 11:46 07/19/12 18:44 170 - 120
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM)RL MDL
Naphthalene 2.2 1.6 ug/Kg ☼ 07/23/12 13:38 07/30/12 10:33 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.6 ug/Kg 07/23/12 13:38 07/30/12 10:33 1☼2-Methylnaphthalene 1.7
1.6 ug/Kg 07/23/12 13:38 07/30/12 10:33 1☼1-Methylnaphthalene 1.8
1.6 ug/Kg 07/23/12 13:38 07/30/12 10:33 1☼Acenaphthylene 5.9
1.6 ug/Kg 07/23/12 13:38 07/30/12 10:33 1☼Acenaphthene 2.0
1.6 ug/Kg 07/23/12 13:38 07/30/12 10:33 1☼Fluorene ND
1.6 ug/Kg 07/23/12 13:38 07/30/12 10:33 1☼Phenanthrene 39
1.6 ug/Kg 07/23/12 13:38 07/30/12 10:33 1☼Anthracene 21
1.6 ug/Kg 07/23/12 13:38 07/30/12 10:33 1☼Fluoranthene 150
1.6 ug/Kg 07/23/12 13:38 07/30/12 10:33 1☼Pyrene 260
1.6 ug/Kg 07/23/12 13:38 07/30/12 10:33 1☼Benzo[a]anthracene 120
1.6 ug/Kg 07/23/12 13:38 07/30/12 10:33 1☼Chrysene 150
1.6 ug/Kg 07/23/12 13:38 07/30/12 10:33 1☼Benzo[b]fluoranthene 130
1.6 ug/Kg 07/23/12 13:38 07/30/12 10:33 1☼Benzo[k]fluoranthene 54
1.6 ug/Kg 07/23/12 13:38 07/30/12 10:33 1☼Benzo[a]pyrene 97
1.6 ug/Kg 07/23/12 13:38 07/30/12 10:33 1☼Indeno[1,2,3-cd]pyrene 71
1.6 ug/Kg 07/23/12 13:38 07/30/12 10:33 1☼Dibenz(a,h)anthracene 17
1.6 ug/Kg 07/23/12 13:38 07/30/12 10:33 1☼Benzo[g,h,i]perylene 200
Terphenyl-d14 95 42 - 151 07/23/12 13:38 07/30/12 10:33 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Gasoline Range Organics - (GC)RL MDL
HI Gasoline Range Organic (C6-C12) ND 17 mg/Kg ☼ 07/17/12 10:13 07/17/12 20:52 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 100 75 - 131 07/17/12 10:13 07/17/12 20:52 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
HI Diesel Range Organics
(>C12-C24)
160 Y 8.3 mg/Kg ☼ 07/20/12 11:46 07/25/12 21:12 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
17 mg/Kg 07/20/12 11:46 07/25/12 21:12 1☼HI Residual Range Organics
(>C24-C32)
1900
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Client Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33932-1Client Sample ID: UW BH 1 1'Matrix: SolidDate Collected: 07/10/12 11:40
Percent Solids: 97.1Date Received: 07/13/12 10:00
o-Terphenyl 86 50 - 150 07/20/12 11:46 07/25/12 21:12 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 6010B - Metals (ICP)RL MDL
Cadmium ND 0.95 mg/Kg ☼ 07/25/12 10:14 07/25/12 22:09 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.9 mg/Kg 07/25/12 10:14 07/25/12 22:09 10☼Lead 79
General ChemistryRL RL
Percent Solids 97 0.10 % 07/17/12 18:49 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.10 % 07/17/12 18:49 1Percent Moisture 2.9
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Client Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33932-2Client Sample ID: UW BH 1 6'Matrix: SolidDate Collected: 07/10/12 11:55
Percent Solids: 98.7Date Received: 07/13/12 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Dichlorodifluoromethane ND 160 ug/Kg ☼ 07/17/12 11:46 07/19/12 19:07 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1600 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Chloromethane ND
33 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Vinyl chloride ND
570 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Bromomethane ND
1600 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Chloroethane ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Trichlorofluoromethane ND
81 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼1,1-Dichloroethene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Methylene Chloride ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼trans-1,2-Dichloroethene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼1,1-Dichloroethane ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼2,2-Dichloropropane ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼cis-1,2-Dichloroethene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Chlorobromomethane ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Chloroform ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼1,1,1-Trichloroethane ND
81 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Carbon tetrachloride ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼1,1-Dichloropropene ND
65 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Benzene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼1,2-Dichloroethane ND
65 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Trichloroethene ND
49 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼1,2-Dichloropropane ND *
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Dibromomethane ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Dichlorobromomethane ND
65 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼cis-1,3-Dichloropropene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Toluene ND
65 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼trans-1,3-Dichloropropene ND
49 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼1,1,2-Trichloroethane ND
81 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Tetrachloroethene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼1,3-Dichloropropane ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Chlorodibromomethane ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Ethylene Dibromide ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Chlorobenzene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Ethylbenzene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼1,1,1,2-Tetrachloroethane ND
41 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼1,1,2,2-Tetrachloroethane ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼m-Xylene & p-Xylene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼o-Xylene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Styrene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Bromoform ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Isopropylbenzene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Bromobenzene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼N-Propylbenzene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼1,2,3-Trichloropropane ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼2-Chlorotoluene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼1,3,5-Trimethylbenzene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼4-Chlorotoluene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼tert-Butylbenzene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼1,2,4-Trimethylbenzene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼sec-Butylbenzene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼1,3-Dichlorobenzene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼4-Isopropyltoluene ND
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Client Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33932-2Client Sample ID: UW BH 1 6'Matrix: SolidDate Collected: 07/10/12 11:55
Percent Solids: 98.7Date Received: 07/13/12 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)RL MDL
1,4-Dichlorobenzene ND 160 ug/Kg ☼ 07/17/12 11:46 07/19/12 19:07 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼n-Butylbenzene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼1,2-Dichlorobenzene ND
810 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼1,2-Dibromo-3-Chloropropane ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼1,2,4-Trichlorobenzene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼1,2,3-Trichlorobenzene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Hexachlorobutadiene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Naphthalene ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:07 1☼Methyl tert-butyl ether ND
Fluorobenzene (Surr) 98 80 - 120 07/17/12 11:46 07/19/12 19:07 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Toluene-d8 (Surr) 95 07/17/12 11:46 07/19/12 19:07 180 - 120
Ethylbenzene-d10 95 07/17/12 11:46 07/19/12 19:07 170 - 120
4-Bromofluorobenzene (Surr) 89 07/17/12 11:46 07/19/12 19:07 170 - 120
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM)RL MDL
Naphthalene ND 1.6 ug/Kg ☼ 07/23/12 13:38 07/27/12 15:39 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.6 ug/Kg 07/23/12 13:38 07/27/12 15:39 1☼2-Methylnaphthalene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 15:39 1☼1-Methylnaphthalene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 15:39 1☼Acenaphthylene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 15:39 1☼Acenaphthene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 15:39 1☼Fluorene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 15:39 1☼Phenanthrene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 15:39 1☼Anthracene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 15:39 1☼Fluoranthene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 15:39 1☼Pyrene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 15:39 1☼Benzo[a]anthracene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 15:39 1☼Chrysene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 15:39 1☼Benzo[b]fluoranthene 1.8
1.6 ug/Kg 07/23/12 13:38 07/27/12 15:39 1☼Benzo[k]fluoranthene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 15:39 1☼Benzo[a]pyrene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 15:39 1☼Indeno[1,2,3-cd]pyrene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 15:39 1☼Dibenz(a,h)anthracene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 15:39 1☼Benzo[g,h,i]perylene 2.0
Terphenyl-d14 90 42 - 151 07/23/12 13:38 07/27/12 15:39 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Gasoline Range Organics - (GC)RL MDL
HI Gasoline Range Organic (C6-C12) ND 16 mg/Kg ☼ 07/17/12 10:13 07/17/12 21:14 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 98 75 - 131 07/17/12 10:13 07/17/12 21:14 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
HI Diesel Range Organics (>C12-C24) ND 8.2 mg/Kg ☼ 07/20/12 11:46 07/25/12 21:32 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
16 mg/Kg 07/20/12 11:46 07/25/12 21:32 1☼HI Residual Range Organics
(>C24-C32)
26
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Client Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33932-2Client Sample ID: UW BH 1 6'Matrix: SolidDate Collected: 07/10/12 11:55
Percent Solids: 98.7Date Received: 07/13/12 10:00
o-Terphenyl 92 50 - 150 07/20/12 11:46 07/25/12 21:32 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 6010B - Metals (ICP)RL MDL
Cadmium ND 0.98 mg/Kg ☼ 07/25/12 10:14 07/25/12 22:22 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.9 mg/Kg 07/25/12 10:14 07/25/12 22:22 10☼Lead ND
General ChemistryRL RL
Percent Solids 99 0.10 % 07/17/12 18:49 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.10 % 07/17/12 18:49 1Percent Moisture 1.3
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Client Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33932-3Client Sample ID: UW BH 2 1'Matrix: SolidDate Collected: 07/10/12 10:40
Percent Solids: 95.9Date Received: 07/13/12 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Dichlorodifluoromethane ND 21 ug/Kg ☼ 07/17/12 11:46 07/19/12 19:30 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
210 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Chloromethane ND
4.3 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Vinyl chloride ND
75 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Bromomethane ND
210 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Chloroethane ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Trichlorofluoromethane ND
11 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼1,1-Dichloroethene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Methylene Chloride ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼trans-1,2-Dichloroethene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼1,1-Dichloroethane ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼2,2-Dichloropropane ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼cis-1,2-Dichloroethene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Chlorobromomethane ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Chloroform ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼1,1,1-Trichloroethane ND
11 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Carbon tetrachloride ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼1,1-Dichloropropene ND
8.6 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Benzene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼1,2-Dichloroethane ND
8.6 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Trichloroethene ND
6.4 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼1,2-Dichloropropane ND *
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Dibromomethane ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Dichlorobromomethane ND
8.6 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼cis-1,3-Dichloropropene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Toluene ND
8.6 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼trans-1,3-Dichloropropene ND
6.4 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼1,1,2-Trichloroethane ND
11 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Tetrachloroethene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼1,3-Dichloropropane ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Chlorodibromomethane ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Ethylene Dibromide ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Chlorobenzene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Ethylbenzene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼1,1,1,2-Tetrachloroethane ND
5.4 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼1,1,2,2-Tetrachloroethane ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼m-Xylene & p-Xylene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼o-Xylene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Styrene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Bromoform ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Isopropylbenzene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Bromobenzene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼N-Propylbenzene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼1,2,3-Trichloropropane ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼2-Chlorotoluene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼1,3,5-Trimethylbenzene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼4-Chlorotoluene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼tert-Butylbenzene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼1,2,4-Trimethylbenzene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼sec-Butylbenzene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼1,3-Dichlorobenzene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼4-Isopropyltoluene ND
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Client Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33932-3Client Sample ID: UW BH 2 1'Matrix: SolidDate Collected: 07/10/12 10:40
Percent Solids: 95.9Date Received: 07/13/12 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)RL MDL
1,4-Dichlorobenzene ND 21 ug/Kg ☼ 07/17/12 11:46 07/19/12 19:30 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼n-Butylbenzene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼1,2-Dichlorobenzene ND
110 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼1,2-Dibromo-3-Chloropropane ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼1,2,4-Trichlorobenzene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼1,2,3-Trichlorobenzene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Hexachlorobutadiene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Naphthalene ND
21 ug/Kg 07/17/12 11:46 07/19/12 19:30 1☼Methyl tert-butyl ether ND
Fluorobenzene (Surr) 99 80 - 120 07/17/12 11:46 07/19/12 19:30 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Toluene-d8 (Surr) 96 07/17/12 11:46 07/19/12 19:30 180 - 120
Ethylbenzene-d10 94 07/17/12 11:46 07/19/12 19:30 170 - 120
4-Bromofluorobenzene (Surr) 89 07/17/12 11:46 07/19/12 19:30 170 - 120
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM)RL MDL
Naphthalene ND 1.7 ug/Kg ☼ 07/23/12 13:38 07/30/12 10:56 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.7 ug/Kg 07/23/12 13:38 07/30/12 10:56 1☼2-Methylnaphthalene ND
1.7 ug/Kg 07/23/12 13:38 07/30/12 10:56 1☼1-Methylnaphthalene ND
1.7 ug/Kg 07/23/12 13:38 07/30/12 10:56 1☼Acenaphthylene 3.6
1.7 ug/Kg 07/23/12 13:38 07/30/12 10:56 1☼Acenaphthene ND
1.7 ug/Kg 07/23/12 13:38 07/30/12 10:56 1☼Fluorene ND
1.7 ug/Kg 07/23/12 13:38 07/30/12 10:56 1☼Phenanthrene 26
1.7 ug/Kg 07/23/12 13:38 07/30/12 10:56 1☼Anthracene 11
1.7 ug/Kg 07/23/12 13:38 07/30/12 10:56 1☼Fluoranthene 110
1.7 ug/Kg 07/23/12 13:38 07/30/12 10:56 1☼Pyrene 220
1.7 ug/Kg 07/23/12 13:38 07/30/12 10:56 1☼Benzo[a]anthracene 110
1.7 ug/Kg 07/23/12 13:38 07/30/12 10:56 1☼Chrysene 150
1.7 ug/Kg 07/23/12 13:38 07/30/12 10:56 1☼Benzo[b]fluoranthene 120
1.7 ug/Kg 07/23/12 13:38 07/30/12 10:56 1☼Benzo[k]fluoranthene 37
1.7 ug/Kg 07/23/12 13:38 07/30/12 10:56 1☼Benzo[a]pyrene 88
1.7 ug/Kg 07/23/12 13:38 07/30/12 10:56 1☼Indeno[1,2,3-cd]pyrene 53
1.7 ug/Kg 07/23/12 13:38 07/30/12 10:56 1☼Dibenz(a,h)anthracene 16
1.7 ug/Kg 07/23/12 13:38 07/30/12 10:56 1☼Benzo[g,h,i]perylene 58
Terphenyl-d14 87 42 - 151 07/23/12 13:38 07/30/12 10:56 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Gasoline Range Organics - (GC)RL MDL
HI Gasoline Range Organic (C6-C12) ND 2.1 mg/Kg ☼ 07/17/12 10:13 07/17/12 22:20 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 100 75 - 131 07/17/12 10:13 07/17/12 22:20 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
HI Diesel Range Organics
(>C12-C24)
42 Y 8.6 mg/Kg ☼ 07/20/12 11:46 07/25/12 21:51 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
17 mg/Kg 07/20/12 11:46 07/25/12 21:51 1☼HI Residual Range Organics
(>C24-C32)
380 Y
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Client Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33932-3Client Sample ID: UW BH 2 1'Matrix: SolidDate Collected: 07/10/12 10:40
Percent Solids: 95.9Date Received: 07/13/12 10:00
o-Terphenyl 91 50 - 150 07/20/12 11:46 07/25/12 21:51 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 6010B - Metals (ICP)RL MDL
Cadmium ND 0.99 mg/Kg ☼ 07/25/12 10:14 07/25/12 22:28 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
3.0 mg/Kg 07/25/12 10:14 07/25/12 22:28 10☼Lead 23
General ChemistryRL RL
Percent Solids 96 0.10 % 07/17/12 18:49 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.10 % 07/17/12 18:49 1Percent Moisture 4.1
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Client Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33932-4Client Sample ID: UW BH 2 7'Matrix: SolidDate Collected: 07/10/12 10:55
Percent Solids: 88.9Date Received: 07/13/12 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Dichlorodifluoromethane ND 16 ug/Kg ☼ 07/17/12 11:46 07/19/12 19:53 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
160 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Chloromethane ND
3.3 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Vinyl chloride ND
58 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Bromomethane ND
160 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Chloroethane ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Trichlorofluoromethane ND
8.2 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼1,1-Dichloroethene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Methylene Chloride ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼trans-1,2-Dichloroethene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼1,1-Dichloroethane ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼2,2-Dichloropropane ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼cis-1,2-Dichloroethene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Chlorobromomethane ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Chloroform ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼1,1,1-Trichloroethane ND
8.2 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Carbon tetrachloride ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼1,1-Dichloropropene ND
6.6 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Benzene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼1,2-Dichloroethane ND
6.6 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Trichloroethene ND
4.9 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼1,2-Dichloropropane ND *
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Dibromomethane ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Dichlorobromomethane ND
6.6 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼cis-1,3-Dichloropropene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Toluene ND
6.6 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼trans-1,3-Dichloropropene ND
4.9 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼1,1,2-Trichloroethane ND
8.2 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Tetrachloroethene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼1,3-Dichloropropane ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Chlorodibromomethane ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Ethylene Dibromide ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Chlorobenzene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Ethylbenzene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼1,1,1,2-Tetrachloroethane ND
4.1 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼1,1,2,2-Tetrachloroethane ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼m-Xylene & p-Xylene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼o-Xylene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Styrene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Bromoform ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Isopropylbenzene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Bromobenzene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼N-Propylbenzene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼1,2,3-Trichloropropane ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼2-Chlorotoluene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼1,3,5-Trimethylbenzene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼4-Chlorotoluene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼tert-Butylbenzene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼1,2,4-Trimethylbenzene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼sec-Butylbenzene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼1,3-Dichlorobenzene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼4-Isopropyltoluene ND
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Client Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33932-4Client Sample ID: UW BH 2 7'Matrix: SolidDate Collected: 07/10/12 10:55
Percent Solids: 88.9Date Received: 07/13/12 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)RL MDL
1,4-Dichlorobenzene ND 16 ug/Kg ☼ 07/17/12 11:46 07/19/12 19:53 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼n-Butylbenzene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼1,2-Dichlorobenzene ND
82 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼1,2-Dibromo-3-Chloropropane ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼1,2,4-Trichlorobenzene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼1,2,3-Trichlorobenzene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Hexachlorobutadiene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Naphthalene ND
16 ug/Kg 07/17/12 11:46 07/19/12 19:53 1☼Methyl tert-butyl ether ND
Fluorobenzene (Surr) 98 80 - 120 07/17/12 11:46 07/19/12 19:53 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Toluene-d8 (Surr) 98 07/17/12 11:46 07/19/12 19:53 180 - 120
Ethylbenzene-d10 95 07/17/12 11:46 07/19/12 19:53 170 - 120
4-Bromofluorobenzene (Surr) 91 07/17/12 11:46 07/19/12 19:53 170 - 120
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM)RL MDL
Naphthalene ND 1.8 ug/Kg ☼ 07/23/12 13:38 07/27/12 18:58 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.8 ug/Kg 07/23/12 13:38 07/27/12 18:58 1☼2-Methylnaphthalene ND
1.8 ug/Kg 07/23/12 13:38 07/27/12 18:58 1☼1-Methylnaphthalene ND
1.8 ug/Kg 07/23/12 13:38 07/27/12 18:58 1☼Acenaphthylene ND
1.8 ug/Kg 07/23/12 13:38 07/27/12 18:58 1☼Acenaphthene ND
1.8 ug/Kg 07/23/12 13:38 07/27/12 18:58 1☼Fluorene ND
1.8 ug/Kg 07/23/12 13:38 07/27/12 18:58 1☼Phenanthrene ND
1.8 ug/Kg 07/23/12 13:38 07/27/12 18:58 1☼Anthracene ND
1.8 ug/Kg 07/23/12 13:38 07/27/12 18:58 1☼Fluoranthene ND
1.8 ug/Kg 07/23/12 13:38 07/27/12 18:58 1☼Pyrene ND
1.8 ug/Kg 07/23/12 13:38 07/27/12 18:58 1☼Benzo[a]anthracene ND
1.8 ug/Kg 07/23/12 13:38 07/27/12 18:58 1☼Chrysene ND
1.8 ug/Kg 07/23/12 13:38 07/27/12 18:58 1☼Benzo[b]fluoranthene 1.9
1.8 ug/Kg 07/23/12 13:38 07/27/12 18:58 1☼Benzo[k]fluoranthene ND
1.8 ug/Kg 07/23/12 13:38 07/27/12 18:58 1☼Benzo[a]pyrene ND
1.8 ug/Kg 07/23/12 13:38 07/27/12 18:58 1☼Indeno[1,2,3-cd]pyrene 2.2
1.8 ug/Kg 07/23/12 13:38 07/27/12 18:58 1☼Dibenz(a,h)anthracene ND
1.8 ug/Kg 07/23/12 13:38 07/27/12 18:58 1☼Benzo[g,h,i]perylene ND
Terphenyl-d14 87 42 - 151 07/23/12 13:38 07/27/12 18:58 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Gasoline Range Organics - (GC)RL MDL
HI Gasoline Range Organic (C6-C12) ND 1.6 mg/Kg ☼ 07/17/12 10:13 07/17/12 22:42 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 99 75 - 131 07/17/12 10:13 07/17/12 22:42 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
HI Diesel Range Organics (>C12-C24) ND 8.4 mg/Kg ☼ 07/20/12 11:46 07/25/12 22:10 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
17 mg/Kg 07/20/12 11:46 07/25/12 22:10 1☼HI Residual Range Organics
(>C24-C32)
ND
TestAmerica SeattlePage 16 of 60 8/9/2012
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Client Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33932-4Client Sample ID: UW BH 2 7'Matrix: SolidDate Collected: 07/10/12 10:55
Percent Solids: 88.9Date Received: 07/13/12 10:00
o-Terphenyl 83 50 - 150 07/20/12 11:46 07/25/12 22:10 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 6010B - Metals (ICP)RL MDL
Cadmium ND 1.0 mg/Kg ☼ 07/25/12 10:14 07/25/12 22:35 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
3.1 mg/Kg 07/25/12 10:14 07/25/12 22:35 10☼Lead ND
General ChemistryRL RL
Percent Solids 89 0.10 % 07/17/12 18:49 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.10 % 07/17/12 18:49 1Percent Moisture 11
TestAmerica SeattlePage 17 of 60 8/9/2012
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Client Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33932-5Client Sample ID: UW BH 3 7'Matrix: SolidDate Collected: 07/10/12 09:30
Percent Solids: 99.0Date Received: 07/13/12 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Dichlorodifluoromethane ND 15 ug/Kg ☼ 07/17/12 11:46 07/19/12 20:16 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
150 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Chloromethane ND
2.9 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Vinyl chloride ND
51 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Bromomethane ND
150 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Chloroethane ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Trichlorofluoromethane ND
7.3 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼1,1-Dichloroethene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Methylene Chloride ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼trans-1,2-Dichloroethene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼1,1-Dichloroethane ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼2,2-Dichloropropane ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼cis-1,2-Dichloroethene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Chlorobromomethane ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Chloroform ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼1,1,1-Trichloroethane ND
7.3 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Carbon tetrachloride ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼1,1-Dichloropropene ND
5.8 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Benzene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼1,2-Dichloroethane ND
5.8 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Trichloroethene ND
4.4 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼1,2-Dichloropropane ND *
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Dibromomethane ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Dichlorobromomethane ND
5.8 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼cis-1,3-Dichloropropene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Toluene ND
5.8 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼trans-1,3-Dichloropropene ND
4.4 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼1,1,2-Trichloroethane ND
7.3 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Tetrachloroethene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼1,3-Dichloropropane ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Chlorodibromomethane ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Ethylene Dibromide ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Chlorobenzene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Ethylbenzene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼1,1,1,2-Tetrachloroethane ND
3.6 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼1,1,2,2-Tetrachloroethane ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼m-Xylene & p-Xylene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼o-Xylene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Styrene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Bromoform ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Isopropylbenzene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Bromobenzene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼N-Propylbenzene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼1,2,3-Trichloropropane ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼2-Chlorotoluene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼1,3,5-Trimethylbenzene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼4-Chlorotoluene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼tert-Butylbenzene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼1,2,4-Trimethylbenzene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼sec-Butylbenzene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼1,3-Dichlorobenzene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼4-Isopropyltoluene ND
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Client Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33932-5Client Sample ID: UW BH 3 7'Matrix: SolidDate Collected: 07/10/12 09:30
Percent Solids: 99.0Date Received: 07/13/12 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)RL MDL
1,4-Dichlorobenzene ND 15 ug/Kg ☼ 07/17/12 11:46 07/19/12 20:16 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼n-Butylbenzene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼1,2-Dichlorobenzene ND
73 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼1,2-Dibromo-3-Chloropropane ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼1,2,4-Trichlorobenzene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼1,2,3-Trichlorobenzene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Hexachlorobutadiene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Naphthalene ND
15 ug/Kg 07/17/12 11:46 07/19/12 20:16 1☼Methyl tert-butyl ether ND
Fluorobenzene (Surr) 97 80 - 120 07/17/12 11:46 07/19/12 20:16 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Toluene-d8 (Surr) 97 07/17/12 11:46 07/19/12 20:16 180 - 120
Ethylbenzene-d10 97 07/17/12 11:46 07/19/12 20:16 170 - 120
4-Bromofluorobenzene (Surr) 91 07/17/12 11:46 07/19/12 20:16 170 - 120
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM)RL MDL
Naphthalene ND 1.6 ug/Kg ☼ 07/23/12 13:38 07/27/12 19:21 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.6 ug/Kg 07/23/12 13:38 07/27/12 19:21 1☼2-Methylnaphthalene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 19:21 1☼1-Methylnaphthalene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 19:21 1☼Acenaphthylene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 19:21 1☼Acenaphthene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 19:21 1☼Fluorene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 19:21 1☼Phenanthrene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 19:21 1☼Anthracene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 19:21 1☼Fluoranthene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 19:21 1☼Pyrene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 19:21 1☼Benzo[a]anthracene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 19:21 1☼Chrysene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 19:21 1☼Benzo[b]fluoranthene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 19:21 1☼Benzo[k]fluoranthene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 19:21 1☼Benzo[a]pyrene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 19:21 1☼Indeno[1,2,3-cd]pyrene 1.9
1.6 ug/Kg 07/23/12 13:38 07/27/12 19:21 1☼Dibenz(a,h)anthracene ND
1.6 ug/Kg 07/23/12 13:38 07/27/12 19:21 1☼Benzo[g,h,i]perylene ND
Terphenyl-d14 89 42 - 151 07/23/12 13:38 07/27/12 19:21 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
HI Diesel Range Organics (>C12-C24) ND 8.3 mg/Kg ☼ 07/20/12 11:46 07/25/12 23:08 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
