Railroad Company · 2020. 10. 14. · Railroad Company ^""~ December 1, 1993 Mr. Christopher P....

Railroad Company""~ December 1, 1993

Mr. Christopher P. Thomas, OSCOffice of SuperfundUnited States Environmental Protection AgencyRegion m (3HW33)841 Chestnut BuildingPhiladelphia, Pennsylvania 19107-4431

RE: Potomac Yard Site, Bi-Weekly Progress Report No. 16 - EPA Docket No. HI-92-61-DC

Dear Mr. Thomas:

Enclosed please find the Bi-Weekly Progress Report No. 16 for the above-referenced project.Richmond, Fredericksburg, and Potomac Railroad Company is submitting this report as requiredin Section 8.7 of the Administrative Order by Consent (AOC).

This progress report covers a two-week period beginning on Saturday, November 6, 1993, andending on Friday, November 19,1993. If you have any questions concerning this report or anyaspect of the project, please me your earliest convenience.

v, I certify under penalty of law that this document and all attachments wereprepared under my direction or supervision in accordance with a system designedto assure that qualified personnel property gather and evaluate the informationsubmitted. Based on my inquiry of the person or persons who manage the systemor those persons directly responsible for gathering the information, theinformation submitted is, to the best of my knowledge and belief, true, accurate,and complete. I am aware that there are significant penalties for submitting falseinformation, including the possibility of fine and imprisonment for knowingviolations.

xn

Scott A. SlagleyProject Coordinator

Enclosure

cc: C. Martin, Esq.C. Flippo, ET1E. Wingert (3HW41)

Main Street Centre • 23rd Floor • 600 East Main Street • Richmond, Virginia 23219(804) 225-1600 • Telecopier (804) 225-1620 fl ft I 07600

PROGRESS REPORT NO. 16

RICHMOND, FREDERICKSBURGAND POTOMAC RAILROAD COMPANY

THE POTOMAC YARD SITE

EPA DOCKET NO. 111-92-61 -DC

Reporting Period:

November 6 through November 19, 1993

ENVIRONMENTAL TECHNOLOGYOF NORTH AMERICA, INC.Interstate Business Park3705 Saunders AvenueRichmond, Virginia 23227(804) 358-5400

AR I 07601

PROGRESS REPORT NO. 16

RICHMOND, FREDERICKSBURG AND POTOMAC RAILROAD COMPANY

THE POTOMAC YARD SITE

EPA DOCKET NO. IH-92-61-DC

Reporting Period: November 6, 1993, through November 19, 1993

WORK COMPLETED

Extent of Contamination Study (ECS1 Work Plan

EH received laboratory results for soil samples collected from the ponds during pond removal.The laboratory results confirmed the results of the TPH screening, that concentrations of TPHin the soil beneath the ponds is less than 100 ppm. These results will be included in the Extentof Contamination Study. A copy of these results is included as an attachment

On Friday, November 12, 1993, ETI gauged all of the monitoring wells at Potomac Yard andevaluated their condition. This information was used to determine if the wells to fill in data gapsin area A-l are properly located. This information was also used to determine whether the wellsin the Yard Tails and Potomac Greens areas are in locations that will be useful in performingthe assessment as presented in the addendum to the ECS Work Plan.

Meetings

No meetings took place during the reporting period.

Free Product Recovery

RF&P continues to review ETT*s plan for more aggressive free product recovery in the CentralOperations Area.

gite Maintenance

Hand bailing of well MW-25 resumed during the reporting period, as this well is outside theCentral Operations Area and will not be addressed by the free product recovery test plan underreview by RF&P. Hand bailing of Central Operation Area wells remains on hold pending adecision on the proposed recovery test plan and on disposal of product which contains lowconcentrations (< 15 ppm) of PCB's.

ARI07602

DATA ANTICIPATED AND ACTIVITIES SCHEDULED

Extent of Contamination Study fECSl Work Plan

The ECS Work Plan will be submitted to EPA, upon approval by RF&P and upon approval ofthe proposed modification to the existing Consent Order.

The Free Product Recovery system proposed by ETI should be implemented by early December,pending approval of RF&P.

Pond Removal

Until the seeding of the ponds and other areas has taken hold, ETI will continue to monitordischarge and erosion and sediment control measures in place at the ponds (ie. check dams, siltfencing, etc) to determine if additional action is necessary.

