ReportcareoFor y 5 Environmental Protection Agency

First International Building1201 Elm StreetDallas, TX 75270Attention: Charles Gazda

o^ugust3l|IiPl!!M^^

^P 9 198f ?•-

^AD/V/SJON |*

P.O.NO. 68-01-6035 Job No. 21881/jig

"oron of Samoles

Enclosed are the reports for sample numbers: F0536, and F0564-F5071,Case number: 580. Chain of Custody was not received.

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••ouic aoG''ecia;e a teleofwie call it you "aw any questions regarding this report. Page 1 of 1 sages.

-. —a; "••s '6001 :'Lily retresents the <inoi''gs of work oerforrreo by me.-'"-•. J 'K'. suDer«isro". _" _ :_ ^ ^

Re/'eweo ana ADorovefl

/ / //.A^.^'...—--Robert Swaim, Ph. D.Staff Chemist

D. J . Northington, Ph. D.Technical Director

'•••s reoort ce'la'ns only 10 t^e samples in^esttgateo ana does not necessarily apply lo other apoarently identical or similar matenals. This report is SiJpmineo tor tnc exclusive Jse o* we ci-eni to -Anom it .s aooressea-py reDroouclion of tnis reDon or use of this LaDO'aiory s name tor aavertising or puolicity purposes without written authonution is pronioited

Ecology and Environment, Inc.

Region VI

MEMORANDUM

TO: Charles Gazda,Chief Compliance Section

FROM: David Anderson, FIT ^ a.E&E Region VI

THRU: K. Malone, FITL ^^E&E Region VI

DATE: September 15 , 1981 ^ ^

RE: TDD F-6-8109-20, Review of Sample Data from Vertac lr\

0Attached is a review of and quantification of 8 well water samples collected by 0the state at Vertac. Only one anomaly appeared in the results, that being thepresence of acetone in 6 of the 8 samples. Acetone has not been present inprevious samples and its presence is probably due to improper preparation ofsample containers or contamination by the analytical lab.

Sources

Standards:EPA Water Quality Criteria DocumentsNovember 28, 1980

Toxici t ies:

- ,v. ^; ^

Registery of Toxic Effects1979 Editiony^fc <(. I F

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ORGANICS TRAFFIC REPORTT) Case Number:

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Sample Site Name/Code:/grtfK Jhc

T) Regional Office:•ximpling Personnel:

.J AD^e.(Name)

•?/ ^•7t-nol(Phone)

ximplingDcrte:

• - 'J -^ -^ / ..S^4*

(Begin) (End)

^) Shipping Information

:x,/Name of Shipper:

-—' " --- <~ ;. - -,?^ - .y/Date Shipped:

Airbill Number:

© Sample Type: (Check One)

___ RunOff

- . WeB

Receiving Water

Leachate

Effluent

Other (specify)

(j) Ship To:

We^ C^^^ Tcth se

\^(y05 P^h^aa^y

Ce^.h^ C.l^

Attn:

^) Description of Sample Location:

H/ / ^/

^) Special Handling Instructions:(e.g., safety precautions, hazardous nature)

; y • •' -, ,./^ /,f/ yREGIONAL OFFICE FILE COPY

Kiffigti

SAMF

LAB

DAT!

DATE

STD

CONC

Acid

21A

22A

24A

31A

34A

57A

58A

59A

60A

64A

65A

Base

1B

5B

8B

9B

12B

l8B

20B

25B

26B

27B

28B

35B

36B

37B

39B

40B

D W€5T COAST T€Ch^

*LE ID F0536

ID 21881A13

; EXTRACTED7/31/81

; INJECTED 8/17/81

ID SENS178 PHEN3E

: FACTOR 1000

Compounds

2, 4, 6-trlchlorophenol

p-chloro-m-cresol

2-chlorophenol

2, 4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol

2,4-dinitrophenol

4,6-dinitro-o-cresol

pentachlorophenol

phenol

/Neutral Compounds

acenaphthene

benzidine

1,2,4-trichlorobenzene

hexachlorobenzene

hexachloroethane

bis(2-chloroethyl)ether

2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1,4-dichlorobenzene

3,3'-dichlorobenzidine

2,4-dinitrotoluene

2,6-dinitrotoluene

1,2-diphenylhydrazine

(as azobenzene)

f luoran thene

4-chlorophenyl phenyl

IICALS6RVH

i5

ug/1

NO

NO

NO

ND

ND

ND*

NO

NO*

117

ND

ND

ND

ND

ND

ND

ND

N D

ND

ND

N D

ND

ND

NDN D

e t h e r N D

:6 INC.

SAMP:

LAB ]

DATE

DATE

STD I

CONC

Base/

41B

42B

43B

52B

53B

54B

55B

56B

61B

62B

63 B

66 B

67B68B

69B

70B

71B

72B

73 B

74B

75B

76B

77B

78B

79B

80B

81B

82B

83B

84B

129B

p-dio0710£S36^ ^

INDUSTRIAL CATEGORY

LE ID F0536

^ D ?1RS1R?

EXTRACTED 7 / ^ 1 / R l

INJECTED s/T^/81

D RFN73q7 R N ^ T n A I A

FACTOR mno

'Neutral Compounds ui

4-bromophenyl phenyl ether

bis(2-chloroisopropyl) ether

bis (2-chloroethoxy) methane

hexachlorobutadiene

hexachlorocyclopentadiene

isophorone

naphthalene

nitrobenzene

N-nitrosodi methyl a mine

N-nitrosodiphenylamine

N-nitrosodi-n-propylamine

bis (2-ethylhexyl) phthalate

butyl benzyl phthalate

di-n-butyl phthalate

di-n-octyl phthalate

diethyl phthalate

dimethyl phthalate

benzo(a) anthracene

benzo(a)pyrene

3,4-benzofluoranthene

b e n z o ( k ) f luoranthene

chrysene

acenaphthylene

anthracene

benzo(ghl )pery lene

fluorene

phenanthrene

d i b e n z o ( a , h ) a n t h r a c e n e

indeno( 1 ,2 ,3-cd)pyrene

pyrene

2,3,7,8-tetrachlorodibenzo-

xin fi^lO^M^ri

^1N D

ND

ND

ND

N D

ND ^>

N D ^u\

ND

N D <-)

ND 0

ND

ND

ND*

ND*

N D

ND

ND

ND

N D

ND

N D

N D

N D

N n

N D

N D

M D

N D

ND

SAMP

LAB

DATE

STD :

CONC

Volat

2V

3V

4V

6V

7V

10V

11V

13V

uv15V

l6V

>imxxm^m)(»)^x^xx^Mixxxxxxxxxxx19V

23V

29V

30V

32V

33V

38V

44V

45V

46V

47V

48V

49V

50V

51V

85V

86V

87V

88V

^ WCS 1 UJAST T6CHNICAL

LE ID F0536

ID 21881V2

INJECTED 8/5/81

ID BFB35 VOA156 DATE INJECTED 8/6/81f A f~"Tt~\T> -

lies

acrolein

acrylonltrile

benzene

carbon tetrachloride

chlorobenzene

1,2-dichloroethane

1,1,1-trichloroethane

1,1-dichloroethane

1,1,2-trichloroethane

1,1,2,2-tetrachloroethane

chloroethane

2-chloroethylvinyl ether

chloroform

1,1-dichloroethylene

1,2-trans-dichloroethylene

1,2-dichloropropane

1,3-dichloropropylene

ethylbenzene

methylene chloride

methyl chloride

methyl bromide

bromoform

dichlorobromomethane

trie hlorofluorome thane

dichlorodif luoromethane

chlorodibromo methane

tetrachloroethylene

toluene

trichloroethylene

vinyl chloride

S6RVICG

LAB ID TRACE N141

DATE EXTRACTED 7/31/81

ug/1

ND

ND

N O

ND

N D

ND

ND

N D

N D

N D

ND

ND

13

ND

ND

ND

N D

N D

19

ND

ND

ND

N D

ND

ND

N D*

N D

N D

N D

INC INnii^TRlAi i ^i.-^ORY

SAMPLE ID F0536

STD ID TRACE #4140

CONC. FACTOR 50

Pesticides

89P aldrin

90P dieldrin

91P chlordane

92P 4 ,4 ' -DDT

93P 4 , 4 ' - D D E

94P 4 , 4 ' - D D D

95P alpha-endosulfan

96P beta-endosulfan

97P endosulfan sulfate

98P endrin

99P endrin aldehyde

100P heptachlor

101P heptachlor epoxide

102P alpha-BHC

103P beta-BHC

104P gamma-BHC

105P delta-BHC

106P PCB-1242

107P PCB-1254

108P PCB-1221

109P PCB-1232

HOP PCB-1248

HIP PCB-1260

112P PCB-1016

113P toxaphene

••'•• = Less than 10 ug/1

(pesticides less than 5 ug/1)

ND = Not detected

-;,--„- ^ ^o^ confirmed by GCMS

GW

ug/1

ND

. ND

ND

ND

ND

^ ND

^ ND-tf<———

N D

0 ND

0 N D

N D

N D

N D

ND

ND

ND

ND

N D

N D

ND

ND

ND

N D

N D

N D

^4f7

17605 Fabnca Way Suite 0 Cerntos. Cali fornia 90701 2 1 3 / 9 2 1 - 9 8 3 1

WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3

QC Report No: 36Sample Number

F0536

A. SURROGATE SPIKE RESULTS

COMPOUND

Benzene - d6

l-Chloro-2-Bromopropane

Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyl

Naphthalene-DS

Fraction

VGA

VOA

VGA

ACID

ACID

B/N

B/N

B/N

Cone.(ug/1)

49

46

48

72

92

69

75

74

(Surrogates only)Spike

Added (uq /1)

50

50

50

100

103

1 0 1

1 0 1

101

%Recovery

98

92

96

72

89

68——————66

74 ^

73 IT

1.

2.

3.

4.

5.

6.

7.

8.

9.

10.

1 1 .

12.

13.

14.

15.

16.

17 .

18.

19.

20.

CAS # COMPOUND NAME FRACTION

% Maximum Score Attained 0

Mass Matching Routine: FIT(specify)

'

————————(m0^938——

^}tml'2t-styrV/ « J* V tff^J^i ^

•' -7

-r-.T- ~^hrif,i w-iv Suita D Cerritos California 90701 ?11 •n^i ^ " 1 1

ORGANICS TRAFFIC REPORT(l) Case Number:

£so

Sample Site Name/Code:

Vfyt^t, J^C ,

© Sample Type: (Check One)

___ RunOff

-X WeH

Receiving Water

Leachate

Effluent

Ofher (specify)

(j) Shy To:

Wcsl- C^sf 7 ' se\<'f7k06 /^/<^

Ce^^f^^ ^^^^^D7P/

Attn:

'^i^^*\ P^^^e^

(^Regional Office:

Sampling Perscnnel:

t^^ M^.^.fftwY)

(^) Mark Volume Level on Sample Bottle

(Name)

.fD/ -^f-no^ Extractable

(Phone)

Sampling Date:

7-J^-^/

Extractable

(Begin) (End)Extractable

(6) Shipping Information Extractable

J^y J^JT// KTi^-mo .^^nr~\rv=i

^y ^JT/i<Zi KTi -mo i f . n r~\rv=ir'

VOA Unpreserved7

/ Name of Shipper:

-7- 3 o " gyVOA Unpreserved(Duplicate)

Date Shipped:

Airbill Number:

DateSampled

7-2 7- /

(7) Description of Sample Location:

Welf ^ ^

(s) Spedai Handling Instructions:(e.g., safety precautions, hazardous nature)

, /^^..i>i (-'-< •''fi'

REGIONAL OFFICE FILE COPY

W€5T COAST TECHNICAL S6RVICG INC. INDUSTRIAL CATEGORY

SAMP

LAB •

DATE

DATE

STD 1

CONC

Acid

21A

22A

2^A

31A

34A

57A

58A

59A

60A

6^A

65A

Base/

1B

5B

8B

9B

12B

18B

20B

25B

26B

27B

28B

35B

36B

37B

39B

^OB

LE ID F0564

[D 21881A2

EXTRACTED 8/1/81

INJECTED 8/9/81

'.'D SENS176 PHEN353

FACTOR 1000

Compounds u

2, L., 6-trichlorophenol

p-chloro-m-cresol

2-chlorophenol

2,4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

^-nitrophenol

2,4-dinitrophenol

U,6-dinitro-o-cresol

pentachlorophenol

phenol

'Neutral Compounds

acenaphthene

benzidine

1,2,^-trichlorobenzene

hexachlorobenzene

hexachloroethane

bis(2-chloroethyl)ether

2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1,4-dichlorobenzene

3,3'-dichlorobenzidine

2,^-dinitrotoluene

2,6-dinitrotoluene

1,2-diphenylhydrazine

(as azobenzene)

f luoranthene

^-chlorophenyl phenyl ether

g/1*

ND

ND

14

ND

ND

ND

ND

ND

ND*

ND

ND

N D

ND

ND

ND

ND

ND

N D

ND

N D

ND

N D

NnN D

ND

SAMP

LAB

DATE

DATE

STD

CONC

Base,

41B

^2B

A3B

52B

53B54B

55B

56B

61B

62 B

63 B

66B

67B

68B

69 B

70B

71B

72B

73B

7AB

75B

76B

77B

78B

79 B

SOB

81B

82B

83B

8^B

129B

p-dic

LE ID F0564

ID 21881B3

. EXTRACTED 7/31/81

INJECTED 8/13/81

ID BENZ397 BNSTD414

FACTOR 1000

/Neutral Compounds us

4-bromophenyl phenyl ether

bis(2-chloroisopropyl) ether

bis (2-chloroethoxy) methane

hexachlorobutadiene

hexachlorocyclopentadiene

isophorone

naphthalene

nitrobenzene

N-nitrosodimethylamine

N-nitrosodiphenylamine

N-nitrosodi-n-propylamine

bis (2-ethylhexyl) phthalate

butyl benzyl phthalate

di-n-butyl phthalate

di-n-octyl phthalate

diethyl phthalate

dimethyl phthalate

benzo(a) anthracene

benzo(a)pyrene

3,4-benzofluoranthene

benzo(k ) f luoran thene

chrysene

acenaphthylene

anthracene

benzo(gh i )pe ry lene

fluorenephenanthrene

d ibenzo (a ,h ) an th racene

indeno( 1 ,2 ,3-cd)pyrene

pvrene

2,3,7,8-tetrachlorodibenzo- l J ' J

(mo is

1ND

ND

ND

ND

N D 0

N D ^——tf\ND

ND 0

N D O

ND

ND

11

ND*

ND*

ND

ND

ND

ND

N D

N D

N D

N D

N D

N D

N n

N nwnN D.05940

'ND

^-^.-^ WCSl t-uAST TECHNICAL

SAMPLE ID F0564

LAB ID 21881V3

DATE INJECTED 8/5/81

STD ID BFB35 VOA156

CONC. FACTOR ———-

Volatiles

2V acrolein

3V acrylonltrlle

4V benzene

6V carbon tetrachloride

7V chlorobenzene

10V 1,2-dichloroethane

11V 1,1,1-trlchloroethane

13V 1,1-dlchloroethane

14V 1,1,2-trichloroethane

15V 1,1,2,2-tetrachloroethane

l6V chloroethane

)imXXmmm»)^}WXMl»MiXXXXXXXXXXX

19V 2-chloroethylvinyl ether

23V chloroform

29V 1,1-dichloroethylene

30V 1,2-trans-dichloroethylene

32V 1,2-dichloropropane

33V 1,3-dichloropropylene

38V ethylbenzene

44V methylene chloride

45V methyl chloride

46V methyl bromide

47V bromoform

48V dichlorobromomethane

49V tr ichlorofluoromethane

50V dichlorodif luoromethane

51V chlorodibromomethane

S5V te t rachloroethvlene

SoV toluene

S7V tr ichloroethvlene

SSV vinvl chloride

17605 FaDnca Way Sui te D Cern'o

SfctWii-c

LAB ID TRACE N144

ug/1

ND

NO

N D

NO

ND

NO

N D

N D

N D

N D

ND

ND*

ND

ND

ND

ND

N D

20

N D

ND

N D

N D

ND

ND

N D

10

N D

W

N D

INC. INLJU^ 1 Mi/-..- v-^< ^uOKY

SAMPLE ID F0564

DATE EXTRACTED 7/31/81

DATE I N J E C T E D 8/6/81

STD ID TRACE N143

CONC. FACTOR 50

Pesticides

89P aldrin

90P dieldrin

91P chlordane

92P 4 ,4 ' -DDT

93P 4 ,4 ' -DDE

94P 4 , 4 ' - D D D

95P alpha-endosulfan

96P beta-endosulfan

97P endosulfan sulfate

98P endrin

99P endrin aldehyde

100P heptachlor

101P heptachlor epoxide

102P alpha-BI-IC

103P beta-BHC

104P gamma-BHC

105P delta-BHC

106P PCB-1242

107P PCB-1254

108P PCB-1221

109P PCB-1232

HOP PCB-1248

H I P PCB-1260

112P PCB-1016

113P toxaphene

••'•" = Less than 10 ug/1

(pest icides less than 5 ug/1)

ND = Not detected

••'•-* = Not confirmed by GCMS

0!2-1-

s. C a l i f o r n i a 90701 213/921-9831 O^'l

Ug/1

0.1**

2.5**

ND

1.6**

NDr-

ND^

O.I1**

^0ND-,

0.1**

1.0**

N D

ND

0.6**

1.5**

1.8**

0.7**

N D

N D

N D

ND

ND

N D

ND

N D

e^5bo

,05941

WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3

QC Report No :_ 36Sample Number

F0564

A. SURROGATE SPIKE RESULTS•

COMPOUND

Benzene - d6

l-Chloro-2-Bromopropa.ne

Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyl

Naphthalene-DS

Fraction

VOA

VOA

VOA

ACID

ACID

B/N

B/N

B/N

C o n e . ( u g / 1 )

49

45

47

84

103

52

64

59

(Surrogates only)Spike

Added (ug /1 )

50

50

50

100

103

1 0 1

1 0 1

1 0 1

%Recovery

98

90

94

84

100

51

63

58

B . TENTATIVELY IDENTIFIED COMPOUNDS

1.

2.

3.

4.

5.

6.

7.

8.

9.

10.

1 1 .

12.

13.

14.

15.

16.

17 .

18.

iq

20.

CAS ft COMPOUND NAME

ACETONE

.

FRACTION

VOA #85

% Maximum Score Attained

Mass Matching Routine: FIT(specify)

882

•

•

(VW^5C^

- ... - n 'i n.s

c

^

^{\'7

ORGANICS TRAFFIC REPORT(T) Case Number:

^0

Sample Site Name/Code:

'/f/t^^ .T^L

©D Sample Type: (Check One)

Run Off

/^Well

——— Ffeoeiving Water

Leachate

Effluent

Ofher (specify)

(J) Ship To:

^J-A C^J-^ Tc^.J^17^W F^bf'.'c^ ^y

Ce^'/^ ^/'

^070fAttn:

A;') c'<-,

(?) Regional Office:Sampling Personnel:

^^J /kIL^W

(^) Mark Volume Level on Sample Bottle

(Name)

;^/ ?-?/-/7^ /Extractable

(Phone)

ScimplingDate:

2,1^-JU-

Extractable

(Begin) (End)Extractable

(^) Shipping Information

T TT-/'J{., , J^ .f t.' (.

Extractable

VOA Unpreserved

Name of Shipper:VOA Unpreserved(Duplicate)

Date Shipped:

.., •— '-•"* •--- ""»-/ 5 .:> ..-) / 3Airbill Number:

(7) Description of Sample Location:

(J) Special Ifandling Instructions:(e.g., safety precautions, hazardous nature)

REGIONAL OFFICE FILE COPY

Q iozsga07105943

WSfSsSs

SAMP

LAB

DATE

DATE

STD •

CONC

Acid

21A

22A

24A

31A

34A

57A

58A

59A

60A

64A

65A

Base/

1B

5B

8B

9B

12B

18B

20B

25 B

26B

27B

28B

35B

36B

37B

39B

40B

-0 WEST COAST TECHNICAL

LE ID F0565

ID 21881A5EXTRACTED s/ i /gi

INJECTED 8/9/81

ID SENS176 PHEN353

FACTOR 1000

Compounds u

2,4,6-trichlorophenol

p-chloro-m-cresol

2-chlorophenol

2,4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol

2,4-dinitrophenol

4,6-dinitro-o-cresol

pentachlorophenol

phenol

Neutral Compounds

acenaphthene

benzidine

1,2,4-trichlorobenzene

hexachlorobenzene

hexachloroethane

bis(2-chloroethyl)ether

2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1,4-dichlorobenzene

3,3'-dichlorobenzidine

2,4-dinitrotoluene

2,6-dinitrotoluene

1,2-diphenylhydrazine

(as azobenzene)

fluoranthene

4-chlorophenvl phenyl ether

5€RV

g/1

ND

NDNONDNDNDND

NDNnNnNn

ND

NO

ND

ND

ND

NDNDNDNDNDND

ND

ND

NnND

ND

IC6 INC.

SAMP

LAB

DATE

DATE

STD ;

CONC

Base/Neutral Compounds u^

41B

42B

43 B

52B

53B

54B

55B

56B

61B

62B

63B

66B

67B

68B

69B

70B

71B

72B

73B

74B

75B

76B

77B

78B

79B

80B

81B

82B

83B

84B

129B

p-dic

INDUSTRIAL CATEGORY

LE ID F0565

ID 21881B6

EXTRACTED 7/31/81

INJECTED 8/13/81

[D BENZ397 BNSTD414

FACTOR 1000

4-bromophenyl phenyl ether

bis(2-chloroisopropyl) ether

bis (2-chloroethoxy) methane

hexachlorobutadiene

hexachlorocyclopentadiene

isophorone

naphthalene

nitrobenzene

N-nitrosodimethylamine

N-nitrosodiphenylamine

N-nitrosodi-n-propylamine

bis (2-ethylhexyl) phthalate

butyl benzyl phthalate

di-n-butyl phthalate

dl-n-octyl phthalate

diethyl phthalate

dimethyl phthalate

benzo(a) anthracene

benzo(a)pyrene

3,4-benzofluoranthene

benzo(k)f luoranthene

chrysene

acenaphthylene

anthracene

benzo(ghi)perylene

fluorene

phenanthrene

d ibenzo(a ,h )an th racene

indeno (1 ,2 ,3-cd) pyrePe^t0^^pvrene '--••€-

2,3,7,8-tetrachlorodibenzo-^ 07105944

^1ND

ND

ND

ND

N^.NilnND-

N[P

ND^

ND

ND10

ND*

ND-*

ND

ND

ND

NDN DN DNDNONDND

NnNn

ND

ND

I^L/il/.v^C

SAMP

LAB

DATE

STD •

CONC

Volat

2V

3V

4V

6V

7V

10V

11V

13V

14V

15V

l6V

)W^xx)&xxxxM^»)«©t»)^xx^eti(8&xxxxxxxxxn19V

23V

29V

30V

32V

33V

38V

44V

45V

46V

47V

48V

49V

50V

51V

85V

86V

87V

88V

^ W6ST COAST TECHNICAL

LE ID F0565

ID 21881V4

INJECTED 8/5/81

ID BFB35 VOA15617 A ^TOD

lies

acrolein

acrylonitrile

benzene

carbon tetrachloride

chlorobenzene

1,2-dichloroethane

1.1,1-trichloroethane

1,1-dichloroethane

1,1,2-trichloroethane

1.1,2,2-tetrachloroethane

chloroethane

2-chloroethylvinyl ether

chloroform

1,1-dichloroethylene

1,2-trans-dichloroethylene

1,2-dichloropropane

1,3-dichloropropylene

ethylbenzene

methylene chloride

methyl chloride

methyl bromide

bromoform

dichlorobromomethane

trichlorofluoromethane

dichlorodifluoromethane

chlorodibromo methane

tetrachloroethvlene

toluene

trichloroethylene

vinyl chloride

.S6RVK

ug/1

ND

NO

ND

N D .

ND

ND

ND

ND

ND

N D

ND

ND

ND

ND

ND

ND

N D

ND

20

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

:e INC.