17 mg/Kg 07/20/12 11:46 07/25/12 23:08 1☼HI Residual Range Organics
(>C24-C32)
ND
o-Terphenyl 89 50 - 150 07/20/12 11:46 07/25/12 23:08 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8081A - Organochlorine Pesticides (GC)RL MDL
Aldrin ND 0.33 ug/Kg ☼ 07/24/12 08:19 07/30/12 16:37 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.33 ug/Kg 07/24/12 08:19 07/30/12 16:37 1☼alpha-BHC ND
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Client Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33932-5Client Sample ID: UW BH 3 7'Matrix: SolidDate Collected: 07/10/12 09:30
Percent Solids: 99.0Date Received: 07/13/12 10:00
Method: 8081A - Organochlorine Pesticides (GC) (Continued)RL MDL
beta-BHC ND 0.33 ug/Kg ☼ 07/24/12 08:19 07/30/12 16:37 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.33 ug/Kg 07/24/12 08:19 07/30/12 16:37 1☼delta-BHC ND
0.33 ug/Kg 07/24/12 08:19 07/30/12 16:37 1☼gamma-BHC (Lindane) ND
0.66 ug/Kg 07/24/12 08:19 07/30/12 16:37 1☼4,4'-DDD ND
0.66 ug/Kg 07/24/12 08:19 07/30/12 16:37 1☼4,4'-DDE ND
0.66 ug/Kg 07/24/12 08:19 07/30/12 16:37 1☼4,4'-DDT ND
0.66 ug/Kg 07/24/12 08:19 07/30/12 16:37 1☼Dieldrin ND
0.33 ug/Kg 07/24/12 08:19 07/30/12 16:37 1☼Endosulfan I ND
0.66 ug/Kg 07/24/12 08:19 07/30/12 16:37 1☼Endosulfan II ND
0.66 ug/Kg 07/24/12 08:19 07/30/12 16:37 1☼Endosulfan sulfate ND
0.66 ug/Kg 07/24/12 08:19 07/30/12 16:37 1☼Endrin ND
0.66 ug/Kg 07/24/12 08:19 07/30/12 16:37 1☼Endrin aldehyde ND
0.66 ug/Kg 07/24/12 08:19 07/30/12 16:37 1☼Heptachlor ND
0.33 ug/Kg 07/24/12 08:19 07/30/12 16:37 1☼Heptachlor epoxide ND
3.3 ug/Kg 07/24/12 08:19 07/30/12 16:37 1☼Methoxychlor ND
0.66 ug/Kg 07/24/12 08:19 07/30/12 16:37 1☼Endrin ketone ND
33 ug/Kg 07/24/12 08:19 07/30/12 16:37 1☼Toxaphene ND
0.33 ug/Kg 07/24/12 08:19 07/30/12 16:37 1☼alpha-Chlordane 2.0
0.33 ug/Kg 07/24/12 08:19 07/30/12 16:37 1☼gamma-Chlordane 1.6
Tetrachloro-m-xylene 66 49 - 123 07/24/12 08:19 07/30/12 16:37 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
DCB Decachlorobiphenyl 85 07/24/12 08:19 07/30/12 16:37 140 - 158
Method: 6010B - Metals (ICP)RL MDL
Arsenic ND 5.9 mg/Kg ☼ 07/25/12 10:14 07/25/12 22:42 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL RL
Percent Solids 99 0.10 % 07/17/12 18:49 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.10 % 07/17/12 18:49 1Percent Moisture 1.0
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Client Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33932-6Client Sample ID: UW BH 4 6'Matrix: SolidDate Collected: 07/10/12 10:20
Percent Solids: 98.3Date Received: 07/13/12 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Dichlorodifluoromethane ND 13 ug/Kg ☼ 07/17/12 11:46 07/19/12 20:39 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
130 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Chloromethane ND
2.6 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Vinyl chloride ND
46 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Bromomethane ND
130 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Chloroethane ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Trichlorofluoromethane ND
6.6 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼1,1-Dichloroethene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Methylene Chloride ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼trans-1,2-Dichloroethene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼1,1-Dichloroethane ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼2,2-Dichloropropane ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼cis-1,2-Dichloroethene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Chlorobromomethane ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Chloroform ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼1,1,1-Trichloroethane ND
6.6 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Carbon tetrachloride ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼1,1-Dichloropropene ND
5.3 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Benzene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼1,2-Dichloroethane ND
5.3 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Trichloroethene ND
3.9 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼1,2-Dichloropropane ND *
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Dibromomethane ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Dichlorobromomethane ND
5.3 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼cis-1,3-Dichloropropene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Toluene ND
5.3 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼trans-1,3-Dichloropropene ND
3.9 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼1,1,2-Trichloroethane ND
6.6 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Tetrachloroethene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼1,3-Dichloropropane ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Chlorodibromomethane ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Ethylene Dibromide ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Chlorobenzene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Ethylbenzene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼1,1,1,2-Tetrachloroethane ND
3.3 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼1,1,2,2-Tetrachloroethane ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼m-Xylene & p-Xylene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼o-Xylene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Styrene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Bromoform ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Isopropylbenzene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Bromobenzene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼N-Propylbenzene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼1,2,3-Trichloropropane ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼2-Chlorotoluene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼1,3,5-Trimethylbenzene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼4-Chlorotoluene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼tert-Butylbenzene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼1,2,4-Trimethylbenzene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼sec-Butylbenzene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼1,3-Dichlorobenzene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼4-Isopropyltoluene ND
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Client Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33932-6Client Sample ID: UW BH 4 6'Matrix: SolidDate Collected: 07/10/12 10:20
Percent Solids: 98.3Date Received: 07/13/12 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)RL MDL
1,4-Dichlorobenzene ND 13 ug/Kg ☼ 07/17/12 11:46 07/19/12 20:39 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼n-Butylbenzene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼1,2-Dichlorobenzene ND
66 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼1,2-Dibromo-3-Chloropropane ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼1,2,4-Trichlorobenzene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼1,2,3-Trichlorobenzene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Hexachlorobutadiene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Naphthalene ND
13 ug/Kg 07/17/12 11:46 07/19/12 20:39 1☼Methyl tert-butyl ether ND
Fluorobenzene (Surr) 98 80 - 120 07/17/12 11:46 07/19/12 20:39 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Toluene-d8 (Surr) 97 07/17/12 11:46 07/19/12 20:39 180 - 120
Ethylbenzene-d10 96 07/17/12 11:46 07/19/12 20:39 170 - 120
4-Bromofluorobenzene (Surr) 93 07/17/12 11:46 07/19/12 20:39 170 - 120
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM)RL MDL
Naphthalene ND 1.7 ug/Kg ☼ 07/23/12 13:38 07/30/12 12:47 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.7 ug/Kg 07/23/12 13:38 07/30/12 12:47 1☼2-Methylnaphthalene ND
1.7 ug/Kg 07/23/12 13:38 07/30/12 12:47 1☼1-Methylnaphthalene ND
1.7 ug/Kg 07/23/12 13:38 07/30/12 12:47 1☼Acenaphthylene ND
1.7 ug/Kg 07/23/12 13:38 07/30/12 12:47 1☼Acenaphthene ND
1.7 ug/Kg 07/23/12 13:38 07/30/12 12:47 1☼Fluorene ND
1.7 ug/Kg 07/23/12 13:38 07/30/12 12:47 1☼Phenanthrene 3.9
1.7 ug/Kg 07/23/12 13:38 07/30/12 12:47 1☼Anthracene ND
1.7 ug/Kg 07/23/12 13:38 07/30/12 12:47 1☼Fluoranthene 6.3
1.7 ug/Kg 07/23/12 13:38 07/30/12 12:47 1☼Pyrene 6.8
1.7 ug/Kg 07/23/12 13:38 07/30/12 12:47 1☼Benzo[a]anthracene 2.4
1.7 ug/Kg 07/23/12 13:38 07/30/12 12:47 1☼Chrysene 7.3
1.7 ug/Kg 07/23/12 13:38 07/30/12 12:47 1☼Benzo[b]fluoranthene 6.8
1.7 ug/Kg 07/23/12 13:38 07/30/12 12:47 1☼Benzo[k]fluoranthene ND
1.7 ug/Kg 07/23/12 13:38 07/30/12 12:47 1☼Benzo[a]pyrene 4.1
1.7 ug/Kg 07/23/12 13:38 07/30/12 12:47 1☼Indeno[1,2,3-cd]pyrene 5.1
1.7 ug/Kg 07/23/12 13:38 07/30/12 12:47 1☼Dibenz(a,h)anthracene ND
1.7 ug/Kg 07/23/12 13:38 07/30/12 12:47 1☼Benzo[g,h,i]perylene 5.7
Terphenyl-d14 84 42 - 151 07/23/12 13:38 07/30/12 12:47 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
HI Diesel Range Organics
(>C12-C24)
11 Y 8.4 mg/Kg ☼ 07/20/12 11:46 07/25/12 23:27 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
17 mg/Kg 07/20/12 11:46 07/25/12 23:27 1☼HI Residual Range Organics
(>C24-C32)
86
o-Terphenyl 92 50 - 150 07/20/12 11:46 07/25/12 23:27 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8081A - Organochlorine Pesticides (GC)RL MDL
Aldrin ND 3.3 ug/Kg ☼ 07/24/12 08:19 07/30/12 17:07 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica SeattlePage 22 of 60 8/9/2012
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Client Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33932-6Client Sample ID: UW BH 4 6'Matrix: SolidDate Collected: 07/10/12 10:20
Percent Solids: 98.3Date Received: 07/13/12 10:00
Method: 8081A - Organochlorine Pesticides (GC) (Continued)RL MDL
alpha-BHC ND 3.3 ug/Kg ☼ 07/24/12 08:19 07/30/12 17:07 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
3.3 ug/Kg 07/24/12 08:19 07/30/12 17:07 10☼beta-BHC ND
3.3 ug/Kg 07/24/12 08:19 07/30/12 17:07 10☼delta-BHC ND
3.3 ug/Kg 07/24/12 08:19 07/30/12 17:07 10☼gamma-BHC (Lindane) ND
6.6 ug/Kg 07/24/12 08:19 07/30/12 17:07 10☼4,4'-DDD ND
6.6 ug/Kg 07/24/12 08:19 07/30/12 17:07 10☼4,4'-DDE ND
6.6 ug/Kg 07/24/12 08:19 07/30/12 17:07 10☼4,4'-DDT ND
6.6 ug/Kg 07/24/12 08:19 07/30/12 17:07 10☼Dieldrin ND
3.3 ug/Kg 07/24/12 08:19 07/30/12 17:07 10☼Endosulfan I ND
6.6 ug/Kg 07/24/12 08:19 07/30/12 17:07 10☼Endosulfan II ND
6.6 ug/Kg 07/24/12 08:19 07/30/12 17:07 10☼Endosulfan sulfate ND
6.6 ug/Kg 07/24/12 08:19 07/30/12 17:07 10☼Endrin ND
6.6 ug/Kg 07/24/12 08:19 07/30/12 17:07 10☼Endrin aldehyde ND
6.6 ug/Kg 07/24/12 08:19 07/30/12 17:07 10☼Heptachlor ND
3.3 ug/Kg 07/24/12 08:19 07/30/12 17:07 10☼Heptachlor epoxide ND
33 ug/Kg 07/24/12 08:19 07/30/12 17:07 10☼Methoxychlor ND
6.6 ug/Kg 07/24/12 08:19 07/30/12 17:07 10☼Endrin ketone ND
330 ug/Kg 07/24/12 08:19 07/30/12 17:07 10☼Toxaphene ND
3.3 ug/Kg 07/24/12 08:19 07/30/12 17:07 10☼alpha-Chlordane ND
3.3 ug/Kg 07/24/12 08:19 07/30/12 17:07 10☼gamma-Chlordane ND
Tetrachloro-m-xylene 47 X 49 - 123 07/24/12 08:19 07/30/12 17:07 10
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
DCB Decachlorobiphenyl 36 X 07/24/12 08:19 07/30/12 17:07 1040 - 158
Method: 6010B - Metals (ICP)RL MDL
Arsenic ND 6.0 mg/Kg ☼ 07/25/12 10:14 07/25/12 23:01 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL RL
Percent Solids 98 0.10 % 07/17/12 18:49 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.10 % 07/17/12 18:49 1Percent Moisture 1.7
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Client Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33932-7Client Sample ID: UW MI-1Matrix: SolidDate Collected: 07/10/12 12:45
Percent Solids: 94.7Date Received: 07/13/12 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS) - RARL MDL
Dichlorodifluoromethane ND 52 ug/Kg ☼ 07/17/12 11:46 07/22/12 21:44 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
520 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Chloromethane ND
10 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Vinyl chloride ND
180 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Bromomethane ND
520 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Chloroethane ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Trichlorofluoromethane ND
26 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼1,1-Dichloroethene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Methylene Chloride ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼trans-1,2-Dichloroethene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼1,1-Dichloroethane ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼2,2-Dichloropropane ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼cis-1,2-Dichloroethene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Chlorobromomethane ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Chloroform ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼1,1,1-Trichloroethane ND
26 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Carbon tetrachloride ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼1,1-Dichloropropene ND
21 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Benzene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼1,2-Dichloroethane ND
21 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Trichloroethene ND
16 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼1,2-Dichloropropane ND *
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Dibromomethane ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Dichlorobromomethane ND
21 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼cis-1,3-Dichloropropene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Toluene ND
21 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼trans-1,3-Dichloropropene ND
16 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼1,1,2-Trichloroethane ND
26 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Tetrachloroethene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼1,3-Dichloropropane ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Chlorodibromomethane ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Ethylene Dibromide ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Chlorobenzene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Ethylbenzene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼1,1,1,2-Tetrachloroethane ND
13 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼1,1,2,2-Tetrachloroethane ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼m-Xylene & p-Xylene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼o-Xylene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Styrene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Bromoform ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Isopropylbenzene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Bromobenzene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼N-Propylbenzene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼1,2,3-Trichloropropane ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼2-Chlorotoluene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼1,3,5-Trimethylbenzene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼4-Chlorotoluene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼tert-Butylbenzene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼1,2,4-Trimethylbenzene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼sec-Butylbenzene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼1,3-Dichlorobenzene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼4-Isopropyltoluene ND
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Client Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33932-7Client Sample ID: UW MI-1Matrix: SolidDate Collected: 07/10/12 12:45
Percent Solids: 94.7Date Received: 07/13/12 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS) - RA (Continued)RL MDL
1,4-Dichlorobenzene ND 52 ug/Kg ☼ 07/17/12 11:46 07/22/12 21:44 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼n-Butylbenzene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼1,2-Dichlorobenzene ND
260 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼1,2-Dibromo-3-Chloropropane ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼1,2,4-Trichlorobenzene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼1,2,3-Trichlorobenzene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Hexachlorobutadiene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Naphthalene ND
52 ug/Kg 07/17/12 11:46 07/22/12 21:44 1☼Methyl tert-butyl ether ND
Fluorobenzene (Surr) 97 80 - 120 07/17/12 11:46 07/22/12 21:44 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Toluene-d8 (Surr) 95 07/17/12 11:46 07/22/12 21:44 180 - 120
Ethylbenzene-d10 94 07/17/12 11:46 07/22/12 21:44 170 - 120
4-Bromofluorobenzene (Surr) 91 07/17/12 11:46 07/22/12 21:44 170 - 120
Trifluorotoluene (Surr) 07/17/12 11:46 07/22/12 21:44 1
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM)RL MDL
Naphthalene 3.0 1.7 ug/Kg ☼ 07/23/12 13:38 07/30/12 11:40 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.7 ug/Kg 07/23/12 13:38 07/30/12 11:40 1☼2-Methylnaphthalene ND
1.7 ug/Kg 07/23/12 13:38 07/30/12 11:40 1☼1-Methylnaphthalene ND
1.7 ug/Kg 07/23/12 13:38 07/30/12 11:40 1☼Acenaphthylene 6.8
1.7 ug/Kg 07/23/12 13:38 07/30/12 11:40 1☼Acenaphthene 7.7
1.7 ug/Kg 07/23/12 13:38 07/30/12 11:40 1☼Fluorene 3.8
1.7 ug/Kg 07/23/12 13:38 07/30/12 11:40 1☼Phenanthrene 110
1.7 ug/Kg 07/23/12 13:38 07/30/12 11:40 1☼Anthracene 39
1.7 ug/Kg 07/23/12 13:38 07/30/12 11:40 1☼Fluoranthene 380
1.7 ug/Kg 07/23/12 13:38 07/30/12 11:40 1☼Pyrene 590
1.7 ug/Kg 07/23/12 13:38 07/30/12 11:40 1☼Benzo[a]anthracene 300
1.7 ug/Kg 07/23/12 13:38 07/30/12 11:40 1☼Chrysene 300
1.7 ug/Kg 07/23/12 13:38 07/30/12 11:40 1☼Benzo[b]fluoranthene 290
1.7 ug/Kg 07/23/12 13:38 07/30/12 11:40 1☼Benzo[k]fluoranthene 120
1.7 ug/Kg 07/23/12 13:38 07/30/12 11:40 1☼Benzo[a]pyrene 220
1.7 ug/Kg 07/23/12 13:38 07/30/12 11:40 1☼Indeno[1,2,3-cd]pyrene 140
1.7 ug/Kg 07/23/12 13:38 07/30/12 11:40 1☼Dibenz(a,h)anthracene 36
1.7 ug/Kg 07/23/12 13:38 07/30/12 11:40 1☼Benzo[g,h,i]perylene 120
Terphenyl-d14 90 42 - 151 07/23/12 13:38 07/30/12 11:40 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Gasoline Range Organics - (GC)RL MDL
HI Gasoline Range Organic (C6-C12) ND 5.2 mg/Kg ☼ 07/17/12 10:13 07/17/12 23:04 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 99 75 - 131 07/17/12 10:13 07/17/12 23:04 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
HI Diesel Range Organics
(>C12-C24)
57 Y 8.0 mg/Kg ☼ 07/20/12 11:46 07/25/12 23:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33932-7Client Sample ID: UW MI-1Matrix: SolidDate Collected: 07/10/12 12:45
Percent Solids: 94.7Date Received: 07/13/12 10:00
Method: 8015B - Diesel Range Organics (DRO) (GC) (Continued)RL MDL
HI Residual Range Organics
(>C24-C32)
490 Y 16 mg/Kg ☼ 07/20/12 11:46 07/25/12 23:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl 93 50 - 150 07/20/12 11:46 07/25/12 23:46 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 6010B - Metals (ICP)RL MDL
Cadmium ND 0.98 mg/Kg ☼ 07/25/12 10:14 07/25/12 23:08 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.9 mg/Kg 07/25/12 10:14 07/25/12 23:08 10☼Lead 93
General ChemistryRL RL
Percent Solids 95 0.10 % 07/17/12 18:49 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.10 % 07/17/12 18:49 1Percent Moisture 5.3
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Client Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33932-8Client Sample ID: UW MI-2Matrix: SolidDate Collected: 07/10/12 14:50
Percent Solids: 95.9Date Received: 07/13/12 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS) - RARL MDL
Dichlorodifluoromethane ND 61 ug/Kg ☼ 07/17/12 11:46 07/22/12 22:06 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
610 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Chloromethane ND
12 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Vinyl chloride ND
210 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Bromomethane ND
610 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Chloroethane ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Trichlorofluoromethane ND
31 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼1,1-Dichloroethene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Methylene Chloride ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼trans-1,2-Dichloroethene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼1,1-Dichloroethane ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼2,2-Dichloropropane ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼cis-1,2-Dichloroethene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Chlorobromomethane ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Chloroform ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼1,1,1-Trichloroethane ND
31 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Carbon tetrachloride ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼1,1-Dichloropropene ND
24 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Benzene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼1,2-Dichloroethane ND
24 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Trichloroethene ND
18 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼1,2-Dichloropropane ND *
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Dibromomethane ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Dichlorobromomethane ND
24 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼cis-1,3-Dichloropropene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Toluene ND
24 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼trans-1,3-Dichloropropene ND
18 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼1,1,2-Trichloroethane ND
31 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Tetrachloroethene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼1,3-Dichloropropane ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Chlorodibromomethane ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Ethylene Dibromide ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Chlorobenzene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Ethylbenzene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼1,1,1,2-Tetrachloroethane ND
15 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼1,1,2,2-Tetrachloroethane ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼m-Xylene & p-Xylene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼o-Xylene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Styrene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Bromoform ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Isopropylbenzene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Bromobenzene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼N-Propylbenzene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼1,2,3-Trichloropropane ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼2-Chlorotoluene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼1,3,5-Trimethylbenzene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼4-Chlorotoluene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼tert-Butylbenzene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼1,2,4-Trimethylbenzene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼sec-Butylbenzene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼1,3-Dichlorobenzene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼4-Isopropyltoluene ND
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Client Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33932-8Client Sample ID: UW MI-2Matrix: SolidDate Collected: 07/10/12 14:50
Percent Solids: 95.9Date Received: 07/13/12 10:00
Method: 8260B - Volatile Organic Compounds (GC/MS) - RA (Continued)RL MDL
1,4-Dichlorobenzene ND 61 ug/Kg ☼ 07/17/12 11:46 07/22/12 22:06 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼n-Butylbenzene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼1,2-Dichlorobenzene ND
310 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼1,2-Dibromo-3-Chloropropane ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼1,2,4-Trichlorobenzene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼1,2,3-Trichlorobenzene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Hexachlorobutadiene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Naphthalene ND
61 ug/Kg 07/17/12 11:46 07/22/12 22:06 1☼Methyl tert-butyl ether ND
Fluorobenzene (Surr) 96 80 - 120 07/17/12 11:46 07/22/12 22:06 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Toluene-d8 (Surr) 95 07/17/12 11:46 07/22/12 22:06 180 - 120
Ethylbenzene-d10 95 07/17/12 11:46 07/22/12 22:06 170 - 120
4-Bromofluorobenzene (Surr) 92 07/17/12 11:46 07/22/12 22:06 170 - 120
Trifluorotoluene (Surr) 07/17/12 11:46 07/22/12 22:06 1
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM)RL MDL
Naphthalene 3.7 1.6 ug/Kg ☼ 07/23/12 13:38 07/30/12 12:02 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.6 ug/Kg 07/23/12 13:38 07/30/12 12:02 1☼2-Methylnaphthalene 4.0
1.6 ug/Kg 07/23/12 13:38 07/30/12 12:02 1☼1-Methylnaphthalene 4.6
1.6 ug/Kg 07/23/12 13:38 07/30/12 12:02 1☼Acenaphthylene 42
1.6 ug/Kg 07/23/12 13:38 07/30/12 12:02 1☼Acenaphthene 6.6
1.6 ug/Kg 07/23/12 13:38 07/30/12 12:02 1☼Fluorene 4.9
1.6 ug/Kg 07/23/12 13:38 07/30/12 12:02 1☼Phenanthrene 120
1.6 ug/Kg 07/23/12 13:38 07/30/12 12:02 1☼Anthracene 50
1.6 ug/Kg 07/23/12 13:38 07/30/12 12:02 1☼Fluoranthene 460
1.6 ug/Kg 07/23/12 13:38 07/30/12 12:02 1☼Pyrene 720
1.6 ug/Kg 07/23/12 13:38 07/30/12 12:02 1☼Benzo[a]anthracene 380
1.6 ug/Kg 07/23/12 13:38 07/30/12 12:02 1☼Chrysene 430
1.6 ug/Kg 07/23/12 13:38 07/30/12 12:02 1☼Benzo[b]fluoranthene 440
1.6 ug/Kg 07/23/12 13:38 07/30/12 12:02 1☼Benzo[k]fluoranthene 140
1.6 ug/Kg 07/23/12 13:38 07/30/12 12:02 1☼Benzo[a]pyrene 310
1.6 ug/Kg 07/23/12 13:38 07/30/12 12:02 1☼Indeno[1,2,3-cd]pyrene 210
1.6 ug/Kg 07/23/12 13:38 07/30/12 12:02 1☼Dibenz(a,h)anthracene 47
1.6 ug/Kg 07/23/12 13:38 07/30/12 12:02 1☼Benzo[g,h,i]perylene 210
Terphenyl-d14 94 42 - 151 07/23/12 13:38 07/30/12 12:02 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Gasoline Range Organics - (GC)RL MDL
HI Gasoline Range Organic (C6-C12) ND 6.1 mg/Kg ☼ 07/17/12 10:13 07/17/12 23:27 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 97 75 - 131 07/17/12 10:13 07/17/12 23:27 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
HI Diesel Range Organics
(>C12-C24)
85 8.6 mg/Kg ☼ 07/20/12 11:46 07/26/12 00:06 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33932-8Client Sample ID: UW MI-2Matrix: SolidDate Collected: 07/10/12 14:50
Percent Solids: 95.9Date Received: 07/13/12 10:00
Method: 8015B - Diesel Range Organics (DRO) (GC) (Continued)RL MDL
HI Residual Range Organics
(>C24-C32)
610 17 mg/Kg ☼ 07/20/12 11:46 07/26/12 00:06 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl 96 50 - 150 07/20/12 11:46 07/26/12 00:06 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 6010B - Metals (ICP)RL MDL
Cadmium ND 1.0 mg/Kg ☼ 07/25/12 10:14 07/25/12 23:14 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
3.0 mg/Kg 07/25/12 10:14 07/25/12 23:14 10☼Lead 130
General ChemistryRL RL
Percent Solids 96 0.10 % 07/17/12 18:49 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.10 % 07/17/12 18:49 1Percent Moisture 4.1
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QC Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 580-115488/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 115678 Prep Batch: 115488
RL MDL
Dichlorodifluoromethane ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 400 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Chloromethane
ND 8.0 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Vinyl chloride
ND 140 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Bromomethane
ND 400 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Chloroethane
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Trichlorofluoromethane
ND 20 ug/Kg 07/17/12 11:46 07/19/12 10:01 11,1-Dichloroethene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Methylene Chloride
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1trans-1,2-Dichloroethene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 11,1-Dichloroethane
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 12,2-Dichloropropane
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1cis-1,2-Dichloroethene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Chlorobromomethane
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Chloroform
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 11,1,1-Trichloroethane
ND 20 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Carbon tetrachloride
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 11,1-Dichloropropene
ND 16 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Benzene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 11,2-Dichloroethane
ND 16 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Trichloroethene
ND 12 ug/Kg 07/17/12 11:46 07/19/12 10:01 11,2-Dichloropropane
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Dibromomethane
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Dichlorobromomethane
ND 16 ug/Kg 07/17/12 11:46 07/19/12 10:01 1cis-1,3-Dichloropropene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Toluene
ND 16 ug/Kg 07/17/12 11:46 07/19/12 10:01 1trans-1,3-Dichloropropene
ND 12 ug/Kg 07/17/12 11:46 07/19/12 10:01 11,1,2-Trichloroethane
ND 20 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Tetrachloroethene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 11,3-Dichloropropane
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Chlorodibromomethane
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Ethylene Dibromide
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Chlorobenzene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Ethylbenzene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 11,1,1,2-Tetrachloroethane
ND 10 ug/Kg 07/17/12 11:46 07/19/12 10:01 11,1,2,2-Tetrachloroethane
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1m-Xylene & p-Xylene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1o-Xylene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Styrene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Bromoform
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Isopropylbenzene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Bromobenzene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1N-Propylbenzene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 11,2,3-Trichloropropane
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 12-Chlorotoluene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 11,3,5-Trimethylbenzene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 14-Chlorotoluene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1tert-Butylbenzene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 11,2,4-Trimethylbenzene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1sec-Butylbenzene
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QC Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 580-115488/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 115678 Prep Batch: 115488
RL MDL
1,3-Dichlorobenzene ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 14-Isopropyltoluene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 11,4-Dichlorobenzene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1n-Butylbenzene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 11,2-Dichlorobenzene
ND 200 ug/Kg 07/17/12 11:46 07/19/12 10:01 11,2-Dibromo-3-Chloropropane
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 11,2,4-Trichlorobenzene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 11,2,3-Trichlorobenzene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Hexachlorobutadiene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Naphthalene
ND 40 ug/Kg 07/17/12 11:46 07/19/12 10:01 1Methyl tert-butyl ether
Fluorobenzene (Surr) 95 80 - 120 07/19/12 10:01 1
MB MB
Surrogate
07/17/12 11:46
Dil FacPrepared AnalyzedQualifier Limits%Recovery
93 07/17/12 11:46 07/19/12 10:01 1Toluene-d8 (Surr) 80 - 120
95 07/17/12 11:46 07/19/12 10:01 1Ethylbenzene-d10 70 - 120
89 07/17/12 11:46 07/19/12 10:01 14-Bromofluorobenzene (Surr) 70 - 120
109 07/17/12 11:46 07/19/12 10:01 1Trifluorotoluene (Surr) 65 - 140
Client Sample ID: Method BlankLab Sample ID: MB 580-115488/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 115886 Prep Batch: 115488
RL MDL
Dichlorodifluoromethane ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 400 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Chloromethane
ND 8.0 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Vinyl chloride
ND 140 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Bromomethane
ND 400 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Chloroethane
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Trichlorofluoromethane
ND 20 ug/Kg 07/17/12 11:46 07/22/12 21:21 11,1-Dichloroethene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Methylene Chloride
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1trans-1,2-Dichloroethene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 11,1-Dichloroethane
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 12,2-Dichloropropane
