Rev 2 to Procedure 12 PMP 3150 PCP.001, …xiiiarv Build'ng o eea must be place1 ed intoi a...
Transcript of Rev 2 to Procedure 12 PMP 3150 PCP.001, …xiiiarv Build'ng o eea must be place1 ed intoi a...
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1NDIAN% tk AMCHIGANPQW R CQMPANYDONALD C. COOK NUCLEAR PLANT
PROCEDURE COVER SHEET
Procedure No.lZ PMP 3150 PCP.001
Revision No.
RADIOACTIYE MASTS PROCESS C0~TROL ~ANNUAL
SCOPE OF REVISION
SIGNATURES
ORIGINAL Rev. 1 REV. 2 Rev. 0
PREPARED BY
QUALiTYASSURAi tC.RE VIE'cV
iNT=RFACING DEBAR i MENTi:EAD CONCURRENC-
DEPARTMEVi T:-BADAPPROVAL
PLANT iVUC'"ARSAFETY COMMITTEE
NT MANAGERAPPROVAL
77
DA:= OF iSSUE
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12 PNP 3150 PCP.001
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XZ rm'a>O PCP.001
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12 P!1P 3150 PCP.001
INDIANA & 5!ICHIGM ELECTRIC COa~PANYDONALD C COOK NUCLZAB P~IT
RADIOACTIVE NASTZ PROCESS CONTROL PROGBAiii
1.0 OBJECTIVE
This manual is to give the necessary d'rections to insurethat all ~lant cenerated adioac"ive wastes are t ansferred,packaged and sh'pped such "hat radioac ive waste sh'=mentand burial regulations are satisfied.
2.0 BE:EBZNCES
2. 1 Code o f Federal Reculations T'ie 49 Pa" s 170-179
2.2 Coce of Federal Regulations Tit'e 10 Parts 19-71, 150
2.3 NRC Radioactive Material License No. 46-13536-01
2.4 State of South Carolina, Radioactive Materials L'censeNo. .097.
2.5 State of ~~iarvland Rad'oac ive Haterials 'License No. i~iD27-001-02.
2.6 Technica'pecifications, Apoendiv A to L'cense No.DPR-58.
2.7 Technical Speci"icaticns, Appendix A to License No.DPR-74.
U.S. Zcologv Incorporated, State or Nevada, Depa" wentor Human Resources, Division of Health, Radioactivei~!aterials License No. 13-11-0043-02.
2.9 U.S. Zcologv incorporated, NRC g Radioact'e i~iaterialsLicense No. 04-03766-01.
2.10 U.S. Fcologv, incor-orated, State o" Nash'gtonRadioac ive i~!aterials L'cense No. (vN-1019-02.
2.11 U.S. =cologv incorporated, NBC, Nashincton License16-19204-01.
Page 1 of 26Rev. 2
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p)~ 50 PCS 001
Depar men o
er 345 Division 60 ror"~ative Rules Chapter ' 'or2 ~ 13 Oregon Adminis~raR oactive Materia~ls, Transport Perm'heOregon Raaisirequirement
t, Corpora'tion Radwaste~ear and Developmen o2.14 Hittman Nuc earService NanuaHandl ng
waste Handling Service Manual.2.15 Chem Nuclear Radwaste Han i
vLarge Quantity shi ments orplicatj.on to transpo ". h,."an should be made
2. p . materj.al i~ itic -'g553 o~ Ac No ~ 20'ursuantto the r« - .
41, as amendedi beingo~„"the publj.c Acts oz ~
D rtmen of State, Po i9 of Act No ~St te pire Safety Boar
ded and Sectionspublj.c Acts o368 of ™he Publ Acts2226i and 13521 o " '33. 2226 I 333 ~'n 5 16 109, ~ '
1978, as amended, be'ngled Laws (<michigan
of~ 333 13521 oz he ygichigan Compi eanc ~
.- Publ'c Health) ~
PRZCAUTZONS3.0
uct s wloi or u ~ 'll be pou ed 'nto any- omB ilding loo drains. 'o
and re%ovexiiiarv Build'ng o
e 1 ed into a container,ea must be place ib keat from entering
are1 soi's must e .
d t 1s and must be cleane u
3.2 No package i~ e hz. ment, xn of a hole, aa. ure,
snot must beindic tio
'p." Pa" icular attenh has an o
"ion wi1 b led o .ot Shia eno Qo esid to welds, znsu ng .
1.a kec o "'ed an
wefor shipmen
smashed prior to p acut up or
3.3
3.4
s tr2.c ~ly p
500 allon tanksk Co fo
e' 00 allon and 1 g
red bv H'hland Tanmanu actu ec v prohwaste is s c i
shipment.
o s 1nto se 1 anv open'gsxv mater'ls o" shipment of racioaa package =or srohibited.
Page 2 of 26Rev. 2
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0 l2 P< aso PCP.ool
Cq-CK OF> AND INFOP-~AT O.1 S="= S
t I Truck/~"a~ler ~ns~ect.on Check-Or SheetAttachmen
Attachment XX Cement Solidification Verification Log
Cement Haste Solidific tion Data SheetAttachment XXXI
Attachment IV Calculation She " "or Cement Solidi-'cat'ono= Resin
Attachment V
Attac? ..ent VX
Attachment VXX
Haste Management Simple Flow Diagram
Responsx,baal'v
U.S. Ecology, Inc. Radioactive ShippingRecord
At"achment VXXX
Attachment ZX
A'ttachment Z
Chem Nuclear Svstems, Xnc., Rad'oac iveShipping Record
Hashincton Low Level Rad'oact've HasteShipment Ce tif'ationNevada Low Level Radioactive Haste Sh'pmentCe t'fication
Attachment XX Nevada Certi"icationA"tachment XXX Driver Instructions for Maintenance of
Exclusive Use Shipment Controls
Attachment XXXX
Attachment XXV
State Police Not'cat'on Forms
Radioact'e Haste T uckRad'ion/Contamination Survev
Attachment XV South Carol'na Rad'oac ive Haste ShipmentCe t'"ication Form
At"achment XVX South Caro'ina Prior Not'"ication andi~|an'st Form
A achme.. Radioact'e Haste Shipment Not'icationForm
oAt achment X x . aVXX" R. dioact've Haste Shipment Cnecko~ Sheet
At"achment XXX
At achment XX
fZif-l00 LinerF~'e Change Sign-Of" Shee"
A"tachment
Attachment X:<XX
Low Level Has e Box Invento=r
Demineralizer Resin Ca'culation SheetPage 3 or. 6Rev. 2
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p II
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12 . 3150 PCP.001
5.0 DETAZLS
The plan" waste processing ecuipment (deminera'"ers,evaporators, etc.) a e designed to process wastes in thechemical and physical orms wnich exist in the operatinglant svsiems. Plane admin'strat've procedures dictate the
plant svstem's chemical ooerating oarameters, and routinesampling of these systems insu e that all parameters arekept with'n the ooerat'ng Limits. Other procedures are ineffect wh'ch -"ever." materials wh'ch effect waste systemoaeration from enter'ng these systems.
Zf alternate or additional ecuipment such as filters,demineralizers, incinerators, etc. are reauired or wasteprocessing they will be operated by the ph'osophyestablished in this manual to assure that the ='nal formsmeet all the regulations =or shipoing and bu ial. Pr'or tothe operat'on of anv alternate eau'pment, procedures will bewritten and approved.
A. Licuid Processina And Solid f'cat.onThe waste evaporators are operated by the instruct'onsgiven in one of the ollowing olant procedures:
1 OHP 4021.002.005 Operation of Waste Evaporator
1 OHP 4021.024.002 Pumping of Waste Evaporator Bot oms
12 OHP 4021.022.00S Placing En Serv'ce and Ooeration 0The South Bor'c Acid EvaporatorXncluding System Kine Up As A Was eEvaporator
1 OHP 4021.022.009 "S" Boric Acid. Evaporator CooldownAnd Pump Out o" Evaporator BotiomsOperating As A Wasto Evaporator
The evaporators are operated for the purpose o"reducina the licuid waste act'vity levels such tha"tnese liauids can be released to tne env'ronment at
'f A wwQ Qconcentracions with'n the L~miis oz .0 ~:R ar 20.Licuids wh'ch are within the lira's, can be releasedd'rect'v without urther processing. With thesere'eases being made the total vo'ume of licuids wn'chrecuire solid'"'ca 'on is reduced. This reduct'onso'idif'ed volume makes it possible for fewer shipmentso" " dioac 've,.at ia's and less volume to be bu"'ed.
The ';..'" of vo'ume reduct'on 's depenceni onconcentration of several chemical ana radiochemicaspec's (See Table Z) .
