Research Contract Report · 68 . field data inputs: rectangular stack area (sq ft) volume sampled,...

APPENDICES

APPENDIX A-1

FIELD DATA AND CALCULATION SHEETS FOR APRil 30 1998 SOURCE TEST

NICKEL CALCULATION SHEET

PLANT Foss Plating SOURCE Exhaust METHOD CARB 433 DATE 43098 STANDARD TEMP (EPA= 68 DEG) 68

RUN NUMBER 1 2 3 FIELD DATA INPUTS BAROMETRIC PRESSURE (Pb) 2975 2975 2975 RECTANGULAR STACK AREA (SQ FT) 178 178 178 PITOT CORRECTION (Cp) 084 084 084 SQRTDELTAP 1040 1050 1050 STACK TEMP (DEG F) 1060 860 1022 STATIC PRESSURE (Ps) 065 065 065 VOLUME SAMPLED (Vm) 77597 78401 79197 METER TEMPERATURE (DEG F) 810 940 890 METERGAMMA 1006 1006 1006 DELTA H (INCHES WATER) 124 127 127 LIQUID COLLECTED (VLC) 422 400 409 02 2090 2090 2090 CO2 001 001 001 SAMPLING TIME (MINUTES) 1260 1260 1260 NOZZLE DIAMETER (INCHES) 0187 0187 0187

PROCESS DATA AMPERE HOURSHOUR 4499 4171 4021

LABORATORY DATA NICKEL (ug) 26000 53000 52000

FLOW RESULTS VOLUME SAMPLED DSCF 75986 74977 76428 VOLUME SAMPLED DSCM 2152 2123 2164 MOISTURE IN SAMPLE (CF) 199 189 193 MOISTURE () 255 246 246 MOLECULAR WEIGHT (DRY) 2884 2884 2884 MOLECULAR WEIGHT (WET) 2856 2857 2857 STACK VELOCITY (FTSEC) 6091 6038 6127 ACTUALCFM 6505 6449 6544 STANDARD CFM 6043 6211 6121 DRY STANDARD CFM 5889 6058 5970

NICKEL RESULTS ISOKINETIC SAMPLING RATE (100 110 956 917 948

NICKEL (mgDSCM) 001208 002496 002403 NICKEL (mgHR) 120899 256953 243714 NICKEL (m~AMP HOUR) 002688 006161 006062

PACIFIC ENVIRONMENTAL SERVICES INC

FIELD DATA

I

- 0 ii 0 m z

0

m

r

m

Plant rc p_~ttJc Date ~--_ _ wa-s t-laquolw--sr Sampling Local ion -l t bull bull

Sample Type ~I V_---~_

Run Number______________

Operator ff J - Hz I ltgt Ambient Temperatnre ____5=--0 fL_______ naromctric Pressure -t-l2 Static Pressure ~ o ( r-

Pilter Number(s) _____-fllt_________

Pretest Leak Rate O CPM -z in Ilg Read And Reconl All Data Every_1 Minutes

Traverse Sampling Clock Gas Meter Point Time Time Reading

Number 0 Vm (minutes) (24 hr clock) (cubic reel)

A-I t 09bull 411ogt z middot1 fltiu 4 li - I i 0 q_ gtlt-I 41uo l 7l Miti -1 l 1

7_( (le s ~ ti a ( 5 0 SS ~1 B

Amiddotbull I n 10c degI I l 4q 1010 4-101

~ 10 ~ ~iLgt 1 t 0 Li LiI l r C) Io 6j 451 I 1-1- 1035 1 lilJ l

lt-1 8t O -it 111 ~ t 10 53 4 14lt q Cp oogt --1l

1 tot llOl S 1 II l il 11t i 0 -I l l I I ~ L I I

~( 2ClO 1-( ltO

Velocity Head

Ps (in 1120) 04t

I I I

I QC

I

I bull l-

I bull t DI I I I bull l- bull 2- deg _ Ibull I-

J~

l l --

fArl- I __

Schematic or Traverse Point Layout

=-1 Orifice Pressure Stack

Differential (in 1120) Temp b H Ts

Desired Actual (f) l o 1 i) In is I 1 lgt- to lS- -1 lo-1 Imiddot z ~- Imiddot Zgt o~ middotl~ Ibull ic- 0~ 0 19 olt1

bull 1 1middot11 o) 1r LC- ov

bull1- 7- I)

~( I ~l 01 I 1 c 110 Ibulllt I o IIltgt lbulll-tdeg I 2- - hO I tt Imiddotgtlt- 11-z u H n bull ~1- Imiddot ll- i OI ( lt 0l-

IX I bulllS 101 - --

Probe Length aml Type 1 c - -L-- L Pitol Tube ID No___$_-__A~-----Nozzle ID No Ami Diameter o middot l ezs-Assumed Moisture __~-z_~-------Meter Dox Number LI_-----------MeIer Delta ll---~~middot3~ti~1--________ t Pactor I I -1 Meter Gamma bull o_ Heater nox Sening_____________ Reference Delta P____-________ Post test Leak Rate o cos Cfolvl 1 o in Ilg lmpinger nox No se Diani Dox No lt~

Drv Gas tvkter Temn Unt[l I leatcd foilter lmringer Inlet Outlet Vacuum Probe nox Temp

Tmin Tm out Tent[ Temp (f) (f) (in Ilg) (f) (f) (f) l- I qc 3 tJA ~A _l- -l 4 f c l ~ 4 lt Re i Lt io ~7- l-1 d 5 I ~1 t 5 I f-i1 I-(bull ~ S 1-Z ~v ji S1)

8-i _ 1 SI ~ r8 ~ Sz

~1- o 511 Jli ampO -4 S-ltt an 81 4 5~ l (I A~ -t i-i 10 li4 51 qo 11 q z I 0 (lt ~degLi 5 ~ gtf

bull J - - - --l-- ~ AD- 01 1_ -I ~u

8~ l

1~ I

o ~s uM Oi u

81

I

FIELD DATA

Plant fo-~ eu-n 4 Dale -gtv 1-tamp Sampling Location_ _E=-ax-trw=~~r______ Sample Type (Ml( igt ~ Run Number__-------------Operator rJ(I 97iltt Ambient Tempera1ure__9o-middote_______ narometric Pressure 1-

S1a1ic Pressure O bull -

Filler Number(s) ___~_A_________

Pretest Leak Rate 1S eFM~ oo8~ C1~ Read And Record All Data Every Minutes

Traverse Sampling Clock Point Time Time

Number 8 Vm rs m

(minutes) (24 hr clock) (cubic feet) (in 1120) A - I C 11-~ poundlegtltuo1 t) 0

1 1 11ol ttct Ibull 0 l)Cjf

I 1I

114 t11

~tl0 -gt () -Z gt

bull l bull

-n-_

ZIH

C l

ltt

11-Z9 Ii lC

11- i

-zc-o

QtC

SoI middotbull -ei 1~ I tsbull C

t 10

I Igt bull Z

gt 1-

-

~(

c io l

l- 1- 0 ltI

I l6

i 2t 4 gtZl-~3t E bull~ I S

)

11 i (

I- I ~ I I ~7 4- bull L I 2 t 411 ll l gt-iU bull l

)