A letter will be sent to Virginia Department of Environmental Quality during the week ofNovember 29, 1993 confirming the closure of the oil/water separator ponds.

Site Maintenance

On November 23, 1993, ETI will perform several tasks relative to site maintenance includingrepair of the silt fence surrounding the soil stockpile, repair of the safety fence around the oilcylinder, and organizing drummed material at the site.

PROBLEMS ENCOUNTERED OR ANTICIPATED

The effects of erosion and a sheen were noticed at the area once occupied by the middle pond.The sheen is believed to be the result of bacteria and not from petroleum.

ETI continues to be unable to find wells MW-23, MW-40, and MW-41, which have beencovered over with gravel due to downsizing traffic. Well lids are also being broken by vehicletraffic.

PREVENTIVE OR MTTTGATIVE ACTIONS

ETI visited the site on Thursday, November 18, 1993 to investigate the status of the middlepond. To confirm the nature of the sheen, a water and soil sampled were collected and analyzedfor TPH. Since seeding has not yet taken hold, steps will be taken to reduce the erosion bycreating a preferential flow path with gravel.

ETI is exploring ways to adapt the well covers to withstand traffic and ensure that they can belocated.

ARI07603

SCHEDULE

ETI will implement work on pond erosion controls on November 23, 1993.

ETI will present recommended well modifications to RF&P during the week of November 29,1993.

MODIFICATIONS MADE IN ACCORDANCE WITH CONSENT ORDER SECTION XVD

None in this reporting period. Approval of the proposed modification to the existing ConsentOrder is expected by the end of November.

fc\WP\RFATOOTOMAC\ntORFTl6.993

AJM0760lf

ANALYTICAL RESULTS

ECS SAMPLES COLLECTED DURING POND REMOVALACTIVITIES

ARI07605

ID CLIENT SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET

PIBLKFFName: INDUSTRIAL & ENVIRONMENTA

Lab Code: IEA Case No.: 1528-039 SDG No.: 10143

Matrix: (soil/water) WATER Lab Sample ID; PIBLKFF

Sample vt/vol: ________ (g/mL) Lab File ID: P6O20002.D

% Moisture; ^____ decanted: fY/N)__ Date Received: ______

Extraction: (SepF/Cont/Sonc) ___ Date Extracted:_______Concentrated Extract Volume: _____(uL) Date Analyzed: 10/20/93

Injection Volume: 1.0(uL) Dilution Factor: 1.0

PC Cleanup: (Y/N) N pH: ___ Sulfur Cleanup: (Y/N) N

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

319-84-6———————alpha-BHC____ '319 -85-7 ———————beta-BHC^1 Q»r P fi"""ft T --m"-»-——-M--~T——-n- J 1 * jV~rPtJ ^

58-89-9—-———*—gamma-BHC (Lindane)76-44-8——————Heptachlor_____'309-00-2——————Aldrin1024-57-3—————Heptachlor epoxide959-98-8——-—-—Endosulfan I_____"60-57-1—————— Dieldrin72-55-9————————4 , 4 ' -DDE——— "72-20-8—————---Endrin72-54-8————————4,4'-DDD/Endo II1031-07-8—————Endosulfan sulfa"Ee"50-29-3——————~4 , 4 ' -DOT72-43-5———•———Methoxychlor__53494-70-5————Endrin ketone7421-36-3—————Endrin aldehyde"57-74-9——————Chlordane (technical)8001-35-2—————Toxaphene12674-11-2—————Aroclor-101611104-28-2—————Aroclor-1221"11141-16-5—————Aroclor-1232"53469-21-9—————Aroclor-1242"12672-29-6—————Aroclor-1248"11097-69-1———-Aroclor-1254"11096-82-5—————ATOClor-1260"

0.0500.0500.0500.0500.0500.0500.0500.0500.100.100.100.100.100.100.500.100.1$0.101.00.500.500.500.500.501.01.0

UUUUUUUUUUUUUUUUUUUUUUUUUU

FORM I PEST 3/90


PBQC93Lab Name: INDUSTRIAL & ENVIRONMENTA

Lab Code: IEA Case No.: 1528-039 SDG No.: 10143Matrix: (soil/water) SOIL Lab Sample ID: PBQC98