SAMP

LAB

DATE

DATE

STD •

CONC

Pesti

89P

90P

91P92P

93P

94P

95P

96P

97P98P

99P

100P

101P

102P

103P

104P

105P

106P

107P

108P

109P

HOP

HIP

112P

113P

* = I

(p<=

ND =* * ^

INDUSTRIAL LATGGORY

LE ID F0565

ID TRACE Ml 52

EXTRACTED 7/31/81

INJECTED 8/7/81

ID TRACE Ml 51

. FACTOR 50

cides

aldrin

dieldrin

chlordane

4,4'-DDT

4.4 '-DDE

4.4'-DDD

alpha-endosulfan

beta-endosulfan

endosulfan sulfate

endrin

endrin aldehyde

heptachlor

heptachlor epoxide

alpha-BHC

beta-BHC

gamma-BHC

delta-BHC

PCB-1242

PCB-1254

PCB-1221

PCB-1232

PCB-1248

PCB-1260

PCB-1016

toxaphene

-ess than 10 ug/I

•sticides less than 5 ug/1)

Not detected

Not confirmed by GCMSO^H^

ug/1

ND

. ND

ND

ND

'yt)———a-'i-ifiW

W

^

'ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

N D

ND

ND

ND

NO

ND

ND

£'554

0710594517605 Fabnca Way, Suite D Cerntos. California 90701 213/921-9831

WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3

QC Report No: 36Sample Number

F0565

A. SURROGATE SPIKE RESULTS

COMPOUND

Benzene - d6

l-Chloro-2-Bromopropane

Toluene - d8

2-Fluorophenol

Phenol - d5Nitrobenzene - d52-FluorobiphenylNaphthalene-DS

Fraction

VOA

VOA

VOA

ACID

ACID

B/N

B/N

B/N

Cone . (uq /1 )

49

44

461

1586665

(Surrogates only)Spike

Added (ug/1)

RD

50

50100103101101101

%Recovery

wfiR

92

11 ^

57 ln

————HT-6564 0

B. TENTATIVELY IDENTIFIED COMPOUNDS

1.2.

3.4.

5.

6.

7.8.9.10.11.12.

13.

14.

15.16.

17.18.

19.

20.

CAS # COMPOUND NAME

ACETONE

FRACTION

VOA #65

% Maximum Score Attained

Mass Matching Routine: FIT(specify)

868

-

u'zJL^ri^5-

07105946

"''"" "^hrir-n w.iv. S i n t n 0 Cprritos. C n l i f o r n i n POTOI ?1'!/03 1-0331

ORGANICS TRAFFIC REPORT(J) Case Number:

^0

Sample Site Name/Code:j/ff^-f-ffL "7^ f

©

-X-

2) Sample Type: (Check One)

Run Off

Wen

Receiving Water

Leachate

Effluent

Other (specify)

@ Shy To:

l/\/es^ Co^5' T^^"*l^(s>05 ^/'^ ^v

Ce^h^ C^h^yo7o/

Attn:

/~i^ df< B^^^d

(^Regional Office:Sampling Peracrmel:

^^ A^fiy>/^

Q[) Mark Volume Level on Sample Botfle

(Name)

L-v 37/-/^/ Extractable

(Phone)

Sampling Date:

.. -•/- </- f/____So^f

Exiractable

(Begin) (End)Extractable

(D Shipping Information

VOA Unpreserved/ Name of Shipper:

?-7J -57

VOA Unpreserved(Duplicate)

Date Shipped:

Airbill Number:

(7) Description of Sample Location:

® Special Hanaling Instructions:(eg., safety precautions, hazardous nature)

REGIONAL OFFICE FILE COPY

WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

SAMP

LAB •

DATE

DATE

STD 1

CONC

Acid

21A

22A

24A

31A

34A

57A

58A

59A60A

64A

65A

Base/

1B

5B

8B

9B

12B

18B

20B

25 B

26B

27B

28B

35B

36B

37B

39B

40B

LE ID F0566

ID 21881A6

EXTRACTED 8/1/81

INJECTED 8/9/81

[D SENS176 PHEN353

FACTOR 1000

Compounds u'

2,4,6-trichlorophenol

p-chloro-m-cresol

2-chlorophenol

2,4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol

2,4-dinitrophenol

4.6-dinitro-o-cresol

pentachlorophenol

phenol

^Neutral Compounds

acenaphthene

benzidine

1,2,4-trichlorobenzene

hexachlorobenzene

hexachloroethane

bis(2-chloroethyl)ether

2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1,4-dichlorobenzene

3,3'-dichlorobenzidine

2,4-dinitrotoluene

2,6-dinitrotoluene

1,2-diphenylhydrazine

(as azobenzene)

fluoranthene

4-chlorophenyl phenyl ether

g/1

ND

NDNDNDNDNDND

ND

ND

NDND

ND

ND

ND

ND

ND

NDND

ND

NDNP

ND

ND

ND

NOND

ND

SAMP

LAB

DATE

DATE

STD

CONC

Base/Neutral Compounds u

41B

42B

43B

52B

53B

54B

55B

56B61B

62B

63B

66B

67B

68B

69B

70B

71B

72B

73 B

74B

75B

76B

77B

78B

79B

SOB

81B

82B

83 B

84B

129B

p-dicu /JlUJayo

LE ID F0566

ID 21881B7

EXTRACTED 7/31/81

INJECTED 8/13/81

ID BENZ397 BNSTD414

FACTOR 1000

4-bromophenyl phenyl ether

bis(2-chloroisopropyl) ether

bis (2-chloroethoxy) methane

hexachlorobutadiene

hexachlorocyclopentadiene

isophorone

naphthalene

nitrobenzene

N-nitrosodimethylamine

N-nitrosodiphenylamine

N-nitrosodi-n-propylamine

bis (2-ethylhexyl) phthalate

butyl benzyl phthalate

di-n-butyl phthalate

di-n-octyl phthalate

diethyl phthalate

dimethyl phthalate

benzo(a) anthracene

benzo(a)pyrene

3,4-benzofluoranthene

benzo(k)f luoranthene

chrysene

acenaphthylene

anthracene

benzo(ghi)perylene

fluorene

phenanthrene

dibenzo(a ,h)an thracene

indeno( 1,2,3-cd)pyrene

pyrene OW^J^l

2,3,7,8-tetrachlorodibenzo-

g/1

ND

ND

ND

N00

NtP—tf^-

ND-

ND

NIP

ND

ND

ND

12

ND*

ND*

ND

ND

ND

ND

ND

NDNDNDN1)NDN DNnNn

L'.L^

rNQ

t^^

SAMP

LAB :

DATE

STD 1

CONC

Volat

2V

3V

4V

6V

7V

10V

11V

13V

14V

15V

l6V

)m%XX»XXXXKX«^)ti©t»)^DOX)^OtX^XXX

19V

23V

29V

30V

32V

33V

38V

44V

45V

46V

47V

48V

49V

50V

51V

85V

86V

87V

88V

^ WEST COAST TECHNICAL

LE ID R0566

ID 21881V9

INJECTED 8/5/81

[D BFB35 VOA156

. FACTOR ----—

lies

acrolein

acrylonitrile

benzene

carbon tetrachloride

chlorobenzene

1,2-dichloroethane

1,1,1-trichloroethane

1,1-dichloroethane

1,1,2-trichloroethane

1,1,2,2-tetrachloroethane

chloroethane

2-chloroethylvinyl ether

chloroform

1,1-dichloroethylene

1,2-trans-dichloroethylene

1,2-dichloropropane

1,3-dichloropropylene

ethylbenzene

methylene chloride

methyl chloride

methyl bromide

bromoform

dichlorobromo methane

trichlorofluoromethane

dichlorodifluoromethane

chlorodibromomethane

tetrachloroethylene

toluene

trichloroethylene

vinyl chloride

.S6RVK

ug/1

NO

ND

NO

ND

N D

ND

ND

N D

ND

N D

ND

ND

ND

ND

ND

ND

ND

ND18

ND

ND

ND

ND

ND

ND

ND

N D

NO

ND

ND

:6 INC.

SAMP

LAB

DATE

DATE

STD

CONC

Pesti

89P

90P

91P

92P

93P

94P

95P

96P

97P

98P

99P

100P

101P

102P

103P

104P

105P

106P

107P

108P

109P

HOP

HIP

112P

113P

* = I

( p <

ND =** ^

INDUSTRIAL CATEGORY

LE ID F0566

ID TRACE #4145

EXTRACTED 7/31/81

INJECTED 8/6/81

ID TRACE #4143

. FACTOR 100

cides

aldrin

dieldrin

chlordane

4,4 '-DDT

4,4 '-DDE

4,4 ' -DDD

alpha-endosulfan

beta-endosulfan

endosulfan sulfate

endrin

endrin aldehyde

heptachlor

heptachlor epoxide

alpha-BHC

beta-BHC

gamma-BHC

delta-BHC

PCB-1242

PCB-1254

PCB-1221

PCB-1232

PCB-1248

PCB-1260

PCB-1016

toxaphene

-ess than 10 ug/1

'sticides less than 5 ug/1)

Not detected

Not confirmed by GCMS

w

ug/1

NO

. ND

ND

WNth

^

NiL

^ND

ND

N D

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

WS5

0710594917605 Fabnca Way. Suite D Cerntos. California 90701 213/921-9831

WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3

QC Report No:_ 36Sample Number

F0566

A. SURROGATE SPIKE RESULTS

COMPOUND

Benzene - d6

l-Chloro-2-Bromopropane

Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyi

Naph-thalene-DS

Fraction

VGA

VOA

VOA

ACID

ACID

B/N

B/N

B/N

C o n c . ( u g / 1 )

48&0.

48

0

0

49

59

57

(Surrogates on ly)Spike

Added ( u q / 1 )

w

w

50

100

103

101

101

101

%Recovery

qfi

as

96

0

0

48

58

56

B. TENTATIVELY IDENTIFIED COMPOUNDS

1.

2.

3.

4.

5.

6.

7.

8.

9.

10.

1 1 .

12 .

13.

14.

15.

16.

17.

18.

19.

20.

CAS # COMPOUND NAME

ACETONE

FRACTION

VOA #86

% Maximum Score Attained

Mass Matching Routine: FIT(specify)

868

•

O^l^rnc.flV/ rf AV» » » 9JAJ\J^

. [W. ^

ORGANICS TRAFFIC REPORT(7) Case Number:

c^

Sample Site Name/Code:

(/^"T^c J^

©

) Sample Type: (Check One)

— RunOff

WeD

Rsoeiving Water

Leachate

Effluent

Ofher (specify)

© Shy To:

^/fsf Co^r 'Tec^^ic^''

1^05 pt^^ ^yCen^o^ Ctl^

fc?^o/Attn:

©Regional Office:

Sampling Personnel:

^/wJ Ak^^fr

(j) Mark Volume Level on Sample Botfle

•(Name)

C / - 371- HDI(Phone)

Extractable

Sampling Date:

?- Uf^ ^f

Ebctractable

rJ>ai^f

(Begin) (End) Extractable

(D Shipping Information

"hy.., \ ) ' J < - f , ^

Extractable

VOA Unpreserved

/ Name of Shipper:VOA Unpreserved(Duplicate)

Date Shipped:

:A^i? 3 5'3'^'3Airbill Number

(7) Description of Sample Location:

Q[) Special Handling Instructions:(e.g., safety precautions, hazardous nature)

REGIONAL OfTICE FILE'COPY

O IOSSSI(yyiogseo ..

WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

SAMP

LAB

DAT!

DATE

STD

CONC

Acid

21A

22A

24A

31A

34A

57A

58A

59A60A

64A

65A

Base

1B

5B

8B

9B

12B

18B

20B

25B

26B

27B

28B

35B

36B

37B

39B

40B

'LE ID F0567

ID 21881

; EXTRACTED 8/1/8

; INJECTED 8/9/8

ID SENS176

; FACTOR 1000

Compounds

2,4,6-trichlorophenol

p-chloro-m-cresol

2-chlorophenol

2,4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol

2,4-dinitrophenol

U,6-dinitro-o-cresol

pentachlorophenol

phenol

/Neutral Compounds

acenaphthene

benzidine

1,2,4-trichlorobenzene

hexachlorobenzene

hexachloroethane

bis(2-chloroethyl)ether

2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1, -dichlorobenzene

3,3'-dichlorobenzidine

2, A-dinitrotoluene

2,6-dinitrotoluene

1,2-diphenylhydrazine

(as azobenzene)

fluoranthene

4-chlorophenyl phenyl

A7

1

.1

PHEN353

ug/1

'TIS

NO

154

153

ND

ND

ND

NnNn

NnNn

ND

ND*

NDND

NDND

ND

ND

ND

ND

NnNH

NnND

e t h e r N D

•.- r\

SAMP I

LAB I

DATE

DATE

STD ID BENZ398 ;BNSTD415

CONC

Base/Neutral Compounds Uj

41B

42B

43B

52B

53B

54B

55B

56B

61B

62 B

63B

66B

67B

68B

69B

70B

71B

72B

73B

7^B

75B

76B

77B

78B

79B

80B

81B

82B

83B

84B

129B

p-dio:

^ .1 ( - .

-E ID F0567

D 21881B8

EXTRACTED 7/31/81

INJECTED 8/13/81

FACTOR 1000

4-bromophenyl phenyl ether

bis(2-chloroisopropyl) ether

bis (2-chloroethoxy) methane

hexachlorobutadiene

hexachlorocyclopentadiene

isophorone

naphthalene

nitrobenzene

N-nitrosodimethylamine

N-nitrosodiphenylamine

N-nitrosodi-n-propylamine

bis (2-ethylhexyl) phthalate

butyl benzyl phthalate

di-n-butyl phthalate

di-n-octyl phthalate

diethyl phthalate

dimethyl phthalate

benzo(a) anthracene

benzo(a)pyrene

3,4-benzofluoranthene

benzo(k) fluoranthene

chrysene

acenaphthylene

anthracene

benzo(ghi)perylene

fluorene

phenanthrene

dibenzo(a ,h)anthracene

indeno( l ,2 ,3-cd)pyrene

pyrene

2,3,7,8-tetrachlorodibenzo-

<in 07105952-. - r.r'-^- -'-n •0'7i QP^ i

g/1

ND

ND

ND

ND

N D ,——c-<t

NDsONDn

NCT"

ND0

—©-ND

ND

29

NDND

NO

ND

ND

ND

ND

ND

ND

ND

ND

NP

ND

NnNnND c

^

Nn SN D ^

ND'^1

fe^<5toa WEST COAST TECHNICAL

SAMPLE ID F0567

LAB ID 21881V10

DATE INJECTED 8/5/81

STD ID BFB35 VOA156

v^UIN^. rA^HJK

Volatiles

2V acrolein

3V acrylonitrile

4V benzene

6V carbon tetrachloride

7V chlorobenzene

10V 1,2-dichloroethane

11V 1,1,1-trichloroethane

13V 1,1-dichloroethane

14V 1,1,2-trichloroethane

15V 1,1,2,2-tetrachloroethane

l6V chloroethane

)imxxmxxm^»m^x%i(eti4^xxxxxxxxxx19V 2-chloroethylvinyl ether

23V chloroform

29V 1,1-dichloroethylene

30V 1,2-trans-dichloroethylene

32V 1,2-dichloropropane

33V 1,3-dichloropropylene

38V ethylbenzene

44V methylene chloride

45V methyl chloride

46V methyl bromide

47V bromoform

48V dichlorobromomethane

49V trichlorofluoromethane

50V dichlorodifluoromethane

51V chlorodibromomethane

85V tetrachloroethylene

86V toluene

87V trichloroethylene

88V vinyl chloride

SERVICE

LAB ID TRACE N146

DATE EXTRACTED 7/31/81

DATE INJECTED 8/6/81

ug/1

ND

NO

NO

ND

ND

ND

ND

ND

ND

N D

ND

ND

ND

ND

ND

ND

ND

ND

20ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

INC INDUSTRIAL FATPGQRY

SAMPLE ID F0567

STD ID TRACE N143

CONC. FACTOR 100

Pesticides

89P aldrin

90P dieldrin

91P chlordane

92P 4.4'-DDT

93P 4.4'-DDE

94P 4.4'-DDD

95P alpha-endosulfan

96P beta-endosulfan

97P endosulfan sulfate

98P endrin

99P endrin aldehyde

100P heptachlor

101P heptachlor epoxide

102P alpha-BHC

103P beta-BHC

104P gamma-BHC

105P delta-BHC

106P PCB-1242

107P PCB-1254

108P PCB-1221

109P PCB-1232

HOP PCB-1248

HIP PCB-1260

112P PCB-1016

113P toxaphene

* = Less than 10 ug/1

(pesticides less than 5 ug/1)

ND = Not detected

** = Not confirmed by GCMS

-^

ug/1

ND

. ND

ND

ND

NOt

Nfi»

^

WMS)ND

ND

ND

ND

ND

ND

ND

ND

ND

N D

ND

ND

ND

ND

ND

N D

^

17605 Fabrica Way, Suite D Cerritos. California 90701 213/921-9831 07105953

W65T COAST T€CHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3

QC Report No: 36Sample Number

F0567

A. SURROGATE SPIKE RESULTS

COMPOUND

Benzene - d6

l-Chloro-2-Bromopropane

Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyi

Naphthalene-DS

Fraction

VOA

VOA

VOA

ACID

ACID

B/N

B/N

B/N

Conc.(uq/1)

44

43

46

40

2

60

68

60

(Surroqates only)Spike

Added (uq/1)

50

50

50

100

103

101

101

101

%Recovery

88

86

92

40

2 ^

59 ,n

67 in59 ^~

B . TENTATIVELY IDENTIFIED COMPOUNDS 0

1.

2.

3.

4.

5.

6.

7.

8.

9.

10.

11 .

12.

13.

14.

15.

16.

17.

18.

19.

20.

CAS # COMPOUND NAME

ACETONE

TETRAHYDROFURAN

DICHLOROPHENOL

CHLOROPHENOL

2,4,5-TRICHLOROPHENOL

DICHLOROPHENOL

UNKNOWN

UNKNOWN

2-ETHYL-1-HEXANOL

TRICHLOROMETHOXYBENZEN

UNKNOWN

UNKNOWN

FRACTION

VOA #86

VOA #130

ACID #146

ACID # 1 9 6

ACID #207

ACID #264

ACID #492

ACID #515

B/N #142

: B/N #296

B/N #324

B/N #330

% Maximum Score Attained

Mass Matching Routine: FIT(specify)

835

993

GENERAL FIT

GENERAL FIT

966

GENERAL FIT

NO GOOD FIT

NOlCOOD FIT

942

GENERAL FIT

NO'SOOD FIT

NO GOOD FIT

OyiO ifia-^^

———————————————r^i-l nr.Qg^-rnr, r.,],r'^-i W-iy ^ in ton forritrT; (''-llif"rnin Qn7D1 71'l n "'I-n'T'I

ORGANICS TRAFFIC REPORT

Sample Site Name/Code:{/y^jn.c. ^ (-

Oc: <. ts^^f ( ( f , f7^

®2) Sample Type: (Check One)

RunQff

WeU

Rsceiving WatBr

Leachate

Effluent--

Other (specify)

© Ship To: ,

W<?^ Co^sf Tec^h'.^/ s>

/^(pOS P^b^c^ ^yCcr^^^J CA//^

9070/Attn:

A i c- i 0^i C- 1 fcM ^ €^

Q Regional Office:Sampling Personnel:

(j) Mark Volume Level on Sample Bottle

/.. /MD^.ft^)/TiT_____ \ \ /(Name)

. / - /-no/ Extractable

(Phone)

Sampling Date:

;^.^-S/ ^f(Begin) (End)

Extractable

(6) Shipping Information Extractable

T 1,^;,. MM^) VOAUnp^en^d/ Name of Shipper:

VOA Unpreserved(Duplicate)

Date Shipped:

Airbill Number:

DaleSampled

(7) Description of Sample Location:

(^) Special Handling Instructions:(e.g., safety precautions, hazardous nature)

REGIONAL OFnCE FILE COPY

W€ST COAST TECHNICAL S6RVIC6 INC. INDUSTRIAL CATEGORY

SAMP

LAB

DATE

DATE

STD •

CONC

Acid

21A

22A

24A

31A

34A

57A

58A

59A

60A

64A

65A

Base/

1B

5B

8B

9B

12B

18B

20B

25B

26B

27B

28B

35B

36B

37B

39B

40B

LE ID F0568

ID 21881A8

EXTRACTED 8/1/81

INJECTED 8/9/81

ID SESN176 PHEN353

FACTOR 1000

Compounds u,

2,4,6-trichlorophenol

p-chloro-m-cresol

2-chlorophenol

2,4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol

2,4-dinitrophenol

4,6-dinitro-o-cresol

pentachlorophenol

phenol

^Neutral Compounds

acenaphthene

benzidine

1,2,4-trichlorobenzene

hexachlorobenzene

hexachloroethane

bis(2-chloroethyl)ether

2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1,4-dichlorobenzene

3,3'-dichlorobenzidine

2,4-dinitrotoluene

2,6-dinitrotoluene

1,2-diphenylhydrazine

(as azobenzene)

fluoranthene

4-chlorophenyl phenyl ether

g/1*

NDND26

NDNOND

NnND

NnNn

ND

ND

NDND

ND

NDNDND

NDNDND

NnND

NnNDND

SAMP

LAB

DATE

DATE

STD :

CONC

Base/Neutral Compounds ui

41B

42B

43B

52B

53B

54B

55B

56 B

61B

62B

63B

66B

67B

68B

69B

70B

71B

72B

73B

74B

75B

76B

77B

78B

79B

SOB

81B

82B

83B

84B

129B

p-dio

LE ID F0568

ID 21881B9

EXTRACTED 7/31/81

INJECTED 8/13/81

ID BENZ398 BNSTD415

FACTOR 1DDO

4-bromophenyl phenyl ether

bis(2-chloroisopropyl) ether

bis (2-chloroethoxy) methane

hexachlorobutadiene

hexachlorocyclopentadiene

isophorone

naphthalene

nitrobenzene

N-nitrosodimethylamine

N-nitrosodiphenylamine

N-nitrosodi-n-propylamine

bis (2-ethylhexyl) phthalate

butyl benzyl phthalate

di-n-butyl phthalate

di-n-octyl phthalate

diethyl phthalate

dimethyl phthalate

benzo(a) anthracene

benzo(a)pyrene

3,4-benzofluoranthene

benzo(k)fluoranthene

chrysene

acenaphthylene

anthracene

benzo(ghi)perylene

fluorene

phenanthrene

dibenzo(a ,h)anthracene

indeno( 1,2,3-cd)pyrene

pyrene

2,3,7,8-tetrachlorodibenzo-,0^105956

•xin

1ND

ND

ND

N D -—''s-NDnNB^

NIT

^

ND

ND

ND

18

ND*

N&

ND

ND

ND

ND

ND

ND

NDND

N D

ND

ND

Nn ^Nn VN n 1:N D ,?

s

,'./

ND

SAMP

LAB

DATE

STD

CONC

Volat

2V

3V

4V

6V

7V

10V

11V

13V

14V

15V

l6V

)™xx»xxxax^»)tm^xMW4Xixxxxxxxxx?o(19V23V

29V

30V

32V

33V

38V

44V

45V

46V

47V

48V

49V

50V51V

85V

86V

87V

9 W€ST COAST TECHNICAL

LE ID F0568

ID 21881V15

INJECTED 8/6/81

ID BFB36 VOA157T- A c"mD

lies

acrolein

acrylonitrile

benzene

carbon tetrachloride

chlorobenzene

1,2-dichloroethane

1,1,1-trichloroethane

1,1-dichloroethane

1,1,2-trichloroethane

1,1,2,2-tetrachloroethane

chloroethane

2-chloroethylvinyl ether

chloroform

1,1-dichloroethylene

1,2-trans-dichloroethylene

1,2-dichloropropane

1,3-dichloropropylene

ethylbenzene

methylene chloride

methyl chloride

methyl bromide

bromoform

dichlorobromo methane

trichlorofluoromethane

dichlorodifluoromethane

chlorodibromomethane

tetrachloroethylene

toluene

trichloroethylene

.SGRVK

ug/1

ND

ND

N D

ND

ND

ND

ND

N D

ND

N D

ND

ND

ND

ND

ND

ND

ND

ND13

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

:e INC.SAMP

LAB

DATE

DATE

STD

CONC

Pesti

89P

90P

91P

92P

93P

94P

95P

96P

97P

98P

99P

100P

101P

102P

103P

104P

105P

106P

107P

108P

109P

HOP

HIP

112P

113P

* = 1

(pe

ND =* * ^

INDUSTRIAL CATEGORY

LE ID F0568

ID TRACE N154

EXTRACTED 7/31/81

INJECTED 8/7/81

ID TRACE M151

. FACTOR 100

cides

aldrin

dieldrin

chlordane

4,4 '-DDT

4,4 ' -DDE

4,4 ' -DDD

alpha-endosulfan

beta-endosulfan

endosulfan sulfate

endrin

endrin aldehyde

heptachlor

heptachlor epoxide

alpha-BHC

beta-BHC

gamma-BHC

delta-BHC

PCB-1242

PCB-1254

PCB-1221

PCB-1232

PCB-1248

PCB-1260

PCB-1016

toxaphene

.-ess than 10 ug/1

•sticides less than 5 ug/l)0

Not detected iv~,-Vf\r,r"^M^b&e^

Not confirmed by GCMS .-' -

ug/1

ND

ND

ND

rNO\^)

%

W

<SD

ND

N D

N D

ND

ND

ND

N D

ND

ND

ND

ND

ND

ND

ND

N D

ND

ND

7105957

88V vinyl chloride

WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3

QC Report No: 36Sample Number

F0568

A. SURROGATE SPIKE RESULTS

COMPOUND

Benzene - d6

l-Chloro-2-Bromopropane

Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyl

Naphthalene-DS

Fraction

VOA

VOA

VOA

ACID

ACID

B/N

B/N

B/N

Cone.(ug/1)

56

49

55

48

61

69

72

67

(Surrogates only)Spike

Added (uq/1)

50

50

50

100

103

101

101

101

%Recovery

1 1 2

98

1 1 0

48

59

68

71

66

B. TENTATIVELY IDENTIFIED COMPOUNDS

1.