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1cis-1,2-Dichloroethene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Chlorobromomethane
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Chloroform
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 11,1,1-Trichloroethane
ND 20 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Carbon tetrachloride
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 11,1-Dichloropropene
ND 16 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Benzene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 11,2-Dichloroethane
ND 16 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Trichloroethene
ND 12 ug/Kg 07/17/12 11:46 07/22/12 21:21 11,2-Dichloropropane
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Dibromomethane
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Dichlorobromomethane
ND 16 ug/Kg 07/17/12 11:46 07/22/12 21:21 1cis-1,3-Dichloropropene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Toluene
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QC Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 580-115488/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 115886 Prep Batch: 115488
RL MDL
trans-1,3-Dichloropropene ND 16 ug/Kg 07/17/12 11:46 07/22/12 21:21 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 12 ug/Kg 07/17/12 11:46 07/22/12 21:21 11,1,2-Trichloroethane
ND 20 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Tetrachloroethene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 11,3-Dichloropropane
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Chlorodibromomethane
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Ethylene Dibromide
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Chlorobenzene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Ethylbenzene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 11,1,1,2-Tetrachloroethane
ND 10 ug/Kg 07/17/12 11:46 07/22/12 21:21 11,1,2,2-Tetrachloroethane
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1m-Xylene & p-Xylene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1o-Xylene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Styrene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Bromoform
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Isopropylbenzene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Bromobenzene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1N-Propylbenzene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 11,2,3-Trichloropropane
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 12-Chlorotoluene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 11,3,5-Trimethylbenzene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 14-Chlorotoluene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1tert-Butylbenzene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 11,2,4-Trimethylbenzene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1sec-Butylbenzene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 11,3-Dichlorobenzene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 14-Isopropyltoluene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 11,4-Dichlorobenzene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1n-Butylbenzene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 11,2-Dichlorobenzene
ND 200 ug/Kg 07/17/12 11:46 07/22/12 21:21 11,2-Dibromo-3-Chloropropane
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 11,2,4-Trichlorobenzene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 11,2,3-Trichlorobenzene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Hexachlorobutadiene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Naphthalene
ND 40 ug/Kg 07/17/12 11:46 07/22/12 21:21 1Methyl tert-butyl ether
Fluorobenzene (Surr) 96 80 - 120 07/22/12 21:21 1
MB MB
Surrogate
07/17/12 11:46
Dil FacPrepared AnalyzedQualifier Limits%Recovery
95 07/17/12 11:46 07/22/12 21:21 1Toluene-d8 (Surr) 80 - 120
94 07/17/12 11:46 07/22/12 21:21 1Ethylbenzene-d10 70 - 120
92 07/17/12 11:46 07/22/12 21:21 14-Bromofluorobenzene (Surr) 70 - 120
111 07/17/12 11:46 07/22/12 21:21 1Trifluorotoluene (Surr) 65 - 140
Client Sample ID: Lab Control SampleLab Sample ID: LCS 580-115488/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 115678 Prep Batch: 115488
Dichlorodifluoromethane 801 627 ug/Kg 78 35 - 135
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
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QC Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 580-115488/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 115678 Prep Batch: 115488
Chloromethane 799 640 ug/Kg 80 50 - 130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Vinyl chloride 800 760 ug/Kg 95 60 - 125
Bromomethane 799 639 ug/Kg 80 30 - 160
Chloroethane 800 709 ug/Kg 89 40 - 155
Trichlorofluoromethane 800 751 ug/Kg 94 25 - 185
1,1-Dichloroethene 801 892 ug/Kg 111 65 - 135
Methylene Chloride 800 830 ug/Kg 104 55 - 140
trans-1,2-Dichloroethene 801 872 ug/Kg 109 65 - 135
1,1-Dichloroethane 800 850 ug/Kg 106 75 - 125
2,2-Dichloropropane 799 719 ug/Kg 90 65 - 135
cis-1,2-Dichloroethene 801 855 ug/Kg 107 65 - 125
Chlorobromomethane 802 834 ug/Kg 104 70 - 125
Chloroform 800 757 ug/Kg 95 70 - 125
1,1,1-Trichloroethane 800 760 ug/Kg 95 70 - 135
Carbon tetrachloride 803 747 ug/Kg 93 65 - 135
1,1-Dichloropropene 802 794 ug/Kg 99 70 - 135
Benzene 799 787 ug/Kg 98 75 - 125
1,2-Dichloroethane 801 757 ug/Kg 95 70 - 135
Trichloroethene 812 829 ug/Kg 102 75 - 125
1,2-Dichloropropane 800 984 * ug/Kg 123 70 - 120
Dibromomethane 802 781 ug/Kg 97 75 - 130
Dichlorobromomethane 809 675 ug/Kg 83 70 - 130
cis-1,3-Dichloropropene 790 683 ug/Kg 86 70 - 125
Toluene 801 782 ug/Kg 98 70 - 125
trans-1,3-Dichloropropene 812 659 ug/Kg 81 65 - 125
1,1,2-Trichloroethane 802 745 ug/Kg 93 60 - 125
Tetrachloroethene 800 818 ug/Kg 102 65 - 140
1,3-Dichloropropane 801 733 ug/Kg 92 75 - 125
Chlorodibromomethane 810 640 ug/Kg 79 65 - 130
Ethylene Dibromide 802 746 ug/Kg 93 70 - 125
Chlorobenzene 800 753 ug/Kg 94 75 - 125
Ethylbenzene 800 783 ug/Kg 98 75 - 125
1,1,1,2-Tetrachloroethane 802 811 ug/Kg 101 75 - 125
1,1,2,2-Tetrachloroethane 799 634 ug/Kg 79 55 - 130
m-Xylene & p-Xylene 1600 1610 ug/Kg 100 80 - 125
o-Xylene 802 807 ug/Kg 101 75 - 125
Styrene 802 830 ug/Kg 103 75 - 125
Bromoform 800 643 ug/Kg 80 55 - 135
Isopropylbenzene 802 831 ug/Kg 104 75 - 130
Bromobenzene 801 728 ug/Kg 91 65 - 120
N-Propylbenzene 800 808 ug/Kg 101 65 - 135
1,2,3-Trichloropropane 802 745 ug/Kg 93 65 - 130
2-Chlorotoluene 801 775 ug/Kg 97 70 - 130
1,3,5-Trimethylbenzene 799 802 ug/Kg 100 65 - 135
4-Chlorotoluene 802 767 ug/Kg 96 75 - 125
tert-Butylbenzene 802 822 ug/Kg 103 65 - 130
1,2,4-Trimethylbenzene 800 819 ug/Kg 102 65 - 135
sec-Butylbenzene 800 827 ug/Kg 103 65 - 130
1,3-Dichlorobenzene 801 725 ug/Kg 91 70 - 125
4-Isopropyltoluene 800 787 ug/Kg 98 75 - 135
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QC Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 580-115488/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 115678 Prep Batch: 115488
1,4-Dichlorobenzene 801 689 ug/Kg 86 70 - 125
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
n-Butylbenzene 800 802 ug/Kg 100 65 - 140
1,2-Dichlorobenzene 800 687 ug/Kg 86 75 - 120
1,2-Dibromo-3-Chloropropane 801 620 ug/Kg 77 40 - 135
1,2,4-Trichlorobenzene 802 540 ug/Kg 67 65 - 130
1,2,3-Trichlorobenzene 800 495 ug/Kg 62 60 - 135
Hexachlorobutadiene 802 704 ug/Kg 88 55 - 140
Naphthalene 800 623 ug/Kg 78 40 - 125
Fluorobenzene (Surr) 80 - 120
Surrogate
100
LCS LCS
Qualifier Limits%Recovery
102Toluene-d8 (Surr) 80 - 120
100Ethylbenzene-d10 70 - 120
1024-Bromofluorobenzene (Surr) 70 - 120
103Trifluorotoluene (Surr) 65 - 140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 580-115488/17-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 115678 Prep Batch: 115488
Dichlorodifluoromethane 801 599 ug/Kg 75 35 - 135 5 30
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Chloromethane 799 635 ug/Kg 79 50 - 130 1 30
Vinyl chloride 800 766 ug/Kg 96 60 - 125 1 30
Bromomethane 799 691 ug/Kg 86 30 - 160 8 30
Chloroethane 800 723 ug/Kg 90 40 - 155 2 30
Trichlorofluoromethane 800 703 ug/Kg 88 25 - 185 7 30
1,1-Dichloroethene 801 828 ug/Kg 103 65 - 135 7 30
Methylene Chloride 800 792 ug/Kg 99 55 - 140 5 30
trans-1,2-Dichloroethene 801 850 ug/Kg 106 65 - 135 3 30
1,1-Dichloroethane 800 825 ug/Kg 103 75 - 125 3 30
2,2-Dichloropropane 799 760 ug/Kg 95 65 - 135 5 30
cis-1,2-Dichloroethene 801 849 ug/Kg 106 65 - 125 1 30
Chlorobromomethane 802 835 ug/Kg 104 70 - 125 0 30
Chloroform 800 745 ug/Kg 93 70 - 125 2 30
1,1,1-Trichloroethane 800 731 ug/Kg 91 70 - 135 4 30
Carbon tetrachloride 803 740 ug/Kg 92 65 - 135 1 30
1,1-Dichloropropene 802 793 ug/Kg 99 70 - 135 0 30
Benzene 799 778 ug/Kg 97 75 - 125 1 30
1,2-Dichloroethane 801 758 ug/Kg 95 70 - 135 0 30
Trichloroethene 812 833 ug/Kg 103 75 - 125 1 30
1,2-Dichloropropane 800 973 * ug/Kg 122 70 - 120 1 30
Dibromomethane 802 808 ug/Kg 101 75 - 130 3 30
Dichlorobromomethane 809 669 ug/Kg 83 70 - 130 1 30
cis-1,3-Dichloropropene 790 684 ug/Kg 87 70 - 125 0 30
Toluene 801 780 ug/Kg 97 70 - 125 0 30
trans-1,3-Dichloropropene 812 679 ug/Kg 84 65 - 125 3 30
1,1,2-Trichloroethane 802 760 ug/Kg 95 60 - 125 2 30
Tetrachloroethene 800 828 ug/Kg 103 65 - 140 1 30
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QC Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 580-115488/17-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 115678 Prep Batch: 115488
1,3-Dichloropropane 801 771 ug/Kg 96 75 - 125 5 30
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Chlorodibromomethane 810 661 ug/Kg 82 65 - 130 3 30
Ethylene Dibromide 802 788 ug/Kg 98 70 - 125 5 30
Chlorobenzene 800 742 ug/Kg 93 75 - 125 1 30
Ethylbenzene 800 770 ug/Kg 96 75 - 125 2 30
1,1,1,2-Tetrachloroethane 802 785 ug/Kg 98 75 - 125 3 30
1,1,2,2-Tetrachloroethane 799 660 ug/Kg 83 55 - 130 4 30
m-Xylene & p-Xylene 1600 1570 ug/Kg 98 80 - 125 3 30
o-Xylene 802 777 ug/Kg 97 75 - 125 4 30
Styrene 802 822 ug/Kg 103 75 - 125 1 30
Bromoform 800 656 ug/Kg 82 55 - 135 2 30
Isopropylbenzene 802 806 ug/Kg 100 75 - 130 3 30
Bromobenzene 801 716 ug/Kg 89 65 - 120 2 30
N-Propylbenzene 800 789 ug/Kg 99 65 - 135 2 30
1,2,3-Trichloropropane 802 776 ug/Kg 97 65 - 130 4 30
2-Chlorotoluene 801 761 ug/Kg 95 70 - 130 2 30
1,3,5-Trimethylbenzene 799 787 ug/Kg 98 65 - 135 2 30
4-Chlorotoluene 802 749 ug/Kg 93 75 - 125 2 30
tert-Butylbenzene 802 807 ug/Kg 101 65 - 130 2 30
1,2,4-Trimethylbenzene 800 798 ug/Kg 100 65 - 135 3 30
sec-Butylbenzene 800 813 ug/Kg 102 65 - 130 2 30
1,3-Dichlorobenzene 801 720 ug/Kg 90 70 - 125 1 30
4-Isopropyltoluene 800 772 ug/Kg 97 75 - 135 2 30
1,4-Dichlorobenzene 801 680 ug/Kg 85 70 - 125 1 30
n-Butylbenzene 800 800 ug/Kg 100 65 - 140 0 30
1,2-Dichlorobenzene 800 698 ug/Kg 87 75 - 120 1 30
1,2-Dibromo-3-Chloropropane 801 698 ug/Kg 87 40 - 135 12 30
1,2,4-Trichlorobenzene 802 566 ug/Kg 71 65 - 130 5 30
1,2,3-Trichlorobenzene 800 562 ug/Kg 70 60 - 135 13 30
Hexachlorobutadiene 802 726 ug/Kg 91 55 - 140 3 30
Naphthalene 800 712 ug/Kg 89 40 - 125 13 30
Fluorobenzene (Surr) 80 - 120
Surrogate
98
LCSD LCSD
Qualifier Limits%Recovery
101Toluene-d8 (Surr) 80 - 120
100Ethylbenzene-d10 70 - 120
1024-Bromofluorobenzene (Surr) 70 - 120
103Trifluorotoluene (Surr) 65 - 140
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM)
Client Sample ID: Method BlankLab Sample ID: MB 580-115950/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 116280 Prep Batch: 115950
RL MDL
Naphthalene ND 1.7 ug/Kg 07/23/12 13:38 07/27/12 14:10 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 1.7 ug/Kg 07/23/12 13:38 07/27/12 14:10 12-Methylnaphthalene
ND 1.7 ug/Kg 07/23/12 13:38 07/27/12 14:10 11-Methylnaphthalene
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QC Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 580-115950/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 116280 Prep Batch: 115950
RL MDL
Acenaphthylene ND 1.7 ug/Kg 07/23/12 13:38 07/27/12 14:10 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 1.7 ug/Kg 07/23/12 13:38 07/27/12 14:10 1Acenaphthene
ND 1.7 ug/Kg 07/23/12 13:38 07/27/12 14:10 1Fluorene
ND 1.7 ug/Kg 07/23/12 13:38 07/27/12 14:10 1Phenanthrene
ND 1.7 ug/Kg 07/23/12 13:38 07/27/12 14:10 1Anthracene
ND 1.7 ug/Kg 07/23/12 13:38 07/27/12 14:10 1Fluoranthene
ND 1.7 ug/Kg 07/23/12 13:38 07/27/12 14:10 1Pyrene
ND 1.7 ug/Kg 07/23/12 13:38 07/27/12 14:10 1Benzo[a]anthracene
ND 1.7 ug/Kg 07/23/12 13:38 07/27/12 14:10 1Chrysene
ND 1.7 ug/Kg 07/23/12 13:38 07/27/12 14:10 1Benzo[b]fluoranthene
ND 1.7 ug/Kg 07/23/12 13:38 07/27/12 14:10 1Benzo[k]fluoranthene
ND 1.7 ug/Kg 07/23/12 13:38 07/27/12 14:10 1Benzo[a]pyrene
ND 1.7 ug/Kg 07/23/12 13:38 07/27/12 14:10 1Indeno[1,2,3-cd]pyrene
ND 1.7 ug/Kg 07/23/12 13:38 07/27/12 14:10 1Dibenz(a,h)anthracene
ND 1.7 ug/Kg 07/23/12 13:38 07/27/12 14:10 1Benzo[g,h,i]perylene
Terphenyl-d14 95 42 - 151 07/27/12 14:10 1
MB MB
Surrogate
07/23/12 13:38
Dil FacPrepared AnalyzedQualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 580-115950/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 116280 Prep Batch: 115950
Naphthalene 336 297 ug/Kg 88 64 - 129
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
2-Methylnaphthalene 334 295 ug/Kg 88 65 - 125
1-Methylnaphthalene 335 301 ug/Kg 90 48 - 148
Acenaphthylene 333 295 ug/Kg 89 69 - 129
Acenaphthene 333 282 ug/Kg 85 65 - 130
Fluorene 336 295 ug/Kg 88 68 - 128
Phenanthrene 335 296 ug/Kg 88 65 - 125
Anthracene 333 312 ug/Kg 94 73 - 123
Fluoranthene 334 304 ug/Kg 91 61 - 121
Pyrene 333 291 ug/Kg 87 54 - 134
Benzo[a]anthracene 334 285 ug/Kg 85 64 - 124
Chrysene 321 291 ug/Kg 91 71 - 126
Benzo[b]fluoranthene 333 256 ug/Kg 77 66 - 136
Benzo[k]fluoranthene 333 288 ug/Kg 87 63 - 143
Benzo[a]pyrene 333 241 ug/Kg 72 68 - 128
Indeno[1,2,3-cd]pyrene 336 222 ug/Kg 66 59 - 139
Dibenz(a,h)anthracene 333 238 ug/Kg 71 57 - 142
Benzo[g,h,i]perylene 333 232 ug/Kg 70 57 - 142
Terphenyl-d14 42 - 151
Surrogate
88
LCS LCS
Qualifier Limits%Recovery
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QC Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 580-115950/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 116280 Prep Batch: 115950
Naphthalene 336 292 ug/Kg 87 64 - 129 2 26
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
2-Methylnaphthalene 334 288 ug/Kg 86 65 - 125 2 27
1-Methylnaphthalene 335 297 ug/Kg 89 48 - 148 1 30
Acenaphthylene 333 295 ug/Kg 89 69 - 129 0 28
Acenaphthene 333 282 ug/Kg 85 65 - 130 0 27
Fluorene 336 295 ug/Kg 88 68 - 128 0 31
Phenanthrene 335 259 ug/Kg 77 65 - 125 13 28
Anthracene 333 296 ug/Kg 89 73 - 123 5 27
Fluoranthene 334 304 ug/Kg 91 61 - 121 0 36
Pyrene 333 302 ug/Kg 91 54 - 134 4 31
Benzo[a]anthracene 334 275 ug/Kg 82 64 - 124 4 27
Chrysene 321 283 ug/Kg 88 71 - 126 3 26
Benzo[b]fluoranthene 333 255 ug/Kg 76 66 - 136 0 31
Benzo[k]fluoranthene 333 299 ug/Kg 90 63 - 143 4 31
Benzo[a]pyrene 333 254 ug/Kg 76 68 - 128 5 30
Indeno[1,2,3-cd]pyrene 336 203 ug/Kg 61 59 - 139 9 29
Dibenz(a,h)anthracene 333 227 ug/Kg 68 57 - 142 5 30
Benzo[g,h,i]perylene 333 227 ug/Kg 68 57 - 142 2 28
Terphenyl-d14 42 - 151
Surrogate
89
LCSD LCSD
Qualifier Limits%Recovery
Method: 8015B - Gasoline Range Organics - (GC)
Client Sample ID: Method BlankLab Sample ID: MB 580-115469/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 115512 Prep Batch: 115469
RL MDL
HI Gasoline Range Organic (C6-C12) ND 4.0 mg/Kg 07/17/12 10:13 07/17/12 18:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
4-Bromofluorobenzene (Surr) 100 75 - 131 07/17/12 18:17 1
MB MB
Surrogate
07/17/12 10:13
Dil FacPrepared AnalyzedQualifier Limits%Recovery
116 07/17/12 10:13 07/17/12 18:17 1Trifluorotoluene (Surr) 53 - 131
Client Sample ID: Lab Control SampleLab Sample ID: LCS 580-115469/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 115512 Prep Batch: 115469
HI Gasoline Range Organic
(C6-C12)
40.0 38.4 mg/Kg 96 64 - 126
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
4-Bromofluorobenzene (Surr) 75 - 131
Surrogate
103
LCS LCS
Qualifier Limits%Recovery
110Trifluorotoluene (Surr) 53 - 131
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QC Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Method: 8015B - Gasoline Range Organics - (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 580-115469/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 115512 Prep Batch: 115469
HI Gasoline Range Organic
(C6-C12)
40.0 37.8 mg/Kg 95 64 - 126 1 30
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
4-Bromofluorobenzene (Surr) 75 - 131
Surrogate
101
LCSD LCSD
Qualifier Limits%Recovery
107Trifluorotoluene (Surr) 53 - 131
Method: 8015B - Diesel Range Organics (DRO) (GC)
Client Sample ID: Method BlankLab Sample ID: MB 580-115815/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 116168 Prep Batch: 115815
RL MDL
HI Diesel Range Organics (>C12-C24) ND 25 mg/Kg 07/20/12 11:46 07/25/12 19:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 50 mg/Kg 07/20/12 11:46 07/25/12 19:17 1HI Residual Range Organics
(>C24-C32)
o-Terphenyl 85 50 - 150 07/25/12 19:17 1
MB MB
Surrogate
07/20/12 11:46
Dil FacPrepared AnalyzedQualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 580-115815/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 116168 Prep Batch: 115815
HI Diesel Range Organics
(>C12-C24)
500 428 mg/Kg 86 75 - 125
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
HI Residual Range Organics
(>C24-C32)
500 508 mg/Kg 102 75 - 125
o-Terphenyl 50 - 150
Surrogate
94
LCS LCS
Qualifier Limits%Recovery
Method: 8081A - Organochlorine Pesticides (GC)
Client Sample ID: Method BlankLab Sample ID: MB 580-115996/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 116403 Prep Batch: 115996
RL MDL
Aldrin ND 0.33 ug/Kg 07/24/12 08:19 07/30/12 15:49 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.33 ug/Kg 07/24/12 08:19 07/30/12 15:49 1alpha-BHC
ND 0.33 ug/Kg 07/24/12 08:19 07/30/12 15:49 1beta-BHC
ND 0.33 ug/Kg 07/24/12 08:19 07/30/12 15:49 1delta-BHC
ND 0.33 ug/Kg 07/24/12 08:19 07/30/12 15:49 1gamma-BHC (Lindane)
ND 0.67 ug/Kg 07/24/12 08:19 07/30/12 15:49 14,4'-DDD
ND 0.67 ug/Kg 07/24/12 08:19 07/30/12 15:49 14,4'-DDE
ND 0.67 ug/Kg 07/24/12 08:19 07/30/12 15:49 14,4'-DDT
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QC Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Method: 8081A - Organochlorine Pesticides (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 580-115996/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 116403 Prep Batch: 115996
RL MDL
Dieldrin ND 0.67 ug/Kg 07/24/12 08:19 07/30/12 15:49 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.33 ug/Kg 07/24/12 08:19 07/30/12 15:49 1Endosulfan I
ND 0.67 ug/Kg 07/24/12 08:19 07/30/12 15:49 1Endosulfan II
ND 0.67 ug/Kg 07/24/12 08:19 07/30/12 15:49 1Endosulfan sulfate
ND 0.67 ug/Kg 07/24/12 08:19 07/30/12 15:49 1Endrin
ND 0.67 ug/Kg 07/24/12 08:19 07/30/12 15:49 1Endrin aldehyde
ND 0.67 ug/Kg 07/24/12 08:19 07/30/12 15:49 1Heptachlor
ND 0.33 ug/Kg 07/24/12 08:19 07/30/12 15:49 1Heptachlor epoxide
ND 3.3 ug/Kg 07/24/12 08:19 07/30/12 15:49 1Methoxychlor
ND 0.67 ug/Kg 07/24/12 08:19 07/30/12 15:49 1Endrin ketone
ND 33 ug/Kg 07/24/12 08:19 07/30/12 15:49 1Toxaphene
ND 0.33 ug/Kg 07/24/12 08:19 07/30/12 15:49 1alpha-Chlordane
ND 0.33 ug/Kg 07/24/12 08:19 07/30/12 15:49 1gamma-Chlordane
Tetrachloro-m-xylene 68 49 - 123 07/30/12 15:49 1
MB MB
Surrogate
07/24/12 08:19
Dil FacPrepared AnalyzedQualifier Limits%Recovery
86 07/24/12 08:19 07/30/12 15:49 1DCB Decachlorobiphenyl 40 - 158
Client Sample ID: Lab Control SampleLab Sample ID: LCS 580-115996/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 116403 Prep Batch: 115996
Aldrin 6.67 6.17 ug/Kg 93 53 - 126
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
alpha-BHC 6.67 5.56 ug/Kg 83 41 - 128
beta-BHC 6.67 6.15 ug/Kg 92 48 - 121
delta-BHC 6.67 4.96 ug/Kg 74 22 - 153
gamma-BHC (Lindane) 6.67 5.69 ug/Kg 85 50 - 127
4,4'-DDD 6.67 6.29 ug/Kg 94 44 - 141
4,4'-DDE 6.67 6.18 ug/Kg 93 47 - 140
4,4'-DDT 6.67 6.16 ug/Kg 92 34 - 159
Dieldrin 6.67 6.54 ug/Kg 98 53 - 134
Endosulfan I 6.67 6.58 ug/Kg 99 52 - 122
Endosulfan II 6.67 6.44 ug/Kg 97 53 - 132
Endosulfan sulfate 6.67 6.12 ug/Kg 92 42 - 128
Endrin 6.67 6.80 ug/Kg 102 46 - 138
Endrin aldehyde 6.67 5.45 ug/Kg 82 12 - 179
Heptachlor 6.67 6.41 ug/Kg 96 50 - 130
Heptachlor epoxide 6.67 6.54 ug/Kg 98 49 - 123
Methoxychlor 6.67 6.66 ug/Kg 100 46 - 154
Endrin ketone 6.67 6.75 ug/Kg 101 45 - 127
alpha-Chlordane 6.67 6.02 ug/Kg 90 46 - 118
gamma-Chlordane 6.67 5.85 ug/Kg 88 49 - 122
Tetrachloro-m-xylene 49 - 123
Surrogate
86
LCS LCS
Qualifier Limits%Recovery
95DCB Decachlorobiphenyl 40 - 158
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QC Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Method: 8081A - Organochlorine Pesticides (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 580-115996/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 116403 Prep Batch: 115996
Aldrin 6.67 6.06 ug/Kg 91 53 - 126 2 24
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
alpha-BHC 6.67 5.57 ug/Kg 84 41 - 128 0 28
beta-BHC 6.67 6.12 ug/Kg 92 48 - 121 0 32
delta-BHC 6.67 4.94 ug/Kg 74 22 - 153 0 36
gamma-BHC (Lindane) 6.67 5.72 ug/Kg 86 50 - 127 1 29
4,4'-DDD 6.67 6.28 ug/Kg 94 44 - 141 0 41
4,4'-DDE 6.67 6.12 ug/Kg 92 47 - 140 1 40
4,4'-DDT 6.67 6.10 ug/Kg 91 34 - 159 1 47
Dieldrin 6.67 6.52 ug/Kg 98 53 - 134 0 32
Endosulfan I 6.67 6.44 ug/Kg 97 52 - 122 2 31
Endosulfan II 6.67 6.44 ug/Kg 97 53 - 132 0 36
Endosulfan sulfate 6.67 6.18 ug/Kg 93 42 - 128 1 43
Endrin 6.67 6.77 ug/Kg 102 46 - 138 0 36
Endrin aldehyde 6.67 5.59 ug/Kg 84 12 - 179 3 47
Heptachlor 6.67 6.23 ug/Kg 93 50 - 130 3 31
Heptachlor epoxide 6.67 6.55 ug/Kg 98 49 - 123 0 31
Methoxychlor 6.67 6.69 ug/Kg 100 46 - 154 0 46
Endrin ketone 6.67 6.79 ug/Kg 102 45 - 127 1 45
alpha-Chlordane 6.67 5.90 ug/Kg 89 46 - 118 2 33
gamma-Chlordane 6.67 5.79 ug/Kg 87 49 - 122 1 32
Tetrachloro-m-xylene 49 - 123
Surrogate
84
LCSD LCSD
Qualifier Limits%Recovery
92DCB Decachlorobiphenyl 40 - 158
Method: 6010B - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 580-116110/9-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 116218 Prep Batch: 116110
RL MDL
Arsenic ND 3.0 mg/Kg 07/25/12 10:14 07/25/12 21:43 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.50 mg/Kg 07/25/12 10:14 07/25/12 21:43 1Cadmium
ND 1.5 mg/Kg 07/25/12 10:14 07/25/12 21:43 1Lead
Client Sample ID: Lab Control SampleLab Sample ID: LCS 580-116110/10-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 116218 Prep Batch: 116110
Arsenic 200 192 mg/Kg 96 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Cadmium 5.00 4.71 mg/Kg 94 80 - 120
Lead 50.0 50.4 mg/Kg 101 80 - 120
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QC Sample ResultsTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Method: 6010B - Metals (ICP) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 580-116110/11-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 116218 Prep Batch: 116110
Arsenic 200 189 mg/Kg 95 80 - 120 1 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Cadmium 5.00 4.66 mg/Kg 93 80 - 120 1 20
Lead 50.0 48.7 mg/Kg 97 80 - 120 3 20
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Lab ChronicleClient: Bureau Veritas North America, Inc. TestAmerica Job ID: 580-33932-1
Project/Site: Urban Works Phase II
Client Sample ID: UW BH 1 1' Lab Sample ID: 580-33932-1Matrix: SolidDate Collected: 07/10/12 11:40
Percent Solids: 97.1Date Received: 07/13/12 10:00
Prep 5035 07/17/12 11:46 EZ115488 TAL SEA
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8260B 1 115678 07/19/12 18:44 SK TAL SEATotal/NA
Prep 3550B 115950 07/23/12 13:38 AA TAL SEATotal/NA
Analysis 8270C SIM 1 116415 07/30/12 10:33 AP TAL SEATotal/NA
Prep 5035 115469 07/17/12 10:13 EZ TAL SEATotal/NA
Analysis 8015B 1 115512 07/17/12 20:52 JMB TAL SEATotal/NA
Prep 3550B 115815 07/20/12 11:46 AA TAL SEATotal/NA
Analysis 8015B 1 116168 07/25/12 21:12 JL TAL SEATotal/NA
Prep 3050B 116110 07/25/12 10:14 PAB TAL SEATotal/NA
Analysis 6010B 10 116218 07/25/12 22:09 SP TAL SEATotal/NA
Analysis D 2216 1 115533 07/17/12 18:49 TAL SEATotal/NA
Client Sample ID: UW BH 1 6' Lab Sample ID: 580-33932-2Matrix: SolidDate Collected: 07/10/12 11:55
Percent Solids: 98.7Date Received: 07/13/12 10:00
Prep 5035 07/17/12 11:46 EZ115488 TAL SEA
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8260B 1 115678 07/19/12 19:07 SK TAL SEATotal/NA
Prep 3550B 115950 07/23/12 13:38 AA TAL SEATotal/NA
Analysis 8270C SIM 1 116280 07/27/12 15:39 AP TAL SEATotal/NA
Prep 5035 115469 07/17/12 10:13 EZ TAL SEATotal/NA
Analysis 8015B 1 115512 07/17/12 21:14 JMB TAL SEATotal/NA
Prep 3550B 115815 07/20/12 11:46 AA TAL SEATotal/NA
Analysis 8015B 1 116168 07/25/12 21:32 JL TAL SEATotal/NA
Prep 3050B 116110 07/25/12 10:14 PAB TAL SEATotal/NA
Analysis 6010B 10 116218 07/25/12 22:22 SP TAL SEATotal/NA
Analysis D 2216 1 115533 07/17/12 18:49 TAL SEATotal/NA
Client Sample ID: UW BH 2 1' Lab Sample ID: 580-33932-3Matrix: SolidDate Collected: 07/10/12 10:40
Percent Solids: 95.9Date Received: 07/13/12 10:00
Prep 5035 07/17/12 11:46 EZ115488 TAL SEA
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8260B 1 115678 07/19/12 19:30 SK TAL SEATotal/NA
Prep 3550B 115950 07/23/12 13:38 AA TAL SEATotal/NA
Analysis 8270C SIM 1 116415 07/30/12 10:56 AP TAL SEATotal/NA
Prep 5035 115469 07/17/12 10:13 EZ TAL SEATotal/NA
Analysis 8015B 1 115512 07/17/12 22:20 JMB TAL SEATotal/NA
Prep 3550B 115815 07/20/12 11:46 AA TAL SEATotal/NA
Analysis 8015B 1 116168 07/25/12 21:51 JL TAL SEATotal/NA
Prep 3050B 116110 07/25/12 10:14 PAB TAL SEATotal/NA
Analysis 6010B 10 116218 07/25/12 22:28 SP TAL SEATotal/NA
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Lab ChronicleClient: Bureau Veritas North America, Inc. TestAmerica Job ID: 580-33932-1
Project/Site: Urban Works Phase II
Client Sample ID: UW BH 2 1' Lab Sample ID: 580-33932-3Matrix: SolidDate Collected: 07/10/12 10:40
Date Received: 07/13/12 10:00
Analysis D 2216 07/17/12 18:491 115533 TAL SEA
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: UW BH 2 7' Lab Sample ID: 580-33932-4Matrix: SolidDate Collected: 07/10/12 10:55
Percent Solids: 88.9Date Received: 07/13/12 10:00
Prep 5035 07/17/12 11:46 EZ115488 TAL SEA
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8260B 1 115678 07/19/12 19:53 SK TAL SEATotal/NA
Prep 3550B 115950 07/23/12 13:38 AA TAL SEATotal/NA
Analysis 8270C SIM 1 116280 07/27/12 18:58 AP TAL SEATotal/NA
Prep 5035 115469 07/17/12 10:13 EZ TAL SEATotal/NA
Analysis 8015B 1 115512 07/17/12 22:42 JMB TAL SEATotal/NA
Prep 3550B 115815 07/20/12 11:46 AA TAL SEATotal/NA
Analysis 8015B 1 116168 07/25/12 22:10 JL TAL SEATotal/NA
Prep 3050B 116110 07/25/12 10:14 PAB TAL SEATotal/NA
Analysis 6010B 10 116218 07/25/12 22:35 SP TAL SEATotal/NA
Analysis D 2216 1 115533 07/17/12 18:49 TAL SEATotal/NA
Client Sample ID: UW BH 3 7' Lab Sample ID: 580-33932-5Matrix: SolidDate Collected: 07/10/12 09:30
Percent Solids: 99.0Date Received: 07/13/12 10:00
Prep 5035 07/17/12 11:46 EZ115488 TAL SEA
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8260B 1 115678 07/19/12 20:16 SK TAL SEATotal/NA
Prep 3550B 115950 07/23/12 13:38 AA TAL SEATotal/NA
Analysis 8270C SIM 1 116280 07/27/12 19:21 AP TAL SEATotal/NA
Prep 3550B 115815 07/20/12 11:46 AA TAL SEATotal/NA
Analysis 8015B 1 116168 07/25/12 23:08 JL TAL SEATotal/NA
Prep 3550B 115996 07/24/12 08:19 SH TAL SEATotal/NA
Analysis 8081A 1 116403 07/30/12 16:37 CM TAL SEATotal/NA
Prep 3050B 116110 07/25/12 10:14 PAB TAL SEATotal/NA
Analysis 6010B 10 116218 07/25/12 22:42 SP TAL SEATotal/NA
Analysis D 2216 1 115533 07/17/12 18:49 TAL SEATotal/NA
Client Sample ID: UW BH 4 6' Lab Sample ID: 580-33932-6Matrix: SolidDate Collected: 07/10/12 10:20
Percent Solids: 98.3Date Received: 07/13/12 10:00
Prep 5035 07/17/12 11:46 EZ115488 TAL SEA
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8260B 1 115678 07/19/12 20:39 SK TAL SEATotal/NA
Prep 3550B 115950 07/23/12 13:38 AA TAL SEATotal/NA
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Lab ChronicleClient: Bureau Veritas North America, Inc. TestAmerica Job ID: 580-33932-1
Project/Site: Urban Works Phase II
Client Sample ID: UW BH 4 6' Lab Sample ID: 580-33932-6Matrix: SolidDate Collected: 07/10/12 10:20
Percent Solids: 98.3Date Received: 07/13/12 10:00
Analysis 8270C SIM 07/30/12 12:47 AP1 116415 TAL SEA
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3550B 115815 07/20/12 11:46 AA TAL SEATotal/NA
Analysis 8015B 1 116168 07/25/12 23:27 JL TAL SEATotal/NA
Prep 3550B 115996 07/24/12 08:19 SH TAL SEATotal/NA
Analysis 8081A 10 116403 07/30/12 17:07 CM TAL SEATotal/NA
Prep 3050B 116110 07/25/12 10:14 PAB TAL SEATotal/NA
Analysis 6010B 10 116218 07/25/12 23:01 SP TAL SEATotal/NA
Analysis D 2216 1 115533 07/17/12 18:49 TAL SEATotal/NA
Client Sample ID: UW MI-1 Lab Sample ID: 580-33932-7Matrix: SolidDate Collected: 07/10/12 12:45
Percent Solids: 94.7Date Received: 07/13/12 10:00
Prep 5035 07/17/12 11:46 EZRA 115488 TAL SEA
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8260B RA 1 115886 07/22/12 21:44 SK TAL SEATotal/NA
Prep 3550B 115950 07/23/12 13:38 AA TAL SEATotal/NA
Analysis 8270C SIM 1 116415 07/30/12 11:40 AP TAL SEATotal/NA
Prep 5035 115469 07/17/12 10:13 EZ TAL SEATotal/NA
Analysis 8015B 1 115512 07/17/12 23:04 JMB TAL SEATotal/NA
Prep 3550B 115815 07/20/12 11:46 AA TAL SEATotal/NA
Analysis 8015B 1 116168 07/25/12 23:46 JL TAL SEATotal/NA
Prep 3050B 116110 07/25/12 10:14 PAB TAL SEATotal/NA
Analysis 6010B 10 116218 07/25/12 23:08 SP TAL SEATotal/NA
Analysis D 2216 1 115533 07/17/12 18:49 TAL SEATotal/NA
Client Sample ID: UW MI-2 Lab Sample ID: 580-33932-8Matrix: SolidDate Collected: 07/10/12 14:50
Percent Solids: 95.9Date Received: 07/13/12 10:00
Prep 5035 07/17/12 11:46 EZRA 115488 TAL SEA
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8260B RA 1 115886 07/22/12 22:06 SK TAL SEATotal/NA
Prep 3550B 115950 07/23/12 13:38 AA TAL SEATotal/NA
Analysis 8270C SIM 1 116415 07/30/12 12:02 AP TAL SEATotal/NA
Prep 5035 115469 07/17/12 10:13 EZ TAL SEATotal/NA
Analysis 8015B 1 115512 07/17/12 23:27 JMB TAL SEATotal/NA
Prep 3550B 115815 07/20/12 11:46 AA TAL SEATotal/NA
Analysis 8015B 1 116168 07/26/12 00:06 JL TAL SEATotal/NA
Prep 3050B 116110 07/25/12 10:14 PAB TAL SEATotal/NA
Analysis 6010B 10 116218 07/25/12 23:14 SP TAL SEATotal/NA
Analysis D 2216 1 115533 07/17/12 18:49 TAL SEATotal/NA
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Lab ChronicleClient: Bureau Veritas North America, Inc. TestAmerica Job ID: 580-33932-1
Project/Site: Urban Works Phase II
Laboratory References:
Anatek Lab = Anatek Labs Inc - Moscow Idaho, 1282 Alturas Dr., Moscow, ID 83843
TAL SEA = TestAmerica Seattle, 5755 8th Street East, Tacoma, WA 98424, TEL (253)922-2310
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Certification SummaryClient: Bureau Veritas North America, Inc. TestAmerica Job ID: 580-33932-1
Project/Site: Urban Works Phase II
Laboratory: TestAmerica SeattleAll certifications held by this laboratory are listed. Not all certifications are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
Alaska (UST) 03-04-13UST-02210State Program
California NELAC 9 1115CA 01-31-13
L-A-B DoD ELAP L2236 01-19-13
L-A-B ISO/IEC 17025 L2236 01-19-13
Montana (UST) State Program 8 N/A 04-30-20
Oregon NELAC 10 WA100007 11-06-12
USDA Federal P330-11-00222 05-20-14
Washington State Program 10 C553 02-17-13
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Sample SummaryTestAmerica Job ID: 580-33932-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
580-33932-1 UW BH 1 1' Solid 07/10/12 11:40 07/13/12 10:00
580-33932-2 UW BH 1 6' Solid 07/10/12 11:55 07/13/12 10:00
580-33932-3 UW BH 2 1' Solid 07/10/12 10:40 07/13/12 10:00
580-33932-4 UW BH 2 7' Solid 07/10/12 10:55 07/13/12 10:00
580-33932-5 UW BH 3 7' Solid 07/10/12 09:30 07/13/12 10:00
580-33932-6 UW BH 4 6' Solid 07/10/12 10:20 07/13/12 10:00
580-33932-7 UW MI-1 Solid 07/10/12 12:45 07/13/12 10:00
580-33932-8 UW MI-2 Solid 07/10/12 14:50 07/13/12 10:00
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CASE NARRATIVE August 6, 2012 Lab Name: Anatek Labs, Inc. 1282 Alturas Drive, Moscow, ID 83843 www.anateklabs.com FL NELAP E87893, NV ID13-2004-31, WA DOE C126, OR ELAP ID200001, MT 0028, ID, CO, NM Project Tracking No.: HVG0027 Anatek Batch: 120716027 Project Summary: Two (2) soil samples were received on 7/16/2011 for herbicide pesticide screen (EPA 8270Cm). The samples were received with the appropriate chain of custody at 5.4C Client Sample ID Anatek Sample ID Method/Prep Method HVG0027-05 (UW BH 3 7’ – Solid/Soil) 120716027-001 EPA 8270Cm HVG0027-06 (UW BH 4 6’ – Solid/Soil) 120716027-002 EPA 8270Cm QA/QC Checks Parameters Yes / No Exceptions / Deviations Sample Holding Time Valid? Y NA Surrogate Recoveries Valid? Y NA QC Sample(s) Recoveries Valid? Y NA Method Blank(s) Valid? Y NA Tune(s) Valid? Y NA Internal Standard Responses Valid? Y NA Initial Calibration Curve(s) Valid? Y NA Continuing Calibration(s) Valid? Y NA Comments: Y NA 1. Holding Time Requirements
No problems encountered. 2. GC/MS Tune Requirements
No problems encountered. 3. Calibration Requirements
No problems encountered. 4. Surrogate Recovery Requirements
No problems encountered. 5. QC Sample (LCS/MS/MSD) Recovery Requirements
No problems encountered.