Sample wt/vol: 30.0 (g/mL) G Lab File ID: P5O15007.D

% Moisture: 0 decanted: (Y/N) N Date Received: / /

Extraction: (SepF/Cont/Sonc) SONC Date Extracted:10/11/93Concentrated Extract Volume: 10000(uL) Date Analyzed: 10/15/93

Injection Volume: l.O(uL) Dilution Factor: 1.0GPC Cleanup: (Y/N) N pH: ___ Sulfur Cleanup: (Y/N) N

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

319-84-6——————alpha-BHC319-85-7——————beta-BHCj;319-86-8——————delta-BHC53-89-9———————gamma-BHC (Lindane)76-44-8———————Heptachlor309-00-2——————Aldrin ____1024-57-3—*-———Heptactilor epoxlde959-98-8——————Endosulfan I_____"60-57-1———————Dieldrin_________72-55-9———————4,4 ' -DDE_________72-20-8———————Endrin33213-65-9—————Endosultan II72-54-8———————4,4 ' -ODD1031-07-8—————Endosulfan suit at a50-29-3————————4,4 ' -DDT__________~72-43-5——————Methoxychior53494-70-5————Endrin ketone7421-36-3—————Endrin aldehyHa"57-74-9-——————Chlordane (technical)8001-35-2—————Toxaphene12674-11-2—————Aroclor-lTJI3~11104-28-2—————Aroclor-1221"11141-16-5—————Aroclor-1232"53469-21-9—————Aroclor-1242"12672-29-6—————Aroclor-1248"11097-69-1—————Aroclor-1254"11096-82-5—————Aroclor-1260"

7.411

0.918.611161217131560

, 596232601202921801603080808030160160

FORM I PEST

JJ

flRl07607

ID CLIENT SAMPLE HO,PESTICIDE ORGANICS ANALYSIS DATA SHEET

MIDDLEPONDb Name: INDUSTRIAL & ENVIRONMENT A

Lalb Code: IEA Case No.: 1528-039 f' SDG No. : 10143

Hatrix: (soil/water) SOIL Lab Sample ID: 931014503

Sample vt/vol: 30.1 (g/mL) G Lab File ID: P6O21007.D% Moisture: 35 decanted: (V/N) N Date Received: 10/07/93

Extraction: (SepF/Cont/Sonc) SONG Date Extracted:10/11/93Concentrated Extract Volume: 10000(uL) Date Analyzed: 10/21/93


GPC Cleanup: (Y/N) N pH: ___ Sulfur Cleanup: (Y/N) NCONCENTRATION UNITS:

CAS NO. COMPOUND (ug/L or Ug/Kg) UG/KG Q

319-85-7 ————319-86-8 ————58-89-9 —————76-44-8 —————309-00-2 ————1024-57-3 ———959-98-8 ————60-57-1 —————72-55-9 —————72-20-8 —————1031-07-8 ———50-29-3 —————72-43-5 —————53494-70-5 ——7421-36-3 ———57-74-9 —————8001-35-2 ———12674-11-2 ——11104-28-2 ——11141-16-5 ——53469-21-9 ——12672-29-6 ——11097-69-1 ——11096-82-5 ——

• i ,—— alpha-BHC . . . r—— beta-BHC—— delta-BHC—— gamma-BHC ( Lindane )—— Heptachlor .—— Aldrin—— Heptachlor epoxide—— Endosulf an I .—— Dieldrin— -4 ,4 '-DDE—— Endrln—— Endosultan sultate—— 4, 4 '-DOT—— Methoxychlor—— Endrln ketone—— Endrln aldehyde—— Chlordane (technical)—— Toxaphene—— Arocior-i6i£—— Aroclor-1221—— Arocior-1232—— Aroclor-1242—— Arocior-1248 .—— Arocior-1254—— Aroclor-1260 . .