2.

3.

4.

5.

6.

7.

8.

9.

10.

1 1 .

12.

13.

14.

15.

16.

17.

18.

19.

20.

CAS # COMPOUND NAME

ACETONE

TETRAHYDROFURAN

FRACTION

VOA #88

VOA #134

% Maximum Score Attained

Mass Matching Routine: FIT(specify)

909

958

•

O'W^i

O'-^inc.oi————————————————————————— IAUDJ,

-rn'-, r ,:.,,,.-, lAi-i.,. i^.i,,^ n Cprri»r'<; Cfllifnrni'n 00701 "1 ^ 'n^i .nni i

ROTECTION AGENCY HWI Sample i&magement Office Sample Number

ORGANICS TRAFFIC REPORTQ Case Number:

S

Sample Site Name/Code:./r^hf , f^(

@ Sample Type: (Check One)

—— RunOff

X Wefl

——— Receiving Water

Leachate

Effluent

OSier (specify)

(J) Shy To: ^\^^ ca^sf TPC^/^/^./ >6 05 pf»b^i c^ ^yerr/-/^ Q/^

9P7^/

(^) Description of Sample Location

(^) Special Handling Instructions:(e.g., safety precautions, hazardous nature)

REGIONAL OFFICE FILE COPY

W€ST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

SAMP

LAB

DATE

DATE

STD •

CONC

Acid

21A

22A

24A

31A

34A

57A

58A

59A

60A

64A

65A

Base/

1B

5B

8B

9B12B

18B

20B

25B

26B

27B

28B

35B

36 B

37B

39B

40 B

LE ID F0569

ID 21881A9

EXTRACTED 8/1/81

INJECTED 8/9/81

[D SENS176 PHEN353

FACTOR 1000

Compounds

2,4,6-trichlorophenol

p-chloro-m-cresol

2-chlorophenol

2,4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol

2,4-dinitrophenol

4,6-dinitro-o-cresol

pentachlorophenol

phenol

^Neutral Compounds

acenaphthene

benzidine

1,2,4-trichlorobenzene

hexachlorobenzene

hexachloroethane

bis(2-chloroethyl)ether

2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1,4-dichlorobenzene

3,3'-dichlorobenzidine

2,4-dinitrotoluene

2,6-dinitrotoluene

1,2-diphenylhydrazine

(as azobenzene)

f luoranthene

4-chlorophenyl phenyl

ug/1*

NDND

21

ND

NDND

NnNDNn*

ND

ND

?q

ND

ND

ND

ND30

50

493

ND

ND

ND

NnNO

e t h e r N D

SAMP

LAB

DATE

DATE

STD :

CONC

Base/

41B

42B

43B

52B

53B54B55B56B61B62B

63B

66B

67B

68B

69B

70B

71B

72B

73B

74B

75B

76B

77B

78B

79B

SOB

81B

82B

83B

84B

129B

p-dic

LE ID F0569

ID 21881B10 & 21881

EXTRACTED 7/31/81

INJECTED 8/13/81 8/21/81

ID BENZ398. BNSTD415/BENZ401 BNSTD418

FACTOR 1000 & 100

•''Neutral Compounds u j

4-bromophenyl phenyl ether

bis(2-chloroisopropyl) ether

bis (2-chloroethoxy) methane

hexachlorobutadiene

hexachlorocyclopentadiene

isophorone

naphthalene

nitrobenzene

N-nitrosodimethylamine

N-nitrosodiphenylamine

N-nitrosodi-n-propylamine

bis (2-ethylhexyl) phthalate

butyl benzyl phthalate

di-n-butyl phthalate

di-n-octyl phthalate

. diethyl phthalate

dimethyl phthalate

benzo(a) anthracene

benzo(a)pyrene

3,4-benzofluoranthene

benzo(k)f luoranthene

chrysene

acenaphthylene

anthracene

benzo(ghi)perylene

fluorene

phenanthrene

d ibenzo(a ,h )an th racene

indeno( l ,2 ,3-cd)pyrene

pyrene

2,3,7,8-tetrachlorodibenzof^/x

xin 0710.S<^0

B13

^LND

ND

ND

NB)

?5-^

NA-^—Ng?ND<*

ND*

ND*

ND*

NDND

ND

ND

ND

N D

ND

ND

ND

Nn

NnNnwnN D

^^ShND 1- '

WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

SAMP

LAB

DATE

STD

CONC

Volat

2V

3V

4V

6V

7V

10V

11V

13V

14V

15V

16V

)™xxmxax^»%mwxMi)ti4mxxxxxxxxx19V23V29V

30V

32V

33V

38V

44V

45V

46V

47V

48V

49V

50V

51V85V

86V87V

88V

LE ID F0569

ID 21881V12 & 21881V16

INJECTED 8/5/81 & 8/6/81

ID BFB35 VOA156 & BFB36 VOA157

. FACTOR ——- & 1/10 D i l u t i o n

lies u

acrolein

acrylonitrile

benzene

carbon tetrachloride

chlorobenzene

1,2-dichloroethane

1,1,1-trichloroethane

1,1-dichloroethane

1,1,2-trichloroethane

1,1,2,2-tetrachloroethane

chloroethane

2-chloroethylvinyl ether

chloroform

1,1-dichloroethylene

1,2-trans-dichloroethylene

1,2-dichloropropane

1,3-dichloropropylene

ethylbenzene

methylene chloride

methyl chloride

methyl bromide

bromoform

dichlorobromo methane

trichlorofluoro methane

dichlorodifluoromethane

chlorodibromomethane

tetrachloroethylene

toluene

trichloroethylene

vinyl chloride

LAB ID TRACE N155

DATE EXTRACTED 7/31/81

g/1

ND

ND*

ND

392

ND

ND

N D

ND

N D

ND

ND

ND

ND

ND

ND

N D

ND

20

ND

ND

ND

ND

ND

ND

ND

ND

16

NP

ND

SAMPLE ID F0569

DATE INJECTED 8/7/81

STD ID TRACE #4156

CONC. FACTOR 100

Pesticides

89P aldrin

90P dieldrin

91P chlordane

92P 4,4 ' -DDT

93P 4,4 ' -DDE

94P 4.4'-DDD

95P ' alpha-endosulfan

96P beta-endosulfan

97P endosulfan sulfate

98P endrin

99P endrin aldehyde

100P heptachlor

101P heptachlor epoxide

102P alpha-BHC

103P beta-BHC

104P gamma-BHC

105P delta-BHC

106P PCB-1242

107P PCB-1254

108P PCB-1221

109P PCB-1232

HOP PCB-1248

HIP PCB-1260

112P PCB-1016

113P toxaphene

* = Less than 10 ug/1

(pesticides less than 5 ug/1)

ND = Not detected

-;;* ^ ^Q^ confirmed by GCMS n

ug/1

ND

NO

ND

•W

•NO-en

ND

ffl

•TO

NO

NO

NO

NO

ND

0.1**

n.3**ND

0.2**

ND

N D

NOND

ND

ND

ND

NO

7105961

WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS. DATA SHEET - Page 3

QC Report No: 36Sample Number

F0569

A. SURROGATE SPIKE RESULTS

COMPOUND

Benzene - d6

l-Chloro-2-Bromopropan6

Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyi

Naphthalene-DS

Fraction

VOA

VOA

VOA

ACID

ACID

B/N

B/N

B/N

Cone.(ug/1)

48

45

47

0

2

72

81

74

(Surrogates only)Spike

Added (ug /1 )

50

50

50

100

103

1 0 1

101

101

%Recovery

96

90

94

0

2 C\J

71 ^—————HT

80

73 0

B . TENTATIVELY IDENTIFIED COMPOUNDS

1.

2.

3.

4.

5.

6.

7.

8.

9.

10.

1 1 .

12.

13.

14.

15.

16.

17 .

18.

19.

20.

CAS # COMPOUND NAME

TOLUENE

CHLOROBENZENE

TRICHLOROBENZENE

FRACTION

VN #43

B/N #68

B/N #209

% Maximum Score Attained

Mass Matching Routine: FIT(specify)

999

991

GENERAL FIT

•

{V^W^ /AC(--

- n'71 fu.nr.0

ORGANICS TRAFFIC REPORT(T) Case Number:

^%0

Sample Site Name/Code:[Ar^ X.f

©) Sample Type: (Check One)

Run Off

WeU

Receiving Water

Leachate

Effluent. -•

Other (specify)

@ Ship To:

W^s^ Co^st' fe^h'i^^^j^^oS ^A^ ^yCe^f^s, C«/'^ /

^D^ot

Attn:

(4) Regional Office:Sampling Personnel:

..^A^ /Uc^^^e

(y Mark Volume Level on Sample Bottle

(Name)

:/ 37/- /7C^/Extractable

(Phone)

Sampling Date:

•-; - ^/ J^^ ^

Extractable

(Begin) (End)Extractable

(6) Shipping Information Extractable

J VOA Unpreserved

Name of Shipper:

-~ "^ -. >-' /.' ^ (_/ - .; /

VOA Unpreserved(Duplicate)

Date Shipped:

-, , ..- -i r~ •"' '—> ~"J' * • - ' ' " / J '-.-.? "S

Airbill Number:

DateSampled

(7) Description of Sample Location:

\J[) Special Handling Instructions:(e.g., safety precautions, hazardous ncrture)

0710257

07105963REGIONAL OFFICE FILE COPY

WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

SAMP

LAB i

DATE

DATE

STD I

CONC

Acid

21A

22A

24A

31A

34A

57A58A59A60A

64A

65A

Base/

1B

5B

8B

9B

12B

l8B

20B

25B

26B

27B

28B

35B

36B

37B

39B

40B

i7pnt - p.,1^.^ , 11.',., Q.n .p [-;

LE ID F0570

ID 21881A10

EXTRACTED 8/1/81

INJECTED 8/10/81

:D SENS177 PHEN354

FACTOR 1000

Compounds w

2,4,6-trlchlorophenol

p-chloro-m-cresol

2-chlorophenol

2,4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol

2,4-dinitrophenol

4,6-dinitro-o-cresol

pentachlorophenol

phenol

'Neutral Compounds

acenaphthene

benzidine

1,2,4-trichlorobenzene

hexachlorobenzene

hexachloroethane

bis(2-chloroethyl)ether

2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1,4-dichlorobenzene3,3'-dichlorobenzidine

2,4-dinitrotoluene

2,6-dinitrotoluene

1,2-diphenylhydrazine

(as azobenzene)

f luoranthene

4-chlorophenyl phenyl ether

g/1

NP

NDNO*

NPNnNUWNnNnNn

ND

ND

N D

ND

ND

NDNONONn*

NnNnNn

NnN D

ND

SAMP I

LAB I

DATE

DATE

STD ID BENZ398 ENSTD415

CONC

Base/Neutral Compounds u.i

41B

42B

43B

52B

53B

54B

55B

• 56B

61B

62B

63B

66B

67B

68B69B70B

71B

72B

73B

74B

75B

76B

77B

78B

79B

80 B

81B

82B

83B

84B

129B

p-dio:

r ' ^ , - ,>nc r ' ^ i i ^ r p i a qn7C1 '?^'~',:^?\-W\^

.E ID F0570

D 21881B11

EXTRACTED 7/31/81

INJECTED 8/13/81

FACTOR 1000

4-bromophenyl phenyl ether

bis(2-chloroisopropyl) ether

bis (2-chloroethoxy) methane

hexachlorobutadiene

hexachlorocyclopentadiene

isophorone

naphthalene

nitrobenzene

N-nitrosodimethylamine

N-nitrosodiphenylamine

N-nitrosodi-n-propylamine

bis (2-ethylhexyl) phthalate

butyl benzyl phthalate

di-n-butyl phthalate

di-n-octyl phthalate

diethyl phthalate

dimethyl phthalate

benzo(a) anthracene

benzo(a)pyrene

3,4-benzofluoranthene

benzo (k ) fluoranthene

chrysene

acenaphthylene

anthracene

benzo(ghi)perylene

fluorene

phenanthrene

d ibenzo(a ,h )an th racene

indeno( 1,2,3-cd)pyrene

pyrene

2,3,7,8-tetrachlorodibenzo-O^;

xin

^1

ND

ND

ND

ND•q-

NC^

NQLnNCT-ND0

ND

ND

ND*

ND*

NO*

N D

ND

ND

ND

N D

N D

N D

N D

ND ^

^- ^

^- ^Nn ^N n °N D " •—

105964N D

VSSSS^ WEST COAST TECHNICAL

SAMPLE ID F0570

LAB ID 21881V17

DATE INJECTED 8/6/81

STD ID BFB36 VOA157

CONC. FACTOR -------

Volatiles

2V acrolein

3V acrylonitrile

4V benzene

6V carbon tetrachloride

7V chlorobenzene

10V 1,2-dichloroethane

11V 1,1,1-trichloroethane

13V 1,1-dichloroethane

14V 1,1,2-trichloroethane

15V 1,1,2.2-tetrachloroethane

l6V chloroethane

)^XX»XXXX)iX^)tmWXMl)tM)XXXXXXXXXXX

19V 2-chloroethylvinyl ether

23V chloroform

29V 1,1-dichloroethylene

30V 1,2-trans-dichloroethylene

32V 1,2-dichloropropane

33V 1,3-dichloropropylene

38V ethylbenzene

44V methylene chloride

45V methyl chloride

46V methyl bromide

47V bromoform

48V dichlorobromomethane

49V trichlorofluoromethane

50V dichlorodifluoromethane

51V chlorodibromomethane

85V tetrachloroethylene

86V toluene

87V trichloroethylene

88V vinyl chloride

SERVICE

DATE EXTRACTED 7/31/81

ug/1

ND

NO

ND

ND

ND

ND

ND

N D

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

13

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

INC. INDUSTRIAL CATEGORY

SAMPLE ID F0570

LAB ID TRACE Ml 57

DATE INJECTED 8/7/81

STD ID TRACE N156

CONC. FACTOR 100

Pesticides

89P aldrin

90P dieldrin

91P chlordane

92P 4.4'-DDT

93P 4.4 ' -DDE

94P 4 ,4 ' -DDD

95P alpha-endosulfan

96P beta-endosulfan

97P endosulfan sulfate

98P endrin

99P endrin aldehyde

100P heptachlor

101P heptachlor epoxide

102P alpha-BHC

103P beta-BHC

104P gamma-BHC

105P delta-BHC

106P PCB-1242

107P PCB-1254

108P PCB-1221

109P PCB-1232

HOP PCB-1248

HIP PCB-1260

112P PCB-1016

113P toxaphene

* = Less than 10 ug/1

(pesticides less than 5 ug/1)

ND = Not detected

** = Not confirmed by GCMS ^ * i^y

ug/1

ND

ND

ND

W3

INfi

WD

ip——©-MND

ND

ND

ND

ND

ND

ND

ND

ND

ND

N D

ND

ND

ND

N D

ND

NO

^

07105965

WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3

QC Report No:Sample Number

F0570

A. SURROGATE SPIKE RESULTS

COMPOUND

Benzene - d6

l-Chloro-2-Bromopropane

Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyl

Naphtha 1ene-D8

Fraction

VOA

VOA

VOA

ACID

ACID

B/N

B/N

B/N

Cone.(ug/1)

56

49

52

2

2

62

75

70

(Surrogates only)Spike

Added (ug/1)

50

50

50

100

103

101

101

101

%Recovery

1 1 2

98

104

2

2 ^

61 u74 .

69 <

B . TENTATIVELY IDENTIFIED COMPOUNOS

1.

2^

3.

4.

5.

6.

7.

8.

9.

10.

11.

12.

13.

14.

15.

16.

17.

18.

19.

20.

CAS % COMPOUND NAME

TETRAHYDROFURAN

UNKNOWN

FRACTION

VOA #131

VOA M21

% Maximum Score Attained

Mass Matching Routine: FIT(specify)

928

NO SOOD FIT

.

-

o^w^

————————————————r>"« ne.'i-n'-, r-^ri.r-1 W.iv SnitP 0 Orritos. Cali-fnrnia 00701 ?11' '92l-Qa31

i 5 St'P i'^d]

Potential Hazardous Waste Site•r<^n-s -^

Charles A. Gazda, ChiefCompliance Section (6SA-SC)

Bruce Elliot, ChiefGeneral Enforcement Branch (6EG)

c^P - 6 ../h—' *

Site NameLocationHazsit NoTDD No.

A. Fiel

T207T207ISSISS

B. §311

1.2.3.

VorktC-'.hr ^^ //<3A/?'/^f - ^ - W-7 -^•

d Report:

0-20-3 recon sampiingCompiiance ReportNon-Notifior Report

potential (completed by 6SA-E

§311 sample collectedAnalytical results attachedProposed §311 action:

attached ( )attached ( )attached ( )attached ( )

) yes ( ) no ( )

yes ( ) no ( )yes ( ) no ( )

r-r-m

00

C.

D.

Were drinking water wellssampled?

Analytical Data: P^/vf-K/

1. FIT data review

no ( )

y

yes ( )

-SQ^O^O by flOPC^I^.

attached (^j

E.

2. Contract lab results:

watersoi l , waste

3. Houston Lab results

Comments:

attached (Xfattached ( )

attached ( )

S£-—A4e-l-e MiLcl ie l I (bW-S :

Ecology and Environment, Inc.

Region VI

MEMORANDUM

TO: Charles Gazda,Chief Compliance Section

FROM: David Anderson, FIT ^.E&E Region VI

THRU: K. Matone, FITL ^Y^^E&E Region VI

' CO

DATE: September 1 5 , 1 9 8 1 '"-LPt

RE: TDD F-6-8109-20, Review of Sample Data from Vertac ^_

Attached is a review of and quantif ication of 8 wel l water samples collected bythe state at Vertac. Only one anomaly appeared in the results, that being thepresence of acetone in 6 of the 8 samples. Acetone has not been present inprevious samples and its presence is probably due to improper preparation ofsample containers or contamination by the analytical lab.

00

Sources

Standards:EPA water Quality Criteria DocumentsNovember 28, 1980

Toxicities:Registery of Toxic Effects1979 Edition

pc

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. . . ^-....- . - . - . - - . ^ur\kno^n

/7) 47

(( n \<^r\

C^\CI-L r ^ e ^ y f b^ns^-nt- /3 A'L-

^ n,';/.''1'^'''' ^1 / SL'-T"'"

^.^J-1-/>^^^/ ^l1^

r\.\ i, / /S^i^^hicrs ph^nc'l

H ^ S p ^ ' ' ' tr< '^'1'"'-

- • ^ i '13^ /

/ / ' I c ,",lc'^' ^et/ i f^ i / b'r'"-7''^^-/

un s^^' v ' ''" '^<''

^33-1

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RANGE

27-L^L^b

3^-^^^^

^ C- - / / Y ^

/? / - L/^^^

m- 5^^b

l; - 2,33^

^- l^f^b

^S- IL-.^^b

) i 7- ^3c^

(, . - I^CC^^

/7 - 3;';-^

).2S— ^^i^-b

^ -^cc^b

^ " ) - ^3.) j.p/;)

-

'//..-Cf::

———-

-——

———

——

——-

LP,\.C.^, r^

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,,

.————

————

——-—-

————.

C O ^ ^ F ' l f S

l^rift^

-ITS—

h/<lA A^-

f]/^^ n.^-

^,nt\ rr\.^.

t^csr^ eh/ore)

•s—

.0^

chic^- lfK//.3^l Z »'"«•- "3 •^•^~

0

0

^ I I<ck I'-'r-' ^h^^i

/^-^

•^7/-,c^^Y.<

CL/II'"'^"I

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0710S981

US Environmental Protection AgencyHazardous Waste Investigation

Sample Management OfficeP.O. Box 818

Alexandria, Virginia 22313(703)683-0885

SEP 21 1981

S & A DIVISION 1I

MEMORANDUM

DATE: September 14, 1981

SUBJECT: RETURN OF SAMPLE TRACKING DOCUMENTSCM0^in

FROM: Sample ^anagenent Office (-{^J^ ^-A^Uts^ 0\

• inTO: Charles Gazda, Project Officer, USEPA Region VI ,—

Enclosed please find the Regional copies of the sample tracking documents576, 577.

for case/s 580, 554, 556, 557, 575 , . Included are a photocopy of the Laboratory

Traff ic Report, the Regional Laboratory Chronicle, and the Regional Analysis

Chronicle. These documents along wi th your copy of the Sampling Tra f f i c Report

comprise the entire Sample Tracking Package. The IFB Laboratory w i l t forward

the Final Analysis' Data Forms directly to the Regional Project Officer or his

designated representative.

The IFB Laboratories will be audited on a quarterly basis (every three

months) for quality control procedures and technical verification by EMSL-LV

and NEIC. Any information from these audits which relates to the samples wi l l

be forwarded to the Region.

If you have any questions on these documents or procedures, please feel

free to call the Sample Management Off ice.

00

0*710^3? -

07105982

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

Laboratory Nome

Case NumberSEP 9^

Sample Description Technician SignatureDate/Ime Extraction Completed

Detedl Below Pertinent Infannafion and /orProblenis Asscaated wifti Esdractkxi

Extractable(Add)

^- ^/ /^ • ..o - '^u^-

i / '/--<-l't7$7"z -

Extractable(Pesticides)

•• / <•-<•-•.-. -' ae<;/ // / ,- y'A^fl^^ -- /'r,7^^

Extractable(Dioxins)

• ~o0

QCExtractable(Base/Neutral)

QC Extractable(Add)

QCExtradable(Pesticides)

QCExtroctable(Dioxins)

Additional Comments:

(measea-

07105983SMO COPY FOR RETURN TO REGION

I AGENCY HWI Sample Management Office

ORGANICS LABORATORY CHRONICLE (ANALYSIS)Sample Number

F 0536

Laboratory Name

Case Number

Sample Description Analyst SignatureDate /Time Analysis Completed

SEP ^wDetail Below Pertinent Information and /or

Problems Associated with Analysis

Extractable(Base/Neutral)

•:' I i^l - L

• r ' ^ [i s I• -.•'.A.^.A [ .

Extractable(Add)

,.-"7/ f^i A

Extractable(Pesticides)

A /••--

Extradable(Dioxins)

VOAUnpreserved 00

VOAUnpreserved(Duplicate)

QCExliactable(Base/Neutral)

QCExfanctable(Add)

QC Extractable(Pesticides)

QCExliadabb(Dioxins)

Additional Comments:

SMO COPY FOR RETURN TO REGION

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

Sample Description Tedmidan SignatureDate /Time Exhaction Completed.

