REPORT on the Activities of Core Facilities
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REPORT ON THE ACTIVITIES OF CORE FACILITIES NANOFABRICATION AND NANOCHARACTERIZATION STRUCTURAL ANALYSIS LABORATORY
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Transcript of REPORT on the Activities of Core Facilities
REPORT ON THE ACTIVITIES OF CORE FACILITIES
NANOFABRICATION AND NANOCHARACTERIZATION
STRUCTURAL ANALYSIS LABORATORY
| 3www.ceitec.eu
CONTENT
ABBREVIATIONS
03 Timeline
Vision and Mission
Staff
Installed and used instruments
Usage
Expected costs in full operation
Technological units
Organizational chart
Services and Collaboration
Case studies
Collaboration
Challenges and Success
Contacts
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CF Core Facilities
BUT Brno University of Technology
MUMEYS
Masaryk University
Ministry of Education, Youth and Sports
TIMELINE
The core facilities Nanofabrication and Nanocharacterization Structural Analysis Laboratoryand are centralized shared re-search resources that provide an access to instruments, technologies and services, as well as expert advice, and other services to researchers and industry. Both core facilities are a part of the research infrastructure CEITEC Nano.
CEITEC project approved by the European Commission
Construction of new CEITEC BUT buildings officially launched
Fusion CF Nanofabrication and CF Nanocharacterization into1 CF Nanofabrication and Nanocharacterization
Implementation of the infrastructure rules to all users
Preparation of infrastructure rules based on the open access principles
CF Nanofabrication, CF Nanocharacterization and CF Structural Analysis Laboratory established
CF laboratories and clean rooms designed
Temporary installation of 12 CFs instruments
Installation of instruments in the provisional buildings
Temporary installation of 3 new CF instruments
Research infrastructure CEITEC Nano on the Czech Roadmap for Research Infrastructures for the period of 2011–2015
First instrument tenders
Contract between BUT and MU regarding the common shared core facilities
Research infrastructure CEITEC Nano on the updatedCzech Roadmap for Research Infrastructuresfor
the period of 2016 - 2020
Research infrastructure CEITEC Nano in MERIL(Mapping of the European Research Infrastructure Landscape)
Installation of the first 3 CF instruments
Start of CEITEC - open access project
Fully operational state of CFs
| |4 5Central European Institut of Technology www.ceitec.eu
VISION AND MISSION
STAFF
INSTALLED AND USED INSTRUMENTS
to perform as facility providing excellentservices to scientific community and industry
to establish the research infrastructure based on the open access rules
to establish short- and long-term cooperation with the scientific community and industry
in-advance to:
provide users the possibility to operate the instruments by themselves
provide access to state-of-art equiment
cooperate with the highly trained personnel
CF Nanofabrication and Nanocharacterization
installed instruments
installed instruments
CF Structural Analysis Laboratory
USAGE
EXPECTED COSTS IN FULL OPERATION
2013 2014 2015 in full operation
| |6 7Central European Institut of Technology www.ceitec.eu
TECHNOLOGICAL UNITS
ORGANIZATIONAL CHART
SERVICES AND COLLABORATION
Core Facility Nanofabrication and NanocharacterizationPortfolio of services
Core Facility Structural Analysis LaboratoryPortfolio of services
CASE STUDIES
Study of light interactionon the submicron structuresCollaboration with plasmonic group at CEITEC BUT
Pattern definition and experimental set-up
Theoretical calculation of light interaction
User training for:
Focused Ion Beam/Scanning Electron Mi-croscope LYRA3
Scanning Near-field Optical Microscopy MV 4000
Structure preparation
Active interface preparation- substrate sputtering (Ti + Au layer)
Structure milling performed by Focused Ion Beam/Scanning Electron Microscope LYRA3
Experimental results confirmed at SNOM Ntegra Solaris and Scanning Near-fiealdOptical Microscopy MV 4000
Publication:
DVOŘÁK, P.; NEUMAN, T.; BŘÍNEK, L.; ŠAMOŘIL, T.; KALOUSEK, R.; DUB, P.; VARGA, P.; ŠIKOLA, T.Control and Near-Field Detection of Surface Plasmon Interference Patterns. NANOLETTERS, 2013, 13 (6), pp 2558-2563.ISSN: 1530-6 84. (IF = 13.025)
| |8 9Central European Institut of Technology www.ceitec.eu
Study of spin circulationin nanodiscsCollaboration with spintronic group at CEITEC BUT
Pattern definition and experimental set-up
User training for:
Focused Ion Beam/Scanning ElectronMicroscope LYRA3
Scanning Near-field Optical Microscopy MV 4000
Lithographic Scaning Probe MicroscopeDimension Icon
Structure preparation
Active interface preparation- substrate sputtering (Ti + Au layer + NiFe)
Pattern definition - multistep electron beam lithography by Focused Ion Beam/Scanning Electron Microscope LYRA3
Structure milling performed by Focused Ion Beam/Scanning Electron Microscope LYRA3
Magnetic vortices observation by Scanning Probe Microscope AutoProbe CP-R and Lithographic SPM Dimension Icon
Experimental results confirmed at University of California, San Diego
Publication:
UHLÍŘ, V.; URBÁNEK, M.; HLADÍK, L.; SPOUSTA, J.; IM, M.; FISCHER, P.; EIBAGI, N.; KAN, J.; FULL-ERTON, E.; ŠIKOLA, T. Dynamic switching of the spin circulation in tapered magnetic nanodisks. Nature Nanotechnology (print), 2013, 8 (5), pp 341-346. ISSN: 748- 3387.(IF =31.17)
Lorentz corrected SAXS spectra with fitted first maxima qmax which is related to long period.