t

6 IIJS It1

l~t 0 ~bull--11 ~1

~~~ (J

fc 4 v Sli 3

I t--~ Ibull

C

-O It 1 Iu

l4o 4 05

jlal 0

5Ca i oo-t i l --

Gas Meter Velocity Reading llead

Probe Length and Type 1 ~s Cu~s LN c Pilot Tube ID No c - bull--------------Nozzle ID No And Diameter o Qt(

Assumed Moismre ___1--________

Meter nox Numher__~~u_-------shyMeter Della 11__ middot i-~actor Meter Gamma middot o

Heater nox Scuing___iJ-----------Reference Della r____________ Post lest Leak Rate----1pound Cll1 Ooos in Ilg lmpinger Ilox No~ nlank nnx No (~

Dry Gas Meter Temp P11mp lka1cd Filler lmpinger Inlet 0111le1 Vacuum Probe nox Temp

Tmin Tm out Temp Temp (F) (F) (in Ill) (F) (F) ff) H4 ~H II ~ 1-A s-s-q 11q ~

4~ M 4 lt ~ 91 4 Sl 41 10 4 t~ ~(I ~-C a1 v I -f s-ltiLo bull I lj

bull 4 ) v 1_ Cltbull -Z ~(~ I bull (fl t 0 Ort f SZ

Tl- gt ampI q r i~ ~bull J9Pa 5U gt

q middot1~ ( q 3 n q 7-

- - Ill I -Lt ~B LUM

Ill I 0fiu

~~ middot~ y I

Schematic of Traverse Point Layout

Orifice Pressure Differential (in 1120)

-6H Desired 10 l bull I 1a

middotZ-S-I bulll 0 lo 11lt 1-H I 1 l lmiddotHbull r-ir lt I deg11 I middot JC l-IP Imiddot l O 11-r -

Actual l I c)

cp 1(deg

tamp bull-

lO II lI l I A

l1 lt t1c lmiddotlC-lmiddot zr v

-1~ S-middotS-bull I (

-

Stack Temp

Ts (F)

0--1 li z

j(

- II

U fl--07 llll a2 cO l-J e C l-~ gt j-1 n

l-R-to( JAigt= l111i I Z Q ii I

~ J bullbull

FIELD DATA

Planl Date

fo-l P~MT-Li 1o i t

Probe Length and Type Pi101 Tube ID No

1 ) gt lti lt= s c -1-A

-middot -I

Sampling Location Q~ (fyenA~( Nozzle ID No And Diameter O ( SJC Sample Type Cnt1z t1gt Assumed lvloisture ___________ Run Number Operator Ambient Tempern1ure

~

f1 Jtt pr J() bull iJobullp

Cu- fnv Meter Dox Number Meler Delta IIreg C factor ~ -

l _

( ~ -z1

l- Darometric Pressure 1-j bull l[ lt Meter Gamma ( ll1J I

S1a1ic Pressure filter Nurnber(s)

-1 o - S IJ P

llealer Dox Selling _i Reference Delta r____________ -

Pre1es1 Lenk Rate~ CfM 10 bull in Ilg Schematic of Post lest Leak Rate 1-50 Cltvl zo in Ilg Read And Record All Dain Every l- Minutes Traverse Point Layout lmpinger Dox No____Bh Dlank nox No lB

I

~ Traverse Sampling Clock Gas Meler Velocity Orifice Pressure Stack Div Gas tvkter Temp Pump lka1cd Filter lmringer 0 Point Time Time Rending llend Differential (in 1120) Temp Inlet O111le1 Vacuum Prohe Dot Temp

Number 8 Vm rs b H Ts Tm in Tm 0111 Temp Temp

0

m

1

(minutes) (24 hr clock) u lL-zo I l4 1- middot+ I f l~4 11 1 l

(cubic feel) tCIB bull ffrac12l Sl~ Sl--l-o RI)

(in 1120) oClgt 0 l I I

Desired l 0 I ltt

bull llt zr-

Acnml Ibulllt) middot-l Imiddot t bulllf

(f) Bi i

o

(f) IAlt~

gtmiddot~

(F) l_ 2-

(in Ilg) ro 30 0 o

(F) i-

(f) A

ff) (0

(o

uO ( 0

~ I

n-

1t 11

14 q JJ IAlI~

I co

Slll1 ~10J 1l1 l

I bull t d

bull Z tItr

I 1-bull zr-bull1 (

ttl o- l08

I10 if iJ

pound I

ll iu

gt lo ~tgt

r rJ -i- ll

I 1 1 I S 0 ~ t o bull I bull1 f I l s I 01i t HC 70 SS-r1

4 (

_

Slt lO l-1 8-A q cSj

51-l i l~~I Sl~ 1

P~ 11S 3

(lIO

lto~o LO l f Ibull I l -

(11 bullbull S 11-Z0-1 ozsmiddot~ 111 I I

Ibull 1 I bull1 I 1

II l middot-l

I(

i ) I lS ir

I 3pound 1 H

I I deg( bull)~ 1t-~ I bull llt

I I 7 I

lu~ lotgt l l

U I II 0 I bull0 I 1--

ej 8l CI) qo ~I 1r1 f1

~~ BC BIJ be R~ rf ll4

J-0 middot 0

middot1 0 0

ZO lO middotro

gt1 deg1~ ~r S ss 5~

lt u

lIJI

10~ l 1

tlli 111

1i-01-1111 t (Z t tz~

(J ~ S ~~I I ut~CJ nU~NgtY

h1 ~ I I -

1t bull I t

(oI~

-

Ill

tr-It l I (1-

Bt BIz-

RI H t ~~ -

LO 7 b

1ltgt- I

15s ---

u[ ~a uyL

l-1 bull e r To 105 I 1~] ((11 ~IIi

55 uu

81

r~=-~~~ ~o-- --ts==

r _ I Z i S ( --middotmiddot ra~s poundlt--TIN C ICJ middotbull--middot -I_ 30 l1 c

Cc c~ ec ~- - A -middotmiddot s=- O =i=-=~i rcssc=e 1 li amp- 1 I

Sc- Cabull- Ccs~ EzC +-0 Cc~ Ceil ~ T-i

- --- -middotmiddot------------c= ~

j- l r ln c lt_--= -3

- ___ ~ n middot~------ ~- A t ~~ C - Cl

-J--ejel ilccmiddot IS I cc middot-- =-i --- -1 bull ---- (_l l e_ cr ced

~-=-=~ = bull E~ ( - ) bull bull =c= it

Smiddot l

L

3

-I

S

(

B - I

2

middot3

y

s (

Q -

1

)

ltt

s-(

I f--so I deg17- I I I a I C~ I I bull I I i V I I I I deg-~ I I LO I ~~ I Io Ii 1 I Ct I I t 2 I ct( I I ( 1 SI I I gt I cq I I I bull 1 I l I I 1-1 I l lt I I I I 0 C I I 0 cit I ltt L I I 11 I 11 I I I- i I l S I I I bull 3 I ctlt I I I 1 I I lj I r~ I -U 1 t1-I ltl~ I I I I I I I

0

5

s-~

0 3

t)

5 3 ~

2-2--

2

s s

3 1

0

~---~ s--~c-bull-middot--__ ---middotmiddot

Sc ~i c - 111 le C ~

~ 1

1 t

I

~Z

T a T

I I

03 I

T

-r=imiddot-e=aIiJcci C f s ticlt IC-f F- E~ (~p3 ) T~p l _ Ce Nt--~= i EO T )bull bull === il

I I I I I I I I III I

II I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I f

I I I I I I I I I

~= z-e ~bullmiddotc=zi ~I I I I I I PJClrIC Nl~C-0bull1-rmiddot1 sv1CS3 llIC

sect388

TRAVERSE POINT LOCATIONS FOR RECTANGULAR DUCTS

PLANT i=o frac14 Plah ~

CATE -2C-qo

poundn~v---SAMPLING LOClTION ~i1c 1 -r~ -s (INSIOc STACK OIMENSIONS llo X

INSIOE_ OF NEAR WALL TO OUTSIOE OF NIPPLE (OistJnca Bl ~

EQUIVALENT STACK 10 It NEAREST UPSTREAM DISTURBANCE 10amp middotnNEAREST DOWNSTREAM DISTURBANCE

NUMBER OF TRAVERSE POINTS l1_ARRAY 3 X I(

CA LC ULA TOR J RJP1D

ILLUSTRATE PORT LOCATIONS

AND STACK DIMENSIONS

C 1

-C]-z I

l ( r 3

J_ c v v

r I c -1

POINT INSIDE OF NEAR

WALL TO TRAVERSE POINT

(Distance A) DISTANCE B

lRAVERSE POINT LOCATiON FROM OUTSIDE OF NIPPLE

(SUM OF DISTANCES A+B)

PORT LO CATION

OISTAICE FROM

EDGE

I 4i-~ c- ~ ILo A zclt

2

3

3--4-- ~-i

bullI amp 6 io

1 B

i 0 I middotB C

-middot 11- 3 l3

i

s

~ 112

--tt Ill 0 ~

117-

I I

b 0

I

TRAVERSE

NUMBER OF STACK

P_CIFIC ENVIRONMENTAi SERVICES INC

MOISTURE RECOVERY SHEET PACIFIC E~VIRONiVIENTAL SERVICES INC

FACIIITY

SOURCE

DATE

RUN

METHOD

BOX

IMPINGER CONTENTS FINAL

GR6--IS

INITLU

GRAMS

r

TOTAL

GRMS

I DL WATER 6J7 a 2-10

2 DI WATER roo -r fgtJ s l L

J EMPTY 9 PC 7 -f- t t)

4 SILICA GEL Trl 7Jlo (L1

TOTAL GRAJvfS COLLECTED

INITALS

MOISTURE RECOVERY SHEET PACIFIC EilVIRONlIENTAL SERViCES INC

FACIJITY

SOURCE

DATE

RUN

METHOD

BOX

ThIPINGER COTiltTS FINAL ThlTIL TOTAL

GRJ-15 GR-15 GRJ-15

I

2

3

4

DI WATER

DI WATER

EMPIT

SILICA GEL

2--Z

~-~

o ~ (

middot1TOTAL GRAflfS COLLECTED 40o

INITALS

iIOISTURE RECOVERY SHEET PACIFIC EifVIRONliIENTAL SER11CES INC

FACIIITY

SOURCE

DATE

RUN

METHOD we zrJ BOX

L-fPINGER CO~TINTS FINAL INITIAL TOTAL

GR-1S GRMS

IIf

~D

I DIWATER

GRltJ-IS

e

2

3

4

DI WATER

EMPTY

SILICA GEL

I 0

IS--L

-~OTAL GRAvS COLLECTED 40 L 9

INITALS

iIOISTURE RECOVERY SHEET

PACIFIC EiVJRONi-IENTAL SERVICES INC

FACfIITY

SOURCE

DATE

RUN

METHOD

BOX

DIPINGER CONTEItTS FINAL Th1TLL TOTAL

GRJ-1S

I DI WATER

2 DI WATER

3 EMPTY

4 SILICA GEL

GRJ1S

t~c

Sf

GRJ-IS

-o~z -og

-o J

-02

TOTAL GRM-1S COLLECTED -4

INlTALS t

NOMENCLATURE

Units Aliquot mls of sample analyzed mls As cross-sectional area of stack ft2

Bp barometric pressure Hg Bwo moisture content of stack gas Cp Pitot tube coefficient Ds stack diameter inch DSCF dry standard cubic feet (through meter) CF DSCFM dry standard cubic feet per minute (in flue gas) CFM L length of rectangular duct inch mg milligrams grams MWd dry molecular weight of stack gas lbmole MWw wet molecular weight of stack gas lbmole Ps static pressure of stack gas H2Q Pstd standard pressure (2992) Hg SCFM standard cubic feet per minute CFM Tm dry gas meter temperature R Ts stack temperature R Tstd standard temperature (SCAQMD = 60deg EPA= 68j R Tstd degC standard temp in degCelcius (SCAQMD = 1556 EPA= 20j Vic Vm

volume of liquid collected gas volume at meter condition

g ft3

Vmstd gas volume at dry standard condition ft3

Vs stack gas velocity ftsec Vwstd moisture volume at standard conditions ft3

w width of rectangular duct inch y accuracy of dry gas meter (gamma) microg micrograms grams Aff orifice differential pressure H2O fip velocity pressure head ( average of square roots) H2O CO carbon monoxide content of stack gas vol CO2 carbon dioxide content of stack gas vol N2 nitrogen content of stack gas vol 02 oxygen content of stack gas vol

1

middotmiddot middot (1) STANDARD METER VOLUME DRY

Vmstd = (Vm) (Y) _(T_std_) (B__p_+----(MI__1_3---6)_) (Tm) (Pstd)

letgt +460) ( -ZHmiddot+( 1 136))

8 1 + 460) (2992)

Vmstd = 1- S middot i ampCo

(2) MOISTURE CONTENT OF EXHAUST GAS

Vwstd = (00000894 ftJ) (Tstd) (Vlc (grams)) gram

Vwstd = (00000894)( v B + 460)( Lf2 - )

Vwstd = ____I_~----q___

Bwo = 100 (Vwstd) (Vwstd + Vmstd)

Bwo = 100 ( middot t 1 ) ( 4 + t S 781 )

Bwo= ------

2

(3) DRY GAS MOLECULAR WEIGHT (MWd)

MWd = (032 x frac3402 ) + (044 x frac34CO2 ) + (028 X (frac34CO + frac34N2 ))

MWd = (032 x 1- 010 ) + (044 x O O 1 ) + (028 x ( O + +I Ci ))

(4) WET GAS MOLECULAR WEIGHT (MWw)

MWw = (MWd) (1 - BWo 100) + 18 ((BWo 100))

MWw = ( -Z 6- B-1) (1--Z -S- 100) + (18 ( z s-( 100))

(5) VELOCITY (Vs)

460Vs = 8549 x CP x ~ x ___Ts_+_- ----=-Ps

(Mw_) X (Bp + 136)

( 0 Ca + 460)vs = 8549 x ( o e- ) x ( 1 o 1 0 ) x 1----------------------

( -Z8- St ) X ( 2 degt ) tdeg + 0 C l )136

Vs= (po 9J

3

(6) AREA OF CIRCULAR STACK (As)

As = (Ds)2

x (31416) 576

( ) 2

X (31416)As=--------------~

576

As= ----

(7) AREA OF A RECTANGULAR STACK (As)

As = (L) (W) 144

As=( le ) ( I e ) I 144

As= -1B-------=--

(8) ACTUAL CUBIC FEET PER MINUTE (ACFM)

ACFM = (Vs) (60) x (As)

ACFM=(ampocil)x(60)x( iri8 )

ACFM =--~_5_0---CS-___

4

(9) ST AND ARD CUBIC FEET PER MINUTE WET (SCFM)

= (ACFM) x Tstd x (Bp) + (Ps136)SCFM Ts 2992

( ( R +460) ( 21+f) + ( 6u ~ I 136))X----=Ua__~X------------=-~--~

( o v +460) 2992

SCFM = --~lte~0_4_gt__

(10) DRY STANDARD CUBIC FEET PER MINUTE (DSCFM)

DSCFM = SCFMx(I - BWo 100)

DSCFM= ( vO-l~ )x(l --z-~ 100)

DSCFM = ___-s_9_S_9__

(11) ISOKINETIC ()

100 x (Ts + 460) x [[(0002669) x (Vic)] +[(Vm) x (Y) (Tm) x [(Pbar) + (Mi) (136)]]]

60 x 0 x Vs x (Ps 136 + Pb) (Dn2 x 0005454)

100 x ( OC + 460) x [[(0002669) ~ (~Z1)] + [(11-ts~ x ( 100( ) ( 8 +460))] x [ltz~1~middot) + ( 2-1136]1)

( ltJO )x( er )x( (o1 )x( 0amp136 +27r)x(0-89 )2 x(0005454)

ISOKINETIC =__9~5_(~-

5

(12) Nickel EMISSIONS

mg Ni DSCM = mg DSCF x 0028317

mg Ni DSCM = ( 1- ~ ) I~ ( 7i8r ) X (0028317)

mg Ni DSCM = -~Cgt--middot0_1_2-_o_e_

1 mg Ni HR= _fL__ x - - x DSCFM EXHAUST x 60

DSCF 1000

mgNiHR= ( Zr o ) x - 1- x(tamp~7 )x(60) ( 7- 7 t Blt ) 1000

mg Ni HR= -ZO bull egt i J

mg Ni Ampere-hour = mg x hr hr Ampere hours

mgNiArnpere-hour= (1-ios~-r)x( 1-IWL) ( deg oo )

mg Ni Ampere-hour= 0 O i l 01J

6

APPENDIX A-2

FIELD DATA AND CALCULATION SHEETS FOR MAY 2 1998 SOURCE TEST



RUNNUMBER 4 5 6 FIELD DATA INPUTS BAROMETRIC PRESSURE (Pb) 2980 2980 2980 RECTANGULAR STACK AREA (SQ FT) 178 178 178 PITOT CORRECTION (Cp) 084 084 084 SQRTDELTAP 0995 1000 1000 STACK TEMP (DEG F) 1090 1110 1100 STATIC PRESSURE (Ps) 060 060 060 VOLUME SAMPLED (Vm) 73635 77044 76974 METER TEMPERATURE (DEG F) 730 840 770 METERGAMMA 1006 1006 1006 DELTA H (INCHES WATER) 114 114 114 LIQUID COLLECTED (VLC) 310 328 404 02 2090 2090 2090 CO2 001 001 001 SAMPLING TIME (MINUTES) 1260 1260 1260 NOZZLE DIAMETER (INCHES) 0188 middot 0188 0188


LABORATORY DATA NICKEL(ug) 34000 22000 14000

FLOW RESULTS VOLUME SAMPLED DSCF 73293 75136 76046 VOLUME SAMPLED DSCM 2075 2128 2153 MOISTURE IN SAMPLE (CF) 146 155 191 MOISTURE () 196 202 245 MOLECULAR WEIGHT (DRY) 2884 2884 2884 MOLECULAR WEIGHT (WED 2863 2862 2857 STACK VELOCITY (FTSEC) 5831 5872 5871 ACTUALCFM 6228 6271 6270 STANDARD CFM 5764 5784 5794 DRY STANDARD CFM 5652 5667 5652

NICKEL RESULTS ISOKINETIC SAMPLING RATE (100plusmn104 955 977 99l

NICKEL (mgDSCM) 001638 001034 000650 NICKEL (mglHR) 157304 99562 62431 NICKEL (mgAMP HOUR) 003608 002224 001352


FIELD DATA

Plant_____-1--Yllt----=-~ Probe Length anc1 Type lt r ( ( Cl] I Date 1 Pitot Tube ID No S 7_

Sampling location_ _z_~~~~--- Nozzle ID No Anc1 Diameter o I J7l Sample Type C ()) Assumed Moisture t---~--------Run Number_____ Meter Dox Number _ __rLA_________ Operator O D Ambient Temperature__~l~J______ Darometric Pressure_~l-=-1-1pgt________

~ Fl Meter Della ll

I_ Factor l Meter Gamma

1

O -1 2 f Static Pressure - o f Heater Dox Sening____-~--------Filter Numbcr(s)___fJ_~_______ Reference Della P ___-=_______

Pretest Leak Rate O CFM reg Read And Record All Data Every

I ) in Hg7 Minutes Schematic or

Traverse Point Layout Post test Leak Rate ltr O

lmpinger Dox No~ CfM middotu in Ilg nlank Dox No ~ 6

I

~ Traverse Sampling c Gas Meter Velocity Orifice Pressure Stack Drv Gas Meter Temp Pump Ileated Filter Impinger n ii n rn z

ii D z rn z 1 r en rn lt 0 m z f)

Point Number

t t J V middotr IA

I 1

J I r lt

Time Time e

(minutes) (24 hr clock) Dmiddot l IO r-

middotL-7 I I I 01 1 iii J ~ J ~ I I 1)

~ ~n lgt l bull1rL - 4

S-1 i _ A I A bullj~ 6tf 1 1 1 J rt -) ) ()-

Reneling Vm

(cubic reel) IVYbullJJO rJ c A-rl( (o I I I -r- middot- o la1J ~ 1 r I

I --o l YII ~ u-v t(

Head Ps

(in H20) 10 010 bull lt I c

I u j bull -

o bulll)Cl7 I bull C

I U 1

Differential (in H20) AH

DesireeI Actual lct - i 1 Ibull 1) l L I I L( bull IL I I( I I ( i 11

1 I I (_ 0 middot i I bull I v

I 0 c I I I L 11middot I I I

I I 4 bull ( lr I I L1 bull fl

I - Lu

Temp Ts (F) lcD

o- 0~

~y oc

0~ middotbull ti -

Io - l6

Inlet Tmin

(F) t middot-t~ ~

- igt o j7r--

--7~-7

Outlet Tm out

(F) 1-

--- y

--t J _q

_ ~ I - Q n L-

Vacuum

(in II~) 7

-l

J )

J

) )

I J

Probe Temp

(F) t-J(

Dox Temp

(F) IA

Temp

ff) __ _ 2

I A

(o i 1

IA - C _ ~

tA) _ L-

C I

I l I

(

I _

I II)-I I _

I ~ (

ltgtl(1

1 _vc 111 ~ l A- bull J ~

iOLbull 0 1upound Ibull 1111 I 0 I~middot CJ

bull J ~ middot__ l - ~ -

l

lt l

I ~ _ tt

I Lbull j I

( lt L

t -lt C ( r

( (

l t IJ

I I CJ I I I

I t I I I

7 J--7 -i -fj - 1-

7 --1l J 7)

_)

1 )

J

v w

CL

(G _J

~lt-I-~

[Jou9 0 w u--~ Di

middot1 ) IJJ I f)I ~

fl V 1 ~

l

Plant

Date

- -bull

1~ 41 Sampling Location ~ tl ---

Sample Type (~ t gt)

Run Number L f) ~ OperatorS Ambient Temperature Darometric Pressure Static Pressure Filter Numbcr(s) Pretest Leak Rate ()

amp J -)_ 5 ~

O C rs--rp

CFM --1) in Ilg Read And Record All Data Every~ Minutes

I Traverse Sampling Clock Gas Meter ~

0 Point Time Time Reading 0 Number B Vm m z (minutes) (24 hr clock) (cubic feet)lt ii 0 A10 11ll1l0 z () J) middotr1 l ) 1 1

m 3 ltI A) 1V middotl l ht 1~ z ~ I ) 1 J l bullbull IJ

V - l ~ 0- )mu j _ ii())- middoti L1 0 lt middott 1 I l--0 1 ti deg I m Y z l OltII Jfl AVU 1)1 ()

I ti _ bull la )-1 A1degt1L -z JY -y~ - It- V

l ) AVVY I ly 1 ~YWv gtl

bull I lO -Al 1 i 7 (J _ X _middot ~ A -~ i u I D07 l

_+ J

i v _ -lI ~ltIIOI - - l

t~ ----

( I ((

FIELD DATA

Probe Length and Type y c l2 c~

~degfmiddotk

Pilot Tube I D No lt- 1 A Nozzle ID No And Diame1er D 1 n J~ Assumed Moisture -Meier Box Number 4( amp Meter Della H

t Factor l L

Meter Gamma o ____I 5 r lleater Box Setting micro_ Reference Della P _____________

Schematic of Post test Leak Ra1e V CFM _O in Ilg Traverse Point Layout lmpinger Dolt No-=1] Blank Dolt No ~

Velocity Orifice Pressure Stack Dry Gas Meler Temp Pump I leated Filler lmpinger Head Differential (in H20) Temp Inlet Outlet Vacuum Probe nox Temp

Ps ~H Ts Tmin Tm out Temp Temp (in I-120) I I

middot1 C

bull I I I

I bull 0 ()

Desired Actual I I I I It

I I I

lh ltLt _L(

I_ v~ I it IIA ~ I f

(F) Ii l

~ I

-J J-middot

tmiddotL t jI

(F) (F) (in II g) (Fl (Fl (F) _ Al~ llh-middot ) (_ ~ r 1 _ - bull C _(t ~ ~lt

IT) middotf() rbullf_ -lt h _7 _

(I) 7lt -~ i bull

f cJ I O lt Ibull f

ft IN I ILI 1J

l bull pound IL

I-I

1 I-

1 -- I

X) J 1 -L-- IJ 1 I

O ll IA middotc1 r _ _- t c

I bull

- d 0

) P ( ampI

I tA I tt I l c--t bull- t4 I t-1

l l-t--J L _ c_c l~

I 1

) -bullt I I

I I I

I -- I

c ) c 1- I ~ Ihl t

) (J I -~ r1 J - I ____ middot

Ibull r (

I () I rl

- -

Idlt- ~ -

f_l Y ~ I~~ flt I y Li1

I 11 J - I

bull I

i L middot middot1 I

r middotmiddotbull

I I

C I IrJ (_

1 I-~ r L bull1f I 0 I~ J I

bull J ( I

_ middot1 1 -

degta Uj MU

I

middot

- -

Plant __ ~

Date 1 Sampling Location ___-f-r-~-=----

Sample Type___f-41tt2f_1~____ Run Number ------~-----Opera10r_______________

Ambient Temperature 4 3 Barometric Pressure 7 pound fQ Static Pressure 6 _ Filler Number(s) NA Pretest Leak Rate O CFM I Cin Hg Read And Record All Data Every L r Minutes

Traverse Sampling Clock Gas Meter Velocity n Point Time Time Reading Head ii Number e Vm Ps rn c z (minutes) (24 hr clock) (cubic feet) (in H20) jj () JJ ll111 0 middot7 l n z JS8 rJ( rV rn I 10- YfO - ldf z bull J ~ J L Ci ) bull ~ Lvll~ r ~ _ 1~ I C ) I l o m D

- 1 L tl l I ~ c ii la JI I( I uv lv

n A I 11 10

m ~

gt z J- t1 _i I I bull (

I IA L -t - ) 1l ~ a - l _ ic 1 r I~ -~ - middot-~ ci bull I -middot A( C I( I 7 ll middotgt _ ( 1hl-

0 )) l I~ Jgtlgt) )( - I I I

gt l yen2- )i -11 I I II 11 yLI 1 I

l ~Q 7l11 i l blH deg111l I i lot gt r Vl l

- I Lgti- 1 --I - I I I

IA I A bull middot1 bulli r - - 1lt1 Ibull i fr ~ I r-

l

I bull1 LI ~ ---- l)o~8Abull ~ I -i - ) ~ gtlt1- - LI - bully DiA

( 7I If I I I - ) I I l I -

FIELD DATA

Probe Length and Type ~ 1

Pitot Tube ID No S -JA---Nozzle ID No Anltl Diameter O lfZL middot~ Assumed Moisture ~ Meter Box Number_____Y__=_t1l-------middot Meter Delta H ) 1

~ Factor I middot I gt

Meter Gamma c_ 5middot JI Heater Box Setting ~ Reference Delta P-------------Post test Leak Rate___Q CFM vin Ilg lmpinger Box No--iJi Blank Box No el

6-t nLt


Orifice Pressure Stack Differential (in H20) Temp

LUI Ts

Drv Gas Meter Temn Pump Ileateltl Filler lmpinger Inlet Outlet Vacuum Probe nox Temp

Tm in Tm out Temp Temp (F) (F) (in Ilg) (Fl (Fl (F)

~ )- middot-i J1- Nbt l--Joi a -lt c0 1 ) r r ti I - ~

It l ~-~

- I ) -c-1-J 1 J(

~

-rt I

1 ---i )I 1 )A

-u rbull-c _ i ~

ryC) -ill bull- lt -lit 7 f

1 5 l1 ~u ~ ~

Desired I [)c

I J tt I ( lt

lltf l l ti( 1

ltLf I 11

bull1 lu

r

111 1 ~

Actual (F) I I ~nbull1 I It

I e- 11 I)

( r ID

1tv llv 10l

I( I L-0

I CA

middot I~ I I VI _t ~~

I I 0 I 11J

1 7

MOISTURE RECOVERY SHEET

PACIFIC ENVIRONlIENTAL SERVICES INC

FACILITY

SOURCE

DATE r2f J

RUN

METHOD

BOX

IMPiiGER CONTE~TS Fm U WTL-L TOTAL bull

I

2

3

4

DI WATER

DJWATER

EMPTY

SILICA GEL

GRA11S GRA1-IS GRJIS

s- J (

_ 0

I 1-- t

3(_o TOTAL GRAMS COLLECTED

INITALS v

MOISTURE RECOERY SHEET PACIFIC ENVIRONlVIENTAL SERVICES INC

FACILITY

SOURCE

DATE rhlrr

RUN

METHOD

BOX rL

IMPINGER CONTENTS

1 DI WATER

7

2

3

DI WATER

EMPTY

4 SILICA GEL

FINAL

GRJIS

foo1

-~OTAL GRAL1S COLLECTED J ) ~

INITIAL

GRAMS

TOTAL

GRMS

I lt -( J t---

S-gt

INTTALS d7

0

MOISTURE RECOVERY SHEET PACIFIC ENVIRON~IENTAL SER-1CES INC

FAC[LITY

SOURCE

DATE

RUN

METHOD

BOX

ll1PINGER COiffElfTS FINAL INITLU

GRltJ~IS GRltMS

I

2

3

4

DI WATER

DI WATER

EMPTY

SILICA GEL

middot irOTAL GRAJvS COLLECTED

INITALS

TOTAL

GR~IS

J)

O-)

r-

~-(

APPENDIX A-3 FIELD DATA AND CALCULATION SHEETS FOR

MAY 29 1998 SOURCE TEST



RUN NUMBER 1 2 3 FIELD DATA INPUTS BAROMETRIC PRESSURE (Pb) 2988 2988 2988 RECTANGULAR STACK AREA (SQ Fr) 178 178 178 PITOT CORRECTION (Cp) 084 084 084 SQRTDELTAP 0990 1050 1050 STACK TEMP (DEG F) 1000 980 970 STATIC PRESSURE (Ps) 070 070 070 VOLUME SAMPLED (Vm) 80668 83075 79107 METER TEMPERATURE (DEG F) 750 770 790 METERGAMMA 0984 0984 0984 DELTA H (INCHES WATER) 127 129 129 LIQUID COLLECTED (VLC) 341 511 224 middot 02 2090 2090 2090 CO2 001 001 001 SAMPLING TIME (MINUTES) 1260 1260 1260 NOZZLE DIAMETER (INCHES) 0187 0187 0187



FLOW RESULTS VOLUME SAMPLED ~SCF 78478 80523 76392 VOLUME SAMPLED DSCM 2222 2280 2163 MOISTURE IN SAMPLE (CF) 161 241 106 MOISTURE () 201 291 137 MOLECULAR WEIGHT (DRY) 2884 2884 2884 MOLECULAR WEIGHT (WET) 2862 2852 2869 STACK VELOCITY (FTSEC) 5748 6096 6073 ACTUALCFM 6139 6511 6486 STANDARD CFM 5790 6163 6150 DRY STANDARD CFM 5674 5984 6066

NICKEL RESULTS ISOKINETIC SAMPLING RATE (100oplusmnlOo) 1024 997 933

NICKEL (mgDSCM) 003240 000325 000647 NICKEL (mgHR) 312339 32993 66705


- -

FIELD DATA

Plant ~--- - bull~middot bull Probe Length and Type 3 - 6 v---f

Date ~ () ~ f 9

t Pilot Tube ID No Nozzle ID No An_d_D_i-an-e-e-r--e-c--[-)-~=-Sampling Location__middot 2 --]

Sample Type (~ c) 7 Assumed Moisture -Meter Box Number --1-f_____Run Number j 7

Operator ( 6( rh Meter Delta H v bull f j-f

Ambient Tcmperature __J--0----- KFactor___---JCO----------llarometric Pressure ii 7bull fl Meter Gamma D 1fl Static Pressure O 1 Cl Heater Box Setting -middot-----------

Reference Delta P -Filter Numbcr(s) -- ------------=---Pretest Leak Rate--Q--C-F-bullM___1_l)___i-n-l-1g- Schematic of Po s l test Leak Rate 2CFM reg ~ in Hg ----- - ---- ------ - - --- - -- -middot -- Minutes Traverse P_oint Layout lmpinger Box No J p Dlank Box NoI I Traverse Sampling Clock Gas Meter Velocity Orifice Pressure Stack Dry Gas Meter Temp Pump llcatcd Filler lmpinger

0 Point Time Time Reading Head Differential (in H20) Temp Inlet Outlet Vacuum Probe Dax Temp Number a Vm Ps 6H Ts Tmin Tm out Temp Temp

(minutes) (24 hr clock) (cubic feet) (in H20) Desired Actual (F) (F) (F) (in H11) (F) (F) (F)

ft cI A UV 9 -5 l ) 1 i I L I bull I i DJ 1 middotJ 1 Jmiddot Altl - 1cJ

-middotbull 1 1 tl o lt ~I) I~ Amiddotu- bull 1-t) I) ) middot1 ~ 71 u V( l An

1 u bl lll J 0 ) rY -f) ) t- v I I

J I ) gt ) V middot1-0 ) pound- - 1o 1 ~~ middotJ middot1 l I -lt

I t ) J 1 ~ middotu gt 0 bull J lb J I (J middot]_ middot-ir ) l I J- Igt I- ) I - tI I C( ~-li i 7~o J J 0 J~) middot1 ~ I ) r ) gt l 7-)

lfJ D 1 H I

~ r -1 l l I [) ) J_JIC ~ I INl ) - ( I~()

) l I IV i-lt middot ) 1 - 0~ ) Y -11

bull) IL ~ l WfltI I - - I

1 J i -lt) t _) 1 - I I ~ 1 gt ( l I - c ~ - h- I I L-

1) _r- J T )t ( bull bull t ~ 7J ) i ( middotta __ IA )J- h )-llV Ii l 1 v _ ) d f middot bull) L ( I lt

vi- 1l bull~Llf1 -- I

( I r 1 ) i) middot) tmiddot) c )) I bull tJf) I J bull I 1 r V - - I ii ~ l I bulll ) ~ 1 I _11 _ I - f middot1

1 ( hLlV I I Cl Jb f1 l 1 1 l 1 1 -f 11 1 ( middot r t) IL )_J bullj r ~1 -l~G -

if - - 1Y middott I Cj 0 )6 1 ri r ) F l _ ( 0( 1r_ -middotr I ) - JI 0 _ jbull) Jf y 1 ) middot lJ ~ ~ II~ 7v r middot V l i 11 _ __r1 ti) 7-lt- In I_ 1- f111

_ I 11 - yen c-Y - _ - ~

- -to-1i 5 6 deg1

__ __________ _

Plant____L-1---LPa~--Datc-----~-+--+----+-L-+-~---S amp Iin g Location ____1-=--=---

Samplc Type ___~~~-l-J-J___

Run Number ____c= _ _______

Operator______-r-+--+---LL---Ambient Temperature __-----ltil----U-

Barometric Pressure _____-4--+---____

I

Static Pressure c ) Filter Number(s) -Pretest Leak Rate O CFM [ Co jn Ilg Read And Record All Data Everv --i M inut

I j Traverse Sampling Clock 0 Point Time Time fi Number 0 rn z (minutes) (24 hr clock) ii lt

A ( I l I c ~bullu no D L1 I 0 z - l J J ~ J J r t- lt l-~ rn

~ l ~ l lol X o

z ( 1 I l i I middot3 Ol) ~- )~

r 1) 1 ~ f t -~ middoti X fOY r rn 0ll IA l middoti- b ~y - ) J - I lt fi 7v ~ rt-- gtI 1-L--rn I1) C I r- 1 j-) I I z _ middot7 uVuu v- l - 0 ) It lgtV V1 -JIlt ~

~~-I j1 vbull- ~JI

- ii _ middotvoP ~ - )

_ 1 - t y J I middott -- l ) II 1 J - )ill_ Y

~ I middot l 4~ n~ r I C- - -ull ) o I f-i

) IU ~)V fu middotmiddot1 T-Z1 I C t 1 I r middot-1 ) I r

J f ~ i-~ U I LI iC 7 middot- lmiddot1-( ~-l_

I I c Iv I l 1-1 11 -

v-1 Dll - ~

Gas Meter Velocity Reading Head

Vm Ps (cubic feet) (in 1120)

FIELD DATA

Probe Length and Type J J-le-Pitot Tube lD Nomiddot--------~--Nozzle ID No And Diameter 6 1 ( J Assumed Moisture ~ Meter Box Number___ _jmiddot~-----

Meter Delta H 1=1-rt C Factor I L_ lt-Meter Gamma b smiddot r

Heater Box Setting bull-

Reference Delta r -Post test Leak Ra-e--Q--C-f--M---~~-in--1-lg

lmpinler Box No cent Blank Box No- -~

Schematic of T Point La


0H Desired Actual I bCn bull I Ibull) I i l t~ I )middot1 - l Ir I J ( ) l r~ )

Stack Temp

Ts (F) ti( I 11

lt j

(

I

Dry Gas Meler Temp Inlet Outlet

Tm in Tm out (F) (F)

bull1 l ~ t h bull( i )4 r ) -7 bull y 1 -

Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(

~ f Llt -vi l bull J

bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l

clb t bull J middot1 lb middotJ

I IP I 7

I Lfo )

I) P ) middot1 I f ~ ~ )

t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~

l i middotmiddot1 (- ) --1 ~ v 1 _

- I (() -J~

c f --- -

I

) clbull

I _ j bull ( bull j_

1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA

Probe Length and Type ~ ( amp(~Plant I u - f J) ~s Pilot Tube ID No___________Date r

Nozzle ID No And Diameter () I tu-Sample Type rJr+t LP) ~ Sampling Location ~Z =

Assumed Moisture Run Number J Meter Dox Number J _ Operator Di [ JY Meter Della H Ambient Temperature bull ~ 5i t C Factor J) b Darometric Pressure f Meler Gamma loz 2y Static Pressure 7= t 7 Heater Dox Selling ____- _______

Filter Number(s) - _- Reference Della P _____________

Pretest Leak Rate () CFM J in Ilg Schematic of Post lest Leak Rate _Q__ CFMreg-J1 in Hg Read And Record All Data Every--- Minutes Traverse Point Layout lmpinger Dox No A--- Dlank Dox No___

Traverse Sampling Clock Gas Meler Velocity Orifice Pressure Stack Dry Gas Meler Temp Pump Healed Filler Impingerl 0 ii Point Time Time Reading Head Differential (in 1120) Temp Inlet Outlet Vacuum Probe 0ox Temp 0 Number a Vm Ps LiH Ts Tmin Tm out Temp Temp m

(minutes) (24 hr clock) (cubic feet) (in 1-120) Desired Actual (F) (F) (F) (in HR) ( ) (E~ (F) ( n11middot -i bull r middot1 JXI I n1 bull f rl ) 1 I II II t7 CJ~

I ~ ~ - 11 v_ I _ L- ( l

-J n--- middot1 A ltJ f -J I

(1 ) l 41 -l ~- ) 1 bull bull _ 5 v- I_ t ~ rl _-- Abull vr - bull I I bull vc JI ri ~l bull lt I 1~ -lt) l )1- J I I 11 l t f

-u _ _f) JlJut- _

r

1 ~t-iri Uf 1 -_ ) J I lfJ I -

- L V

i- _ n1 r- I iPfbull -7r t 1-l - sv C n I I) - h 1 I I OLJ D ~ bull 0 middot L-

j l i middot I ( A 4t middot II _ I 1 V 1l I t I t ) l bull t I A( 1middotmiddot-- 0_ _ ) -er71iA IA (If bull ( - ~ 2- - A I l D _- middot I tl 1- bull Vj I l A r- 7_bull I - I ti _- lt- _ - - gt ~ lC III v I fo J1 r LA l bull J -

- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I

t1 l ampr--gtrn middot i) I bull Jl Igt itv - - I - t - ) bull IL ltf- - I oo I gt lil --1 - I y I 1 l ) I - I J xc- IA I i-middot ffil I I 1 iJ bull l Ill middot ) - -c middot1 lo

-middot I ( - n-- I I I vt I bull gt 1middot i10 11 (p ~I copyI I fv - ) V

-middot [I -

~--VI _ II r Ill ~ bull _ bull I - - - I

MOISTURE RECOVERY SHEET PACIFIC ENVIR0NlVIENTAL SERVICES INC

FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS

I 0 middot I 1J fi1J03 r10n -=t583 (ll

2 0 I li 1-fJOi -_ rJ lt amp524 $ 3 EMPTY F1b 51~ -z r 4 SILICA GEL F6Y ~ 81 ( l r~

lroTAL GRAMs COLLECTED

INITALS

llOISTURE RECOVERY SHEET PACIFIC ENVIRONNIENTAL SERVICES INC

FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS

ltS23 ~ J 7a-~qmiddotlto-z

SICi

80 =

J middot7

l 1 r

lroTAL GRAMS COLLECTED sl-l

INITALS a 7

lIOISTURE RECOVERY SHEET PACIFIC ENVIRONNIENTAL SERVICES INC

FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN

METHOD lfrh k) BOX Camp

IiYIPINGER CONTENTS FINAL

GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S

I oi ti ~NO amp17 c b-11 O o 7 2 o~ 1-1 IJ o~ ---r 7_ t

- G0~ 2 o 6J3 EivPTY pound r r - 5~3-

4 SILICA GEL 71f r ~H5 le ti

lrorAL GRAMS COLLECTED I~ Y

INITALS f7

APPENDIX B-1

LABORATORY DATA FOR APRIL 30 AND MAY 2 1998 SOURCE TESTS

21

IICIS WEST COAST ANALYTICAL SERVICE INC -11lt1h tial Clio11isrs

May 12 1998

PACIFIC ENVIRONMENTAL SERVICES 13100 Brooks Drive suite 100 Baldwin Park CA 91706

Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT

Samples Received Seven (7) Liquids Date Received 050498 Purchase Order No 102-98-0105B

The samples were analyzed as follows

Analysis

Nickel and Chromium by ICPMS 2

(frac34~gt1~iCharles JacksUh~middot G Sha MS Senior Staff Chemist Senior Chemist

This report is to be reproduced in its entirety of 2

9840 Albunis Avenue bull Santa Fe Springs CA 90670 bull 562bull948bull2225 bull FAX 562bull948bull5850 bull httpwwwwcaslabcom

WEST COAST ANALYTICAL SERVICE INC

PACIFIC ENVIRONMENTAL SERVICES Job No 38042 Attn Dennis Becvar May 12 1998

LABORATORY REPORT

Nickel and Chromium Quantitative Analysis Report

Inductively Coupled Plasma-Mass Spectrometry

Sample ID

Run 1 Run 2 Run 3 Run 4 Run 5 Run 6 Blank

Detection Limit

Date Analyzed

Sample Run 3 Matrix Impinger

Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed

Nickel Chromium Volume Nickel Chromium yg ygY9Ll Y9Ll ill

78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98

Quality Control summary

Parts Per Billion (ug1)

5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110

This report is to be reproduced in its entirety Page 2 of 2

Abbreviations Summary

General Reporting Abbreviations

B Blank - Indicates that the compound was found in both the sample and the blank The sample value is reported without blank subtraction If the sample value is less than lOX the blank value times the sample dilution factor the compound may be present as a laboratory contaminant

D Indicates that the sample was diluted and consequently the surrogates were too dilute to accurately measure

DL Detection Limit - Is the minimum value which we believe can be detected in the sample with a high degree of confidence taking into account dilution factors and interferences The reported detection limits are equal to or greater than Method Detection Limits (MDL) to allow for day to day and instrument to instrument variations in sensitivity

J Indicates that the value is an estimate

ND Not Detected - Indicates that the compound was not found in the sample at or above the detection limit

ppm Parts per million (billion) in liquids is usually equivalent ppb to mg1 (ug1) or in solids to mgk~ (ugkg) In the gas

phase it is equivalent to ul1 (ulm )

TR Trace - Indicates that the compound was observed at a value less than our normal reported Detection Limit (DL) but we feel its presence may be important to you These values are subject to large errors and low degrees of confidence

kg kilogram mg milligram 1 liter m meter g gram ug microgram ul microliter

QC Abbreviations

Control QC Limits are determined from historical data The test amp value must be within the Control Limits for the test

Warning to be considered valid Based on historical data Limits the confidence intervals are 95 for warning limits and

99 for control limits

Error Percent Error - This is a measure of accuracy based on the analysis of a Laboratory Control Standard (LCS) An LCS is a reference sample of known value such as an NIST Standard Reference Material (SRM) The Error is expressed in percent as the difference between the known value and the experimental value divided by the known value The LCS may simply be a solution based standard which confirms calibration (ICV or CCV - initial or continuing calibration verification) or it may be a reference sample taken through preparation and analysis

CHAIN OF CU JDV RECORD

COMPAN )1 m~--1 --pfio~ECT MM-JAGER -~gtM 6c 1t~bull middot WEST COAST ANALYTICAL SERVICE INC ADD bull PROJECT NAME RgtJJ___Lt~bullmiddotbullmiddot 9840 Alburtis Avenue ---LL~c------~+--~c=----~~=frl--7-f PROJECT NO ~2 middot ()0 Santa Fe Springs CA 90670 PHON ~lllt~UCt ~~-IM-it=--~rc PURCHASE ORDER NO _________ (310) 948-2225 Fax (310) 948-5850 MAIL REP

COMMENTS

J~ ~ 1frac14~ ~h tv-d ck--frrr1--~ Nl

~

If samplemiddot Is liquid amp has sediment or If sample Is multi-phased should we particulate should we test each phase separately ___bull middot test middotw(rate only test onlymiddot ONE phase Which phase ___ mix sample by shaking mix all phases by shaking if possible

test particulate only

---~ Sample 10 I ~ J Remarks

t~lv f( k-~

R~ )

1- Vo R- )~ ~-amp 1gt I flltmiddot 1t V

A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v

RellT~( fi-- Rellnl(ulahed by

Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company

NOTE Samples are discarded 30 days after date of final report

U I I I I I I I I C-

U I I I I I I I I L Ll_~bull-

I

Date1(gt8 ~r Rcelved by middotR - (( 9rtbullJV=-gtJamp(_ C~ l) C~ I i

Daletflme I Received by -)

OateTlme Received by rmiddot

While Copymiddot WCAS bull Yellow - Aepo1 bull Pink Clienl

-j 1 7 11 I_y

y I f (

f l-1 I Y f I f I f f I ti f r I f I Y

Company Af-C DaefTJme

fSJLJlJ IQmiddot (01m Company DateTime

Company DateTime

WCAS Job No N1 R n 42 0

APPENDIX B-2

LABORATORY DATA FOR MAY 29 1998 SOURCE TEST

22

wms WEST COAST ANALYTICAL SERVICE INC A11t1h ri ti C1imiddot111irs

June 10 1 1998

PACIFIC ENVIRONMENTAL SERVICES 13100 Brooks Drive Suite 100 Baldwin Park CA 91706

Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT

Samples Received Eight (8) Liquids Date Received 052998 Purchase Order No 102-98-01058


Analysis

Chromium and Nickel by ICPMS 2 - 3

a~JCH Charles Jac7~D Senior Staff Chemist

PhD


9840 Alburtis Avenue bull Santa Fe Springs CA 90670 bull 562bull948bull2225 bull FAX 562bull948bull5850 bull httpwwwwcaslabcom


PACIFIC ENVIRONMENTAL SERVICES Job No 38288 Attn Dennis Becvar June 10 1998

LABORATORY REPORT

Chromium and Nickel Quantitative Analysis Report


Chromium Nickel Impinger Chromium Nickel Sample ID (ug 1) (ug1) ill lY9J lY9J

Blank Field ND 21 006 NDlt006 OlJ

Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14

Detection Limit 1 01

Date Analyzed 6-5-98


Sample Foss Run 2 Matrix Impinger


Chromium Nickel

Sample 41 183 Duplicate 39 179

Average 4 181 Sample RPO 50 22

Spike Cone 100 100

MS Result 102 110 Recovery 98 919


This report is to be reproduced in its entirety Page 2 of J



LABORATORY REPORT

Nickel Quantitative Analysis Report


Total micrograms per Filter

Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001


Quality Control Summary

Sample Batch QC Matrix Filter


Nickel

Sample ND

Spike Cone 10

MS Result 96 Recovery 96

MSD Result 97 Recovery 97

Spike RPD 10










ppm Parts per million (billion) in liquids is usually equivalent ppb to mg1 (ug1) or in solids to mgkj (ugkg) In the gas

phase it is equivalent to _ul1 (ulm )

TR Tracemiddot- Indicates that the compound was observed at a value less than our normal reported Detection Limit (DL) but we feel its presence may be important to you These values are subject to large errors and low degrees of confidence

kg kilogram mg milligram l liter m meter g gram ug microgram ul microliter

QC Abbreviations





CHAIN OF CUSTODY RECORD

PROJECT MANAGER Atl-shyPROJECT NAME ~~ PROJECT NO r~~-----r-+-=4--+----

PURCHASE ORDER NO _________

WEST COllST llNllLYTICllL SERVICE INC middot9840 lllburlis llvenue Santa Fe Springs Cll 90670 (310) 948-2225 Fax (310) 948-5850

If sample is liquid amp has sediment or If sample is multi-phased should we COMMENTS particulate should we test each phase separately ___ test filtrate only test only ONE phase Which phase Ykk - P~c4-J~v

mix sample by shaking mix all phases by shaking if possible SfL-L test particulate only

I I I I I I I I I I I I I I I I I I I I I I I I MIiTRiX

~

iiiQ 1f o J4II ~ i ~--~middottimiddot ff~ i l -Il ipound ~--$ j-$ - if 1- ifl middott J

I

I

(

Sample ID I

I (~~~ -r_ I middots

1-

1 1 I r--i JIL J )

I

JJ Ft4

bullo-o middotk S O ~J~ii_i 0 (tl-Jcsf~cJJtffocJlcJ 1 tf Rem1rk1~ ttt4i t

f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II

Relinquished bll ------ Co~ 0tfrac34J il_elved byl 1 l _--NA co~VVCA~ ~a ~e ~middotrx

Rellnqul1hed by C6mpany OateTline Received by u Company Dlilefllo e

Rollnqulohed by Company DateTlme Reoelved by Company DalefTlme

fn

NOTE Samples are discarded 30 days after date of final report Whllo Copymiddot WCAS bull VtiNOw bull Aepof1 bull Pink middot Client WCASJob No 11 J ) 8 - 8 8

APPENDIX B-3

LABORATORY DATA FOR WORKPLACE AIR MONITORING

VEST COAST ANALYTICAL SERVICE INC riil cmiddoti11r