121212121212121224242424

-' - -241202424120240120120120120120240240

UUUUUUUUUUUUUUUUUUUUUUUUU

FORM I PEST 3/90

fiR!07608

ID CLIENT SAMPLE NOPESTICIDE ORGANICS ANALYSIS DATA SHEET

SOUTHPONDLab Name: INDUSTRIAL & ENVIRONMENTA


Matrix: (soil/water) SOIL Lab Sample ID: 931014301Sample vt/vol: 30.0 (g/mL) G Lab File ID: P6O20012.D

% Moisture: 21 decanted: (Y/N) N Date Received: 10/06/93Extraction: (SepF/Cont/Sonc) SONG Date Extracted:10/11/93

Concentrated Extract Volume: 10000(uL) Date Analyzed: 10/21/93Injection Volume: 1.0(uL) Dilution Factor: 1.0

"PC Cleanup: (Y/N) N pH: ___ Sulfur Cleanup: (Y/N) NCONCENTRATION UNITS:

CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

319-85-7 -----319-86-8 -----58-89-9 —— ——76-44-8 —— ——309-00-2 —— —1024-57-3 ———959-98-8 — ——60-57-1 —— ——72-55-9 —————72-20-8 —— ——72-54-8 —— ——1031-07-8 ———50-29-3 ------72-43-5—— ——53494-70-5 ——7421-36-3 ———57-74-9 —————8001-35-2 ———12674*11-2 ——11104-28-2 ——11141-16-5 ——53469-21-9 ——12672-29-6 ——11097-69-1 ——11096-82-5 ——

—— alpha-BHC—— beta-BHC—— delta-BHC—— aamma-BHC tLlndane)—— Heptacnior—— Aldrin—— Heptacnior epoxida—— Endosulfan I—— Dieldrin—— 4, 4 * -DDE-- — Endrin—— 4,4f-DDD/EndO II—— Endosuiran sulfate—— 4,4'-DDT—— Methoxychlor—— Endrln Xetone—— Endrln aldehyde—— cniordane( technical)—— Toxaphene—— Arocior-ioie—— Arocior-1221— — Aroclor-1232—— ATOClOr-1242—— ATOClor-1243—— Arocior-1254—— Arocior-1260

10101010101010102020202020201002020-100200100100100100100200

\ 200• *N

uuuuuuuuuuuuuuuuuuuuuuuuuu

FORM I PEST 3/90

ID '., ;' -r -. CLIENT SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET

NORTHPONDCOMT,ab Name: INDUSTRIAL & ENVIRONMENTA

Code: IEA Case No;: 1528-039 *$' SDG No.: 10143

Matrix: (soil/water) SOIL Lab Sample ID: 931023708

Sample wt/vol: 60.1 (g/mL) G Lab File ID: P5O25006.D* Moisture: 21 decanted: (Y/N) N Date Received: 10/11/93

Extraction: (SepF/Cont/Sonc) SONG Date Extracted:10/11/93Concentrated Extract Volume: 10000(uL) Date Analyzed: 10/25/93


GPC Cleanup: (Y/N) N pH: ___ Sulfur Cleanup: (Y/N) NCONCENTRATION UNITS:

GAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

319-85-7 -----319-86-8 ————58-89-9 ------76-44-8 —————309-00-2 ————1024*57-3 ———959-98-8 ————60-57-1 —————72-55-9 —————72-20-8 —————33213-65-9 ——72-54-8 —————1031-07-8 ———50-29-3 —————72-43-5 —————53494-70-5 ——7421-36-3 ———57-74-9 — - ———8001-35-2 ———12674-11-2 ——11104-28-2 ——11141-16-5 ——53469-21-9 ——12672-29-6 ——11097-69-1 ——11096-82-5 ——

—— alpha-BHC '• •-. r—— beta-BHC—— delta-BHC—— gamma-BHC (Llndane)—— Heptachlor—— Aldrin—— Heptacnior epoxide—— EndosulCan I—— Dleiorin—— 4, 4 '-DDE— -Endrln—— Endosuitan n—— 4i4'-DDD—— Endosulfan sultate—— 4, 4 '-DOT—— Metnoxycnior—— Endrln Ketone .—— Endrln aldehyde—— cniordane (technical)• —— Toxaphene—— Aroclor-lbl6—— Aroclor-1221- — Aroclor-1232—— Arocior-1242—— Arocior-1248—— Arocior-1254—— Arocior-1260

'-

5.05.05.05.05.05.05.05.010101010101010

• 50ia10501005050505050100; K 100

uu. uuuuutJuuuuuuuu. uuuuuuuuuuu

FORM I PEST 3/90

ARI076IO

1C CLIENT SAMPLE NOSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SOUTHPONDMSD

Lab Code: IEA Case No.: 1528-039 Method: SW-846 SDG No.: 10143

Matrix: (soil/water) SOIL Lab Sample ID: 931014301MSDSample wt/vol: 30.1 (g/mL) G Lab File ID: 1013606.D