I^tailBekwPerfnentlniamntm and/orProblenisAsaodatedwilhEsctiaction

Extractable(Base/Neutral)

/y^J^^- • / 1 ' ^^/f/^____^^r

Extractable(Add)

^^^a^ ^ J^i^i/ ^'f } ~"? A

^ --< ''? I L-C^T? -

^' / T^--'''!^^.^-

Extroctables)

^ ^ a5< -&<?°ia»y

9/^//^___________/^^^^ - ^

Extractable(Dioxins)

0''m

QC Extractable(Base/Neutral)

';/;,, . - »i'7- -

^.-r^-"

00

QCExhuctable(Add)

'(-'•••/'•. '-'- // ,.v^.-^-^^f^

/3/S~-../-

QC Extractable(Pestiddes)

QCExtreictable(Dioxins)

Additional Comments:

SMO COPY FOR RETUBN TO REGION

ORGANICS LABORATORY CHRONICLE (ANALYSIS)Sample Number

W 0564

Laboratory Name

Case Number. S8PSample Description Analyst Signature

Date /Tune Ancdyas CompletedDetcril BekawPertmenti^CTinalionand/cT

Problems Assodated with Ancdyas

Extrnctoble(Base/Neutral)

^//y^,-^ ' /"^r^J^ ^^

Extzactable(Add)

Ebcbactable5)

^ - . ' : / ^ •/-•

<^ L.iExtractable(Dioxins)

LPt

VOA Unpreserved00

VOA Unpreserved(Duplicate)

/ /';; i -<• -^' -/^-' /

-M.QCEidractable(Base/Neutral)

QC Extractable(Add)

QCExfaactable(Pesticides)

QC Extractable(Dioxins)

Additional Comments:

SMO COPY FOR RETURN TO REGION

<mo%B&5"

07105986

iple Management Umce

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

Laboratory Name

Case NumberSEP 9W

Sample Description . Technkaan SignatureDate /Time Extraction Completed

Deted Bekw Pertinent infexmalidn and/orRrdslemsAsscckitedwiftiEJctox'tion

Exttactable(Base/Neutral)

^^a^^ .^ ^^-^^(

^//^___________^S~/ WS. -6 //

^/^ „_______„ /S^T//^r,!:^-^C' ^ ^^-{^SX^

^/5l ^_______/^

Exbuctable(Add)

ExtractaUes)

Extractable(Dioxins)

QCExtructable(Base/Neutral)

00

QCExtrcidable(Add)

QCExtroctable(Pesticides)

1 '' /i'''^n :-<(. 6-

QCExtractable(Dioxins)

Additional Comments:

SMO COPY FOR RETURN TO REGION

;t° ST^ )N AGENCY HWI Sample Management Office

ORGANICS LABORATORY CHRONICLE (ANALYSIS)I Sample Number

IF 0565

Laboratory Name

Case Number. SEPSample Description Analyst Signature

Date/Tune Analysis CompletedDetail Below Pertinent Infonncrtion and/or

Problems Associated with Analysis

Extractable(Base/Neutral)

on^V I' { ! ' I^-—.^.i^-^J^,' \, A^

Extractable(Add)

Extractable(Pesticides)

...-/^W-

IJ. ' .A .00

-Oi-Extractable

(Dioxms)LTl

VOA Unpreserved'S5"0

VOA Unpreserved(Duplicate)

^/.-A ./

QCExtKidable(Base/Neutrcd)

QCExtixictable(Add)

QCExtradnble(Pesticides)

QC Extractable(Dioxins)

Additional Comments:

SMO COPY FOR RETURN TO REGION

OBGANICS LABORATORY CHRONICLE (EXTRACTIONS)

SEP

i:' -'' Sample Number

tP 056&

Saraple Description Technician SrcinatureDate /Time Extraction Completed

Deteril Bekw PertiniMitInionriationand/orPioblenas Associated wiftiExtractial

ExtaackdJe(Base/Neutrcd)

ExtracfcAle(Aad)

(•' ^^C^€3L^

/wEschcoctadw(Pesticides)

Z^^--^^ <^ ^sy^^y^^.

y-^y/f/______/^^ ^-^ - ^^Exbuctable(Dioxms)

QCExtradable(Base/Neutrcd)

00

QC Extendable(Add)

QCExtroctable(Pesticides)

QCExtrctdafale(Dioxins)

Additional Comments:

SMO COPY FOR RETURN TO REGION

I AGENCY HWI Sample Management OfficeSample Number

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

Laboratary Name

Case Number.

Scanple Description Analyst SignatureDate /Time Analysis Completed

SEP 91981Detail Below Pertinent Infomialion and/or

Problems Associated with Ancdyas

Extnictoble(Base/Neulral)

Extractable(Add)

•^w^l^ v' f ^Y' ( A

——^^

Extractable(Pesticides) '( y

'r.^ / ^ / ^h

{ ; ( ) ^. .--•v--;. . ^^A.0

Extractable(Dioxins)

VOAUnpreserved- .•f • i 0

0

VOAUnpreserved(Duplicate)

QCExtroctable(Base/Neutral)

QCExtiactable(Add)

QCExtiadable(Pesticides)

QC Extractable(Dioxins)

Additional Comments:

SMO COPY FOR RETURN TO REGION

OBGANICS IABORATOBY 'CHRONICLE (EXTRACTIONS)

Laboratory Nome

Case NumberSEP

Sample Description Technician SignatureDate/TBn&ExtracScn Completed

ttetafl BekwPerfeiHitInfaroiafion and/cyPrcMemsAsacdated« i Exiradion

Extxactable(Base/Neutral)

^ac^^^'^ -s^m^i/

gy^/^/ ____/^/yy , i l /^ y^^s^'

ExtrnctnUe(Add)

ExfaactaUe

-0"

\D

QC Ebctractable(Base/Neutml)

0

0

QCExtroctable(Add)

QCExtractable(Pesticides)

QCExIractable(Dioxins)

Aaditional Comments:

SMO COPY FOR RETURN TO REGION

)N AGENCY HWT Sample Management Office

ORGANICS LABORATORY CHRONICLE (ANALYSIS)'Sample Number

0567

Laboratory Name

Case Number. SEP 91981

Sample Description Analyst SignatureDate/Time Ancdyas Completed

Detail Below Pertinent Infannatton and / orProblems Associated with Ancdyas

Extmctable(Bose/Neutrcri)

r'^, 7, /-"'fcrl. v ( / .

Exfauctoble(Add)

u '..-^ {\ \ } f f^J^-^^ ^A-^f ,/ f\

^^UM

-'L,0 ( ^ExtractaUe(Dioxins) C^

-0"

v0VOA Unpreserved

VOA Unpreserved(Duplicate)

00

QC Extractable(Base/Neutrcd)

QCExIractable(Add)

QC Extractable(Pesdddes)

QC Extractable(Dioxins)

Additional Comments:

SMO COPY FOR RETURN TO REGION

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)S- Sample Number •

r 05681

Laboratory Nome

Case Number.

Sample D6sciiptjoii. Techrricym Sgncrtiire •Date/Time Exiiaction Completed

DeterilBelowPerfnentlhiontoafcti and/orPirchtemsAssocacttedwifliEsdracticn

y^^^

^ I /flExbackdJe(Base/Neutrai)

//4^^f-^ ^ c^a^^

8/^) /s/dr/^^i^c^ ^ •:y^^^^

-?/3//^________^

Extractable(Add)

Extractable(Koxins)

0' 0

QCExtractable(Base/Neutrai)

00

QCExfanctable(Add)

QCExtractable(Pesticides)

QCExtractable(Dioxins)

Additional Comments:

SMO COPY FOR RETURN TO REGION

"It WO't'

iGENCY HWI Sample Management Office

ORGANICS LABORATORY CHRONICLE (ANALYSIS)|fcSampteNumber

EF 0568

LAorcriory Name

Case Number. SEP ^w

Sample Description Analyst SignatureDate/Time Anatyas Completed

DetedBekwPertinentInfanna&XKand/orPrchlems Associated with Analysis

rsKv^V^v^'V'wQ

(Base/Neutrcd)

ExtractaUe(Add)

Extroctable(Pesticides)

ExtractaUe(Dioxins)

0

\0

VOA Unpreserved. . . " J t f / r i / ' " ,

-' y • /

r- ..;., !,, . Loo

VOA Unpreserved(Duplicate)

QCExtractable(Base/Neutecd)

QCExtractable(Add)

QCExtractable(Pesticides)

QCExtractable(Dioxins)

Additional Comments:

SMO COPY FOR RETURN TO REGION

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

Laboratory Nome

Case Number

Sample Description •• ^ „ ^^IfedB'ucKm Signature. Date/Time Exircicticn Completed

Deteni BelcwPeifee firfeiniaficftcind/OrPnAtemsAssocKrtedwtti ExteicticHi

ExIiackdJe(Base/Neutrai)

^-'^/ ^ffK^ftM ftt^

C^rcL^h-^ 'Extractahle(Add)

Exfanctahte(Pesticides)

//^€C^ ^ t^^

^/^hi_____/^/^^a^ ^^^^7

•9-/2f/yi________^£>0

Extractable(Dioxins)

0

vO

QC Extractable(Base/Neutrcri)

00

QC Extractable(Add)

QC Extractable(Pestiddes)

QC Extractable(Dioxins)

Additicaial Comments:

SMO COPY FOR RETURN TO REGION

rENCY HWI Sample Management Office

ORGANICS LABORATORY CHRONICLE (ANALYSIS)|? Sample Number

0569

Laboratory Name

Case Number. 8EP S1"1

Sample Description Analyst SignatureDate/Tune Analyas Completed

Detoril Bekw Pertinent Infonnaficn and /acPrciblemsAsscciated with Ancdysis

Extractable(Base/Neuhxd)

Extractable(Add)

ExtractaUeB)

Ebdractable(Dioxins)

VOA Unpreserved'A"' -

/-^'! » . /

:.-' .- .. < ^

00

VOA Unpreserved(Duplicate)

QCExfaudable(Base/Neutral)

QCExtrcictable(Add)

QCExtractable(Pestiddes)

QCExtractable(Dioxins)

Additional Comments:

SMO COPY FOR RETURN TO REGION '. ..- ^ -,' --£f»;,.._

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

Laboratory Name

Case Number

Sample Description,: .: Technician Signature -•Date/TuneExtrciction Conipleted

' .C? ^I • • » ,>W ..-•X • • y

DefcdIBelowPialinatihieeHg ^- PnAtemsAsasdated wilbExtracticn

Exhndable(Base/Neutrcd)

^^^i^^'

^/^/, , _ /3/S^a^--^'^- <5r <^<»^

7/3//^ /^^

Extractable(Add)

Extractable(Pesticides) ^^ - . ,

Extroctable(Dioxins)

0\0

QC Extmctabre.(Base/Neutral)

00

QC Extractable(Add)

QC Extractable(Pesdddes)

QC Extractable(Dioxins)

Additional Comments:

SMO COPY FOR RETURN TO REGION

ON AGENCY FIWI So^de Monaqement Office

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

Case Number, SEP 9

Sample Description r.:v.^y-^ - -Ancdyst Signature- ' . > A -•'.:. Date/rnneAnaIygs Completed

Extnx'tnhle ;(Base/Neutral) eu%"ExtractaUe(Add)

Exfmctables) CD

ExtractaUe(Dioxins)

VOA Unpreserved-/^

r^^JU ( {00

VOA Unpreserved(Duplicate)

QCExtractahle(Base/Neutrcd)

QCExtractable(Add)

QCExtroctable(Pestiddes)

QCExtractable(Dioxins)

Additional Comments:

SMO COPY FOR RETURN TO REGION

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

Laboratory Nome

Case Number

fv -----^1- - T* • I I •••• I! ^Loampie uescnption ' Technician SignatureDcrte/TinKEbdiaction Completed

DetodlBebwPerlmentInfonnatfcti and/orProbtemsAsscckitedwthEJdiacttan

^^<^;5r

^///^/______/o?^rExtzuctable(Base/Neutral)

Extractable(Add)

EbctrcictaMe(Pesticides) ^/^(/^ - ^ U^~

ExtractaUe -(Dioxins)

0

<0

QC Extrnctezble(Base/Neutral)

00

QCExtractable(Add)

QCExtructable(Pesticides)

QCExtradable(Dioxins)

Additional Comments:

•--- L, ^%sy»—

SMO COPY FOR RETURN TO REGION

r AGENCY HWI Sample Management Office

ORGANICS LABORATORY CHRONICLE (ANALYSIS)(^ Sample Number

^: 0571

Laboratory Name

Case Number _

Sample Analyst SignatureCterte/InneAncdyas Ccxn]deted

SEP 91981

Deteril Bebw Pertinent Infanixriia'i and/orProblems Associated with Analysis

Extractable(Base/Neutral)

Extractable(Add)

., .T/W^.-^ /• / I /• •

k. .JL- L .Extractable ^(Pesticides) o

Extractable(Dioxins)

VOA Unpreserved00

VOA Unpreserved(Duplicate)

QC Extractable(Base/Neutral)

QCExIractable(Add)

QCExtraclable(Pesticides)

QC Extractable(Dioxins)

Additional Comments:

- ^^-f..

SMO COPY FOR RETURN TO REGION

">? A T!

isszy\ BBOlt."•'( men®

U.S. ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management OfficeP.O. Box 818. Alexandria. Virginia 22313-703 557-2490 • FIE •557-2490

ORGANICS TBAFnC REPORTSample Number

F 053S

©Case Number:

Sample Site Name/Code:

VP.nT^.

©2) Sample Type: (Check One)

— RunOff

Well

Receiving Water

Leachate

Eifluent

© Ship To:

Attn:

Oher (specify)

©Regional Office:

Sampling Personnel:

© Mark Volume Level on Sample Bottle

(Name)0 / Extractable

DateSampled

© Analysis Lab:Rec'dby: ^> ^^Legu^CDrrt^/Tim^Rpf'd -?/3//^^/^7-

Sample Condition on fteceipt(e.g. broken, no ice, Chainoi-lStstody, etc.)

0(Phone)

Sampling Date:Extractable

\^J6 duJSTft^ -^AfcA-.^MQ ..L<M^t*A/O <l^L^mu^i*^<'^^as^ U-dV. -^j;^]-c<u n^u ,A£^ fif ^?y&T'

(Begin) (End)Extractable

© Shipping mformation Extractable

VOA Unpreserved

Name oi Shipper:VOA Unpreserved(Duplicate)

Date Shipped:

Airbill Number

© Description of Sample Location:

®) Special Handling Instructions:(i' g, :AiietY prccrrnfaons, h(-i7.ardous nature)

07106001T "R I'T^PY rnr; "!--n \w Tr^ •-mn

SAMI

LAB

DATE

STD

CONC

Vola-

2V

3V

4V

6V

7V

10V

11V

13V

14V

15V

16V

u^mmwmM&mwm^^n\m19V

23V

29V

30V

32V

33V

38V

44V

45V

46V

47V

48V

49V

50V

51V

85V

86V

87V

88V

R WEST COAST TECHNICAL

'LE ID LAB BLANK

ID 21881V14

; INJECTED 8/6/81

ID BFB36 VOA157

:. FACTOR ————--

tiles

acrolein

acrylonitrile

benzene

carbon tetrachloride

chlorobenzene

1,2-dichloroethane

1,1,1-trlchloroethane

1,1-dichloroethane

1,1,2-trichloroethane

1,1,2,2-tetrachloroethane

chloroethane

2-chloroethylvinyl ether

chloroform

1,1-dichloroethylene

1,2-trans-dichloroethylene

1,2-dichloropropane

1,3-dichloropropylene

ethylbenzene

methylene chloride

methyl chloride

methyl bromide

bromoform

dichlorobromo methane

trichlorofluoromethane

dichlorodifluoromethane

chlorodibromo methane

tetrachloroethylene

toluene

trichloroethylene

vinyl chloride

S6RVK

ug/1

NnND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

14

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

CEINC

SAMI

LAB

DATI

DATI

STD

CON(

Pest-

89P

90P

91P

92P

93P

94P

95P

96P

97P

98P

99P

100P

101P

102P

103P

104P

105P

106P

107P

108P

109P

HOP

HIP

112P

113P

* =

(p

ND =** ^

. INDUSTRIAL CATEGORY

'LE ID NO SAMPLE

ID

:: EXTRACTED

; INJECTED

ID

;. FACTOR

Lcides

aldrin

dieldrin

chlordane

4,4 '-DDT

4,4 ' -DDE

4.4'-DDD

alpha-endosulfan

beta-endosulfan

endosulfan sulfate

endrin

endrin aldehyde

heptachlor

heptachlor epoxide

alpha-BHC

beta-BHC

gamma-BHC

delta-BHC

PCB-1242

PCB-1254

PCB-1221

PCB-1232

PCB-1248

PCB-1260

PCB-1016

toxaphene

Less than 10 ug/1

esticides less than 5 ug/1)

Not detected

Not confirmed by GCMS(mo tsi

ug/1

NA

NA

NA

MAl

IW

^

NA,

K&

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

A

t—

0710600217605 Fabnca Way, Suite D Cerntos. California 90701 213/921-9831

WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3

QC Report No:Sample Number

LAB BLANK

A. SURROGATE SPIKE RESULTS

COMPOUND

Benzene - d6

l-Chloro-2-Bromopropane

Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyl

Naphthalene-DS

Fraction

VOA

VOA

VOA

ACID

ACID

B/N

B/N

B/N

C o n e . ( u g / 1 )

54

50

56„

-

(Surrogates only)Spike

Added (ug/1)

50

50

50

-

-

-

%Recovery

108

100

112^

^^~^0

——————^~

(-1

B . TENTATIVELY IDENTIFIED COMPOUNDS 0

1.

2.

3.

4.

5.

6.

7.

8.

9.

10.

1 1 .

12.

13.

14.

15.

16.

17.

18.

19.

20.

CAS # COMPOUND NAME FRACTION

% Maximum Score Attained

Mass Matching Routine: FIT(specify)

'

/-1»-<-1 f\ryfSJf———vf-ivrwS.Z

07106003^o^ '--ihrii-n Wiv SmtpD Cerritos. California 90701 SIS.''0"1-"'^ I

W€5T COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

SAMP

LAB

DATE

DATE

STD

CONC

Acid

21A

22A

24A

31A

34A

57A

58A

59A

60A

64A

65A

Base/

1B

5B

8B

9B

12B

18B

20B

25B

26B

27B

28B

35B

36B

37B

39B

LE ID METHOD BLANK

ID 21881A1

EXTRACTED 8/1/81

INJECTED 8/9/81

ID SENS176 PHEN353

FACTOR 1000

Compounds u

2,4,6-trichlorophenol

p-chloro-m-cresol

2-chlorophenol

2,4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol

2,4-dinitrophenol

4,6-dinitro-o-cresol

pentachlorophenol

phenol

/Neutral Compounds

acenaphthene

benzidine

1,2,4-trichlorobenzene

hexachlorobenzene

hexachloroethane

bis(2-chloroethyl)ether

2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1,4-dichlorobenzene

3,3'-dichlorobenzidine

2,4-dinitrotoluene

2,6-dinitrotoluene

1,2-diphenylhydrazine

(as azobenzene)

f luoranthene

g/1

ND

ND

ND

ND

ND

ND

N D

ND

N D

NnND

ND

ND

N D

ND

ND

ND

N D

N D

N D

ND

ND

ND

ND

NDND

SAMP]

LAB I

DATE

DATE

STD I

CONC

Base/

41B

42B

43 B

52B

53B

54B

55B

56B

61B

62B

63B

66 B

67B

68 B

69B

70B

71B

72B

73 B

74B

75B

76B

77B

78B

79B

80 B

81B

82B

83B

84B

-E ID METHOD B L A N K

D 21881B1

EXTRACTED 7/31/81

INJECTED 8/13/81

D BENZ397 BNSTD414

FACTOR 1000

Neutral Compounds u

4-bromophenyl phenyl ether

bis(2-chloroisopropyl) ether

bis (2-chloroethoxy) methane

hexachlorobutadiene

hexachlorocyclopentadiene

isophorone

naphthalene

nitrobenzene

N-nitrosodi methyl a mine

N-nitrosodiphenylamine

N-nitrosodi-n-propylamine

bis (2-ethylhexyl) phthalate

butyl benzyl phthalate

di-n-butyl phthalate

di-n-octyl phthalate

diethyl phthalate

dimethyl phthalate

benzo(a ) anthracene

benzo(a)pyrene

3,4-benzofluoranthene

b e n z o ( k ) f luoranthene

chrysene

acenaphthylene

anthracene

benzo(gh i )pe ry lene

fluorene

phenanthrene

d i b e n z o ( a , h ) a n t h r a c e n e

indeno( 1,2,3-cd )pyrene

pyrene ^^ww-^'-^Q-

g/1

N D

ND

ND

W

HD-^e—JtiD<ss<^ND

ND

ND

ND

N D

*

ND

*

N D

ND

ND

NDND

ND

N DN DNON D

N nNnN D

40B 4-chlorophenyl phenyl ether ND 129B 2,3,7,8-tetrachlorodibenzo-rtr-<jiogQ04

p-dioxin______________________ND

WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

SAMP

LAB

DATE

STD

CONC

Volat

2V

3V

4V

6V

7V

10V

11V

13V

14V

15V

16V

)imXX»XX^KX^)^WX)^X<XiXXXXXXXXXXX

19V

23V

29V

30V

32V

33V38V44V

45V

46V

47V

48V

49V

50V

51V85V

86V

87V

88V

LE ID LAB B L A N K

ID 21881V1

I N J E C T E D 8/5/81

ID BFB34 VOA156r- APTTIP

;iles

acrolein

acrylonitrile

benzene

carbon tetrachloride

chlorobenzene

1,2-dichloroethane

1,1,1-trichloroethane

1,1-dichloroethane

1,1,2-t.richloroethane

1,1,2,2-tetrachloroethane

chloroethane

2-chloroethylvinyl ether

chloroform

1,1-dichloroethylene

1,2-trans-dichloroethylene

1,2-dichloropropane

1,3-dichloropropylene

ethylbenzene

methylene chloride

methyl chloride

methyl bromide

bromoform

dichlorobromome thane

trichlorofluoro methane

die hlorodifluorome thane

chlorodibromomethane

tetrachloroethvlene

toluene

trichloroethylene

vinyl chloride

-

ug/1

ND

ND

ND

ND

N D

N D

ND

N D

N D

N D

ND

ND

ND

ND

ND

ND

N D

ND

19

ND

N D

ND

ND

ND 113P

ND

ND*

ND

N D

ND

SAMP

LAB

DATE

DATE

STD

CONC

Pesti

89P

90P

91P

92P

93P

94P

95P

96P

97P

98P

99P

100P

101P

102P

103P

104P

105P

106P

107P

108P

109P

HOP

HIP

112P

* = I

( p e

ND =-,',- •;';• ^

LE ID METHOD BLANK

ID TRACE #4142

EXTRACTED 7/31/81

INJECTED 8/6/81

ID TRACE M140

. FACTOR 100

cides

aldrin

dieldrin

chlordane

4 , 4 ' - D D T

4 , 4 ' - D D E

4 , 4 ' - D D D

alpha-endosulfan

beta-endosulfan

endosulfan sulfate

endrin

endrin aldehyde

heptachlor

heptachlor epoxide

alpha-BHC

beta-BHC

'gamma-BHC

delta-BHC

PCB-1242

PCB-1254

PCB-1221

. PCB-1232

PCB-1248

PCB-1260

PCB-1016

toxaphene

.ess than 10 ug/1

'sticides less than 5 ug/D

Not detected n^-i f\'\) i JL\}i\Not confirmed by GCMS

071

ug/1

ND

ND

ND

^D

^D

^ND

9D0

N D

ND

N D

N D

N D

ND

ND

ND

ND

N D

N D

N D

ND

ND

N D

N D

N D

N D

rt5t4-f

06005

WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3

QC Report No: 36Sample Number

LAB BLANK

A. SURROGATE SPIKE RESULTS

COMPOUND

Benzene - d6

l-Chloro-2-Bromopropane

Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyl

Naphthalene-DS

Fraction

VOA

VOA

VOA

ACID

ACID

B/N

B/N

B/N

Cone.(ug/1)

43 l

42

45

66

79

46

55

54

(Surrogates only)Spike

Added (uq /1)

50

50

50

100

103

1 0 1

1 0 1

101

%Recovery

86

84

90

66

77

45 ^0

54 "-————^&-

53

B . TENTATIVELY IDENTIFIED COMPOUNDS

1.

2.

3.

4.

5.

6.

7.

8.

9.

10.

1 1 .

12.

13.

14.

15 .

16.

17.

18.

19.

20.

CAS # COMPOUND NAME FRACTION

% Maximum Score Attained

Mass Matching Routine: FIT(specify)

OW^sK-^

07106006

IA/-.V ^ [ l i l r iO fprritn<; C^l i f^rni - on-Til nn "•.OPT

•UPlNTITfiTION REPORT F ILE; 21SS1B2

flTfl: 21881B2.TI3/-13/S1 10:47:80UMPLE: F053G - LflB BLftNK

;ONDS. : E^T/Z. 1 /S 1 CF=l!230"ORMUI. 0 : P1^7"?'13'* TN^TPi'rcMT: F ' ' WJSr-lITT?:^ r'.': '"'":•'.;'14 nNF.LYST- nT "47?

i-lOUMT-F;'7';;"! •••: F'EF.l':M'•;T.•/(F•ErF.l•',REl"!:•'; RE';P.F?;CT?

1.if- •'ni-iT' ''" ('"'"iia

1-~-

\0

00

07106007

oyiogeib-

NO NAME.43 NfiFHTTOLENE CS•4'3 UHKriCU;-;50 Uni Cl,;;.;

Tirc23:43

REF RRT r ETH1 3.000 ft BB

flRER ^r-'^L'NT ";TOT''?^^^'tn;7 —r'^ '"^'^n f fi^ /t < - ,^-^1^-'^'-'-^ • ^•C-','JU^i L_li_]/ L, I 1 ,(,'-—

0.437 l"! FE

00

00

'S: 14 1 P.F?? ft [-•-

^^ n - b tL- ^^tAx^c^a

NO R E T C L ) P1TTIO RRT(L) RATIO RNMT l"smT(L) R . F P C R.F'"-:rL) PRTIO1 2B;40 I . eO 1.000 1.05 30.00 30.00 1.1:33 1 . D C Q 1.133

9

1011 10:35 0.97 0.512 P."? 7.64 75.!""? I.C.-'O 0.335 '?,'-a12131415161713ISSO21-)-'^'^i—3324 1S;E2 1.S1 G.S~2 I .e i 1.3S ZO.1''" O.e^S '~1.??Q 3 ,G5':5?b:7^0.,u

:93031 22:32 1 .P3 l.B?B 1.0° 1.54 30.C3 3.E?S I.;;'?'? ^.':53233343536373S39404112

C^

\0

00

i-" „ i'"' ' i"f <"' •''"""''' '1 r^'' /~''' ^~''~' ''"' i i"'

07106009

-<mo%rr

81280.