May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT

Samples Received Date Received Purchase Order No Project No

Nine (9) Filter Samples 050498 102-98-0lOSB 3278003


Analysis Page

Nickel by ICPMS 2

~~t~UctlCharles JacV~DshySenior Staff Chemist


9840 Albunis Avenue bull Sama Fe Springs CA 90670 bull 562bull948middot2225 bull FAX 562middot948bull5850 bull httpwwwwcaslabcom



LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00



Client PACIFIC ENVIRONMENTAL SERVICES Job Number 38288

Nickel Quantitative Jnalysis Report

Inductively Coupled Plasma-Maas Spectrometry

Total microgramQ per Filter

sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit



iample Batch QC Matrix Filter

Total micrograms per Flter

Nickel

sample ND

Spike Cone 10

MS Result 96 t Recovery 96


Spike RPO 10


8660 Nnc OS8S-8t6-0Ipoundar








ppm Parts per million (billion) in liquids is usually equivalent ppb to mg1 (ug1) or in solids to mgki (ugkg) In the gas


TR Trace - Indicates that the compound was observed at a value less than our-normal reported Detection Limit (DL) but we feel its presence may be important to you These values are subject to large errors and low degrees of confidence


QC Abbreviations

Control QC Limits are determined from historical data The test amp value must be within the control Limits for the test




lJ CHAIN OF CU JDY RECORD

p MAIL RE

PROJECT MANAGER PROJECT NAME PROtlECTNO PURCHASE ORDER NO _________

WEST COllST llNllLYTICllL SERVICE INC 9840 lllburlis llvenue Santa Fe Springs Cll 90670 (310) 948-2225 Fax (310) 948-5850

-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q

If sample is liquid amp has sediment or If sample is multi-phased should w~ particulate should we test each phase separately ___ test filtrate only test only ONE phase Which phase ___ mix sample by shaking mix all phases by shaking if possible ___ test particulate only

I lt- AY q_ I ) --l ~

Ar- tl6JJDO~ SemplelD

J ~ I

~ 2-- -

1i J bull

I(

A~ l ItI tI--- - Fgt - ft(-

l_~~--bull

Relllll_uullsshh~y 0 J1lt- lJL Rellnqulahed by

Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company

lipoundJ Oatejlme lJbulllved by _ ----~)

ltvqf_ (J()Ll)_cfwJlA L ComR~JJ(y-b DateTime

~1ltiltt_ lDbulllD Company OalJrthte- V I Received by Company DateTime

Company OeleT I Rec d by Company DateTime

----middot- _NOTE Samples are discarded 30 days alter dale of linal repon bullmiddotmiddotmiddot WCAS Job No -11lh--~~~1038041

APPENDIXC

COPY OF THE PERMIT TO OPERATE

ft 3109458262 P02 _

I

I I

SOUTH COAST AIR OUAUTY MANAGEMENT DISTRICT 211l651ast Copley Drive Diamond Bar CA 91765

PERMIT TO OPERATE PfflN Nn nfl111

7ur 1idt _t 1tt111H --ANNUALlYIIIIG q ~II~ orchonamiddot If lhbull ~for ONIWll lffleMdlfu (lfJlle 11f) ti flOt ~ l1y 1114 apirotiD ~ COlllact tJt Dim

AN ZOlol14

a

Paa I

LeplOwncr or Opctator POSS PLATING CO INC

81~SlCURA WAY SANTA 118 SlIUNGS CA JU670 ATTN CAROL~

Eqwpmcnl localed al li110 S~CURA WAY SAtllA FE SPRJNOS CA 90610-2ljg

~~Deampaipcioa I NICKEL PIATING UNE CONSISTING OP I 1 NICICELPLATING TANK Nobull 12-0 LX6-9W X5-3 H 237((XX) BTUHR GAS mjTED

WITH A 72 KVA REC 1IFIER

i NICICEL PIATING TANK No~12-0 L X4-0 W X 5-3 H 2376000 BTIJHR GAS~~ wrrH A 72 KV A RrC fiPiER

l NICKEL PIATING TANK No 1 12-0 L X4-0 W X 5middot3 H 237(i(XX) BTUHR GAS ~TED WlIH A 72 KVA RECIIPlR

4 NICXEL PLA11NG TANK No 2 rzq L X8-0 W X 5-3 H 2376000 BTUHR GAll ~TED NlIH A 72 KVA RiCI1riEk I

I s DE-SMtmER TANK No 6 12-0 L X3-0 W X S-3 H UNHEATED middot

6 METAL SURFACE aEANING TANK No 8 12-0 L X3-5 w x5-3middot H 2376000 sruk GAS HEATED WITH A 18 KVA K~l11lllR

7 DE-SMUITER TANK No 10 12-0 L X3-6bull W X SmiddotJ H UNliEATED I

8 METALSURPACEaEAJIIING TANXNo12 12-0 lX3-6 W X 5-3 H 2376000 BTUJ1m GAS HATED

9 METALSURPACE ClEANING TANK No14 12-0 L X3middot6 W X 5middot3 H 2376000 BTIJ~ OAS HHATED

10 METAL SURFACE CLEANING TANK No u l2(f L XJ-6 w x f-3 H 2376000 eruhtR GAS HEATED

I

11 METAL SURFACE CUANING TANK No18 12-0 LX30- W X 5bull3middot H UNHEATED

12 TRl-ltHROME PLATING TANK No 22 12-0 L X4-0 W X 5bull3bull H 2376000 BTUHR G l~ HEATC wrrH A 96 ICVA RlCtiPIElL iI

I

13 ASSOClATED RJNSETANKS j I IORIGINAL I

I i i

fr 3109458262 P03 I

SOUTH COAST AIR QUALITY MANAGEMENT DISTRICT 1865 East Copley Drive Diamond Sar CA o rn~

PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I

CON1TNUA110N OF PlRJUTTO OPERATE

Conditiom

1 OPERATION OF THIS EQUIPMENT SHAU BE CONDUCTED IN COMPLIANCE wriH AU lJA1~ AND SPECIFICATIONS SUBMITTEIgt WTnl THE APlLICATION UNDlR Wilpi THIS PERMIT IS ISSUED UNLESS OTHERWJSB NOTED ISaQW

I

2 1HJS EQUIPME(I SHALL BE PROPERLY MAINTAINED AND KEPT IN GOOD OP~TING

3

C-ONDmON AT ALL TIMBS

THE POUOWING TANX(S) SHAU NOT BE HEATED

DE-$MUITBR TANK NO 6 DampSMU1Tlll TANIC NO 10 METALSORFACe ~ TANK NO JA

NOTICE

IN ACCORDANCE WlTH RULE 206 THIS PIDlMIT TO OPERATE OR COPY SHALL BE JSTED UN OR wmmr 8 MEIERS OF THE EQUJlMEITT

i

THIS PEJUampT DOES NOT AUIllORIZE THE EMISSION OF AIR COlffAMINANTS 1N EX~middotOF THOSE AllOWED UY DIVISION Zb OP nm HEALTH AND SAlY CODe OP nm STA OP CAUFORNIA OR 11m RU~ QFTHEAIR (JUALlTY MANAGEMENT DISTRICT THlS IT CANNOT BE CONSIDERED tS PERMISSION TO VIOLATI 100STING LAWS ORDINAN RJOVlATIONS OR STAltna OF OTHER GOVERNMENI AGENCIEs

BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD

EQUIPMENT CALIBRATION DATA

DRY GAS METER AND ORIFICE CALIBRATION

Dry Gas Meter No 8804737 Meter Box No BA Reference Dry Gas Meter No 25507 IRockwelll

Barometric Pressure 2977 Calibration Date 41798 Calibration Performed By J Rubio

0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l

Orifice Initial final Reference lnlllal Final Test Temperature Run

Time

Flow

Rate

Meier

Gamma

Dell H l

Manometer Reference Reference Gas DGM DGM DGM Reference DGM DGM DGM

Soiling DGM DGM Volume Reading Ra ~lng Volume DGM Inlet Outlet Average

Reading Reading

HbullH20 Vbullft3 v-13 Vr-ft3 Vbulllt3 Vbulllt3 Vdbulllt3 trbullF lbullf lbullf Id minutes Obullcfm

06 295775 307037 1 t262 365878 378970 middotmiddotbull__middot _middot 11292bull 71 76 71

73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781

20 318863 329065 10202 388808 399014 bull io209bullbullmiddot 73 88 77 82 130 077 t011 1814

40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II


Dry Gas Meter No 6846739 Matar Box No 3A Reference Dry Gas Matar No 25507 (Rockwell

Barometric Praampsura 2980 Calibration Data 4115198 C alibratlon Performed By JRubio

0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference

Volume I R dlng ( Reeding I Volume I OGM

Vrbullfl3 I Vbullft3 I Vbulll13 I Vdbullfl3 I trbullF

1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM

Inlet Outlet Average

tbullF lbullF td minutea

71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII

GLASS NOZZLE CALIBRATIONS CALIBRATED BY Joe Rubio DATE 121897

NOZZLE ID READING (INCHES) AVG DIA

1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration

Plant Foss Plating Source Exhaust Method GARB 433

A C

B

A= 01880 B = 01890 C = 01840

Average = 01870

Pacific Environmental Services Inc

-------------------------------- sect18~

_

PACIFIC ENVIRONMENTAL SERVICES INC -------------J

Pitot Tube Calibration Data Sheet

Calibrated by

Date

S -51 (TU~ ~ w~if-0 TC )Pitot Tube ID ---13 (a ( lt1_ l_I)Effective Length _____=--___l-T____________

Pitot Tube Assembly Level ~Yes 0 No

Pitot Tube Openings Damaged 0 No

If Yes Exela in 4 f ~ h oQI c nJtlu a-J-- o L 11 -w-J_ - 1 LL - U I 1 0 7 l ---

N-W-JjVkul - 0 (_

zf bull ( lt10deg) 0 ( lt100)al = a2 = 0 p 0(lt10deg)P1 = fl2 0(lt10deg) -~ It

0 0 0 9131Y = if e = A=

f5_Z = A sin Y = cm (in) 032 cm (lt11 in)

W = A sin 8 r= cm (in) ooa cm (lt1n in)

PA= O dtJ cm (in)

0 middot4 (]Pe = cm (in) 0 1c-D1 = cm (in)

Comments

L-R- ~ Jv

Calibration Required 0 Yes ifNo

____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To

o fAc1Rt OJmicro~~mz_ Date 6 I 2--1 ~B ~

I

e ~ Total pages middot3 (mcudini cover pagJ) I

This message is intended only for the use of the person or entity to wbicb ii is addressed and 111ampy contain information

lt

I

that is privileged and confidential Ifthe reader ofthis message is aol tho intended recipient you are hereby aotiiied that Idissemination or distnbution ofthis infcnnation to other than the iDtcoded recipient is suialy prohlbiled IIfyou received this in error please notify us immediately by phone can aod return this message to me by us postal service I

Thank you Please deliver immediately to the proper recipient J I

1) essage

-lt

_

) t

~ 6929 E Slausoa Ave Los Angeles Ca 90040

Phoae 213 722 8810 Fax 213 888 1493

- ATLAS TEsTlliGIABORAToRIESrnc I

Facsimile Coversheet I

I itJ Q-4frac34)OJAIJ From I

i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t

w ~ bull ~ qtJus transmission Is unclear Pteau adlseATUS TESTING UBORATORIES INC

F-

FRl1 TO 16268140820 P03JAI~ IC)lllIU IJ0Vrv1VlI- __

6929 EAST SLAUSON AVENUE LOS ANGELES CA 90040

(213) 722--6810 FAX (213) 888-1493

CERT DATE f)S middot 13 middotfK

bull~100 B~obli- i)1ve too RECERT DATE OI middot 13 bull 1 t

5AIJ0

lV d- CA 17Camp

C~tli~M(i)11 kcrcJ Arbull PAGE_2_oF ~ Foss tA-tvb Jlltli) Ssv1 J4 41~ CERTIFICATION Ju~ ff ~~~ (1-~

This is to certify Ampere-Hour Meters at he abOve plant were checked on lhe above date witll recorded data provided below This certification was accomptiShed by comparison to the following meter which was certified as Indicated and is traceable to NIST

FLUKE DMM SIN 636302n

ho ff 2

S-t tG 7

DATE CERTIFIED I I middot o 4 middot Ci S

1 l 0

24amp 110

In accordance with ISO 10012-1 ANSI 2540-1

FOR INFORMATION ONLY

AlUSTUTNv8QAA11lle NC san llltIS IIEPORT ASlltECCIN~UHTW PIOlilrTY 0FOL cueT~R1QHl3-~ 1ampgt101NG Q11 WAmi14 APPIOVN (lN0 ne MAY ~y IE _OOUCS) JIJUJ AS APltOIETICN OF OUII CllampNT AgtCl OURSampVE5

CIIJlSl0I CAUIIIAlICN aucs CZ)

TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02

ATLAS TESTING LABORATORIES INC 6929 EAST SLAUSON AVENUE

LOS ANGELES CA 90040 (213) 722-8810 FAX (213) 888-1493

I I

I CERT DATE Ofmiddot 13 -cg

RECERT CATE OJ middot 13 middot IK

BleW i f- (I cA crr1camp ATL i I ll lt-l [1

c~lll-reuroNT Loe+-~~ A-T PAGE__ OF h_ Jv JJhk9 I I

l 3tC ~w4- iA1 7 CERTIFICATION

Jfv 7f- ~ S-f111()J c ~A This is to cellify that the following ammeters and voltmeters at the above plant were certffled on he above (tale to be within manufacturers specifications of t 2 of fllD scale by comparison with the Atlas Testing Laboratories meters shown below The Atlas Test Lab meters were in tum certified as indicated Dy Accurate Calibration

CALIBRATION INSTRUMENTS CERT DATE

SimpsQn Voltmeter middotSIN A2244 l

Simpson Voltmeter SIN 3218

1 -10middot Extecl( Clamp-On DMM SIN WA26804 i i Fluke~M SIN 68630277

I I

METERSSURVEYEOC lbullAPPROVED

TANK~OR POWER SOURCS AMMETJR VOLTMETER

I i ~

Ii

bull

In accordance wih ISO 10012-1 ANSI 2540-1

ATtgtS TSSTINC __rOAlliS INC ~TSMS _AT A3 nEcl__Pll~Ol Olfl CUINl~CHAIGHTS AU11amp5ER1iI llNl)IHO OUR 111iN-V-CND- CNY lli~EigtROOICliC N lUL)ASA PAOTECTICN Qjl 01itQeltr NIIJOURSlveS

OUYSl0amp CAUIAATIOlt FltlAM5 (1)



CERT DATE 05 middot 13 -~g

RECERT DATE 03 middot 13 middot ilr

Bl cw i rolt K- cA cgti neamp ATL l I llYF1

euro4ur~~CIV Lou4--e-r A-7 i PAGE__ OF _1-__

lo IJfrac34~~ (v_4 7 CERTlF1CAT10N J1v Pr Fr ~1-tvoI cf ~c

This is to certify that the following ammeters and voltmeters at the above plant were certified on the above date to be within manufacturers specifications ofplusmn 2 of full scale by comparison with the Atlas Testing Laboratories meters shown below The Atlas Test Lab meters were in tum certified as indicated by Accurate Calibration

middot CALIBRATION INSTRUMENTS CERT DATE NIST

Simpson Voltmeter SIN A2244


Extech Clamp-On DMM SIN WA26804 1 (0middot

Fiuke DMM SN 68630277 1-5JOl11

METERS SURVEYED I l = APPROVED

TANK OR POWER SOURCE AMMETER VOLTMETER

R-ei ~ I

Rec~ 2


ATJ-S TESTING 1A8CRATOA1ES INC SUBMITS TMIS REPORT AS TME CCNFfCEr-tTIAl pqcP~TY CF OUR OENT REROOUCTICN RICt-4TS ARE RESERVED PENCING CUA WRITTEN APPrtOv Al (ANO TMEN MAY ONLY ee rtEROCUCpound0 IN F1JUJ AS A PROTECTJCN OF OUR CLIENT N40 OUAsaves

OUTSIOE CLlBRATION FORMS [1)

ATLAS TESTING LABORATORIES INC


(213) 722-8810 FM (213) 888-1493

CERi DATE OSmiddot 13 middotJg

l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE

)_J__w t1x ( CA 917camp ATL _f1__l_1-=81__

C~~1-GV- k~rc7 Ar ~ PAGE__2_ OF ]_Foss Pt A-1AIb Ji0 kv ul4y CERTIFICATION

5~7J- M ~raquo6~ 7~ 9q5-v This is to certify Ampere-Hour Meters at the above plant were checked on the above date with recorded data provided below This certification was accomplished by comparison to the following meter which was certified as indicated and is traceable to NIST

FLUKE DMM ISN 68630277 DA TE CERTIFIED

middotBttiff~~~i~~lj~~~aif~5-~~8~itli~i1~)poundl~~j Jl~t7c~-j AlVr--iov ~ I

210

2llt

degE-V1d Q 16v A rY() ~

-In accordance with ISO 10012-1 ANSI 2540-1

FOR INFORMATION ONLY fILAS TESTING LAB~TORIES INC

ATlOS TESTlNltl LABCltHORIES ltNC SUBMITS TlltIS REPORT AS THE COlt~ICENTli-L PROPERTY 0~ OUR OIENT REPRODUCTION RICMTS ARE RESERVEO PENCINC CUR WRflTEN APPROVAL tANO THEN MAY ONLY aE ~couceo IN FUUJ AS A PROTECTICN 0~ OUR OtENT ANO CJASSVES

OUTSICE CALISAATION ~RMS (21)

APPENDIX E-1

PROCESS DATA FOR APRIL 30 1998 SOURCE TEST

NICKEL PLATING PROCESS DATA

Company Name Fo~s Plott1 Date ~ tJoJ Test ID Page L_ of_pound

Time er 10 er 1s 1 5pound)

Tank i~1 Rr1ala+ 13rqt ~ -~--

r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)

Volt Meter (volt) ro bb PO 7) Rn CJ Tank Temp (degrees Fl Lin 90 ~)

7t7 -ft 1t2

Nickel Solution (ozqal)

Surface Tension (dynescm)

Platino Rate

Air Aqitation (on or off) 011 1111 O) on nn 1~

Air Pressure rosiq) g R p p I P Time tt)f t1Jt c t~ Tank 71J ( P1r I _JJ r 1 t JlMMY- f loJ Totalizer R((I lJ I 4-t~ JA ftttJIJ IYlcfot -f11pf otJSJ-9J

Amo Meter (amps) oo ~] J IYgttJ ~

90

~ zoVolt Meter (volt) Po ~o 9) 70

Tank Temp (deorees Fl ~) JS 110 75 lo S



Platinq Rate

Air Aoitation (on or off) 0J OA )~ Air Pressure (osia) P p p R f

Time tJ r11 J ( Tank ll~ r P r JAJ J ~i~ -amp IfJ-t I Totalizer

JOvP9 lJJ6~90 ))( 7C P-f i ~9711 ]j ftp~

Amp Meter (amps) ~ltoo 00 g-) kJO ~ Otgt 21110

Volt Meter (volt) PO 7t p 70 yr ~(

Tank Temp (dearees F) -90 Jj ~5 9t s5

Nickel Solution (ozaal) Surface Tension (dynescm)

Platinq Rate

Air Aaitation (on or off) 01 CA _ A 6 nA

Air Pressure (psig)



Company Name For Ploh1 Date t JofI Test ID Pageamp_of_pound

Time 11-SS 1ns I j C

Tank gAI- ( 1 bull-- f ra~t I nnot lrro1i r r fl __J Totalizer OlJ79

I

tJK JQ )1 7)middot9~ lypjr I- - -

Amp Meter (amps) 9CltJ ~ 111J - ltI() P~lO PJ()

Volt Meter (volt) ~) ~) -7 ) ~o 7J

90

~)

0Tank Temp (degrees F) ~ ~ -10 O



Platina Rate

Air Aqitation (on or off) OYI OY 011 II on Air Pressure (osia) p f p i d p Time YO 2C~ _

Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ

Volt Meter (volt) ~o 7J 7 jJ_ J o 70

Tank Temp (degrees F) 4 t 90 9 30

Nickel Solution (ozqal) Surface Tension (dynescm)

Platinq Rate

Air Agitation (on or off)

Air Pressure (psig)

C1 Ah AJ ~ p F p F 9

Time rr~J 7-JO ~N Tank r~ r Ar14f A---J- r_f___ P _ FhJf Totalizer ~ 0771 J~P~ II1 nfr1~ t7~fCO

Amp Meter (amos) ~YO POO PC70 ~ltJO t7(J tJO

Volt Meter (volt) 7 I) 7 I) 7 70 ~ Tank Temp (degrees F) ~17 10 ft 10 ~t) 1)

Nickel Solution (ozgal) Surface Tension (dvnescm)

Platinq Rate

Air Agitation (on or off) on ( 0 -A tM

Air Pressure (psig) J7 r p P p

Ir-----



Company Name Toss P ah( Date tJoP Test ID Page2ofpound_

Time ~~O

Tank JltI~

Totalizer oftfP Amo Meter (amos) PCJCJ

Volt Meter (volt) 7C)

Tank Temo (deqrees F) yen(

Nickel Solution (ozoal)

Surface Tension (dvnescm)

Platinq Rate

Air Aoitation (on or off) Cl

Air Pressure (psiq) I Time ii

Tank 71 Totalizer ampf)JL

Amp Meter (amps) 71170

Volt Meter (volt) zo Tank Temp (deqrees F) --90



Platino Rate

Air Aqitation (on or off) 01

Air Pressure (osiq) Time ((I)

Tank Prtgt1-

Totalizer 0~-9

Amo Meter (amos) (J(J

Volt Meter (volt) -71

Tank Temo (degrees F) -yen

Nickel Solution (ozqal) Surface Tension (dvnescm)

Platino Rate

Air Aqitation (on or off) 7II

Air Pressure (psig) f

9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~

1 -ftr ohs 2CJOO COO

C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2

PROCESS DATA FOR MAY 2 1998 SOURCE TEST


Company Name sr PJohi Datemiddot sz7F Test ID Page z ofpound_

Time 1middotos Tank Rra1

I

Totalizer 11001 1~

Amp Meter (amps) 1JOO

Volt Meter (volt) l~1

Tank Temp (deqrees F) 1J



Platina Rate

Air Aqitation (on or off) oFf Air Pressure (osia) t)

Time 1 ro Tank J -

Totalizer O~_M

Amp Meter (amps) 70tO

Volt Meter (volt) 12

Tank Temo (dearees F) -9J

Nickel Solution (ozQal)

Surface Tension (dynescml

Platino Rate

Air Aaitation (on or off) () I==

Air Pressure (psia) 0

Time bull 1r Tank Rr t Totalizer do ~ao-

Amp Meter (amps) J ~

Volt Meter (volt) tJ1

Tank Temo (dearees F) YO

Nickel Solution (ozlaal) Surface Tension (dynescm)

Platinq Rate

Air Aaitation (on or off) -fF Air Pressure (psig) 0

s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70

FF r tmiddotos f_ __ t

7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0

1middot 35 -r rq- s n~it I

00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n

go( ~frnt r Rri~ Ufff ~~II

~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0



Company Name Fos Platmiddot1 Date gttJI Test ID Page~ of L Time il 1o srr Tank n A- n- ~r-~t 11~- Br1q_1 S 13r~J

tC)J tJTotalizer oJtIJ

JO ~11 f 7r9 n-r2c1

~oz~~

Amp Meter (amps) ZOa rCJO 2 77t) jC)t) ~CtJO RtgtIJ

Volt Meter (volt) It 2 ~c t2_ 6 ~

70

9amp POTank Temo (deqrees F) 41 O oC l

Nickel Solution (ozgal)


Platinq Rate

Air Aoitation (on or off) n= -tf nfF I) rf nff I) Ff Air Pressure osiq) 0 0 6 0 0 0 Time f_7 ~-~r Tank Totalizer

)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP

Amp Meter (amps) 7nlVI 1voo 10oo 800 tooo PCIO

Volt Meter (volt) 02 16 a~ b ~ fe(deg

Tank Temo (deorees F) 3J O -1f Z) r J

Nickel Solution (ozgal) Surface Tension (dynescm)

Platinq Rate

Air Aaitation (on or off) ff nff tf aff n[+ nF+ Air Pressure (osio) 0 0 o 0 0 0 Time 4middot(( r0 r ~( Tank e4 r llrtJJ 7--1t (~middot ~l-r f=- Jr D

Totalizer llircent97 hrf1 )J(1 7-6c l))19 lnpf1n

Amo Meter (amps) 2CJO Pl717 n- Pa ~IYYi Pl)n

Volt Meter (volt) 1 - 11_l t2~ Ypound Tank Temp (degrees F) -ff O 1 CJ -f

Nickel Solution ( ozgal) Surface Tension (dvnescm)

Platina Rate

Air Agitation (on or off) A f -r+ rF ff tJFF ff

Air Pressure (psig) 0 (J 0 0 0 0



Company Name Forr roh -f Date Sz9t Test ID Page f of G

Time rrr t~

Tank 7 -1 ( (OJI J)J (n L lJ r P _u-

Totalizer y~ YJ~I cJ2f-1 ~~f9 I 7~44 7)~

Amo Meter (amps) ~an

ycJ() yJ 2~ PJ

Volt Meter (volt) t7 t tf I 2 9( J~ 9tf Tank Temp (deqrees F) ~ J 4 tl 91 tJ

Nickel Solution (ozlaal)


Plating Rate

Air Aoitation (on or off) 7 ofl )ft Jh -H T7 Air Pressure (psig) CJ 0 C) t CJ Time If( ~1 6JJ Tank -fJ --~r bullf b _J ltr~f (~rJ o~Jfc r hr Totalizer ~fz4 ofo tr-r 0f 0rtJ cJfJ

Amp Meter (amps) 7YYgt j()CJ ooo PttJ 200o PtJO

Volt Meter (volt) tl2 y t tJ ~ 96 tJ1 t Tank Temp (deQrees Fl ~r Cl 9f C) I 0

Nickel Solution (ozoal) Surface Tension (dynescm)

Platina Rate

Air Aoitation (on or off) 7e- rr -f c~ JC

Air Pressure (psiq) 0 0 0 0 Time 7) 7 bull) ( 7-9J Tank ~ L r -1 77 ~ r -ii AA r Totalizer oifPrs nfi

O~f-1P

C1f2-9 Pt 07JP

Amo Meter (amps) 2000 YOO ~000 YOO ~ntYJ PcJO

Volt Meter (volt) 0 ~p Cl2 y _) 9P

Tank Temo (deqrees F) ~ ltO -4r C +J


Plating Rate

Air Aaitation (on or off) orr ofr oF Cl--- t7rdeg (7f Air Pressure (psig) 0 0 0 0 0 0


PACIFIC ENVIRONMENTAL SERVICES INC CARB Method 433 Tank Data Report

Facility Foss Plating Source Bright and Semi Bright Tank Method CARB 433 Test Date 43098-5298

Run l Time Description Quantity Tank 920 Towel Boxes were in 8 Bright

Roll Bars were in 2 Bright 923 Towel Boxes were in 4 Semi Bright

Tubs were in 2 middot Semi Bright 930 Bars were in 6 Semi Bright

Roll Bars were in 2 Semi Bright 938 Towel Boxes were out 8 Bright

Roll Bars were out 2 Bright 940 Manifolds were in 16 Bright

Tubs were out 2 Semi Bright Towel Boxes were out 4 Semi Bright

945 Hollow Tubes were in 22 Bri_ght Pointed Hangers were in 8 Bright

10 I 0 Bars were out 6 Semi Bright Roll Bars were out 2 Semi Bright

1030 Manifolds were out 16 Bright Hollow Tubes were out 4 Bright Pointed Han_gers were out 8 Bright

1040 Towel Boxes were in 6 Semi Bright Bumpers were in 2 Semi Bright Unions were in 4 Semi Bright

1045 Stubbies were in 24 Bright 1105 Stubbies were out 24 Bright 11 I 5 Towel Boxes were out 6 Semi Bright

Bumpers were out 2 Semi Bright Unions were out 4 Semi Bright


Run 2 Time Description Quantity Tank 1200 ZV were in 16 Bright

Bars were in 6 Bright 1220 Bars were in 22 Bright

Stand Bases were in 6 Bright 1226 Roll Bars were in 6 Semi Bright

Rails were in 4 Semi Bright 1230 ZV were out 16 Bright

Bars were out 6 Bright 1235 Towel Boxes were in 8 Semi Bright

Easi Rod were in 10 Semi Bright Rails were in 40 Bright Roll Bars were in 6 Bright

1238 Roll Bars were out 6 Semi Bright Rails were out 4 Semi Bright bull

1245 Bars were out 22 Bright Stand Bases were out 6 Bright Towel Boxes were out 8 Semi Bright Easi Rod were out 10 Semi Bright

1305 Rails were out 40 Bright Roll Bars were out 6 Bri_ght

13 IS Bumpers were in 12 Semi Bright Plates were in 4 Semi Bright Prongs were in 36 Bright Plates were in 4 Bright

1328 Prongs were out 36 Bright Plates were out 4 Bright Bars were in 10 Bright Rails were in 4 Bright

1338 Bumpers were out 12 Semi Bright Plates were out 4 Semi Bright Bars were out 10 Bright Rails were out 4 Bright

2

PACIFIC ENVIRON11ENTAL SERVICES INC CARB Method 433

TankData Report Run 3 Time Description Quantity Tank 1442 Towe Paper were in 8 Bright

Manifolds were in 6 Semi Bright Bumpers were in 6 Semi Bright Stand Bases were in 6 Bright

1450 Manifolds were out 6 Semi Bright Bumpers were out 6 Semi Bright

1454 Bars were in 108 Semi Bright Stand Bases were out 6 Bright Towel Paper were out 8 Bright

I 500 Plates were in 6 Bright Bars were in 6 Bright

I 5 12 Bars were out 108 Semi Bright Stand Bases were in 7 Semi Bright Bars were in 8 Semi Bright

1520 Towel Paper were in 8 Bright lt

Stand Bases were in 20 Bright Plates were out 6 Bright Bars were out 6 Bright

1545 Stand Bases were out 7 Semi Bright Bars were out 8 Semi Bright

1603 Towel Papers were out 8 Bright Stand Bases were out 20 Bright Chairs were in 4 Bright

1620 Chairs were out 4 Bright

3

APPENDIXF

LABORATORY DATA FOR THE SEMI-BRIGHT NICKEL PLATING SOLUTION

TO AT TECH lsiI P0405-08-1998 09 14A1 FR01 WAL

WlllI IA~1611a ampaAIIIATIIUllg Ill 1t744 MONT YICTA AVENJE bull CHINO CALIFORNIA 91710 middot (9081 amp27-3828 bull FU~ 827-o4111

cusrOMlR__A_T_O_T_E_C_H_US_A_I_N_c_________ WAL NO~ 805011 7

DATiAiCilViD___ocs1coccc_98__

IRIS BUCHANAN 99DATE OF REPORT_o_5__o_7____ 1ATTNTION~------------------

MARK 90 SE1I-BR_I6_HT NICKEL PLATING SOLUTIONSAMPLE IOENTiflCATION

Sa111pl11 ~057

GALLON_g_______$AMPL11EOi__o_s_1_0_6_~9_B__TANK NO

ANALYSIS 8TANDAIID IUSULTS

~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal

t-i I ClltEl CHLORIDE 7 1 ml I

a RIC ACID l ~42 ml 587 0gal

I

liH 343 3 43 I

SURFACE I

TENSION 42 dynecm 342 dynecm

~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0

ATOTECH USA P0305--09-1998 09 131=t1 FR01 ~ TO

WIITIII llla1111AL LIIIIITIIHll 11 H1111 1~144 MONff VISTA AVNU bull CHINO CALllOlffIIA 91710 bull (109) 927bull382a bull FAX IIIOOl 827~9I

ATOTECH USA INC 8050118WAL NO_________ CUSTOMrn-----------middot-------

050698DATE llllClIVO______

middotATTENTJO_________________ 0~0798IRIS BUCHANAN 0ATm0F REPORT______

P1ARK 90 sett-BRIGHT NICKEL PLATING SOLUTION SAMPLE IDENTIFICATION

Sample I 1~8 5~ 15-R () ~ 050698TANK NO ~ ~1-GALLONS SAMPLE-______

ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE

NI ClltEL DilOR I DE

BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050

10JWI02CONT bull I r i bull middot

90 39td llIQNJW S1 l-03lCllll poundSgt0P50pound9Z9

1

TO ATOTECH USA P02~--eG-1999 09113AI FROf IJlL

Wi8TIII Ill~1TIIAL LAl8IATlllii11 Illa 1$744 MONTamp i18tll AVENUE bull CHINO CALllORNIA 11710 (9081127-3621 bull lAX (9091 627-0491

CUSTOM11________________ B050119

0510698

AT0TECH USA INC Wll No_________

DATE RECEIVE_______i IRIS BUCHANAN 050798[ATTiNTI0middot_________________ OATEOFAEPOflT______

1

HARK ~o ~I-BRIGHT NICKEL PLATIN8 SOLUTION SgtMPtE IDlNTIACATION -1059

GALLON_______SAMPLEO__o_5__o_b_l98__TANI( NO ~ fgt 3

ANALYSIS STANDARD IU5ULTS

ljICKEL

jNlCKEL SULFATE NI CKEI CHLORIDE

isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I

LB ~d II~ ltSl1 1lt)3lOllt 6s=st e66tte01s0

TO ATOTECH USA PBi05-08-1998 09 1sit1 FRCM IJAL

WTII AIALTTIIAL LlllllTlllll9 UH)c 1376 MOHTE VISTA AVENUE bull CHINO C4IFOAMA 111710 (IIOQl bull27deg3BH bull u (9011112Hl411

ATOTECH USA INC middot 8(150114CUSTOMe_______________ bull-- WAJ NO_________

DATE RECEIE0__0_5_1_0_6_19_8__

-~10___I_R_I_s_s_uc_H_AN_AN___________ DATE OF REPORl__o_s__o7_1_9_B_

NARK 90 SBII-BRlGHT NICKEL PLATING SOLUTION iSAMPLf IDENTIFICATION

TANK NO 8ALLON________$VIIP1eo_______0506~8

AMALVIIS STANDAJIID lltSULTS

I

jRAW DATA

NICKEL ~04 ml 819 o~11al

NICKEL SULFATE J06 ozgal

~ I Ctm OLOR I DE 16 9

ml 548 ozgal I I BORIC ACID

i j 14 1 ml ~-83 ozgal

~H -~ 3o5

I

SURFACE TENSION I

(349 dynbulllc111 349 dynbullcm

i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl

z0 ~d 6sst e66te01s0

TO ATOTECH USA Pe605-08-1998 09bull 1uM FRCM liA

WlII AIAt1T8Cll LIIIIATlllll9 IIIC 137U MONTE YIST -VENUI bull CHINO CALIFORNIA 91710 bull (909) 827bull3829 bull PAX (110111 827oamp1

~ClJSTOMeR____A_T_ WAL NO__ _ __--shy_TE_C_H_US_A_I_N_c________ e_oso_1_1_5

DAT ACe1veo__o_s_1_0_1_1_9_e_

iATTINTION__I_R_l_S_B_u_cH_A_NA_N___~---- ___ DATE OF RiPORT_o_s__0_7__9_8__

MARK 90 SE~I-BRIGHT NICKEL PLATING SOLUTIONjSAMPLE I0ENTIFICATION

__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V

~ ~~GALLON~______SA~PLEO__o_s_1_o_h__9_B__TANK NO

AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp

l SURFACE TENSION i IM-901 i I

I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm

052 4 45 middotgill 1000 ilbulll

6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9

TO ATOTECH USA P 05 05-08-1998 09 14AI FR01 IA

WITIIJ AILf11CAL Llllll19111i Sla 13744 MONTI VISTA AVENUE CHINO CAUPOfNIA91110 bull (901) 127-3e28 middot FiX (9091 e27-o491

ATOTECH USA lNC 805011 oWAL NoCUSTOME~----------------- ---------DATE RECE1VE0 __o_s_1_0_6_1_9_B_

ATTENTlO____I_R_I_S_B_UC_H_A_N_A_N________ 108198DATE OF REPORT__o_5__ _ _ _

NARIlt 90 SEl11-BRI0HT NICKEi PLATING SOLUTIONSAMPLE IDENTIFICATION

Samp 1 a 1 1056

TANK NO 1l) ~ ~-GALLONS________$AMPUP___o_s__o6_1_9_B_

ANALYSIS STANDARD IIUULTII

NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal

_ jOOQ CONT ibullbull

1bull

1gt0 ~d IIQKJW S1 I-Cl3ll 6s=st 866tt001s0

~OJf bull 0~~7--lt)l-U

DATE J41e PAGE L_or_L_ ---shymiddotmiddot-shyliB tJllJl mw a

CS)lJ PACIFIC ENVIRONMENTAL SERVICE CHAIN-OF-CUSTODY RECORD CD4J - ~ J1

MDJEcrNAME l==oJJ ~l yeni ~ METHODS 1 ~ - coMErs

CDcouPNAME middoty ES O _ ~ ~ CONTAINER TYPE REfERlNCE f - 13tUO-V t JZ-rrt-~O ~ 1 ~ ~ l ~

J1 ADDRESS -I I tm 7il ()7i V ~ bull t ~ ~ ~ ~ 8

U1 rl _ f II middot __ )ltL f- (- ~ 7 0 b ~ j ~ -J ~ l5

1SAllllfRS SIGNATURE) 1 )1 1 ~ - -=t If

c$AllllE DATE 1114 LOCAIIOIO ~ s ~ ~ ~ Q _ t-J

w 9te k~r 4hAo ~ 11- tJ ~ a

J1

CS)J ~ u2 fl v I t 5 (l J - Q i_ Jo r I I 1 ~~r1 _ e_3

w

I d r1 i I C Cl ll - Q

J J~ II v v I J [) 1If 1)

I tf rfJ I I ti middot JI Y 11 ~

Igt -i

~ Gw--o~ D E REUNOUISI~ OAR RELIIODUISIEDBY DATE JOTAL NUYBEROFCONTAlERS

r- __ lfbull ~

SIGNATURE - bull -f ampIGNAllJRE SAMlIECOJDTIONS i4 - - Z_ - - 4 1----1 1-----1 RECEIVED ON ICE YES NO H TitIf TIME Igt1--------------1 TIME

PPIHTED - ~)I~ PRINTED NAME sebullbulleo s NOV I~ ~ YE Sr

COl6AHY COflfNlY COMPIINY SPECIAL SIIPMENT IHAlOtlG

I RECEIVED BY IMTE ~~IVEDBY (l DATE -RE7CEN-E-DBY---------4--D-AI-E~ORSTORAGEREOUIREUENTS

middot- f --1- middot- ~lt_ ~ bull~bullNmtI StGNAp - IJ SIOPMTIft SIClNAWR

4 bull middot - R (ta 1-------------1 TltETIME TWIE P~NAIIE PflltHfONAME PRINIEONAME i

~4 1- t1r~fo Butn~~ a

co11rANY COMPIINYCOMNfY = ~ J_tf

Tclopholle (Ill) 1561400 13100 Brooks Dribulle Baldwin Pork Calilbml1 91706 Fu (Ill) amp14-0120

APPENDIXG

LABORATORY DATA FOR THE BRIGHT NICKEL PLATING SOLUTION

Brent America Inc 16961 KnonAvenul La Mirod C11liforni11 90638-6015

SERVICE THROUGH SOLUTIONS

TANK NO 5JMfLF INICKEL PLATING SOLUTION TANK VOLUME IZ(-l I Plltamp7 PROCESS

SAMPLE DA TE Afo1 t- 6 lffl r

CUSTOMER SERVICE ANALYSIS

OPTIMUM RECOMMENDED BATH COMPOSITION ANALYSIS CONCENTRATION ADDITIONS

Nickel Metal ozgal

Nickel Sulfate ozgal ~ Nickel Chloride ozgal 0 98 Boric Acid ozgal B-if pH 4 OJ

ADDITIVES

REMARKS amp SPECIAL INSTRUCTIONS

Cleaning and Meh1 Treating Chemicals tor Over 50 Yea~

Brent America Inc 16961 KnonAvenue LtMirado C11ifomia 90638-6015


s A f-f PE II 2TANK NONICKEL PLATING SOLUTION TANK VOLUME kamp -2 cite 16fr PROCESS

SAMPLE DA TE



Nickel Metal ozgal

Nickel Sulfate ozgal

Nickel Chloride ozgal

Boric Acid ozgal

pH

ADDITIVES

REMARKS amp SPECIAL INSTftUCTIONS

Brent America Inc 6961 KnortAbulltniu La Mirada California 90638-60S

SERVICE THROUGH SOLLJTIONS

SIIf--1tr -II JTANK NO NICKEL PLATING SOLUTION TANK VOLUME kN- U 2Jlft PROCESS

SAMPLEDATE Jflzlt ~998



Nickel Metal ozgal

Nicitel Sulfate ozgal


Boric Acid ozgal

pH

ADDITIVES


BrentAmerica Inc 16961 KnonAnu LaMira4 Clifornia 90638-60S

SERVICE THROUGH SOLLTTIONS

TANK NO S-ltCLC P 4NICKEL PLATING SOLUTION TANK VOLUME k~- 4 rtlIJlfr PROCESS

SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES


OPTIMUM ANALYSIS CONCENTRATION

IL C I 4 26 lo-~ Boz

4 17

RECOMMENDED ADDITIONS


Clesning snd Mela Treating Chsmca1 er Ov-r ~O Yea~

Brent America Inc 16961 KnonAvmu~ Liz Mirada Colifornio 90638-6015


Sl)ltj~--1 6TANK NO -----c--_f)NICKEL PLATING SOLUTION TANK VOLUME 4N- -(l)~(6lr PROCESS

SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES


amprent America Inc 16961 KnortAven11e LIiMinda California 906JU0J5


Slf-Jc--r (TANK NO NICKEL PLATING SOLUTION TANK VOLUME 4- ~ ~40lfr PROCESS

SAMPLE DATE l4j~f19~



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES


13744 MONTE VISTA AVENUE middot CHINO CALIFORNIA 91710 middot (909) 627middot3628 middot FAX (909) 627-0491

PACIFIC ENVIRONMENTAL SRVCSINCCUSTOM En____________________ WAL N08060640

DATE RECEIVED ( 2 c

-- middotmiddotmiddot middot B~--~=middotATTENTION____________________ DATE OF REPORT_______

SAMPLE IDENTIFICATION

-~-----l___GALLONS________SAMPLEO_bull__-___S_i_bull____

ANALYSIS STANDARD RESULTS

SURFACE TENS IOtl 31J dynecm

1RM 1002 CONT

-~~TlI 11111amp iT~~ll 1l~llII~gt ~IS 13744 MONTE VISTA AVENUE bull CHINO CALIFORNIA 91710 (909) 827middot3628 middot FAX (909) 827-0491

PACIFIC ENVIRONMENTAL SRVCSINC CUSTOME~--------------------

middotmiddot) -middot - 7 s middotsDATE RECEIVED ________

)ElNT- -bull--- =itATTENTION_____________________

BFIGHT NTGL SAMPLE IDENTIFICATION

~o_____-_c___GALLONS________SAMPLED__O_______r_=__


SUFFACE TENSION 31 2 dyrecm

ORM 1002 CONT

13744 MONTE VISTA AVENUE middot CHINO CALIFORNIA 91710 middot (909) 627-3628 middot FAX (909) 627-0491

PACIFIC ENVIRONMENTAL SRVCSINC Q(-l() L4WAL NO -middot ~ i CUSTOME~-------------------

062 9 3DATE RECEIVED-_______

Pl~-= 2~~~l~- middotmiddot ~ - middot- middotmiddotATTENTION____________________ DATE OF REPORT_-______

BRIGHT NICVEL SAMPLE IDENTIFICATION

t8) bullI (l~26~3~ NO________GALLON________SAMPLED________


SURFACE TENSION

ORM 1002 CONT

13744 MONTE VISTA AVENUE middot CHINO CALIFORNIA 91710 (909) 627-3626 FAX (909) 627-0491

CUSTOMER~__F_A_c__I_F_I_C_E_N__I_F__N_l_1E_N_T_A_L_S_middotmiddotF_bull_c_s_I_~_ic_ WAL NO 8060643

ATTENTION____D_E_N_N_I_S_B_E_C_1_middotP_F__________ DATE OF REPORT __c_)~__-_2___9_E_


Jid______r__GALLONS_______SAMPLED___)6__1 _-6__o___ _


SUFFACE TENS I Ot

lRM 1002 CONT

13744 MONTE VISTA AVENUE middot CHINO CALIFORNIA 91710 (909) 627middot3628 middot FAX (909) 627-0491

PACIFIC ENVIRONMENTAL SRVCSINC 8060644CUSTOME___________________ WAL NO_________

062698DATE RECEIVED _______

DENN IS BEC c Cbull-- 2middot= 9~~ATTENTION___________________ DATE OF REPORT _______


~ NO_______GALLONS_______SAMPLED_______


SUFFACE TENSION 31 3 cynecm

)RM 1002 CONT

13744 MONTE VISTA AVENUE bull CHINO CALIFORNIA 91710 (909) 627-3626 middot FAX (909) 627-0491

PACIFIC ENVIRONMENTAL SRVCSINC 8(gt6(gt64~WAL NO - - -CUSTOME~------------------

06126198DATE RECEIVED

DENN IS BECVAFATTENTION___________________ DATE OF REPORT b 29 98

BRIGHT NI CfltCL SAMPLE IDENTIFICATION

77J c (16 9R~-NO_______GALLONS_______SAMPLED - -


SURFACE TENSION 335 dynecm

(

ORM 1002 CONT

Appendix G

Model Source Test Protocol

MODEL SOURCE TEST PROTOCOL FOR NICKEL EMISSION MEASUREMENTS

Prepared For

Prepared On

Prepared By

Telephone

SOURCE TEST PROTOCOL FOR NICKEL EMISSION MEASUREMENTS

TABLE OF CONTENTS

Page

SECTION 1 INTRODUCTION

SECTION 2 EQUIPMENT AND PROCESS DESCRIPTION

SECTION 3 TESTING METHODOLOGY

SECTION 4 RESULTS

SECTION 5 QUALITY ASSURANCEQUALITY CONTROL

LIST OF TABLES

Table 1 Example Data Summary for Nickel Emissions

Table 2 Example Data Summary of Process Conditions

Table 3 Calibration Procedures and Criteria for CARB Method 433

Table 4 Quality Assurance Objectives for Precision and Accuracy

LIST OF FIGURES

Figure I Sampling Location and Discharge Fan

Figure 2 Plan View of System

Figure 3 Diagram of Emission Control Device

Figure 4 Schematic Diagram ofCARB Method 433 Sampling Train

APPENDICES

APPENDIX A FIELD DATA AND CALCULATION SHEETS

APPENDIX B EXAMPLE CHAIN OF CUSTODY FORM

APPENDIX C COPY OF PERMIT TO OPERATE


GENERAL INFORMATION

Facility

Contact Telephone Fax

Source Test Coordinators

Telephone Fax

Telephone Fax

Source Testing Contractor


Schedule


10 INTRODUCTION

Describe the location of the test and the purpose of the emissions testing program

20 EQUIPMENT AND PROCESS DESCRIPTION

The following is a summary of the tanks and the rectifiers in use at the subject nickel plating

facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation

A diagram showing the tanks and ventilation system is shown as Figure 1 A plan view of the

plating area and roof vents is included as Figure 2 These plating tanks will utilize a forced draft

ventilation system during the test which includes a XXXX cfm fan Plastic sheeting will be placed

around the plating tanks to assure all plating emissions are captured by the ventilation system and

to assure that the contribution of background nickel is minimized These plating tanks are [not]

vented to an emissions control device A diagram of the emission control device is included as

Figure 3 This testing program will be conducted over a XX day period

APPENDIX A-1

FIELD DATA AND CALCULATION SHEETS FOR APRil 30 1998 SOURCE TEST










FIELD DATA

I

- 0 ii 0 m z

0

m

r

m



Run Number______________







7_( (le s ~ ti a ( 5 0 SS ~1 B





~( 2ClO 1-( ltO

Velocity Head

Ps (in 1120) 04t

I I I

I QC

I

I bull l-


J~

l l --

fArl- I __






bull1- 7- I)






8-i _ 1 SI ~ r8 ~ Sz


bull J - - - --l-- ~ AD- 01 1_ -I ~u

8~ l

1~ I

o ~s uM Oi u

81

I

FIELD DATA






Number 8 Vm rs m



I 1I

114 t11

~tl0 -gt () -Z gt

bull l bull

-n-_

ZIH

C l

ltt

11-Z9 Ii lC

11- i

-zc-o

QtC


t 10

I Igt bull Z

gt 1-

-

~(

c io l

l- 1- 0 ltI

I l6


)

11 i (


)

t

6 IIJS It1

l~t 0 ~bull--11 ~1