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6. Method Blank Requirements The method blanks were non-detect (<MDL) for all analytes. No problems encountered. 7. Internal Standard(s) Response Requirements
No problems encountered.
8. Comments
N/A I certify that this data package is in compliance with the terms and conditions of the contract. Release of the data contained in this data package has been authorized by the Laboratory Manager or his designee.
Page 49 of 60 8/9/2012
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Client: TEST AMERICA - HONOLULU, HI
Attn: KRISTIE REILLY
Address: 99-193 AIEA HEIGHTS DRIVE
AIEA, HI 96701-3900
Analytical Results Report
Batch #: 120716027
Project Name: HVG0027
Anatek Labs, Inc.1282 Alturas Drive • Moscow, ID 83843 • (208) 883-2839 • Fax (208) 882-9246 • email [email protected]
504 E Sprague Ste. D • Spokane WA 99202 • (509) 838-3999 • Fax (509) 838-4433 • email [email protected]
120716027-001Sample Number
Matrix Soil
Parameter Result Units Analysis Date Analyst Method QualifierPQL
Client Sample ID
Sampling Date 7/10/2012
Sampling Time 9:30 AM
Date/Time Received 7/16/2012
Extraction DateHVG0027-05 (UW BH 3 7 - SOLID/SOIL) 7/24/2012
10:53 AM
MDL
Comments
mg/kg EMP7/27/20122,3,4,6-Tetrachlorophenol EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Ametryne EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Atraton EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Atrazine EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Azinphos-methyl EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Bolstar EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Bromacil EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Carbophenothion EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Chlorpyrifos EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Coumaphos EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Demeton EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Diazinon EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Dichlorvos EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Dimethenamid EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Dimethoate EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Disulfoton EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012EPN EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Ethoprop EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Ethyl parathion EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Fensulfothion EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Fenthion EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Hexachlorphene EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Hexazinone EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Malathion EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Merphos EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Methyl parathion EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Mevinphos EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Naled EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Pentachlorophenol EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Phorate EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Phosmet EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Prometon EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Prometryn EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Propazine EPA 8270CMODND 0.10.05
Page 1 of 4Monday, August 06, 2012
Certifications held by Anatek Labs ID: EPA:ID00013; AZ:0701; CO:ID00013; FL(NELAP):E87893; ID:ID00013; IN:C-ID-01; KY:90142; MT:CERT0028; NM: ID00013; OR:ID200001-002; WA:C595Certifications held by Anatek Labs WA: EPA:WA00169; ID:WA00169; WA:C585; MT:Cert0095
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Client: TEST AMERICA - HONOLULU, HI
Attn: KRISTIE REILLY
Address: 99-193 AIEA HEIGHTS DRIVE
AIEA, HI 96701-3900
Analytical Results Report
Batch #: 120716027
Project Name: HVG0027
Anatek Labs, Inc.1282 Alturas Drive • Moscow, ID 83843 • (208) 883-2839 • Fax (208) 882-9246 • email [email protected]
504 E Sprague Ste. D • Spokane WA 99202 • (509) 838-3999 • Fax (509) 838-4433 • email [email protected]
120716027-001Sample Number
Matrix Soil
Parameter Result Units Analysis Date Analyst Method QualifierPQL
Client Sample ID
Sampling Date 7/10/2012
Sampling Time 9:30 AM
Date/Time Received 7/16/2012
Extraction DateHVG0027-05 (UW BH 3 7 - SOLID/SOIL) 7/24/2012
10:53 AM
MDL
Comments
mg/kg EMP7/27/2012Ronnel EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Secbumeton EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Simazine EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Simetryn EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Stirophos EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Sulfotep EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Terbuthylazine EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Terbutryn EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Tokuthion EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Trichloronate EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Trifluralin EPA 8270CMODND 0.10.05
Surrogate Data
Surrogate Standard Percent Recovery Control Limits
Sample Number 120716027-001
Method
Terphenyl-d14 107.1 30-140EPA 8270CMOD
Page 2 of 4Monday, August 06, 2012
Certifications held by Anatek Labs ID: EPA:ID00013; AZ:0701; CO:ID00013; FL(NELAP):E87893; ID:ID00013; IN:C-ID-01; KY:90142; MT:CERT0028; NM: ID00013; OR:ID200001-002; WA:C595Certifications held by Anatek Labs WA: EPA:WA00169; ID:WA00169; WA:C585; MT:Cert0095
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Client: TEST AMERICA - HONOLULU, HI
Attn: KRISTIE REILLY
Address: 99-193 AIEA HEIGHTS DRIVE
AIEA, HI 96701-3900
Analytical Results Report
Batch #: 120716027
Project Name: HVG0027
Anatek Labs, Inc.1282 Alturas Drive • Moscow, ID 83843 • (208) 883-2839 • Fax (208) 882-9246 • email [email protected]
504 E Sprague Ste. D • Spokane WA 99202 • (509) 838-3999 • Fax (509) 838-4433 • email [email protected]
120716027-002Sample Number
Matrix Soil
Parameter Result Units Analysis Date Analyst Method QualifierPQL
Client Sample ID
Sampling Date 7/10/2012
Sampling Time 10:20 AM
Date/Time Received 7/16/2012
Extraction DateHVG0027-06 (UW BH 4 6 - SOLID/SOIL) 7/24/2012
10:53 AM
MDL
Comments
mg/kg EMP7/27/20122,3,4,6-Tetrachlorophenol EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Ametryne EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Atraton EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Atrazine EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Azinphos-methyl EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Bolstar EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Bromacil EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Carbophenothion EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Chlorpyrifos EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Coumaphos EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Demeton EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Diazinon EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Dichlorvos EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Dimethenamid EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Dimethoate EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Disulfoton EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012EPN EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Ethoprop EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Ethyl parathion EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Fensulfothion EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Fenthion EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Hexachlorphene EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Hexazinone EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Malathion EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Merphos EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Methyl parathion EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Mevinphos EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Naled EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Pentachlorophenol EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Phorate EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Phosmet EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Prometon EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Prometryn EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Propazine EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Ronnel EPA 8270CMODND 0.10.05
Page 3 of 4Monday, August 06, 2012
Certifications held by Anatek Labs ID: EPA:ID00013; AZ:0701; CO:ID00013; FL(NELAP):E87893; ID:ID00013; IN:C-ID-01; KY:90142; MT:CERT0028; NM: ID00013; OR:ID200001-002; WA:C595Certifications held by Anatek Labs WA: EPA:WA00169; ID:WA00169; WA:C585; MT:Cert0095
Page 52 of 60 8/9/2012
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Client: TEST AMERICA - HONOLULU, HI
Attn: KRISTIE REILLY
Address: 99-193 AIEA HEIGHTS DRIVE
AIEA, HI 96701-3900
Analytical Results Report
Batch #: 120716027
Project Name: HVG0027
Anatek Labs, Inc.1282 Alturas Drive • Moscow, ID 83843 • (208) 883-2839 • Fax (208) 882-9246 • email [email protected]
504 E Sprague Ste. D • Spokane WA 99202 • (509) 838-3999 • Fax (509) 838-4433 • email [email protected]
120716027-002Sample Number
Matrix Soil
Parameter Result Units Analysis Date Analyst Method QualifierPQL
Client Sample ID
Sampling Date 7/10/2012
Sampling Time 10:20 AM
Date/Time Received 7/16/2012
Extraction DateHVG0027-06 (UW BH 4 6 - SOLID/SOIL) 7/24/2012
10:53 AM
MDL
Comments
mg/kg EMP7/27/2012Secbumeton EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Simazine EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Simetryn EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Stirophos EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Sulfotep EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Terbuthylazine EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Terbutryn EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Tokuthion EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Trichloronate EPA 8270CMODND 0.10.05
mg/kg EMP7/27/2012Trifluralin EPA 8270CMODND 0.10.05
Surrogate Data
Surrogate Standard Percent Recovery Control Limits
Sample Number 120716027-002
Method
Terphenyl-d14 105.9 30-140EPA 8270CMOD
Authorized Signature
John Coddington, Lab Manager
MCL EPA's Maximum Contaminant Level
ND Not Detected
PQL Practical Quantitation Limit
This report shall not be reproduced except in full, without the written approval of the laboratory.The results reported relate only to the samples indicated.Soil/solid results are reported on a dry-weight basis unless otherwise noted.
Page 4 of 4Monday, August 06, 2012
Certifications held by Anatek Labs ID: EPA:ID00013; AZ:0701; CO:ID00013; FL(NELAP):E87893; ID:ID00013; IN:C-ID-01; KY:90142; MT:CERT0028; NM: ID00013; OR:ID200001-002; WA:C595Certifications held by Anatek Labs WA: EPA:WA00169; ID:WA00169; WA:C585; MT:Cert0095
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Client: TEST AMERICA - HONOLULU, HI
Attn: KRISTIE REILLY
Address: 99-193 AIEA HEIGHTS DRIVE
AIEA, HI 96701-3900
Analytical Results Report
Batch #: 120716027
Project Name: HVG0027
Quality Control Data
Anatek Labs, Inc.1282 Alturas Drive • Moscow, ID 83843 • (208) 883-2839 • Fax (208) 882-9246 • email [email protected]
504 E Sprague Ste. D • Spokane WA 99202 • (509) 838-3999 • Fax (509) 838-4433 • email [email protected]
Parameter %Rec
Lab Control Sample
LCS Result LCS Spike AR %Rec Analysis DateUnits Prep Date
7/27/2012Trifluralin 1 105.01.05 40-150mg/kg 7/24/2012
7/27/2012Terbutryn 1 79.00.790 40-150mg/kg 7/24/2012
7/27/2012Simetryn 1 74.90.749 40-150mg/kg 7/24/2012
7/27/2012Simazine 1 95.30.953 40-150mg/kg 7/24/2012
7/27/2012Propazine 1 70.50.705 40-150mg/kg 7/24/2012
7/27/2012Prometon 1 69.10.691 40-150mg/kg 7/24/2012
7/27/2012Pentachlorophenol 1 32.80.328 20-150mg/kg 7/24/2012
7/27/2012Hexazinone 1 78.40.784 20-120mg/kg 7/24/2012
7/27/2012Diazinon 1 84.70.847 20-120mg/kg 7/24/2012
7/27/2012Bromacil 1 66.80.668 20-120mg/kg 7/24/2012
7/27/2012Atrazine 1 116.01.16 40-150mg/kg 7/24/2012
7/27/2012Atraton 1 67.90.679 40-150mg/kg 7/24/2012
7/27/2012Ametryne 1 66.30.663 20-120mg/kg 7/24/2012
Parameter %Rec
Matrix Spike DuplicateMSD
ResultMSDSpike Analysis DateUnits %RPD
AR%RPD Prep Date
Parameter %Rec
Matrix Spike
Sample NumberMS
ResultMS
SpikeAR
%Rec Analysis DateUnitsSampleResult Prep Date
120724021-008A 7/27/2012Trifluralin 1 94.10.941 40-150mg/kgND 7/24/2012
120724021-008A 7/27/2012Terbutryn 1 71.50.715 40-150mg/kgND 7/24/2012
120724021-008A 7/27/2012Simetryn 1 46.70.467 40-150mg/kgND 7/24/2012
120724021-008A 7/27/2012Simazine 1 83.40.834 40-150mg/kgND 7/24/2012
120724021-008A 7/27/2012Propazine 1 63.50.635 40-150mg/kgND 7/24/2012
120724021-008A 7/27/2012Prometon 1 57.50.575 40-150mg/kgND 7/24/2012
120724021-008A 7/27/2012Pentachlorophenol 1 20.20.202 20-150mg/kgND 7/24/2012
120724021-008A 7/27/2012Hexazinone 1 57.30.573 20-120mg/kgND 7/24/2012
120724021-008A 7/27/2012Diazinon 1 77.10.771 20-120mg/kgND 7/24/2012
120724021-008A 7/27/2012Bromacil 1 60.10.601 20-120mg/kgND 7/24/2012
120724021-008A 7/27/2012Atrazine 1 105.01.05 40-150mg/kgND 7/24/2012
120724021-008A 7/27/2012Atraton 1 42.60.426 40-150mg/kgND 7/24/2012
120724021-008A 7/27/2012Ametryne 1 55.60.556 20-120mg/kgND 7/24/2012
Page 1 of 3Monday, August 06, 2012
Comments:
Certifications held by Anatek Labs ID: EPA:ID00013; AZ:0701; CO:ID00013; FL(NELAP):E87893; ID:ID00013; IN:C-ID-01; KY:90142; MT:CERT0028; NM: ID00013; OR:ID200001-002; WA:C595Certifications held by Anatek Labs WA: EPA:WA00169; ID:WA00169; WA:C585; MT:Cert0095
Page 54 of 60 8/9/2012
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Client: TEST AMERICA - HONOLULU, HI
Attn: KRISTIE REILLY
Address: 99-193 AIEA HEIGHTS DRIVE
AIEA, HI 96701-3900
Analytical Results Report
Batch #: 120716027
Project Name: HVG0027
Quality Control Data
Anatek Labs, Inc.1282 Alturas Drive • Moscow, ID 83843 • (208) 883-2839 • Fax (208) 882-9246 • email [email protected]
504 E Sprague Ste. D • Spokane WA 99202 • (509) 838-3999 • Fax (509) 838-4433 • email [email protected]
Parameter %Rec
Matrix Spike DuplicateMSD
ResultMSDSpike Analysis DateUnits %RPD
AR%RPD Prep Date
7/27/2012Trifluralin 1 100.01.00 mg/kg 6.1 0-50 7/24/2012
7/27/2012Terbutryn 1 76.10.761 mg/kg 6.2 0-50 7/24/2012
7/27/2012Simetryn 1 51.80.518 mg/kg 10.4 0-50 7/24/2012
7/27/2012Simazine 1 87.10.871 mg/kg 4.3 0-50 7/24/2012
7/27/2012Propazine 1 68.90.689 mg/kg 8.2 0-50 7/24/2012
7/27/2012Prometon 1 60.00.600 mg/kg 4.3 0-50 7/24/2012
7/27/2012Pentachlorophenol 1 20.40.204 mg/kg 1.0 0-50 7/24/2012
7/27/2012Hexazinone 1 59.80.598 mg/kg 4.3 0-50 7/24/2012
7/27/2012Diazinon 1 81.10.811 mg/kg 5.1 0-50 7/24/2012
7/27/2012Bromacil 1 64.90.649 mg/kg 7.7 0-50 7/24/2012
7/27/2012Atrazine 1 118.01.18 mg/kg 11.7 0-50 7/24/2012
7/27/2012Atraton 1 47.30.473 mg/kg 10.5 0-50 7/24/2012
7/27/2012Ametryne 1 59.20.592 mg/kg 6.3 0-50 7/24/2012
Parameter
Method Blank
Result Analysis DateUnits PQL Prep Date
7/27/20122,3,4,6-Tetrachlorophenol ND mg/kg 0.1 7/24/2012
7/27/2012Ametryne ND mg/kg 0.1 7/24/2012
7/27/2012Atraton ND mg/kg 0.1 7/24/2012
7/27/2012Atrazine ND mg/kg 0.1 7/24/2012
7/27/2012Azinphos-methyl ND mg/kg 0.1 7/24/2012
7/27/2012Bolstar ND mg/kg 0.1 7/24/2012
7/27/2012Bromacil ND mg/kg 0.1 7/24/2012
7/27/2012Carbophenothion ND mg/kg 0.1 7/24/2012
7/27/2012Chlorpyrifos ND mg/kg 0.1 7/24/2012
7/27/2012Coumaphos ND mg/kg 0.1 7/24/2012
7/27/2012Demeton ND mg/kg 0.1 7/24/2012
7/27/2012Diazinon ND mg/kg 0.1 7/24/2012
7/27/2012Dichlorvos ND mg/kg 0.1 7/24/2012
7/27/2012Dimethenamid ND mg/kg 0.1 7/24/2012
7/27/2012Dimethoate ND mg/kg 0.1 7/24/2012
7/27/2012Disulfoton ND mg/kg 0.1 7/24/2012
7/27/2012EPN ND mg/kg 0.1 7/24/2012
7/27/2012Ethoprop ND mg/kg 0.1 7/24/2012
7/27/2012Ethyl parathion ND mg/kg 0.1 7/24/2012
7/27/2012Fensulfothion ND mg/kg 0.1 7/24/2012
Page 2 of 3Monday, August 06, 2012
Comments:
Certifications held by Anatek Labs ID: EPA:ID00013; AZ:0701; CO:ID00013; FL(NELAP):E87893; ID:ID00013; IN:C-ID-01; KY:90142; MT:CERT0028; NM: ID00013; OR:ID200001-002; WA:C595Certifications held by Anatek Labs WA: EPA:WA00169; ID:WA00169; WA:C585; MT:Cert0095
Page 55 of 60 8/9/2012
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Client: TEST AMERICA - HONOLULU, HI
Attn: KRISTIE REILLY
Address: 99-193 AIEA HEIGHTS DRIVE
AIEA, HI 96701-3900
Analytical Results Report
Batch #: 120716027
Project Name: HVG0027
Quality Control Data
Anatek Labs, Inc.1282 Alturas Drive • Moscow, ID 83843 • (208) 883-2839 • Fax (208) 882-9246 • email [email protected]
504 E Sprague Ste. D • Spokane WA 99202 • (509) 838-3999 • Fax (509) 838-4433 • email [email protected]
Parameter
Method Blank
Result Analysis DateUnits PQL Prep Date
7/27/2012Fenthion ND mg/kg 0.1 7/24/2012
7/27/2012Hexachlorphene ND mg/kg 0.1 7/24/2012
7/27/2012Hexazinone ND mg/kg 0.1 7/24/2012
7/27/2012Malathion ND mg/kg 0.1 7/24/2012
7/27/2012Merphos ND mg/kg 0.1 7/24/2012
7/27/2012Methyl parathion ND mg/kg 0.1 7/24/2012
7/27/2012Mevinphos ND mg/kg 0.1 7/24/2012
7/27/2012Naled ND mg/kg 0.1 7/24/2012
7/27/2012Pentachlorophenol ND mg/kg 0.1 7/24/2012
7/27/2012Phorate ND mg/kg 0.1 7/24/2012
7/27/2012Phosmet ND mg/kg 0.1 7/24/2012
7/27/2012Prometon ND mg/kg 0.1 7/24/2012
7/27/2012Prometryn ND mg/kg 0.1 7/24/2012
7/27/2012Propazine ND mg/kg 0.1 7/24/2012
7/27/2012Ronnel ND mg/kg 0.1 7/24/2012
7/27/2012Secbumeton ND mg/kg 0.1 7/24/2012
7/27/2012Simazine ND mg/kg 0.1 7/24/2012
7/27/2012Simetryn ND mg/kg 0.1 7/24/2012
7/27/2012Stirophos ND mg/kg 0.1 7/24/2012
7/27/2012Sulfotep ND mg/kg 0.1 7/24/2012
7/27/2012Terbuthylazine ND mg/kg 0.1 7/24/2012
7/27/2012Terbutryn ND mg/kg 0.1 7/24/2012
7/27/2012Tokuthion ND mg/kg 0.1 7/24/2012
7/27/2012Trichloronate ND mg/kg 0.1 7/24/2012
7/27/2012Trifluralin ND mg/kg 0.1 7/24/2012
AR Acceptable RangeND Not DetectedPQL Practical Quantitation LimitRPD Relative Percentage Difference
Page 3 of 3Monday, August 06, 2012
Comments:
Certifications held by Anatek Labs ID: EPA:ID00013; AZ:0701; CO:ID00013; FL(NELAP):E87893; ID:ID00013; IN:C-ID-01; KY:90142; MT:CERT0028; NM: ID00013; OR:ID200001-002; WA:C595Certifications held by Anatek Labs WA: EPA:WA00169; ID:WA00169; WA:C585; MT:Cert0095
Page 56 of 60 8/9/2012
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Login Report
Anatek Labs, Inc.1282 Alturas Drive • Moscow, ID 83843 • (208) 883-2839 • Fax (208) 882-9246 • email [email protected]
504 E Sprague Ste. D • Spokane WA 99202 • (509) 838-3999 • Fax (509) 838-4433 • email [email protected]
Order ID: 120716027Customer Name: TEST AMERICA - HONOLULU, HI
99-193 AIEA HEIGHTS DRIVE
Contact Name: KRISTIE REILLY
Comment:
Order Date: 7/16/2012
Project Name: HVG0027
AIEA HI 96701-3900
Sample #: 120716027-001
Date Collected: 7/10/2012
Date Received: 7/16/2012 10:53:00 A
Customer Sample #: HVG0027-05 (UW BH 3 7 - SOLID/SOIL)
Comment:
Collector:
Matrix: SoilQuantity: 2
Recv'd:
Test Method Due Date PriorityLab
%Moisture 7/26/2012%moisture Normal (6-10 Days)M
PEST SCREEN TAHH 8270 7/26/2012EPA 8270CMOD Normal (6-10 Days)M
Sample #: 120716027-002
Date Collected: 7/10/2012
Date Received: 7/16/2012 10:53:00 A
Customer Sample #: HVG0027-06 (UW BH 4 6 - SOLID/SOIL)
Comment:
Collector:
Matrix: SoilQuantity: 2
Recv'd:
Test Method Due Date PriorityLab
%Moisture 7/26/2012%moisture Normal (6-10 Days)M
PEST SCREEN TAHH 8270 7/26/2012EPA 8270CMOD Normal (6-10 Days)M
SAMPLE CONDITION RECORD
Samples received in a cooler? Yes
Samples received intact? Yes
What is the temperature inside the cooler? 5.4
Samples received with a COC? Yes
Samples received within holding time? Yes
Are all sample bottles properly preserved? Yes
Are VOC samples free of headspace? N/A
Is there a trip blank to accompany VOC samples? N/A
Labels and chain agree? Yes
Page 57 of 60 8/9/2012
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Page 58 of 60 8/9/2012
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Page 59 of 60 8/9/2012
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Login Sample Receipt Checklist
Client: Bureau Veritas North America, Inc. Job Number: 580-33932-1
Login Number: 33932
Question Answer Comment
Creator: Riley, Nicole
List Source: TestAmerica Seattle
List Number: 1
TrueRadioactivity either was not measured or, if measured, is at or below
background
N/AThe cooler's custody seal, if present, is intact. Not present
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice. Water present in cooler; indicates evidence of
melted ice.