Page 4 o 26Rev. 2
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'
s 'I
12 PkiP 3150 PC2.001
Zf the concent ation oz boron is allowed to increaseabove the ''mits of Table Z the concentratescr~s"aI.lize in the evaporator when cooled down forpump-out, creating mechanica3. problems or theevaoorator and pumps. To orevent crvstallization ofevaoorator concentrates the corcentration oz boron iskeot below the limits of Table Z and sodium hvd oxideis added as reauired to maintain an elevated oH toconvert the H3303 to sodium tetraboraze which is much
more soluble than H3303.
330 —:2HaQH 'fa234o7 . H20
The concent at'on of chlorides in the evapora orconcentrates is kept below the 3.'m' of Table Z inorder to orevent materia3. damage to the evaoorator. Z"the concentration is al'owed to 'ncrease above the3.imit of Table Z there is a oossib''itv o" co» osion ofthe evaporator 'nternal surzaces, including tne neatertubes. Zf these tubes are corzoded to the point wherethey wou'd leak, activ'ty would enter the steam system.These tubes wou3.d tnen have to be olugged or replaced.
The ac ivity leve's in the evaporator concen rates a e.monitored as an aid to evaluate the need or shieldedtransoort eauipment.
Samples a e taken pe iod'callv bv Chemical Sect'onpe sonnel during tne batcn evapo"ato ope ation tomain"ain tne evaoorator bottoms within the limits ofTable Z, however, evaporator bottoms maybe prooerlvsolidified for shipping and. bu ial within tne 1'mi"s ofTable ZZ by the use of he procedures given 'n th'sprogram.
Page 5 of 25P.ev. 2
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l ~~ ~
I
12 PNP 3150 PCP.001
TABLE INaste Evaporator Normal Oaeratina Limits
BORON, B 20,000 to 30,000 porn as B
CHLORiDES, Cl
Gross Bv total
>9.0
500 ppm
0.2 uci/cc
Page 6 of 26Rev. 2
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j12 PNP 3150 PCP.001
r
TABLE IX
Waste Evaporator Concent=ates L'm's For Solid'ica 'on
BORON
CHLORZDES
ACT1VZTY OF
FZSSZON AND
ACTIVATION PRODUCTS
0 » 40,000 ppm
3 - 11
0 - 1000 ppm
0 - 0.0001 Hillicurie/gram Transport Group
0 - 0.005 Millicurie/gram Transport Group
0 — 0.3 ~hi}.lieu 'e/gram Transport Group i"
Page 7 of. 26Rev. 2
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~ ~
L ~ I 12 P~G'150 PCP.001
SOLIDlFXCATZO".l BY US. OF C
SYST" 2 DESCRIPTION
The svstems described he»e'n are designed to handle thesolidi ication of liquids, evapora or bottoms and othe"concentrated liauids, spen»csin, o" other miscellaneous wastes.
Nas e eed System
The waste =eed svstem cons'sts o= n electr'c motor drivenpump and waste supply 1'ne to trans"e» waste to the line".The Naste Evapo" d'or Bot"oms S"orage Tank Transfer Pumptakes suction = om the ''cuid waste storage tank and pumpswaste into the 1'ner. Nhen usinc; temporarv concent atesholding tanks, waste is pumped through flexible nosedirectlv to the line" with a portable electr'c pump. Theliner 's "'ied until a pre-se" level is reached as detectedbv a leve'enso" suspended =rom tne liner. (See A3 ttachmentZ1Z)
Cement Feed System
Cement and sodium metasi''cate are put into hoppers and areaugered 'nto he liner. Upon con" cting the licuid waste,the sod'um metasil'cate begins to act, shortening the settime o" the cement. Each 'incr is supplied, wi"h an internalmixing device designed to provide thorough mi..'ng of theen ire line coI tents A m zing mo or moun ed on he top 0the liner prior to the "'ll'ng opera 'o.. 's start d prior tothe add'ion of cement..'1izing cont'nues for approximatelytwentv minutes after add'tion o" the cement and sod'ummetasilicate or until the motor automatically trips off dueto high esistance to mixing.
The cement =eed sys em also has a vent 1'ne tocontro'ementdust. Flexible nose is connected at the loading
=lange. Nhen cement 's augered 'nto tne l'ner from thehoppers a vacuum on th's line d aws o=f the a'" being vented=ron the liner. The a'" is th n conveved to tne vent airr'ter.
Page 8 o 26Rv. 2
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12 PtL~ 3150 PCP.001
COLLECTION AND AUAZYS'ZS OF S92lPLES
General Recuirem nts
The PCP shall be used to verify the solidification of atleast one representative test specimen rom at leas everytenth batch.o each tvpe o wet adioactive waste (e.g.evaporator bot"oms, bor''c acid solution).For the purposes of the PCP a batch is defined as the amountin the HZ~ST at the time of sampling p ior to pumping to thesolidifica"ion equipment.
I anv test specimen fails to sol'di y, the batch under testshall be suspended unt'l such time as add'tional testspecimens can be obtained, alternative solid'ficat'onparameters can be determined in acccrcance with the ProcessControl P ocram, anc a subsecuent t;est ve '='essolidi ica" ion. Sol''cation o= the batch mav then beresumed using the alternate solid'ication parametersde termined.
Xf the init'al test specimen from a batch of waste fails toverify solidific tion then representative test specimensshall be collected from each consecutive ba"ch o= tne sametype of waste unt'' three (3) consecutive initial testspecimens demonstrate solidi 'cat'ons. The p"ocess shall bemodified as required to assure so'idi 'c tio~ of subsequentbatches of waste.
For, high activ'tv waste, where the handlinq o= samples couldresult in personnel radiation exposures which areinconsistent with the ALMQ. Principle, representativenonrad'oac"ive samples wil be procuced and tested. Thesesamples should be as close to ne actual wast in. thei"phvs'cal and chemica'roper"'s as possible to ver'fvproper sol'd'cation: parameters.
Pace 9 of 26Rev. 2
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~~
\ 12 Pta 3150 PCP.001
Waste So' d ' icat'n Data Sheet Attachment ZZl
A Waste Solid''cat'on Data Sheet will be mainta'ned oreach test sample solidified. Each data sneet vill containpe tinent in ormation on the test samp" e and tne batchnumbers o vastes solidi=ied based on each test sample.
The Waste Sol'di='cation Data Sheet vill conta'n pert'ner.tinformation on the characterist'cs o the test samplesolid'=ied so as to verify,solidification o. the subsecuent10 batches of simila wastes vithout retesting.The Test Sample Data will include, but not be |.imited to,the type o" vaste s'olidified, major radioact've const'tue..tspH, volume o sample, identi"icatior. o= oil 'n samples and
he ratio o f tne sample to the final volume o = hesolidifiec product.
The Waste Solidification Data Shee" will include the batchnumbe , batcn volume, and date solid'f'ed, for each batchsol'd''ed based on the sample described on the test sampledata sheet.
Collec"'o.. Of Samples
Two samples of the batch o" liauid to be solidif'ed shall betaken =or analysis. Sample sizes shall be compat'ble wi"nthe s andard size sample used for the radioact'vity analysisand the second for the chemical ar.alvsis. I theadioactiv'v levels are too high to permit full size
samples to be taken then smal'er samples shall be taken w.'ththe results-corrected accordingly.
Page 10 o 26Pev. 2
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12 PMP 3150 PCP.001
TEST SOLEDZPlCnT ON AtcD ACCZPTANC" C2ZT 3EA
Test So'ificationTest Solid-'fications should be conaucted using a 1000ml disposable beaker or similar size container. Mixingshould be accomplished bv s-irr'ng unt''1 a homogeneousmixture is obtained. (Min'mum stirring t'me 5minutes.)
Neasu e 'nto the mixirg vesse'3S ml. of the waste tobe solidified.Measure out 479 grams of (Portland l) cement arc 68.56grams of sodium metasilica"e (anhydrous) and acd thisto the waste to be solidi=ied. The cement and sodiummetasilicate (anhvc ous) must be rom tne same 'ot ofmat ria s wh'ch are to be usec for the solidification.
two lots are to be usea "hen «he tes« mus oe maaewith the evact proportions o= each lot which are to beused in the line".Mix the cement (Por"'anc i) and socium metasi'icate(anhydrous) togethe" and slowlv add this mivture to thetest sample while ' is be'ng st'rred.A ter ten (10) minutes of mixing and a homoceneousmixture is obtained allo~ "he waste to stand for amin'mum of 60 minutes.
Solidi ication Acceatabil'tvThe following criteria defines an acceptable solidifica ionprocess ana process parameters.