~~~ (J

fc 4 v Sli 3

I t--~ Ibull

C

-O It 1 Iu

l4o 4 05

jlal 0

5Ca i oo-t i l --













Ill I 0fiu

~~ middot~ y I





Actual l I c)

cp 1(deg

tamp bull-

lO II lI l I A



-

Stack Temp

Ts (F)

0--1 li z

j(

- II



~ J bullbull

FIELD DATA

Planl Date

fo-l P~MT-Li 1o i t



-middot -I


~



l _

( ~ -z1



-1 o - S IJ P



I



0

m

1




Desired l 0 I ltt

bull llt zr-


(f) Bi i

o

(f) IAlt~

gtmiddot~

(F) l_ 2-

(in Ilg) ro 30 0 o

(F) i-

(f) A

ff) (0

(o

uO ( 0

~ I

n-

1t 11

14 q JJ IAlI~

I co

Slll1 ~10J 1l1 l

I bull t d

bull Z tItr

I 1-bull zr-bull1 (

ttl o- l08

I10 if iJ

pound I

ll iu

gt lo ~tgt

r rJ -i- ll


4 (

_


51-l i l~~I Sl~ 1

P~ 11S 3

(lIO



Ibull 1 I bull1 I 1

II l middot-l

I(

i ) I lS ir

I 3pound 1 H


I I 7 I

lu~ lotgt l l




J-0 middot 0

middot1 0 0

ZO lO middotro


lt u

lIJI

10~ l 1

tlli 111

1i-01-1111 t (Z t tz~


h1 ~ I I -

1t bull I t

(oI~

-

Ill

tr-It l I (1-

Bt BIz-

RI H t ~~ -

LO 7 b

1ltgt- I

15s ---

u[ ~a uyL

l-1 bull e r To 105 I 1~] ((11 ~IIi

55 uu

81

r~=-~~~ ~o-- --ts==




- --- -middotmiddot------------c= ~

j- l r ln c lt_--= -3

- ___ ~ n middot~------ ~- A t ~~ C - Cl



Smiddot l

L

3

-I

S

(

B - I

2

middot3

y

s (

Q -

1

)

ltt

s-(


0

5

s-~

0 3

t)

5 3 ~

2-2--

2

s s

3 1

0


Sc ~i c - 111 le C ~

~ 1

1 t

I

~Z

T a T

I I

03 I

T




I I I I I I I I I


sect388



CATE -2C-qo








C 1

-C]-z I

l ( r 3

J_ c v v

r I c -1






PORT LO CATION

OISTAICE FROM

EDGE


2

3

3--4-- ~-i

bullI amp 6 io

1 B

i 0 I middotB C

-middot 11- 3 l3

i

s

~ 112

--tt Ill 0 ~

117-

I I

b 0

I

TRAVERSE

NUMBER OF STACK



FACIIITY

SOURCE

DATE

RUN

METHOD

BOX


GR6--IS

INITLU

GRAMS

r

TOTAL

GRMS






INITALS


FACIJITY

SOURCE

DATE

RUN

METHOD

BOX


GRJ-15 GR-15 GRJ-15

I

2

3

4

DI WATER

DI WATER

EMPIT

SILICA GEL

2--Z

~-~

o ~ (


INITALS


FACIIITY

SOURCE

DATE

RUN

METHOD we zrJ BOX


GR-1S GRMS

IIf

~D

I DIWATER

GRltJ-IS

e

2

3

4

DI WATER

EMPTY

SILICA GEL

I 0

IS--L


INITALS



FACfIITY

SOURCE

DATE

RUN

METHOD

BOX


GRJ-1S

I DI WATER

2 DI WATER

3 EMPTY

4 SILICA GEL

GRJ1S

t~c

Sf

GRJ-IS

-o~z -og

-o J

-02


INlTALS t

NOMENCLATURE




g ft3




1



letgt +460) ( -ZHmiddot+( 1 136))

8 1 + 460) (2992)




Vwstd = (00000894)( v B + 460)( Lf2 - )

Vwstd = ____I_~----q___


Bwo = 100 ( middot t 1 ) ( 4 + t S 781 )

Bwo= ------

2



MWd = (032 x 1- 010 ) + (044 x O O 1 ) + (028 x ( O + +I Ci ))


MWw = (MWd) (1 - BWo 100) + 18 ((BWo 100))

MWw = ( -Z 6- B-1) (1--Z -S- 100) + (18 ( z s-( 100))

(5) VELOCITY (Vs)

460Vs = 8549 x CP x ~ x ___Ts_+_- ----=-Ps

(Mw_) X (Bp + 136)

( 0 Ca + 460)vs = 8549 x ( o e- ) x ( 1 o 1 0 ) x 1----------------------

( -Z8- St ) X ( 2 degt ) tdeg + 0 C l )136

Vs= (po 9J

3


As = (Ds)2

x (31416) 576

( ) 2

X (31416)As=--------------~

576

As= ----


As = (L) (W) 144

As=( le ) ( I e ) I 144

As= -1B-------=--


ACFM = (Vs) (60) x (As)


ACFM =--~_5_0---CS-___

4



( ( R +460) ( 21+f) + ( 6u ~ I 136))X----=Ua__~X------------=-~--~

( o v +460) 2992




DSCFM= ( vO-l~ )x(l --z-~ 100)

DSCFM = ___-s_9_S_9__

(11) ISOKINETIC ()


60 x 0 x Vs x (Ps 136 + Pb) (Dn2 x 0005454)




5



mg Ni DSCM = ( 1- ~ ) I~ ( 7i8r ) X (0028317)



DSCF 1000






6

APPENDIX A-2











FIELD DATA



~ Fl Meter Della ll


1






I



Point Number

t t J V middotr IA

I 1

J I r lt

Time Time e





Reneling Vm



Head Ps


I u j bull -


I U 1






I - Lu

Temp Ts (F) lcD

o- 0~

~y oc

0~ middotbull ti -

Io - l6

Inlet Tmin

(F) t middot-t~ ~

- igt o j7r--

--7~-7

Outlet Tm out

(F) 1-

--- y

--t J _q

_ ~ I - Q n L-

Vacuum

(in II~) 7

-l

J )

J

) )

I J

Probe Temp

(F) t-J(

Dox Temp

(F) IA

Temp

ff) __ _ 2

I A

(o i 1

IA - C _ ~

tA) _ L-

C I

I l I

(

I _

I II)-I I _

I ~ (

ltgtl(1

1 _vc 111 ~ l A- bull J ~



l

lt l

I ~ _ tt

I Lbull j I

( lt L

t -lt C ( r

( (

l t IJ

I I CJ I I I

I t I I I

7 J--7 -i -fj - 1-

7 --1l J 7)

_)

1 )

J

v w

CL

(G _J

~lt-I-~

[Jou9 0 w u--~ Di


fl V 1 ~

l

Plant

Date

- -bull




amp J -)_ 5 ~

O C rs--rp









_+ J


t~ ----

( I ((

FIELD DATA


~degfmiddotk


t Factor l L





middot1 C

bull I I I

I bull 0 ()


I I I

lh ltLt _L(


(F) Ii l

~ I

-J J-middot

tmiddotL t jI



(I) 7lt -~ i bull

f cJ I O lt Ibull f

ft IN I ILI 1J

l bull pound IL

I-I

1 I-

1 -- I

X) J 1 -L-- IJ 1 I


I bull

- d 0

) P ( ampI


l l-t--J L _ c_c l~

I 1

) -bullt I I

I I I

I -- I

c ) c 1- I ~ Ihl t

) (J I -~ r1 J - I ____ middot

Ibull r (

I () I rl

- -

Idlt- ~ -


I 11 J - I

bull I


r middotmiddotbull

I I

C I IrJ (_


bull J ( I

_ middot1 1 -

degta Uj MU

I

middot

- -

Plant __ ~






n A I 11 10

m ~



0 )) l I~ Jgtlgt) )( - I I I



- I Lgti- 1 --I - I I I


l


( 7I If I I I - ) I I l I -

FIELD DATA





6-t nLt



LUI Ts




It l ~-~

- I ) -c-1-J 1 J(

~

-rt I

1 ---i )I 1 )A

-u rbull-c _ i ~


1 5 l1 ~u ~ ~

Desired I [)c

I J tt I ( lt

lltf l l ti( 1

ltLf I 11

bull1 lu

r

111 1 ~


I e- 11 I)

( r ID

1tv llv 10l

I( I L-0

I CA


I I 0 I 11J

1 7



FACILITY

SOURCE

DATE r2f J

RUN

METHOD

BOX


I

2

3

4

DI WATER

DJWATER

EMPTY

SILICA GEL


s- J (

_ 0

I 1-- t


INITALS v


FACILITY

SOURCE

DATE rhlrr

RUN

METHOD

BOX rL

IMPINGER CONTENTS

1 DI WATER

7

2

3

DI WATER

EMPTY

4 SILICA GEL

FINAL

GRJIS

foo1


INITIAL

GRAMS

TOTAL

GRMS

I lt -( J t---

S-gt

INTTALS d7

0


FAC[LITY

SOURCE

DATE

RUN

METHOD

BOX


GRltJ~IS GRltMS

I

2

3

4

DI WATER

DI WATER

EMPTY

SILICA GEL


INITALS

TOTAL

GR~IS

J)

O-)

r-

~-(












- -

FIELD DATA


Date ~ () ~ f 9













lfJ D 1 H I

~ r -1 l l I [) ) J_JIC ~ I INl ) - ( I~()

) l I IV i-lt middot ) 1 - 0~ ) Y -11








_ I 11 - yen c-Y - _ - ~

- -to-1i 5 6 deg1

__ __________ _



Run Number ____c= _ _______



I




~ l ~ l lol X o



~~-I j1 vbull- ~JI






I I c Iv I l 1-1 11 -

v-1 Dll - ~



FIELD DATA









Stack Temp

Ts (F) ti( I 11

lt j

(

I




Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(


bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l


I IP I 7

I Lfo )


t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~


- I (() -J~

c f --- -

I

) clbull


1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation

















FIELD DATA

I

- 0 ii 0 m z

0

m

r

m



Run Number______________







7_( (le s ~ ti a ( 5 0 SS ~1 B





~( 2ClO 1-( ltO

Velocity Head

Ps (in 1120) 04t

I I I

I QC

I

I bull l-


J~

l l --

fArl- I __






bull1- 7- I)






8-i _ 1 SI ~ r8 ~ Sz


bull J - - - --l-- ~ AD- 01 1_ -I ~u

8~ l

1~ I

o ~s uM Oi u

81

I

FIELD DATA






Number 8 Vm rs m



I 1I

114 t11

~tl0 -gt () -Z gt

bull l bull

-n-_

ZIH

C l

ltt

11-Z9 Ii lC

11- i

-zc-o

QtC


t 10

I Igt bull Z

gt 1-

-

~(

c io l

l- 1- 0 ltI

I l6


)

11 i (


)

t

6 IIJS It1

l~t 0 ~bull--11 ~1

~~~ (J

fc 4 v Sli 3

I t--~ Ibull

C

-O It 1 Iu

l4o 4 05

jlal 0

5Ca i oo-t i l --













Ill I 0fiu

~~ middot~ y I





Actual l I c)

cp 1(deg

tamp bull-

lO II lI l I A



-

Stack Temp

Ts (F)

0--1 li z

j(

- II



~ J bullbull

FIELD DATA

Planl Date

fo-l P~MT-Li 1o i t



-middot -I


~



l _

( ~ -z1



-1 o - S IJ P



I



0

m

1




Desired l 0 I ltt

bull llt zr-


(f) Bi i

o

(f) IAlt~

gtmiddot~

(F) l_ 2-

(in Ilg) ro 30 0 o

(F) i-

(f) A

ff) (0

(o

uO ( 0

~ I

n-

1t 11

14 q JJ IAlI~

I co

Slll1 ~10J 1l1 l

I bull t d

bull Z tItr

I 1-bull zr-bull1 (

ttl o- l08

I10 if iJ

pound I

ll iu

gt lo ~tgt

r rJ -i- ll


4 (

_


51-l i l~~I Sl~ 1

P~ 11S 3

(lIO



Ibull 1 I bull1 I 1

II l middot-l

I(

i ) I lS ir

I 3pound 1 H


I I 7 I

lu~ lotgt l l




J-0 middot 0

middot1 0 0

ZO lO middotro


lt u

lIJI

10~ l 1

tlli 111

1i-01-1111 t (Z t tz~


h1 ~ I I -

1t bull I t

(oI~

-

Ill

tr-It l I (1-

Bt BIz-

RI H t ~~ -

LO 7 b

1ltgt- I

15s ---

u[ ~a uyL

l-1 bull e r To 105 I 1~] ((11 ~IIi

55 uu

81

r~=-~~~ ~o-- --ts==




- --- -middotmiddot------------c= ~

j- l r ln c lt_--= -3

- ___ ~ n middot~------ ~- A t ~~ C - Cl



Smiddot l

L

3

-I

S

(

B - I

2

middot3

y

s (

Q -

1

)

ltt

s-(


0

5

s-~

0 3

t)

5 3 ~

2-2--

2

s s

3 1

0


Sc ~i c - 111 le C ~

~ 1

1 t

I

~Z

T a T

I I

03 I

T




I I I I I I I I I


sect388



CATE -2C-qo








C 1

-C]-z I

l ( r 3

J_ c v v

r I c -1






PORT LO CATION

OISTAICE FROM

EDGE


2

3

3--4-- ~-i

bullI amp 6 io

1 B

i 0 I middotB C

-middot 11- 3 l3

i

s

~ 112

--tt Ill 0 ~

117-

I I

b 0

I

TRAVERSE

NUMBER OF STACK



FACIIITY

SOURCE

DATE

RUN

METHOD

BOX


GR6--IS

INITLU

GRAMS

r

TOTAL

GRMS






INITALS


FACIJITY

SOURCE

DATE

RUN

METHOD

BOX


GRJ-15 GR-15 GRJ-15

I

2

3

4

DI WATER

DI WATER

EMPIT

SILICA GEL

2--Z

~-~

o ~ (


INITALS


FACIIITY

SOURCE

DATE

RUN

METHOD we zrJ BOX


GR-1S GRMS

IIf

~D

I DIWATER

GRltJ-IS

e

2

3

4

DI WATER

EMPTY

SILICA GEL

I 0

IS--L


INITALS



FACfIITY

SOURCE

DATE

RUN

METHOD

BOX


GRJ-1S

I DI WATER

2 DI WATER

3 EMPTY

4 SILICA GEL

GRJ1S

t~c

Sf

GRJ-IS

-o~z -og

-o J

-02


INlTALS t

NOMENCLATURE




g ft3




1



letgt +460) ( -ZHmiddot+( 1 136))

8 1 + 460) (2992)




Vwstd = (00000894)( v B + 460)( Lf2 - )

Vwstd = ____I_~----q___


Bwo = 100 ( middot t 1 ) ( 4 + t S 781 )

Bwo= ------

2



MWd = (032 x 1- 010 ) + (044 x O O 1 ) + (028 x ( O + +I Ci ))


MWw = (MWd) (1 - BWo 100) + 18 ((BWo 100))

MWw = ( -Z 6- B-1) (1--Z -S- 100) + (18 ( z s-( 100))

(5) VELOCITY (Vs)

460Vs = 8549 x CP x ~ x ___Ts_+_- ----=-Ps

(Mw_) X (Bp + 136)

( 0 Ca + 460)vs = 8549 x ( o e- ) x ( 1 o 1 0 ) x 1----------------------

( -Z8- St ) X ( 2 degt ) tdeg + 0 C l )136

Vs= (po 9J

3


As = (Ds)2

x (31416) 576

( ) 2

X (31416)As=--------------~

576

As= ----


As = (L) (W) 144

As=( le ) ( I e ) I 144

As= -1B-------=--


ACFM = (Vs) (60) x (As)


ACFM =--~_5_0---CS-___

4



( ( R +460) ( 21+f) + ( 6u ~ I 136))X----=Ua__~X------------=-~--~

( o v +460) 2992




DSCFM= ( vO-l~ )x(l --z-~ 100)

DSCFM = ___-s_9_S_9__

(11) ISOKINETIC ()


60 x 0 x Vs x (Ps 136 + Pb) (Dn2 x 0005454)




5



mg Ni DSCM = ( 1- ~ ) I~ ( 7i8r ) X (0028317)



DSCF 1000






6

APPENDIX A-2











FIELD DATA



~ Fl Meter Della ll


1






I



Point Number

t t J V middotr IA

I 1

J I r lt

Time Time e





Reneling Vm



Head Ps


I u j bull -


I U 1






I - Lu

Temp Ts (F) lcD

o- 0~

~y oc

0~ middotbull ti -

Io - l6

Inlet Tmin

(F) t middot-t~ ~

- igt o j7r--

--7~-7

Outlet Tm out

(F) 1-

--- y

--t J _q

_ ~ I - Q n L-

Vacuum

(in II~) 7

-l

J )

J

) )

I J

Probe Temp

(F) t-J(

Dox Temp

(F) IA

Temp

ff) __ _ 2

I A

(o i 1

IA - C _ ~

tA) _ L-

C I

I l I

(

I _

I II)-I I _

I ~ (

ltgtl(1

1 _vc 111 ~ l A- bull J ~



l

lt l

I ~ _ tt

I Lbull j I

( lt L

t -lt C ( r

( (

l t IJ

I I CJ I I I

I t I I I

7 J--7 -i -fj - 1-

7 --1l J 7)

_)

1 )

J

v w

CL

(G _J

~lt-I-~

[Jou9 0 w u--~ Di


fl V 1 ~

l

Plant

Date

- -bull




amp J -)_ 5 ~

O C rs--rp









_+ J


t~ ----

( I ((

FIELD DATA


~degfmiddotk


t Factor l L





middot1 C

bull I I I

I bull 0 ()


I I I

lh ltLt _L(


(F) Ii l

~ I

-J J-middot

tmiddotL t jI



(I) 7lt -~ i bull

f cJ I O lt Ibull f

ft IN I ILI 1J

l bull pound IL

I-I

1 I-

1 -- I

X) J 1 -L-- IJ 1 I


I bull

- d 0

) P ( ampI


l l-t--J L _ c_c l~

I 1

) -bullt I I

I I I

I -- I

c ) c 1- I ~ Ihl t

) (J I -~ r1 J - I ____ middot

Ibull r (

I () I rl

- -

Idlt- ~ -


I 11 J - I

bull I


r middotmiddotbull

I I

C I IrJ (_


bull J ( I

_ middot1 1 -

degta Uj MU

I

middot

- -

Plant __ ~






n A I 11 10

m ~



0 )) l I~ Jgtlgt) )( - I I I



- I Lgti- 1 --I - I I I


l


( 7I If I I I - ) I I l I -

FIELD DATA





6-t nLt



LUI Ts




It l ~-~

- I ) -c-1-J 1 J(

~

-rt I

1 ---i )I 1 )A

-u rbull-c _ i ~


1 5 l1 ~u ~ ~

Desired I [)c

I J tt I ( lt

lltf l l ti( 1

ltLf I 11

bull1 lu

r

111 1 ~


I e- 11 I)

( r ID

1tv llv 10l

I( I L-0

I CA


I I 0 I 11J

1 7



FACILITY

SOURCE

DATE r2f J

RUN

METHOD

BOX


I

2

3

4

DI WATER

DJWATER

EMPTY

SILICA GEL


s- J (

_ 0

I 1-- t


INITALS v


FACILITY

SOURCE

DATE rhlrr

RUN

METHOD

BOX rL

IMPINGER CONTENTS

1 DI WATER

7

2

3

DI WATER

EMPTY

4 SILICA GEL

FINAL

GRJIS

foo1


INITIAL

GRAMS

TOTAL

GRMS

I lt -( J t---

S-gt

INTTALS d7

0


FAC[LITY

SOURCE

DATE

RUN

METHOD

BOX


GRltJ~IS GRltMS

I

2

3

4

DI WATER

DI WATER

EMPTY

SILICA GEL


INITALS

TOTAL

GR~IS

J)

O-)

r-

~-(












- -

FIELD DATA


Date ~ () ~ f 9













lfJ D 1 H I

~ r -1 l l I [) ) J_JIC ~ I INl ) - ( I~()

) l I IV i-lt middot ) 1 - 0~ ) Y -11








_ I 11 - yen c-Y - _ - ~

- -to-1i 5 6 deg1

__ __________ _



Run Number ____c= _ _______



I




~ l ~ l lol X o



~~-I j1 vbull- ~JI






I I c Iv I l 1-1 11 -

v-1 Dll - ~



FIELD DATA









Stack Temp

Ts (F) ti( I 11

lt j

(

I




Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(


bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l


I IP I 7

I Lfo )


t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~


- I (() -J~

c f --- -

I

) clbull


1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








I

FIELD DATA






Number 8 Vm rs m



I 1I

114 t11

~tl0 -gt () -Z gt

bull l bull

-n-_

ZIH

C l

ltt

11-Z9 Ii lC

11- i

-zc-o

QtC


t 10

I Igt bull Z

gt 1-

-

~(

c io l

l- 1- 0 ltI

I l6


)

11 i (


)

t

6 IIJS It1

l~t 0 ~bull--11 ~1

~~~ (J

fc 4 v Sli 3

I t--~ Ibull

C

-O It 1 Iu

l4o 4 05

jlal 0

5Ca i oo-t i l --













Ill I 0fiu

~~ middot~ y I





Actual l I c)

cp 1(deg

tamp bull-

lO II lI l I A



-

Stack Temp

Ts (F)

0--1 li z

j(

- II



~ J bullbull

FIELD DATA

Planl Date

fo-l P~MT-Li 1o i t



-middot -I


~



l _

( ~ -z1



-1 o - S IJ P



I



0

m

1




Desired l 0 I ltt

bull llt zr-


(f) Bi i

o

(f) IAlt~

gtmiddot~

(F) l_ 2-

(in Ilg) ro 30 0 o

(F) i-

(f) A

ff) (0

(o

uO ( 0

~ I

n-

1t 11

14 q JJ IAlI~

I co

Slll1 ~10J 1l1 l

I bull t d

bull Z tItr

I 1-bull zr-bull1 (

ttl o- l08

I10 if iJ

pound I

ll iu

gt lo ~tgt

r rJ -i- ll


4 (

_


51-l i l~~I Sl~ 1

P~ 11S 3

(lIO



Ibull 1 I bull1 I 1

II l middot-l

I(

i ) I lS ir

I 3pound 1 H


I I 7 I

lu~ lotgt l l




J-0 middot 0

middot1 0 0

ZO lO middotro


lt u

lIJI

10~ l 1

tlli 111

1i-01-1111 t (Z t tz~


h1 ~ I I -

1t bull I t

(oI~

-

Ill

tr-It l I (1-

Bt BIz-

RI H t ~~ -

LO 7 b

1ltgt- I

15s ---

u[ ~a uyL

l-1 bull e r To 105 I 1~] ((11 ~IIi

55 uu

81

r~=-~~~ ~o-- --ts==




- --- -middotmiddot------------c= ~

j- l r ln c lt_--= -3

- ___ ~ n middot~------ ~- A t ~~ C - Cl



Smiddot l

L

3

-I

S

(

B - I

2

middot3

y

s (

Q -

1

)

ltt

s-(


0

5

s-~

0 3

t)