FalseCooler Temperature is acceptable. Cooler temperature outside required temperature
criteria.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the sample IDs on the containers and
the COC.
Samples logged in according to client ID
matching TA-Hon lab numbers.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided. Logged in according to date/time on COC-
TA-Hon labels do not list date or time.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AVOA sample vials do not have headspace or bubble is <6mm (1/4") in
diameter.
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked. No analysis requiring residual chlorine check
assigned.
TestAmerica SeattlePage 60 of 60 8/9/2012
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ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Seattle5755 8th Street EastTacoma, WA 98424Tel: (253)922-2310
TestAmerica Job ID: 580-33901-1Client Project/Site: Urban Works Phase II
For:Bureau Veritas North America, Inc.970 North Kalaheo AvenueSuite C-316Kailua, Hawaii 96734
Attn: Patrick Casey
Authorized for release by:8/20/2012 2:12:49 PM
Pam JohnsonProject Manager [email protected]
This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Bureau Veritas North America, Inc.Project/Site: Urban Works Phase II
TestAmerica Job ID: 580-33901-1
Page 2 of 48TestAmerica Seattle
8/20/2012
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33
Subcontract Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48
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Case NarrativeClient: Bureau Veritas North America, Inc. TestAmerica Job ID: 580-33901-1
Project/Site: Urban Works Phase II
Job ID: 580-33901-1
Laboratory: TestAmerica Seattle
Narrative
Receipt
The samples were received on 7/12/2012 9:35 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperatures of the 3 coolers at receipt time were 5.0º C, 5.3º C and 5.9º C.
Except:
The following sample UW MW-2 (580-33901-2) was received with headspace in one of the sample voa vial containers. The headspace in
this one container was larger than 1/4". Five HCl VOA vial containers remain for this sample without notable headsapce. The sample has
been logged in.
The container labels for the following samples UW MW-1 (580-33901-1), UW MW-2 (580-33901-2), UW MW-3 (580-33901-3) and UW
MW-4 (580-33901-4) did not match the information listed on the Chain-of-Custody (COC). The container labels for each sample list UW
BH/MW followed by the corresponding sample number for the sample IDs. The Chain-of-Custody (COC) lists the sample IDs as UW MW-
(the corresponding number) for each sample. The samples were logged in according to the Chain-of-Custody (COC) for the sample IDs
thus without the BH insert into the sample IDs.
The container labels on the VOA vial containers for the following samples UW MW-3 (580-33901-3) and MW-4 (580-33901-4) did not
match the information listed on the Chain-of-Custody (COC).
Sample UW MW-3 (580-33901-3): The container labels on the HCl preserved voa vials list a time of 11:15. The Chain-of-Custody (COC)
lists a time of 10:30 for this sample.
Sample MW-4 (580-33901-4): A time of 12:50 is listed on the container labels on each voa vial for this sample while the Chain-of-Custody
(COC) lists a time of 12:20.
In both instances listed above, the samples were logged in according to the sampling times listed on the Chain-of-Custody (COC).
GC/MS VOA
No analytical or quality issues were noted.
GC/MS VOA
No analytical or quality issues were noted.
GC/MS Semi VOA - Method 8270C SIM
In analytical batch 115710, the laboratory control sample (LCS) and / or the laboratory control sample duplicate (LCSD) for prep batch
115337 recovered low for the following analytes: naphthalene, benzo(b)fluoranthene, benzo(k)fluoranthene and fluorene. Re-extraction
and/or re-analysis was performed outside of holding time with acceptable results. Both sets of data have been reported.
No other analytical or quality issues were noted.
GC Semi VOA - Method 8081A
In analytical batch 115871, the closing continuing calibration verification (CCV# 26 and 27) associated with preparation batch 115477 did
not meet control limits. Sample matrix is suspected to have contributed to this failure, as noticed in the sample extracts. In addition, the
affected samples have been re-analyzed with similar results; therefore, the data have been qualified and reported.
In analytical batch 115871, surrogate recovery for the following samples UW MW-3 (580-33901-3) and UW MW-4 (580-33901-4) from
preparation batch 115477 was outside control limits. Evidence of matrix interference is present, as observed and noted in the sample
extracts; therefore, re-extraction was not performed. The affected samples were re-analyzed with confirming results.
No other analytical or quality issues were noted.
Metals
No analytical or quality issues were noted.
Subcontract Work - Method 8270 Pesticide Screen
This method was subcontracted to Anatek Labs Inc - Moscow Idaho. The subcontract certification is different from those listed on the
TestAmerica cover page of this final report.
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Case NarrativeClient: Bureau Veritas North America, Inc. TestAmerica Job ID: 580-33901-1
Project/Site: Urban Works Phase II
Job ID: 580-33901-1 (Continued)
Laboratory: TestAmerica Seattle (Continued)
Organic Prep
No analytical or quality issues were noted.
TestAmerica SeattlePage 4 of 48 8/20/2012
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Definitions/GlossaryTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Qualifiers
GC/MS Semi VOA
Qualifier Description
* LCS or LCSD exceeds the control limits
Qualifier
H Sample was prepped or analyzed beyond the specified holding time
GC Semi VOA
Qualifier Description
^ ICV,CCV,ICB,CCB, ISA, ISB, CRI, CRA, DLCK or MRL standard: Instrument related QC exceeds the control limits.
Qualifier
X Surrogate is outside control limits
Glossary
These commonly used abbreviations may or may not be present in this report.
☼ Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CNF Contains no Free Liquid
DL, RA, RE, IN Indicates a Dilution, Reanalysis, Re-extraction, or additional Initial metals/anion analysis of the sample
EDL Estimated Detection Limit
EPA United States Environmental Protection Agency
MDL Method Detection Limit
ML Minimum Level (Dioxin)
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RL Reporting Limit
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica SeattlePage 5 of 48 8/20/2012
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Client Sample ResultsTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33901-1Client Sample ID: UW MW-1Matrix: WaterDate Collected: 07/10/12 15:18
Date Received: 07/12/12 09:35
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Dichlorodifluoromethane ND 1.0 ug/L 07/24/12 17:30 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
5.0 ug/L 07/24/12 17:30 1Chloromethane ND
1.0 ug/L 07/24/12 17:30 1Vinyl chloride ND
5.0 ug/L 07/24/12 17:30 1Bromomethane ND
5.0 ug/L 07/24/12 17:30 1Chloroethane ND
1.0 ug/L 07/24/12 17:30 1Trichlorofluoromethane ND
1.0 ug/L 07/24/12 17:30 11,1-Dichloroethene ND
3.0 ug/L 07/24/12 17:30 1Methylene Chloride ND
1.0 ug/L 07/24/12 17:30 1trans-1,2-Dichloroethene ND
1.0 ug/L 07/24/12 17:30 11,1-Dichloroethane ND
1.0 ug/L 07/24/12 17:30 12,2-Dichloropropane ND
1.0 ug/L 07/24/12 17:30 1cis-1,2-Dichloroethene ND
1.0 ug/L 07/24/12 17:30 1Chlorobromomethane ND
1.0 ug/L 07/24/12 17:30 1Chloroform ND
1.0 ug/L 07/24/12 17:30 11,1,1-Trichloroethane ND
1.0 ug/L 07/24/12 17:30 1Carbon tetrachloride ND
1.0 ug/L 07/24/12 17:30 11,1-Dichloropropene ND
1.0 ug/L 07/24/12 17:30 1Benzene ND
1.0 ug/L 07/24/12 17:30 11,2-Dichloroethane ND
1.0 ug/L 07/24/12 17:30 1Trichloroethene ND
1.0 ug/L 07/24/12 17:30 11,2-Dichloropropane ND
1.0 ug/L 07/24/12 17:30 1Dibromomethane ND
1.0 ug/L 07/24/12 17:30 1Dichlorobromomethane ND
1.0 ug/L 07/24/12 17:30 1cis-1,3-Dichloropropene ND
1.0 ug/L 07/24/12 17:30 1Toluene ND
1.0 ug/L 07/24/12 17:30 1trans-1,3-Dichloropropene ND
1.0 ug/L 07/24/12 17:30 11,1,2-Trichloroethane ND
1.0 ug/L 07/24/12 17:30 1Tetrachloroethene ND
1.0 ug/L 07/24/12 17:30 11,3-Dichloropropane ND
1.0 ug/L 07/24/12 17:30 1Chlorodibromomethane ND
1.0 ug/L 07/24/12 17:30 1Ethylene Dibromide ND
1.0 ug/L 07/24/12 17:30 1Chlorobenzene ND
1.0 ug/L 07/24/12 17:30 1Ethylbenzene ND
1.0 ug/L 07/24/12 17:30 11,1,1,2-Tetrachloroethane ND
1.0 ug/L 07/24/12 17:30 11,1,2,2-Tetrachloroethane ND
2.0 ug/L 07/24/12 17:30 1m-Xylene & p-Xylene ND
1.0 ug/L 07/24/12 17:30 1o-Xylene ND
1.0 ug/L 07/24/12 17:30 1Styrene ND
1.0 ug/L 07/24/12 17:30 1Bromoform ND
1.0 ug/L 07/24/12 17:30 1Isopropylbenzene ND
1.0 ug/L 07/24/12 17:30 1Bromobenzene ND
1.0 ug/L 07/24/12 17:30 1N-Propylbenzene ND
1.0 ug/L 07/24/12 17:30 11,2,3-Trichloropropane ND
1.0 ug/L 07/24/12 17:30 12-Chlorotoluene ND
1.0 ug/L 07/24/12 17:30 11,3,5-Trimethylbenzene ND
1.0 ug/L 07/24/12 17:30 14-Chlorotoluene ND
1.0 ug/L 07/24/12 17:30 1tert-Butylbenzene ND
1.0 ug/L 07/24/12 17:30 11,2,4-Trimethylbenzene ND
1.0 ug/L 07/24/12 17:30 1sec-Butylbenzene ND
1.0 ug/L 07/24/12 17:30 11,3-Dichlorobenzene ND
1.0 ug/L 07/24/12 17:30 14-Isopropyltoluene ND
TestAmerica SeattlePage 6 of 48 8/20/2012
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Client Sample ResultsTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33901-1Client Sample ID: UW MW-1Matrix: WaterDate Collected: 07/10/12 15:18
Date Received: 07/12/12 09:35
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)RL MDL
1,4-Dichlorobenzene ND 1.0 ug/L 07/24/12 17:30 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 ug/L 07/24/12 17:30 1n-Butylbenzene ND
1.0 ug/L 07/24/12 17:30 11,2-Dichlorobenzene ND
2.0 ug/L 07/24/12 17:30 11,2-Dibromo-3-Chloropropane ND
1.0 ug/L 07/24/12 17:30 11,2,4-Trichlorobenzene ND
1.0 ug/L 07/24/12 17:30 11,2,3-Trichlorobenzene ND
1.0 ug/L 07/24/12 17:30 1Hexachlorobutadiene ND
1.0 ug/L 07/24/12 17:30 1Naphthalene ND
1.0 ug/L 07/24/12 17:30 1Methyl tert-butyl ether ND
Fluorobenzene (Surr) 99 80 - 120 07/24/12 17:30 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Toluene-d8 (Surr) 87 07/24/12 17:30 185 - 120
Ethylbenzene-d10 96 07/24/12 17:30 180 - 120
4-Bromofluorobenzene (Surr) 90 07/24/12 17:30 175 - 120
Trifluorotoluene (Surr) 103 07/24/12 17:30 180 - 120
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM)RL MDL
Naphthalene 0.12 * 0.10 ug/L 07/16/12 08:52 07/19/12 13:39 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.13 ug/L 07/16/12 08:52 07/19/12 13:39 102-Methylnaphthalene ND
0.10 ug/L 07/16/12 08:52 07/19/12 13:39 101-Methylnaphthalene ND
0.10 ug/L 07/16/12 08:52 07/19/12 13:39 10Acenaphthylene ND
0.10 ug/L 07/16/12 08:52 07/19/12 13:39 10Acenaphthene ND
0.10 ug/L 07/16/12 08:52 07/19/12 13:39 10Fluorene ND *
0.10 ug/L 07/16/12 08:52 07/19/12 13:39 10Phenanthrene 0.49
0.10 ug/L 07/16/12 08:52 07/19/12 13:39 10Anthracene 0.15
0.10 ug/L 07/16/12 08:52 07/19/12 13:39 10Fluoranthene 1.0
0.10 ug/L 07/16/12 08:52 07/19/12 13:39 10Pyrene 0.87
0.10 ug/L 07/16/12 08:52 07/19/12 13:39 10Benzo[a]anthracene 0.47
0.10 ug/L 07/16/12 08:52 07/19/12 13:39 10Chrysene 0.46
0.10 ug/L 07/16/12 08:52 07/19/12 13:39 10Benzo[b]fluoranthene 0.50 *
0.10 ug/L 07/16/12 08:52 07/19/12 13:39 10Benzo[k]fluoranthene 0.21 *
0.20 ug/L 07/16/12 08:52 07/19/12 13:39 10Benzo[a]pyrene 0.43
0.10 ug/L 07/16/12 08:52 07/19/12 13:39 10Indeno[1,2,3-cd]pyrene 0.38
0.10 ug/L 07/16/12 08:52 07/19/12 13:39 10Dibenz(a,h)anthracene ND
0.10 ug/L 07/16/12 08:52 07/19/12 13:39 10Benzo[g,h,i]perylene 0.34
Terphenyl-d14 75 20 - 150 07/16/12 08:52 07/19/12 13:39 10
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) - RERL MDL
Naphthalene 0.27 H 0.10 ug/L 07/20/12 10:57 07/25/12 23:24 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.13 ug/L 07/20/12 10:57 07/25/12 23:24 12-Methylnaphthalene ND H
0.10 ug/L 07/20/12 10:57 07/25/12 23:24 11-Methylnaphthalene ND H
0.10 ug/L 07/20/12 10:57 07/25/12 23:24 1Acenaphthylene ND H
0.10 ug/L 07/20/12 10:57 07/25/12 23:24 1Acenaphthene ND H
0.10 ug/L 07/20/12 10:57 07/25/12 23:24 1Fluorene ND H
0.10 ug/L 07/20/12 10:57 07/25/12 23:24 1Phenanthrene 0.16 H
0.10 ug/L 07/20/12 10:57 07/25/12 23:24 1Anthracene ND H
0.10 ug/L 07/20/12 10:57 07/25/12 23:24 1Fluoranthene 0.14 H
TestAmerica SeattlePage 7 of 48 8/20/2012
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Client Sample ResultsTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33901-1Client Sample ID: UW MW-1Matrix: WaterDate Collected: 07/10/12 15:18
Date Received: 07/12/12 09:35
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) - RE (Continued)RL MDL
Pyrene 0.12 H 0.10 ug/L 07/20/12 10:57 07/25/12 23:24 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.10 ug/L 07/20/12 10:57 07/25/12 23:24 1Benzo[a]anthracene ND H
0.10 ug/L 07/20/12 10:57 07/25/12 23:24 1Chrysene ND H
0.10 ug/L 07/20/12 10:57 07/25/12 23:24 1Benzo[b]fluoranthene ND H
0.10 ug/L 07/20/12 10:57 07/25/12 23:24 1Benzo[k]fluoranthene ND H
0.20 ug/L 07/20/12 10:57 07/25/12 23:24 1Benzo[a]pyrene ND H
0.10 ug/L 07/20/12 10:57 07/25/12 23:24 1Indeno[1,2,3-cd]pyrene ND H
0.10 ug/L 07/20/12 10:57 07/25/12 23:24 1Dibenz(a,h)anthracene ND H
0.10 ug/L 07/20/12 10:57 07/25/12 23:24 1Benzo[g,h,i]perylene ND H
Terphenyl-d14 87 20 - 150 07/20/12 10:57 07/25/12 23:24 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Gasoline Range Organics - (GC)RL MDL
HI Gasoline Range Organic (C6-C12) ND 0.050 mg/L 07/16/12 13:11 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 101 70 - 130 07/16/12 13:11 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Trifluorotoluene (Surr) 113 07/16/12 13:11 170 - 130
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
HI Diesel Range Organics (>C12-C24) ND 0.25 mg/L 07/16/12 09:10 07/17/12 23:07 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 mg/L 07/16/12 09:10 07/17/12 23:07 1HI Residual Range Organics
(>C24-C32)
1.4
o-Terphenyl 82 50 - 150 07/16/12 09:10 07/17/12 23:07 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 6010B - Metals (ICP) - DissolvedRL MDL
Cadmium ND 0.010 mg/L 07/23/12 10:35 07/24/12 20:44 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.030 mg/L 07/23/12 10:35 07/24/12 20:44 1Lead ND
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Client Sample ResultsTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33901-2Client Sample ID: UW MW-2Matrix: WaterDate Collected: 07/10/12 14:22
Date Received: 07/12/12 09:35
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Dichlorodifluoromethane ND 1.0 ug/L 07/24/12 17:54 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
5.0 ug/L 07/24/12 17:54 1Chloromethane ND
1.0 ug/L 07/24/12 17:54 1Vinyl chloride ND
5.0 ug/L 07/24/12 17:54 1Bromomethane ND
5.0 ug/L 07/24/12 17:54 1Chloroethane ND
1.0 ug/L 07/24/12 17:54 1Trichlorofluoromethane ND
1.0 ug/L 07/24/12 17:54 11,1-Dichloroethene ND
3.0 ug/L 07/24/12 17:54 1Methylene Chloride ND
1.0 ug/L 07/24/12 17:54 1trans-1,2-Dichloroethene ND
1.0 ug/L 07/24/12 17:54 11,1-Dichloroethane ND
1.0 ug/L 07/24/12 17:54 12,2-Dichloropropane ND
1.0 ug/L 07/24/12 17:54 1cis-1,2-Dichloroethene ND
1.0 ug/L 07/24/12 17:54 1Chlorobromomethane ND
1.0 ug/L 07/24/12 17:54 1Chloroform ND
1.0 ug/L 07/24/12 17:54 11,1,1-Trichloroethane ND
1.0 ug/L 07/24/12 17:54 1Carbon tetrachloride ND
1.0 ug/L 07/24/12 17:54 11,1-Dichloropropene ND
1.0 ug/L 07/24/12 17:54 1Benzene ND
1.0 ug/L 07/24/12 17:54 11,2-Dichloroethane ND
1.0 ug/L 07/24/12 17:54 1Trichloroethene ND
1.0 ug/L 07/24/12 17:54 11,2-Dichloropropane ND
1.0 ug/L 07/24/12 17:54 1Dibromomethane ND
1.0 ug/L 07/24/12 17:54 1Dichlorobromomethane ND
1.0 ug/L 07/24/12 17:54 1cis-1,3-Dichloropropene ND
1.0 ug/L 07/24/12 17:54 1Toluene ND
1.0 ug/L 07/24/12 17:54 1trans-1,3-Dichloropropene ND
1.0 ug/L 07/24/12 17:54 11,1,2-Trichloroethane ND
1.0 ug/L 07/24/12 17:54 1Tetrachloroethene ND
1.0 ug/L 07/24/12 17:54 11,3-Dichloropropane ND
1.0 ug/L 07/24/12 17:54 1Chlorodibromomethane ND
1.0 ug/L 07/24/12 17:54 1Ethylene Dibromide ND
1.0 ug/L 07/24/12 17:54 1Chlorobenzene ND
1.0 ug/L 07/24/12 17:54 1Ethylbenzene ND
1.0 ug/L 07/24/12 17:54 11,1,1,2-Tetrachloroethane ND
1.0 ug/L 07/24/12 17:54 11,1,2,2-Tetrachloroethane ND
2.0 ug/L 07/24/12 17:54 1m-Xylene & p-Xylene ND
1.0 ug/L 07/24/12 17:54 1o-Xylene ND
1.0 ug/L 07/24/12 17:54 1Styrene ND
1.0 ug/L 07/24/12 17:54 1Bromoform ND
1.0 ug/L 07/24/12 17:54 1Isopropylbenzene ND
1.0 ug/L 07/24/12 17:54 1Bromobenzene ND
1.0 ug/L 07/24/12 17:54 1N-Propylbenzene ND
1.0 ug/L 07/24/12 17:54 11,2,3-Trichloropropane ND
1.0 ug/L 07/24/12 17:54 12-Chlorotoluene ND
1.0 ug/L 07/24/12 17:54 11,3,5-Trimethylbenzene ND
1.0 ug/L 07/24/12 17:54 14-Chlorotoluene ND
1.0 ug/L 07/24/12 17:54 1tert-Butylbenzene ND
1.0 ug/L 07/24/12 17:54 11,2,4-Trimethylbenzene ND
1.0 ug/L 07/24/12 17:54 1sec-Butylbenzene ND
1.0 ug/L 07/24/12 17:54 11,3-Dichlorobenzene ND
1.0 ug/L 07/24/12 17:54 14-Isopropyltoluene ND
TestAmerica SeattlePage 9 of 48 8/20/2012
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Client Sample ResultsTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33901-2Client Sample ID: UW MW-2Matrix: WaterDate Collected: 07/10/12 14:22
Date Received: 07/12/12 09:35
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)RL MDL
1,4-Dichlorobenzene ND 1.0 ug/L 07/24/12 17:54 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 ug/L 07/24/12 17:54 1n-Butylbenzene ND
1.0 ug/L 07/24/12 17:54 11,2-Dichlorobenzene ND
2.0 ug/L 07/24/12 17:54 11,2-Dibromo-3-Chloropropane ND
1.0 ug/L 07/24/12 17:54 11,2,4-Trichlorobenzene ND
1.0 ug/L 07/24/12 17:54 11,2,3-Trichlorobenzene ND
1.0 ug/L 07/24/12 17:54 1Hexachlorobutadiene ND
1.0 ug/L 07/24/12 17:54 1Naphthalene ND
1.0 ug/L 07/24/12 17:54 1Methyl tert-butyl ether ND
Fluorobenzene (Surr) 97 80 - 120 07/24/12 17:54 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Toluene-d8 (Surr) 89 07/24/12 17:54 185 - 120
Ethylbenzene-d10 101 07/24/12 17:54 180 - 120
4-Bromofluorobenzene (Surr) 94 07/24/12 17:54 175 - 120
Trifluorotoluene (Surr) 100 07/24/12 17:54 180 - 120
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM)RL MDL
Naphthalene ND * 0.10 ug/L 07/16/12 08:52 07/19/12 14:01 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.13 ug/L 07/16/12 08:52 07/19/12 14:01 102-Methylnaphthalene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:01 101-Methylnaphthalene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:01 10Acenaphthylene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:01 10Acenaphthene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:01 10Fluorene ND *
0.10 ug/L 07/16/12 08:52 07/19/12 14:01 10Phenanthrene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:01 10Anthracene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:01 10Fluoranthene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:01 10Pyrene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:01 10Benzo[a]anthracene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:01 10Chrysene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:01 10Benzo[b]fluoranthene ND *
0.10 ug/L 07/16/12 08:52 07/19/12 14:01 10Benzo[k]fluoranthene ND *
0.20 ug/L 07/16/12 08:52 07/19/12 14:01 10Benzo[a]pyrene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:01 10Indeno[1,2,3-cd]pyrene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:01 10Dibenz(a,h)anthracene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:01 10Benzo[g,h,i]perylene ND
Terphenyl-d14 72 20 - 150 07/16/12 08:52 07/19/12 14:01 10
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) - RERL MDL
Naphthalene ND H 0.10 ug/L 07/20/12 10:57 07/25/12 23:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.13 ug/L 07/20/12 10:57 07/25/12 23:46 12-Methylnaphthalene ND H
0.10 ug/L 07/20/12 10:57 07/25/12 23:46 11-Methylnaphthalene ND H
0.10 ug/L 07/20/12 10:57 07/25/12 23:46 1Acenaphthylene ND H
0.10 ug/L 07/20/12 10:57 07/25/12 23:46 1Acenaphthene ND H
0.10 ug/L 07/20/12 10:57 07/25/12 23:46 1Fluorene ND H
0.10 ug/L 07/20/12 10:57 07/25/12 23:46 1Phenanthrene ND H
0.10 ug/L 07/20/12 10:57 07/25/12 23:46 1Anthracene ND H
0.10 ug/L 07/20/12 10:57 07/25/12 23:46 1Fluoranthene ND H
TestAmerica SeattlePage 10 of 48 8/20/2012
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Client Sample ResultsTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33901-2Client Sample ID: UW MW-2Matrix: WaterDate Collected: 07/10/12 14:22
Date Received: 07/12/12 09:35
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) - RE (Continued)RL MDL
Pyrene ND H 0.10 ug/L 07/20/12 10:57 07/25/12 23:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.10 ug/L 07/20/12 10:57 07/25/12 23:46 1Benzo[a]anthracene ND H
0.10 ug/L 07/20/12 10:57 07/25/12 23:46 1Chrysene ND H
0.10 ug/L 07/20/12 10:57 07/25/12 23:46 1Benzo[b]fluoranthene ND H
0.10 ug/L 07/20/12 10:57 07/25/12 23:46 1Benzo[k]fluoranthene ND H
0.20 ug/L 07/20/12 10:57 07/25/12 23:46 1Benzo[a]pyrene ND H
0.10 ug/L 07/20/12 10:57 07/25/12 23:46 1Indeno[1,2,3-cd]pyrene ND H
0.10 ug/L 07/20/12 10:57 07/25/12 23:46 1Dibenz(a,h)anthracene ND H
0.10 ug/L 07/20/12 10:57 07/25/12 23:46 1Benzo[g,h,i]perylene ND H
Terphenyl-d14 77 20 - 150 07/20/12 10:57 07/25/12 23:46 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Gasoline Range Organics - (GC)RL MDL
HI Gasoline Range Organic (C6-C12) ND 0.050 mg/L 07/16/12 14:17 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 99 70 - 130 07/16/12 14:17 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Trifluorotoluene (Surr) 106 07/16/12 14:17 170 - 130
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
HI Diesel Range Organics (>C12-C24) ND 0.25 mg/L 07/16/12 09:10 07/17/12 23:29 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 mg/L 07/16/12 09:10 07/17/12 23:29 1HI Residual Range Organics
(>C24-C32)
ND
o-Terphenyl 80 50 - 150 07/16/12 09:10 07/17/12 23:29 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 6010B - Metals (ICP) - DissolvedRL MDL
Cadmium ND 0.010 mg/L 07/23/12 10:35 07/24/12 20:50 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.030 mg/L 07/23/12 10:35 07/24/12 20:50 1Lead ND
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Client Sample ResultsTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33901-3Client Sample ID: UW MW-3Matrix: WaterDate Collected: 07/10/12 10:30
Date Received: 07/12/12 09:35
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Dichlorodifluoromethane ND 1.0 ug/L 07/24/12 18:18 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
5.0 ug/L 07/24/12 18:18 1Chloromethane ND
1.0 ug/L 07/24/12 18:18 1Vinyl chloride ND
5.0 ug/L 07/24/12 18:18 1Bromomethane ND
5.0 ug/L 07/24/12 18:18 1Chloroethane ND
1.0 ug/L 07/24/12 18:18 1Trichlorofluoromethane ND
1.0 ug/L 07/24/12 18:18 11,1-Dichloroethene ND
3.0 ug/L 07/24/12 18:18 1Methylene Chloride ND
1.0 ug/L 07/24/12 18:18 1trans-1,2-Dichloroethene ND
1.0 ug/L 07/24/12 18:18 11,1-Dichloroethane ND
1.0 ug/L 07/24/12 18:18 12,2-Dichloropropane ND
1.0 ug/L 07/24/12 18:18 1cis-1,2-Dichloroethene ND
1.0 ug/L 07/24/12 18:18 1Chlorobromomethane ND
1.0 ug/L 07/24/12 18:18 1Chloroform ND
1.0 ug/L 07/24/12 18:18 11,1,1-Trichloroethane ND
1.0 ug/L 07/24/12 18:18 1Carbon tetrachloride ND
1.0 ug/L 07/24/12 18:18 11,1-Dichloropropene ND
1.0 ug/L 07/24/12 18:18 1Benzene ND
1.0 ug/L 07/24/12 18:18 11,2-Dichloroethane ND
1.0 ug/L 07/24/12 18:18 1Trichloroethene ND
1.0 ug/L 07/24/12 18:18 11,2-Dichloropropane ND
1.0 ug/L 07/24/12 18:18 1Dibromomethane ND
1.0 ug/L 07/24/12 18:18 1Dichlorobromomethane ND
1.0 ug/L 07/24/12 18:18 1cis-1,3-Dichloropropene ND
1.0 ug/L 07/24/12 18:18 1Toluene ND
1.0 ug/L 07/24/12 18:18 1trans-1,3-Dichloropropene ND
1.0 ug/L 07/24/12 18:18 11,1,2-Trichloroethane ND
1.0 ug/L 07/24/12 18:18 1Tetrachloroethene ND