The solid'cation is consiaered acceptable, '= uponvisual inspection of the sample, tne waste appea s hati" would hold i"s shape '= removec from the bea'<er andi" resists penet=at'on, anc no more than 0.5. o= thetotal volume o» the beaker is " ee water.
Solidification Unacceat bil'tvIf the waste'ails arv o= the c "e ia set =or h above,t..e so 'a'=icat'on wil be termec u..accep- ble and anew se" of sol'ifica"ion parameters will neea to beestablished.
Tf the test solic'=ication is unaccep"able «hen thesame test p ocedures must be =o'lowec on eachsubsecuent batcn of «he same type of waste untiL three(3) consecut've test samples are so''c'='ec.
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12 P5L~ 3150 PCP. 001
Alternate Solidification Parameters
If a test samp3.e ails to provide acceptable solid'ficationof the waste the following procedures should be followed:
Mix eaual volumes of dry cement and water to ensurethat the prob3.em is not a bad batch of cement.
2. Add addi"ional caus 'c solution to the sample to raise.tne pH above 8, i" recu'red.
3. I the.,waste is on'y oart'ally solidified, use lowewaste to cemen" rat'os.Prepare test as ol'ows allowinq at least one hou" =oreach test to so3.idify. If each test doesn't sol'ify,go to the ne..t set o" parameters.
MLSHaste
GHCemen
TZST
G~~(
Sodium NetaS'licate
(Anhvdrous)
Ga13.onsHaste
LIH:-R
BagsCement
BagsSodium MetaSi 'cate
(Anhvd ous)
1. 400 523 75.4 ~ 712 83 11
2. 375 567 82.3 668 88 12
3. 350 592 89.1 623 94 ~ 13
4. 325 624 96.0 - 579 99 14
Packages of cement solid'ed licuid wastes wil3. be held for amin'mum of twenty four (24) hours after solidifications, andver'ication of compliance will be just pr'or to 'oading orshipment and will be documented on Attachment II.Solid'f'cation of ''cuids other tha.. evapora o oo toms maybecome necessary and wi3.3. be done such i:at compliance with allthe aporopr'te regu'ati ns is ve ified pr'or to shipment.
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12 Pt& 315 0 PCP . 0 p 1
B. Comaressibles Nastes
All contaminated or, potentially contaminated compressiblewaste will be taken to a designatec area ne r the nvcraulicbaler. The waste vill then be compressed into d ums.
Material wnich wou'd be in nonccmpliance wi"h theappropriate regu'ations wil'ot be placec '.".to a oackagefor baling.A3. drums which have been filled will be documented as tothe number o= the package, cescription of the contents, dateanc init'als o= person =''nc package anc radioactivesurvev data. "-ach package wil'e sealed and stcrec unt'3.loaded =or shipmenz. arc Burial.Prio to 3.oacing, the package must be cnecked bvEnvironmental Sect'on pe sonnel =or anv incic tion c" holesfa''ures or weak spots at the seams, we3.cs or otherwise.
All of the above ope at'ons are per"ormed within the limitsof the olloving procecure:
12 THP 6010 BAD.303 Solic Nas e Hanc3. ng anc D umming
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~glI
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12 P."1P 3150 PCP.001
C. Noncomoressible Naste-FiltersAll licuic process type "''ters should be remo:ea by thespeci ic 'ndividual filters change procecure (See AttachmentVX, page 5 of 5) and transoortea to the Drumming Poom. ~ oensure adequate drain tiime for removal of =ree stand'ngliquid, fi3.ters must be drainea as follows:Pilter 'Jte ~1inimum Drain T'me
Reactor Coolant
Seal Nate"Injection
coub le-stage stainlesssteel pleated paper
single-stage s a''sssteel p l.ea "ed nape"
15 minutes
15 minutes(10*)
Spent Fue3. Pit
Soent Fuel P'tSkimmer
coub1e-stage sta''sssteel pleatec pape"
doub le-stage s tain's ssteel pleat d paper
1 3 vill,ilute s
'5 minutes
Refue'ng NaterPurification
double-stage stainlessstee3. pleated oaper
15 mi..utes
Seal Nater Return douhle-stage stain3.esssteel 'pleatec oaoer
15 minutes
CVCS Ton Evchance single-stage stalnl esssteel leated paper
1 5 Pillnu e s(10")
B.A. "=vaooratorConcent atesCondensate
single-stage s ain~esssteel pleatea paper
15 minutes(3 0%)
Boric Acid 30" c'oth wrapoed 15 minutes*"
Naste =vaporator 30" cloth wrappedFeed anc Condensa"e
15 minutes"*
Temporary-ReactorCavity and SpentFuel Pit
20" cloth wrapoed10" cloth w aooea
1 5 minutes (1 Qw)15 minutes (5")
/
Large f'ers or h'ch activity ='lters shou3.d be storec 'nthe d~ thev we~e original'v placed in when removed. P'aceall drums 'n s orage area pe" 12 THP 6010 RAD.303: Sol'cNaste Handl'ng and Druviming.
~ t(lnlmt m craln - me cetermlnea by test ~ ng.~","1ax'mum number o= this t':oe of filter is 8 pe" crum.
For proper documentAt"achment XZ."-'ters not analyz cBarnwell Burial S't
'on required dur'ng =''ter changes, see
or solidifiea can not be shiooec to the
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12 P&1P 3150 PCP.001
Miscellaneous-Includina Absolute, and Heaa P'tersAll miscellaneous noncompressible waste must be placed in ametal bov as soon as possible after determination the itemis to be disposed of. No 1'cuid or damp items oz anv kindare- to be placed in metal boves. No metal bov is to besea'ed until 't has been visually inspected bv Env'ronmentalSection personnel, has been numbered and a description othe contents, including approximate ite... si e and amount, 'scompleted on the Low Level Haste Bov Inven"ory, Att chmentXXI.
NOTE: Any box 'which is g eater than 640 cubic feet mustbe placarded on both s'des and 'th ends.
Scintillation VialsNOTE: Insure t:he =ollowing procedure is followed "or
packaging and shipping scintillat'on z'uids.1. Obtain a fif"y-five (55) ga'on waste d w (DOT 17H)
place in the hot lab and label "Po sc'tilla ionvials Only - DO NOT Ship to Barnwel'". Line the drumwith a minimum four (4) mil plastic liner.
2. The final p oduct to absorbent material ratio must notevceed one-to-two.
*3. Place approvimately 3" oz absorbent at he bottom ofthe drum.
4. Place 6" of vials (not to be opened) 'n the container.
S. Place 6" of absorbent in the container.
6. Place 6" oz v'ls in the con a'ne
7. Fil'he remainder of the conta'ne w'th absorbentmate ial.
8. Close container and take to the 587'rumming Poom.
9. Replace w'h new barrel and fol'cw abovelingo
steps =o"
*Approved absorbents1. Diatomaceous Ea" h (Medium G ade)2. Super Pine {Diatomite)3. Speedi Dry4. Hi - Dzy5. Calatom (j>f-P78)6. Ploor Dry 85 Super=inc7. Instant -
Dr'.
Sa e — — Sorb (Pentraso b)Page 15 o" 26Rev. 2
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12 P&IP 3150 PCP. 001
D. RESINS
Spen" res'ns are normally trans e ed to tne spent resinstorage tank to await packaging or shipment. The prooerliner ard cask to be used or the resin shipment wil'edetermined by the activitv of the resin to be packaged(At achment ZV) . The cask to be usea ' determined "romthose available =rom Chem-Huclea and Hittman ';Iuclear andDevelooment Co o., in the'r Radwaste Hardl'ng Servicetianuals. Afte the prope" cask is deciaed on and rece'ved.ac the plant (including checking for contam'nation as perproceau"e 12 THP 6040 PER.467 it should be prepared forshipment using 12 THP 6040 PER.470 "Resir. Transfer "-romSoent Res'n Storage Tank To A Cask", 12 THP 6040 PER.467"Cask Handl'ng", ana this Process Control ~Ianual.
The package, when full, will be checked .or free wa eroe ioaica'ly urti'hipoed. he check for free wate"
wil'ncludecewatering for each check. Th's wil'e done bypumping licuia of= the too or crain'na or pullinc suction
rom the bot om. Each di ferent type of package used w llbe tested such that the volume of licuid wnich mav beremain'ng in the package is known o" each dewate"ing methodused. The volume wn'ch could be r maining will alwavs beunder the volume allowed by the NRC, DOT ana Burial Siteregulations at the time of sh'poing.
Zf regulations recu're resin sol'di ication it will be done afterdewate 'ng by use o" tne cement solia'fication ou line wh'chfo''ows and Attachment V.
Collec 'on of Samples
1. Raa' logical oro"ection
1. 1 Comolv wi l aoo 1'ab ' Radia 'on York Permits.