5 3 ~

2-2--

2

s s

3 1

0


Sc ~i c - 111 le C ~

~ 1

1 t

I

~Z

T a T

I I

03 I

T




I I I I I I I I I


sect388



CATE -2C-qo








C 1

-C]-z I

l ( r 3

J_ c v v

r I c -1






PORT LO CATION

OISTAICE FROM

EDGE


2

3

3--4-- ~-i

bullI amp 6 io

1 B

i 0 I middotB C

-middot 11- 3 l3

i

s

~ 112

--tt Ill 0 ~

117-

I I

b 0

I

TRAVERSE

NUMBER OF STACK



FACIIITY

SOURCE

DATE

RUN

METHOD

BOX


GR6--IS

INITLU

GRAMS

r

TOTAL

GRMS






INITALS


FACIJITY

SOURCE

DATE

RUN

METHOD

BOX


GRJ-15 GR-15 GRJ-15

I

2

3

4

DI WATER

DI WATER

EMPIT

SILICA GEL

2--Z

~-~

o ~ (


INITALS


FACIIITY

SOURCE

DATE

RUN

METHOD we zrJ BOX


GR-1S GRMS

IIf

~D

I DIWATER

GRltJ-IS

e

2

3

4

DI WATER

EMPTY

SILICA GEL

I 0

IS--L


INITALS



FACfIITY

SOURCE

DATE

RUN

METHOD

BOX


GRJ-1S

I DI WATER

2 DI WATER

3 EMPTY

4 SILICA GEL

GRJ1S

t~c

Sf

GRJ-IS

-o~z -og

-o J

-02


INlTALS t

NOMENCLATURE




g ft3




1



letgt +460) ( -ZHmiddot+( 1 136))

8 1 + 460) (2992)




Vwstd = (00000894)( v B + 460)( Lf2 - )

Vwstd = ____I_~----q___


Bwo = 100 ( middot t 1 ) ( 4 + t S 781 )

Bwo= ------

2



MWd = (032 x 1- 010 ) + (044 x O O 1 ) + (028 x ( O + +I Ci ))


MWw = (MWd) (1 - BWo 100) + 18 ((BWo 100))

MWw = ( -Z 6- B-1) (1--Z -S- 100) + (18 ( z s-( 100))

(5) VELOCITY (Vs)

460Vs = 8549 x CP x ~ x ___Ts_+_- ----=-Ps

(Mw_) X (Bp + 136)

( 0 Ca + 460)vs = 8549 x ( o e- ) x ( 1 o 1 0 ) x 1----------------------

( -Z8- St ) X ( 2 degt ) tdeg + 0 C l )136

Vs= (po 9J

3


As = (Ds)2

x (31416) 576

( ) 2

X (31416)As=--------------~

576

As= ----


As = (L) (W) 144

As=( le ) ( I e ) I 144

As= -1B-------=--


ACFM = (Vs) (60) x (As)


ACFM =--~_5_0---CS-___

4



( ( R +460) ( 21+f) + ( 6u ~ I 136))X----=Ua__~X------------=-~--~

( o v +460) 2992




DSCFM= ( vO-l~ )x(l --z-~ 100)

DSCFM = ___-s_9_S_9__

(11) ISOKINETIC ()


60 x 0 x Vs x (Ps 136 + Pb) (Dn2 x 0005454)




5



mg Ni DSCM = ( 1- ~ ) I~ ( 7i8r ) X (0028317)



DSCF 1000






6

APPENDIX A-2











FIELD DATA



~ Fl Meter Della ll


1






I



Point Number

t t J V middotr IA

I 1

J I r lt

Time Time e





Reneling Vm



Head Ps


I u j bull -


I U 1






I - Lu

Temp Ts (F) lcD

o- 0~

~y oc

0~ middotbull ti -

Io - l6

Inlet Tmin

(F) t middot-t~ ~

- igt o j7r--

--7~-7

Outlet Tm out

(F) 1-

--- y

--t J _q

_ ~ I - Q n L-

Vacuum

(in II~) 7

-l

J )

J

) )

I J

Probe Temp

(F) t-J(

Dox Temp

(F) IA

Temp

ff) __ _ 2

I A

(o i 1

IA - C _ ~

tA) _ L-

C I

I l I

(

I _

I II)-I I _

I ~ (

ltgtl(1

1 _vc 111 ~ l A- bull J ~



l

lt l

I ~ _ tt

I Lbull j I

( lt L

t -lt C ( r

( (

l t IJ

I I CJ I I I

I t I I I

7 J--7 -i -fj - 1-

7 --1l J 7)

_)

1 )

J

v w

CL

(G _J

~lt-I-~

[Jou9 0 w u--~ Di


fl V 1 ~

l

Plant

Date

- -bull




amp J -)_ 5 ~

O C rs--rp









_+ J


t~ ----

( I ((

FIELD DATA


~degfmiddotk


t Factor l L





middot1 C

bull I I I

I bull 0 ()


I I I

lh ltLt _L(


(F) Ii l

~ I

-J J-middot

tmiddotL t jI



(I) 7lt -~ i bull

f cJ I O lt Ibull f

ft IN I ILI 1J

l bull pound IL

I-I

1 I-

1 -- I

X) J 1 -L-- IJ 1 I


I bull

- d 0

) P ( ampI


l l-t--J L _ c_c l~

I 1

) -bullt I I

I I I

I -- I

c ) c 1- I ~ Ihl t

) (J I -~ r1 J - I ____ middot

Ibull r (

I () I rl

- -

Idlt- ~ -


I 11 J - I

bull I


r middotmiddotbull

I I

C I IrJ (_


bull J ( I

_ middot1 1 -

degta Uj MU

I

middot

- -

Plant __ ~






n A I 11 10

m ~



0 )) l I~ Jgtlgt) )( - I I I



- I Lgti- 1 --I - I I I


l


( 7I If I I I - ) I I l I -

FIELD DATA





6-t nLt



LUI Ts




It l ~-~

- I ) -c-1-J 1 J(

~

-rt I

1 ---i )I 1 )A

-u rbull-c _ i ~


1 5 l1 ~u ~ ~

Desired I [)c

I J tt I ( lt

lltf l l ti( 1

ltLf I 11

bull1 lu

r

111 1 ~


I e- 11 I)

( r ID

1tv llv 10l

I( I L-0

I CA


I I 0 I 11J

1 7



FACILITY

SOURCE

DATE r2f J

RUN

METHOD

BOX


I

2

3

4

DI WATER

DJWATER

EMPTY

SILICA GEL


s- J (

_ 0

I 1-- t


INITALS v


FACILITY

SOURCE

DATE rhlrr

RUN

METHOD

BOX rL

IMPINGER CONTENTS

1 DI WATER

7

2

3

DI WATER

EMPTY

4 SILICA GEL

FINAL

GRJIS

foo1


INITIAL

GRAMS

TOTAL

GRMS

I lt -( J t---

S-gt

INTTALS d7

0


FAC[LITY

SOURCE

DATE

RUN

METHOD

BOX


GRltJ~IS GRltMS

I

2

3

4

DI WATER

DI WATER

EMPTY

SILICA GEL


INITALS

TOTAL

GR~IS

J)

O-)

r-

~-(












- -

FIELD DATA


Date ~ () ~ f 9













lfJ D 1 H I

~ r -1 l l I [) ) J_JIC ~ I INl ) - ( I~()

) l I IV i-lt middot ) 1 - 0~ ) Y -11








_ I 11 - yen c-Y - _ - ~

- -to-1i 5 6 deg1

__ __________ _



Run Number ____c= _ _______



I




~ l ~ l lol X o



~~-I j1 vbull- ~JI






I I c Iv I l 1-1 11 -

v-1 Dll - ~



FIELD DATA









Stack Temp

Ts (F) ti( I 11

lt j

(

I




Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(


bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l


I IP I 7

I Lfo )


t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~


- I (() -J~

c f --- -

I

) clbull


1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








FIELD DATA

Planl Date

fo-l P~MT-Li 1o i t



-middot -I


~



l _

( ~ -z1



-1 o - S IJ P



I



0

m

1




Desired l 0 I ltt

bull llt zr-


(f) Bi i

o

(f) IAlt~

gtmiddot~

(F) l_ 2-

(in Ilg) ro 30 0 o

(F) i-

(f) A

ff) (0

(o

uO ( 0

~ I

n-

1t 11

14 q JJ IAlI~

I co

Slll1 ~10J 1l1 l

I bull t d

bull Z tItr

I 1-bull zr-bull1 (

ttl o- l08

I10 if iJ

pound I

ll iu

gt lo ~tgt

r rJ -i- ll


4 (

_


51-l i l~~I Sl~ 1

P~ 11S 3

(lIO



Ibull 1 I bull1 I 1

II l middot-l

I(

i ) I lS ir

I 3pound 1 H


I I 7 I

lu~ lotgt l l




J-0 middot 0

middot1 0 0

ZO lO middotro


lt u

lIJI

10~ l 1

tlli 111

1i-01-1111 t (Z t tz~


h1 ~ I I -

1t bull I t

(oI~

-

Ill

tr-It l I (1-

Bt BIz-

RI H t ~~ -

LO 7 b

1ltgt- I

15s ---

u[ ~a uyL

l-1 bull e r To 105 I 1~] ((11 ~IIi

55 uu

81

r~=-~~~ ~o-- --ts==




- --- -middotmiddot------------c= ~

j- l r ln c lt_--= -3

- ___ ~ n middot~------ ~- A t ~~ C - Cl



Smiddot l

L

3

-I

S

(

B - I

2

middot3

y

s (

Q -

1

)

ltt

s-(


0

5

s-~

0 3

t)

5 3 ~

2-2--

2

s s

3 1

0


Sc ~i c - 111 le C ~

~ 1

1 t

I

~Z

T a T

I I

03 I

T




I I I I I I I I I


sect388



CATE -2C-qo








C 1

-C]-z I

l ( r 3

J_ c v v

r I c -1






PORT LO CATION

OISTAICE FROM

EDGE


2

3

3--4-- ~-i

bullI amp 6 io

1 B

i 0 I middotB C

-middot 11- 3 l3

i

s

~ 112

--tt Ill 0 ~

117-

I I

b 0

I

TRAVERSE

NUMBER OF STACK



FACIIITY

SOURCE

DATE

RUN

METHOD

BOX


GR6--IS

INITLU

GRAMS

r

TOTAL

GRMS






INITALS


FACIJITY

SOURCE

DATE

RUN

METHOD

BOX


GRJ-15 GR-15 GRJ-15

I

2

3

4

DI WATER

DI WATER

EMPIT

SILICA GEL

2--Z

~-~

o ~ (


INITALS


FACIIITY

SOURCE

DATE

RUN

METHOD we zrJ BOX


GR-1S GRMS

IIf

~D

I DIWATER

GRltJ-IS

e

2

3

4

DI WATER

EMPTY

SILICA GEL

I 0

IS--L


INITALS



FACfIITY

SOURCE

DATE

RUN

METHOD

BOX


GRJ-1S

I DI WATER

2 DI WATER

3 EMPTY

4 SILICA GEL

GRJ1S

t~c

Sf

GRJ-IS

-o~z -og

-o J

-02


INlTALS t

NOMENCLATURE




g ft3




1



letgt +460) ( -ZHmiddot+( 1 136))

8 1 + 460) (2992)




Vwstd = (00000894)( v B + 460)( Lf2 - )

Vwstd = ____I_~----q___


Bwo = 100 ( middot t 1 ) ( 4 + t S 781 )

Bwo= ------

2



MWd = (032 x 1- 010 ) + (044 x O O 1 ) + (028 x ( O + +I Ci ))


MWw = (MWd) (1 - BWo 100) + 18 ((BWo 100))

MWw = ( -Z 6- B-1) (1--Z -S- 100) + (18 ( z s-( 100))

(5) VELOCITY (Vs)

460Vs = 8549 x CP x ~ x ___Ts_+_- ----=-Ps

(Mw_) X (Bp + 136)

( 0 Ca + 460)vs = 8549 x ( o e- ) x ( 1 o 1 0 ) x 1----------------------

( -Z8- St ) X ( 2 degt ) tdeg + 0 C l )136

Vs= (po 9J

3


As = (Ds)2

x (31416) 576

( ) 2

X (31416)As=--------------~

576

As= ----


As = (L) (W) 144

As=( le ) ( I e ) I 144

As= -1B-------=--


ACFM = (Vs) (60) x (As)


ACFM =--~_5_0---CS-___

4



( ( R +460) ( 21+f) + ( 6u ~ I 136))X----=Ua__~X------------=-~--~

( o v +460) 2992




DSCFM= ( vO-l~ )x(l --z-~ 100)

DSCFM = ___-s_9_S_9__

(11) ISOKINETIC ()


60 x 0 x Vs x (Ps 136 + Pb) (Dn2 x 0005454)




5



mg Ni DSCM = ( 1- ~ ) I~ ( 7i8r ) X (0028317)



DSCF 1000






6

APPENDIX A-2











FIELD DATA



~ Fl Meter Della ll


1






I



Point Number

t t J V middotr IA

I 1

J I r lt

Time Time e





Reneling Vm



Head Ps


I u j bull -


I U 1






I - Lu

Temp Ts (F) lcD

o- 0~

~y oc

0~ middotbull ti -

Io - l6

Inlet Tmin

(F) t middot-t~ ~

- igt o j7r--

--7~-7

Outlet Tm out

(F) 1-

--- y

--t J _q

_ ~ I - Q n L-

Vacuum

(in II~) 7

-l

J )

J

) )

I J

Probe Temp

(F) t-J(

Dox Temp

(F) IA

Temp

ff) __ _ 2

I A

(o i 1

IA - C _ ~

tA) _ L-

C I

I l I

(

I _

I II)-I I _

I ~ (

ltgtl(1

1 _vc 111 ~ l A- bull J ~



l

lt l

I ~ _ tt

I Lbull j I

( lt L

t -lt C ( r

( (

l t IJ

I I CJ I I I

I t I I I

7 J--7 -i -fj - 1-

7 --1l J 7)

_)

1 )

J

v w

CL

(G _J

~lt-I-~

[Jou9 0 w u--~ Di


fl V 1 ~

l

Plant

Date

- -bull




amp J -)_ 5 ~

O C rs--rp









_+ J


t~ ----

( I ((

FIELD DATA


~degfmiddotk


t Factor l L





middot1 C

bull I I I

I bull 0 ()


I I I

lh ltLt _L(


(F) Ii l

~ I

-J J-middot

tmiddotL t jI



(I) 7lt -~ i bull

f cJ I O lt Ibull f

ft IN I ILI 1J

l bull pound IL

I-I

1 I-

1 -- I

X) J 1 -L-- IJ 1 I


I bull

- d 0

) P ( ampI


l l-t--J L _ c_c l~

I 1

) -bullt I I

I I I

I -- I

c ) c 1- I ~ Ihl t

) (J I -~ r1 J - I ____ middot

Ibull r (

I () I rl

- -

Idlt- ~ -


I 11 J - I

bull I


r middotmiddotbull

I I

C I IrJ (_


bull J ( I

_ middot1 1 -

degta Uj MU

I

middot

- -

Plant __ ~






n A I 11 10

m ~



0 )) l I~ Jgtlgt) )( - I I I



- I Lgti- 1 --I - I I I


l


( 7I If I I I - ) I I l I -

FIELD DATA





6-t nLt



LUI Ts




It l ~-~

- I ) -c-1-J 1 J(

~

-rt I

1 ---i )I 1 )A

-u rbull-c _ i ~


1 5 l1 ~u ~ ~

Desired I [)c

I J tt I ( lt

lltf l l ti( 1

ltLf I 11

bull1 lu

r

111 1 ~


I e- 11 I)

( r ID

1tv llv 10l

I( I L-0

I CA


I I 0 I 11J

1 7



FACILITY

SOURCE

DATE r2f J

RUN

METHOD

BOX


I

2

3

4

DI WATER

DJWATER

EMPTY

SILICA GEL


s- J (

_ 0

I 1-- t


INITALS v


FACILITY

SOURCE

DATE rhlrr

RUN

METHOD

BOX rL

IMPINGER CONTENTS

1 DI WATER

7

2

3

DI WATER

EMPTY

4 SILICA GEL

FINAL

GRJIS

foo1


INITIAL

GRAMS

TOTAL

GRMS

I lt -( J t---

S-gt

INTTALS d7

0


FAC[LITY

SOURCE

DATE

RUN

METHOD

BOX


GRltJ~IS GRltMS

I

2

3

4

DI WATER

DI WATER

EMPTY

SILICA GEL


INITALS

TOTAL

GR~IS

J)

O-)

r-

~-(












- -

FIELD DATA


Date ~ () ~ f 9













lfJ D 1 H I

~ r -1 l l I [) ) J_JIC ~ I INl ) - ( I~()

) l I IV i-lt middot ) 1 - 0~ ) Y -11








_ I 11 - yen c-Y - _ - ~

- -to-1i 5 6 deg1

__ __________ _



Run Number ____c= _ _______



I




~ l ~ l lol X o



~~-I j1 vbull- ~JI






I I c Iv I l 1-1 11 -

v-1 Dll - ~



FIELD DATA









Stack Temp

Ts (F) ti( I 11

lt j

(

I




Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(


bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l


I IP I 7

I Lfo )


t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~


- I (() -J~

c f --- -

I

) clbull


1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








r~=-~~~ ~o-- --ts==




- --- -middotmiddot------------c= ~

j- l r ln c lt_--= -3

- ___ ~ n middot~------ ~- A t ~~ C - Cl



Smiddot l

L

3

-I

S

(

B - I

2

middot3

y

s (

Q -

1

)

ltt

s-(


0

5

s-~

0 3

t)

5 3 ~

2-2--

2

s s

3 1

0


Sc ~i c - 111 le C ~

~ 1

1 t

I

~Z

T a T

I I

03 I

T




I I I I I I I I I


sect388



CATE -2C-qo








C 1

-C]-z I

l ( r 3

J_ c v v

r I c -1






PORT LO CATION

OISTAICE FROM

EDGE


2

3

3--4-- ~-i

bullI amp 6 io

1 B

i 0 I middotB C

-middot 11- 3 l3

i

s

~ 112

--tt Ill 0 ~

117-

I I

b 0

I

TRAVERSE

NUMBER OF STACK



FACIIITY

SOURCE

DATE

RUN

METHOD

BOX


GR6--IS

INITLU

GRAMS

r

TOTAL

GRMS






INITALS


FACIJITY

SOURCE

DATE

RUN

METHOD

BOX


GRJ-15 GR-15 GRJ-15

I

2

3

4

DI WATER

DI WATER

EMPIT

SILICA GEL

2--Z

~-~

o ~ (


INITALS


FACIIITY

SOURCE

DATE

RUN

METHOD we zrJ BOX


GR-1S GRMS

IIf

~D

I DIWATER

GRltJ-IS

e

2

3

4

DI WATER

EMPTY

SILICA GEL

I 0

IS--L


INITALS



FACfIITY

SOURCE

DATE

RUN

METHOD

BOX


GRJ-1S

I DI WATER

2 DI WATER

3 EMPTY

4 SILICA GEL

GRJ1S

t~c

Sf

GRJ-IS

-o~z -og

-o J

-02


INlTALS t

NOMENCLATURE




g ft3




1



letgt +460) ( -ZHmiddot+( 1 136))

8 1 + 460) (2992)




Vwstd = (00000894)( v B + 460)( Lf2 - )

Vwstd = ____I_~----q___


Bwo = 100 ( middot t 1 ) ( 4 + t S 781 )

Bwo= ------

2



MWd = (032 x 1- 010 ) + (044 x O O 1 ) + (028 x ( O + +I Ci ))


MWw = (MWd) (1 - BWo 100) + 18 ((BWo 100))

MWw = ( -Z 6- B-1) (1--Z -S- 100) + (18 ( z s-( 100))

(5) VELOCITY (Vs)

460Vs = 8549 x CP x ~ x ___Ts_+_- ----=-Ps

(Mw_) X (Bp + 136)

( 0 Ca + 460)vs = 8549 x ( o e- ) x ( 1 o 1 0 ) x 1----------------------

( -Z8- St ) X ( 2 degt ) tdeg + 0 C l )136

Vs= (po 9J

3


As = (Ds)2

x (31416) 576

( ) 2

X (31416)As=--------------~

576

As= ----


As = (L) (W) 144

As=( le ) ( I e ) I 144

As= -1B-------=--


ACFM = (Vs) (60) x (As)


ACFM =--~_5_0---CS-___

4



( ( R +460) ( 21+f) + ( 6u ~ I 136))X----=Ua__~X------------=-~--~

( o v +460) 2992




DSCFM= ( vO-l~ )x(l --z-~ 100)

DSCFM = ___-s_9_S_9__

(11) ISOKINETIC ()


60 x 0 x Vs x (Ps 136 + Pb) (Dn2 x 0005454)




5



mg Ni DSCM = ( 1- ~ ) I~ ( 7i8r ) X (0028317)



DSCF 1000






6

APPENDIX A-2











FIELD DATA



~ Fl Meter Della ll


1






I



Point Number

t t J V middotr IA

I 1

J I r lt

Time Time e





Reneling Vm



Head Ps


I u j bull -


I U 1






I - Lu

Temp Ts (F) lcD

o- 0~

~y oc

0~ middotbull ti -

Io - l6

Inlet Tmin

(F) t middot-t~ ~

- igt o j7r--

--7~-7

Outlet Tm out

(F) 1-

--- y

--t J _q

_ ~ I - Q n L-

Vacuum

(in II~) 7

-l

J )

J

) )

I J

Probe Temp

(F) t-J(

Dox Temp

(F) IA

Temp

ff) __ _ 2

I A

(o i 1

IA - C _ ~

tA) _ L-

C I

I l I

(

I _

I II)-I I _

I ~ (

ltgtl(1

1 _vc 111 ~ l A- bull J ~



l

lt l

I ~ _ tt

I Lbull j I

( lt L

t -lt C ( r

( (

l t IJ

I I CJ I I I

I t I I I

7 J--7 -i -fj - 1-

7 --1l J 7)

_)

1 )

J

v w

CL

(G _J

~lt-I-~

[Jou9 0 w u--~ Di


fl V 1 ~

l

Plant

Date

- -bull




amp J -)_ 5 ~

O C rs--rp









_+ J


t~ ----

( I ((

FIELD DATA


~degfmiddotk


t Factor l L





middot1 C

bull I I I

I bull 0 ()


I I I

lh ltLt _L(


(F) Ii l

~ I

-J J-middot

tmiddotL t jI



(I) 7lt -~ i bull

f cJ I O lt Ibull f

ft IN I ILI 1J

l bull pound IL

I-I

1 I-

1 -- I

X) J 1 -L-- IJ 1 I


I bull

- d 0

) P ( ampI


l l-t--J L _ c_c l~

I 1

) -bullt I I

I I I

I -- I

c ) c 1- I ~ Ihl t

) (J I -~ r1 J - I ____ middot

Ibull r (

I () I rl

- -

Idlt- ~ -


I 11 J - I

bull I


r middotmiddotbull

I I

C I IrJ (_


bull J ( I

_ middot1 1 -

degta Uj MU

I

middot

- -

Plant __ ~






n A I 11 10

m ~



0 )) l I~ Jgtlgt) )( - I I I



- I Lgti- 1 --I - I I I


l


( 7I If I I I - ) I I l I -

FIELD DATA





6-t nLt



LUI Ts




It l ~-~

- I ) -c-1-J 1 J(

~

-rt I

1 ---i )I 1 )A

-u rbull-c _ i ~


1 5 l1 ~u ~ ~

Desired I [)c

I J tt I ( lt

lltf l l ti( 1

ltLf I 11

bull1 lu

r

111 1 ~


I e- 11 I)

( r ID

1tv llv 10l

I( I L-0

I CA


I I 0 I 11J

1 7



FACILITY

SOURCE

DATE r2f J

RUN

METHOD

BOX


I

2

3

4

DI WATER

DJWATER

EMPTY

SILICA GEL


s- J (

_ 0

I 1-- t


INITALS v


FACILITY

SOURCE

DATE rhlrr

RUN

METHOD

BOX rL

IMPINGER CONTENTS

1 DI WATER

7

2

3

DI WATER

EMPTY

4 SILICA GEL

FINAL

GRJIS

foo1


INITIAL

GRAMS

TOTAL

GRMS

I lt -( J t---

S-gt

INTTALS d7

0


FAC[LITY

SOURCE

DATE

RUN

METHOD

BOX


GRltJ~IS GRltMS

I

2

3

4

DI WATER

DI WATER

EMPTY

SILICA GEL


INITALS

TOTAL

GR~IS

J)

O-)

r-

~-(












- -

FIELD DATA


Date ~ () ~ f 9













lfJ D 1 H I

~ r -1 l l I [) ) J_JIC ~ I INl ) - ( I~()

) l I IV i-lt middot ) 1 - 0~ ) Y -11








_ I 11 - yen c-Y - _ - ~

- -to-1i 5 6 deg1

__ __________ _



Run Number ____c= _ _______



I




~ l ~ l lol X o



~~-I j1 vbull- ~JI






I I c Iv I l 1-1 11 -

v-1 Dll - ~



FIELD DATA









Stack Temp

Ts (F) ti( I 11

lt j

(

I




Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(


bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l


I IP I 7

I Lfo )


t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~


- I (() -J~

c f --- -

I

) clbull


1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








sect388



CATE -2C-qo








C 1

-C]-z I

l ( r 3

J_ c v v

r I c -1






PORT LO CATION

OISTAICE FROM

EDGE


2

3

3--4-- ~-i

bullI amp 6 io

1 B

i 0 I middotB C

-middot 11- 3 l3

i

s

~ 112

--tt Ill 0 ~

117-

I I

b 0

I

TRAVERSE

NUMBER OF STACK



FACIIITY

SOURCE

DATE

RUN

METHOD

BOX


GR6--IS

INITLU

GRAMS

r

TOTAL

GRMS






INITALS


FACIJITY

SOURCE

DATE

RUN

METHOD

BOX


GRJ-15 GR-15 GRJ-15

I

2

3

4

DI WATER

DI WATER

EMPIT

SILICA GEL

2--Z

~-~

o ~ (


INITALS


FACIIITY

SOURCE

DATE

RUN

METHOD we zrJ BOX


GR-1S GRMS

IIf

~D

I DIWATER

GRltJ-IS

e

2

3

4

DI WATER

EMPTY

SILICA GEL

I 0

IS--L


INITALS



FACfIITY

SOURCE

DATE

RUN

METHOD

BOX


GRJ-1S

I DI WATER

2 DI WATER

3 EMPTY

4 SILICA GEL

GRJ1S

t~c

Sf

GRJ-IS

-o~z -og

-o J

-02


INlTALS t

NOMENCLATURE




g ft3




1



letgt +460) ( -ZHmiddot+( 1 136))

8 1 + 460) (2992)




Vwstd = (00000894)( v B + 460)( Lf2 - )

Vwstd = ____I_~----q___


Bwo = 100 ( middot t 1 ) ( 4 + t S 781 )

Bwo= ------

2



MWd = (032 x 1- 010 ) + (044 x O O 1 ) + (028 x ( O + +I Ci ))


MWw = (MWd) (1 - BWo 100) + 18 ((BWo 100))

MWw = ( -Z 6- B-1) (1--Z -S- 100) + (18 ( z s-( 100))

(5) VELOCITY (Vs)

460Vs = 8549 x CP x ~ x ___Ts_+_- ----=-Ps

(Mw_) X (Bp + 136)

( 0 Ca + 460)vs = 8549 x ( o e- ) x ( 1 o 1 0 ) x 1----------------------

( -Z8- St ) X ( 2 degt ) tdeg + 0 C l )136

Vs= (po 9J

3


As = (Ds)2

x (31416) 576

( ) 2

X (31416)As=--------------~

576

As= ----


As = (L) (W) 144

As=( le ) ( I e ) I 144

As= -1B-------=--


ACFM = (Vs) (60) x (As)


ACFM =--~_5_0---CS-___

4



( ( R +460) ( 21+f) + ( 6u ~ I 136))X----=Ua__~X------------=-~--~

( o v +460) 2992




DSCFM= ( vO-l~ )x(l --z-~ 100)

DSCFM = ___-s_9_S_9__

(11) ISOKINETIC ()


60 x 0 x Vs x (Ps 136 + Pb) (Dn2 x 0005454)




5



mg Ni DSCM = ( 1- ~ ) I~ ( 7i8r ) X (0028317)



DSCF 1000






6

APPENDIX A-2











FIELD DATA



~ Fl Meter Della ll


1






I



Point Number

t t J V middotr IA

I 1

J I r lt

Time Time e





Reneling Vm



Head Ps


I u j bull -


I U 1






I - Lu

Temp Ts (F) lcD

o- 0~

~y oc

0~ middotbull ti -

Io - l6

Inlet Tmin

(F) t middot-t~ ~

- igt o j7r--

--7~-7

Outlet Tm out

(F) 1-

--- y

--t J _q

_ ~ I - Q n L-

Vacuum

(in II~) 7

-l

J )

J

) )

I J

Probe Temp

(F) t-J(

Dox Temp

(F) IA

Temp

ff) __ _ 2

I A

(o i 1

IA - C _ ~

tA) _ L-

C I

I l I

(

I _

I II)-I I _

I ~ (

ltgtl(1

1 _vc 111 ~ l A- bull J ~



l

lt l

I ~ _ tt

I Lbull j I

( lt L

t -lt C ( r

( (

l t IJ

I I CJ I I I

I t I I I

7 J--7 -i -fj - 1-

7 --1l J 7)

_)

1 )

J

v w

CL

(G _J

~lt-I-~

[Jou9 0 w u--~ Di


fl V 1 ~

l

Plant

Date

- -bull




amp J -)_ 5 ~

O C rs--rp









_+ J


t~ ----

( I ((

FIELD DATA


~degfmiddotk


t Factor l L





middot1 C

bull I I I

I bull 0 ()


I I I

lh ltLt _L(


(F) Ii l

~ I

-J J-middot

tmiddotL t jI



(I) 7lt -~ i bull

f cJ I O lt Ibull f

ft IN I ILI 1J

l bull pound IL

I-I

1 I-

1 -- I

X) J 1 -L-- IJ 1 I


I bull

- d 0

) P ( ampI


l l-t--J L _ c_c l~

I 1

) -bullt I I

I I I

I -- I

c ) c 1- I ~ Ihl t

) (J I -~ r1 J - I ____ middot

Ibull r (

I () I rl

- -

Idlt- ~ -


I 11 J - I

bull I


r middotmiddotbull

I I

C I IrJ (_


bull J ( I

_ middot1 1 -

degta Uj MU

I

middot

- -

Plant __ ~






n A I 11 10

m ~



0 )) l I~ Jgtlgt) )( - I I I



- I Lgti- 1 --I - I I I


l


( 7I If I I I - ) I I l I -

FIELD DATA





6-t nLt



LUI Ts




It l ~-~

- I ) -c-1-J 1 J(

~

-rt I

1 ---i )I 1 )A

-u rbull-c _ i ~


1 5 l1 ~u ~ ~

Desired I [)c

I J tt I ( lt

lltf l l ti( 1

ltLf I 11

bull1 lu

r

111 1 ~


I e- 11 I)

( r ID

1tv llv 10l

I( I L-0

I CA


I I 0 I 11J

1 7



FACILITY

SOURCE

DATE r2f J

RUN

METHOD

BOX


I

2

3

4

DI WATER

DJWATER

EMPTY

SILICA GEL


s- J (

_ 0

I 1-- t


INITALS v


FACILITY

SOURCE

DATE rhlrr

RUN

METHOD

BOX rL

IMPINGER CONTENTS

1 DI WATER

7

2

3

DI WATER

EMPTY

4 SILICA GEL

FINAL

GRJIS

foo1


INITIAL

GRAMS

TOTAL

GRMS

I lt -( J t---

S-gt

INTTALS d7

0


FAC[LITY

SOURCE

DATE

RUN

METHOD

BOX


GRltJ~IS GRltMS

I

2

3

4

DI WATER

DI WATER

EMPTY

SILICA GEL


INITALS

TOTAL

GR~IS

J)