PATA: 21881B2 R lBIC68/13/81 10-.47:e9SAMPLE; FG536 - LAB BLAESKRANGE: G 1,1909 LABEL: 11

m 2 3

SCA^S 50 TO E 7 ?C/Ai: F672331 H

0, 4.9 Q'JAt-t: A 0. 1 .0 BASE: U 20, 3

401

\^- ./- \^. 315 353 ! i 433 . ,, (-1— c - ,-: nTt-";^ 9 ft-, f-v'i oc^^^•w'' • ~^>- --,. -,,,. ,-> ,_\, \^_i\ »'i' :j ~)-'.^> „ •- ^ _.;-' ••'w U'l.^S'k, -..'s'-- - .—J ';-" :L"l-i'

6C3469-k , ^ , . T,

SCANTTKT7

DUAL HASS SFECTPJJH68/13/81 10:47:63 + 10:17SAS1PLE; FC535 - LAR ELA'^KEt-IH^KED (S !53 2H GT)

DATA: 21831B2 RIS9CALI: FC723C1 ;/!

BASE It/E: f;3/ 1.:-;'EIC: 71.^5./ f 55.

_,_^,_ .."T

!'I „.

0 0 1 6 2 1

DUAL «ASS SFECTEUn68/13/81 ie:47:69 + IS: HSAHPLE; FC53S - LAB BLAKKENHANCED <S 15B 2E1 87)

BATA: 2183152 ^^3 BASH n/5: I-;;?/ -:'C/.LI: FC723ol 1:1 EIC: 7 '^ . / :.;79.

T ~~ -r ""'—-T—T— T-H/E ^ ?C" 159

_i_._L__J__J__L_'_ i- I i I I I i I i_.J__\_..I_i i i_^i, .. i_ . '

0 0 1 6 2 2

DUAL MASS STECTElf:!e8/!3/81 10:-17:63 + 22:33SAnPLE: F':33S - LAS rLAt:KEHHA':CE3 (S 153 W GT)

DA7A; 2i83[B2 ^^33CALI: FC7233! (:!

BASE S'/E: i1..?/ I - . : 'RIC: 121.5. / ' • 8 7 .

^( ; / ^^A '

""T——r"

0 0 1 6 2 5

^ WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3

QC Report No:, 36Sample Number

F0571 Cont.

A. SURROGATE S P I K E RESULTS

COMPOUND

Benzene - d6

l-Chloro-2-Bromopropans

Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyl

Naphthalene-DS

Fraction

VOA

VOA

VOA

ACID

ACID

B/N

B/N

B/N

C o n e . ( u g / 1 )

(Surrogates on ly)Spike

Added (ug /1 )%

Recovery

e^—————CM-

\0

0

B . TENTATIVELY IDENTIFIED COMPOUNDS

1.

2.

3.

4.

5.

6.

7.

8.

9.

10.

1 1 .

12 .

13.

14.

15 .

16.

17.

18.

19.

20.

CAS # COMPOUND NAME

CHLOROPHENOL

TRICHLOROMETHOXY-

BENZENE

UNKNOWN

HYDROCARBON

HYDROCARBON

HYDROCARBON

HYDROCARBON

FRACTION

B/N # 2 1 3

B/N #301

B/N #334

B/N #456

B/N #489

B/N #509

B/N # 5 1 8

% Maximum Score Attained

Mass Matching Routine: FIT(specify)

GENERAL FIT

GENERAL FIT

NO GOOD FIT

GENERAL FIT

GENERAL FIT

GENERAL FIT

GENERAL FIT

'

(mn^ni.i

- » •0^-1 /»r;'i-"''?^l- - —4 Jl.O.'-.b .tJ^

WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3

QC Report No: 36Sample Number

F0571

A. SURROGATE SPIKE RESULTS

COMPOUND

Benzene - d6

l-Chloro-2-Broniopropane

Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-FluorobiphenyJL

Naphtha 1ene-D8

Fraction

VOA

VOA

VOA

ACID

ACID

B/N

B/N

B/N

Conc.(ug/1)

54

42

54

50

75

105

91

88

(Surrogates only)Spike

Added (ug/1)

50

50

50

100

103

101

101

101

%Recovery

108

84

108

50 IT

73 C\

104 ^

90. ^

87 c

B. TENTATIVELY IDENTIFIED COMPOUNDS

1.

2.

3.

4.

5.

6.

7.

8.

9.

10.

11.

12.

13.

14.

15.

16.

17.

18.

19.

20.

CAS % COMPOUND NAME

ACETONE

2-METHYLPROPANAL

BUTANAL

PENTANE

CYCLOHEXANE

1-BUTANOL

3-METHYLHEXANE

2-METHYLHEXANE

4-CHLOROPHENOL

UNKNOWN

',4,5-TRICHLOROPHENOL

4.5-DICHLORO-2-METHOXY

PHENOL

DICHLOROPHENOL

UNKNOWN

UNKNOWN

UNKNOWN

UNKNOWN

CHLORO-METHYL-BENZENE

2-ETHYL-1-HEXANOL

FRACTION

VOA #88VOA #135

VOA #158

VOA #184

VOA #193

VOA #208

VOA #337

VOA #346

ACID #92

ACID #194

ACID #208

ACID #229

ACID #265

ACID #287

AICD # 3 1 9

ACID #454

B/N #47

B/N #106

B/N #126

% Maximum Score Attained

Mass Matching Routine: FIT(specify)

965

874

983

935

987

973

985

990

792

NO GOOD FIT

696

935

GENERAL FIT

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

GENERAL FIT lUbUlt

963 0^3-0^24

r>r r.,l,r.r,-. ».«.'-.. .• c;||jfr.n ramtn<!. C.-llifrirni-l "0701 ?n fa^.gff^f

WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

SAMP

LAB

DATE

STD •

CONC

Volat

2V

3V

4V

6V

7V

10V

11V

13V

14V

15V

l6V

m^nw^u^wwwJW^mwuwunn19V

23V

29V

30V

32V

33V

38V

44V

45V

46V

47V

48V

49V

50V

51V

85V

86V

87V

88V

LE ID F0571

ID 21881V18 & 21i

INJECTED 8/6/81

ID BFB36 VOA157

« rA'^.i 'JK

iles

acrolein

acrylonitrile

benzene

carbon tetrachloride

chlorobenzene

1,2-dichloroethane

1,1,1-trichloroethane

1,1-dichloroethane

1,1,2-trichloroethane

1,1,2,2-tetrachloroethane

chloroethane

2-chloroethylvinyl ether

chloroform

1,1-dichloroethylene

1,2-trans-dichloroethylene

1,2-dichloropropane

1,3-dichloropropylene

ethylbenzene

methylene chloride

methyl chloride

methyl bromide

bromoform

dichlorobromo methane

trichlorofluoro methane

dichlorodifluoromethane

chlorodibromomethane

tetrachloroethylene

toluene

trichloroethylene

vinyl chloride

381V19

ug/1

ND

NO

124

ND

*

ND

ND

N D

ND

ND

ND

ND*

*

ND

ND

ND*

13

ND

ND

ND

ND

ND

ND

ND

ND

270QO*

ND

SAMPI

LAB I

DATE

DATE

STD I

CONC.

Pestic

89P

90P

91P

92P

93P

94P

95P

96P

97P

98P

99P

100P

101P

102P

103P

104P

105P106P

107P

108P

109P

HOP

111P

112P

113P

* = L

(pe

ND =* * ^

VOA ND =

-E ID F0571

D TRACE #4158

EXTRACTED 7/31/81

INJECTED 8/7/81

D TRACE #4156

FACTOR 100

tides

aldrin

dieldrin

chlordane

4,4 ' -DDT

4,4 ' -DDE

4.4 ' -DDD

alpha-endosulfan

beta-endosulfan

endosulfan sulfate

endrin

endrin aldehyde

heptachlor

heptachlor epoxide

alpha-BHC

beta-BHC

gamma-BHC

delta-BHC

PCB-1242

PCB-1254

PCB-1221

PCB-1232

PCB-1248

PCB-1260

PCB-1016

toxaphene

ess than 10 ug/1

sticides less than 5 ug/1)

Not detected

Not confirmed by GCMS

less than 2 ug/1 fvy&^w

ug/1

ND

ND

^^

N§^

——————Q-

1

N D

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

N D

NO

ND

NOND

ND

N D

(W06oi6

-K25

WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

SAMP

LAB

DATE

DATE

STD :

CONC

Acid

21A

22A

24A

31A

34A

57A

58A

59A

60A

64A

65A

Base/

1B

5B

8B

9B

12B

18B

20B

25B

26B

27B

28B

35B

36B

37B

39B

40B

LE ID F0571

ID 21881A11 & 21881A12

EXTRACTED 8/1/81

INJECTED 8/10/81

ID SENS177 PHEN354

FACTOR 1000 & 20

Compounds

2,4,6-trichlorophenol

p-chloro-m-cresol

2-chlorophenol

2,4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol

2,4-dinitrophenol

4,6-dinitro-o-cresol

pentachlorophenol

phenol

•^Neutral Compounds

acenaphthene

benzidine

1,2,4-trichlorobenzene

hexachlorobenzene

hexachloroethane

bis(2-chloroethyl)ether

2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1,4-dichlorobenzene

3,3'-dichlorobenzidine

2,4-dinitrotoluene

2,6-dinitrotoluene

1,2-diphenylhydrazine

(as azobenzene)

fluoranthene

4-chlorophenyl phenyl ether ND

ug/1

2400

ND

4000

14000

ND

ND

ND

NDND

ND

1200

ND

ND

33

ND

ND

ND

ND*

ND*

ND

NDND

NnND

SAMP

LAB

DATE

DATE

STD

CONC

Base/Neutral Compounds u;

41B

42B

43B

52B

53B54B

55B56B

61B

62 B

63B

66 B

67B

68B

69B70B

71B72B

73B

74B

75B

76B

77B

78B79B80B

81B

82B

83B

84B

129B

p-dic

LE ID F0571

ID 21881B12

EXTRACTED 7/31/81

INJECTED 8/21/81

ID BENZ401 BNSTD418

FACTOR 1000

4-bromophenyl phenyl ether

bis(2-chloroisopropyl) ether

bis (2-chloroethoxy) methane

hexachlorobutadiene

hexachlorocyclopentadiene

isophorone

naphthalene

nitrobenzene

N-nitrosodimethylamine

N-nitrosodiphenylamine

N-nitrosodi-n-propylamine

bis (2-ethylhexyl) phthalate

butyl benzyl phthalate

di-n-butyl phthalate

di-n-octyl phthalate

diethyl phthalate

dimethyl phthalate

benzo(a) anthracene

benzo(a)pyrene

3,4-benzofluoranthene

benzo(k)f luoranthene

chrysene

acenaphthylene

anthracene

benzo(ghi)perylene

fluorene

phenanthrene

dibenzo(a ,h)an thracene

indeno( 1,2,3-cd)]3yr,ene,,^ (T/106U-17

pyrene

2,3,7,8-tetrachlorodiben£b'?K^

>xin

g/1

ND

ND

ND

ND

N D r-N D ^

ND'0

NDQ

NDO

ND

ND

17*

*

*

*

ND

ND

ND

ND

N D

ND

ND

N D

ND

N D

NnNnNnND

^t2G~

ND

ORGANICS TRAFFIC REPORT3) Sample Type: (Check One)

—— RunOtf

Well

Receiving Water

Leachate

Effluent

. Ofher (specify)

Attn:

Regional Office:npling Personnel:

(j) Mark Volume Level on Sample Bottle

; i •• /'••••^ ^ /. ! i 'J ,/•/•'•€-

(Name).-• 7 / / Extradable

DateSampled

(D AncdysisLab:Rec'dby: / ^ ^v^^sm.Date/Time Rec'd ^//^ //^ah

Sample Condition on ReceipN(eg. broken, no ice, Chain-of-Custoay-etc.)

(Phone)

mphng Date:Extractable

(W ret J^ed. OTuJwiMw{, CJLULtoalLu, ftt^J^JUk.•tf^M ^e nJb, rrvtTAfJl

Begin) (End)Extiactable

3 Shipping Information Extradable

,1 VOAUnpreserved

Name o( Shipper:VOA Unpreserved(Duplicate)

Date Shipped:

Airbill Number:

T) Description of Sample Location:

® Special Handling Instructions:(e g.. safety prr'caununs, hi,curcioua nature)

07106018

LAB COPY FOR RETURN TO SMO

BSD ORGANICS TRAFFIC REPORT IMtrrq(T) Case Number

.^^

Sample Site Name/Code:

@ Regional Office:Sampling Personnel:

f - , ' ) , - • • / '. • .-'. . . ; . , f ,1 / , / < ^ / / / ' / < ,••;.//••/(Name)

.."0 < "•" 7! - i ? I(Phone)

Sampling Date::' ' /' "/ .'•...--• f

(Begin) (End)

(J) Shipping Infonnation

7'.. .T^...,-' Name of Shipper

Date Shipped-'

» .— •— ~ -T• - : ' . ' * ^ > ,' '\

Aubill Number:

(7) Description of Sample Location:

'/ - • • ' / ^ -^

(^) Special Handling Instructions:(ea,, aaiety precautions, haaardousnuturB)

07106019» ^

^ -'. . . • - - ' ' • ; -• • / / ' WWZ'BZS~

© Sample Type: (Check One)

Run Off

.'-': Wpll

—— Receiving Water

,.. I iam-l-irrtP

——— Effluent

Ofhor C<3penfy)

(j) Mark Volume Level on San

:/

Extractable

ExtractaUe

Extractable

Extractable

VOA Unpreserved

VOA Unpreserved(Duplicate)

nple Bottle

DateSampled

-7-^-y/^

,-••• . '• ' • /

;' - " :>'/

(j) Shy To:-, ^- f / /^ / ^ •"•

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(J) Analysis Lab: Q^Rec'dby /&^i ^^0^Dote/Tim^Rfic'd ??/5/>% ^ -

Somple Condition on Beoeipt(e.g. broken, no ice, Chain-ofOistody, etc.)

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ORGANICS TRAFnC REPORTSample Number

©Case Number- • ~!

^'J ^ J

Sample Site Name/Cede:

©2) Sample Type: (Check One)

— RunOff

-/1^ lir 11

© Ship To:

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Receiving Water

Leachate

Effluent

, Ofrier (specify)

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Attn:

©Regional Office:Sampling Personnel:

Q[) Mark Volume Level on Sample Bottle

(Name)

S-."/ ?7/ - / 7^/Extractable

(Phone)

Sampling Date:Extractable

DateSampled

(J) Analysis Lab:Rec'dby: ^i^ ^ ^iOUDate/TimeRec'd •7/3/^ //»7

Sample Condition on Receipt(e.g. broken, no ioe, Chain-of^Aistody, etc.

AID (luJ^askt M^cno^^t^^ou^e^^^^

(Begin) (End)Extractable

(6) Shipping Intormation Extractable

VOA Unpreserved

Name of Shipper:VOA Unpreserved(Duplicate)

Date Shipped:

"• "?- .,•1

Airbill Number

(7) Description of Sample Location:

Q) Special Handling Instructions:®(e g., safety precautions, hazardous ncTture)

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" ,*•' A ^' U.S. ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

PO Box818.A!».y.md™,Vinwin2231^-7Cl3 557.2490'FTS 557-2490

ORGANICS TRAFnC REPORTSample Number

F 0567

©Case Number:s^-o

Somple Site Name /Code:

©

\-

2) Sample Type: (Check One)

— RunOff

. Well

. Receiving Water

. Leachate

Effluent

Ofher (specify)

(J) Ship To:

v./9 J t r^.-'Jl ^ ( : C - 5 r!'^

/' .-. / r •r i

Attn:

7

©Regional Office:Sampling PeisonneL

© Mark Volume Level on Sample Bottle

(Name)

C2Z——2Z———Z^_(Phone)

Sampling Date:Extractable

DateSampled

?-.,• -/ • I/

(J) Analysis Lab: ^Reed by: A^* ^ f »Date/rime Rec'd / //^

Sample Condition on Beceipt(e.g. broken, no ice, Chain-ofOistody, etc.)

-</<-» A.lA/Sb^ ^<<Srffc<y crAJ~3.^'e>^'

//o (rjui^^^^^^-^'y--^ .^ / ^^AE» / ^tM.ffXJ-^-i i

(Begin) (End)Extractable

(i) Shipping Information Extractable

VOA Unpreserved

Name ot ShipperVOAUnpreserved(Duplicate)

Date Shipped:

Airbill Number

(7) Description of Sample Location:

./ '

(J) Special Handling Instructions:(e i;., safety precautions, hciairdous notui'e) 07106021

U.S. ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office }PaBcx8l3.A^xan.^i.V^nra<-i22313 703 b57^.4'JO-t-TS -W 2.190 \

ORGANICS TRAFnC REPORT© Case Number:

.cs'c?

Sample Site Name /Code:

©2) Sample Type: (Check One)

— RunOff

WeH

Receiving Water

Leachate

Effluent

Ofher (specify)

(j) Shy To:

y/s"^ v •-'^•s ' /rr"»/ •

^J5 A ^ - ^ -

•? -»-/ ^:' \ 1'. {< ( '^

^.^••>/

Attn:

^ \" ^< '^^J

(7) Regioncd Office:

Sampling Personnel;

/: ;: ;;../'/- ff

(j) Mark Volume Level on Sample Botfle

DateSampled

(Name)

^ - -^/Extractable

(]D Analysis Lab: C\JRec'dby: /^A^' A^Date/TimeRecd j»^/^/ //^

Sample Conditional Receipt(eg. broken, no ice, Chain-of-Custody, e

0. ..(Phone)

Sampling Date:Extractable

(Begin) (End)Extractable

(^) Shipping Information Extractable

"T' / VOA Unpreserved

Name of ShipperVOA Unpreserved(Duplicate)

Date Shipped:

.- ,A ,.—" ^ --, —'' .-'• -1 3 / -?

Airbill Number

(7) Description of Sample Location:

® Special Handling Instructions:(e.g., anfety precautions, h<,-!znrdous nature)

I An ^~-r~'nv T-^M-. •

o^o^^T"07106022

U.S. ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office557 -2490 •FTS 557-2490

ORGANICS TRAFFIC REPORTSample Number

Sample Site Name/Code:

(?) Sample Type: (Check One)

—— RunOif

^S- Well

——— Receiving Water

——— Leachate

—— Effluent

——— CXher (specify)

(D Ship To:

'y^ (^'^ 7?(-'- ^ ' /-.'•7 5 ^ ,. .-• . y

^ - ' . / .

Attn:

@ Regional Office:

Sampling Personnel:

(D Mark Volume Level on Sample Botfle

• ; „• .r : " <•(Name)

'•?/. / 2LExtractable

DateSampled

@ AnalysisLab: .Reed by: A^^ . g^gzZ

Date/Time Rec'd ^ft' ^^

Sample Condition on Receipt(e.g. broken, no ice, Chain-of-fiystody, etc.)

(Phone)

Sampling Date:Extractable

(Begin) (End)Extractable

(6) Shipping Information Extractable

VOA Unpreserved

Name of Shipper:VOA Unpreserved(Duplicate)

Date Shipped:

Airbill Number.

(T) Description of Sample Looation:

® Special HandUng Instructions:(eg., sulcty pnscautions, hcizardous natiire)

T ^ n f^/^PV r'/ o r'T~"-r m^r 'T\- i

wwsesz-^07106023

U.S. ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management OfficeP.O Ecx8i8 AieKTn'Inci.Vir-iini.'i;^!^ . ".":• '-^•-^ffl-F'lS 55774^)

ORGANICS TRAFnC REPORTSample Number >

©Case Number.7^0

Saniple Site Name/Code:

©y Sample Type: (Check One)

— RunOff

WeU

Receiving Water

Leachate

Effluent

Other (spedfy)

q>.'7, "

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-5' /-'-/'/- ^ i'';/'••/,/• .. , , ^ /

• / ^

7^^ 3 /-

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Attn:

f^i- , ,••! (-'J

Q) Regional Office:Scanpling Personnel:

• i ' i ' / . . r ' / - f C

© Mark Volume Level on Sample Bottle

DaleSampled

(Name)^7/ J'// - .' 7r-/ Extractable

(Phone)

(J) AnalysisLab: ^Rec'dby: , ^* ,j^^^Date/Time Rec'd //^ //^/z

Sample Condition on receipt(e.g. broken, no ice, Chcrin-of^listody, etc.)

•Qe /.., ./

Sampling Date:• /. 'C / ~a~

(Begin) (End)Extractable

(J) Shipping Information Extractable

VOAUnpreserved } /Name of Shipper:

VOAUnpreserved(Duplicate)

Date Shipped:

^^ -J / i

Airbill Number

(7) Description of Sample Location:

/'.- / / -: /1 • \ ' . - /

(y Special Handling Instructions:(e.g., safety precnuhons, hcizardous nature)

^<1-0^105^33—

07106024i ^ R r^uv mp Rrrr TPM TV-^ CM^I

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U.S. ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management OfficeP.O.Box8I8,Alox;^-i^i.V;r<-Ji^ci223'3 .703 557 2490-FTS 557-2490

ORGANICS TRAFnC REPORTSample Number

F 0571

0 Case Number:

5^0_©

Sample Site Name/Code:

2) Sample Type: (Check One)

—— RunQff

X- Well

—— Receiving Water

__ Leachate

—— Effluent

—— Other (specify)

@ Ship To:'/f^ (•}f.•.\'f / e c ' - f ^ ' f •/

'•^•S ^•,^,./. iv-^.. / . /. /

Attn:

^^ , .•-• ft ^

Q Regional Office:

Sampling Personnel:

Q Mark Volume Level on Sample Bottle

• / , - /' /, -'.../^ f?(Name)

^l_2i—2^L Extractable

DateSampled

(J) Analysis Lab:Rec'dby: . fc^t. ^^ry/Date/Tune Reed ^•?//</Ky^7

Sample Condition on Receipt *(e.g. broken, no ice, Chain-of-CuStody, etc.)

(Phone)

Sampling Date:Extractable

(Begin) (End)ExtractaHe

(6) Shipping Information Extractable

/ •? VOAUnpreserved

Name of Shipper:VOAUnpreserved(Duplicate)

Date Shipped:

Airbill Number

: (7) Description of Sample Location:

C'

\s) Special Handling Instructions:(e.g., s-iiety precautions, ticnnrdous nature)

I AR (-OPY FOR RF-n fRN TO ?MO

(3<1_—

0'?^OS634--

07106025

ORGANICS TRAFFIC REPORT(T) Case Number:

^

Sample Site Name/Code:

JL

©2) Sample Type: (Check One)

— RunOff

WeH

Receiving Water

Leachate

——— Effluent

^ OSier (specify) /-^ 6 B l ^ ^ K

©ShipTo: . „ . . . ,

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Attn:

/-^c^ ^^hfS

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Sampling Peraarmel:

^^^; M^D^/^

Q[) Mark Volume Level on Sample Bottle

(Name) \

;. J ^ / - / 7 0 /Extractable

(Phone)

Sampling Date:

• ^ l f ] - - S i St-^t

Extractable

(Begin) (End) Extractable

(6^ Shipping Information

—<— ~T~ / ,, i,..., ^^•J • / ( p

Name of Shipper:

-?- -:•- S l

Extractable

VOA Unpreserved

VOAUnpreserved(Duplicate)

Date Shipped:

Airbill Number

(7) Description of Sample Location:

Lab ^t^^

\J[) Special Handling Instructions:(e.g., safety precautions, hazardous nature)

REGIONAL OFFICE FILE COPY

bample No: t-UbbbLab Standard ID:

TRACE Ml 52 & 4153

STD I . D . TRACE #4151

U . S . ENVIRONMENTAL PROTECTION AGENCY

HWI SAMPLE MANAGEMENT OFFICE

QUALITY CONTROL REPORTB. DUPLICATE ANALYSIS

Lab Mame-.HEST COAST TECHNICAL SERVICE. INC.Report No:______^fi________Page 5___ of ___5_____

0<l

Ss

ft

:OMPOUNO (including surroqates)

P. P. %

<i

\

\

<

^his'QC Report also covers the following sample numbers: F0535. F0536, F0564-F0571. C0592-C0596, G0360-G0364i ., 00 4-^—3—Z————

4

3

k

«»^

S——3..