1.2 Tes" samples which usedisposed o= by olac ngsolid'='cation.
actual waste shall be'n the d'sposal 1'ner after
1.3 A Naste So''a'fication Data Sheet will bemainta'ned =or each test sample sol'di ied'. Eachaata shee" will contain pertinent in=orma ion onthe test sample and the batch nu-.her of wastsol'a''='ed basea on each test sample.
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Waste Solidi "icat'cn Dat Sheet
The Waste Sol=: '=ic t'on Data Sheet wil'ontain pertinentinformation on the characteristics oz tne test sample solid'fiedso as to veri y solidif'cat'cn oz subsecuent batches of simi3.arwastes without retesting.
2.
The test sample cata for spent resin w'3.l 'nclude, but notnecessarily be limited to, tne type oz waste solidified,volume of sample and rat'o of sample vo3.ume tc the zina3.volume of the solidi ied product.The waste so i"'cat'on data sheet w''1 'nclude the Ba chNumber, Batch Volume, and Date So3.'d'='ed, =or each batchsolidified based on sample described.
Collection of Samnles
One sample shal3. be taken fo analvs ' The sam+le shal3. becompat'ble with tne st nd r si" sample used =o= the cammaisotopic analysis. 1'f the radioact'v'"y leve's are too hichto permit full size samp'es to be taken, then smallersamples shal3. be taken with the resu3.ts correctedaccordingly. Sample sizes shall be determined by RadiationProtect'on personnel.
2. Samples should be drawn to allow adecuate time to ™omp'etethe recuired testing and veri ica-ion o solidificationprior to the planned waste sol'di"icat'on procedure.
Test Solidification and Access nceCr'te"'.
Waste Cond't'oninc
L.l I large (i.e., oam c using) cuantit'es ofdetergents are presen , the sample should betreated with an anti-foaming agent. The cuant'tyof ant'- oaming agent e u'red shall be recozdedon At"achment ~ ZZ.
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12 PMP 3150 PCP.001
1.2 Zf oil is present in cuantities greater than 1$ byvolume, the oil should either be emoved by
- skimming, or emulsification agents should be used.to break up tne oil. The auantity of anysubstance adcec to the samp3.e for this purposeshall oe recorced on Attaca~ent ZZZ.
Test Sold.dl:Lcat1on
Anv sample to be solidi=iec sha3.3. be pretre tec as.spec'=ied in Sec"ion 1 unde" Test Solidi=ication andAc"eptanc Criteria.
2 ~ Test Solidi='cations snould be conducted using a 1000ml. disposal beaker or similar size cont incr. M'zinashou d be accomplished bv st'ing with an electr'cmixer until a homogeneous mixture 's obtained, but inno case =or less than three (3) minutes.
3. For the test solidif'cations o res'n, measure into twomixing vessels 240 gms o" uncompacted dewa" erec csine ch anc adc 90 ml of water.
4. Measure out the reau'rec quantities o" cemen- andanhydrous sodium metasilicate as shown below. Vo3.umesare =or loose, unccmpactec material.
Grams Cement Grams Anh;c=ous Sociun Metasilic teWaste Sam+le A Sample B S anal A Sa. oleResins
Resins
5.
189 236 19 24
265 346 27 35
Slowlv adc the cement to the test samp e while ''t isbeing mixed.
6. er all o.- the cene -„ is added, slowly ac" theanhycrous sodium metas'licate to the test sanple whilei" is beinc mixed.
7. A"ter suf='c' (3 m'nutes =-=" " a'1 cement andanhyc ous sodium metasi'icate is acced) m'zing soa homogeneous mixture 's obta'nec 3.low the wastestand for a minimum o= 4 hours.
tha0 o
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~ ~'
12 P.'1P'150 PCP.001
Solidificat'on Acceotabi3.itv
The following criteria define an acceptable solidif'cat'onorocess and process parameters:
1. The sample solidiri ations are considered acceptable ithere is no visual o" drainable free water.
~e ~ The sample sol'd''ations e corside ed acceptable i.upon visual inspection tne waste appears that it wouldhold i s shape i= removed from the oeaker and i"resists penet at'on by a rigid stick.
3. The sample so3.idi icatiors establ'sh a range from tneratios o" cemert to waste that will esult in anacceptable oroduct.
Solid' cat'on Ur. cceotabil'vXf the waste, fails any of the cr'teria set =orth in theSection Soliai=ication Acceptability, thesolidi icat'on wil'e termed unacceptable and a newset of sol'a'f'cation parameters wil'eec to be
.establishec under the orocedures in the SectionA3.ternate Sol'cificat'on Parameters.
2. Xf the t st sol'ci icat'on is unacceptable then thesame test procedures mus- be followed on eachsubsequen batch of the same type or waste unt'1 threeconsecutive test samples are sol'd'.'ec.
A.l ernate Sol'di 'c 'on Paramete s
Xf a test samp'e fails to provide acceptable solid''ca ion ofthe waste tne =ollow'nc procedures should be followed:
Mix equa'olumes of c=v cement and water to ensurethat the problem is no a bad batch of cement.
2. X" the waste is only partially sol'ci=ied, use lowewaste to cement and anhycrous sodium metasil'cateratios. Using the recommencec quartities o" cement andanhvd ous socium metas'''cate, re"uce the waste samplevolume to 215 gms anc continue =eauc'nc the samplevolume by 25 gms unti'e acceptabi'ity c=ite"ia aremet.
NOT"S:
l. The weign of annv rous soc=um me"asil'cate 'sthe cement we'g'".t.
10 pe c n" o
e'c for aica"iors,
to loac'nc
~ Packages o cement so'idifi c " s''ns wi'' be hminimum of twenty-four (24) nou"s a=te
so3.'d'eri='a"'onof compl'nce w''e just priorsn'pment anc will be documented on A achment
ancor
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12 PMP 3150 PCP.001
E. LOADING
Prior to loading a Truck/Trai3.er Inspection shall be maaeusing check of= sheet Attachment Z. All transport vehiclesarriving on site or shipment o" radioactive waste will havea contamination and radiation survey taken prior to entryinto the Auxiliary Building. If the vehicle will not beentering the Auxiliary Builaing, the survey must beper ormed orior to loaaing. Loaa'ng of a cask onto a truckwill be as oer 12 THP 6040 PER.467 "Cask Handling". Loadingof the cask or truck will be such that the packages w'll beloaded as to minimize the exposure toward the front of thet uck. The Ba nwell, South Carolina burial site recuiresthat mixed (bar els and boxes) shipments of low speci"'cactivity materials on sole use vehicles be arranged so thatall boxes are placed toward the back of the truck. TheBeattv, Nevada buria''te doesn't have this recrui ement andboxes and barrels can be mixed on the truck with the onerequirement being that ba" els be olac d on barrels andboxes be olaced on boxes. All loads must be braced tominimize movement of packages auring normal transoort.After December 31, 1982, all arum shipments to the BarnwellBurial Site wil'e palletized. or shipoea in. ooen top vansor on lat bed traile s.
F. NOTIFZCATZON SCH"DULE
For "Large Quantity" Shipments
Aoolication to transoort a "larg auantitv" "radioact'vematerial shipmen" in M'higan should be maae oursuant to thereauirements o" R29.553 of Act. No. 207 of the Public Actsof 1941, as amended, being 29.3 c of the Mich'gan CompiledLaws (Deoartment of State Police - State Fire Safety hoard)and Section 9 of Ac . No. 380 of the Public Acts of 1965, asamended, and Sect'ons 2226, 2233, and 13521 o= Ac No. 368of the Publ'c Acts of 1978, as amenaed be'ng 3 16.109,333.2226, 333.2233 and 333.13521 of the Michigan Comoi'eaLaws .(Michigan Department of Public Health).
The governor or his designee of each state through which the'a. orementioned shioment will " ave must be given advancenot'cat'on 'n acco"dance with .itle '0-Energy Coae oFederal Regulations. P r- 571.5a.
* A "large cuan'itv" shipment is that which 's greate" than 200curies of Group ZZZ and ZV radionucl'des.
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gt
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k~ ~ 12 PtiP 3150 PCP. 001
As burial space is recuired
Both the Beatty, Nevada and R'chland, Nashington burialsites do not have volume al'ocation plans. For burial spacecall:Beatty, Nevada - Steve CarpenterU.S. Ecology, Inc.
702-553-2203
Richland, Washington - Vern D. Apple - 509-377-2411U. S. Zcology, Enc.