1.0 ug/L 07/24/12 18:18 11,3-Dichloropropane ND
1.0 ug/L 07/24/12 18:18 1Chlorodibromomethane ND
1.0 ug/L 07/24/12 18:18 1Ethylene Dibromide ND
1.0 ug/L 07/24/12 18:18 1Chlorobenzene ND
1.0 ug/L 07/24/12 18:18 1Ethylbenzene ND
1.0 ug/L 07/24/12 18:18 11,1,1,2-Tetrachloroethane ND
1.0 ug/L 07/24/12 18:18 11,1,2,2-Tetrachloroethane ND
2.0 ug/L 07/24/12 18:18 1m-Xylene & p-Xylene ND
1.0 ug/L 07/24/12 18:18 1o-Xylene ND
1.0 ug/L 07/24/12 18:18 1Styrene ND
1.0 ug/L 07/24/12 18:18 1Bromoform ND
1.0 ug/L 07/24/12 18:18 1Isopropylbenzene ND
1.0 ug/L 07/24/12 18:18 1Bromobenzene ND
1.0 ug/L 07/24/12 18:18 1N-Propylbenzene ND
1.0 ug/L 07/24/12 18:18 11,2,3-Trichloropropane ND
1.0 ug/L 07/24/12 18:18 12-Chlorotoluene ND
1.0 ug/L 07/24/12 18:18 11,3,5-Trimethylbenzene ND
1.0 ug/L 07/24/12 18:18 14-Chlorotoluene ND
1.0 ug/L 07/24/12 18:18 1tert-Butylbenzene ND
1.0 ug/L 07/24/12 18:18 11,2,4-Trimethylbenzene ND
1.0 ug/L 07/24/12 18:18 1sec-Butylbenzene ND
1.0 ug/L 07/24/12 18:18 11,3-Dichlorobenzene ND
1.0 ug/L 07/24/12 18:18 14-Isopropyltoluene ND
TestAmerica SeattlePage 12 of 48 8/20/2012
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Client Sample ResultsTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33901-3Client Sample ID: UW MW-3Matrix: WaterDate Collected: 07/10/12 10:30
Date Received: 07/12/12 09:35
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)RL MDL
1,4-Dichlorobenzene ND 1.0 ug/L 07/24/12 18:18 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 ug/L 07/24/12 18:18 1n-Butylbenzene ND
1.0 ug/L 07/24/12 18:18 11,2-Dichlorobenzene ND
2.0 ug/L 07/24/12 18:18 11,2-Dibromo-3-Chloropropane ND
1.0 ug/L 07/24/12 18:18 11,2,4-Trichlorobenzene ND
1.0 ug/L 07/24/12 18:18 11,2,3-Trichlorobenzene ND
1.0 ug/L 07/24/12 18:18 1Hexachlorobutadiene ND
1.0 ug/L 07/24/12 18:18 1Naphthalene ND
1.0 ug/L 07/24/12 18:18 1Methyl tert-butyl ether ND
Fluorobenzene (Surr) 96 80 - 120 07/24/12 18:18 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Toluene-d8 (Surr) 87 07/24/12 18:18 185 - 120
Ethylbenzene-d10 99 07/24/12 18:18 180 - 120
4-Bromofluorobenzene (Surr) 92 07/24/12 18:18 175 - 120
Trifluorotoluene (Surr) 99 07/24/12 18:18 180 - 120
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM)RL MDL
Naphthalene ND * 0.10 ug/L 07/16/12 08:52 07/19/12 14:23 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.13 ug/L 07/16/12 08:52 07/19/12 14:23 102-Methylnaphthalene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:23 101-Methylnaphthalene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:23 10Acenaphthylene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:23 10Acenaphthene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:23 10Fluorene ND *
0.10 ug/L 07/16/12 08:52 07/19/12 14:23 10Phenanthrene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:23 10Anthracene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:23 10Fluoranthene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:23 10Pyrene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:23 10Benzo[a]anthracene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:23 10Chrysene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:23 10Benzo[b]fluoranthene ND *
0.10 ug/L 07/16/12 08:52 07/19/12 14:23 10Benzo[k]fluoranthene ND *
0.20 ug/L 07/16/12 08:52 07/19/12 14:23 10Benzo[a]pyrene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:23 10Indeno[1,2,3-cd]pyrene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:23 10Dibenz(a,h)anthracene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:23 10Benzo[g,h,i]perylene ND
Terphenyl-d14 75 20 - 150 07/16/12 08:52 07/19/12 14:23 10
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) - RERL MDL
Naphthalene ND H 0.10 ug/L 07/20/12 10:57 07/26/12 00:08 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.13 ug/L 07/20/12 10:57 07/26/12 00:08 12-Methylnaphthalene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:08 11-Methylnaphthalene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:08 1Acenaphthylene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:08 1Acenaphthene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:08 1Fluorene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:08 1Phenanthrene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:08 1Anthracene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:08 1Fluoranthene ND H
TestAmerica SeattlePage 13 of 48 8/20/2012
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Client Sample ResultsTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33901-3Client Sample ID: UW MW-3Matrix: WaterDate Collected: 07/10/12 10:30
Date Received: 07/12/12 09:35
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) - RE (Continued)RL MDL
Pyrene ND H 0.10 ug/L 07/20/12 10:57 07/26/12 00:08 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.10 ug/L 07/20/12 10:57 07/26/12 00:08 1Benzo[a]anthracene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:08 1Chrysene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:08 1Benzo[b]fluoranthene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:08 1Benzo[k]fluoranthene ND H
0.20 ug/L 07/20/12 10:57 07/26/12 00:08 1Benzo[a]pyrene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:08 1Indeno[1,2,3-cd]pyrene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:08 1Dibenz(a,h)anthracene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:08 1Benzo[g,h,i]perylene ND H
Terphenyl-d14 72 20 - 150 07/20/12 10:57 07/26/12 00:08 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
HI Diesel Range Organics (>C12-C24) ND 0.25 mg/L 07/16/12 09:10 07/17/12 23:50 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 mg/L 07/16/12 09:10 07/17/12 23:50 1HI Residual Range Organics
(>C24-C32)
0.98
o-Terphenyl 80 50 - 150 07/16/12 09:10 07/17/12 23:50 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8081A - Organochlorine Pesticides (GC)RL MDL
Aldrin ND 0.010 ug/L 07/17/12 10:54 07/22/12 16:40 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.010 ug/L 07/17/12 10:54 07/22/12 16:40 1alpha-BHC ND
0.020 ug/L 07/17/12 10:54 07/22/12 16:40 1beta-BHC ND
0.010 ug/L 07/17/12 10:54 07/22/12 16:40 1delta-BHC ND
0.010 ug/L 07/17/12 10:54 07/22/12 16:40 1gamma-BHC (Lindane) ND
0.020 ug/L 07/17/12 10:54 07/22/12 16:40 14,4'-DDD ND ^
0.020 ug/L 07/17/12 10:54 07/22/12 16:40 14,4'-DDE ND
0.020 ug/L 07/17/12 10:54 07/22/12 16:40 14,4'-DDT ND ^
0.020 ug/L 07/17/12 10:54 07/22/12 16:40 1Dieldrin ND
0.020 ug/L 07/17/12 10:54 07/22/12 16:40 1Endosulfan I ND
0.020 ug/L 07/17/12 10:54 07/22/12 16:40 1Endosulfan II ND
0.020 ug/L 07/17/12 10:54 07/22/12 16:40 1Endosulfan sulfate ND
0.020 ug/L 07/17/12 10:54 07/22/12 16:40 1Endrin ND
0.050 ug/L 07/17/12 10:54 07/22/12 16:40 1Endrin aldehyde ND
0.010 ug/L 07/17/12 10:54 07/22/12 16:40 1Heptachlor ND
0.010 ug/L 07/17/12 10:54 07/22/12 16:40 1Heptachlor epoxide ND
0.10 ug/L 07/17/12 10:54 07/22/12 16:40 1Methoxychlor ND ^
0.020 ug/L 07/17/12 10:54 07/22/12 16:40 1Endrin ketone ND
1.0 ug/L 07/17/12 10:54 07/22/12 16:40 1Toxaphene ND
0.010 ug/L 07/17/12 10:54 07/22/12 16:40 1alpha-Chlordane ND
0.010 ug/L 07/17/12 10:54 07/22/12 16:40 1gamma-Chlordane ND
Tetrachloro-m-xylene 72 18 - 181 07/17/12 10:54 07/22/12 16:40 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
DCB Decachlorobiphenyl 36 X 07/17/12 10:54 07/22/12 16:40 153 - 122
Method: 6010B - Metals (ICP) - DissolvedRL MDL
Arsenic ND 0.060 mg/L 07/23/12 10:35 07/24/12 20:57 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33901-4Client Sample ID: UW MW-4Matrix: WaterDate Collected: 07/10/12 12:20
Date Received: 07/12/12 09:35
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Dichlorodifluoromethane ND 1.0 ug/L 07/24/12 18:44 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
5.0 ug/L 07/24/12 18:44 1Chloromethane ND
1.0 ug/L 07/24/12 18:44 1Vinyl chloride ND
5.0 ug/L 07/24/12 18:44 1Bromomethane ND
5.0 ug/L 07/24/12 18:44 1Chloroethane ND
1.0 ug/L 07/24/12 18:44 1Trichlorofluoromethane ND
1.0 ug/L 07/24/12 18:44 11,1-Dichloroethene ND
3.0 ug/L 07/24/12 18:44 1Methylene Chloride ND
1.0 ug/L 07/24/12 18:44 1trans-1,2-Dichloroethene ND
1.0 ug/L 07/24/12 18:44 11,1-Dichloroethane ND
1.0 ug/L 07/24/12 18:44 12,2-Dichloropropane ND
1.0 ug/L 07/24/12 18:44 1cis-1,2-Dichloroethene ND
1.0 ug/L 07/24/12 18:44 1Chlorobromomethane ND
1.0 ug/L 07/24/12 18:44 1Chloroform ND
1.0 ug/L 07/24/12 18:44 11,1,1-Trichloroethane ND
1.0 ug/L 07/24/12 18:44 1Carbon tetrachloride ND
1.0 ug/L 07/24/12 18:44 11,1-Dichloropropene ND
1.0 ug/L 07/24/12 18:44 1Benzene ND
1.0 ug/L 07/24/12 18:44 11,2-Dichloroethane ND
1.0 ug/L 07/24/12 18:44 1Trichloroethene ND
1.0 ug/L 07/24/12 18:44 11,2-Dichloropropane ND
1.0 ug/L 07/24/12 18:44 1Dibromomethane ND
1.0 ug/L 07/24/12 18:44 1Dichlorobromomethane ND
1.0 ug/L 07/24/12 18:44 1cis-1,3-Dichloropropene ND
1.0 ug/L 07/24/12 18:44 1Toluene ND
1.0 ug/L 07/24/12 18:44 1trans-1,3-Dichloropropene ND
1.0 ug/L 07/24/12 18:44 11,1,2-Trichloroethane ND
1.0 ug/L 07/24/12 18:44 1Tetrachloroethene ND
1.0 ug/L 07/24/12 18:44 11,3-Dichloropropane ND
1.0 ug/L 07/24/12 18:44 1Chlorodibromomethane ND
1.0 ug/L 07/24/12 18:44 1Ethylene Dibromide ND
1.0 ug/L 07/24/12 18:44 1Chlorobenzene ND
1.0 ug/L 07/24/12 18:44 1Ethylbenzene ND
1.0 ug/L 07/24/12 18:44 11,1,1,2-Tetrachloroethane ND
1.0 ug/L 07/24/12 18:44 11,1,2,2-Tetrachloroethane ND
2.0 ug/L 07/24/12 18:44 1m-Xylene & p-Xylene ND
1.0 ug/L 07/24/12 18:44 1o-Xylene ND
1.0 ug/L 07/24/12 18:44 1Styrene ND
1.0 ug/L 07/24/12 18:44 1Bromoform ND
1.0 ug/L 07/24/12 18:44 1Isopropylbenzene ND
1.0 ug/L 07/24/12 18:44 1Bromobenzene ND
1.0 ug/L 07/24/12 18:44 1N-Propylbenzene ND
1.0 ug/L 07/24/12 18:44 11,2,3-Trichloropropane ND
1.0 ug/L 07/24/12 18:44 12-Chlorotoluene ND
1.0 ug/L 07/24/12 18:44 11,3,5-Trimethylbenzene ND
1.0 ug/L 07/24/12 18:44 14-Chlorotoluene ND
1.0 ug/L 07/24/12 18:44 1tert-Butylbenzene ND
1.0 ug/L 07/24/12 18:44 11,2,4-Trimethylbenzene ND
1.0 ug/L 07/24/12 18:44 1sec-Butylbenzene ND
1.0 ug/L 07/24/12 18:44 11,3-Dichlorobenzene ND
1.0 ug/L 07/24/12 18:44 14-Isopropyltoluene ND
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Client Sample ResultsTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33901-4Client Sample ID: UW MW-4Matrix: WaterDate Collected: 07/10/12 12:20
Date Received: 07/12/12 09:35
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)RL MDL
1,4-Dichlorobenzene ND 1.0 ug/L 07/24/12 18:44 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 ug/L 07/24/12 18:44 1n-Butylbenzene ND
1.0 ug/L 07/24/12 18:44 11,2-Dichlorobenzene ND
2.0 ug/L 07/24/12 18:44 11,2-Dibromo-3-Chloropropane ND
1.0 ug/L 07/24/12 18:44 11,2,4-Trichlorobenzene ND
1.0 ug/L 07/24/12 18:44 11,2,3-Trichlorobenzene ND
1.0 ug/L 07/24/12 18:44 1Hexachlorobutadiene ND
1.0 ug/L 07/24/12 18:44 1Naphthalene ND
1.0 ug/L 07/24/12 18:44 1Methyl tert-butyl ether ND
Fluorobenzene (Surr) 97 80 - 120 07/24/12 18:44 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Toluene-d8 (Surr) 86 07/24/12 18:44 185 - 120
Ethylbenzene-d10 101 07/24/12 18:44 180 - 120
4-Bromofluorobenzene (Surr) 91 07/24/12 18:44 175 - 120
Trifluorotoluene (Surr) 99 07/24/12 18:44 180 - 120
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM)RL MDL
Naphthalene ND * 0.10 ug/L 07/16/12 08:52 07/19/12 14:45 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.13 ug/L 07/16/12 08:52 07/19/12 14:45 102-Methylnaphthalene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:45 101-Methylnaphthalene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:45 10Acenaphthylene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:45 10Acenaphthene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:45 10Fluorene ND *
0.10 ug/L 07/16/12 08:52 07/19/12 14:45 10Phenanthrene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:45 10Anthracene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:45 10Fluoranthene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:45 10Pyrene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:45 10Benzo[a]anthracene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:45 10Chrysene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:45 10Benzo[b]fluoranthene ND *
0.10 ug/L 07/16/12 08:52 07/19/12 14:45 10Benzo[k]fluoranthene ND *
0.20 ug/L 07/16/12 08:52 07/19/12 14:45 10Benzo[a]pyrene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:45 10Indeno[1,2,3-cd]pyrene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:45 10Dibenz(a,h)anthracene ND
0.10 ug/L 07/16/12 08:52 07/19/12 14:45 10Benzo[g,h,i]perylene ND
Terphenyl-d14 75 20 - 150 07/16/12 08:52 07/19/12 14:45 10
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) - RERL MDL
Naphthalene ND H 0.10 ug/L 07/20/12 10:57 07/26/12 00:31 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.13 ug/L 07/20/12 10:57 07/26/12 00:31 12-Methylnaphthalene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:31 11-Methylnaphthalene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:31 1Acenaphthylene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:31 1Acenaphthene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:31 1Fluorene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:31 1Phenanthrene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:31 1Anthracene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:31 1Fluoranthene ND H
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Client Sample ResultsTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID: 580-33901-4Client Sample ID: UW MW-4Matrix: WaterDate Collected: 07/10/12 12:20
Date Received: 07/12/12 09:35
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) - RE (Continued)RL MDL
Pyrene ND H 0.10 ug/L 07/20/12 10:57 07/26/12 00:31 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.10 ug/L 07/20/12 10:57 07/26/12 00:31 1Benzo[a]anthracene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:31 1Chrysene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:31 1Benzo[b]fluoranthene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:31 1Benzo[k]fluoranthene ND H
0.20 ug/L 07/20/12 10:57 07/26/12 00:31 1Benzo[a]pyrene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:31 1Indeno[1,2,3-cd]pyrene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:31 1Dibenz(a,h)anthracene ND H
0.10 ug/L 07/20/12 10:57 07/26/12 00:31 1Benzo[g,h,i]perylene ND H
Terphenyl-d14 82 20 - 150 07/20/12 10:57 07/26/12 00:31 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
HI Diesel Range Organics (>C12-C24) ND 0.25 mg/L 07/16/12 09:10 07/18/12 00:12 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 mg/L 07/16/12 09:10 07/18/12 00:12 1HI Residual Range Organics
(>C24-C32)
ND
o-Terphenyl 81 50 - 150 07/16/12 09:10 07/18/12 00:12 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8081A - Organochlorine Pesticides (GC)RL MDL
Aldrin ND 0.010 ug/L 07/17/12 10:54 07/22/12 16:56 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.010 ug/L 07/17/12 10:54 07/22/12 16:56 1alpha-BHC ND
0.020 ug/L 07/17/12 10:54 07/22/12 16:56 1beta-BHC ND
0.010 ug/L 07/17/12 10:54 07/22/12 16:56 1delta-BHC ND
0.010 ug/L 07/17/12 10:54 07/22/12 16:56 1gamma-BHC (Lindane) ND
0.020 ug/L 07/17/12 10:54 07/22/12 16:56 14,4'-DDD ND ^
0.020 ug/L 07/17/12 10:54 07/22/12 16:56 14,4'-DDE ND
0.020 ug/L 07/17/12 10:54 07/22/12 16:56 14,4'-DDT ND ^
0.020 ug/L 07/17/12 10:54 07/22/12 16:56 1Dieldrin ND
0.020 ug/L 07/17/12 10:54 07/22/12 16:56 1Endosulfan I ND
0.020 ug/L 07/17/12 10:54 07/22/12 16:56 1Endosulfan II ND
0.020 ug/L 07/17/12 10:54 07/22/12 16:56 1Endosulfan sulfate ND
0.020 ug/L 07/17/12 10:54 07/22/12 16:56 1Endrin ND
0.050 ug/L 07/17/12 10:54 07/22/12 16:56 1Endrin aldehyde ND
0.010 ug/L 07/17/12 10:54 07/22/12 16:56 1Heptachlor ND
0.010 ug/L 07/17/12 10:54 07/22/12 16:56 1Heptachlor epoxide ND
0.10 ug/L 07/17/12 10:54 07/22/12 16:56 1Methoxychlor ND ^
0.020 ug/L 07/17/12 10:54 07/22/12 16:56 1Endrin ketone ND
1.0 ug/L 07/17/12 10:54 07/22/12 16:56 1Toxaphene ND
0.010 ug/L 07/17/12 10:54 07/22/12 16:56 1alpha-Chlordane ND
0.010 ug/L 07/17/12 10:54 07/22/12 16:56 1gamma-Chlordane ND
Tetrachloro-m-xylene 67 18 - 181 07/17/12 10:54 07/22/12 16:56 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
DCB Decachlorobiphenyl 32 X 07/17/12 10:54 07/22/12 16:56 153 - 122
Method: 6010B - Metals (ICP) - DissolvedRL MDL
Arsenic ND 0.060 mg/L 07/23/12 10:35 07/24/12 21:04 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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QC Sample ResultsTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 580-116018/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 116018
RL MDL
Dichlorodifluoromethane ND 1.0 ug/L 07/24/12 13:09 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 5.0 ug/L 07/24/12 13:09 1Chloromethane
ND 1.0 ug/L 07/24/12 13:09 1Vinyl chloride
ND 5.0 ug/L 07/24/12 13:09 1Bromomethane
ND 5.0 ug/L 07/24/12 13:09 1Chloroethane
ND 1.0 ug/L 07/24/12 13:09 1Trichlorofluoromethane
ND 1.0 ug/L 07/24/12 13:09 11,1-Dichloroethene
ND 3.0 ug/L 07/24/12 13:09 1Methylene Chloride
ND 1.0 ug/L 07/24/12 13:09 1trans-1,2-Dichloroethene
ND 1.0 ug/L 07/24/12 13:09 11,1-Dichloroethane
ND 1.0 ug/L 07/24/12 13:09 12,2-Dichloropropane
ND 1.0 ug/L 07/24/12 13:09 1cis-1,2-Dichloroethene
ND 1.0 ug/L 07/24/12 13:09 1Chlorobromomethane
ND 1.0 ug/L 07/24/12 13:09 1Chloroform
ND 1.0 ug/L 07/24/12 13:09 11,1,1-Trichloroethane
ND 1.0 ug/L 07/24/12 13:09 1Carbon tetrachloride
ND 1.0 ug/L 07/24/12 13:09 11,1-Dichloropropene
ND 1.0 ug/L 07/24/12 13:09 1Benzene
ND 1.0 ug/L 07/24/12 13:09 11,2-Dichloroethane
ND 1.0 ug/L 07/24/12 13:09 1Trichloroethene
ND 1.0 ug/L 07/24/12 13:09 11,2-Dichloropropane
ND 1.0 ug/L 07/24/12 13:09 1Dibromomethane
ND 1.0 ug/L 07/24/12 13:09 1Dichlorobromomethane
ND 1.0 ug/L 07/24/12 13:09 1cis-1,3-Dichloropropene
ND 1.0 ug/L 07/24/12 13:09 1Toluene
ND 1.0 ug/L 07/24/12 13:09 1trans-1,3-Dichloropropene
ND 1.0 ug/L 07/24/12 13:09 11,1,2-Trichloroethane
ND 1.0 ug/L 07/24/12 13:09 1Tetrachloroethene
ND 1.0 ug/L 07/24/12 13:09 11,3-Dichloropropane
ND 1.0 ug/L 07/24/12 13:09 1Chlorodibromomethane
ND 1.0 ug/L 07/24/12 13:09 1Ethylene Dibromide
ND 1.0 ug/L 07/24/12 13:09 1Chlorobenzene
ND 1.0 ug/L 07/24/12 13:09 1Ethylbenzene
ND 1.0 ug/L 07/24/12 13:09 11,1,1,2-Tetrachloroethane
ND 1.0 ug/L 07/24/12 13:09 11,1,2,2-Tetrachloroethane
ND 2.0 ug/L 07/24/12 13:09 1m-Xylene & p-Xylene
ND 1.0 ug/L 07/24/12 13:09 1o-Xylene
ND 1.0 ug/L 07/24/12 13:09 1Styrene
ND 1.0 ug/L 07/24/12 13:09 1Bromoform
ND 1.0 ug/L 07/24/12 13:09 1Isopropylbenzene
ND 1.0 ug/L 07/24/12 13:09 1Bromobenzene
ND 1.0 ug/L 07/24/12 13:09 1N-Propylbenzene
ND 1.0 ug/L 07/24/12 13:09 11,2,3-Trichloropropane
ND 1.0 ug/L 07/24/12 13:09 12-Chlorotoluene
ND 1.0 ug/L 07/24/12 13:09 11,3,5-Trimethylbenzene
ND 1.0 ug/L 07/24/12 13:09 14-Chlorotoluene
ND 1.0 ug/L 07/24/12 13:09 1tert-Butylbenzene
ND 1.0 ug/L 07/24/12 13:09 11,2,4-Trimethylbenzene
ND 1.0 ug/L 07/24/12 13:09 1sec-Butylbenzene
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QC Sample ResultsTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 580-116018/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 116018
RL MDL
1,3-Dichlorobenzene ND 1.0 ug/L 07/24/12 13:09 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 1.0 ug/L 07/24/12 13:09 14-Isopropyltoluene
ND 1.0 ug/L 07/24/12 13:09 11,4-Dichlorobenzene
ND 1.0 ug/L 07/24/12 13:09 1n-Butylbenzene
ND 1.0 ug/L 07/24/12 13:09 11,2-Dichlorobenzene
ND 2.0 ug/L 07/24/12 13:09 11,2-Dibromo-3-Chloropropane
ND 1.0 ug/L 07/24/12 13:09 11,2,4-Trichlorobenzene
ND 1.0 ug/L 07/24/12 13:09 11,2,3-Trichlorobenzene
ND 1.0 ug/L 07/24/12 13:09 1Hexachlorobutadiene
ND 1.0 ug/L 07/24/12 13:09 1Naphthalene
ND 1.0 ug/L 07/24/12 13:09 1Methyl tert-butyl ether
Fluorobenzene (Surr) 98 80 - 120 07/24/12 13:09 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
92 07/24/12 13:09 1Toluene-d8 (Surr) 85 - 120
106 07/24/12 13:09 1Ethylbenzene-d10 80 - 120
97 07/24/12 13:09 14-Bromofluorobenzene (Surr) 75 - 120
108 07/24/12 13:09 1Trifluorotoluene (Surr) 80 - 120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 580-116018/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 116018
Dichlorodifluoromethane 20.1 17.1 ug/L 85 30 - 155
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Chloromethane 20.0 17.9 ug/L 89 40 - 125
Vinyl chloride 20.1 18.1 ug/L 90 50 - 145
Bromomethane 20.0 18.4 ug/L 92 30 - 145
Chloroethane 20.1 18.4 ug/L 92 60 - 135
Trichlorofluoromethane 20.1 17.2 ug/L 86 60 - 145
1,1-Dichloroethene 20.1 18.9 ug/L 94 70 - 130
Methylene Chloride 20.1 19.1 ug/L 95 55 - 140
trans-1,2-Dichloroethene 20.1 18.6 ug/L 93 60 - 140
1,1-Dichloroethane 20.1 17.5 ug/L 87 70 - 135
2,2-Dichloropropane 20.0 22.1 ug/L 110 70 - 135
cis-1,2-Dichloroethene 20.1 21.0 ug/L 104 70 - 125
Chlorobromomethane 20.1 20.7 ug/L 103 65 - 130
Chloroform 20.1 19.2 ug/L 96 65 - 135
1,1,1-Trichloroethane 20.1 19.8 ug/L 99 65 - 130
Carbon tetrachloride 20.1 19.5 ug/L 97 65 - 140
1,1-Dichloropropene 20.1 20.6 ug/L 102 75 - 130
Benzene 20.0 21.0 ug/L 105 80 - 120
1,2-Dichloroethane 20.1 16.8 ug/L 83 70 - 130
Trichloroethene 20.3 22.0 ug/L 108 70 - 125
1,2-Dichloropropane 20.1 21.1 ug/L 105 75 - 125
Dibromomethane 20.1 20.5 ug/L 102 75 - 125
Dichlorobromomethane 20.3 19.8 ug/L 98 75 - 120
cis-1,3-Dichloropropene 19.8 21.7 ug/L 110 70 - 130
Toluene 20.1 21.6 ug/L 108 75 - 120
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QC Sample ResultsTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 580-116018/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 116018
trans-1,3-Dichloropropene 20.4 20.7 ug/L 102 55 - 140
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
1,1,2-Trichloroethane 20.1 20.3 ug/L 101 75 - 125
Tetrachloroethene 20.0 17.7 ug/L 88 45 - 150
1,3-Dichloropropane 20.1 19.9 ug/L 99 75 - 125
Chlorodibromomethane 20.3 21.1 ug/L 104 60 - 135
Ethylene Dibromide 20.1 20.4 ug/L 101 80 - 120
Chlorobenzene 20.0 21.6 ug/L 108 80 - 120
Ethylbenzene 20.0 22.6 ug/L 113 75 - 125
1,1,1,2-Tetrachloroethane 20.1 22.0 ug/L 109 80 - 130
1,1,2,2-Tetrachloroethane 20.0 19.5 ug/L 97 65 - 130
m-Xylene & p-Xylene 40.2 42.5 ug/L 106 75 - 130
o-Xylene 20.1 21.5 ug/L 107 80 - 120
Styrene 20.1 21.5 ug/L 107 65 - 135
Bromoform 20.1 21.5 ug/L 107 70 - 130
Isopropylbenzene 20.1 22.4 ug/L 111 75 - 125
Bromobenzene 20.1 21.1 ug/L 105 75 - 125
N-Propylbenzene 20.0 23.4 ug/L 117 70 - 130
1,2,3-Trichloropropane 20.1 19.0 ug/L 95 75 - 125
2-Chlorotoluene 20.1 22.1 ug/L 110 75 - 125
1,3,5-Trimethylbenzene 20.0 22.9 ug/L 114 75 - 130
4-Chlorotoluene 20.1 21.1 ug/L 105 75 - 130
tert-Butylbenzene 20.1 22.7 ug/L 113 70 - 130
1,2,4-Trimethylbenzene 20.0 21.4 ug/L 107 75 - 130
sec-Butylbenzene 20.1 22.1 ug/L 110 70 - 125
1,3-Dichlorobenzene 20.1 21.1 ug/L 105 75 - 125
4-Isopropyltoluene 20.1 21.3 ug/L 106 75 - 130
1,4-Dichlorobenzene 20.1 20.2 ug/L 101 75 - 125
n-Butylbenzene 20.1 21.7 ug/L 108 70 - 135
1,2-Dichlorobenzene 20.1 20.8 ug/L 104 70 - 120
1,2-Dibromo-3-Chloropropane 20.1 22.6 ug/L 113 50 - 130
1,2,4-Trichlorobenzene 20.1 24.8 ug/L 123 65 - 135
1,2,3-Trichlorobenzene 20.1 24.1 ug/L 120 55 - 140
Hexachlorobutadiene 20.1 22.3 ug/L 111 50 - 140
Naphthalene 20.1 21.0 ug/L 105 55 - 140
Methyl tert-butyl ether 20.1 18.4 ug/L 92 65 - 125
Fluorobenzene (Surr) 80 - 120
Surrogate
101
LCS LCS
Qualifier Limits%Recovery
101Toluene-d8 (Surr) 85 - 120
110Ethylbenzene-d10 80 - 120
1104-Bromofluorobenzene (Surr) 75 - 120
109Trifluorotoluene (Surr) 80 - 120
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 580-116018/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 116018
Dichlorodifluoromethane 20.1 17.0 ug/L 84 30 - 155 1 30
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
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QC Sample ResultsTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 580-116018/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 116018