Reciprocal space maps using different beam collimations.
Perspective-view SEM micrograph of 8 µm tall Si0.1Ge0.9 crys-tals with the embedded superlattice structure on top.
Long period determination in partially crystalline polyolefin
Reciprocal space mapping of facetted Si/Ge microcrystals with deposited strain-symmetrized SiGe/Ge superlattices
Collaboration with company Polymer Institute Brno
Collaboration with research group Functional Properties of Nanostructures at CEITEC MU
Method:
Method:
Equipment:
Equipment:
Small angle X-ray scattering (SAXS),transmission geometry
reciprocal space mapping
X-ray diffractometer Rigaku SmartLab 9kW
X-ray diffractometer Rigaku SmartLab 9kW
Publication:
MEDUNA, M.; FALUB, V.; ISA, F.; CHRASTINA, D; KREILIGER, T.; ISELLA, G.; VON KÄNEL, H. Re-construction of crystal shapes by X-ray na-nodiffraction from three-dimensional super-lattices. Journal of Applied Crystallography, 2014, 47, ISSN: 2030-2037. (IF = 3.95)
| |10 11Central European Institut of Technology www.ceitec.eu
Preparation and characterization of doped titanium dioxide printed layers
Collaboration with research group Advanced CeramicMaterials at CEITEC BUT
Method:
Equipment:
X-ray powder diffraction
X-ray diffractometer Rigaku SmartLab 3kW
Publication:
KRALOVA, M.; DZIK, P.; VESELY, M.; CIHLAR, J. Preparation and characterization of doped titanium dioxide printed layers. Catalysis To-day, 2014, 230, p. 188 – 196. (IF = 3.309)
XRD spectra: pure titania
XRD spectra: Ti_3Fe
XRD spectra: Ti_Ag_7Fe
IN 2013 AND 2014 WE COLLABORATED...
| |12 13Central European Institut of Technology www.ceitec.eu
Quoted from the evaluation reports of czech research infrastructures provided by international experts. The evaluation was managed by Ministry of Education, Youth and Sports, Czech Republic in 2014.
to attract the users all around the world and provide state-of-the-art instrumentation
to guarantee the fair open access for everyone and “self-service” policy
to establish a multidisciplinary centre whose level of integration enables the researchers from different fields to join their resources and expertise and allows the realization of their projects
to integrate approach to fabrication of complex functional nanostructures and nanomaterials, and analysis of their structural, mechanical, electronic, optical, and chemical properties
to foster the development of advanced materials by providing the top-class instruments for detailed analysis of their structural and chemical properties
Installation of all core instruments will be performed in 2015
Core facilities Nanofabrication and Nanocharacteri-zation and Structural Analysis Laboratory will be fully operable in 2016
Core facilities Nanofabrication and Nanocharacteri-zation and Structural Analysis Laboratory successful-ly passed the MEYS evaluation as part of the research infrastructure CEITEC Nano
Research infrastructure CEITEC Nano declared on the Czech Roadmap for Research Infrastructures for the period of 2016 – 2020
Research Infrastructure CEITEC Nano in european database of research infrastructures MERIL
Uniqueness at a national and good recognition at international level
CONTACTS
Centre of Laboratories
Core facility Nanofabrication and Nanocharacterization
Core facility Structural Analysis Laboratory
UV Direct Write Laser system
Optical microsope Atomic LayerDeposition System
Vacuum FTIR
Spectroscopic reflectometer Wire bonder Scanning Near-FieldOptical Microscope
Scanning ElectronMicroscope/e-beam writer
NIR/VIS/UV SpectroscopicEllipsometers
Focused Ion Beam/ScanningElectron Microscope
Mechanical profilometer VUV spectrometer VUVAS 1000 Lithographic ScanningProbe Microscope
Resist stripper SPM/microRaman/PhotoLuminiscence system
Heidelberg Instruments DWL 66 FS
Olympus MX 51 Cambridge NanoTech Fiji 200 Bruker Vertex80v + Hyperion 3000
Ocean Optics Nano Calc 2000 TPT HB 16 Nanonics MV 4000
Tescan Mira3 J. A. Woollam IR-Vase, V-Vase Tescan Lyra3 XMH
Bruker Dektat XT McPherson Bruker Dimension Icon
Diener Nano Plasma cleaner T-MDT NTegra Spectra, Solaris 3
Martin Buršík
Martin Buršík Marek Eliáš Alois Nebojsa
David Škoda Martin Buršík Dalibor Šulc
Eva Kolíbalová Alois Nebojsa Eva Kolíbalová
Dalibor Šulc Alois Nebojsa Dalibor Šulc
Marek Eliáš
David Škoda
Alois [email protected]
[email protected] [email protected] [email protected]
[email protected] [email protected] [email protected]
[email protected] [email protected] [email protected]
[email protected] [email protected] [email protected]
Nanofabricationand Nanocharacterization
X-ray powder diffractometer X-ray diffractometer
Rigaku Smartlab 3kW Rigaku SmartLab 9kW
Pavla Roupcová
Ondřej Man
Ondřej [email protected]
Structural Analysis Laboratory
CEITEC BUT - Central European Institute of Technology
Brno University of Technology
Technická 3058/10, CZ-61600 Brno, Czech Republic
www.ceitec.eu