At least 3 months before shipment
The Ba nwell, South Caro'ina Bu ial Site has~ a volumeallocation plan. Fo" bu ial space and allocat'on numberscall:Barnwell, S. C. - Angie Jones
VAP/PNP Dept. Linda Bragg(CNSX) Lewis Rouse
803-259-3577803-259-3578
Call Hittman Nuclear and Development Corporation ortransportation and scheduled sn'pment date confirmation ancfollow with a lette».HNDC - Chuck Stout - 312-232-6133
At 1 ast 7 days prior to shipment
Notifv the Michigan Department of Public Health of thescheduled date of sh'pment and est'mated curie conten
Mich. Dept. of Public Health - Joe Hennigan 517 3 3Mike McCarty
Prior Not'fication and Man'fest must be sen" to the Sta e o=South Carolina and tne Barnwell Buria'ite to be received72 hours prior to shipment a" iva'.Ve ify that th proposed carr'er has a valid petit totransport radioac"ive mate ials in the S a"e o Oregon.This ver'".cat'on is onlv recuir d when the consignee is theRichland Burial Site.
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4
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12 Pl& 3150 PCP.001
Dav of shinment, nrior to deaar ure
Notify burial site be'ng shipped to. For shipments to theBarnwell Site, the route through South Caro3.ina must begiven.
Barnwell Burial SiteChem-NuclearSystems, Inc.
Beatty Burial SiteU.S. =-coloav, Inc.
Angie Jones - 803-259-3577Linda Bragg - 803-259-3578
Steve Carpente - 702-553-2203
R'chland Burial Site - Ve n D. Apple - 509-377-2411
If there a e anvHanifest "or themust be notiried
charges in "he Prior Hotific tion andBarnwell Site, the State o South Carolinain addit'on to the Burial Site.
State o- S. C. — Virgil AutrvBetty Bethea - 803-758-7806i(im l3ob3.e
Hoti 'cation of the Michigan State Po3.ice must be givenpr'or to shipment. (See Attachment XIII)Michigan State Police - 616-469-1111
SHIP P IitG
All shipping of radioac=ive ma"eria3.s for burial or forother reasons are reauired by procecure to comply with a'lNRC and DOT regulations. All packaging in the above stepsof this proaram are designed to insure compliance wi h allthe appropr 'te regulations. The followina procedu es areused to insure and!or veri y'compliance with theregu3.at'ons.
PNI 33.50 Receipt And Shipmen" 0 Rad'oactive.aterials ~
THI 3150 Receip" And Shipment Of Radioact'vel|ateria's.
12 THP 6010 RAD.304
12 THP 6040 PER.467
Sh'pment 0= Radioact've liateria3.s
Cask Handl'na
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12 PIG'150 PCP.Q01
The following will be the orde in which the Radioact'veShipment Records (RSR) are to be completed pr'or to anyforms being distributed to the espective personnel.
1.2.3.
4 ~
5.
Completion of shipp'ng, recordsRP Supervisor for s'gnatureEnvironmental Section =or signature and correctioncheck on RSR forms.Carrier for signatureThree (3) copies o" the Chem Nuclear (RSR), and U.S.Ecology, Inc. (RSR) are to be made.
Distribution As Follows:
The originals of tne Shipping Papers will go to theollow'ng personnel, witn copies also listed:
D. C. COOK NUCLEAP. PLA;JT
State Police Notification FormRadioactive Haste Shipment Notification FormRadioac"ive Has"e Shipmen Checkof SheetTruck/Trailer Inspection Check-0f" SheetOriginal To Env™onmen al Sect'onDemineralizer Resin Calculation SheetOriginal To RP1 Copy To Env'=onmental1 Copy To D iverBARN!'(rLL HASTE SPINAGE~'"NT FAC LITY - RSR
Hhite OriginalCanary OriginalPink Original1 Copy1 Copy1 Cony„
To Dr'verTo Environmental SectionTo DrLvezTo StoresTo RP Sec"ionTo HHDC
STATE OF S. C. PN&H AND CERTIFICATION FORMS
3 Copies
1 Copy
Or'inal1 Copy
South Carolina Prior Not'ica"ion andHan fes »orm to Dr'verSouth Caro'ina Prio" No""='cation andManifest Form to Environmental Sect'onSouth Carol'na Radioactive HasteSh'pment Certif'cat'on Fo"m to Dr'verSouth Carolina Radioac ive HasteSh'pment Cer ification Form toEnv'' ronment:al Section
Page 23 o= 26Rev. 2
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12 PNP 3150 PCP.003.
OriginalWhite Or'inalPink Original
«1 Copy2 White DisposaiS'e Copies1 Carrie CopvOrigira3.
U.S. EcoIogv, Inc. {RSR)U.S. Ecology, Inc. (RSR)Nevaaa Low Level Raaioact've WasteShipment Cert'='cat'onDemineraI'ze Resin C iculation SheetNevaca Ce "' 'at'nSouth Caro''na P ior Not = cat'on ana!grani=est Fo mSouth Carol'na Radioact've WasteShipment Cer ''at'n,Radioactive Waste ruck Rad'tion/Contamina"ion Survev
"1 CopyOriginal3 Copies
1 Copy
1 Copy
DRIVER OF TRANSPORT V:-HICLEOrigina'ittman Nuclear & Development Corp.Driver Instructions =or ."maintenance ofExclusive Use Shipment ControlsWashington Low Level Radioactive WasteShipment Certi 'ationBarnwell Waste Hanagement Facil'y (RSP.)Barnwe3.1 'ste Management Fac 1'ty (RSR)Resin Gamma Spectrum P. intout
NOTE: he driver of the transport vehic3.e will be giventwo or more extra placards/placarc holaers forreplacement purposes if znv o= the affixedalacards become Lost or aamagec during transit.For transport vehicles wh'ch the placard holder ispermanent'y a="'xea on all =our (4) siaes, extrapiaca ds will not neec to be given to the d 've".
FiP1IROViii'~i'TAL S»»m~ yOVBarnwell Was e ~management Facility (RSR)State Police Noti=ication FormRadioactive Haste Shipment Not'icat'onFormRac'oactive Waste Sh'pment Checko""SheetRad'ation/Contam'nat'on ruck SurveyResin Garma Spectrum Pr.'ntoutU.S. Ecology, Inc. (RSR)Nevaca Low LeveI Radioactive wasteSh'pment Cer"'='cationNevaca Cert'cationWashington Low Level Racicact've WasteShipment Cert'icat'onSouth Carolira Pr'or Not'=icat'on andFxnifest FormSouth Carol'na Racioactive WasteS>ipmen Ce t'=ica ionT-uck/T=aiie= Inspect'on Check-O=f SheetDeminerai zer Resin Calculation Sheet
Canary Or gznaOriginalOriginalOriginal
~ Copy*Copy
Customer CopvCopy
CopyCopv
Copy
Copy
Or~gznal*Copy
*Only when res' is he'rc shippec. A pagegamraa spec" um p 'ntout anc a Dem'neral'zer Rev. 2Resin calculat'on shee™» -...ust be provicedfor each package contain'rg esii heingshipped.
![Page 36: Rev 2 to Procedure 12 PMP 3150 PCP.001, …xiiiarv Build'ng o eea must be place1 ed intoi a container, b keat from entering are 1 soi's must e. s and must be cleane u d t 1 3.2 No](https://reader033.fdocuments.us/reader033/viewer/2022042204/5ea53f586750b55ccf34f036/html5/thumbnails/36.jpg)
12 PMP 3150 PCP.001
RADZATZOH PROTECTZON SEC ZON
1 CopyOriginal1 CopyOriginal
Barnwell Waste Management Facility (RSR)Radiation/Contamination Truck SurveyU. S. Ecology, Znc. (RSR)Demineralize Resin Calculation Sneet
TRAZ;IZ';IG
Personnel who routinelv handle and snip rad'oactive waste(see Attac'nment VZ) wil'e trained at least annuallv on thecurrent regulations (see References Section) and the plantinstructions and procedures which app3.y to Naste Handling.
Page 26 o= 26Rev. 2
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12 P!Lb 3150 PCP.QQ1Nw'i Cgtf~»%<~ T
Ib1vP+» /mba
SHXP.'K~itT NO.
Pr'or to I.oadinq, "ae ="'o"Ji..c '"ens re "" be e.".amined anddocumented on t!lis checklist =or eac.'". vehicle
"ransportinc'adioactivewaste -rom ".'".e "'t site:
(2}
(3)
tPruc 1» / IP «a q l e «Pl q
RemarksTruck/Tra er "'nee'sRe.".la ksTr iler Sec nc: ra;..eRemarksLoad 'e-wownsRemarks
Z"JEST:ALS
(5) T"uck/Tra.: eRemarksTruck/TraL '
Rema ks
~ Aw«<,o «g
~laca QBQ
Xniti ls ind'cate ins-ection was mace nc = saccent h'e. = '"B...s =„=Bctin sa=e
1Ouilc g COnt- Ct ~ Ltt..aan .'uc - lc DBVB 'Oment.Person Contacted
"s were'oil or loac a«B(3 2-232-6'3)
D tVehicle inspection cri"B ia as =o'lows:
(1) Truck/T"a'ler Ti" s - A mini...um o= 1/'6" "reac, no =ah«icexposed on sicewall, no c .ts o" in ju™ies 'nto ah '.