Chloromethane 20.0 17.2 ug/L 86 40 - 125 4 30
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Vinyl chloride 20.1 18.5 ug/L 92 50 - 145 2 30
Bromomethane 20.0 17.6 ug/L 88 30 - 145 4 30
Chloroethane 20.1 17.8 ug/L 89 60 - 135 3 30
Trichlorofluoromethane 20.1 17.0 ug/L 85 60 - 145 1 30
1,1-Dichloroethene 20.1 18.9 ug/L 94 70 - 130 0 30
Methylene Chloride 20.1 19.6 ug/L 98 55 - 140 3 30
trans-1,2-Dichloroethene 20.1 19.0 ug/L 94 60 - 140 2 30
1,1-Dichloroethane 20.1 18.0 ug/L 90 70 - 135 2 30
2,2-Dichloropropane 20.0 22.6 ug/L 113 70 - 135 2 30
cis-1,2-Dichloroethene 20.1 21.1 ug/L 105 70 - 125 1 30
Chlorobromomethane 20.1 20.8 ug/L 104 65 - 130 1 30
Chloroform 20.1 19.1 ug/L 95 65 - 135 1 30
1,1,1-Trichloroethane 20.1 20.1 ug/L 100 65 - 130 1 30
Carbon tetrachloride 20.1 19.7 ug/L 98 65 - 140 1 30
1,1-Dichloropropene 20.1 20.8 ug/L 103 75 - 130 1 30
Benzene 20.0 21.7 ug/L 108 80 - 120 3 30
1,2-Dichloroethane 20.1 16.9 ug/L 84 70 - 130 1 30
Trichloroethene 20.3 21.7 ug/L 107 70 - 125 1 30
1,2-Dichloropropane 20.1 20.4 ug/L 102 75 - 125 3 30
Dibromomethane 20.1 20.0 ug/L 99 75 - 125 3 30
Dichlorobromomethane 20.3 20.0 ug/L 99 75 - 120 1 30
cis-1,3-Dichloropropene 19.8 21.8 ug/L 110 70 - 130 0 30
Toluene 20.1 21.9 ug/L 109 75 - 120 1 30
trans-1,3-Dichloropropene 20.4 21.2 ug/L 104 55 - 140 2 30
1,1,2-Trichloroethane 20.1 19.8 ug/L 99 75 - 125 2 30
Tetrachloroethene 20.0 20.3 ug/L 101 45 - 150 14 30
1,3-Dichloropropane 20.1 20.0 ug/L 100 75 - 125 0 30
Chlorodibromomethane 20.3 21.3 ug/L 105 60 - 135 1 30
Ethylene Dibromide 20.1 20.2 ug/L 100 80 - 120 1 30
Chlorobenzene 20.0 22.7 ug/L 113 80 - 120 5 30
Ethylbenzene 20.0 22.9 ug/L 114 75 - 125 2 30
1,1,1,2-Tetrachloroethane 20.1 22.2 ug/L 110 80 - 130 1 30
1,1,2,2-Tetrachloroethane 20.0 19.8 ug/L 99 65 - 130 2 30
m-Xylene & p-Xylene 40.2 43.7 ug/L 109 75 - 130 3 30
o-Xylene 20.1 22.0 ug/L 109 80 - 120 2 30
Styrene 20.1 22.1 ug/L 110 65 - 135 2 30
Bromoform 20.1 22.0 ug/L 110 70 - 130 2 30
Isopropylbenzene 20.1 22.3 ug/L 111 75 - 125 0 30
Bromobenzene 20.1 21.3 ug/L 106 75 - 125 1 30
N-Propylbenzene 20.0 23.4 ug/L 117 70 - 130 0 30
1,2,3-Trichloropropane 20.1 19.2 ug/L 95 75 - 125 1 30
2-Chlorotoluene 20.1 22.0 ug/L 110 75 - 125 0 30
1,3,5-Trimethylbenzene 20.0 23.8 ug/L 119 75 - 130 4 30
4-Chlorotoluene 20.1 21.5 ug/L 107 75 - 130 1 30
tert-Butylbenzene 20.1 23.4 ug/L 117 70 - 130 3 30
1,2,4-Trimethylbenzene 20.0 22.1 ug/L 110 75 - 130 4 30
sec-Butylbenzene 20.1 23.0 ug/L 115 70 - 125 4 30
1,3-Dichlorobenzene 20.1 21.5 ug/L 107 75 - 125 2 30
4-Isopropyltoluene 20.1 21.3 ug/L 106 75 - 130 0 30
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QC Sample ResultsTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 580-116018/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 116018
1,4-Dichlorobenzene 20.1 20.9 ug/L 104 75 - 125 3 30
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
n-Butylbenzene 20.1 21.7 ug/L 108 70 - 135 0 30
1,2-Dichlorobenzene 20.1 21.1 ug/L 105 70 - 120 1 30
1,2-Dibromo-3-Chloropropane 20.1 23.3 ug/L 116 50 - 130 3 30
1,2,4-Trichlorobenzene 20.1 25.7 ug/L 128 65 - 135 3 30
1,2,3-Trichlorobenzene 20.1 25.4 ug/L 127 55 - 140 5 30
Hexachlorobutadiene 20.1 24.4 ug/L 122 50 - 140 9 30
Naphthalene 20.1 21.6 ug/L 108 55 - 140 3 30
Methyl tert-butyl ether 20.1 18.5 ug/L 92 65 - 125 1 30
Fluorobenzene (Surr) 80 - 120
Surrogate
101
LCSD LCSD
Qualifier Limits%Recovery
101Toluene-d8 (Surr) 85 - 120
113Ethylbenzene-d10 80 - 120
1104-Bromofluorobenzene (Surr) 75 - 120
107Trifluorotoluene (Surr) 80 - 120
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM)
Client Sample ID: Method BlankLab Sample ID: MB 580-115337/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 115710 Prep Batch: 115337
RL MDL
Naphthalene ND 0.10 ug/L 07/16/12 08:52 07/19/12 11:25 10
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.13 ug/L 07/16/12 08:52 07/19/12 11:25 102-Methylnaphthalene
ND 0.10 ug/L 07/16/12 08:52 07/19/12 11:25 101-Methylnaphthalene
ND 0.10 ug/L 07/16/12 08:52 07/19/12 11:25 10Acenaphthylene
ND 0.10 ug/L 07/16/12 08:52 07/19/12 11:25 10Acenaphthene
ND 0.10 ug/L 07/16/12 08:52 07/19/12 11:25 10Fluorene
ND 0.10 ug/L 07/16/12 08:52 07/19/12 11:25 10Phenanthrene
ND 0.10 ug/L 07/16/12 08:52 07/19/12 11:25 10Anthracene
ND 0.10 ug/L 07/16/12 08:52 07/19/12 11:25 10Fluoranthene
ND 0.10 ug/L 07/16/12 08:52 07/19/12 11:25 10Pyrene
ND 0.10 ug/L 07/16/12 08:52 07/19/12 11:25 10Benzo[a]anthracene
ND 0.10 ug/L 07/16/12 08:52 07/19/12 11:25 10Chrysene
ND 0.10 ug/L 07/16/12 08:52 07/19/12 11:25 10Benzo[b]fluoranthene
ND 0.10 ug/L 07/16/12 08:52 07/19/12 11:25 10Benzo[k]fluoranthene
ND 0.20 ug/L 07/16/12 08:52 07/19/12 11:25 10Benzo[a]pyrene
ND 0.10 ug/L 07/16/12 08:52 07/19/12 11:25 10Indeno[1,2,3-cd]pyrene
ND 0.10 ug/L 07/16/12 08:52 07/19/12 11:25 10Dibenz(a,h)anthracene
ND 0.10 ug/L 07/16/12 08:52 07/19/12 11:25 10Benzo[g,h,i]perylene
Terphenyl-d14 72 20 - 150 07/19/12 11:25 10
MB MB
Surrogate
07/16/12 08:52
Dil FacPrepared AnalyzedQualifier Limits%Recovery
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QC Sample ResultsTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 580-115337/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 115710 Prep Batch: 115337
Naphthalene 10.1 6.58 ug/L 65 65 - 125
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
2-Methylnaphthalene 10.0 6.77 ug/L 68 65 - 125
1-Methylnaphthalene 10.1 6.89 ug/L 69 65 - 125
Acenaphthylene 9.99 7.46 ug/L 75 70 - 125
Acenaphthene 10.0 6.75 ug/L 68 65 - 125
Fluorene 10.1 7.05 ug/L 70 70 - 125
Phenanthrene 10.1 7.50 ug/L 75 70 - 125
Anthracene 9.99 8.07 ug/L 81 60 - 125
Fluoranthene 10.0 8.07 ug/L 81 75 - 125
Pyrene 9.99 7.70 ug/L 77 75 - 125
Benzo[a]anthracene 10.0 8.33 ug/L 83 70 - 125
Chrysene 9.64 7.48 ug/L 78 75 - 125
Benzo[b]fluoranthene 10.0 6.70 * ug/L 67 70 - 125
Benzo[k]fluoranthene 9.99 7.19 ug/L 72 70 - 125
Benzo[a]pyrene 10.0 7.51 ug/L 75 55 - 125
Indeno[1,2,3-cd]pyrene 10.1 8.79 ug/L 87 65 - 125
Dibenz(a,h)anthracene 10.0 8.66 ug/L 87 65 - 130
Benzo[g,h,i]perylene 10.0 8.15 ug/L 82 65 - 125
Terphenyl-d14 20 - 150
Surrogate
82
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 580-115337/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 115710 Prep Batch: 115337
Naphthalene 10.1 6.35 * ug/L 63 65 - 125 4 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
2-Methylnaphthalene 10.0 6.59 ug/L 66 65 - 125 3 20
1-Methylnaphthalene 10.1 6.68 ug/L 66 65 - 125 3 20
Acenaphthylene 9.99 7.32 ug/L 73 70 - 125 2 20
Acenaphthene 10.0 6.58 ug/L 66 65 - 125 3 20
Fluorene 10.1 6.86 * ug/L 68 70 - 125 3 20
Phenanthrene 10.1 7.17 ug/L 71 70 - 125 5 20
Anthracene 9.99 7.86 ug/L 79 60 - 125 3 20
Fluoranthene 10.0 7.88 ug/L 79 75 - 125 2 20
Pyrene 9.99 7.56 ug/L 76 75 - 125 2 20
Benzo[a]anthracene 10.0 8.01 ug/L 80 70 - 125 4 20
Chrysene 9.64 7.20 ug/L 75 75 - 125 4 20
Benzo[b]fluoranthene 10.0 6.45 * ug/L 64 70 - 125 4 20
Benzo[k]fluoranthene 9.99 6.78 * ug/L 68 70 - 125 6 20
Benzo[a]pyrene 10.0 7.29 ug/L 73 55 - 125 3 20
Indeno[1,2,3-cd]pyrene 10.1 8.34 ug/L 83 65 - 125 5 20
Dibenz(a,h)anthracene 10.0 8.10 ug/L 81 65 - 130 7 20
Benzo[g,h,i]perylene 10.0 7.62 ug/L 76 65 - 125 7 20
Terphenyl-d14 20 - 150
Surrogate
78
LCSD LCSD
Qualifier Limits%Recovery
TestAmerica SeattlePage 23 of 48 8/20/2012
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QC Sample ResultsTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 580-115806/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 116157 Prep Batch: 115806
RL MDL
Naphthalene ND 0.10 ug/L 07/20/12 10:55 07/25/12 22:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.13 ug/L 07/20/12 10:55 07/25/12 22:17 12-Methylnaphthalene
ND 0.10 ug/L 07/20/12 10:55 07/25/12 22:17 11-Methylnaphthalene
ND 0.10 ug/L 07/20/12 10:55 07/25/12 22:17 1Acenaphthylene
ND 0.10 ug/L 07/20/12 10:55 07/25/12 22:17 1Acenaphthene
ND 0.10 ug/L 07/20/12 10:55 07/25/12 22:17 1Fluorene
ND 0.10 ug/L 07/20/12 10:55 07/25/12 22:17 1Phenanthrene
ND 0.10 ug/L 07/20/12 10:55 07/25/12 22:17 1Anthracene
ND 0.10 ug/L 07/20/12 10:55 07/25/12 22:17 1Fluoranthene
ND 0.10 ug/L 07/20/12 10:55 07/25/12 22:17 1Pyrene
ND 0.10 ug/L 07/20/12 10:55 07/25/12 22:17 1Benzo[a]anthracene
ND 0.10 ug/L 07/20/12 10:55 07/25/12 22:17 1Chrysene
ND 0.10 ug/L 07/20/12 10:55 07/25/12 22:17 1Benzo[b]fluoranthene
ND 0.10 ug/L 07/20/12 10:55 07/25/12 22:17 1Benzo[k]fluoranthene
ND 0.20 ug/L 07/20/12 10:55 07/25/12 22:17 1Benzo[a]pyrene
ND 0.10 ug/L 07/20/12 10:55 07/25/12 22:17 1Indeno[1,2,3-cd]pyrene
ND 0.10 ug/L 07/20/12 10:55 07/25/12 22:17 1Dibenz(a,h)anthracene
ND 0.10 ug/L 07/20/12 10:55 07/25/12 22:17 1Benzo[g,h,i]perylene
Terphenyl-d14 87 20 - 150 07/25/12 22:17 1
MB MB
Surrogate
07/20/12 10:55
Dil FacPrepared AnalyzedQualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 580-115806/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 116157 Prep Batch: 115806
Naphthalene 10.1 8.00 ug/L 79 65 - 125
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
2-Methylnaphthalene 10.0 8.10 ug/L 81 65 - 125
1-Methylnaphthalene 10.1 8.19 ug/L 82 65 - 125
Acenaphthylene 9.99 8.41 ug/L 84 70 - 125
Acenaphthene 10.0 8.09 ug/L 81 65 - 125
Fluorene 10.1 8.22 ug/L 82 70 - 125
Phenanthrene 10.1 8.65 ug/L 86 70 - 125
Anthracene 9.99 8.28 ug/L 83 60 - 125
Fluoranthene 10.0 8.72 ug/L 87 75 - 125
Pyrene 9.99 8.53 ug/L 85 75 - 125
Benzo[a]anthracene 10.0 8.15 ug/L 81 70 - 125
Chrysene 9.64 7.95 ug/L 82 75 - 125
Benzo[b]fluoranthene 10.0 7.52 ug/L 75 70 - 125
Benzo[k]fluoranthene 9.99 8.02 ug/L 80 70 - 125
Benzo[a]pyrene 10.0 7.13 ug/L 71 55 - 125
Indeno[1,2,3-cd]pyrene 10.1 7.48 ug/L 74 65 - 125
Dibenz(a,h)anthracene 10.0 7.53 ug/L 75 65 - 130
Benzo[g,h,i]perylene 10.0 7.98 ug/L 80 65 - 125
Terphenyl-d14 20 - 150
Surrogate
85
LCS LCS
Qualifier Limits%Recovery
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QC Sample ResultsTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 580-115806/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 116157 Prep Batch: 115806
Naphthalene 10.1 8.58 ug/L 85 65 - 125 7 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
2-Methylnaphthalene 10.0 8.68 ug/L 87 65 - 125 7 20
1-Methylnaphthalene 10.1 8.82 ug/L 88 65 - 125 7 20
Acenaphthylene 9.99 8.98 ug/L 90 70 - 125 7 20
Acenaphthene 10.0 8.64 ug/L 86 65 - 125 7 20
Fluorene 10.1 8.77 ug/L 87 70 - 125 6 20
Phenanthrene 10.1 9.01 ug/L 90 70 - 125 4 20
Anthracene 9.99 8.63 ug/L 86 60 - 125 4 20
Fluoranthene 10.0 9.13 ug/L 91 75 - 125 5 20
Pyrene 9.99 8.90 ug/L 89 75 - 125 4 20
Benzo[a]anthracene 10.0 8.27 ug/L 83 70 - 125 1 20
Chrysene 9.64 8.35 ug/L 87 75 - 125 5 20
Benzo[b]fluoranthene 10.0 7.66 ug/L 77 70 - 125 2 20
Benzo[k]fluoranthene 9.99 9.05 ug/L 91 70 - 125 12 20
Benzo[a]pyrene 10.0 7.69 ug/L 77 55 - 125 8 20
Indeno[1,2,3-cd]pyrene 10.1 7.66 ug/L 76 65 - 125 2 20
Dibenz(a,h)anthracene 10.0 8.00 ug/L 80 65 - 130 6 20
Benzo[g,h,i]perylene 10.0 8.62 ug/L 86 65 - 125 8 20
Terphenyl-d14 20 - 150
Surrogate
84
LCSD LCSD
Qualifier Limits%Recovery
Method: 8015B - Gasoline Range Organics - (GC)
Client Sample ID: Method BlankLab Sample ID: MB 580-115334/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 115334
RL MDL
HI Gasoline Range Organic (C6-C12) ND 0.050 mg/L 07/16/12 10:13 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
4-Bromofluorobenzene (Surr) 103 70 - 130 07/16/12 10:13 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
122 07/16/12 10:13 1Trifluorotoluene (Surr) 70 - 130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 580-115334/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 115334
HI Gasoline Range Organic
(C6-C12)
1.00 1.02 mg/L 102 50 - 150
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
4-Bromofluorobenzene (Surr) 70 - 130
Surrogate
103
LCS LCS
Qualifier Limits%Recovery
102Trifluorotoluene (Surr) 70 - 130
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QC Sample ResultsTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Method: 8015B - Gasoline Range Organics - (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 580-115334/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 115334
HI Gasoline Range Organic
(C6-C12)
1.00 1.04 mg/L 104 50 - 150 2 30
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
4-Bromofluorobenzene (Surr) 70 - 130
Surrogate
103
LCSD LCSD
Qualifier Limits%Recovery
106Trifluorotoluene (Surr) 70 - 130
Method: 8015B - Diesel Range Organics (DRO) (GC)
Client Sample ID: Method BlankLab Sample ID: MB 580-115360/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 115461 Prep Batch: 115360
RL MDL
HI Diesel Range Organics (>C12-C24) ND 0.25 mg/L 07/16/12 09:10 07/17/12 22:03 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.50 mg/L 07/16/12 09:10 07/17/12 22:03 1HI Residual Range Organics
(>C24-C32)
o-Terphenyl 77 50 - 150 07/17/12 22:03 1
MB MB
Surrogate
07/16/12 09:10
Dil FacPrepared AnalyzedQualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 580-115360/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 115461 Prep Batch: 115360
HI Diesel Range Organics
(>C12-C24)
5.00 4.25 mg/L 85 75 - 125
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
HI Residual Range Organics
(>C24-C32)
5.00 4.66 mg/L 93 75 - 125
o-Terphenyl 50 - 150
Surrogate
72
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 580-115360/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 115461 Prep Batch: 115360
HI Diesel Range Organics
(>C12-C24)
5.00 4.35 mg/L 87 75 - 125 2 25
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
HI Residual Range Organics
(>C24-C32)
5.00 4.69 mg/L 94 75 - 125 1 25
o-Terphenyl 50 - 150
Surrogate
69
LCSD LCSD
Qualifier Limits%Recovery
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QC Sample ResultsTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Method: 8081A - Organochlorine Pesticides (GC)
Client Sample ID: Method BlankLab Sample ID: MB 580-115477/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 115818 Prep Batch: 115477
RL MDL
Aldrin ND 0.010 ug/L 07/17/12 10:54 07/20/12 20:31 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.010 ug/L 07/17/12 10:54 07/20/12 20:31 1alpha-BHC
ND 0.020 ug/L 07/17/12 10:54 07/20/12 20:31 1beta-BHC
ND 0.010 ug/L 07/17/12 10:54 07/20/12 20:31 1delta-BHC
ND 0.010 ug/L 07/17/12 10:54 07/20/12 20:31 1gamma-BHC (Lindane)
ND 0.020 ug/L 07/17/12 10:54 07/20/12 20:31 14,4'-DDD
ND 0.020 ug/L 07/17/12 10:54 07/20/12 20:31 14,4'-DDE
ND 0.020 ug/L 07/17/12 10:54 07/20/12 20:31 14,4'-DDT
ND 0.020 ug/L 07/17/12 10:54 07/20/12 20:31 1Dieldrin
ND 0.020 ug/L 07/17/12 10:54 07/20/12 20:31 1Endosulfan I
ND 0.020 ug/L 07/17/12 10:54 07/20/12 20:31 1Endosulfan II
ND 0.020 ug/L 07/17/12 10:54 07/20/12 20:31 1Endosulfan sulfate
ND 0.020 ug/L 07/17/12 10:54 07/20/12 20:31 1Endrin
ND 0.050 ug/L 07/17/12 10:54 07/20/12 20:31 1Endrin aldehyde
ND 0.010 ug/L 07/17/12 10:54 07/20/12 20:31 1Heptachlor
ND 0.010 ug/L 07/17/12 10:54 07/20/12 20:31 1Heptachlor epoxide
ND 0.10 ug/L 07/17/12 10:54 07/20/12 20:31 1Methoxychlor
ND 0.020 ug/L 07/17/12 10:54 07/20/12 20:31 1Endrin ketone
ND 1.0 ug/L 07/17/12 10:54 07/20/12 20:31 1Toxaphene
ND 0.010 ug/L 07/17/12 10:54 07/20/12 20:31 1alpha-Chlordane
ND 0.010 ug/L 07/17/12 10:54 07/20/12 20:31 1gamma-Chlordane
Tetrachloro-m-xylene 72 18 - 181 07/20/12 20:31 1
MB MB
Surrogate
07/17/12 10:54
Dil FacPrepared AnalyzedQualifier Limits%Recovery
74 07/17/12 10:54 07/20/12 20:31 1DCB Decachlorobiphenyl 53 - 122
Client Sample ID: Lab Control SampleLab Sample ID: LCS 580-115477/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 115818 Prep Batch: 115477
Aldrin 0.200 0.181 ug/L 91 44 - 139
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
alpha-BHC 0.200 0.180 ug/L 90 41 - 133
beta-BHC 0.200 0.189 ug/L 94 54 - 130
delta-BHC 0.200 0.169 ug/L 84 7 - 169
gamma-BHC (Lindane) 0.200 0.187 ug/L 94 53 - 134
4,4'-DDD 0.200 0.195 ug/L 97 40 - 152
4,4'-DDE 0.200 0.188 ug/L 94 43 - 148
4,4'-DDT 0.200 0.190 ug/L 95 37 - 162
Dieldrin 0.200 0.194 ug/L 97 46 - 145
Endosulfan I 0.200 0.192 ug/L 96 49 - 132
Endosulfan II 0.200 0.195 ug/L 97 54 - 138
Endosulfan sulfate 0.200 0.188 ug/L 94 48 - 130
Endrin 0.200 0.202 ug/L 101 51 - 142
Endrin aldehyde 0.200 0.197 ug/L 99 27 - 183
Heptachlor 0.200 0.187 ug/L 93 53 - 130
Heptachlor epoxide 0.200 0.195 ug/L 97 54 - 125
Methoxychlor 0.200 0.205 ug/L 103 47 - 167
Endrin ketone 0.200 0.206 ug/L 103 48 - 134
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QC Sample ResultsTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Method: 8081A - Organochlorine Pesticides (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 580-115477/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 115818 Prep Batch: 115477
alpha-Chlordane 0.200 0.194 ug/L 97 40 - 131
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
gamma-Chlordane 0.200 0.181 ug/L 90 46 - 131
Tetrachloro-m-xylene 18 - 181
Surrogate
81
LCS LCS
Qualifier Limits%Recovery
88DCB Decachlorobiphenyl 53 - 122
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 580-115477/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 115818 Prep Batch: 115477
Aldrin 0.200 0.182 ug/L 91 44 - 139 0 38
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
alpha-BHC 0.200 0.181 ug/L 91 41 - 133 0 41
beta-BHC 0.200 0.191 ug/L 95 54 - 130 1 34
delta-BHC 0.200 0.166 ug/L 83 7 - 169 2 49
gamma-BHC (Lindane) 0.200 0.189 ug/L 94 53 - 134 1 42
4,4'-DDD 0.200 0.200 ug/L 100 40 - 152 2 47
4,4'-DDE 0.200 0.191 ug/L 95 43 - 148 2 43
4,4'-DDT 0.200 0.196 ug/L 98 37 - 162 3 49
Dieldrin 0.200 0.196 ug/L 98 46 - 145 1 39
Endosulfan I 0.200 0.194 ug/L 97 49 - 132 1 40
Endosulfan II 0.200 0.198 ug/L 99 54 - 138 2 37
Endosulfan sulfate 0.200 0.193 ug/L 96 48 - 130 3 34
Endrin 0.200 0.208 ug/L 104 51 - 142 3 41
Endrin aldehyde 0.200 0.202 ug/L 101 27 - 183 2 43
Heptachlor 0.200 0.192 ug/L 96 53 - 130 3 39
Heptachlor epoxide 0.200 0.197 ug/L 98 54 - 125 1 35
Methoxychlor 0.200 0.210 ug/L 105 47 - 167 2 37
Endrin ketone 0.200 0.210 ug/L 105 48 - 134 2 37
alpha-Chlordane 0.200 0.195 ug/L 98 40 - 131 1 43
gamma-Chlordane 0.200 0.183 ug/L 91 46 - 131 1 40
Tetrachloro-m-xylene 18 - 181
Surrogate
80
LCSD LCSD
Qualifier Limits%Recovery
89DCB Decachlorobiphenyl 53 - 122
Method: 6010B - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 580-115917/13-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 116240 Prep Batch: 115917
RL MDL
Cadmium ND 0.010 mg/L 07/23/12 10:35 07/24/12 13:26 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.030 mg/L 07/23/12 10:35 07/24/12 13:26 1Lead
ND 0.060 mg/L 07/23/12 10:35 07/24/12 13:26 1Arsenic
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QC Sample ResultsTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Method: 6010B - Metals (ICP) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 580-115917/14-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 116240 Prep Batch: 115917
Cadmium 0.100 0.107 mg/L 107 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Lead 1.00 1.02 mg/L 102 80 - 120
Arsenic 4.00 4.07 mg/L 102 80 - 120
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 580-115917/15-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 116240 Prep Batch: 115917
Cadmium 0.100 0.106 mg/L 106 80 - 120 0 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Lead 1.00 1.02 mg/L 102 80 - 120 0 20
Arsenic 4.00 4.16 mg/L 104 80 - 120 2 20
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Lab ChronicleClient: Bureau Veritas North America, Inc. TestAmerica Job ID: 580-33901-1
Project/Site: Urban Works Phase II
Client Sample ID: UW MW-1 Lab Sample ID: 580-33901-1Matrix: WaterDate Collected: 07/10/12 15:18
Date Received: 07/12/12 09:35
Analysis 8260B 07/24/12 17:30 SK1 116018 TAL SEA
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3520C 115337 07/16/12 08:52 AC TAL SEATotal/NA
Analysis 8270C SIM 10 115710 07/19/12 13:39 AP TAL SEATotal/NA
Prep 3520C RE 115806 07/20/12 10:57 RD TAL SEATotal/NA
Analysis 8270C SIM RE 1 116157 07/25/12 23:24 AP TAL SEATotal/NA
Analysis 8015B 1 115334 07/16/12 13:11 JMB TAL SEATotal/NA
Prep 3520C 115360 07/16/12 09:10 AC TAL SEATotal/NA
Analysis 8015B 1 115461 07/17/12 23:07 KKW TAL SEATotal/NA
Prep 3005A 115917 07/23/12 10:35 PAB TAL SEADissolved
Analysis 6010B 1 116240 07/24/12 20:44 SP TAL SEADissolved
Client Sample ID: UW MW-2 Lab Sample ID: 580-33901-2Matrix: WaterDate Collected: 07/10/12 14:22
Date Received: 07/12/12 09:35
Analysis 8260B 07/24/12 17:54 SK1 116018 TAL SEA
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3520C 115337 07/16/12 08:52 AC TAL SEATotal/NA
Analysis 8270C SIM 10 115710 07/19/12 14:01 AP TAL SEATotal/NA
Prep 3520C RE 115806 07/20/12 10:57 RD TAL SEATotal/NA
Analysis 8270C SIM RE 1 116157 07/25/12 23:46 AP TAL SEATotal/NA
Analysis 8015B 1 115334 07/16/12 14:17 JMB TAL SEATotal/NA
Prep 3520C 115360 07/16/12 09:10 AC TAL SEATotal/NA
Analysis 8015B 1 115461 07/17/12 23:29 KKW TAL SEATotal/NA
Prep 3005A 115917 07/23/12 10:35 PAB TAL SEADissolved
Analysis 6010B 1 116240 07/24/12 20:50 SP TAL SEADissolved
Client Sample ID: UW MW-3 Lab Sample ID: 580-33901-3Matrix: WaterDate Collected: 07/10/12 10:30
Date Received: 07/12/12 09:35
Analysis 8260B 07/24/12 18:18 SK1 116018 TAL SEA
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3520C 115337 07/16/12 08:52 AC TAL SEATotal/NA
Analysis 8270C SIM 10 115710 07/19/12 14:23 AP TAL SEATotal/NA
Prep 3520C RE 115806 07/20/12 10:57 RD TAL SEATotal/NA
Analysis 8270C SIM RE 1 116157 07/26/12 00:08 AP TAL SEATotal/NA
Prep 3520C 115360 07/16/12 09:10 AC TAL SEATotal/NA
Analysis 8015B 1 115461 07/17/12 23:50 KKW TAL SEATotal/NA
Prep 3510C 115477 07/17/12 10:54 AW TAL SEATotal/NA
Analysis 8081A 1 115871 07/22/12 16:40 EK TAL SEATotal/NA
Prep 3005A 115917 07/23/12 10:35 PAB TAL SEADissolved
Analysis 6010B 1 116240 07/24/12 20:57 SP TAL SEADissolved
TestAmerica SeattlePage 30 of 48 8/20/2012
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Lab ChronicleClient: Bureau Veritas North America, Inc. TestAmerica Job ID: 580-33901-1
Project/Site: Urban Works Phase II
Client Sample ID: UW MW-4 Lab Sample ID: 580-33901-4Matrix: WaterDate Collected: 07/10/12 12:20
Date Received: 07/12/12 09:35
Analysis 8260B 07/24/12 18:44 SK1 116018 TAL SEA
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3520C 115337 07/16/12 08:52 AC TAL SEATotal/NA
Analysis 8270C SIM 10 115710 07/19/12 14:45 AP TAL SEATotal/NA
Prep 3520C RE 115806 07/20/12 10:57 RD TAL SEATotal/NA
Analysis 8270C SIM RE 1 116157 07/26/12 00:31 AP TAL SEATotal/NA
Prep 3520C 115360 07/16/12 09:10 AC TAL SEATotal/NA
Analysis 8015B 1 115461 07/18/12 00:12 KKW TAL SEATotal/NA
Prep 3510C 115477 07/17/12 10:54 AW TAL SEATotal/NA
Analysis 8081A 1 115871 07/22/12 16:56 EK TAL SEATotal/NA
Prep 3005A 115917 07/23/12 10:35 PAB TAL SEADissolved
Analysis 6010B 1 116240 07/24/12 21:04 SP TAL SEADissolved
Laboratory References:
Anatek Lab = Anatek Labs Inc - Moscow Idaho, 1282 Alturas Dr., Moscow, ID 83843
TAL SEA = TestAmerica Seattle, 5755 8th Street East, Tacoma, WA 98424, TEL (253)922-2310
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Certification SummaryClient: Bureau Veritas North America, Inc. TestAmerica Job ID: 580-33901-1
Project/Site: Urban Works Phase II
Laboratory: TestAmerica SeattleAll certifications held by this laboratory are listed. Not all certifications are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
Alaska (UST) 03-04-13UST-02210State Program
California NELAC 9 1115CA 01-31-13
L-A-B DoD ELAP L2236 01-19-13
L-A-B ISO/IEC 17025 L2236 01-19-13
Montana (UST) State Program 8 N/A 04-30-20
Oregon NELAC 10 WA100007 11-06-12
USDA Federal P330-11-00222 05-20-14
Washington State Program 10 C553 02-17-13
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Sample SummaryTestAmerica Job ID: 580-33901-1Client: Bureau Veritas North America, Inc.