\

4 V

COMPOUND NAME

METHYLENE CHLORIDE

BENZENE-D6

1-CHLORO-2-BROMOPROPANE

TOLUENE-D8

PESTICIDES NONE DETECTED

CONCENTRATION (uq /1 )

Aliquot 1 (D,)

20

49

44

46

ND

Aliquot 2 (D^)

19

49

45

48

ND

Relative PercentDifference

(RPD)*

5

0

2

4

0

(D, - OJ*RPD = - , 1 — 2 X 100pnpn)^^

Ldu JLdilualu m. V U A 1 5 0 I KrtLL t f 4 1 b U

STD I.D.; TRACE #4159HMI SAMPLE MANAGEMENT OFFICE Report No:

Page 4 of

QUALITY CONTROL REPORTA. MATRIX SPIKE ANALYSIS

0lk^^

^cM

COMPOUND (including surrogates)

P. P. #

- . . „ „ „ . , ^, y.ii . - . i .-...-L - rnR^K cnRQC cncc/1 cnK7i rr>CQO rncoc fnicn nnic/i

4

0

8

0

4

4

6

7

V

V

V

V

COMPOUND NAME

METHYLENE CHLORIDE

BENZENE

TOLUENE

CHLOROBENZENE

BENZENE-06

1-CHLORO-2-BROMOPROPANE

TOLUENE-08

HEPTACHLOR

ALDRIN

DIELDRIN

4,4 ' -DOT

SampleResult (SR)

20

ND

NO

NO

49

44

46

ND

NO

ND

ND

CONCENTRATION (ug/1)Spiked SampleResult (SSR)

21

24

21

46

48

46

51

3.3

2.9

4.4

4.4

SpikeAdded (SA)

0

25

25

25

50

50

50

4.9

5.0

5.0

4.6

%Recovery*

96

84

184

96

92

102

67

58

88

95

0 0 1 6 3 b* Recovery = ^"^ x 100

(SA)

^dillple No:_____hUbb4___Lab Standard~TDlPHEN353

U.S. ENVIRONMENTAL PROTECTION AGENCY

HWI SAMPLE MANAGEMENT OFFICE

QUALITY CONTROL REPORTB. DUPLICATE ANALYSIS

Lab Name:NEST COAST TECHNICAL SERVICE. INC.Report No:____36__________Page 5 of 5_____

i—i<^J

ca-cy;

:OMPOUMD (including surrogates)

P. P. #

6

3

2

c,

1

1

A

A

A

COMPOUND NAME

PHENOL

2,4-DICHLOROPHENOL

2,4.6-TRICHLOROPHENOL

PHENOL-05

DIETHYLPHTHALATE

DI-N-BUTYLPHTHALATE

BIS(2-ETHYLHEXYL)PHTHALATE

1,2,4-TRICHLOROBENZENE

NITROBENZENE D5

2-FLUOROBIPHENYL

NAPHTHALENE D8

2-FLUOROPHENOL

CONCENTRATION (uq/1)

Aliquot 1 (D,)

1

1 4

2

103

1

2

1 1

ND

52

64

59

84

Aliquot 2 (0^)

ND

14

2

109

1

2

8

1

57

67

63

89

Relative PercentDifference

(RPD)*

100

0

0

6

0

0

,32

100

9

5

7

6

This QC Report also covers the following sample numbers: F0535, F0536.-F0564-F0571, C0592-F0596, G0360-G0364———————————————————————______—001 639———————————

*RPD(0^ - D^)

[(TT.-T-D^X 100

Hiu JLauuuiu iu. t^hLllJO-.) HNI SAMPLE MANAGEMENT OFFICE Report No:'Page 4 of

QUALITY CONTROL REPORTA . MATRIX SPIKE ANALYSIS

S<2^0W0u

:OMPOUND (includinq surroqates)

P. P. #

6

3

2

2

2

5

1

1

2

4

A

A

A

A

A

COMPOUND NAME

PHENOL

2,4-DICHLOROPHENOL

2,4,6-TRICHLOROPHENOL

PENTACHLOROPHENOL

4-CHLORO-M-CRESOL

2-CHLOROPHENOL

PHENOL-Df)

4-NTTROPHFNOI

2-FLUOROPHENOL

1.2.4-TRICHLOROBEN7FNE

ACENAPHTHFNE

2.6-DINITROTOLUENE

DI-N-BUTYLPHTHALATE

PYRENE

N-NITROSO-DI-N-PROPYLAMINE

1,4-DICHLOROBENZENE

NITROBENZENE

2-FLUOROBIPHENYl

NAPHTHALENE D8

SampleResult (SR)

1

1 4

2

ND

ND

ND

103

ND

84

ND

ND

ND

2

ND

ND

ND

52

64

59

.

CONCENTRATION (uq/1)Spiked SampleResult (SSR)

27

9

ND

24

23

29

65

737

53

32

37

35

6

32

27

30

67

69

67

SpikeAdded (SA)

52

-

-

52

51

54

103

536

100

51

51

50

53

50

51

51

101

101

101

%Recovery*

50

-

46

45

54

63

138

53

63

73

70

8

64

53

59

66

68

66

This QC Report also covers the following sample numbers: F0535' F0536' F0564-F0571, C0592-C0596, G0360-G0364

0 0 1 6 4 0* Recovery - (SSR-SR) , IQO W^^-

(SA)

saagi

SAMt

LAB

DATE

STD

CONC

Vola-

2V

3V

4V

6V

7V

10V

11V

13V

14V

15V

16V

n^mmwmiMw^mmwwnnmn19V23V

29V

30V

32V

33V

38V

44V

45V

46V

47V

48V

49V

50V

51V

85V

86V

87V

88V

Ul WEST COAST T€CHNICAL

'LE ID LAB BLANK

ID 21881V14

; INJECTED 8/6/81

ID BFB36 VOA157

:. FACTOR ————--

tiles

acrolein

acrylonitrile

benzene

carbon tetrachloride

chlorobenzene

1,2-dichloroethane

1,1,1-trichloroethane

1,1-dichloroethane

1,1,2-trichloroethane

1,1,2,2-tetrachloroethane

chloroethane

2-chloroethylvinyl ether

chloroform

1,1-dichloroethylene

1,2-trans-dichloroethylene

1,2-dichloropropane

1,3-dichloropropylene

ethylbenzene

methylene chloride

methyl chloride

methyl bromide -

bromoform

dichlorobromo methane

trichlorofluoromethane

dichlorodifluoromethane

chlorodibromomethane

tetrachloroethylene

toluene

trichloroethylene

vinyl chloride

SERVI

ug/1

NO

,NDND

ND

ND

ND

. ND

NDNnND

Nn

ND

ND

ND

ND

ND

ND

ND

14

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

C61NC

SAM!

LAB

DAT!

DAT!

STD

CON(

Pest

89P

90P

91P

92P

93P

94P

95P

96P

97P

98P

99P

100P

101P

102P

103P

104P

105P

106P

107P

108P

109P

HOP

HIP

112P

113P

* =

(PND =** ^

. INDUSTRIAL CATEGORY

^E ID NO SAMPLE

ID

; EXTRACTED

; INJECTED

ID

:. FACTOR

icides

aldrin

dieldrin

chlordane

4,4'-DDT

4,4 '-DDE

4,4'-DDD

alpha-endosulfan

beta-endosulfan

endosulfan sulfate

endrin

endrin aldehyde

heptachlor

heptachlor epoxide

alpha-BHC

beta-BHC

gamma-BHC

delta-BHC

PCB-1242

PCB-1254

PCB-1221

PCB-1232

PCB-1248

PCB-1260

PCB-1016

toxaphene

Less than 10 ug/1

esticides less than 5 ug/1)

Not detected

Not confirmed by GCMSvr+ifli

ug/1NA

NA

NA

NA

^A

^A

^NA

r^A

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

5032(5^—

17605 Fabrica Way. Suite D Cerritos, Caltfornia 90701 213/921-9831

WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3

QC Report No:_ 36Sample Number

LAB BLANK

A. SURROGATE SPIKE RESULTS

COMPOUND

Benzene - d6

l-Chloro-2-Bromopropane

Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyl

Naphthalene-DS

Fraction

VOA

VOA

VOA

ACID

ACID

B/N

B/N

B/N

C o n e . ( u g / 1 )

43 I

42

45

66

79

46

55

54

(Surrogates only)Soi ke

Added (uq /1)

50

50

50

100

103

101

101

101

%Recovery

86

84

90

66

77 C\J

45 ^

54 "

53 o

B . TENTATIVELY IDENTIFIED COMPOUNDS0

1.

2.

3.

4.

5.

6.

7.

8.

9.

10.

1 1 .

12.

13.

14.

15 .

16.

17.

18.

19.

20.

CAS # COMPOUND NAME FRACTION

% Maximum Score Attained

Mass Matching Routine: FIT(specify)

.

0710603-

0^10^642

i-r-.n', r-,]-ir'rn Wnv Sl i i tpD Cprrjtos. California qf)701 ? 1 3 ' 0 2 1 - 9 8 3 1

SSSf^

SAMP

LAB

DATE

STD •

CONC

Volat

2V

3V

4V

6V

7V

10V

11V

13V

14V

15V

16V

)l»MXXMX^KX»^W©tX^XDOXMDtMiXXXXXXXXXn

19V

23V

29V

30V

32V

33V

38V

44V

45V

46V

47V

48V

49V

50V

51V

85V

86V

87V

88V

a W€ST COAST TECHNICAL

LE ID LAB BLANK

ID 21881V1

INJECTED 8/5/81

ID BFB34 VOA156TrAC""mR

iles

acrolein

acrylonitrile

benzene

carbon tetrachloride

chlorobenzene

1,2-dichloroethane

1,1,1-trichloroethane

1,1-dichloroethane

1,1,2-trichloroethane

1,1,2,2-tetrachloroethane

chloroethane

2-chlorpethylvinyl ether

chloroform

1,1-dichloroethylene

1,2-trans-dichloroethylene

1,2-dichloropropane

1,3-dichloropropylene

ethylbenzene

methylene chloride

methyl chloride

methyl bromide

bromoform

dichlorobromomethane

trichlorofluoromethane

dichlorodifluoromethane

chlorodibromomethane

tetrachloroethylene

toluene

trichloroethylene

vinyl chloride

.SGRVIQ

ug/1

ND

ND

N D

ND

N D

ND

ND

N D '

ND

N D

ND

ND

ND

ND

ND

ND

N D

ND

19

ND

ND

ND

ND

ND

ND

ND*

NDND

ND

E I N C .

SAMP

LAB

DATE

DATE

STD '.

CONC

Pesti.

89P

90P

91P

92P

93P

94P

95P

96P

97P

98P

99P

100P

101P

102P

103P

104P

105P

106P

107P

108P

109P

HOP

HIP

112P

113P

A = I

(p.

ND =•A" '^

INDUSTRIAL CATEGORY

LE ID METHOD BLANK

ID TRACE #4142

EXTRACTED 7/31/81

INJECTED 8/6/81

[D TRACE #4140

. FACTOR 100

cides

aldrin

dieldrin

chlordane

4,4 ' -DDT

4,4 ' -DDE

4,4 ' -DDD

alpha-endosulfan

beta-endosulfan

endosulfan sulfate

endrin

endrin aldehyde

heptachlor

heptachlor epoxide

alpha-BHC

beta-BHC

- gamma-BHC

delta-BHC

PCB-1242

PCB-1254

PCB-1221

PCB-1232

PCB-1248

PCB-1260

PCB-1016

toxaphene

..ess than 10 ug/1

•sticides less than 5 ug/1)

Not detected 0'«'10

Not confirmed by GCMS

0^102643

,

ug/1

ND

ND

ND

^D

3°^A-/JjD

OStD

^D

ND

N D

N D

N D

ND

ND

ND

ND

ND

ND

N D

ND

ND

ND

ND

N D

ND

6034

^

WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

SAMP

LAB •

DATE

DATE

STD 1

CONC

Acid

21A

22A

24A

31A

34A

SPA

58A

59A

60A

64A

65A

Base/

1B

5B

8B

9B

12B

18B

20B

25B

26B

27B

28B '

35B

36B

37B

39B

40B

LE ID METHOD B L A N K

ID 21881A1

EXTRACTED 8/1/81

INJECTED 8/9/81

;D SENS176 PHEN353

FACTOR 1000

Compounds u,

2,4,6-trichlorophenol

p-chloro-m-cresol

2-chlorophenol

2,4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol

2,4-dinitrophenol

4,6-dinitro-o-cresol

pentachlorophenol

phenol

Neutral Compounds

acenaphthene

benzidine

1,2,4-trichlorobenzene

hexachlorobenzene

hexachloroethane

bis(2-chloroethyl)ether

2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1,4-dichlorobenzene

3,3'-dichlorobenzidine

2,4-dinitrotoluene

2,6-dinitrotoluene

1,2-diphenylhydrazine

(as azobenzene)

f luoranthene

4-chlorophenyl phenyl ether

g/1

ND

ND

ND

ND

NONDN D

ND

ND

ND

ND

ND

ND

N D

ND

N D

NDND

ND

N D

ND

ND

ND

ND

NDND

ND

SAMPI

LAB I

DATE

DATE

STD I:

CONC

Base/

41B

42B

43 B

52B

53B

54B

55 B• 56B

61B62B

63B

66B

67B

68B

69B

70B

71B

72B

73B

74B

75B

76B

77B

78B

79B

SOB

81B

82B

83B

84 B

129B

p-dio;

-I

D

E

I

D

F

N.

4-bromophenyl phenyl ether

bis(2-chloroisopropyl) ether

bis (2-chloroethoxy) methane

N-nitrosodi-n-propylamine

bis (2-ethylhexyl) phthalate

butyl benzyl phthalate

di-n-butyl phthalate

dl-n-octyl phthala te

diethyl phthalate

dimethyl phthalate

b e n z o ( a ) anthracene

benzo(a)pyrene

3, 4-benzofluoranthene

b e n z o ( k ) f l u o r a n t h e n e

benzo(gh l )pe ry l ene

d i b e n z o ( a , h ) a n t h r a c e n e

indeno( 1,2,3-cd)pyrene N D

pyrene wn f\^n^ii-—i-i—————————u «'.1U<JU«J5—2,3,7,8-tetrachlorodibenzo-

<in QW^Wr

^ ID METHOD B L A N K

21881B1

:XTRACTED 7/31/81

NJECTED 8/13/^1

BENZ397 BNSTD414

'ACTOR 1000

eutral Compounds u

hexachlorobutadiene

hexachlorocyclopentadiene

isophorone

naphthalene

nitrobenzene

N-nitrosodimethylamine

N-nitrosodiphenylamine

chrysene

acenaphthylene

anthracene

fluorene

phenanthrene

g/1

N D

ND

ND

^

fffi)

Nt)

W<BD

N D

ND

ND

N DND*

ND

*

N D

ND

ND

NDN D

NDN DN DN D

N DNnN D

N D

s-' '

"ND

WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3

QC Report No: 36Sample Number

F0571 Cont.

A. SURROGATE SPIKE RESULTS

COMPOUND

Benzene - d6

l-Chloro-2-Bromopropane

Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyl

Naphthalene-DS

Fraction

VOA

VOA

VOA

ACID

ACID

B/N

B/N

B/N

Cone.(ug/1)

(Surrogates only)Spike

Added (uq/1)%

Recovery

in«^v0

<-)

B . TENTATIVELY IDENTIFIED COMPOUNDS0

1.

2.

3.

4.

5.

6.

7.

8.

9.

10.

1 1 .

12.

13.

14.

15.

16.

17 .

18.

19.

20.

CAS # COMPOUND NAME

CHLOROPHENOL

TRICHLOROMETHOXY-

BENZENE

UNKNOWN

HYDROCARBON

HYDROCARBON

HYDROCARBON

HYDROCARBON

FRACTION

B/N # 2 1 3

B/N #301

B/N #334

B/N #456

B/N #489

B/N #509

B/N # 5 1 8

% Maximum Score Attained

Mass Matching Routine: FIT(specify)

GENERAL FIT

GENERAL FIT

NO GOOD FIT

GENERAL FIT

GENERAL FIT

GENERAL FIT

GENERAL FIT

.

07106036

WW^c^-

~n W,-.v P.ntp 0 Corritn?;. Cnlifornin P0701 p^.-n^ i^i-n '

WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3

QC Report No: 36Sample Number

F0571

A. SURROGATE SPIKE RESULTS

COMPOUND

Benzene - d6

l-Chloro-2-Bromopropane

Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyl

Naphthalene-DS

Fraction

VOA

VGA

VOA

ACID

ACID

B/N

B/N

B/N

C o n e . ( u g / 1 )

54

42

54

50

75

105

91

88

(Surrogates only)Spike

Added ( u q / 1 )

50

50

50

100

103

101

101

101

%Recovery

108

84

108

50

73 ^0

104 ^

90 \0

87 ^

B . TENTATIVELY IDENTIFIED COMPOUNDS0

1.

2.

3.

4.

5.

6.

7.

8.

9.

10.

1 1 .

12.

13.

14.

15 .

16.

17.

18.

19.

20.

CAS # COMPOUND NAME

ACETONE

2-METHYLPROPANAL

BUTANAL

PENTANE

CYCLOHEXANE

1-BUTANOL

3-METHYLHEXANE

2-METHYLHEXANE

4-CHLOROPHENOL

UNKNOWN

',4,5-TRICHLOROPHENOL

4,5-DICHLORO-2-METHOXY

PHENOL

DICHLOROPHENOL

UNKNOWN

UNKNOWN

UNKNOWN

UNKNOWN

CHLORO-METHYL-BENZENE

2-ETHYL-1-HEXANOL

FRACTION

VOA #88

VOA # 1 3 5

VOA # 1 5 8

VOA #184

VOA #193

VOA #208

VOA #337

VOA #346

ACID #92

ACID # 1 9 4

ACID #208

ACID #229

ACID #265

ACID #287

AICD # 3 1 9

ACID #454

B/N #47

B/N # 1 0 6

B/N # 1 2 6

% Maximum Score Attained

Mass Matching Routine: FIT(specify)

965

874

983

935

987

973

985

990

792

NO GOOD FIT

696

935

GENERAL FIT

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT 071060.37

GENERAL FIT

963 0^^646 c^—

' ' • ,11 .10 n rnrritnr r'-ihfnrnn nnpm in n^i-omi

WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

SAMPLE ID F0571 • SAMPLE ID FQ571

LAB ID 21881V18 & 21881V19 LAB ID TRACE #4158

DATE INJECTED 8/6/81 DATE EXTRACTED 7/31/81

STD ID BFB36 VOA157 DATE INJECTED 8/7/81

CONC. FACTOR ----- STD ID TRACE #4156

Volatiles

2V acrolein

3V acrylonitrile

4V benzene

6V carbon tetrachloride

7V chlorobenzene

10V 1,2-dichloroethane

11V 1,1,1-trichloroethane

13V 1,1-dichloroethane

14V 1,1, 2-trichloroethane

15V 1,1,2,2-tetrachloroethane

l6V chloroethane

)imxx»max^)^3^x)^i)^<mxxxxxxxxx19V 2-chloroethylvinyl ether

23V chloroform

29V 1,1-dichloroethylene

30V 1,2-trans-dichloroethylene

32V 1,2-dichloropropane

33V 1,3-dichloropropylene

38V ethylbenzene

44V methylene chloride

45V methyl chloride

46V methyl bromide

47V bromoform

48V dichlorobromomethane

49V tr ichlorofluoromethane

50V dichlorodifluoromethane

51V chlorodibromomethane

85V tetrachloroethylene

86V toluene

87V trichloroethylene

88V vinyl chloride

ug/1

ND

ND

124

ND

*

ND

ND

N D

ND

N D

ND

N D

*

*

ND

ND

N D*

13

ND

ND

ND

ND

ND

ND

ND

N D

27000*

ND

CONC. FACTOR 100

Pesticides

89P aldrin

90P dieldrin

91P chlordane

92P 4 ,4 ' -DDT

93P 4 ,4 ' -DDE

94P 4 , 4 ' - D D D

95P alpha-endosulfan

9oP beta-endosulfan

97P endosulfan sulfate

98P endrin

99P endrin aldehyde

100P heptachlor

101P heptachlor epoxide

102P alpha-BHC

103P beta-BHC

104P gamma-BHC

105P delta-BHC

106P PCB-1242

107P PCB-1254

108P PCB-1221

109P PCB-1232

HOP PCB-1248

HIP PCB-1260

112P PCB-1016

113P toxaphene

* = Less than 10 ug/1

(pesticides less than 5

ND = Not detected

** = Not confirmed by GC

VOA ND = less than 2 ug/1fWi-9

ug/1

N D

ND

ND

NID~

N^^0

ND

Nto

N<P

ND

N D

N D

N D

ND

ND

N D

ND

ND

ND

N D

ND

ND

ND

N D

N D

N D

ug/1)

^ W106038-i

W€5T COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

SAMP

LAB

DATE

DATE

STD •

CONC

Acid

21A

22A

24A

31A

34A

57A

58A

59A

60A

64A

65A

Base/

1B

5B

8B

9B

12B

18B

20B

25B

26B

27B

28B

35B

36B

37B

39B

40B

LE ID F0571

ID 21881A11 & 21881A12

EXTRACTED 8/1/81

INJECTED 8/10/81

ID SENS177 PHEN354

FACTOR 1000 & 20

Compounds

2,4,6-trichlorophenol

p-chloro-m-cresol

2-chlorophenol

2,4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol

2,4-dinitrophenol

4,6-dinitro-o-cresol

pentachlorophenol

phenol

^Neut ra l Compounds

acenaphthene

benzidine

1,2,4-trichlorobenzene

hexachlorobenzene

hexachloroethane

bis(2-chloroethyl)ether

2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1,4-dichlorobenzene

3,3'-dichlorobenzidine

2,4-dinitrotoluene

2,6-dinitrotoluene

1,2-diphenylhydrazine

(as azobenzene)

f luoranthene

4-chlorophenyl phenyl e t h e r N D

ug/1

2400

ND

4000

14000

NO

ND

N D

ND

ND

ND

1200

ND

ND

33

ND

N D

ND

ND*

ND*

ND

NO

ND

NDN D

SAMP

LAB

DATE

DATE

STD •

CONC

Base/

41B

42B

43B

52B

53B

54B

55B56 B

61B

62 B

63 B

66B

67B

68B

69B

70B

71B

72B

73B

74B

75B

76B

77B

78B

79B

80 B

81B

82B

83B

84B

129B

p-dic

LE ID F0571

ID 21881B12

EXTRACTED 7/31/81

INJECTED 8/21/81

ID BENZ401 BNSTD418

FACTOR 1000

''Neutral Compounds u

4-bromophenyl phenyl ether

bis (2-chloroisopropyl) ether

bis (2-chloroethoxy) methane

hexachlorobutadiene

hexachlorocyclopentadiene

isophorone

naphthalene

nitrobenzene

N-nitrosodi methyl a mine

N-nitrosodiphenylamine

N-nitrosodi-n-propylamine

bis (2-ethylhexyl) phthalate

butyl benzyl phthalate

di-n-butyl phthalate

di-n-octyl phthalate

diethyl phthalate

dimethyl phthalate

b e n z o ( a ) anthracene

benzo(a)pyrene

3, 4-benzofluoranthene

benzo (k ) f luoranthene

chrysene

acenaphthylene

anthracene

benzo(gh i )pe ry lene

fluorene

phenanthrene

d ibenzo (a ,h )an th racene

indeno( 1,2,3-cd)pyrene

pyrenen»"(-

2,3,7,8-tetrachlorodibenzo-"—

>xin WW£f^K~

g/1

ND

ND

ND

NEto

ND^

ND^

Nt^

NOD

N D

ND

ND

17•k

*

*

*

ND

ND

ND

NPN D

NDNONDNONnNO

NnN nN D

l06(^

N D

WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3

QC Report No:Sampte Number

F0570

A. SURROGATE S P I K E RESULTS

COMPOUND

Benzene - d6

l-Chloro-2-Bromopropane

Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyl

Naphthalene-DS

Fraction

VOA

VOA

VOA

ACID

ACID

B/N

B/N

B/N

C o n e . ( u g / 1 )

56

49

52

2

2

62

75

70

(Surrogates only)Spike

Added (ug /1)

50

50

50

100

103

101

101

101

%Recovery

112

98

104

2

2 C

61

74 \

69 <

r\f0

3

B . TENTATIVELY IDENTIFIED COMPOUNDS

1.2.

3.

4.

5.

6.

7.

8.

9.

10.

1 1 .

12.

13 .

14.

15 .

16.

17 .

18.

19.

20.