(2) . uck/.ra'ler bneels - Check =or v's'h'e cracked wneels,loose luc nuts ox''sinq s"uds.
(3) T"ailer Bed anc "." me - Check visuall. =or c=acks ancbreaks. Check ma'.". ra's "or any v's'h'e cracks in ra'sand assoc'a"Bd welcs. On an~. crop =rame tra''e s, tfe drooarea is "'.".e most susceptih e "o crackinc. I" any cracks areobserved in ma'n a'ls, t" ''er shoulc he ce c''..ed andcar Le immecia elv no 'edLoad Tie-Downs - Check cw~'Bany visible cracks. Cables should he
aosL"ioned so "hat cah' co ..o" """ Banc shackles shall be =ree o= c= cks.
cooc coildL i Lon (snould he
ac.". o".".er. Raic'ne s
(5} T uck/ « ' e c. s - C .Bcks o«oQB a on oz nead-lip. s,*+pail J,icf ts I h ake 'n s af Q Q Bcticfia1 sic als.
(6) Truck/ railer P'acarced — Placarding; on =ro..t, sices ancrecui «BQ ~
Paae 1 o 1Rev 2
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Cement Snlidification Verific:ation I
Li»er tlo.
LilleL Vol'lrl(Q
Cement lbs. /bag
Sodiwn t4.tasilicate 3bs./bag(hrrhydroo"l
Date Tine
Tirre Start
Conpletion Date
Corrpletion Tina
Cen)ent Lot I/or DaL.e Arrived
Sodium lletasilicate (Nrhydroo') Lot Il/or. D<lte lKcexved
Verification Date
Verification Tine
Verified By
Ship Date
DM'l'. CAIJAPSNMl'l
PBDCFSS) J)l'ii%f1
tN(LSC['I1I.I
0'lMHt ll ll~~O
CGf tQMl'S n>rnms
Sc))rcll.f3('atlc)ll Ver r.ficclLloll
I here))y cerLify tlrat a viural ior'pection of tire tllllX. 1 irrer i)as beer) c:un<br@ted 'rL'east 24 hoursaft:c r Lhe irulicated corr|l)lc)Lion d'ate arrd time air(1 tlr<rt there wn<s rrot any irrdication of freest<rrrdillg) icloid.
Da te
T3 lne
llHIR Sol)ervi sor
Page 1 of )Bev. 2
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12 PMP 3150 PCP.001ATTACHMENT ZZIBatch No:Sample iVo:Date:
C=~E~fT YiASTZ SOLIDIFICATION DATA SHE- T OR
(.ype of $Nasze)
Batch No: Sample 3o:
Sample Volume, ml:
H(1) .
Indications o- Oil/Dete gent:
Other !major Constituents:
. Quantity of CementAdded:
Quantity of SodiumMeta. Silicate(Anhydrous)
Cement Lot =../or DateReceived
Sodium Hetas'icat(Anhydrous) Lot -,'./or DateRece'ved
Final Produc" to Haste Ratio:
Product Acc ptahility:
Rad'nuclides P esen":(Zso ones a Concen"rations)
If pH adjustmen is recuired notechemical used, cuan"itv used and pHa=ter adjustment.
Pace 1 o" 1Rev. 2
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12 Pr.lP 315'0 PCP. 001A T:-.C.I'~Ah'V
SOLID = IC. TIOif DATA =A"L=S
SUi~'~L~'Z
For head resin, the 'icehsed cask oayload is linitihg for theHV-100 Series 1 aad H'1-100 Se 'es 2. t/eight is hot a linitihgfactor =or the HN-600, H'H-100 Ser'es 3, H~i-100S, ahd HH-200.
222d +~SLl
Ser'es 1
i~?-100Cow~ scI 4 Series 3
Ei-100S:"2<-200 Bl-600
Usable.Volw~ 142 142 142 65
~ABBY. SolL™MieWas'ol. ft~ 120. 3 142 '42 60
~h:<. HasL". Vol.
Hater &dc~ atV~~v. Pasih Vol.gal.
'03. 0
223 ~ 5
QArC ~ v
214. 5
116. 5
223
116. 5 49. 3 53, 4
253.2 106.9 ~15 9
Cam" Ad&1 ft.'agsfatso %dePcvr~ 100.'-. ~cs
52. '
't ~ r 'tr 7
59
5.5
59
3 ~ 3 2.4
2/
2.5
v pRC~ ~v~hLe~1 R/h Coh=c- 12 12 5 800 100
Page 'f 1
Rev ~ 2
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I It)»IF.IrtAltt Id P.tla
a
(ant( SIAl'I Alt;Arf
X X VLSI(I vent.
ItA5I(fvAt.
m»(In»l»rlt»ta
Itnttl IOR It trrIAttLS
5 IAl lbttOtrAItttLI
((>lait)
(I (AttItA' I
VA5I(fYAI'.fili(»S j )
->>.—OCn:tr.
IAILCS(Roti latch.'ttl
5 ttttl Slf tttkfAttl.r
VAS I ((VAI.(Otttr. IAtrr.
VASIII vPr.fnt»t. lAIL
—6
Itt ttt I I It tt Itt0IAttt.
tlltYS
VA'll( I V>trttttt>lit)AI(o tlltta tl la
. L
vASI( (vAr
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Shit( a(SIIIIROtl >I(al AttlIrl»ltt(RA(II(RS
L"-I
Vln S»ll'I'lttn
CAStt
VASI( IYAR.
f0»l I tt I RAI(alltr5
10 CIRC
t llm tu< art~ Q
10 Stllral»0CA'R
SUI IO tLISI( VrtttACIttfltfSlSI(rl
r<rt~ ttu Ltt'Ist
tO CJ1D Ctt't
CA
C; ~
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I Dt
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a I
il llia III
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12 PtIP 3l50 PCP.001ATTACI)tlLtf1'X
tA'I~.IVBIZSTBI2 WAPFl
PAXLSS PIJKGBI&) BY SUPLN'ISED BY VEMIIED BY TNQNTHG BYHaste '1'ransport toBo>(-Karrel
Bo:(-Barrel I'illzng
Ba(lloacL'1veCn))te»t-IsotopicBa tinVc)c):age Sc ale(la»(l la))cled
Pac)(age Qualit>yVeri1 i c)c) tion'I'r»c): Ioa(li!)(g
re)(!k a»d Pac):clgeJ»'>f)ect10» a»()Surve)taclloactlvQS)))ppl»g Ih!(X>L(I
Prior t4tifi(')tin»
ContracL )hint.Perse»»el
7lPersonnel
Ihc)lat lo» Prot.C))(J'))ic() 1 'Itic)l.
Cn»LracLVc '1 1'A3»»e lI'..»Virn)U)>: ntalVerso)«)c 1
> Ll > >> \'0> I a>>CD
IL'cl)a»ic
IL)(liat:ion Prot.I 4').so»» '1 /B)VLLO»l)i!»t'c11
B)virorUw'nta l
I>)viro)U)x»L'c)l
BAD.303
BAD.303
BAD.304
IED. 300
rm.30'eP
IBAD.304
))AD.30<) PCP
I CP
BadlaLlon Prot.51>inte»a»ceSu >Qrvi sorB )(Iiatxo» Prot.Haintena»cew)) x.rv1)>or14«)ic)tin» I'rnt:.S))) >erv1 s(>l
lh')( I) cl t1()n Vl OL.S)))>QLv! HOL/Blvi r I'()LSn»l >elB1viro»)» nL'lVers(>) «)cl )..h>V>>O>>l»'>L1>V( rsor«)el/I t) int;.
~>ul >Qlv!snrIt'«Iiatio» PrnL'.Su))erv 1 1 ~) L /I~lvlLO»))lintc)1Bc)()) c)L'10» I'LOL.Su))c'rvls(>) /lb)virO)U)>t »tc) II'h)vl.rn)llN.'»ta I
-Ihc laLlon ProLQctlonhb lnte»anceSu mrvisnr.)taxation ProtectionGut >rvisnr/lb>vi ro)U)> nta 1I'1()iatio» Prot:ectionSI )I>ervisor/I:»vi ron.Vc)l..S(>) )»L:1lta()1 clt'ln»
PL'AL'')lvlrc>)
Ulled Alt:alV(1Lc<>»»L) l.