O-)

r-

~-(












- -

FIELD DATA


Date ~ () ~ f 9













lfJ D 1 H I

~ r -1 l l I [) ) J_JIC ~ I INl ) - ( I~()

) l I IV i-lt middot ) 1 - 0~ ) Y -11








_ I 11 - yen c-Y - _ - ~

- -to-1i 5 6 deg1

__ __________ _



Run Number ____c= _ _______



I




~ l ~ l lol X o



~~-I j1 vbull- ~JI






I I c Iv I l 1-1 11 -

v-1 Dll - ~



FIELD DATA









Stack Temp

Ts (F) ti( I 11

lt j

(

I




Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(


bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l


I IP I 7

I Lfo )


t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~


- I (() -J~

c f --- -

I

) clbull


1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation









FACIIITY

SOURCE

DATE

RUN

METHOD

BOX


GR6--IS

INITLU

GRAMS

r

TOTAL

GRMS






INITALS


FACIJITY

SOURCE

DATE

RUN

METHOD

BOX


GRJ-15 GR-15 GRJ-15

I

2

3

4

DI WATER

DI WATER

EMPIT

SILICA GEL

2--Z

~-~

o ~ (


INITALS


FACIIITY

SOURCE

DATE

RUN

METHOD we zrJ BOX


GR-1S GRMS

IIf

~D

I DIWATER

GRltJ-IS

e

2

3

4

DI WATER

EMPTY

SILICA GEL

I 0

IS--L


INITALS



FACfIITY

SOURCE

DATE

RUN

METHOD

BOX


GRJ-1S

I DI WATER

2 DI WATER

3 EMPTY

4 SILICA GEL

GRJ1S

t~c

Sf

GRJ-IS

-o~z -og

-o J

-02


INlTALS t

NOMENCLATURE




g ft3




1



letgt +460) ( -ZHmiddot+( 1 136))

8 1 + 460) (2992)




Vwstd = (00000894)( v B + 460)( Lf2 - )

Vwstd = ____I_~----q___


Bwo = 100 ( middot t 1 ) ( 4 + t S 781 )

Bwo= ------

2



MWd = (032 x 1- 010 ) + (044 x O O 1 ) + (028 x ( O + +I Ci ))


MWw = (MWd) (1 - BWo 100) + 18 ((BWo 100))

MWw = ( -Z 6- B-1) (1--Z -S- 100) + (18 ( z s-( 100))

(5) VELOCITY (Vs)

460Vs = 8549 x CP x ~ x ___Ts_+_- ----=-Ps

(Mw_) X (Bp + 136)

( 0 Ca + 460)vs = 8549 x ( o e- ) x ( 1 o 1 0 ) x 1----------------------

( -Z8- St ) X ( 2 degt ) tdeg + 0 C l )136

Vs= (po 9J

3


As = (Ds)2

x (31416) 576

( ) 2

X (31416)As=--------------~

576

As= ----


As = (L) (W) 144

As=( le ) ( I e ) I 144

As= -1B-------=--


ACFM = (Vs) (60) x (As)


ACFM =--~_5_0---CS-___

4



( ( R +460) ( 21+f) + ( 6u ~ I 136))X----=Ua__~X------------=-~--~

( o v +460) 2992




DSCFM= ( vO-l~ )x(l --z-~ 100)

DSCFM = ___-s_9_S_9__

(11) ISOKINETIC ()


60 x 0 x Vs x (Ps 136 + Pb) (Dn2 x 0005454)




5



mg Ni DSCM = ( 1- ~ ) I~ ( 7i8r ) X (0028317)



DSCF 1000






6

APPENDIX A-2











FIELD DATA



~ Fl Meter Della ll


1






I



Point Number

t t J V middotr IA

I 1

J I r lt

Time Time e





Reneling Vm



Head Ps


I u j bull -


I U 1






I - Lu

Temp Ts (F) lcD

o- 0~

~y oc

0~ middotbull ti -

Io - l6

Inlet Tmin

(F) t middot-t~ ~

- igt o j7r--

--7~-7

Outlet Tm out

(F) 1-

--- y

--t J _q

_ ~ I - Q n L-

Vacuum

(in II~) 7

-l

J )

J

) )

I J

Probe Temp

(F) t-J(

Dox Temp

(F) IA

Temp

ff) __ _ 2

I A

(o i 1

IA - C _ ~

tA) _ L-

C I

I l I

(

I _

I II)-I I _

I ~ (

ltgtl(1

1 _vc 111 ~ l A- bull J ~



l

lt l

I ~ _ tt

I Lbull j I

( lt L

t -lt C ( r

( (

l t IJ

I I CJ I I I

I t I I I

7 J--7 -i -fj - 1-

7 --1l J 7)

_)

1 )

J

v w

CL

(G _J

~lt-I-~

[Jou9 0 w u--~ Di


fl V 1 ~

l

Plant

Date

- -bull




amp J -)_ 5 ~

O C rs--rp









_+ J


t~ ----

( I ((

FIELD DATA


~degfmiddotk


t Factor l L





middot1 C

bull I I I

I bull 0 ()


I I I

lh ltLt _L(


(F) Ii l

~ I

-J J-middot

tmiddotL t jI



(I) 7lt -~ i bull

f cJ I O lt Ibull f

ft IN I ILI 1J

l bull pound IL

I-I

1 I-

1 -- I

X) J 1 -L-- IJ 1 I


I bull

- d 0

) P ( ampI


l l-t--J L _ c_c l~

I 1

) -bullt I I

I I I

I -- I

c ) c 1- I ~ Ihl t

) (J I -~ r1 J - I ____ middot

Ibull r (

I () I rl

- -

Idlt- ~ -


I 11 J - I

bull I


r middotmiddotbull

I I

C I IrJ (_


bull J ( I

_ middot1 1 -

degta Uj MU

I

middot

- -

Plant __ ~






n A I 11 10

m ~



0 )) l I~ Jgtlgt) )( - I I I



- I Lgti- 1 --I - I I I


l


( 7I If I I I - ) I I l I -

FIELD DATA





6-t nLt



LUI Ts




It l ~-~

- I ) -c-1-J 1 J(

~

-rt I

1 ---i )I 1 )A

-u rbull-c _ i ~


1 5 l1 ~u ~ ~

Desired I [)c

I J tt I ( lt

lltf l l ti( 1

ltLf I 11

bull1 lu

r

111 1 ~


I e- 11 I)

( r ID

1tv llv 10l

I( I L-0

I CA


I I 0 I 11J

1 7



FACILITY

SOURCE

DATE r2f J

RUN

METHOD

BOX


I

2

3

4

DI WATER

DJWATER

EMPTY

SILICA GEL


s- J (

_ 0

I 1-- t


INITALS v


FACILITY

SOURCE

DATE rhlrr

RUN

METHOD

BOX rL

IMPINGER CONTENTS

1 DI WATER

7

2

3

DI WATER

EMPTY

4 SILICA GEL

FINAL

GRJIS

foo1


INITIAL

GRAMS

TOTAL

GRMS

I lt -( J t---

S-gt

INTTALS d7

0


FAC[LITY

SOURCE

DATE

RUN

METHOD

BOX


GRltJ~IS GRltMS

I

2

3

4

DI WATER

DI WATER

EMPTY

SILICA GEL


INITALS

TOTAL

GR~IS

J)

O-)

r-

~-(












- -

FIELD DATA


Date ~ () ~ f 9













lfJ D 1 H I

~ r -1 l l I [) ) J_JIC ~ I INl ) - ( I~()

) l I IV i-lt middot ) 1 - 0~ ) Y -11








_ I 11 - yen c-Y - _ - ~

- -to-1i 5 6 deg1

__ __________ _



Run Number ____c= _ _______



I




~ l ~ l lol X o



~~-I j1 vbull- ~JI






I I c Iv I l 1-1 11 -

v-1 Dll - ~



FIELD DATA









Stack Temp

Ts (F) ti( I 11

lt j

(

I




Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(


bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l


I IP I 7

I Lfo )


t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~


- I (() -J~

c f --- -

I

) clbull


1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation









FACIJITY

SOURCE

DATE

RUN

METHOD

BOX


GRJ-15 GR-15 GRJ-15

I

2

3

4

DI WATER

DI WATER

EMPIT

SILICA GEL

2--Z

~-~

o ~ (


INITALS


FACIIITY

SOURCE

DATE

RUN

METHOD we zrJ BOX


GR-1S GRMS

IIf

~D

I DIWATER

GRltJ-IS

e

2

3

4

DI WATER

EMPTY

SILICA GEL

I 0

IS--L


INITALS



FACfIITY

SOURCE

DATE

RUN

METHOD

BOX


GRJ-1S

I DI WATER

2 DI WATER

3 EMPTY

4 SILICA GEL

GRJ1S

t~c

Sf

GRJ-IS

-o~z -og

-o J

-02


INlTALS t

NOMENCLATURE




g ft3




1



letgt +460) ( -ZHmiddot+( 1 136))

8 1 + 460) (2992)




Vwstd = (00000894)( v B + 460)( Lf2 - )

Vwstd = ____I_~----q___


Bwo = 100 ( middot t 1 ) ( 4 + t S 781 )

Bwo= ------

2



MWd = (032 x 1- 010 ) + (044 x O O 1 ) + (028 x ( O + +I Ci ))


MWw = (MWd) (1 - BWo 100) + 18 ((BWo 100))

MWw = ( -Z 6- B-1) (1--Z -S- 100) + (18 ( z s-( 100))

(5) VELOCITY (Vs)

460Vs = 8549 x CP x ~ x ___Ts_+_- ----=-Ps

(Mw_) X (Bp + 136)

( 0 Ca + 460)vs = 8549 x ( o e- ) x ( 1 o 1 0 ) x 1----------------------

( -Z8- St ) X ( 2 degt ) tdeg + 0 C l )136

Vs= (po 9J

3


As = (Ds)2

x (31416) 576

( ) 2

X (31416)As=--------------~

576

As= ----


As = (L) (W) 144

As=( le ) ( I e ) I 144

As= -1B-------=--


ACFM = (Vs) (60) x (As)


ACFM =--~_5_0---CS-___

4



( ( R +460) ( 21+f) + ( 6u ~ I 136))X----=Ua__~X------------=-~--~

( o v +460) 2992




DSCFM= ( vO-l~ )x(l --z-~ 100)

DSCFM = ___-s_9_S_9__

(11) ISOKINETIC ()


60 x 0 x Vs x (Ps 136 + Pb) (Dn2 x 0005454)




5



mg Ni DSCM = ( 1- ~ ) I~ ( 7i8r ) X (0028317)



DSCF 1000






6

APPENDIX A-2











FIELD DATA



~ Fl Meter Della ll


1






I



Point Number

t t J V middotr IA

I 1

J I r lt

Time Time e





Reneling Vm



Head Ps


I u j bull -


I U 1






I - Lu

Temp Ts (F) lcD

o- 0~

~y oc

0~ middotbull ti -

Io - l6

Inlet Tmin

(F) t middot-t~ ~

- igt o j7r--

--7~-7

Outlet Tm out

(F) 1-

--- y

--t J _q

_ ~ I - Q n L-

Vacuum

(in II~) 7

-l

J )

J

) )

I J

Probe Temp

(F) t-J(

Dox Temp

(F) IA

Temp

ff) __ _ 2

I A

(o i 1

IA - C _ ~

tA) _ L-

C I

I l I

(

I _

I II)-I I _

I ~ (

ltgtl(1

1 _vc 111 ~ l A- bull J ~



l

lt l

I ~ _ tt

I Lbull j I

( lt L

t -lt C ( r

( (

l t IJ

I I CJ I I I

I t I I I

7 J--7 -i -fj - 1-

7 --1l J 7)

_)

1 )

J

v w

CL

(G _J

~lt-I-~

[Jou9 0 w u--~ Di


fl V 1 ~

l

Plant

Date

- -bull




amp J -)_ 5 ~

O C rs--rp









_+ J


t~ ----

( I ((

FIELD DATA


~degfmiddotk


t Factor l L





middot1 C

bull I I I

I bull 0 ()


I I I

lh ltLt _L(


(F) Ii l

~ I

-J J-middot

tmiddotL t jI



(I) 7lt -~ i bull

f cJ I O lt Ibull f

ft IN I ILI 1J

l bull pound IL

I-I

1 I-

1 -- I

X) J 1 -L-- IJ 1 I


I bull

- d 0

) P ( ampI


l l-t--J L _ c_c l~

I 1

) -bullt I I

I I I

I -- I

c ) c 1- I ~ Ihl t

) (J I -~ r1 J - I ____ middot

Ibull r (

I () I rl

- -

Idlt- ~ -


I 11 J - I

bull I


r middotmiddotbull

I I

C I IrJ (_


bull J ( I

_ middot1 1 -

degta Uj MU

I

middot

- -

Plant __ ~






n A I 11 10

m ~



0 )) l I~ Jgtlgt) )( - I I I



- I Lgti- 1 --I - I I I


l


( 7I If I I I - ) I I l I -

FIELD DATA





6-t nLt



LUI Ts




It l ~-~

- I ) -c-1-J 1 J(

~

-rt I

1 ---i )I 1 )A

-u rbull-c _ i ~


1 5 l1 ~u ~ ~

Desired I [)c

I J tt I ( lt

lltf l l ti( 1

ltLf I 11

bull1 lu

r

111 1 ~


I e- 11 I)

( r ID

1tv llv 10l

I( I L-0

I CA


I I 0 I 11J

1 7



FACILITY

SOURCE

DATE r2f J

RUN

METHOD

BOX


I

2

3

4

DI WATER

DJWATER

EMPTY

SILICA GEL


s- J (

_ 0

I 1-- t


INITALS v


FACILITY

SOURCE

DATE rhlrr

RUN

METHOD

BOX rL

IMPINGER CONTENTS

1 DI WATER

7

2

3

DI WATER

EMPTY

4 SILICA GEL

FINAL

GRJIS

foo1


INITIAL

GRAMS

TOTAL

GRMS

I lt -( J t---

S-gt

INTTALS d7

0


FAC[LITY

SOURCE

DATE

RUN

METHOD

BOX


GRltJ~IS GRltMS

I

2

3

4

DI WATER

DI WATER

EMPTY

SILICA GEL


INITALS

TOTAL

GR~IS

J)

O-)

r-

~-(












- -

FIELD DATA


Date ~ () ~ f 9













lfJ D 1 H I

~ r -1 l l I [) ) J_JIC ~ I INl ) - ( I~()

) l I IV i-lt middot ) 1 - 0~ ) Y -11








_ I 11 - yen c-Y - _ - ~

- -to-1i 5 6 deg1

__ __________ _



Run Number ____c= _ _______



I




~ l ~ l lol X o



~~-I j1 vbull- ~JI






I I c Iv I l 1-1 11 -

v-1 Dll - ~



FIELD DATA









Stack Temp

Ts (F) ti( I 11

lt j

(

I




Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(


bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l


I IP I 7

I Lfo )


t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~


- I (() -J~

c f --- -

I

) clbull


1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation









FACIIITY

SOURCE

DATE

RUN

METHOD we zrJ BOX


GR-1S GRMS

IIf

~D

I DIWATER

GRltJ-IS

e

2

3

4

DI WATER

EMPTY

SILICA GEL

I 0

IS--L


INITALS



FACfIITY

SOURCE

DATE

RUN

METHOD

BOX


GRJ-1S

I DI WATER

2 DI WATER

3 EMPTY

4 SILICA GEL

GRJ1S

t~c

Sf

GRJ-IS

-o~z -og

-o J

-02


INlTALS t

NOMENCLATURE




g ft3




1



letgt +460) ( -ZHmiddot+( 1 136))

8 1 + 460) (2992)




Vwstd = (00000894)( v B + 460)( Lf2 - )

Vwstd = ____I_~----q___


Bwo = 100 ( middot t 1 ) ( 4 + t S 781 )

Bwo= ------

2



MWd = (032 x 1- 010 ) + (044 x O O 1 ) + (028 x ( O + +I Ci ))


MWw = (MWd) (1 - BWo 100) + 18 ((BWo 100))

MWw = ( -Z 6- B-1) (1--Z -S- 100) + (18 ( z s-( 100))

(5) VELOCITY (Vs)

460Vs = 8549 x CP x ~ x ___Ts_+_- ----=-Ps

(Mw_) X (Bp + 136)

( 0 Ca + 460)vs = 8549 x ( o e- ) x ( 1 o 1 0 ) x 1----------------------

( -Z8- St ) X ( 2 degt ) tdeg + 0 C l )136

Vs= (po 9J

3


As = (Ds)2

x (31416) 576

( ) 2

X (31416)As=--------------~

576

As= ----


As = (L) (W) 144

As=( le ) ( I e ) I 144

As= -1B-------=--


ACFM = (Vs) (60) x (As)


ACFM =--~_5_0---CS-___

4



( ( R +460) ( 21+f) + ( 6u ~ I 136))X----=Ua__~X------------=-~--~

( o v +460) 2992




DSCFM= ( vO-l~ )x(l --z-~ 100)

DSCFM = ___-s_9_S_9__

(11) ISOKINETIC ()


60 x 0 x Vs x (Ps 136 + Pb) (Dn2 x 0005454)




5



mg Ni DSCM = ( 1- ~ ) I~ ( 7i8r ) X (0028317)



DSCF 1000






6

APPENDIX A-2











FIELD DATA



~ Fl Meter Della ll


1






I



Point Number

t t J V middotr IA

I 1

J I r lt

Time Time e





Reneling Vm



Head Ps


I u j bull -


I U 1






I - Lu

Temp Ts (F) lcD

o- 0~

~y oc

0~ middotbull ti -

Io - l6

Inlet Tmin

(F) t middot-t~ ~

- igt o j7r--

--7~-7

Outlet Tm out

(F) 1-

--- y

--t J _q

_ ~ I - Q n L-

Vacuum

(in II~) 7

-l

J )

J

) )

I J

Probe Temp

(F) t-J(

Dox Temp

(F) IA

Temp

ff) __ _ 2

I A

(o i 1

IA - C _ ~

tA) _ L-

C I

I l I

(

I _

I II)-I I _

I ~ (

ltgtl(1

1 _vc 111 ~ l A- bull J ~



l

lt l

I ~ _ tt

I Lbull j I

( lt L

t -lt C ( r

( (

l t IJ

I I CJ I I I

I t I I I

7 J--7 -i -fj - 1-

7 --1l J 7)

_)

1 )

J

v w

CL

(G _J

~lt-I-~

[Jou9 0 w u--~ Di


fl V 1 ~

l

Plant

Date

- -bull




amp J -)_ 5 ~

O C rs--rp









_+ J


t~ ----

( I ((

FIELD DATA


~degfmiddotk


t Factor l L





middot1 C

bull I I I

I bull 0 ()


I I I

lh ltLt _L(


(F) Ii l

~ I

-J J-middot

tmiddotL t jI



(I) 7lt -~ i bull

f cJ I O lt Ibull f

ft IN I ILI 1J

l bull pound IL

I-I

1 I-

1 -- I

X) J 1 -L-- IJ 1 I


I bull

- d 0

) P ( ampI


l l-t--J L _ c_c l~

I 1

) -bullt I I

I I I

I -- I

c ) c 1- I ~ Ihl t

) (J I -~ r1 J - I ____ middot

Ibull r (

I () I rl

- -

Idlt- ~ -


I 11 J - I

bull I


r middotmiddotbull

I I

C I IrJ (_


bull J ( I

_ middot1 1 -

degta Uj MU

I

middot

- -

Plant __ ~






n A I 11 10

m ~



0 )) l I~ Jgtlgt) )( - I I I



- I Lgti- 1 --I - I I I


l


( 7I If I I I - ) I I l I -

FIELD DATA





6-t nLt



LUI Ts




It l ~-~

- I ) -c-1-J 1 J(

~

-rt I

1 ---i )I 1 )A

-u rbull-c _ i ~


1 5 l1 ~u ~ ~

Desired I [)c

I J tt I ( lt

lltf l l ti( 1

ltLf I 11

bull1 lu

r

111 1 ~


I e- 11 I)

( r ID

1tv llv 10l

I( I L-0

I CA


I I 0 I 11J

1 7



FACILITY

SOURCE

DATE r2f J

RUN

METHOD

BOX


I

2

3

4

DI WATER

DJWATER

EMPTY

SILICA GEL


s- J (

_ 0

I 1-- t


INITALS v


FACILITY

SOURCE

DATE rhlrr

RUN

METHOD

BOX rL

IMPINGER CONTENTS

1 DI WATER

7

2

3

DI WATER

EMPTY

4 SILICA GEL

FINAL

GRJIS

foo1


INITIAL

GRAMS

TOTAL

GRMS

I lt -( J t---

S-gt

INTTALS d7

0


FAC[LITY

SOURCE

DATE

RUN

METHOD

BOX


GRltJ~IS GRltMS

I

2

3

4

DI WATER

DI WATER

EMPTY

SILICA GEL


INITALS

TOTAL

GR~IS

J)

O-)

r-

~-(












- -

FIELD DATA


Date ~ () ~ f 9













lfJ D 1 H I

~ r -1 l l I [) ) J_JIC ~ I INl ) - ( I~()

) l I IV i-lt middot ) 1 - 0~ ) Y -11








_ I 11 - yen c-Y - _ - ~

- -to-1i 5 6 deg1

__ __________ _



Run Number ____c= _ _______



I




~ l ~ l lol X o



~~-I j1 vbull- ~JI






I I c Iv I l 1-1 11 -

v-1 Dll - ~



FIELD DATA









Stack Temp

Ts (F) ti( I 11

lt j

(

I




Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(


bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l


I IP I 7

I Lfo )


t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~


- I (() -J~

c f --- -

I

) clbull


1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation










FACfIITY

SOURCE

DATE

RUN

METHOD

BOX


GRJ-1S

I DI WATER

2 DI WATER

3 EMPTY

4 SILICA GEL

GRJ1S

t~c

Sf

GRJ-IS

-o~z -og

-o J

-02


INlTALS t

NOMENCLATURE




g ft3




1



letgt +460) ( -ZHmiddot+( 1 136))

8 1 + 460) (2992)




Vwstd = (00000894)( v B + 460)( Lf2 - )

Vwstd = ____I_~----q___


Bwo = 100 ( middot t 1 ) ( 4 + t S 781 )

Bwo= ------

2



MWd = (032 x 1- 010 ) + (044 x O O 1 ) + (028 x ( O + +I Ci ))


MWw = (MWd) (1 - BWo 100) + 18 ((BWo 100))

MWw = ( -Z 6- B-1) (1--Z -S- 100) + (18 ( z s-( 100))

(5) VELOCITY (Vs)

460Vs = 8549 x CP x ~ x ___Ts_+_- ----=-Ps

(Mw_) X (Bp + 136)

( 0 Ca + 460)vs = 8549 x ( o e- ) x ( 1 o 1 0 ) x 1----------------------

( -Z8- St ) X ( 2 degt ) tdeg + 0 C l )136

Vs= (po 9J

3


As = (Ds)2

x (31416) 576

( ) 2

X (31416)As=--------------~

576

As= ----


As = (L) (W) 144

As=( le ) ( I e ) I 144

As= -1B-------=--


ACFM = (Vs) (60) x (As)


ACFM =--~_5_0---CS-___

4



( ( R +460) ( 21+f) + ( 6u ~ I 136))X----=Ua__~X------------=-~--~

( o v +460) 2992




DSCFM= ( vO-l~ )x(l --z-~ 100)

DSCFM = ___-s_9_S_9__

(11) ISOKINETIC ()


60 x 0 x Vs x (Ps 136 + Pb) (Dn2 x 0005454)




5



mg Ni DSCM = ( 1- ~ ) I~ ( 7i8r ) X (0028317)



DSCF 1000






6

APPENDIX A-2











FIELD DATA



~ Fl Meter Della ll


1






I



Point Number

t t J V middotr IA

I 1

J I r lt

Time Time e





Reneling Vm



Head Ps


I u j bull -


I U 1






I - Lu

Temp Ts (F) lcD

o- 0~

~y oc

0~ middotbull ti -

Io - l6

Inlet Tmin

(F) t middot-t~ ~

- igt o j7r--

--7~-7

Outlet Tm out

(F) 1-

--- y

--t J _q

_ ~ I - Q n L-

Vacuum

(in II~) 7

-l

J )

J

) )

I J

Probe Temp

(F) t-J(

Dox Temp

(F) IA

Temp

ff) __ _ 2

I A

(o i 1

IA - C _ ~

tA) _ L-

C I

I l I

(

I _

I II)-I I _

I ~ (

ltgtl(1

1 _vc 111 ~ l A- bull J ~



l

lt l

I ~ _ tt

I Lbull j I

( lt L

t -lt C ( r

( (

l t IJ

I I CJ I I I

I t I I I

7 J--7 -i -fj - 1-

7 --1l J 7)

_)

1 )

J

v w

CL

(G _J

~lt-I-~

[Jou9 0 w u--~ Di


fl V 1 ~

l

Plant

Date

- -bull




amp J -)_ 5 ~

O C rs--rp









_+ J


t~ ----

( I ((

FIELD DATA


~degfmiddotk


t Factor l L





middot1 C

bull I I I

I bull 0 ()


I I I

lh ltLt _L(


(F) Ii l

~ I

-J J-middot

tmiddotL t jI



(I) 7lt -~ i bull

f cJ I O lt Ibull f

ft IN I ILI 1J

l bull pound IL

I-I

1 I-

1 -- I

X) J 1 -L-- IJ 1 I


I bull

- d 0

) P ( ampI


l l-t--J L _ c_c l~

I 1

) -bullt I I

I I I

I -- I

c ) c 1- I ~ Ihl t

) (J I -~ r1 J - I ____ middot

Ibull r (

I () I rl

- -

Idlt- ~ -


I 11 J - I

bull I


r middotmiddotbull

I I

C I IrJ (_


bull J ( I

_ middot1 1 -

degta Uj MU

I

middot

- -

Plant __ ~






n A I 11 10

m ~



0 )) l I~ Jgtlgt) )( - I I I



- I Lgti- 1 --I - I I I


l


( 7I If I I I - ) I I l I -

FIELD DATA





6-t nLt



LUI Ts




It l ~-~

- I ) -c-1-J 1 J(

~

-rt I

1 ---i )I 1 )A

-u rbull-c _ i ~


1 5 l1 ~u ~ ~

Desired I [)c

I J tt I ( lt

lltf l l ti( 1

ltLf I 11

bull1 lu

r

111 1 ~


I e- 11 I)

( r ID

1tv llv 10l

I( I L-0

I CA


I I 0 I 11J

1 7



FACILITY

SOURCE

DATE r2f J

RUN

METHOD

BOX


I

2

3

4

DI WATER

DJWATER

EMPTY

SILICA GEL


s- J (

_ 0

I 1-- t


INITALS v


FACILITY

SOURCE

DATE rhlrr

RUN

METHOD

BOX rL

IMPINGER CONTENTS

1 DI WATER

7

2

3

DI WATER

EMPTY

4 SILICA GEL

FINAL

GRJIS

foo1


INITIAL

GRAMS

TOTAL

GRMS

I lt -( J t---

S-gt

INTTALS d7

0


FAC[LITY

SOURCE

DATE

RUN

METHOD

BOX


GRltJ~IS GRltMS

I

2

3

4

DI WATER

DI WATER

EMPTY

SILICA GEL


INITALS

TOTAL

GR~IS

J)

O-)

r-

~-(












- -

FIELD DATA


Date ~ () ~ f 9













lfJ D 1 H I

~ r -1 l l I [) ) J_JIC ~ I INl ) - ( I~()

) l I IV i-lt middot ) 1 - 0~ ) Y -11








_ I 11 - yen c-Y - _ - ~

- -to-1i 5 6 deg1

__ __________ _



Run Number ____c= _ _______



I




~ l ~ l lol X o



~~-I j1 vbull- ~JI






I I c Iv I l 1-1 11 -

v-1 Dll - ~



FIELD DATA









Stack Temp

Ts (F) ti( I 11

lt j

(

I




Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(


bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l


I IP I 7

I Lfo )


t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~


- I (() -J~

c f --- -

I

) clbull


1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

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) t


Phoae 213 722 8810 Fax 213 888 1493




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(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

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1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



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R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

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foo 0011 TT

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7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




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~)




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Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

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PJO

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JJ

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Zfqj

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o~

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yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

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fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








NOMENCLATURE




g ft3




1



letgt +460) ( -ZHmiddot+( 1 136))

8 1 + 460) (2992)




Vwstd = (00000894)( v B + 460)( Lf2 - )

Vwstd = ____I_~----q___


Bwo = 100 ( middot t 1 ) ( 4 + t S 781 )

Bwo= ------

2



MWd = (032 x 1- 010 ) + (044 x O O 1 ) + (028 x ( O + +I Ci ))


MWw = (MWd) (1 - BWo 100) + 18 ((BWo 100))

MWw = ( -Z 6- B-1) (1--Z -S- 100) + (18 ( z s-( 100))

(5) VELOCITY (Vs)

460Vs = 8549 x CP x ~ x ___Ts_+_- ----=-Ps

(Mw_) X (Bp + 136)

( 0 Ca + 460)vs = 8549 x ( o e- ) x ( 1 o 1 0 ) x 1----------------------

( -Z8- St ) X ( 2 degt ) tdeg + 0 C l )136

Vs= (po 9J

3


As = (Ds)2

x (31416) 576

( ) 2

X (31416)As=--------------~

576

As= ----


As = (L) (W) 144

As=( le ) ( I e ) I 144

As= -1B-------=--


ACFM = (Vs) (60) x (As)


ACFM =--~_5_0---CS-___

4



( ( R +460) ( 21+f) + ( 6u ~ I 136))X----=Ua__~X------------=-~--~

( o v +460) 2992




DSCFM= ( vO-l~ )x(l --z-~ 100)

DSCFM = ___-s_9_S_9__

(11) ISOKINETIC ()


60 x 0 x Vs x (Ps 136 + Pb) (Dn2 x 0005454)




5



mg Ni DSCM = ( 1- ~ ) I~ ( 7i8r ) X (0028317)



DSCF 1000






6

APPENDIX A-2











FIELD DATA



~ Fl Meter Della ll


1






I



Point Number

t t J V middotr IA

I 1

J I r lt

Time Time e





Reneling Vm



Head Ps


I u j bull -


I U 1






I - Lu

Temp Ts (F) lcD

o- 0~

~y oc

0~ middotbull ti -

Io - l6

Inlet Tmin

(F) t middot-t~ ~

- igt o j7r--

--7~-7

Outlet Tm out

(F) 1-

--- y

--t J _q

_ ~ I - Q n L-

Vacuum

(in II~) 7

-l

J )

J

) )

I J

Probe Temp

(F) t-J(

Dox Temp

(F) IA

Temp

ff) __ _ 2

I A

(o i 1

IA - C _ ~

tA) _ L-

C I

I l I

(

I _

I II)-I I _

I ~ (

ltgtl(1

1 _vc 111 ~ l A- bull J ~



l

lt l

I ~ _ tt

I Lbull j I

( lt L

t -lt C ( r

( (

l t IJ

I I CJ I I I

I t I I I

7 J--7 -i -fj - 1-

7 --1l J 7)

_)

1 )

J

v w

CL

(G _J

~lt-I-~

[Jou9 0 w u--~ Di


fl V 1 ~

l

Plant

Date

- -bull




amp J -)_ 5 ~

O C rs--rp









_+ J


t~ ----

( I ((

FIELD DATA


~degfmiddotk


t Factor l L





middot1 C

bull I I I

I bull 0 ()