Level: (low/med) LOW Date Received: 10/06/93

% Moisture: 21 decanted: (Y/N) N Date Extracted:10/11/93

Concentrated Extract Volume: 1000(uL) Date Analyzed: 10/13/93

Injection Volume: 2.0(uL) Dilution Factor: 1.0GPC Cleanup: (Y/N) N pH:

CONCENTRATION UNITS:GAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

100-02-7 ——132-64-9 ——121-14-2 ——84-66-2 ———7005-72-3—

100-01-6 ——534-52-1 ——

101—55—3 —— •AW* •* i«* *#118-74-1 ——87-86-5 ———85-01-8 ———120-12-7 ——84-74-2 ———206-44-0 ——129-00-0 ——85-68-7 ———91-94-1 ———56-55-3 ———218-01-9 ——117-81-7 ——117-84-0 ——205-99-2 ——

, 207-08-9 ——

193-39-5 ——53— 70— 3™ —191—24—2 ——100-51-6 ——65-85-0 ———

——— 2 , 4 -Dinitrophenol——— 4-Nitrophenol——— Dibenzofuran——— 2 , 4-Dlnltrotoluene——— Diethylphthalate——— 4-chiorophenyl-phenyiether——— Fluorene——— 4-Nitroaniline——— 4 9 6-Dinitro-2-raethylphenoJ.——— N-Nitrosodlphenyiamine (l)——— 4-Bromophenyl-phenylether——— Hexachlorobenzene——— Pentachlorophenol——— pnenanthrene——— Anthracene——— Di-n-butylphthalate——— Fluoranthene——— pyrene——— Butyibenzylphthalate——— 3,3'-Dichlorobenzidine— , —— eenzo (a) anthracene——— Chrysene——— &is(2~&thylhexyl}phthalate——— Di-n-octylphthalate——— Benzo(b) t luoranthene——— Benzo(Jc) nuoranthene——— Benzo (a) pyrene——— indenod, 2 , 3-cd) pyrene——— Dibenz (a, h) anthracene——— Benzo(g,h, ijperylene——— Benzyl Alcohol——— Benzole Acid

2000310042017004204204202000200042042042030004204202104201600420830420420420420420

K 420420420

* * 4204208302000

U

U

UUUUUUUU

UUJU

UUUUUUUUUUUUUU

(1) - Cannot be separated from Diphenylamine

FORM I SV-2 3/90

f l R I 0 7 6 l l

IB CLIENT SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SOUTHPONDMSDLab Name: INDUSTRIAL & EKVIRONHENTA

Code: IEA Case No.: 1528-039 Method: SW-846 SDG No.: 10143

Matrix: (soil/water) SOIL Lab Sample ID: 931014301MSD

Sample wt/vol: 30.1 (g/mL) G Lab File ID: 1013606.DLevel: (low/med) LOW Date Received: 10/06/93

% Moisture: 21 decanted: (Y/N) N Date Extracted:10/11/93Concentrated Extract Volume: 1000(uL) Date Analyzed: 10/13/93

Injection Volume: 2*0(uL) Dilution Factor: 1.0GPC Cleanup: (Y/N) N pH:

CONCENTRATION UNITS:GAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

111-44-4 ———95-57-8 ————541-73-1 ———106-46-7 ———95-50-1 ————95-48-7 ————108-60-1- --106-44-5 ———621-64-7 ———67-72-1 ————98-95-3 ————78-59-1 ————88-75-5 ————105-67-9 ———111-91-1 ———

120-82-1 ———91-20-3 ————106-47-8 ———87-68-3 ————59-50-7 ————91-57-6 ————77-47-4 ————

95-95-4 ————91-58-7 ————88-74-4 ————131-11-3 ———208-96-8 ———606-20-2 ———99-09-2 ————83-32-9 ————