I'h)vlrn)«w.»ta 1
Ic!fs()»»c'B)vl.ro)U)>-'»ta1
Ver."a) Ir)el
I h)vi l'c)»))l"»LalI'ers()) «)()1
I'lc)nt lta(l latin»V)nL. S))p.')r/I.'»v i )-n») lr.» L ') 1) U)v1 re) Ua>»t))1
Badic)Lion Prott'ai»t(inc)»CeSu mrvisorBadlaLion ProtIL>)i»te»anceSu >LvisnrB')(liat!on ProSulx.rvlsor
lt')d)atlo» ProtSu)>erv i s(>r/I.~)vir. I'I r n»».BU)vi rn) wIQ» ta 1I'Qr.a)«)( lI'hvlre)MI)1»talI QL ~i%)))) lel
B')(lic)t:i(>» ProtI'~1V i r(>)in%.'))t.alVer ~>»))elBadic)tion Proth)vim»«x.»I;nlI'cirso»»e l.
Hnvlrc«U))enta 1
Page 2 of 5Bev. 2
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I
12 PPIP 3150 I'CP.001ATI'hQII1EMl'X
CA IPIti.SSIBIJ llAS'IP.
PIKCMSII.)ste 'I'ra»sf)ort toDr)Un))fng Ihxx))
Baler Ofx'ration
Badi oact.lveC()nte»L. Isotof)i.cItatioPacl(a(ge Sealedand fal)cled
Pacf (ago Qual 1 tpVerifi(:1)tionTruck IAadln(g
'I'r))ck an(3 Pa()adageI»s[)(?Ctl oil alKlS))rveB'IdioactiveSl)if)f)in(j t(ecn) d
PI~WFD BYConL.racL. Itaint.Perse)mel
Contr')ct BadlaL'ionPrntectior> Per~~)nelBadiation Prot.Q«UI)ical 'I'~cf).
Bad)-It)on Prot.ContractI 61 .'oui)(!1I'.hlvlro)UILDnt llPerse) welI ti).l))L(.'1)anceIk.(!I)an ic/ContractVerso)U)el
Personn( 1/L'nv i rona.»La 1B)(l)aLion Prot.Bwiro)U)a ntalPe). so)U )elB)vlro)U)r)n ta1
PBOCEDtjllHIIAD.303
BAD.303
BAI>. 304
BAD.303
IIAD.303 ICP
IQD.3II4 I'CP
BAD. 304 I'CP
PCP
St JPERVISED BYBadlatlon Prot.plaint:ena»ceSu )exvisorladiat)on Prot.
~Su x~rvisorIha(li()tior) ProL.Sup3rv i!)AL
Ih«f 1 aL'loll P).oL.~>uf)e). v iso) /I.:~!vir. P(!rsonnelI'~)viro)U))»t ) 1
Pe fsell))elI:4)vlro)UI)2»ta1
Pe) so) U)el/Il)int.~+~ill harv) s()llt«liat i on ProL.s))PQ) Vlliol /
I~)vi ro)Uir nL'I) 1
fh«l)at i on ProL..Suf w~l. vis())./Ih)vir. Verso»ne If>lv))O)UI) '»L")1
Vi,"Rlt"?Et'Yfh latlon ProtectionI'lln
L'anal�)ce
Su rvisorBadiatlon Protection+G) I Mlv1sorft.MIiat:)on ProtecLlonSof)ervim)r/L'nviron.I'orso»nelIh«fi)!I:won Prot.L'»vire!U!x.nta1
I'e) x!»»(.lIJ)vl r()lUIL~nta 1
P(!rso))»I l.
Blvl)o)U)le)lta)I'i)rtin))I)el
lb)vi)o)UI)»talI'erS()I)» 1
I'.Iar)t lta(fiat:innPI ot.e(:I: ion m»f )Or/fa)vi) (»UI~»LalId )Vl) OIUI).':ll't:1 l
TBAItfIt% BYBadiatlon ProtHaintenanceQu rvlsorBadiatl.on Protail I fvlsorlta(llaLion ProtSuf)elvxsor
I4« latlon ProtS))p.rvisor. /B)viro)UI)"ntallh lvlro)UIQ))ta l.
Per&)n»(!1l h'IV103)lilt IlthlPa.'1. Son) «!1
fh)diat ion ProtStlf)ervlso) /I'5)vl 1 onlll!))t'al
S)lf)(..rvl'r/I hvi.r V(.rson.I'5 )Vl 1 OIUIL'Ilt(1 1
Pa(feBev.
3of 52
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)12 PhlP 3l50 PCP.001ATl'ACIIMW'I'I
r.rrnms
PI)OCI'"3S
Vent — Dra nFilter llousing
Util ty OperatorAu)(iliary Fquip.Operator
OIIP 021.003.0002 OIIP 4021.003.0001 OIIP 4021.003.0092 OIIP 4021.003.009PCP
PEAf01(htED BY PBQCEDURI SIIPERVISQ) BYU»1t SupervisorAssistant ShiftSupQLvisor
VERIFIED BYUn t SupervisorAssistant ShiftSupervisor
TBAINING BYUn t SupervisorAssisL'clnt ShiftSupervisor
F .lter Br~))ovalan(1 I L cll)s I'el. L'0
DLlu))))in(I Boou)B )rrel Filli»g
Packag(. Sealedarel I c)lx'. led
Co»te»L Isot:opicIb)tioPackage Q))cll i.tyVerificat:io»Blrrel Ia)(l)ngir)t:o CaskCa )I; Closure
I taintenclnceVerso)urel
ht) l»LQ»cl1lee)'erso) u)el
Co)) trac: tIV).so»»el
0 l(A))iCcl 1.
'I'Q(:hn.i (: ii)nPnvi ro) u)e»ta1I e) sIll lr '1hta 1) ltenclnceN~chi)»icIfli »Lena»ceI L~C.'hcl I)1(.
lttlV 5021.001.001I)M).303
'IM).313htllP 5021.001. 001IND.303
rtAD.304
IIAD.304
IIAI).304lrCV
I tat.467
I'IX.467
Badlatio» Prot.hL') l»t:I)MinceS» x)rvi&)1.
ht') 1»teni))leeGu )Qrvls()rBl(liat;lo» Prot.Gl)ILervlc)()1 /L'»vir. Perso)uuelBadiatiO)1Prot ectio»
~S() x.'rviu( rrBlvl):olu)L)nta1
Per.an»r) 1
Fnviro)e) ntalVers()»))c lLaws ro)uuenta1VQ).sonne1
B11d i)L'lon P).oLeclL) l»L'('.1)i))leeI Ql. sonne]It;)(Ili)I:ion Protec.G»I)Q). Vilur/I')wir.I L'.Lson»ellh)(I>c) tion Vr()tec.I'hlv) l01u1&»tellVc!1, so»»ulIt:)(Iicltio» Protec.G))ILQ1'v 1 sorh)V)1 Alulc)IL'cl) Pe).'Sonr:nvrrnlnollt;lrVerso»»elI')Ilre)uue»La1I Q'rso»»e 1
I~WXro)u)r)»tcl 1
I'QLsolll)el
Bad>at:son Prott'ai))to»cl)1CQGu x!rvisorItadi ation PLQLItlintenance
~Su )( nnsorlt)(I>at on Prot.Supervisor/E»v.Pi)Iso»»elltadiat:ion Prot.Ver!Lo)Lnel
Puv ro)u)L'ntalPerson»rllFnviro)u))entalVerso) )lie lBlvlrnrlln ntnrr'I.'rnomlol
Truck and CaskIn: paction-Suwey
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12 PHP 3150 PCP ,001AttaCimeflt IX
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12 PtiP 3150 PCP.001ATTACHtiENT XI
CER I.ICATZON
THIS IS TO C=PTIFY THAT I HAV" R-AD AID UtiDERSTA'iD THEREQUIREt'|EtiTS OF LICEtiSE v 1 3 1 1 00 4 3 0 2 ISSUED TiO U ~ S ~ ECOLOGY IItiC. BY THE HEVADA DEPAR. tKNT OF HUa4AN R" SOURC=S FOR TH" RECEIPTAND DISPOSAL OF RADIOACTIVE:QTERIALS AT BEATTY, H VADA~ ASDESCRIBED ZH PARAGRAPHS 5.1.1.3; 5.1.1.4; 5.1.1.5; 5.1.1.6 anc5.4.6.1 OF THr. U.S. "COLOGY, ItiC. SI OPERATIONS ';GQiUAL, AtiD IFURTHER C RTIFY HA ™HE ."WTE. ALS Itl T..IS SHIPt'~'HT ARE IHCOtiFORi~iITY hiTH HOSE REQUIRE~K iTS.