CAS # COMPOUND NAME

TETRAHYDROFURAN

UNKNOWN

FRACTION

VOA # 1 3 1

VOA #421

% Maximum Score Attained

Mass Matching Routine: FIT(specify)

928

NO GOOD FIT

———————————071060^

c^w^u^——

W€5T COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

SAMP

LAB

DATE

STD •

CONC

Volat

2V

3V

4V

6V

7V

10V

11V

13V

14V

15V

l6V

>imxxmxm»)^)^x^xx^iwomxxxxxxxx19V23V

29V

30V

32V

33V38V44V45V46V

47V

48V

49V

50V51V

85V

86V

87V

88V

LE ID F0570

ID 21881V17

INJECTED 8/6/81

ID BFB36 VOA157f A r'TC^D

iles

acrolein

acrylonitrile

benzene

carbon tetrachloride

chlorobenzene

1,2-dichloroethane

1,1,1-trichloroethane

1,1-dichloroethane

1,1, 2-trichloroethane

1,1,2, 2-tetrachloroethane

chloroethane

2-chloroethylvinyl ether

chloroform

1,1-dichloroethylene

1,2-trans-dichloroethylene

1,2-dichloropropane

1,3-dichloropropylene

ethylbenzene

methylene chloride

methyl chloride

methyl bromide

bromoform

dichlorobromo methane

trichlorofluoromethane

dichlorodifluoromethane

chlorodibromomethane

tetrachloroethylene

toluene

trichloroethylene

vinyl chloride

ug/1

NO

N D

NO

ND

ND

N D

ND

N D

N D

N D

ND

N D

ND

ND

ND

ND

ND

ND

13

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

SAMP

LAB

DATE

DATE

STD :

CONC

Pesti

89P

90P

91P

92P

93P94P

95P96P

97P98P

99P

100P

101P

102P

103P

104P

105P

106P

107P

108P

109P

HOP

HIP

112P

113P

* = 1

( P ^ND =-«- •,': ^

LE ID F057D

ID TRACE N157

EXTRACTED 7/31/81

INJECTED 8/7/81

ID TRACE #4156

. FACTOR 100

cides u

aldrin

dieldrin

chlordane

4,4 ' -DDT

4 , 4 ' - D D E

4 , 4 ' - D D D

alpha-endosulfan

beta-endosulfan

endosulfan sulfate

endrin

endrin aldehyde

heptachlor

heptachlor epoxide

alpha-BHC

beta-BHC

gamma-BHC

delta-BHC

PCB-1242

PCB-1254

PCB-1221

PCB-1232

PCB-1248

PCB-1260

PCB-1016

toxaphene

-.ess than 10 ug/1

isticides less than 5 ug/1)

Not detected O'HOeNot confirmed by GCMS ," .

(meseso-

g/iND

ND

ND

ND=>

^'sO

ND

ND^>

NCP

ND

N D

N D

N D

ND

ND

N D

ND

N D

N D

N D

ND

ND

ND

N D

N D

N D

;041

WSfSa^.

SAMP

LAB •

DATE

DATE

STD 1

CONC

Acid

21A

22A

24A

31A

34A

SPA

58A

59A

60A

64A

65A

Base/

1B

5B

8B

9B

12B

18B

20B

25B

26B

27B

28B

35B

36B

37B

39B

40B

H W6ST COAST TECHNICAL

LE ID F0570

ID 21881A10

EXTRACTED 8/1/81

INJECTED 8/10/81

:D SENS177 PHEN354

FACTOR 1000

Compounds u

2,4,6-trichlorophenol

p-chloro-m-cresol

2-chlorophenol

2,4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol

2,4-dinitrophenol

4,6-dinitro-o-cresol

pentachlorophenol

phenol

^Neut ra l Compounds

acenaphthene

benzidine

1,2,4-trichlorobenzene

hexachlorobenzene

hexachloroe thane

bis(2-chloroethyl)ether

2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1,4-dichlorobenzene

3,3'-dichlorobenzidine

2,4-dinitrotoluene

2,6-dinitrotoluene

1,2-diphenylhydrazine

(as azobenzene)

f luoranthene

4-chlorophenyl phenyl ether

5€F

g/1

NO

ND

ND*

N nNDNnNn'N nNnNn

ND

N D

N D

ND

N D

NDND

NDN H*

N H

ND

NH

NnND

ND

•- p

<vice INC.SAMP

LAB

DATE

DATE

STD ID BENZ398 mSTD415

CONC

Base/Neutral Compounds us

41B

42B

43B

52B

53B

54B

55B

56 B

61B

62 B

63B

66B

67B

68B

69B

70B

71B

72B

73B

74B

75B

76B

77B

78B

79B

80B

81B

82B

83B

84B

129B

p-dio

i",, -1., ^ .--i.i,,

INDUSTRIAL CATEGORY

LE ID F0570

ID 21881B11

EXTRACTED 7/31/81

INJECTED 8/13/81

FACTOR 1000

4-bromophenyl phenyl ether

bis(2-chloroisopropyl) ether

bis (2-chloroethoxy) methane

hexachlorobutadiene

hexachlorocyclopentadiene

isophorone

naphthalene

nitrobenzene

N-nitrosodi methyl a mine

N-nitrosodiphenylamine

N-nitrosodi-n-p ropy la mine

bis (2-ethylhexyl) phthalate

butyl benzyl phthalate

di-n-butyl phthalate

di-n-octyl phthalate

diethyl phthalate

dimethyl phthalate

b e n z o ( a ) anthracene

benzo(a )py rene

3,4-benzofluoranthene

benzo(k ) f luo ran thene

chrysene

acenaphthylene

anthracene

benzo(gh i )pe ry lene

fluorene

phenanthrene

d i b e n z o ( a , h ) a n t h r a c e n e

indeno( 1 ,2,3-cd)pyrene

pyrene

2,3,7,8-tetrachlorodiberyy^Og

xin

.,,^^ ,.,,,gai0^&3r-^^

^iN D

N D

ND

ND^

NanND^

NC^

NDo

ND

ND

ND*

N D*

ND*

ND

N D

ND

NDN D

N DN DN D

N HNnN nN nN nN D

042N D

WeST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3

QC Report No: 36Sample Number

F0569

A. SURROGATE S P I K E RESULTS

COMPOUND

Benzene - d6

l-Chloro-2-Bromopropane

Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyl

Naphthalene-DS

Fraction

VOA

VOA

VOA

ACID

ACID

B/N

B/N

B/N

C o n e . ( u g / 1 )

48

45

47

0

2

72

81

74

(Surrogates only)Spike

Added ( u g / 1 )

50

50

50

100

103

101

101

101

/,Recovery

96

90

94

0

2 C\J

71 ^

80 \u

73 c

B . TENTATIVELY IDENTIFIED COMPOUNDS

1.2.

3.

4.

5.

6.

7.

8.

9.

10.

1 1 .

12.

13.

14.

15 .

16.

17.

18.

19.

20.

CAS # COMPOUND NAME

TOLUENE

CHLOROBENZENE

TRICHLOROBENZENE

FRACTION

3/N H3

B/N #68

B/N #209

% Maximum Score Attained

Mass Matching Routine: FIT(specify)

999

991

GENERAL FIT

(m06043

. -»

WlOUim'1^————

WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

SAMPLE ID F0569

LAB ID 21881V12 & 21881V16

DATE INJECTED 8/5/81 & 8/6/81

STD ID BFB35 VOA156 & BFB36 VOA157

CONC. FACTOR ---- & 1/10 D i l u t i o n

Volatiles u

2V acrolein

3V acrylonitrile

4V benzene

6V carbon tetrachloride

7V chlorobenzene

10V 1,2-dichloroethane

11V 1,1,1-trtchloroethane

13V 1,1-dichloroethane

14V 1,1,2-trichloroethane

15V 1,1,2,2-tetrachloroethane

l6V chloroethane

)imxxm^m^)^x^x)^-X(Xixxxxxxxxxxx19V 2-chloroethylvinyl ether

23V chloroform

29V 1,1-dichloroethylene

30V 1,2-trans-dichloroethylene

32V 1,2-dichloropropane

33V 1,3-dichloropropylene

38V ethylbenzene

44V methylene chloride

45V methyl chloride

46V methyl bromide

47V bromoform

48V dichlorobromomethane

49V tr ichlorofluoromethane

50V dichlorodifluoromethane

51V chlorodibromomethane

85V tetrachloroethylene

86V toluene

87V trichloroethylene

88V vinyl chloride

LAB ID TRACE #4155

DATE EXTRACTED 7/31/81

g/1

ND

N D*

ND

392

ND

ND

N D

ND

N D

ND

ND

ND

ND

ND

ND

ND

ND

20

ND

ND

ND

ND

ND

ND

ND

ND

16ND

ND

SAMPLE ID F0569

DATE INJECTED 8/7/81

STD ID TRACE #4156

CONC. FACTOR 100

Pesticides

89P aldrin

90P dieldrin

91P chlordane

92P 4 ,4 ' -DDT

93P 4 ,4 ' -DDE

94P 4 ,4 ' -DDD

95P alpha-endosulfan

96P beta-endosulfan

97P endosulfan sulfate

98P endrin

99P endrin aldehyde

100P heptachlor

101P heptachlor epoxide

102P alpha-BHC

103P beta-BHC

104P gamma-BHC

105P delta-BHC

106P PCB-1242

107P PCB-1254

108P PCB-1221

109P PCB-1232

HOP 'PCB-1248

HIP PCB-1260

112P PCB-1016

113P toxaphene

'"" = Less than 10 ug/1

(pesticides less than 5 ug/1)

ND = Not detected ^i

-;.-* ^ ^Q^ confirmed by GCMS

fyTfT

ug/1

ND

ND

ND

NO^

Nl!^

^

ND^

NO

ND

N D

N D

N D

ND

0.1**

0.3**

ND

0.2**

N D

N D

N D

ND

ND

N D

N D

N D

^106044/'?

s'71 1

) WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

E ID F0569

3 21881A9

EXTRACTED 8/1/81

INJECTED 8/9/81

3 SENS176 PHEN353

FACTOR 1000

Compounds

2,4,6-trichlorophenol

p-chloro-m-cresol

2-chlorophenol

2, A-dichlorophenol

2,A-dimethylphenol

2-nitrophenol

^-nitrophenol

2,^-dinitrophenol

4,6-dinttro-o-cresol

pentachlorophenol

phenol

' /Neutral Compounds

acenaphthene

benzidine

1,2,4-trichlorobenzene

hexachlorobenzene

hexachloroethane

bis (2-chloroethyDether

2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

i 1,4-dichlorobenzene

i 3,3 '-dichlorobenzidine

3 2,4-dinitrotoluene

3 2,6-dinitrotoluene

3 1,2-diphenylhydrazine

(as azobenzene)

3 f luoranthene

B 4-chlorophenyl phenyl

ug/1*

ND

ND

21

NOND

NnN0NnN0*

ND

NO

29

ND

ND

ND

ND30

50

493

ND

NnNO

NOND

e t h e r N D

SAMP

LAB

DATE

DATE

STD •

CONC

Base/

41B

42B

43B

52B

53B

54B

55B

56B61B

62B

63B

66B

67B

68B

69 B

70B

71B

72B

73B

74B

75B

76B

77B

78B

79B

SOB

81B

82B

83B

84B

129B

p-dic

LE ID F0569

ID 21881B10 & 21881B13

EXTRACTED 7/31/81

INJECTED 8/13/81 8/21/81

ID BENZ398 BNSTD415/BENZ401 BNSTD418

FACTOR 1000 & 100

Neutral Compounds u;

^-bromophenyl phenyl ether

bis(2-chloroisopropyl) ether

bis (2-chloroethoxy) methane

hexachlorobutadiene

hexachlorocyclopentadiene

isophorone

naphthalene

nitrobenzene

N-nitrosodi methyl a mine

N-nitrosodiphenylamine

N-nitrosodi-n-p ropy la mine

bis (2-ethylhexyl) phthalate

butyl benzyl phthalate

di-n-butyl phthalate

di-n-octyl phthalate

diethyl phthalate

dimethyl phthalate

benzo(a ) anthracene

benzo(a)pyrene

3,4-benzofluoranthene

benzo (k ) f luo ran thene

chrysene

acenaphthylene

anthracene

benzo(ghi )pery lene

fluorene

phenanthrene

d ibenzo (a ,h )an th racene

indeno(1,2 ,3-cd)pyrene

pyrene

2,3,7,8-tetrachlorodibenzo-

,xin -WIO^S^Q

sZlN D

ND

ND

ND

ND

ND

ND

ND

N D,:*

ND*

N D*

ND*

ND

ND

ND

ND

N D

ND

ND

NO

NO

ND

NnNnN HN D

c:

WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

SAMP

LAB

DATE

STD '

CONC

Volat

2V

3V

4V

6V

7V

10V

11V

13V

14V

15V

16V

)imxxM^Km»)^x^xMi^mxxxxxxxxx19V

23V

29V

30V

32V

33V

38V

44V

45V

46V

47V

48V

49V

50V

51V

85V

86V

87V

88V

LE ID F0568

ID 21881V15

INJECTED 8/6/81

ID BFB36 VOA157V A PTnD

iles

acrolein

acrylonitrile

benzene

carbon tetrachloride

chlorobenzene

1,2-dichloroethane

1,1,1-trichloroethane

1,1-dichloroethane

1,1, 2-trichloroethane

1,1, 2,2-tetrachloroethane

chloroethane

2-chloroethylvinyl ether

chloroform

1,1-dichloroethylene

1,2-trans-dichloroethylene

1,2-dichloropropane

1,3-dichloropropylene

ethylbenzene

methylene chloride

methyl chloride

methyl bromide

bromoform

dichlorobromomethane

trichlorofluoromethane

dichlorodifluoromethane

chlorodibromomethane

tetrachloroethylene

toluene

trichloroethylene

vinyl chloride

ug/1

ND

ND

N D

ND

ND

ND

ND

N D

ND

N D

ND

ND

ND

ND

ND

ND

ND

N D13

ND

ND

ND

ND

ND

ND

ND

N D

ND

N D

ND

SAMP

LAB

DATE

DATE

STD

CONC

Pesti

89P

90P

91P

92P

93P94P95P96P

97P

98P

99P

100P

101P

102P

103P

104P

105P

106P

107P

108P

109P

HOP

HIP

112P

113P

* = ]

( p <

ND =

LE ID

ID

EXTRACTED

INJECTED

ID

. FACTOR

cides

aldrin

dieldrin

chlordane

4,4 ' -DDT

4,4 ' -DDE

4 , 4 ' - D D D

alpha-endosulfan

beta-endosulfan

endosulfan

endrin

endrin aldehyde

heptachlor

heptachlor

alpha-BHC

beta-BHC

gamma-BHC

delta-BHC

PCB-1242

PCB-1254

PCB-1221

PCB-1232

PCB-1248

PCB-1260

PCB-1016

toxaphene

Less than 10

'sticides less

Not detected

Not confirme

F0568

TRACE #4154

7/31/81

8/7/81

TRACE #4151

100

sulfate

epoxide

ug/1

than 5 ug/1)

d by GCMS07106<• /

ug/1

ND

ND

ND

^

^

NiP

ND^

N&>

ND

N D

N D

N D

ND

ND

ND

ND

N D

N D

N D

NOND

ND

ND

ND

N D

347

W€5T COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

SAMP

LAB

DATE

DATE

STD

CONC

Acid

21A

22A

24A

31A

34A

57A

58A

59A

60A

64A

65A

Base,

1B

5B

8B

9B

12B

18B

20B

25B

26B

27B

28B

35B

36B

37B

39B

40B

LE ID F0568

ID 21881A8

EXTRACTED 8/1/81

INJECTED 8/9/81

ID SESN176 PHEN353

FACTOR 1000

Compounds u,

2, 4 , 6-trichlorophenol

p-chloro-m-cresol

2-chlorophenol

2,4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol

2,4-dinitrophenol

4,6-dinitro-o-cresol

pentachlorophenol

phenol

/Neutral Compounds

acenaphthene

benzidine

1,2, 4-trichlorobenzene

hexachlorobenzene

hexachloroethane

bis(2-chloroethyl)ether

2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1,4-dichlorobenzene

3,3'-dichlorobenzidine

2,4-dinitrotoluene

2,6-dinitrotoluene

1,2-diphenylhydrazine

(as azobenzene)

f luoranthene

4-chlorophenyl phenyl ether

g/1

*

ND

ND26

ND

ND

ND

ND

NDND

N D

ND

ND

N D

ND

ND

ND

N D

ND

N D

ND

ND

ND

ND

NnND

ND

SAMP

LAB

DATE

DATE

STD

CONC

Base/

41B

42B

43B

52B

53B

54B

55B

56B

61B

62B

63B

66 B

67B68B

69 B

70B

71B

72B

73B

74B

75B

76B

77B

78B

79B

80B

81B

82B

83B

84B

129B

p-dic

LE ID F0568

ID 21881B9

EXTRACTED 7/31/81

INJECTED 8/13/81

ID BENZ398 BNSTD415

FACTOR 1000

Neutral Compounds u j

4-bromophenyl phenyl ether

bis(2-chloroisopropyl) ether

bis (2-chloroethoxy) methane

hexachlorobutadiene

hexachlorocyclopentadiene

isophorone

naphthalene

nitrobenzene

N-nitrosodi methyl a mine

N-nitrosodiphenylamine

N-nitrosodi-n-propylamine

bis (2-ethylhexyl) phthalate

butyl benzyl phthalate

di-n-butyl phthalate

di-n-octyl phthalate

diethyl phthalate

dimethyl phthalate

benzo (a ) anthracene

benzo(a)pyrene

3,4-benzofluoranthene

benzo(k) f luoran thene

chrysene

acenaphthylene

anthracene

benzo(gh i )pe ry l ene

fluorene

phenanthrene

d ibenzo (a ,h ) an th racene

indeno( 1,2,3-cd)pyrene

pyrene ND ^

2,3,7,8-tetrachlorodibenzoy *

>xin

0'ywwy

g/1

N D

ND

ND

^0NDinND^

ND""0

ND^

ND

ND

ND

18

N D*

ND

N D

N D

ND

ND

NDN D

ND

ND

N D

N D

N D

Nn

Nn

N n

ND^ „

WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3

QC Report No: 36Sample Number

F0567

A. SURROGATE SPIKE RESULTS

COMPOUND

Benzene - d6

l-Chloro-2-Bromopropane

Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyl

Naphthalene-DS

Fraction

VOA

VGA

VOA

ACID

ACID

B/N

B/N

B/N

C o n e . ( u q / 1 )

44

43

46

40

2

60

68

60

(Surrogates only)Spike

Added ( u g / 1 )

50

50

50

100

103

101

101

101

%Recovery

88

86

92

40

2 r59 L

67 \

59 '

B . TENTATIVELY IDENTIFIED COMPOUNDS

1.

2.

3.

4.

5.

6.

7.

8.

9.

10.

1 1 .

12 .

13.

14.

15.

16.

17.

18.

1 9 .

20.

CAS # COMPOUND NAME

ACETONE

TETRAHYDROFURAN

DICHLOROPHENOL

CHLOROPHENOL

2,4,5^TRICHLOROPHENOL

DICHLOROPHENOL

UNKNOWN

UNKNOWN

2-ETHYL-1-HEXANOL

TRICHLOROMETHOXYBENZENi

UNKNOWN

UNKNOWN

FRACTION

VOA #86

VOA # 1 3 0

ACID #146

ACID # 1 9 6

ACID #207

ACID #264

ACID #492

ACID # 5 1 5

B/N #142

; B/N #296

B/N #324

B/N #330

% Maximum Score Attained

Mass Matching Routine: FIT(specify)

835

993

GENERAL FIT

GENERAL FIT

966

GENERAL FIT

NO GOOD FIT

NO'^GOOD FIT

942

GENERAL FIT

NO'tSOOD FIT

NO GOOD FIT

—————————————071060

C————————W10WSQ——

Alf .» t Ja '4 .

SAMP

LAB

DATE

STD •

CONC

Volat

2V

3V

4V

6V

7V

10V

11V

13V

14V

15V

16V

)imxxmxxmK»)^x^x)4xi)tMixxxxxxxxxxx19V

23V

29V

30V

32V

33V

38V

44V

45V

46V

47V

48V

49V

50V

51V

85V

86V

87V

88V

H WEST COAST TECHNICAL

LE ID F0567

ID 21881V10

INJECTED 8/5/81

ID BFB35 VOA156

. r A^. 1 UK

lies

acrolein

acrylonitrile

benzene

carbon tetrachloride

chlorobenzene

1,2-dichloroethane

1,1,1-trichloroethane

1,1-dichloroethane

1,1,2-trichloroethane

1,1,2,2-tetrachloroethane

chloroethane

2-chloroethylvinyl ether

chloroform

1,1-dichloroethylene

1,2-trans-dichloroethylene

1,2-dichloropropane

1,3-dichloropropylene

ethylbenzene

methylene chloride

methyl chloride

methyl bromide

bromoform

dichlorobromomethane

trichlorofluoromethane

dichlorodifluoromethane

chlorodibromomethane

tetrachloroethylene

toluene

trichloroethylene

vinyl chloride

.56RVK

ug/1

ND

ND

N D

ND

ND

ND

N D

N D

ND

N D

ND

N D

ND

ND

ND

ND

ND

N D

20ND

ND

ND

N D

ND

ND

ND

ND

ND

ND

ND

:6 INC.