Project/Site: Urban Works Phase II
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
580-33901-1 UW MW-1 Water 07/10/12 15:18 07/12/12 09:35
580-33901-2 UW MW-2 Water 07/10/12 14:22 07/12/12 09:35
580-33901-3 UW MW-3 Water 07/10/12 10:30 07/12/12 09:35
580-33901-4 UW MW-4 Water 07/10/12 12:20 07/12/12 09:35
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CASE NARRATIVE August 20, 2012 Lab Name: Anatek Labs, Inc. 1282 Alturas Drive, Moscow, ID 83843 www.anateklabs.com FL NELAP E87893, NV ID13-2004-31, WA DOE C126, OR ELAP ID200001, MT 0028, ID, CO, NM Project Tracking No.: URBAN WORKS PHASE II Anatek Batch: 120807029 Project Summary: Two (2) water samples were received on 8/2/2012 for pesticide screen (EPA 8270Cm). The samples were received with the appropriate chain of custody at 1.0C. Note: samples were received past hold time with no requested tests. Client authorized analysis of samples past hold time on 8/6/2012. Client Sample ID Anatek Sample ID Method/Prep Method UW MW-3 120807029-001 EPA 8270Cm UW MW-4 120807029-002 EPA 8270Cm QA/QC Checks Parameters Yes / No Exceptions / Deviations Sample Holding Time Valid? N See Note Surrogate Recoveries Valid? Y NA QC Sample(s) Recoveries Valid? Y NA Method Blank(s) Valid? Y NA Tune(s) Valid? Y NA Internal Standard Responses Valid? Y NA Initial Calibration Curve(s) Valid? Y NA Continuing Calibration(s) Valid? Y NA Comments: Y NA 1. Holding Time Requirements
Samples analyzed past hold time at client request. 2. GC/MS Tune Requirements
No problems encountered. 3. Calibration Requirements
No problems encountered. 4. Surrogate Recovery Requirements
No problems encountered. 5. QC Sample (LCS/MS/MSD) Recovery Requirements
No problems encountered.
Page 1 of 13Page 34 of 48 8/20/2012
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6. Method Blank Requirements The method blanks were non-detect (<MDL) for all analytes. No problems encountered. 7. Internal Standard(s) Response Requirements
No problems encountered.
8. Comments
N/A I certify that this data package is in compliance with the terms and conditions of the contract. Release of the data contained in this data package has been authorized by the Laboratory Manager or his designee.
Page 2 of 13Page 35 of 48 8/20/2012
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Client: TEST AMERICA TACOMA
Attn: PAM JOHNSON
Address: 5755 8TH STREET EAST
TACOMA, WA 98424
Analytical Results Report
Batch #: 120807029
Project Name: URBAN WORKS PHASE II
Anatek Labs, Inc.1282 Alturas Drive • Moscow, ID 83843 • (208) 883-2839 • Fax (208) 882-9246 • email [email protected]
504 E Sprague Ste. D • Spokane WA 99202 • (509) 838-3999 • Fax (509) 838-4433 • email [email protected]
120807029-001Sample Number
Matrix Water
Parameter Result Units Analysis Date Analyst Method QualifierPQL
Client Sample ID
Sampling Date 7/10/2012
Sampling Time 10:30 AM
Date/Time Received 8/2/2012
Sample Location
Extraction DateUW MW-3 8/13/2012
11:13 AM
MDL
Comments
ug/L EMP8/16/20122,3,4,6-Tetrachlorophenol EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Ametryne EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Atraton EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Atrazine EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Azinphos-methyl EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Bolstar EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Bromacil EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Carbophenothion EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Chlorpyrifos EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Coumaphos EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Demeton EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Diazinon EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Dichlorvos EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Dimethenamid EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Dimethoate EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Disulfoton EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012EPN EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Ethoprop EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Ethyl parathion EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Fensulfothion EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Fenthion EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Hexachlorphene EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Hexazinone EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Malathion EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Merphos EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Methyl parathion EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Mevinphos EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Naled EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Pentachlorophenol EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Phorate EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Phosmet EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Prometon EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Prometryn EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Propazine EPA 8270CMODND 0.5 H30.1
Page 1 of 4Monday, August 20, 2012
Certifications held by Anatek Labs ID: EPA:ID00013; AZ:0701; CO:ID00013; FL(NELAP):E87893; ID:ID00013; IN:C-ID-01; KY:90142; MT:CERT0028; NM: ID00013; OR:ID200001-002; WA:C595Certifications held by Anatek Labs WA: EPA:WA00169; ID:WA00169; WA:C585; MT:Cert0095
Page 3 of 13Page 36 of 48 8/20/2012
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Client: TEST AMERICA TACOMA
Attn: PAM JOHNSON
Address: 5755 8TH STREET EAST
TACOMA, WA 98424
Analytical Results Report
Batch #: 120807029
Project Name: URBAN WORKS PHASE II
Anatek Labs, Inc.1282 Alturas Drive • Moscow, ID 83843 • (208) 883-2839 • Fax (208) 882-9246 • email [email protected]
504 E Sprague Ste. D • Spokane WA 99202 • (509) 838-3999 • Fax (509) 838-4433 • email [email protected]
120807029-001Sample Number
Matrix Water
Parameter Result Units Analysis Date Analyst Method QualifierPQL
Client Sample ID
Sampling Date 7/10/2012
Sampling Time 10:30 AM
Date/Time Received 8/2/2012
Sample Location
Extraction DateUW MW-3 8/13/2012
11:13 AM
MDL
Comments
ug/L EMP8/16/2012Ronnel EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Secbumeton EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Simazine EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Simetryn EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Stirophos EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Sulfotep EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Terbuthylazine EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Terbutryn EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Tokuthion EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Trichloronate EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Trifluralin EPA 8270CMODND 0.5 H30.1
Surrogate Data
Surrogate Standard Percent Recovery Control Limits
Sample Number 120807029-001
Method
Terphenyl-d14 121.8 30-140EPA 8270CMOD
Page 2 of 4Monday, August 20, 2012
Certifications held by Anatek Labs ID: EPA:ID00013; AZ:0701; CO:ID00013; FL(NELAP):E87893; ID:ID00013; IN:C-ID-01; KY:90142; MT:CERT0028; NM: ID00013; OR:ID200001-002; WA:C595Certifications held by Anatek Labs WA: EPA:WA00169; ID:WA00169; WA:C585; MT:Cert0095
Page 4 of 13Page 37 of 48 8/20/2012
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Client: TEST AMERICA TACOMA
Attn: PAM JOHNSON
Address: 5755 8TH STREET EAST
TACOMA, WA 98424
Analytical Results Report
Batch #: 120807029
Project Name: URBAN WORKS PHASE II
Anatek Labs, Inc.1282 Alturas Drive • Moscow, ID 83843 • (208) 883-2839 • Fax (208) 882-9246 • email [email protected]
504 E Sprague Ste. D • Spokane WA 99202 • (509) 838-3999 • Fax (509) 838-4433 • email [email protected]
120807029-002Sample Number
Matrix Water
Parameter Result Units Analysis Date Analyst Method QualifierPQL
Client Sample ID
Sampling Date 7/10/2012
Sampling Time 12:20 PM
Date/Time Received 8/2/2012
Sample Location
Extraction DateUW MW-4 8/13/2012
11:13 AM
MDL
Comments
ug/L EMP8/16/20122,3,4,6-Tetrachlorophenol EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Ametryne EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Atraton EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Atrazine EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Azinphos-methyl EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Bolstar EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Bromacil EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Carbophenothion EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Chlorpyrifos EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Coumaphos EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Demeton EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Diazinon EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Dichlorvos EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Dimethenamid EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Dimethoate EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Disulfoton EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012EPN EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Ethoprop EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Ethyl parathion EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Fensulfothion EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Fenthion EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Hexachlorphene EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Hexazinone EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Malathion EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Merphos EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Methyl parathion EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Mevinphos EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Naled EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Pentachlorophenol EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Phorate EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Phosmet EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Prometon EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Prometryn EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Propazine EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Ronnel EPA 8270CMODND 0.5 H30.1
Page 3 of 4Monday, August 20, 2012
Certifications held by Anatek Labs ID: EPA:ID00013; AZ:0701; CO:ID00013; FL(NELAP):E87893; ID:ID00013; IN:C-ID-01; KY:90142; MT:CERT0028; NM: ID00013; OR:ID200001-002; WA:C595Certifications held by Anatek Labs WA: EPA:WA00169; ID:WA00169; WA:C585; MT:Cert0095
Page 5 of 13Page 38 of 48 8/20/2012
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Client: TEST AMERICA TACOMA
Attn: PAM JOHNSON
Address: 5755 8TH STREET EAST
TACOMA, WA 98424
Analytical Results Report
Batch #: 120807029
Project Name: URBAN WORKS PHASE II
Anatek Labs, Inc.1282 Alturas Drive • Moscow, ID 83843 • (208) 883-2839 • Fax (208) 882-9246 • email [email protected]
504 E Sprague Ste. D • Spokane WA 99202 • (509) 838-3999 • Fax (509) 838-4433 • email [email protected]
120807029-002Sample Number
Matrix Water
Parameter Result Units Analysis Date Analyst Method QualifierPQL
Client Sample ID
Sampling Date 7/10/2012
Sampling Time 12:20 PM
Date/Time Received 8/2/2012
Sample Location
Extraction DateUW MW-4 8/13/2012
11:13 AM
MDL
Comments
ug/L EMP8/16/2012Secbumeton EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Simazine EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Simetryn EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Stirophos EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Sulfotep EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Terbuthylazine EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Terbutryn EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Tokuthion EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Trichloronate EPA 8270CMODND 0.5 H30.1
ug/L EMP8/16/2012Trifluralin EPA 8270CMODND 0.5 H30.1
Surrogate Data
Surrogate Standard Percent Recovery Control Limits
Sample Number 120807029-002
Method
Terphenyl-d14 117.2 30-140EPA 8270CMOD
Authorized Signature
John Coddington, Lab Manager
H3 Sample was received and analyzed past holding time.
MCL EPA's Maximum Contaminant Level
ND Not Detected
PQL Practical Quantitation Limit
This report shall not be reproduced except in full, without the written approval of the laboratory.The results reported relate only to the samples indicated.Soil/solid results are reported on a dry-weight basis unless otherwise noted.
Page 4 of 4Monday, August 20, 2012
Certifications held by Anatek Labs ID: EPA:ID00013; AZ:0701; CO:ID00013; FL(NELAP):E87893; ID:ID00013; IN:C-ID-01; KY:90142; MT:CERT0028; NM: ID00013; OR:ID200001-002; WA:C595Certifications held by Anatek Labs WA: EPA:WA00169; ID:WA00169; WA:C585; MT:Cert0095
Page 6 of 13Page 39 of 48 8/20/2012
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Client: TEST AMERICA TACOMA
Attn: PAM JOHNSON
Address: 5755 8TH STREET EAST
TACOMA, WA 98424
Analytical Results Report
Batch #: 120807029
Project Name: URBAN WORKS PHASE II
Quality Control Data
Anatek Labs, Inc.1282 Alturas Drive • Moscow, ID 83843 • (208) 883-2839 • Fax (208) 882-9246 • email [email protected]
504 E Sprague Ste. D • Spokane WA 99202 • (509) 838-3999 • Fax (509) 838-4433 • email [email protected]
Parameter %Rec
Lab Control Sample
LCS Result LCS Spike AR %Rec Analysis DateUnits Prep Date
8/16/2012Pentachlorophenol 5 70.83.54 40-150ug/L 8/13/2012
8/16/2012Ametryne 5 95.64.78 40-150ug/L 8/13/2012
8/16/2012Atrazine 5 75.43.77 40-150ug/L 8/13/2012
8/16/2012Azinphos-methyl 5 81.44.07 20-110ug/L 8/13/2012
8/16/2012Bolstar 5 99.04.95 40-150ug/L 8/13/2012
8/16/2012Chlorpyrifos 5 108.25.41 40-150ug/L 8/13/2012
8/16/2012Diazinon 5 102.25.11 40-150ug/L 8/13/2012
8/16/2012Ethyl parathion 5 96.64.83 40-150ug/L 8/13/2012
8/16/2012Hexazinone 5 85.04.25 40-150ug/L 8/13/2012
8/16/2012Malathion 5 97.64.88 40-150ug/L 8/13/2012
8/16/2012Methyl parathion 5 87.84.39 40-150ug/L 8/13/2012
8/16/20122,3,4,6-Tetrachlorophenol 5 95.64.78 40-150ug/L 8/13/2012
8/16/2012Naled 5 97.24.86 40-150ug/L 8/13/2012
8/16/2012Trifluralin 5 127.06.35 40-150ug/L 8/13/2012
8/16/2012Phorate 5 92.64.63 40-150ug/L 8/13/2012
8/16/2012Phosmet 5 104.05.20 40-150ug/L 8/13/2012
8/16/2012Prometon 5 89.44.47 40-150ug/L 8/13/2012
8/16/2012Prometryn 5 100.85.04 40-150ug/L 8/13/2012
8/16/2012Propazine 5 52.82.64 40-150ug/L 8/13/2012
8/16/2012Ronnel 5 109.45.47 40-150ug/L 8/13/2012
8/16/2012Simazine 5 44.22.21 40-150ug/L 8/13/2012
8/16/2012Stirophos 5 98.84.94 40-150ug/L 8/13/2012
8/16/2012Terbutryn 5 97.44.87 40-150ug/L 8/13/2012
8/16/2012Tokuthion 5 89.04.45 40-150ug/L 8/13/2012
8/16/2012Trichloronate 5 94.64.73 40-150ug/L 8/13/2012
8/16/2012Mevinphos 5 119.45.97 40-150ug/L 8/13/2012
Parameter %Rec
Lab Control Sample DuplicateLCSDResult
LCSDSpike Analysis DateUnits %RPD
AR%RPD Prep Date
8/16/2012Phorate 5 99.04.95 ug/L 6.7 0-50 8/13/2012
8/16/2012Ametryne 5 102.25.11 ug/L 6.7 0-50 8/13/2012
Page 1 of 4Monday, August 20, 2012
Comments:
Certifications held by Anatek Labs ID: EPA:ID00013; AZ:0701; CO:ID00013; FL(NELAP):E87893; ID:ID00013; IN:C-ID-01; KY:90142; MT:CERT0028; NM: ID00013; OR:ID200001-002; WA:C595Certifications held by Anatek Labs WA: EPA:WA00169; ID:WA00169; WA:C585; MT:Cert0095
Page 7 of 13Page 40 of 48 8/20/2012
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Client: TEST AMERICA TACOMA
Attn: PAM JOHNSON
Address: 5755 8TH STREET EAST
TACOMA, WA 98424
Analytical Results Report
Batch #: 120807029
Project Name: URBAN WORKS PHASE II
Quality Control Data
Anatek Labs, Inc.1282 Alturas Drive • Moscow, ID 83843 • (208) 883-2839 • Fax (208) 882-9246 • email [email protected]
504 E Sprague Ste. D • Spokane WA 99202 • (509) 838-3999 • Fax (509) 838-4433 • email [email protected]
Parameter %Rec
Lab Control Sample DuplicateLCSDResult
LCSDSpike Analysis DateUnits %RPD
AR%RPD Prep Date
8/16/2012Atrazine 5 80.04.00 ug/L 5.9 0-50 8/13/2012
8/16/2012Azinphos-methyl 5 84.64.23 ug/L 3.9 0-50 8/13/2012
8/16/2012Bolstar 5 109.65.48 ug/L 10.2 0-50 8/13/2012
8/16/2012Chlorpyrifos 5 104.25.21 ug/L 3.8 0-50 8/13/2012
8/16/2012Diazinon 5 106.25.31 ug/L 3.8 0-50 8/13/2012
8/16/2012Hexazinone 5 95.84.79 ug/L 11.9 0-50 8/13/2012
8/16/2012Malathion 5 98.64.93 ug/L 1.0 0-50 8/13/2012
8/16/2012Methyl parathion 5 88.24.41 ug/L 0.5 0-50 8/13/2012
8/16/2012Mevinphos 5 110.85.54 ug/L 7.5 0-50 8/13/2012
8/16/20122,3,4,6-Tetrachlorophenol 5 101.65.08 ug/L 6.1 0-50 8/13/2012
8/16/2012Pentachlorophenol 5 74.23.71 ug/L 4.7 0-50 8/13/2012
8/16/2012Trifluralin 5 123.26.16 ug/L 3.0 0-50 8/13/2012
8/16/2012Phosmet 5 108.45.42 ug/L 4.1 0-50 8/13/2012
8/16/2012Prometon 5 89.84.49 ug/L 0.4 0-50 8/13/2012
8/16/2012Prometryn 5 104.25.21 ug/L 3.3 0-50 8/13/2012
8/16/2012Propazine 5 35.41.77 ug/L 7.6 0-50 8/13/2012
8/16/2012Ronnel 5 110.05.50 ug/L 0.5 0-50 8/13/2012
8/16/2012Simazine 5 50.42.52 ug/L 13.1 0-50 8/13/2012
8/16/2012Stirophos 5 107.25.36 ug/L 8.2 0-50 8/13/2012
8/16/2012Terbutryn 5 111.25.56 ug/L 13.2 0-50 8/13/2012
8/16/2012Tokuthion 5 98.44.92 ug/L 10.0 0-50 8/13/2012
8/16/2012Trichloronate 5 97.44.87 ug/L 2.9 0-50 8/13/2012
8/16/2012Naled 5 95.44.77 ug/L 1.9 0-50 8/13/2012
Parameter
Method Blank
Result Analysis DateUnits PQL Prep Date
8/16/20122,3,4,6-Tetrachlorophenol ND ug/L 0.5 8/13/2012
8/16/2012Ametryne ND ug/L 0.5 8/13/2012
8/16/2012Atraton ND ug/L 0.5 8/13/2012
8/16/2012Atrazine ND ug/L 0.5 8/13/2012
8/16/2012Azinphos-methyl ND ug/L 0.5 8/13/2012
8/16/2012Bolstar ND ug/L 0.5 8/13/2012
Page 2 of 4Monday, August 20, 2012
Comments:
Certifications held by Anatek Labs ID: EPA:ID00013; AZ:0701; CO:ID00013; FL(NELAP):E87893; ID:ID00013; IN:C-ID-01; KY:90142; MT:CERT0028; NM: ID00013; OR:ID200001-002; WA:C595Certifications held by Anatek Labs WA: EPA:WA00169; ID:WA00169; WA:C585; MT:Cert0095
Page 8 of 13Page 41 of 48 8/20/2012
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Client: TEST AMERICA TACOMA
Attn: PAM JOHNSON
Address: 5755 8TH STREET EAST
TACOMA, WA 98424
Analytical Results Report
Batch #: 120807029
Project Name: URBAN WORKS PHASE II
Quality Control Data
Anatek Labs, Inc.1282 Alturas Drive • Moscow, ID 83843 • (208) 883-2839 • Fax (208) 882-9246 • email [email protected]
504 E Sprague Ste. D • Spokane WA 99202 • (509) 838-3999 • Fax (509) 838-4433 • email [email protected]
Parameter
Method Blank
Result Analysis DateUnits PQL Prep Date
8/16/2012Bromacil ND ug/L 0.5 8/13/2012
8/16/2012Carbophenothion ND ug/L 0.5 8/13/2012
8/16/2012Chlorpyrifos ND ug/L 0.5 8/13/2012
8/16/2012Coumaphos ND ug/L 0.5 8/13/2012
8/16/2012Demeton ND ug/L 0.5 8/13/2012
8/16/2012Diazinon ND ug/L 0.5 8/13/2012
8/16/2012Dichlorvos ND ug/L 0.5 8/13/2012
8/16/2012Dimethenamid ND ug/L 0.5 8/13/2012
8/16/2012Dimethoate ND ug/L 0.5 8/13/2012
8/16/2012Disulfoton ND ug/L 0.5 8/13/2012
8/16/2012EPN ND ug/L 0.5 8/13/2012
8/16/2012Ethoprop ND ug/L 0.5 8/13/2012
8/16/2012Ethyl parathion ND ug/L 0.5 8/13/2012
8/16/2012Fensulfothion ND ug/L 0.5 8/13/2012
8/16/2012Fenthion ND ug/L 0.5 8/13/2012
8/16/2012Hexachlorphene ND ug/L 0.5 8/13/2012
8/16/2012Hexazinone ND ug/L 0.5 8/13/2012
8/16/2012Malathion ND ug/L 0.5 8/13/2012
8/16/2012Merphos ND ug/L 0.5 8/13/2012
8/16/2012Methyl parathion ND ug/L 0.5 8/13/2012
8/16/2012Mevinphos ND ug/L 0.5 8/13/2012
8/16/2012Naled ND ug/L 0.5 8/13/2012
8/16/2012Pentachlorophenol ND ug/L 0.5 8/13/2012
8/16/2012Phorate ND ug/L 0.5 8/13/2012
8/16/2012Phosmet ND ug/L 0.5 8/13/2012
8/16/2012Prometon ND ug/L 0.5 8/13/2012
8/16/2012Prometryn ND ug/L 0.5 8/13/2012
8/16/2012Propazine ND ug/L 0.5 8/13/2012
8/16/2012Ronnel ND ug/L 0.5 8/13/2012
8/16/2012Secbumeton ND ug/L 0.5 8/13/2012
8/16/2012Simazine ND ug/L 0.5 8/13/2012
8/16/2012Simetryn ND ug/L 0.5 8/13/2012
8/16/2012Stirophos ND ug/L 0.5 8/13/2012
8/16/2012Sulfotep ND ug/L 0.5 8/13/2012
Page 3 of 4Monday, August 20, 2012
Comments:
Certifications held by Anatek Labs ID: EPA:ID00013; AZ:0701; CO:ID00013; FL(NELAP):E87893; ID:ID00013; IN:C-ID-01; KY:90142; MT:CERT0028; NM: ID00013; OR:ID200001-002; WA:C595Certifications held by Anatek Labs WA: EPA:WA00169; ID:WA00169; WA:C585; MT:Cert0095
Page 9 of 13Page 42 of 48 8/20/2012
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Client: TEST AMERICA TACOMA
Attn: PAM JOHNSON
Address: 5755 8TH STREET EAST
TACOMA, WA 98424
Analytical Results Report
Batch #: 120807029
Project Name: URBAN WORKS PHASE II
Quality Control Data
Anatek Labs, Inc.1282 Alturas Drive • Moscow, ID 83843 • (208) 883-2839 • Fax (208) 882-9246 • email [email protected]
504 E Sprague Ste. D • Spokane WA 99202 • (509) 838-3999 • Fax (509) 838-4433 • email [email protected]
Parameter
Method Blank
Result Analysis DateUnits PQL Prep Date
8/16/2012Terbuthylazine ND ug/L 0.5 8/13/2012
8/16/2012Terbutryn ND ug/L 0.5 8/13/2012
8/16/2012Tokuthion ND ug/L 0.5 8/13/2012
8/16/2012Trichloronate ND ug/L 0.5 8/13/2012
8/16/2012Trifluralin ND ug/L 0.5 8/13/2012
AR Acceptable RangeND Not DetectedPQL Practical Quantitation LimitRPD Relative Percentage Difference
Page 4 of 4Monday, August 20, 2012
Comments:
Certifications held by Anatek Labs ID: EPA:ID00013; AZ:0701; CO:ID00013; FL(NELAP):E87893; ID:ID00013; IN:C-ID-01; KY:90142; MT:CERT0028; NM: ID00013; OR:ID200001-002; WA:C595Certifications held by Anatek Labs WA: EPA:WA00169; ID:WA00169; WA:C585; MT:Cert0095
Page 10 of 13Page 43 of 48 8/20/2012
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Login Report
Anatek Labs, Inc.1282 Alturas Drive • Moscow, ID 83843 • (208) 883-2839 • Fax (208) 882-9246 • email [email protected]
504 E Sprague Ste. D • Spokane WA 99202 • (509) 838-3999 • Fax (509) 838-4433 • email [email protected]
Order ID: 120807029Customer Name: TEST AMERICA TACOMA
5755 8TH STREET EAST
Contact Name: PAM JOHNSON
Comment:
Order Date: 8/7/2012
Project Name: URBAN WORKS PHASE II
TACOMA WA 98424
Sample #: 120807029-001
Date Collected: 7/10/2012
Date Received: 8/2/2012 11:13:00 A
Customer Sample #: UW MW-3
Comment:
Collector:
Matrix: WaterQuantity: 1
Recv'd:
Test Method Due Date PriorityLab
PEST SCREEN TAHH 8270 8/14/2012EPA 8270CMOD Normal (6-10 Days)M
Sample #: 120807029-002
Date Collected: 7/10/2012
Date Received: 8/2/2012 11:13:00 A
Customer Sample #: UW MW-4
Comment:
Collector:
Matrix: WaterQuantity: 1
Recv'd:
Test Method Due Date PriorityLab
PEST SCREEN TAHH 8270 8/14/2012EPA 8270CMOD Normal (6-10 Days)M
SAMPLE CONDITION RECORD
Samples received in a cooler? Yes
Samples received intact? Yes
What is the temperature inside the cooler? 1.0
Samples received with a COC? Yes
Samples received within holding time? Yes
Are all sample bottles properly preserved? Yes
Are VOC samples free of headspace? N/A
Is there a trip blank to accompany VOC samples? N/A
Labels and chain agree? Yes
Page 11 of 13Page 44 of 48 8/20/2012
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Page 12 of 13Page 45 of 48 8/20/2012
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Page 13 of 13Page 46 of 48 8/20/2012
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Page 47 of 48 8/20/2012
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Login Sample Receipt Checklist
Client: Bureau Veritas North America, Inc. Job Number: 580-33901-1
Login Number: 33901
Question Answer Comment
Creator: Riley, Nicole
List Source: TestAmerica Seattle
List Number: 1
TrueRadioactivity either was not measured or, if measured, is at or below
background
N/AThe cooler's custody seal, if present, is intact. Not present
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
FalseThere are no discrepancies between the sample IDs on the containers and
the COC.
See NCM.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided. See NCM.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
FalseVOA sample vials do not have headspace or bubble is <6mm (1/4") in
diameter.
See NCM.
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked. No analysis requiring residual chlorine check
assigned.
TestAmerica SeattlePage 48 of 48 8/20/2012
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