COMPANY
AUTHORZZ ED S ZGiiATURE
TITLE
DATE
Page 1 ofRev. 2
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12 --'-' 5oATTACHMENT XXX
D18 RUC OHS FOR ~IAZNTZN&ilC" GFEfiCLUSXVE USE SniP"'"NT CONTROLS
Thissh'oadin
mipmen is to be maintained as an exclus've use shi n t'p
~ ening must be per=ormed by a single consigner having the
exc3.usive use oz the vehicle. Unloading must be done bv theconsignee, and only at the des'nated destinat'on.Repositioning or movement oz anv loaded material vi"houwr'tten permission or the consignor or Hittman Nuclear &
Development Cor orat'on 's prohibit
Page 1 o~ 1Rev. 2
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12 PNP 3150 PCP.001ATTACH."1ENT XZZZ
S.ATE POLICE:TOTZFICATION FORM
A.
B.
C.
CAi~ER':OAF'OLOR
AilD NJHBER OF CAB
COLOR, .'lUHBER, AilDLEiilGTH OF TRAILER
D. ROUTE FROl1 P~~N 'HROUG"NZCHZGAH AiND IilDIA~lA
TYPE AiilD DESCRIPT ONOF COHTAZi'lER
DESCRZPTZO'l 0- SHiP '" lT
G i i~ ZI'1U~4 'RDIAT Oil LOSELZn '~a/1 R AT 6 "-"==-= FRO:-1TRAILER
TOTAL CURIE CCtlT"al OFSHIP< I='.:T
I TZ"+ A."lD DATE OF S'ZP!1EilT
J. COl1PAi~lY ilAL~< I 6 l1 Elec" r ' Co. D. C. Cook P1an
K. YOUR NAi1E
Brxacman, 1i .
Page 1 or 1Rev. 2
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INCOMING SURVEY - FLAT""EO
12 PMP 3150 PCP .001Attachment XIV
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INCOMING SUR1 7 - lA > OR 'Rr':GTOP
12 PMP 3150 PCP .001Attachment XIV
"All smears <50 dpm and .allreadings <.2 mR/hr, unlessnoted'
m~ ~
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Technician
Time Instrument
OUTGO'G SUR>!KY - V"" 0"- -" —">
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r a i 1er-.-.'ateMax. Rad. Level (C) T)me
~ Max. Rad. Level (6') Technician
Max. Rad. Level (3') Instrumentage 2 ofexv
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12 PHP 3150 PCP .001Attachment X IV
INCOMING SUR>lEY «Al 1 smears <50 dcm and al 1
readincs <.2 mR/hr, unlessnoted.
1 a ~~ ~
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OUTGOING SURYA: C„S
f
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i4!ax. Rad. Level (C)
i'iax. Rad. Level (6')
Time
Technician
Max. Rad. Level (3') InstrumentS
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Tma BRA~(5i$4)
12 PNP 3150 PCP .0'!Attachment XVI~c ve Aascs 3" ~c ? ~ 'wc '~~ 4CI'~sst
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12 PMP 3150 PCP.(ATTACHMENT XVI:I
Radioac"ive Waste Shipment Check Of Shee"
Prior to Shiament Date
Shipment No.
Prior Notification Forms <tailed
Allacation No.
Recuixement:
Gite Date «n 4 «a«ea.~ 1
At leas seven (7) days pxior to date of shipment
BarbellBeattyRichland
Gtate InitialMichiganSouth Carolina
Pr'or Noti"'cation Eorms e3.ecaaied *(If Flailing Recuireme.." IsNot L4Iet)
Requirement.:
Sita
At least seventy-two {72} hou s pr'ar to arrivalof shipment at tne Buria'ite.
InitialBarbellBeattyRichland
Priox Noti 'cat'on Given (Telephone}
Recuirement:
Gtate
Michigan
Date Init'lAt least seven days pr'ox to date o= shipment.
Shipment Schedule Arranced (Telephane)
Recuirement: When shipping schedule has been determ'ned vithapplicable Bu. ial Site.
niKC Personnel Contacted Date ZaitiaiSh'ment Schedule Arranced (i~lail)
Recuix'ement: On dav of telephone notification.HNDC Personnel "-orms Mailed To (Name)
Pace 1 of 2Rev. 2
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>e ca'm1 ~ 12 P??P 3150 PCP.001
ATTACHMENT XVTZZ
Date of Shipment
State Police Hotificat'onRequirement: At least one hour prior to shipment departure.
Date T'me In'"ial
Bur'al Site NotificationRequirement: To be given when shipment depa ts plant s'te.Date Time Pe sonnel Cont cted Site Initial
BarnwellBeattyRichland
State NotificationRequirement: Noti 'cat'on given only i= there is a change in
the PN&?i Form.
Time Pe sonnel Contacted State InitialSouth
Carol'na
Radioactive Sh'ament Record (RSR) Check For Completeness
Requirement. Thorough check of every colure on RSR for properword.'ng and correc info~tion.
Date Time RSR Initial
Vehicle lPackaae Check
Chem-~luc learU.S. =-col.cgy, Inc.
Date Time Vehic'e Tni te al Packace In'i lPlacardedSurveyed
LabeledSe* edSurveyed
Page 2 o 2Rev. 2
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12 PMP 3150 PCP ,001Attach))ent X EX
F~t.;=; ='".B(7S2
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Page 1 of 1
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SHEET OF
12 PtG? 3150 PCP. 001ATTACKIEtlT XXIBOX alO.
LCK7 '~ $ %5T"- BZ{ Lga~ZO~Z
bXZE hWKXZ~~SZBL. SOLID ~H OiK'r. ~O MQL~ OR LIQUID FCGNWVKRS.
DES~~i.~CA APP:"QX. SIZE c~~tD &iCLiuZ DAT I D~ITL~
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Page 1 of 1Rev, 2
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1 ~12 P~iP 3150 PCP.001ATT3CEMENT Zn
CRAG=" SZC.i~
NCTE The t'm ~~~cd bet,am Step 1 and Step 2 aust he great~~t~ or ~1 to '5 minutes.
GP~~WtS car / ~x / av
STEP 1 ~ Pil~-Vente5 and Dta'-.ea (cia~ca '~p) / /place tMs fern cn pap pane" at,"'ch site.
HGZH
SZEP 2: Rerrave =U.", ~~spar" m 587'ru~gRocm and olace in Dn~ (ti~ f'~" " "~mved~ ~~ing) .
NZE: Fil"or rust ".zt have a congruousz'cw of water cm ".g =an it.Xt should only >a c"i~i".g.
Caut'on: Use ev"~acare, wing placi;g ""o"ilt~ into there~sv~g ccu. el toavoid sowaiirqc"nomination.
STZ? 2 mm minus ~33~~ Dra'1 T~s. ~iirutes
5hinte~anc oerscI ml shed cave =own toRP oe scrawl cove~".g tm~ jcb.
BADDZIO'A PKlV~CN
FilterFilte
Drum Nur~
Contact Badiaticn Reading
hCTE: L~ the~t m"ation msu~ tsare ctheater t~an 2200cm/100 ~~ tlat bar=elmus" he deconr ~
un'helevels are lessthan 2200 ca@/100 an~as~ r~rce9,.
3'adiaticn Paaiir.a
Af~ ~let'™go" t~'s si~t, BP s.'"~~" =or~ to ~"~ =re'~~~»Sec~en
Page 1o 1Rev. 2
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12 Pt<> 3150 PCP. 001A ~&CHANT XZZZ
DEZKPKZZH 3HZ'MZKZOi' M
iM-54Co-57Co-58Co~0
I-131Cs-134Cs-13oCs-3.37BaLa-1 40Zr-95iW-95So-124
~~~ATZ&lB2f ZAG
(a)HZ~O'.lOF K71RL
CCKMZEQZZC'l
1.00
(b)-./10
0.47I 0.09I U.55
1.32 I
1. 43
0+870.94 I
0 '30.410.420.98 I
(c)DPCSUBE
CCiK. ~GTXGJl(a) x (b)
'ZCP~D.%~Plyw~l PZSZil(a) x (e)
Exnosure C"n~ibutim (c) = Frac"'cn o" total conco~~~tion (a) z -./10 (b)
Bcpasure at. 1 nate ~ 100 n1. sar@le =
Xf reading taken at 3 ft., R/hr a" 1 rat» = R/hr at 3 f". z .836x .836
(B) Resin volte zac~ = ft'n cask x 283.2
x 283.2
x (8)
'3rtm1, acmviM is resin = st at 1 meter x r sin volcan .actor (d)Toz~ ' cx)~~e ~i~MLLLon Ic)
Pe o~ hv
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Ci (e)
Dat=
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