SAMP

LAB

DATE

DATE

STD :

CONC

Pesti

89P

90P

91P

92P

93P

94P

95P96P

97P98P

99P

100P

101P

102P

103P

104P

105P

106P

107P

108P

109P

HOP

HIP

112P

113P

* = ]

( P <ND --;.- * ^

INDUSTRIAL CATEGORY

LE ID F0567

ID TRACE #41

EXTRACTED 7/31/81

INJECTED 8/6/81

ID TRACE #41

. FACTOR 100

cides

aldrin

dieldrin

chlordane

4,4 ' -DDT

4,4 ' -DDE

4,4 ' -DDD

alpha-endosulfan

beta-endosulfan

endosulfan sulfate

endrin

endrin aldehyde

heptachlor

heptachlor epoxide

alpha-BHC

beta-BHC

gamma-BHC

delta-BHC

PCB-1242

PCB-1254

PCB-1221

PCB-1232

PCB-1248

PCB-1260

PCB-1016

toxaphene

l.ess than 10 ug/1

'sticides less than 5 ug/1

Not detected

Not confirmed by GCMS

46

43

ug/1

ND

. ND

ND

N D

ND°——————tf\

NDn

ND-

NtP

ND^

ND

N D

N D

ND

ND

N D

ND

N D

N D

N D

ND

N D

ND

N D

N D

N D

)

07106050

/-''/iy^wse^

213/921-983117605 Fabrics Way. Suite D Cerntos. California 90701

WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

SAMP

LAB '

DATE

DATE

STD I

CONC

Acid

21A

22A

2^A

31A

34A

57A

58A

59A60A

6AA

65A

Base/

1B

5B

8B

9B

12B

l8B

20B

25B

26B

27B

28B

35B

36B

37B

39B

Z^OB

LE ID F0567

CD 21881

EXTRACTED 8/1/8

INJECTED 8/9/8

.D SENS176

FACTOR 1000

Compounds

2,4,6-trichlorophenol

p-chloro-m-cresol

2-chlorophenol

2,4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol

2,4-dinitrophenol

4,6-dinitro-o-cresol

pentachlorophenol

phenol

'Neutral Compounds

acenaphthene

benzidine

1,2,4-trichlorobenzene

hexachlorobenzene

hexachloroethane

bis(2-chloroethyl)ether

2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1, Zt-dichlorobenzene

3,3'-dichlorobenzidine

2,4-dinitrotoluene

2,6-dinitrotoluene

1,2-diphenylhydrazine

(as azobenzene)

f luoranthene

4-chlorophenyl phenyl

A7

1

1

PHEN353

ug/1

7S

ND

154

153

ND

ND

ND

N0

NnNnNn

ND

ND*

ND

ND

ND

ND

ND

N D

ND

ND

ND

ND

NnND

e t h e r N D

SAMP]

LAB 1

DATE

DATE

STD I

CONC

Base/

41B

42B

43B

52B

53B

54B

55B

56B

61B

62B

63B

66B67B68B

69B

70B

71B

72B

73B

74B

75B

76B

77B

78B

79B

80B

81B

82B

83B

84B

129B

p-dio

.E ID F0567

.D 21881B8

EXTRACTED 7/31/81

INJECTED 8/13/81

D BENZ398 !£NSTD415

FACTOR 1000

Neutral Compounds ui

4-bromophenyl phenyl ether

bis(2-chloroisopropyl) ether

bis (2-chloroethoxy) methane

hexachlorobutadiene

hexachlorocyclopentadiene

isophorone

naphthalene

nitrobenzene

N-nitrosodimethylamine

N-nitrosodiphenylamine

N-nitrosodi-n-propylamine

bis (2-ethylhexyl) phthalate

butyl benzyl phthalate

di-n-butyl phthalate

di-n-octyl phthalate

diethyl phthalate

dimethyl phthalate

benzo(a ) anthracene

benzo(a)pyrene

3,4-benzofluoranthene

benzo(k) f luoran thene

chrysene

acenaphthylene

anthracene

benzo(ghi )pery lene

fluorene

phenanthrene

d ibenzo(a ,h )an th racene

indeno( 1,2,3-cd)pyrene

pyrene

2,3,7,8-tetrachlorodibenzo-

xin

1ND

ND

ND

NDC^

^LHND^o

ND-^-

N D 0

0ND

ND

ND

29

ND

ND

ND

ND

N D

ND

ND

ND

N D

ND

N D

N D

ND

Nn

NnNnNnN D

L06051N D

WEST COAST TECHNICAL S6RVIC6 INC. INDUSTRIAL CATEGORY

SAMP

LAB

DATE

STD

CONC

Volat

2V

3V

4V

6V

7V

10V

11V

13V

14V

15V

16V

>imxxm^Km»)tm^xxsm<Mxxxxxxxxxx19V

23V

29V

30V

32V

33V

38V

44V

45V

46V

47V

48V

49V

50V

51V

85V

86V

87V

88V

LE ID R0566

ID 21881V9

INJECTED 8/5/81

ID BFB35 VOA156 DATE INJECTED 8/6/81

. FACTOR -------

:iles ui

acrolein

acrylonitrile

benzene

carbon tetrachloride

chlorobenzene

1,2-dichloroethane

1,1,1-trichloroethane

1,1-dichloroethane

1,1, 2-trlchloroethane

1,1,2,2-tetrachloroethane

chloroethane

2-chloroethylvinyl ether

chloroform

1,1-dlchloroethylene

1,2-trans-dichloroethylene

1,2-dichloropropane

1,3-dichloropropylene

ethylbenzene

methylene chloride

methyl chloride

methyl bromide

bromoform

dichlorobromo methane

tr ichlorofluoromethane

die hlorodifluorome thane

chlorodibromomethane

tetrachloroethylene

toluene

trichloroethylene

vinyl chloride

17605 Fabrica Way, Suite D

LAB ID TRACE #4145

DATE EXTRACTED 7/31/81

STD ID TRACE #4143

1ND

N D

N D

N D

N D

N D

N D

N D

N D

N D

ND

ND

ND

ND

ND

N D

ND

N D

18

ND

N D

N D

N D

ND

ND

N D

N D

NP

N D

N D

Cen

SAMPLE ID F0566

CONC. FACTOR 100

Pesticides

89P aldrin

90P dieldrin

91P chlordane

92P 4 ,4 ' -DDT

93P 4 , 4 ' - D D E

94P 4 , 4 ' - D D D

95P alpha-endosulfan

96P beta-endosulfan

97P endosulfan sulfate

98P endrin

99P endrin aldehyde

100P heptachlor

101P heptachlor epoxide

102P alpha-BHC

103P beta-BHC

104P gamma-BHC

105P delta-BHC

106P PCB-1242

107P PCB-1254

108P PCB-1221

109P PCB-1232

HOP PCB-1248

HIP PCB-1260

112P PCB-1016

113P toxaphene

* = Less than 10 ug/1

(pesticides less than 5 ug/1)

ND = Not detected

-"-* = Not confirmed by GCMS

0'

(mo^entos. C a l i f o r n i a 90701 213/921-9831

Ug/1

N D

. ND

ND

ND

^——<©•^W-

N9

NV

N D

N D

ND

ND

ND

ND

ND

N D

N D

N D

N D

ND

ND

N D

ND

N D

10^053

^

EST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

i F0566

21881A6

^ACTED 8/1/81

CTED 8/9/81

SENS176 PHEN353

TOR 1000

rounds u'

6-trichlorophenol

iloro-m-cresol

^lorophenol

-dichlorophenol

-dimethylphenol

i.trophenol

itrophenol

-dinitrophenol

-dinitro-o-cresol

.tachlorophenol

"nol

:tral Compounds

^naphthene

^zidine

2,4-trichlorobenzene

xachlorobenzene

<achloroethane

;(2-chloroethyl)ether

:hloronapthalene

2-dichlorobenzene

3-dichlorobenzene

4-dichlorobenzene

3'-dichlorobenzidine

^-dinitrotoluene

6-dlnitrotoluene

2-diphenylhydrazine

is azobenzene)

•Joranthene

-chlorophenyl phenyl ether

g/1

NO

ND

NO

NO

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

N D

ND

ND

ND

ND

NnND

ND

SAMP

LAB

DATE

DATE

STD

CONC

Base,

41B

42B

^3B

52B

53B54B

55 B

56B61B62B

63B

66B67B68B69B

70B

71B

72B

73B

7AB

75B

76B

77B

78B

79BSOB

81B

82B

83B

84B

129B

p-di<

LE ID F0566

ID 21881B7

EXTRACTED 7/31/81

INJECTED 8/13/81

ID BENZ397 BNSTD414

FACTOR 1000

/Neutral Compounds u

4-bromophenyl phenyl ether

bis(2-chloroisopropyl) ether

bis (2-chloroethoxy) methane

hexachlorobutadiene

hexachlorocyclopentadiene

isophorone

naphthalene

nitrobenzene

N-nitrosodi methyl a mine

N-nitrosodiphenylamine

N-nitrosodi-n-propylamine

bis (2-ethylhexyl) phthalate

butyl benzyl phthalate

di-n-butyl phthalate

di-n-octyl phthalate

diethyl phthalate

dimethyl phthalate

benzo(a ) anthracene

benzo(a)pyrene

3,4-benzofluoranthene

benzo(k) f luoranthene

chrysene

acenaphthylene

anthracene

benzo(ghi )pery lene

fluorene

phenanthrene

dibenzo(a ,h)an thracene

indenod, 2,3-cd)pyrene

pyrene

2,3,7,8-tetrachlorodibenzo-

?xin (TW^f^S^

g/1

NDND

ND

ND

ND

ND

ND

ND

ND

ND

ND

12

ND*

ND*

ND

ND

ND

ND

N D

ND

ND

ND

N D

ND

Nn

N DNnN D

i^

iber

only)%

:overy

98

38

52

1

1 ^

i7 ^0

.5 \0

-4 Z

.1. W6ST COAST TECHNICAL

SAMPLE ID F0565

LAB ID 21881V4

DATE INJECTED 8/5/81

STD ID BFB35 VOA156

CONC. FACTOR - ----

Volatiles

2V acrolein

3V acrylonitrile

4V benzene

6V carbon tetrachloride

7V chlorobenzene

10V 1,2-dichloroethane

11V 1,1,1-trichloroethane

13V 1,1-dichloroethane

14V 1,1,2-trichloroethane

15V 1,1,2,2-tetrachloroethane

l6V chloroethane

)imXXM^m^»mWXXiXl^(fXimXXXXXXXX

19V 2-chloroethylvlnyl ether

23V chloroform

29V 1,1-dichloroethylene

30V 1,2-trans-dichloroethylene

32V 1,2-dichloropropane

33V 1,3-dichloropropylene

38V ethylbenzene

44V methylene chloride

45V methyl chloride

46V methyl bromide

47V bromoform

48V dichlorobromomethane

49V tr ichlorofluoromethane

50V dichlorodifluoromethane

51V chlorodibromomethane

85V tetrachloroethylene

86V toluene

87V trichloroethylene

88V vinyl chloride

SERVICE

LAB ID TRACE #4152

DATE EXTRACTED 7/31/81

DATE INJECTED 8/7/81

ug/1

ND

ND

N D

N D .

ND

ND

ND

N D

N D

N D

ND

ND

ND

ND

ND

ND

N D

N D

2D

N D

ND

N D

ND

ND

ND

ND

N D

N D

N D

N D

INC INnU^TRlAl L AT^GQRY

SAMPLE ID F0565

STD ID TRACE #4151

CONC. FACTOR 50

Pesticides u

89P aldrin

90P dieldrin

91P chlordane

92P 4 ,4 ' -DDT

93P 4.4 '-DDE

94P 4 ,4 ' -DDD

95P alpha-endosulfan

96P beta-endosulfan

97P endosulfan sulfate

98P endrin

99P endrin aldehyde

100P heptachlor

101P heptachlor epoxide

102P alpha-BHC

103P beta-BHC

104P gamma-BHC

105P delta-BHC

106P PCB-1242

107P PCB-1254

108P PCB-1221

109P PCB-1232

HOP PCB-1248

HIP PCB-1260

112P PCB-1016

113P toxaphene

* = Less than 10 ug/1

(pesticides less than 5 ug/1)

ND = Not detected

-.'•-* = Not confirmed by GCM&ingQgg

g/1

N D

ND

ND

ND

1^Ww-N^>

N?

N D

N D

N D

ND

ND

ND

ND

ND

N D

N D

ND

ND

ND

ND

ND

ND

17605 Fabnca Way, Suite D Cerntos, California 90701 213/921-9831

W€ST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

SAMP

LAB

DATE

DATE

STD

CONC

Acid

21A

22A

2^A

31A

34A

SPA

58A

59A

60A64A65A

Base,

1B

5B

8B

9B

12B

18B

20B

25B

26B

27B

28B

35B

36B

37B

39B

40B

LE ID F0565

ID 21881A5

EXTRACTED 8/1/81

INJECTED 8/9/81

ID SENS176 PHEN353

FACTOR 1000

Compounds u;

2, , 6-trichlorophenol

p-chloro-m-cresol

2-chlorophenol

2,4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol

2,^-dinitrophenol

4,6-dinitro-o-cresol

pentachlorophenol

phenol

/Neutral Compounds

acenaphthene

benzidine

1,2,/r-trichlorobenzene

hexachlorobenzene

hexachloroethane

bis(2-chloroethyl)ether

2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1, /t-dichlorobenzene

3,3'-dichlorobenzidine

2, Zt-dinitrotoluene

2,6-dinitrotoluene

1,2-diphenylhydrazine

(as azobenzene)

f luoranthene

4-chlorophenyl phenyl ether

g/1

ND

ND

NONDNDNDND

NnNDNnNn

ND

ND

ND

ND

ND

ND

ND

ND

N DNDND

NnND

NDND

ND

SAMP

LAB

DATE

DATE

STD :

CONC

Base/Neutral Compounds U j

41B

Z»2B

^3B

52B

53B

54B

55B

56B61B62B

63B

66B67B

68B

69B70B

71B

72B

73B

74B

75B

76B

77B

78B

79B

80 B

81B

82B

83B

84B

129B

p-dic

LE ID F0565

ID 21881B6

EXTRACTED 7/31/81

INJECTED 8/13/81

[D BENZ397 BNSTD414

FACTOR 1000

^-bromophenyl phenyl ether

bis(2-chloroisopropyl) ether

bis (2-chloroethoxy) methane

hexachlorobutadiene

hexachlorocyclopentadiene

isophorone

naphthalene

nitrobenzene

N-nitrosodimethylamine

N-nitrosodiphenylamine

N-nitrosodi-n-propylamine

bis (2-ethylhexyl) phthalate

butyl benzyl phthalate

di-n-butyl phthalate

di-n-octyl phthalate

diethyl phthalate

dimethyl phthalate

benzo(a) anthracene

benzo(a)pyrene

3,4-benzofluoranthene

benzo(k)f luoranthene

chrysene

acenaphthylene

anthracene

benzo(ghi)perylene

fluorene

phenanthrene

dibenzo(a ,h)an thracene

indeno( 1,2,3-cd)pyrene

pyrene

2,3,7,8-tetrachlorodibenzo-07j0^)xln nffltf>yfifift

^1N D

ND

ND

ND

N D ^——•<£)ND^n

ND^-

ND 0

ND

ND

ND

10

ND*

ND*

N D

ND

ND

ND

N D

ND

N D

ND

N D

Nn

N nN nNnN D

106057ND

h^.Y ;-';*•'

SAMP

LAB

DATE

STD •

CONC

Volat

2V

3V

4V

6V

7V

10V

11V

13V

14V

15V

16V

)imxxm^Km»)^jWX)^Mixxxxxxxxxxx19V

23V

29V

30V

32V

33V

38V

44V

45V

46V

47V

48V

49V

50V

51V

85V

86V

87V

88V

^ WEST COAST TECHNICAL

LE ID F0564

ID 21881V3

INJECTED 8/5/81

ID BFB35 VOA156T- A f~"rr\'D

lies

acrolein

acrylonitrile

benzene

carbon tetrachloride

chlorobenzene

1,2-dichloroethane

1,1,1-trichloroethane

1,1-dichloroethane

1,1, 2-trichloroethane

1,1,2,2-tetrachloroethane

chloroethane

2-chloroethylvinyl ether

chloroform

1,1-dichloroethylene

1,2-trans-dichloroethylene

1,2-dichloropropane

1,3-dichloropropylene

ethylbenzene

methylene chloride

methyl chloride

methyl bromide

bromoform

dichlorobromomethane

trie hlorofluoro methane

dichlorodifluoromethane

chlorodibromomethane

tetrachloroethylene

toluene

trichloroethylene

vinvl chloride

.S6RVIC

ug/1

ND

ND

N D

ND

N D

N D

ND

N D

ND

N D

ND

ND*

ND

ND

N D

N D

N D

20

ND

ND

ND

ND

ND

ND

ND

10

N D

N D

N D

:(= INC.

SAMP

LAB

DATE

DATE

STD

CONC

Pesti

89P

90P

91P

92P

93P

94P

95P

96P

97P

98P

99P

100P

101P

102P

103P

104P

105P

106P

107P

108P

109P

HOP

HIP

112P

113P

* = 1

( P ^ND =* -A- ^

INDUSTRIA

LE ID

ID

EXTRACTED

INJECTED

ID

. FACTOR

cides

aldrin

dieldrin

chlordane

4 ,4 ' -DDT

4,4 ' -DDE

4 , 4 ' - D D D

alpha-endosulfan

beta-endosulfan

endosulfan

endrin

endrin aldehyde

heptachlor

heptachlor

alpha-BHC

beta-BHC

gamma-BHC

delta-BHC

PCB-1242

PCB-1254

PCB-1221

PCB-1232

PCB-1248

PCB-1260

PCB-1016

toxaphene

l.ess than 10

isticides less

Not detected

Not confirme

L. i-ATt=(30RY

F0564

TRACE #4144

7/31/81

8/6/81

TRACE N143

50

2.5**

sulfate

epoxide

0.7**

ug/1

than 5 ug/1)

0710<d by GCMS

n^v^fw-ev-a

ug/1

0:1**

N D

1.6**

N^YO

^

o.y*NP

^0.1**

1.0**

N D

ND

0.6**

1.5**

1.8**

ND

N D

ND

ND

ND

N D

N D

N D

5059

17605 Fabnca Way. Suite D Cerntos, California 90701 213/921-9831

WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

SAMP

LAB •

DATE

DATE

STD 1

CONC

Acid

21A

22A

24A

31A

34A

SPA

58A

59A60A

64A

65A

Base/

1B

5B

8B

9B

12B

18B

20B

25B

26B

27B

28B

35B

36B

37B

39B

LOB

LE ID F0564ID 21881A2

EXTRACTED 8/1/81

INJECTED 8/9/81

ID SENS176 PHEN353

FACTOR 1000

Compounds u

2,4,6-trichlorophenol

p-chloro-m-cresol

2-chlorophenol

2,4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol

2,4-dinitrophenol

4,6-dinitro-o-cresol

pentachlorophenol

phenol

Neutral Compounds

acenaphthene

benzidine

1,2,4-trichlorobenzene

hexachlorobenzene

hexachloroethane

bis(2-chloroethyl)ether

2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1,4-dichlorobenzene

3,3'-dichlorobenzidine

2,4-dinitrotoluene

2,6-dinitrotoluene

1,2-diphenylhydrazine

(as azobenzene)

fluoranthene

4-chlorophenyl phenyl ether

g/1*

ND

ND

14

ND

ND

N D

ND

ND

ND*

ND

ND

N D

ND

ND

ND

ND

ND

N D

ND

ND

ND

ND

NDND

ND

SAMP

LAB •

DATE

DATE

STD ]

CONC

Base/

41B

42B

43 B

52B

53B

54B

55B

•56B61B62B

63B

66 B67B68B

69B

70B

71B

72B

73B

74B

75B

76B

77B

78B

79B80B

81B

82B

83B

84B

129B

p-dio

LE ID F0564

ID 21881B3

EXTRACTED 7/31/81

INJECTED 8/13/81

^D BENZ397 BNSTD414

FACTOR 1000

''Neutral Compounds u,

4-bromophenyl phenyl ether

bis(2-chloroisopropyl) ether

bis (2-chloroethoxy) methane

hexachlorobutadiene

hexachlorocyclopentadiene

isophorone

naphthalene

nitrobenzene

N-nitrosodimethylamine

N-nitrosodiphenylamine

N-nitrosodi-n-propylamine

bis (2-ethylhexyl) phthalate

butyl benzyl phthalate

di-n-butyl phthalate

di-n-octyl phthalate

.diethyl phthalate

dimethyl phthalate

benzo(a) anthracene

benzo(a)pyrene

3,4-benzofluoranthene

benzo(k) f luoran thene

chrysene

acenaphthylene

anthracene

benzo(ghi)perylene

fluorene

phenanthrene

dibenzo(a ,h)anthracene

indeno( l ,2 ,3-cd)pyrene

pyrene

2,3,7,8-tetrachlorodibenz(9-^H

xin 0' U*5WQ

gZlN D

ND

ND

ND

^ND^

ND--

ND0

N D

ND

ND

11

ND*

ND*

N D

ND

ND

ND

N D

N DN D

N D

ND

ND

N D

N D

N D

N D

96060'ND

WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY

SAMF

LAB

DATE

STD

CONC

Volal

2V

3V

4V

6V

7V

10V

11V

13V

14V

15V

16V

)™xxmxax^)^3»xx^x<mxxxxxxxxx19V23V

29V

30V

32V

33V

38V

44V

45V

46V

47V

48V

49V

50V

51V

85V

86V

87V

88V

'LE ID F0536

ID 21881V2

: INJECTED 8/5/81

ID BFB35 VOA156

:. FACTOR -----

tiles i

acrolein

acrylonitrile

benzene

carbon tetrachloride

chlorobenzene

1,2-dichloroethane

1,1, l-trichloroethane

1,1-dichloroethane

1,1,2-trichloroethane

1,1,2,2-tetrachloroethane

chloroethane

2-chloroethylvinyl ether

chloroform

1,1-dichloroethylene

1,2-trans-dichloroethylene

1,2-dichloropropane

1,3-dichloropropylene

ethylbenzene

methylene chloride

methyl chloride

methyl bromide

bromoform

dichlorobromomethane

trichlorofluoro me thane

dichlorodifluorome thane

chlorodibromo methane

tetrachloroethylene

toluene

trichloroethylene

vinyl chloride

17605 Fabrica Way. Suite

Llg/1

ND

N D

N D

ND

N D

N D

ND

N D

N D

N D

ND

ND

13

N D

ND

N D

N D

N D

19

ND

N D

N D

N D

ND

ND

N D*

N D

N D

ND

D Cen

SAMF

LAB

DATE

DATI

STD

CONC

Pesti

89P

90P

91P

92P

93P

94P

95P

96P

97P98P

99P100P

101P

102P

103P

104P

105P

106P

107P

108P

109PHOP

HIP

112P

113P

-"-

(P 1

ND =^- ^

ntos. Ca l i f

'LE ID F053

ID TRAC

; EXTRACTED 7/31

; INJECTED 8/6/

ID TRAC

;. FACTOR 50

Icides

aldrin

dieldrin

chlordane

4,4 ' -DDT

4,4 ' -DDE

4,4 ' -DDD

alpha-endosulfan

beta-endosulfan

endosulfan sulfate

endrin

endrin aldehyde

heptachlor

heptachlor epoxide

alpha-BHC

beta-BHC

gamma-BHC

delta-BHC

PCB-1242

PCB-1254

PCB-1221

PCB-1232

PCB-1248

PCB-1260

PCB-1016

toxaphene

Less than 10 ug/1

esticides less than 5

Not detected

Not confirmed by GC

ornia 90701 213/921-9831

[6

;E N141

/81

'81

;E N140

ug/1

N D

. ND

ND

ND

<W

^00

^

^(ffp

N D

N D

N D

ND

ND

ND

ND

N D

N D

N D

N D

N D

ND

N D

N D

ND

ug/1)

^ 07106062

n "i nvc. fnV *A<J»<.io/JL

vss/e^t

SAMP

LAB :

DATE

DATE

STD 1

CONC

Acid

21A

22A

24A

31A

34A

SPA

58A

59A60A

64A

65A

Base/

1B

5B

8B

9B

12B

18B

20B

25B

26B

27B

28B

35B

36B

37B

39B

40B

D WGSTCOASi ,^. 1CAL

LE ID F0536

[D 21881A13

EXTRACTED7/31/81

INJECTED 8/17/81

•'D SENS178 PHEN355

FACTOR 1000

Compounds u

2,4,6-trichlorophenol

p-chloro-m-cresol

2-chlorophenol

2,4-dichlorophenol

2,4-dimethylphenol

2-nitrophenol

4-nitrophenol *

2,4-dinitrophenol

4,6-dinitro-o-cresol

pentachlorophenol

phenol

'Neutral Compounds

acenaphthene

benzidine

1,2,4-trlchlorobenzene

hexachlorobenzene

hexachloroethane

bis(2-chloroethyl)ether

2-chloronapthalene

1,2-dichlorobenzene

1,3-dichlorobenzene

1,4-dichlorobenzene

3,3'-dichlorobenzidine

2,4-dinitrotoluene

2,6-dinitrotoluene

1,2-diphenylhydrazine

(as azobenzene)

f luoranthene

4-chlorophenyl phenyl ether

S6RVK

g/lNO

ND

ND

ND

ND

ND

ND

NO*

117

ND

ND

ND

ND

ND

NDND

N D

N D

N D

ND

ND

ND

NnND

ND

C€ INC.

SAMP]

LAB 1

DATE

DATE

STD I

CONC

Base/

41B

42B

43B

52B

53B

54B

55B

56 B

61B

62B63B

66 B

67B

68B

69B

70B

71B

72B

73B

74B

75B

76B

77B

78B

79B

80B

81B

82B

83 B

84B

129B

p-dio

INDUSTRIAL CATEGORY

-E ID FOMfi

•D ?1RR1R?

EXTRACTED 7/.'n/fii

INJECTED f i /n /Ri

D RFN7.W RNSTn^U

FACTOR mnn

Neutral Compounds u^

4-bromophenyl phenyl ether

bis(2-chloroisopropyl) ether

bis (2-chloroethoxy) methane

hexachlorobutadiene

hexachlorocyclopentadiene

isophorone

naphthalene

nitrobenzene

N-nitrosodi methyl a mine

N-nitrosodiphenylamine

N-nitrosodi-n-propylamine

bis (2-ethylhexyl) phthalate

butyl benzyl phthalate

di-n-butyl phthalate

di-n-octyl phthalate

diethyl phthalate

dimethyl phthalate

benzo(a) anthracene

benzo(a)pyrene

3,4-benzofluoranthene

benzo(k) f luoran thene

chrysene

acenaphthylene

anthracene

benzo(ghi)perylene

fluorene

phenanthrene

d ibenzo(a ,h )an th racene

indeno( 1,2,3-cd)pyrene

pyrene

2,3,7,8-tetrachlorodiben0»y^()<xln n^Tmnrw

g/lND

ND

ND

ND

N^T- e-NtbN&-

NP

NP

ND

ND

ND

ND*

ND*

ND

ND

ND

NDN D

mND

N D

N D

N n

NnNnN nN D

K063.ND

W6ST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3

QC Report No: 28Sample Number

LAB BLANK & BFB

A. SURROGATE SPIKE RESULTS

COMPOUND

Benzene - d6

l-Chloro-2-Bromopropane

Toluene - d8

2-Fluorophenol

Phenol - d5

Nitrobenzene - d5

2-Fluorobiphenyl

Naphthalene-DS

Fraction

VOA

VOA

VOA

ACID

ACID

B/N

B/N

B/N

C o n e . ( u g / 1 )

52

52

55

96

62

58

68

2

(Surrogates only)Spike

Added (ug /1 )

50

50

50

142

10298

100

102

%Recovery

104

104

110

68

———^-^59 .r

68 ^

2 ^

B . TENTATIVELY IDENTIFIED COMPOUNDS 0

1.2.

3.

4.

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CAS # COMPOUND NAME

UNKNOWN

UNKNOWN

UNKNOWN

FRACTION

B/N #221

B/N #317

B/N #330

% Maximum Score Attained

Mass Matching Routine: FIT(specify)

NO GOOD FIT

NO GOOD FIT

NO GOOD FIT

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07106064

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