I I I

lh ltLt _L(


(F) Ii l

~ I

-J J-middot

tmiddotL t jI



(I) 7lt -~ i bull

f cJ I O lt Ibull f

ft IN I ILI 1J

l bull pound IL

I-I

1 I-

1 -- I

X) J 1 -L-- IJ 1 I


I bull

- d 0

) P ( ampI


l l-t--J L _ c_c l~

I 1

) -bullt I I

I I I

I -- I

c ) c 1- I ~ Ihl t

) (J I -~ r1 J - I ____ middot

Ibull r (

I () I rl

- -

Idlt- ~ -


I 11 J - I

bull I


r middotmiddotbull

I I

C I IrJ (_


bull J ( I

_ middot1 1 -

degta Uj MU

I

middot

- -

Plant __ ~






n A I 11 10

m ~



0 )) l I~ Jgtlgt) )( - I I I



- I Lgti- 1 --I - I I I


l


( 7I If I I I - ) I I l I -

FIELD DATA





6-t nLt



LUI Ts




It l ~-~

- I ) -c-1-J 1 J(

~

-rt I

1 ---i )I 1 )A

-u rbull-c _ i ~


1 5 l1 ~u ~ ~

Desired I [)c

I J tt I ( lt

lltf l l ti( 1

ltLf I 11

bull1 lu

r

111 1 ~


I e- 11 I)

( r ID

1tv llv 10l

I( I L-0

I CA


I I 0 I 11J

1 7



FACILITY

SOURCE

DATE r2f J

RUN

METHOD

BOX


I

2

3

4

DI WATER

DJWATER

EMPTY

SILICA GEL


s- J (

_ 0

I 1-- t


INITALS v


FACILITY

SOURCE

DATE rhlrr

RUN

METHOD

BOX rL

IMPINGER CONTENTS

1 DI WATER

7

2

3

DI WATER

EMPTY

4 SILICA GEL

FINAL

GRJIS

foo1


INITIAL

GRAMS

TOTAL

GRMS

I lt -( J t---

S-gt

INTTALS d7

0


FAC[LITY

SOURCE

DATE

RUN

METHOD

BOX


GRltJ~IS GRltMS

I

2

3

4

DI WATER

DI WATER

EMPTY

SILICA GEL


INITALS

TOTAL

GR~IS

J)

O-)

r-

~-(












- -

FIELD DATA


Date ~ () ~ f 9













lfJ D 1 H I

~ r -1 l l I [) ) J_JIC ~ I INl ) - ( I~()

) l I IV i-lt middot ) 1 - 0~ ) Y -11








_ I 11 - yen c-Y - _ - ~

- -to-1i 5 6 deg1

__ __________ _



Run Number ____c= _ _______



I




~ l ~ l lol X o



~~-I j1 vbull- ~JI






I I c Iv I l 1-1 11 -

v-1 Dll - ~



FIELD DATA









Stack Temp

Ts (F) ti( I 11

lt j

(

I




Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(


bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l


I IP I 7

I Lfo )


t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~


- I (() -J~

c f --- -

I

) clbull


1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation










letgt +460) ( -ZHmiddot+( 1 136))

8 1 + 460) (2992)




Vwstd = (00000894)( v B + 460)( Lf2 - )

Vwstd = ____I_~----q___


Bwo = 100 ( middot t 1 ) ( 4 + t S 781 )

Bwo= ------

2



MWd = (032 x 1- 010 ) + (044 x O O 1 ) + (028 x ( O + +I Ci ))


MWw = (MWd) (1 - BWo 100) + 18 ((BWo 100))

MWw = ( -Z 6- B-1) (1--Z -S- 100) + (18 ( z s-( 100))

(5) VELOCITY (Vs)

460Vs = 8549 x CP x ~ x ___Ts_+_- ----=-Ps

(Mw_) X (Bp + 136)

( 0 Ca + 460)vs = 8549 x ( o e- ) x ( 1 o 1 0 ) x 1----------------------

( -Z8- St ) X ( 2 degt ) tdeg + 0 C l )136

Vs= (po 9J

3


As = (Ds)2

x (31416) 576

( ) 2

X (31416)As=--------------~

576

As= ----


As = (L) (W) 144

As=( le ) ( I e ) I 144

As= -1B-------=--


ACFM = (Vs) (60) x (As)


ACFM =--~_5_0---CS-___

4



( ( R +460) ( 21+f) + ( 6u ~ I 136))X----=Ua__~X------------=-~--~

( o v +460) 2992




DSCFM= ( vO-l~ )x(l --z-~ 100)

DSCFM = ___-s_9_S_9__

(11) ISOKINETIC ()


60 x 0 x Vs x (Ps 136 + Pb) (Dn2 x 0005454)




5



mg Ni DSCM = ( 1- ~ ) I~ ( 7i8r ) X (0028317)



DSCF 1000






6

APPENDIX A-2











FIELD DATA



~ Fl Meter Della ll


1






I



Point Number

t t J V middotr IA

I 1

J I r lt

Time Time e





Reneling Vm



Head Ps


I u j bull -


I U 1






I - Lu

Temp Ts (F) lcD

o- 0~

~y oc

0~ middotbull ti -

Io - l6

Inlet Tmin

(F) t middot-t~ ~

- igt o j7r--

--7~-7

Outlet Tm out

(F) 1-

--- y

--t J _q

_ ~ I - Q n L-

Vacuum

(in II~) 7

-l

J )

J

) )

I J

Probe Temp

(F) t-J(

Dox Temp

(F) IA

Temp

ff) __ _ 2

I A

(o i 1

IA - C _ ~

tA) _ L-

C I

I l I

(

I _

I II)-I I _

I ~ (

ltgtl(1

1 _vc 111 ~ l A- bull J ~



l

lt l

I ~ _ tt

I Lbull j I

( lt L

t -lt C ( r

( (

l t IJ

I I CJ I I I

I t I I I

7 J--7 -i -fj - 1-

7 --1l J 7)

_)

1 )

J

v w

CL

(G _J

~lt-I-~

[Jou9 0 w u--~ Di


fl V 1 ~

l

Plant

Date

- -bull




amp J -)_ 5 ~

O C rs--rp









_+ J


t~ ----

( I ((

FIELD DATA


~degfmiddotk


t Factor l L





middot1 C

bull I I I

I bull 0 ()


I I I

lh ltLt _L(


(F) Ii l

~ I

-J J-middot

tmiddotL t jI



(I) 7lt -~ i bull

f cJ I O lt Ibull f

ft IN I ILI 1J

l bull pound IL

I-I

1 I-

1 -- I

X) J 1 -L-- IJ 1 I


I bull

- d 0

) P ( ampI


l l-t--J L _ c_c l~

I 1

) -bullt I I

I I I

I -- I

c ) c 1- I ~ Ihl t

) (J I -~ r1 J - I ____ middot

Ibull r (

I () I rl

- -

Idlt- ~ -


I 11 J - I

bull I


r middotmiddotbull

I I

C I IrJ (_


bull J ( I

_ middot1 1 -

degta Uj MU

I

middot

- -

Plant __ ~






n A I 11 10

m ~



0 )) l I~ Jgtlgt) )( - I I I



- I Lgti- 1 --I - I I I


l


( 7I If I I I - ) I I l I -

FIELD DATA





6-t nLt



LUI Ts




It l ~-~

- I ) -c-1-J 1 J(

~

-rt I

1 ---i )I 1 )A

-u rbull-c _ i ~


1 5 l1 ~u ~ ~

Desired I [)c

I J tt I ( lt

lltf l l ti( 1

ltLf I 11

bull1 lu

r

111 1 ~


I e- 11 I)

( r ID

1tv llv 10l

I( I L-0

I CA


I I 0 I 11J

1 7



FACILITY

SOURCE

DATE r2f J

RUN

METHOD

BOX


I

2

3

4

DI WATER

DJWATER

EMPTY

SILICA GEL


s- J (

_ 0

I 1-- t


INITALS v


FACILITY

SOURCE

DATE rhlrr

RUN

METHOD

BOX rL

IMPINGER CONTENTS

1 DI WATER

7

2

3

DI WATER

EMPTY

4 SILICA GEL

FINAL

GRJIS

foo1


INITIAL

GRAMS

TOTAL

GRMS

I lt -( J t---

S-gt

INTTALS d7

0


FAC[LITY

SOURCE

DATE

RUN

METHOD

BOX


GRltJ~IS GRltMS

I

2

3

4

DI WATER

DI WATER

EMPTY

SILICA GEL


INITALS

TOTAL

GR~IS

J)

O-)

r-

~-(












- -

FIELD DATA


Date ~ () ~ f 9













lfJ D 1 H I

~ r -1 l l I [) ) J_JIC ~ I INl ) - ( I~()

) l I IV i-lt middot ) 1 - 0~ ) Y -11








_ I 11 - yen c-Y - _ - ~

- -to-1i 5 6 deg1

__ __________ _



Run Number ____c= _ _______



I




~ l ~ l lol X o



~~-I j1 vbull- ~JI






I I c Iv I l 1-1 11 -

v-1 Dll - ~



FIELD DATA









Stack Temp

Ts (F) ti( I 11

lt j

(

I




Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(


bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l


I IP I 7

I Lfo )


t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~


- I (() -J~

c f --- -

I

) clbull


1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation










MWd = (032 x 1- 010 ) + (044 x O O 1 ) + (028 x ( O + +I Ci ))


MWw = (MWd) (1 - BWo 100) + 18 ((BWo 100))

MWw = ( -Z 6- B-1) (1--Z -S- 100) + (18 ( z s-( 100))

(5) VELOCITY (Vs)

460Vs = 8549 x CP x ~ x ___Ts_+_- ----=-Ps

(Mw_) X (Bp + 136)

( 0 Ca + 460)vs = 8549 x ( o e- ) x ( 1 o 1 0 ) x 1----------------------

( -Z8- St ) X ( 2 degt ) tdeg + 0 C l )136

Vs= (po 9J

3


As = (Ds)2

x (31416) 576

( ) 2

X (31416)As=--------------~

576

As= ----


As = (L) (W) 144

As=( le ) ( I e ) I 144

As= -1B-------=--


ACFM = (Vs) (60) x (As)


ACFM =--~_5_0---CS-___

4



( ( R +460) ( 21+f) + ( 6u ~ I 136))X----=Ua__~X------------=-~--~

( o v +460) 2992




DSCFM= ( vO-l~ )x(l --z-~ 100)

DSCFM = ___-s_9_S_9__

(11) ISOKINETIC ()


60 x 0 x Vs x (Ps 136 + Pb) (Dn2 x 0005454)




5



mg Ni DSCM = ( 1- ~ ) I~ ( 7i8r ) X (0028317)



DSCF 1000






6

APPENDIX A-2











FIELD DATA



~ Fl Meter Della ll


1






I



Point Number

t t J V middotr IA

I 1

J I r lt

Time Time e





Reneling Vm



Head Ps


I u j bull -


I U 1






I - Lu

Temp Ts (F) lcD

o- 0~

~y oc

0~ middotbull ti -

Io - l6

Inlet Tmin

(F) t middot-t~ ~

- igt o j7r--

--7~-7

Outlet Tm out

(F) 1-

--- y

--t J _q

_ ~ I - Q n L-

Vacuum

(in II~) 7

-l

J )

J

) )

I J

Probe Temp

(F) t-J(

Dox Temp

(F) IA

Temp

ff) __ _ 2

I A

(o i 1

IA - C _ ~

tA) _ L-

C I

I l I

(

I _

I II)-I I _

I ~ (

ltgtl(1

1 _vc 111 ~ l A- bull J ~



l

lt l

I ~ _ tt

I Lbull j I

( lt L

t -lt C ( r

( (

l t IJ

I I CJ I I I

I t I I I

7 J--7 -i -fj - 1-

7 --1l J 7)

_)

1 )

J

v w

CL

(G _J

~lt-I-~

[Jou9 0 w u--~ Di


fl V 1 ~

l

Plant

Date

- -bull




amp J -)_ 5 ~

O C rs--rp









_+ J


t~ ----

( I ((

FIELD DATA


~degfmiddotk


t Factor l L





middot1 C

bull I I I

I bull 0 ()


I I I

lh ltLt _L(


(F) Ii l

~ I

-J J-middot

tmiddotL t jI



(I) 7lt -~ i bull

f cJ I O lt Ibull f

ft IN I ILI 1J

l bull pound IL

I-I

1 I-

1 -- I

X) J 1 -L-- IJ 1 I


I bull

- d 0

) P ( ampI


l l-t--J L _ c_c l~

I 1

) -bullt I I

I I I

I -- I

c ) c 1- I ~ Ihl t

) (J I -~ r1 J - I ____ middot

Ibull r (

I () I rl

- -

Idlt- ~ -


I 11 J - I

bull I


r middotmiddotbull

I I

C I IrJ (_


bull J ( I

_ middot1 1 -

degta Uj MU

I

middot

- -

Plant __ ~






n A I 11 10

m ~



0 )) l I~ Jgtlgt) )( - I I I



- I Lgti- 1 --I - I I I


l


( 7I If I I I - ) I I l I -

FIELD DATA





6-t nLt



LUI Ts




It l ~-~

- I ) -c-1-J 1 J(

~

-rt I

1 ---i )I 1 )A

-u rbull-c _ i ~


1 5 l1 ~u ~ ~

Desired I [)c

I J tt I ( lt

lltf l l ti( 1

ltLf I 11

bull1 lu

r

111 1 ~


I e- 11 I)

( r ID

1tv llv 10l

I( I L-0

I CA


I I 0 I 11J

1 7



FACILITY

SOURCE

DATE r2f J

RUN

METHOD

BOX


I

2

3

4

DI WATER

DJWATER

EMPTY

SILICA GEL


s- J (

_ 0

I 1-- t


INITALS v


FACILITY

SOURCE

DATE rhlrr

RUN

METHOD

BOX rL

IMPINGER CONTENTS

1 DI WATER

7

2

3

DI WATER

EMPTY

4 SILICA GEL

FINAL

GRJIS

foo1


INITIAL

GRAMS

TOTAL

GRMS

I lt -( J t---

S-gt

INTTALS d7

0


FAC[LITY

SOURCE

DATE

RUN

METHOD

BOX


GRltJ~IS GRltMS

I

2

3

4

DI WATER

DI WATER

EMPTY

SILICA GEL


INITALS

TOTAL

GR~IS

J)

O-)

r-

~-(












- -

FIELD DATA


Date ~ () ~ f 9













lfJ D 1 H I

~ r -1 l l I [) ) J_JIC ~ I INl ) - ( I~()

) l I IV i-lt middot ) 1 - 0~ ) Y -11








_ I 11 - yen c-Y - _ - ~

- -to-1i 5 6 deg1

__ __________ _



Run Number ____c= _ _______



I




~ l ~ l lol X o



~~-I j1 vbull- ~JI






I I c Iv I l 1-1 11 -

v-1 Dll - ~



FIELD DATA









Stack Temp

Ts (F) ti( I 11

lt j

(

I




Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(


bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l


I IP I 7

I Lfo )


t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~


- I (() -J~

c f --- -

I

) clbull


1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation









As = (Ds)2

x (31416) 576

( ) 2

X (31416)As=--------------~

576

As= ----


As = (L) (W) 144

As=( le ) ( I e ) I 144

As= -1B-------=--


ACFM = (Vs) (60) x (As)


ACFM =--~_5_0---CS-___

4



( ( R +460) ( 21+f) + ( 6u ~ I 136))X----=Ua__~X------------=-~--~

( o v +460) 2992




DSCFM= ( vO-l~ )x(l --z-~ 100)

DSCFM = ___-s_9_S_9__

(11) ISOKINETIC ()


60 x 0 x Vs x (Ps 136 + Pb) (Dn2 x 0005454)




5



mg Ni DSCM = ( 1- ~ ) I~ ( 7i8r ) X (0028317)



DSCF 1000






6

APPENDIX A-2











FIELD DATA



~ Fl Meter Della ll


1






I



Point Number

t t J V middotr IA

I 1

J I r lt

Time Time e





Reneling Vm



Head Ps


I u j bull -


I U 1






I - Lu

Temp Ts (F) lcD

o- 0~

~y oc

0~ middotbull ti -

Io - l6

Inlet Tmin

(F) t middot-t~ ~

- igt o j7r--

--7~-7

Outlet Tm out

(F) 1-

--- y

--t J _q

_ ~ I - Q n L-

Vacuum

(in II~) 7

-l

J )

J

) )

I J

Probe Temp

(F) t-J(

Dox Temp

(F) IA

Temp

ff) __ _ 2

I A

(o i 1

IA - C _ ~

tA) _ L-

C I

I l I

(

I _

I II)-I I _

I ~ (

ltgtl(1

1 _vc 111 ~ l A- bull J ~



l

lt l

I ~ _ tt

I Lbull j I

( lt L

t -lt C ( r

( (

l t IJ

I I CJ I I I

I t I I I

7 J--7 -i -fj - 1-

7 --1l J 7)

_)

1 )

J

v w

CL

(G _J

~lt-I-~

[Jou9 0 w u--~ Di


fl V 1 ~

l

Plant

Date

- -bull




amp J -)_ 5 ~

O C rs--rp









_+ J


t~ ----

( I ((

FIELD DATA


~degfmiddotk


t Factor l L





middot1 C

bull I I I

I bull 0 ()


I I I

lh ltLt _L(


(F) Ii l

~ I

-J J-middot

tmiddotL t jI



(I) 7lt -~ i bull

f cJ I O lt Ibull f

ft IN I ILI 1J

l bull pound IL

I-I

1 I-

1 -- I

X) J 1 -L-- IJ 1 I


I bull

- d 0

) P ( ampI


l l-t--J L _ c_c l~

I 1

) -bullt I I

I I I

I -- I

c ) c 1- I ~ Ihl t

) (J I -~ r1 J - I ____ middot

Ibull r (

I () I rl

- -

Idlt- ~ -


I 11 J - I

bull I


r middotmiddotbull

I I

C I IrJ (_


bull J ( I

_ middot1 1 -

degta Uj MU

I

middot

- -

Plant __ ~






n A I 11 10

m ~



0 )) l I~ Jgtlgt) )( - I I I



- I Lgti- 1 --I - I I I


l


( 7I If I I I - ) I I l I -

FIELD DATA





6-t nLt



LUI Ts




It l ~-~

- I ) -c-1-J 1 J(

~

-rt I

1 ---i )I 1 )A

-u rbull-c _ i ~


1 5 l1 ~u ~ ~

Desired I [)c

I J tt I ( lt

lltf l l ti( 1

ltLf I 11

bull1 lu

r

111 1 ~


I e- 11 I)

( r ID

1tv llv 10l

I( I L-0

I CA


I I 0 I 11J

1 7



FACILITY

SOURCE

DATE r2f J

RUN

METHOD

BOX


I

2

3

4

DI WATER

DJWATER

EMPTY

SILICA GEL


s- J (

_ 0

I 1-- t


INITALS v


FACILITY

SOURCE

DATE rhlrr

RUN

METHOD

BOX rL

IMPINGER CONTENTS

1 DI WATER

7

2

3

DI WATER

EMPTY

4 SILICA GEL

FINAL

GRJIS

foo1


INITIAL

GRAMS

TOTAL

GRMS

I lt -( J t---

S-gt

INTTALS d7

0


FAC[LITY

SOURCE

DATE

RUN

METHOD

BOX


GRltJ~IS GRltMS

I

2

3

4

DI WATER

DI WATER

EMPTY

SILICA GEL


INITALS

TOTAL

GR~IS

J)

O-)

r-

~-(












- -

FIELD DATA


Date ~ () ~ f 9













lfJ D 1 H I

~ r -1 l l I [) ) J_JIC ~ I INl ) - ( I~()

) l I IV i-lt middot ) 1 - 0~ ) Y -11








_ I 11 - yen c-Y - _ - ~

- -to-1i 5 6 deg1

__ __________ _



Run Number ____c= _ _______



I




~ l ~ l lol X o



~~-I j1 vbull- ~JI






I I c Iv I l 1-1 11 -

v-1 Dll - ~



FIELD DATA









Stack Temp

Ts (F) ti( I 11

lt j

(

I




Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(


bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l


I IP I 7

I Lfo )


t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~


- I (() -J~

c f --- -

I

) clbull


1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation










( ( R +460) ( 21+f) + ( 6u ~ I 136))X----=Ua__~X------------=-~--~

( o v +460) 2992




DSCFM= ( vO-l~ )x(l --z-~ 100)

DSCFM = ___-s_9_S_9__

(11) ISOKINETIC ()


60 x 0 x Vs x (Ps 136 + Pb) (Dn2 x 0005454)




5



mg Ni DSCM = ( 1- ~ ) I~ ( 7i8r ) X (0028317)



DSCF 1000






6

APPENDIX A-2











FIELD DATA



~ Fl Meter Della ll


1






I



Point Number

t t J V middotr IA

I 1

J I r lt

Time Time e





Reneling Vm



Head Ps


I u j bull -


I U 1






I - Lu

Temp Ts (F) lcD

o- 0~

~y oc

0~ middotbull ti -

Io - l6

Inlet Tmin

(F) t middot-t~ ~

- igt o j7r--

--7~-7

Outlet Tm out

(F) 1-

--- y

--t J _q

_ ~ I - Q n L-

Vacuum

(in II~) 7

-l

J )

J

) )

I J

Probe Temp

(F) t-J(

Dox Temp

(F) IA

Temp

ff) __ _ 2

I A

(o i 1

IA - C _ ~

tA) _ L-

C I

I l I

(

I _

I II)-I I _

I ~ (

ltgtl(1

1 _vc 111 ~ l A- bull J ~



l

lt l

I ~ _ tt

I Lbull j I

( lt L

t -lt C ( r

( (

l t IJ

I I CJ I I I

I t I I I

7 J--7 -i -fj - 1-

7 --1l J 7)

_)

1 )

J

v w

CL

(G _J

~lt-I-~

[Jou9 0 w u--~ Di


fl V 1 ~

l

Plant

Date

- -bull




amp J -)_ 5 ~

O C rs--rp









_+ J


t~ ----

( I ((

FIELD DATA


~degfmiddotk


t Factor l L





middot1 C

bull I I I

I bull 0 ()


I I I

lh ltLt _L(


(F) Ii l

~ I

-J J-middot

tmiddotL t jI



(I) 7lt -~ i bull

f cJ I O lt Ibull f

ft IN I ILI 1J

l bull pound IL

I-I

1 I-

1 -- I

X) J 1 -L-- IJ 1 I


I bull

- d 0

) P ( ampI


l l-t--J L _ c_c l~

I 1

) -bullt I I

I I I

I -- I

c ) c 1- I ~ Ihl t

) (J I -~ r1 J - I ____ middot

Ibull r (

I () I rl

- -

Idlt- ~ -


I 11 J - I

bull I


r middotmiddotbull

I I

C I IrJ (_


bull J ( I

_ middot1 1 -

degta Uj MU

I

middot

- -

Plant __ ~






n A I 11 10

m ~



0 )) l I~ Jgtlgt) )( - I I I



- I Lgti- 1 --I - I I I


l


( 7I If I I I - ) I I l I -

FIELD DATA





6-t nLt



LUI Ts




It l ~-~

- I ) -c-1-J 1 J(

~

-rt I

1 ---i )I 1 )A

-u rbull-c _ i ~


1 5 l1 ~u ~ ~

Desired I [)c

I J tt I ( lt

lltf l l ti( 1

ltLf I 11

bull1 lu

r

111 1 ~


I e- 11 I)

( r ID

1tv llv 10l

I( I L-0

I CA


I I 0 I 11J

1 7



FACILITY

SOURCE

DATE r2f J

RUN

METHOD

BOX


I

2

3

4

DI WATER

DJWATER

EMPTY

SILICA GEL


s- J (

_ 0

I 1-- t


INITALS v


FACILITY

SOURCE

DATE rhlrr

RUN

METHOD

BOX rL

IMPINGER CONTENTS

1 DI WATER

7

2

3

DI WATER

EMPTY

4 SILICA GEL

FINAL

GRJIS

foo1


INITIAL

GRAMS

TOTAL

GRMS

I lt -( J t---

S-gt

INTTALS d7

0


FAC[LITY

SOURCE

DATE

RUN

METHOD

BOX


GRltJ~IS GRltMS

I

2

3

4

DI WATER

DI WATER

EMPTY

SILICA GEL


INITALS

TOTAL

GR~IS

J)

O-)

r-

~-(












- -

FIELD DATA


Date ~ () ~ f 9













lfJ D 1 H I

~ r -1 l l I [) ) J_JIC ~ I INl ) - ( I~()

) l I IV i-lt middot ) 1 - 0~ ) Y -11








_ I 11 - yen c-Y - _ - ~

- -to-1i 5 6 deg1

__ __________ _



Run Number ____c= _ _______



I




~ l ~ l lol X o



~~-I j1 vbull- ~JI






I I c Iv I l 1-1 11 -

v-1 Dll - ~



FIELD DATA









Stack Temp

Ts (F) ti( I 11

lt j

(

I




Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(


bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l


I IP I 7

I Lfo )


t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~


- I (() -J~

c f --- -

I

) clbull


1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation










mg Ni DSCM = ( 1- ~ ) I~ ( 7i8r ) X (0028317)



DSCF 1000






6

APPENDIX A-2











FIELD DATA



~ Fl Meter Della ll


1






I



Point Number

t t J V middotr IA

I 1

J I r lt

Time Time e





Reneling Vm



Head Ps


I u j bull -


I U 1






I - Lu

Temp Ts (F) lcD

o- 0~

~y oc

0~ middotbull ti -

Io - l6

Inlet Tmin

(F) t middot-t~ ~

- igt o j7r--

--7~-7

Outlet Tm out

(F) 1-

--- y

--t J _q

_ ~ I - Q n L-

Vacuum

(in II~) 7

-l

J )

J

) )

I J

Probe Temp

(F) t-J(

Dox Temp

(F) IA

Temp

ff) __ _ 2

I A

(o i 1

IA - C _ ~

tA) _ L-

C I

I l I

(

I _

I II)-I I _

I ~ (

ltgtl(1

1 _vc 111 ~ l A- bull J ~



l

lt l

I ~ _ tt

I Lbull j I

( lt L

t -lt C ( r

( (

l t IJ

I I CJ I I I

I t I I I

7 J--7 -i -fj - 1-

7 --1l J 7)

_)

1 )

J

v w

CL

(G _J

~lt-I-~

[Jou9 0 w u--~ Di


fl V 1 ~

l

Plant

Date

- -bull




amp J -)_ 5 ~

O C rs--rp









_+ J


t~ ----

( I ((

FIELD DATA


~degfmiddotk


t Factor l L





middot1 C

bull I I I

I bull 0 ()


I I I

lh ltLt _L(


(F) Ii l

~ I

-J J-middot

tmiddotL t jI



(I) 7lt -~ i bull

f cJ I O lt Ibull f

ft IN I ILI 1J

l bull pound IL

I-I

1 I-

1 -- I

X) J 1 -L-- IJ 1 I


I bull

- d 0

) P ( ampI


l l-t--J L _ c_c l~

I 1

) -bullt I I

I I I

I -- I

c ) c 1- I ~ Ihl t

) (J I -~ r1 J - I ____ middot

Ibull r (

I () I rl

- -

Idlt- ~ -


I 11 J - I

bull I


r middotmiddotbull

I I

C I IrJ (_


bull J ( I

_ middot1 1 -

degta Uj MU

I

middot

- -

Plant __ ~






n A I 11 10

m ~



0 )) l I~ Jgtlgt) )( - I I I



- I Lgti- 1 --I - I I I


l


( 7I If I I I - ) I I l I -

FIELD DATA





6-t nLt



LUI Ts




It l ~-~

- I ) -c-1-J 1 J(

~

-rt I

1 ---i )I 1 )A

-u rbull-c _ i ~


1 5 l1 ~u ~ ~

Desired I [)c

I J tt I ( lt

lltf l l ti( 1

ltLf I 11

bull1 lu

r

111 1 ~


I e- 11 I)

( r ID

1tv llv 10l

I( I L-0

I CA


I I 0 I 11J

1 7



FACILITY

SOURCE

DATE r2f J

RUN

METHOD

BOX


I

2

3

4

DI WATER

DJWATER

EMPTY

SILICA GEL


s- J (

_ 0

I 1-- t


INITALS v


FACILITY

SOURCE

DATE rhlrr

RUN

METHOD

BOX rL

IMPINGER CONTENTS

1 DI WATER

7

2

3

DI WATER

EMPTY

4 SILICA GEL

FINAL

GRJIS

foo1


INITIAL

GRAMS

TOTAL

GRMS

I lt -( J t---

S-gt

INTTALS d7

0


FAC[LITY

SOURCE

DATE

RUN

METHOD

BOX


GRltJ~IS GRltMS

I

2

3

4

DI WATER

DI WATER

EMPTY

SILICA GEL


INITALS

TOTAL

GR~IS

J)

O-)

r-

~-(












- -

FIELD DATA


Date ~ () ~ f 9













lfJ D 1 H I

~ r -1 l l I [) ) J_JIC ~ I INl ) - ( I~()

) l I IV i-lt middot ) 1 - 0~ ) Y -11








_ I 11 - yen c-Y - _ - ~

- -to-1i 5 6 deg1

__ __________ _



Run Number ____c= _ _______



I




~ l ~ l lol X o



~~-I j1 vbull- ~JI






I I c Iv I l 1-1 11 -

v-1 Dll - ~



FIELD DATA









Stack Temp

Ts (F) ti( I 11

lt j

(

I




Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(


bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l


I IP I 7

I Lfo )


t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~


- I (() -J~

c f --- -

I

) clbull


1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








APPENDIX A-2











FIELD DATA



~ Fl Meter Della ll


1






I



Point Number

t t J V middotr IA

I 1

J I r lt

Time Time e





Reneling Vm



Head Ps


I u j bull -


I U 1






I - Lu

Temp Ts (F) lcD

o- 0~

~y oc

0~ middotbull ti -

Io - l6

Inlet Tmin

(F) t middot-t~ ~

- igt o j7r--

--7~-7

Outlet Tm out

(F) 1-

--- y

--t J _q

_ ~ I - Q n L-

Vacuum

(in II~) 7

-l

J )

J

) )

I J

Probe Temp

(F) t-J(

Dox Temp

(F) IA

Temp

ff) __ _ 2

I A

(o i 1

IA - C _ ~

tA) _ L-

C I

I l I

(

I _

I II)-I I _

I ~ (

ltgtl(1

1 _vc 111 ~ l A- bull J ~



l

lt l

I ~ _ tt

I Lbull j I

( lt L

t -lt C ( r

( (

l t IJ

I I CJ I I I

I t I I I

7 J--7 -i -fj - 1-

7 --1l J 7)

_)

1 )

J

v w

CL

(G _J

~lt-I-~

[Jou9 0 w u--~ Di


fl V 1 ~

l

Plant

Date

- -bull




amp J -)_ 5 ~

O C rs--rp









_+ J


t~ ----

( I ((

FIELD DATA


~degfmiddotk


t Factor l L





middot1 C

bull I I I

I bull 0 ()


I I I

lh ltLt _L(


(F) Ii l

~ I

-J J-middot

tmiddotL t jI



(I) 7lt -~ i bull

f cJ I O lt Ibull f

ft IN I ILI 1J

l bull pound IL

I-I

1 I-

1 -- I

X) J 1 -L-- IJ 1 I


I bull

- d 0

) P ( ampI


l l-t--J L _ c_c l~

I 1

) -bullt I I

I I I

I -- I

c ) c 1- I ~ Ihl t

) (J I -~ r1 J - I ____ middot

Ibull r (

I () I rl

- -

Idlt- ~ -


I 11 J - I

bull I


r middotmiddotbull

I I

C I IrJ (_


bull J ( I

_ middot1 1 -

degta Uj MU

I

middot

- -

Plant __ ~






n A I 11 10

m ~



0 )) l I~ Jgtlgt) )( - I I I



- I Lgti- 1 --I - I I I


l


( 7I If I I I - ) I I l I -

FIELD DATA





6-t nLt



LUI Ts




It l ~-~

- I ) -c-1-J 1 J(

~

-rt I

1 ---i )I 1 )A

-u rbull-c _ i ~


1 5 l1 ~u ~ ~

Desired I [)c

I J tt I ( lt

lltf l l ti( 1

ltLf I 11

bull1 lu

r

111 1 ~


I e- 11 I)

( r ID

1tv llv 10l

I( I L-0

I CA


I I 0 I 11J

1 7



FACILITY

SOURCE

DATE r2f J

RUN

METHOD

BOX


I

2

3

4

DI WATER

DJWATER

EMPTY

SILICA GEL


s- J (

_ 0

I 1-- t


INITALS v


FACILITY

SOURCE

DATE rhlrr

RUN

METHOD

BOX rL

IMPINGER CONTENTS

1 DI WATER

7

2

3

DI WATER

EMPTY

4 SILICA GEL

FINAL

GRJIS

foo1


INITIAL

GRAMS

TOTAL

GRMS

I lt -( J t---

S-gt

INTTALS d7

0


FAC[LITY

SOURCE

DATE

RUN

METHOD

BOX


GRltJ~IS GRltMS

I

2

3

4

DI WATER

DI WATER

EMPTY

SILICA GEL


INITALS

TOTAL

GR~IS

J)

O-)

r-

~-(












- -

FIELD DATA


Date ~ () ~ f 9













lfJ D 1 H I

~ r -1 l l I [) ) J_JIC ~ I INl ) - ( I~()

) l I IV i-lt middot ) 1 - 0~ ) Y -11








_ I 11 - yen c-Y - _ - ~

- -to-1i 5 6 deg1

__ __________ _



Run Number ____c= _ _______



I




~ l ~ l lol X o



~~-I j1 vbull- ~JI






I I c Iv I l 1-1 11 -

v-1 Dll - ~



FIELD DATA









Stack Temp

Ts (F) ti( I 11

lt j

(

I




Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(


bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l


I IP I 7

I Lfo )


t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~


- I (() -J~

c f --- -

I

) clbull


1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation

















FIELD DATA



~ Fl Meter Della ll


1






I



Point Number

t t J V middotr IA

I 1

J I r lt

Time Time e





Reneling Vm



Head Ps


I u j bull -


I U 1






I - Lu

Temp Ts (F) lcD

o- 0~

~y oc

0~ middotbull ti -

Io - l6

Inlet Tmin

(F) t middot-t~ ~

- igt o j7r--

--7~-7

Outlet Tm out

(F) 1-

--- y

--t J _q

_ ~ I - Q n L-

Vacuum

(in II~) 7

-l

J )

J

) )

I J

Probe Temp

(F) t-J(

Dox Temp

(F) IA

Temp

ff) __ _ 2

I A

(o i 1

IA - C _ ~

tA) _ L-

C I

I l I

(

I _

I II)-I I _

I ~ (

ltgtl(1

1 _vc 111 ~ l A- bull J ~



l

lt l

I ~ _ tt

I Lbull j I

( lt L

t -lt C ( r

( (

l t IJ

I I CJ I I I

I t I I I

7 J--7 -i -fj - 1-

7 --1l J 7)

_)

1 )

J

v w

CL

(G _J

~lt-I-~

[Jou9 0 w u--~ Di


fl V 1 ~

l

Plant

Date

- -bull




amp J -)_ 5 ~

O C rs--rp









_+ J


t~ ----

( I ((

FIELD DATA


~degfmiddotk


t Factor l L





middot1 C

bull I I I

I bull 0 ()


I I I

lh ltLt _L(


(F) Ii l

~ I

-J J-middot

tmiddotL t jI



(I) 7lt -~ i bull

f cJ I O lt Ibull f

ft IN I ILI 1J

l bull pound IL

I-I

1 I-

1 -- I

X) J 1 -L-- IJ 1 I


I bull

- d 0

) P ( ampI


l l-t--J L _ c_c l~

I 1

) -bullt I I

I I I

I -- I

c ) c 1- I ~ Ihl t

) (J I -~ r1 J - I ____ middot

Ibull r (

I () I rl

- -

Idlt- ~ -


I 11 J - I

bull I


r middotmiddotbull

I I

C I IrJ (_


bull J ( I

_ middot1 1 -

degta Uj MU

I

middot

- -

Plant __ ~






n A I 11 10

m ~



0 )) l I~ Jgtlgt) )( - I I I



- I Lgti- 1 --I - I I I


l


( 7I If I I I - ) I I l I -

FIELD DATA





6-t nLt



LUI Ts




It l ~-~

- I ) -c-1-J 1 J(

~

-rt I

1 ---i )I 1 )A

-u rbull-c _ i ~


1 5 l1 ~u ~ ~

Desired I [)c

I J tt I ( lt

lltf l l ti( 1

ltLf I 11

bull1 lu

r

111 1 ~


I e- 11 I)

( r ID

1tv llv 10l

I( I L-0

I CA


I I 0 I 11J

1 7



FACILITY

SOURCE

DATE r2f J

RUN

METHOD

BOX


I

2

3

4

DI WATER

DJWATER

EMPTY

SILICA GEL


s- J (

_ 0

I 1-- t


INITALS v


FACILITY

SOURCE

DATE rhlrr

RUN

METHOD

BOX rL

IMPINGER CONTENTS

1 DI WATER

7

2

3

DI WATER

EMPTY

4 SILICA GEL

FINAL

GRJIS

foo1


INITIAL

GRAMS

TOTAL

GRMS

I lt -( J t---

S-gt

INTTALS d7

0


FAC[LITY

SOURCE

DATE

RUN

METHOD

BOX


GRltJ~IS GRltMS

I

2

3

4

DI WATER

DI WATER

EMPTY

SILICA GEL


INITALS

TOTAL

GR~IS

J)

O-)

r-

~-(












- -

FIELD DATA


Date ~ () ~ f 9













lfJ D 1 H I

~ r -1 l l I [) ) J_JIC ~ I INl ) - ( I~()

) l I IV i-lt middot ) 1 - 0~ ) Y -11








_ I 11 - yen c-Y - _ - ~

- -to-1i 5 6 deg1

__ __________ _



Run Number ____c= _ _______



I




~ l ~ l lol X o



~~-I j1 vbull- ~JI






I I c Iv I l 1-1 11 -

v-1 Dll - ~



FIELD DATA









Stack Temp

Ts (F) ti( I 11

lt j

(

I




Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(


bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l


I IP I 7

I Lfo )


t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~


- I (() -J~

c f --- -

I

) clbull


1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








Plant

Date

- -bull




amp J -)_ 5 ~

O C rs--rp









_+ J


t~ ----

( I ((

FIELD DATA


~degfmiddotk


t Factor l L





middot1 C

bull I I I

I bull 0 ()


I I I

lh ltLt _L(


(F) Ii l

~ I

-J J-middot

tmiddotL t jI



(I) 7lt -~ i bull

f cJ I O lt Ibull f

ft IN I ILI 1J

l bull pound IL

I-I

1 I-

1 -- I

X) J 1 -L-- IJ 1 I


I bull

- d 0

) P ( ampI


l l-t--J L _ c_c l~

I 1

) -bullt I I

I I I

I -- I

c ) c 1- I ~ Ihl t

) (J I -~ r1 J - I ____ middot

Ibull r (

I () I rl

- -

Idlt- ~ -


I 11 J - I

bull I


r middotmiddotbull

I I

C I IrJ (_


bull J ( I

_ middot1 1 -

degta Uj MU

I

middot

- -

Plant __ ~






n A I 11 10

m ~



0 )) l I~ Jgtlgt) )( - I I I



- I Lgti- 1 --I - I I I


l


( 7I If I I I - ) I I l I -

FIELD DATA





6-t nLt



LUI Ts




It l ~-~

- I ) -c-1-J 1 J(

~

-rt I

1 ---i )I 1 )A

-u rbull-c _ i ~


1 5 l1 ~u ~ ~

Desired I [)c

I J tt I ( lt

lltf l l ti( 1

ltLf I 11

bull1 lu

r

111 1 ~


I e- 11 I)

( r ID

1tv llv 10l

I( I L-0

I CA


I I 0 I 11J

1 7



FACILITY

SOURCE

DATE r2f J

RUN

METHOD

BOX


I

2

3

4

DI WATER

DJWATER

EMPTY

SILICA GEL


s- J (

_ 0

I 1-- t


INITALS v


FACILITY

SOURCE

DATE rhlrr

RUN

METHOD

BOX rL

IMPINGER CONTENTS

1 DI WATER

7

2

3

DI WATER

EMPTY

4 SILICA GEL

FINAL

GRJIS

foo1


INITIAL

GRAMS

TOTAL

GRMS

I lt -( J t---

S-gt

INTTALS d7

0


FAC[LITY

SOURCE

DATE

RUN

METHOD

BOX


GRltJ~IS GRltMS

I

2

3

4

DI WATER

DI WATER

EMPTY

SILICA GEL


INITALS

TOTAL

GR~IS

J)

O-)

r-

~-(












- -

FIELD DATA


Date ~ () ~ f 9













lfJ D 1 H I

~ r -1 l l I [) ) J_JIC ~ I INl ) - ( I~()

) l I IV i-lt middot ) 1 - 0~ ) Y -11








_ I 11 - yen c-Y - _ - ~

- -to-1i 5 6 deg1

__ __________ _



Run Number ____c= _ _______



I




~ l ~ l lol X o



~~-I j1 vbull- ~JI






I I c Iv I l 1-1 11 -

v-1 Dll - ~



FIELD DATA









Stack Temp

Ts (F) ti( I 11

lt j

(

I




Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(


bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l


I IP I 7

I Lfo )


t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~


- I (() -J~

c f --- -

I

) clbull


1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








- -

Plant __ ~






n A I 11 10

m ~



0 )) l I~ Jgtlgt) )( - I I I



- I Lgti- 1 --I - I I I


l


( 7I If I I I - ) I I l I -

FIELD DATA





6-t nLt



LUI Ts




It l ~-~

- I ) -c-1-J 1 J(

~

-rt I

1 ---i )I 1 )A

-u rbull-c _ i ~


1 5 l1 ~u ~ ~

Desired I [)c

I J tt I ( lt

lltf l l ti( 1

ltLf I 11

bull1 lu

r

111 1 ~


I e- 11 I)

( r ID

1tv llv 10l

I( I L-0

I CA


I I 0 I 11J

1 7



FACILITY

SOURCE

DATE r2f J

RUN

METHOD

BOX


I

2

3

4

DI WATER

DJWATER

EMPTY

SILICA GEL


s- J (

_ 0

I 1-- t


INITALS v


FACILITY

SOURCE

DATE rhlrr

RUN

METHOD

BOX rL

IMPINGER CONTENTS

1 DI WATER

7

2

3

DI WATER

EMPTY

4 SILICA GEL

FINAL

GRJIS

foo1


INITIAL

GRAMS

TOTAL

GRMS

I lt -( J t---

S-gt

INTTALS d7

0


FAC[LITY

SOURCE

DATE

RUN

METHOD

BOX


GRltJ~IS GRltMS

I

2

3

4

DI WATER

DI WATER

EMPTY

SILICA GEL


INITALS

TOTAL

GR~IS

J)

O-)

r-

~-(












- -

FIELD DATA


Date ~ () ~ f 9













lfJ D 1 H I

~ r -1 l l I [) ) J_JIC ~ I INl ) - ( I~()

) l I IV i-lt middot ) 1 - 0~ ) Y -11








_ I 11 - yen c-Y - _ - ~

- -to-1i 5 6 deg1

__ __________ _



Run Number ____c= _ _______



I




~ l ~ l lol X o



~~-I j1 vbull- ~JI






I I c Iv I l 1-1 11 -

v-1 Dll - ~



FIELD DATA









Stack Temp

Ts (F) ti( I 11

lt j

(

I




Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(


bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l


I IP I 7

I Lfo )


t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~


- I (() -J~

c f --- -

I

) clbull


1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation










FACILITY

SOURCE

DATE r2f J

RUN

METHOD

BOX


I

2

3

4

DI WATER

DJWATER

EMPTY

SILICA GEL


s- J (

_ 0

I 1-- t


INITALS v


FACILITY

SOURCE

DATE rhlrr

RUN

METHOD

BOX rL

IMPINGER CONTENTS

1 DI WATER

7

2

3

DI WATER

EMPTY

4 SILICA GEL

FINAL

GRJIS

foo1


INITIAL

GRAMS

TOTAL

GRMS

I lt -( J t---

S-gt

INTTALS d7

0


FAC[LITY

SOURCE

DATE

RUN

METHOD

BOX


GRltJ~IS GRltMS

I

2

3

4

DI WATER

DI WATER

EMPTY

SILICA GEL


INITALS

TOTAL

GR~IS

J)

O-)

r-

~-(












- -

FIELD DATA


Date ~ () ~ f 9













lfJ D 1 H I

~ r -1 l l I [) ) J_JIC ~ I INl ) - ( I~()

) l I IV i-lt middot ) 1 - 0~ ) Y -11








_ I 11 - yen c-Y - _ - ~

- -to-1i 5 6 deg1

__ __________ _



Run Number ____c= _ _______



I




~ l ~ l lol X o



~~-I j1 vbull- ~JI






I I c Iv I l 1-1 11 -

v-1 Dll - ~



FIELD DATA









Stack Temp

Ts (F) ti( I 11

lt j

(

I




Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(


bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l


I IP I 7

I Lfo )


t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~


- I (() -J~

c f --- -

I

) clbull


1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation









FACILITY

SOURCE

DATE rhlrr

RUN

METHOD

BOX rL

IMPINGER CONTENTS

1 DI WATER

7

2

3

DI WATER

EMPTY

4 SILICA GEL

FINAL

GRJIS

foo1


INITIAL

GRAMS

TOTAL

GRMS

I lt -( J t---

S-gt

INTTALS d7

0


FAC[LITY

SOURCE

DATE

RUN

METHOD

BOX


GRltJ~IS GRltMS

I

2

3

4

DI WATER

DI WATER

EMPTY

SILICA GEL


INITALS

TOTAL

GR~IS

J)

O-)

r-

~-(












- -

FIELD DATA


Date ~ () ~ f 9













lfJ D 1 H I

~ r -1 l l I [) ) J_JIC ~ I INl ) - ( I~()

) l I IV i-lt middot ) 1 - 0~ ) Y -11








_ I 11 - yen c-Y - _ - ~

- -to-1i 5 6 deg1

__ __________ _



Run Number ____c= _ _______



I




~ l ~ l lol X o



~~-I j1 vbull- ~JI






I I c Iv I l 1-1 11 -

v-1 Dll - ~



FIELD DATA









Stack Temp

Ts (F) ti( I 11

lt j

(

I




Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(


bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l


I IP I 7

I Lfo )


t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~


- I (() -J~

c f --- -

I

) clbull


1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation









FAC[LITY

SOURCE

DATE

RUN

METHOD

BOX


GRltJ~IS GRltMS

I

2

3

4

DI WATER

DI WATER

EMPTY

SILICA GEL


INITALS

TOTAL

GR~IS

J)

O-)

r-

~-(












- -

FIELD DATA


Date ~ () ~ f 9













lfJ D 1 H I

~ r -1 l l I [) ) J_JIC ~ I INl ) - ( I~()

) l I IV i-lt middot ) 1 - 0~ ) Y -11








_ I 11 - yen c-Y - _ - ~

- -to-1i 5 6 deg1

__ __________ _



Run Number ____c= _ _______



I




~ l ~ l lol X o



~~-I j1 vbull- ~JI






I I c Iv I l 1-1 11 -

v-1 Dll - ~



FIELD DATA









Stack Temp

Ts (F) ti( I 11

lt j

(

I




Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(


bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l


I IP I 7

I Lfo )


t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~


- I (() -J~

c f --- -

I

) clbull


1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation



















- -

FIELD DATA


Date ~ () ~ f 9













lfJ D 1 H I

~ r -1 l l I [) ) J_JIC ~ I INl ) - ( I~()

) l I IV i-lt middot ) 1 - 0~ ) Y -11








_ I 11 - yen c-Y - _ - ~

- -to-1i 5 6 deg1

__ __________ _



Run Number ____c= _ _______



I




~ l ~ l lol X o



~~-I j1 vbull- ~JI






I I c Iv I l 1-1 11 -

v-1 Dll - ~



FIELD DATA









Stack Temp

Ts (F) ti( I 11

lt j

(

I




Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(


bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l


I IP I 7

I Lfo )


t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~


- I (() -J~

c f --- -

I

) clbull


1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








__ __________ _



Run Number ____c= _ _______



I




~ l ~ l lol X o



~~-I j1 vbull- ~JI






I I c Iv I l 1-1 11 -

v-1 Dll - ~



FIELD DATA









Stack Temp

Ts (F) ti( I 11

lt j

(

I




Pump Vacuum

(in Hg) -middot-

-- )

-)

Heated Probe Temp

(F) JI

l

Filter Dox

Temp (F) t IA ( -

lmpingcr Temp

(F) _ gt (

(

_ middots r tbull

I lt- -1 k -(


bull J 7 l h J

I i ) I

i lt ~r

~ -

_ middot J

( rJ ) --d 1

J q I

h-i 5 r -

--- -~

-

J_l

V -

A Al

l


I IP I 7

I Lfo )


t

v -~

ltbull I

r r_bull I

bull I

1 middot middot1 ~


- I (() -J~

c f --- -

I

) clbull


1 -

L

oo11

f ]A

I

v

bull I I -

-

mbullbullI0

f

FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








FIELD DATA








I ~ ~ - 11 v_ I _ L- ( l



-u _ _f) JlJut- _

r


- L V



- - 7- t-lo TO )- ) J JI) L) f-v ) - ) I



-middot [I -



FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation









FACILITY

SOURCE

DATE

RUN

METHOD

BOX


GRAJVIS

INITIAL

GRAMS

TOTAL

GRMIS




INITALS


FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation









FACILITY

SOURCE

DATE

RUN

METHOD tJ BOX

EYIPINGER

I

2

3

4

CONTENTS

0 I ~ 1-~03

01 JJ 1-~o

EMPTY

SILICA GEL

FINAL

GRA1IS

cfcr~i rolJ_

S-2J

f292

INITIAL TOTAL C

GRAMS GRAMS


SICi

80 =

J middot7

l 1 r


INITALS a 7


FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation









FACILITY ~o~s g-- l

SOURCE

DATE os - 2-c- ct~

3RUN



GRltIYIS

INITLL

GRAt-1S

TOTAL

GRAt1S





INITALS f7

APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








APPENDIX B-1


21


May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation









May 12 1998


Attn Dennis Becvar

Job No 38042 s

LABORATORY REPORT



Analysis







LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation










LABORATORY REPORT



Sample ID


Detection Limit

Date Analyzed


Sample Duplicate

Average Sample RPO

Spike Cone

MS Result Recovery

Date Analyzed


78 33 0332 26 11 130 20 0408 53 8 150 930 0348 52 320

66 67 0522 34 3 48 67 0455 22 3 51 3 0281 14 08

09 ND 0253 02 NDlt02

01 1

5-7-98



5-7-98

Nickel

151 156

1535 33

100

241 875

Chromium

930 940

935 11

100

1060 110













QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation



















QC Abbreviations







COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation










COMMENTS


~




t~lv f( k-~

R~ )


A

Ymiddot )f

J_

1iJl1i

Jh1

1~~ ~Ji sw 5v


Rellnqul1hed by

f

I-

i f f

(

J

Company IES-Company

Company




I





-j 1 7 11 I_y

y I f (




Company DateTime


APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








APPENDIX B-2


22


June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation









June 10 1 1998


Attn Dennis Becvar

Job No 38288 s

LABORATORY REPORT



Analysis



PhD





LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation










LABORATORY REPORT





Foss Run 1 65 148 0485 J2 72

Foss Run 2 41 18 0414 1 7 74

Foss Run J 24 JS 037 89 14






Chromium Nickel



Spike Cone 100 100






LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation










LABORATORY REPORT




Sample ID Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection Limit 001





Nickel

Sample ND

Spike Cone 10



Spike RPD 10














QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation



















QC Abbreviations












~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation















~


I

I

(

Sample ID I


1-

1 1 I r--i JIL J )

I

JJ Ft4


f

t bull 1-A-LwI

( I

1- 1 tf_1~ i- y ( A)i rhJ_ r )

i- - )

~) y

1h f I ftr (

II




fn


APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








APPENDIX B-3



May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation









May 12 1998


Attn Dennis Becvar

Job No 38041 s

LABORATORY REPORT




Analysis Page

Nickel by ICPMS 2






LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation










LABORATORY REPORT




Sample ID Nickel

AMB 1 430 49 AMB 2 430 002 AMB 3 430 34 AMB 4 430 41

AMB 1 52 43 AMB 2 52 56 AMB 3 52 34 AMB 4 52 71

Filter Blank 001

Detection Limit 001





Nickel

Sample 003

Spike Cone 10



Spike RPO 00







sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation












sample Nickel

IH Filter 1 55

IH Filter 2 15

IH Filter 3 45

IH Filter 4 33

Detection timit





Nickel

sample ND

Spike Cone 10



Spike RPO 10














QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation



















QC Abbreviations






p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



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I



1) essage

-lt

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Phoae 213 722 8810 Fax 213 888 1493




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I -

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I

- I i

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F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

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Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

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Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

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fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation









p MAIL RE



-_

I COMMENTS

~ ~ I

frac34i

j E J J ~

~ ~ Q Q


I lt- AY q_ I ) --l ~


J ~ I

~ 2-- -

1i J bull

I(


l_~~--bull


Rellnqul1hed by

~3 Remarks

1 -( 1 tko 7 -f

~c r 1 ) 1 f

[I+- j_ 1 rj1- 7 l riIY t 1 ii ( y

y y 1Jflt-

Company






APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








APPENDIXC


ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








ft 3109458262 P02 _

I

I I




AN ZOlol14

a

Paa I















I



I


I i i

fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








fr 3109458262 P03 I


PERMIT TO OPERATE

11rmi1 No W71Sl

AN206C24 Pgtce I


Conditiom


I


3




NOTICE


i


BXEClJlIVE OFACE~

~n ~J~_

ByDorrisM~I

Oaobcr7 1992 i

ORIGINAL

APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








APPENDIXD





0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation











0

~ ~ lt

~ z i m z i r

m JJ lt 0 m l


Time

Flow

Rate

Meier

Gamma

Dell H l



Reading Reading



73 280 040 1000 t74 I

10 307316 318041 10726 377240 387978 foiii( 72 80 74 77 190 068 1008 t781


40 329476 340453 10978 399436 410418 bull tcraquo~iW 74 88 80 84 100 108 1008 1853

~

Average 1006 1792

11bull[II




0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation











0 0 m z s ~ z m

~ en m u s 0 m z

Orlllce

M nom ter

S ulng

HbullH20

bull 05bull

10

20 bullmiddot

(0

Initial Fln1I

Reference Reference

OGM OGM

Reading Reading

Vbullfl3 Vbullfl3

251778 262188

282682 272751

273310 283879

284997 295231

Reference

Gas

lnlllol

DGM

Fino

DGM

Test

OGM Reference



1o39dl 389841 I 380285 I 16424 I 68

ioosJgtI 3eo766 I 390952 I ~ K~~7 10

01119+1 391500 I 401942 L io~~2bull1 11

1021-iltI 402241 I 413521 I S1Jeo 1 12

Temperature Aun

TimeDGM OGM DGM



71 68 280

84 73 180

91 77 130

96 80 100

Flow

Rate

Obullcfm

040

055

078

100

MelOI I Della H)

Gamma

1769

1778

1745

0925 middot 2112

fl

Average 0984 1851

111CII



1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation










1 2 3

A1 0115 0114 0113 0114

A2 0193 0192 0193 0193

A3 0255 0256 0255 0255

A4 0312 0313 0314 0313

AS C38 G380 0380 03i9

A6 0433 0432 0433 0433

A 0501 0499 0500 0500 lt

B1 0114 0114 0114 0114

B2 0192 0192 0192 0192

83 0253 0253 0254 0253

B4 0312 0310 0310 0311

85 0382 0382 0382 0382

B6 0433 0432 0433 0433

B7 0499 0498 0498 0498

X2 0158 0159 0162 0160

X3 0187 0187 0186 0187

X4 210 0211 0209 0210

XS 0239 0241 0239 0240

X9 0334 0336 0336 0335

X16 0250 0251 0252 0251

MS 0274 0275 0275 0275

44PB 0310 0307 0309 0309

Calibrated by

Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








Nozzle Calibration


A C

B

A= 01880 B = 01890 C = 01840

Average = 01870


-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








-------------------------------- sect18~

_



Calibrated by

Date





N-W-JjVkul - 0 (_


0 0 0 9131Y = if e = A=



PA= O dtJ cm (in)


Comments

L-R- ~ Jv


____________

0

06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








06-02-1998 1251PM FR01 TO 16268140020 P01

To


I



lt

I



1) essage

-lt

_

) t


Phoae 213 722 8810 Fax 213 888 1493




i I

r)

-bullmiddot

I -

I i i I I i

I

I I I I I

i

I

i f

I

- I i

I t


F-



(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation










(213) 722--6810 FAX (213) 888-1493



5AIJ0

lV d- CA 17Camp




ho ff 2

S-t tG 7


1 l 0

24amp 110





TOTAL P03

06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








06-02-1998 1252PM FRCM TO 162681401320 P02



I I











I I



I i ~

Ii

bull



















R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation























R-ei ~ I

Rec~ 2






(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation










(213) 722-8810 FM (213) 888-1493


l~lOO B-oolt~ i)f 0

1ve 1co RECERi DATE






210

2llt






APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








APPENDIX E-1






r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation












r n+ l- t s 1t I---

--ft4

lOO

Totalizer

Amp Meter (amps)

Oo t q IL

i90D

ZsPI

foo 0011 TT

~ ) ~

eJ

nnr-Jl

f) )I)


7t7 -ft 1t2



Platino Rate




90





Platinq Rate








Platinq Rate


Air Pressure (psig)






I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation












I




90

~)




Platina Rate


Tank Totalizer

Amp Meter (amps)

fi_AJ

A~r~f

OrJ

rn J r f

PJO

7Jr 71J

JJ

r - J

n1i

JO)

Zfqj

)7])

o~

f __

1-~ _ A7

yJ




Platinq Rate


Air Pressure (psig)






Platinq Rate



Ir-----




Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation










Time ~~O

Tank JltI~






Platinq Rate








Platino Rate



Tank Prtgt1-

Totalizer 0~-9





Platino Rate



9_fS

r fAJ r - t

t7299 49s-p

amp7 J ~))

71 o O 0

Cl~ 0l

I _-_

fP-J f~ -1~


C PO

it -O

OIJ

I ~Lmiddot-r

r f_ JJ

~tf67~ C)fofltt

fcO PtJCJ rO 6I

f~ yen0

rJi v F

r ettJ t7spound

9JO

rO JC

P

j ifgti urJ7

Poo tO

(7

7~

(

J lt~J

middoten __ JI R 1

rJ~rPJ

17t 1~ -

f 2JO J_(Jf)

O (J

~CJ J~

7~ 0J

R R vsmiddot55

Jir9 - J _JL

0~P 17fff(7

POO POO

CJ

9t7 JO

7H JA

p -~t

fhJ- _r 0 -

-4o I2h9P~ -P~O

yClO tJtJ 70C

PI 6 7

CJ -+) O

d) (~

p F p


APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








APPENDIX E-2





I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation











I

Totalizer 11001 1~






Platina Rate


Time 1 ro Tank J -

Totalizer O~_M






Platino Rate








Platinq Rate


s R ~_ 1

rr 4~I

1nn6

9t

JO

o Fl tI

j l-A~

cxho~ Pt11

Yh 1C)

Ff

()

s n~t lO 1)16

JPlO

9G

scJ

riFF 0

r20 triiT JJ7ifJ

nlJr

t

70


7ft

rI

tJ1

-fC)

tiff ()

2fr 1ro+ J ~ p-

-

2Jn

)t

-ft

rr 0

1~QJ ~M)) )

IOIJ

6 50

Ff tI

J Pm-

f-LC

C-no

9~

O

()

~ 11a+ m1l~9

ftJO

C

CJ

rt 0


00~ff 00 11

2DOO Poo

J1 9t5 _a 70

ofF cfF ~

~-JI

7hol (Aoif

~~~ -~ 1ai- 791

tooo Pro

tJ~ 9 -

-fCJ

fp oFi= ti n


~OCO PlCJ

2 9C ~C1 10

1itF nFf tJ 0





JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation











JO ~11 f 7r9 n-r2c1

~oz~~



70




Platinq Rate


)tJj

Jl7~CJ7-I-

r f_~J

llll-19

~-bullA(

7ht1 I9

rpound-l All 70

A~1

c7oM

- Z7 TJIIW r_f

ofJrP





Platinq Rate






Platina Rate






Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation










Time rrr t~




ycJ() yJ 2~ PJ




Plating Rate





Platina Rate



O~f-1P

C1f2-9 Pt 07JP





Plating Rate






























2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation



































2













3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation




















3

APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








APPENDIXF








Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation














Sa111pl11 ~057



~AW DATA

NICKEL I

8 25 ozgal

NICKEL SULFATE

307 oiiJal



I

liH 343 3 43 I

SURFACE I


~-901 ()33

i bull I

S0 ~d 111DY-OW 1511 l-0310111 6Sst 866180S0








ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation















ANALYSIS STANdegRD

~ICKEI

NICKEL SULFATE


BORIC ACID

pH QJRFACE TENS ION

M-901

~AW DATA

10 3 ml

middot7 2 ml

140 ml

~-45

345 dynecm i I

q51

807 ozgal

572 ozia1

580 ozgal

34 dynecm

443 gaJ 1000 gal

65=51 86618050



1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








1



CUSTOM11________________ B050119

0510698



1




ljICKEL


isoRIC ACID

pH I

SURFACE TENSION I

ljl-901

RAW DATA

o7 1111

i

3 ml

)44 1111

~-58

3~4 dynecm

Q52

844 oZiJal

31 4 OZiJal

578 Ciiiilampl

S98 ozgal

354 dyn~cm

446 gal 1000 9al

Imiddot I I

i~CONT bull bull I





DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation











DATE RECEIE0__0_5_1_0_6_19_8__





I

jRAW DATA






~H -~ 3o5

I

SURFACE TENSION I


i-1-901

bs2 444 gal

middot 1000 val

i

i i

bull

I i

Ii

lOllfI 100ll CONI

TOTtL Pefl








__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation














__s_a_rnp_1_e_1_1_0_5_s__~_49amp_ Cl-3V


AMALVSIS RlSULTS

MICKEL I

I

iNICKEL SULFATE

~IC~ CHLORIDE

~ORlC Ac10

HIIp


I

I I I I

I

I lOIIM 002 CON1

I E0 3pound)11d

tfAW DATA I205 ml i

7 1 1111 I

i 144 ml

s20 oga1

565 o~ilal

~95 ozgal

359 dynecm


6ss1 e66tte01s0

I I

middot1

I I

middotI

El01S0E9Z9






Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation













Samp 1 a 1 1056



NICKEL

NICKEL SULFATE

NI CKEL CHLORIDE

BORIC ACID

pH

SURFACE TENSION

middot M-901

RAW DATA

103 ml

i 1 ml

3b6

34d dynecna

052

809 ozgal

lOO ozgal

564 oz ial

5~ 019al

366

346 dynacm

448 gal 1000 cal


1bull












J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation


















J1


w




Igt -i


r- __ lfbull ~










APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








APPENDIXG








Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation














Nickel Metal ozgal


ADDITIVES






SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation











SAMPLE DA TE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation














Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES





SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation











SAMPLE DA TE

BATH COMPOSITION

Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




4 17







SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation











SAMPLE DATE



Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES








Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation














Nickel Metal ozgal



Boric Acid ozgal

pH

ADDITIVES




DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation










DATE RECEIVED ( 2 c






1RM 1002 CONT









ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation
















ORM 1002 CONT








SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation















SURFACE TENSION

ORM 1002 CONT







SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation














SUFFACE TENS I Ot

lRM 1002 CONT









)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation
















)RM 1002 CONT









(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation
















(

ORM 1002 CONT

Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








Appendix G



Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation









Prepared For

Prepared On

Prepared By

Telephone


TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation









TABLE OF CONTENTS

Page




SECTION 4 RESULTS


LIST OF TABLES





LIST OF FIGURES





APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








APPENDICES





GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation









GENERAL INFORMATION

Facility



Telephone Fax

Telephone Fax



Schedule


10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation









10 INTRODUCTION




facility

Tank No

Operating Amperage

Dimensions (LxWxH)

Tank Contents

Emission Control

Lip Exhaust

Fume Hood

Air Agitation








Research Contract Report · 68 . field data inputs: rectangular stack area (sq ft) volume sampled,...

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Transcript of Research Contract Report · 68 . field data inputs: rectangular stack area (sq ft) volume sampled,...