——— Phenol——— bis ( 2 -Chloroethy 1 ) ether—— -2-Chlorophenoi——— 1,3-Dichlorobenzene—— »1, 4-Dlchlorobenzene—— 1,2-Dichiorobenzene——— 2 -Metnyipnenoi—— -2 , 2 ' -oxybis (l-Chloropropane)— . — 4-Methylphenol——— N-Nltroso-dl-n-prbpylamine—— Hexachloroe thane—— Nitrobenzene——— Isojphorone——— 2-Nitrophenol——— 2 * 4-Dlmethylphenol——— bis (2-Chioroethoxy) methane _——— 2 , 4-Dichlorophenol——— 1,2 , 4-Trichlorobenzene .——— Naphthalene—— 4-Chloroaniline—— Hexachlorobutadiene- —— 4-Chloro-3-methylphenol——— 2-Hethylnaphthalene—— Hexachlorocyclopentadiene __—— 2 , 4 , 6-Tr ichlorophenol——— 2 , 4 , 5-Trichlorophenol——— 2 -Chloronaphthalene—— 2-Nitroaniline—— Dlmethylphthaiate——— Acenaphthylene——— 2 , 6-Dinitrotoluene——— 3-Nitroaniline——— Acenaphthene

2700420290042018004204204204201800420420420420420420Jt 1/V42U18004208304202700420420420420420200042042042020001700

U

uUUUU

UUUUUUU

UUU

UUUUUUUUUU

FORM I SV-1 3/90

1C CLIENT SAMPLE NO,SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ________

SOUTHPONDMSLab Name: INDUSTRIAL & ENVIRONMENTA

Lab Code: IEA Case No* : 1528-039 Method: SW-846 SDG No.: 10143-

Matrix: (soil/water) SOIL Lab Sample ID: 9310I4301MSSample wt/vol: 30.0 (g/mL) G Lab File ID: 1013605.D

Level: (low/med) LOW -— Date Received: 10/06/93



Injection Volume: 2.0{uL) Dilution Factor: 1.0

GPC Cleanup: (Y/N) N pH:


51-28-5———————2,4-DinitrophenolT.OO-02-7——————4-Nitrophenol___"132-64-9———————Dibenzofuran121-14-2——————2,4-Dinitrotoluene84-66-2——~———Diethylphthalate7005-72-3—————4-Chlorophenyl-phenylether86-73-7———————Fluorene_____100*01-6——————4-Nitroanlline534-52-1——————4,6-Dinitro-2-metnyipnenoi_86-30-6———————N-Nitrosodiphenylamine (1)"101-55-3—————-4-Bromophenyl-phenylether^J118-74-1——-_————Hexachlorobenzene _____87-86-5———————Pentachlorophenol________85-01-S———————Phenanthrene__________._120-12-7——————Anthracene34-74-2———————Di-n-butylphthalate206-44-0——————Fluoranthene______"129-00-0——————Pyrene85-68-7———————Butylbenzylphthalate91-94-1———————3,3'-Dichlorobenzidine56-55-3———————Benzo(a) anthracene218-01-9——————Chrysene1-17-81-7——————bis (2-Ethylhexyl) phthalate117-84-0——————Di=n-octylphthalate_____~205-99-2——————Benzo (b) fluoranthena_____207-08-9———----Benzo(k)fluoranthen&_____50-32-8———————Benzo (a) pyrene_________193-39-5——————Indeno (1,2,3-cd) pyrene53-70-3———————Dibenz (a,h) anthracene____191-24-2——————Benzo(g,h, I) perylene_____100-51-6——————Benzyl Alcohol__________65-85-0——————-Benzoic Acid

20003100420180042042042020002000420420420310042042046042017004208404204204204204204204204204204208402000

U

UUUUUUUU

U

UUUUUUUUUUUUUU

(1) - Cannot be separated from DiphenylamineFORM I SV-2 3/90

ARI076I3

IB CLIENT SAMPLE NOSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET


Lab Code: IEA Case No*: 1528-039 Method: SW-846 SDG No.: 10143

Matrix: (soil/water) SOIL Lab Sample ID: 931014301MSSample wt/vol: 30.0 (g/mL) G Lab File ID: 1013605. D


% Moisture: 21 decanted: (Y/N) N Date Extracted: 10/11/93

Concentrated Extract Volume: 1000 (uL) Date Analyzed: 10/13/93



111-44-4 ———— -aR..R*7_O_ __ _

541-73-1 ———— -106-46-7 ———— -95-50-1 ————— -95-48-7 ————— -108-60-1 —————.*. w -« t w

621-64-7 —————67-72-1 —————98-95-3 —————78-59-1 —————88-75-5 —————105-67-9 —————111-91-1 —————

120-82-1 —————91-20-3 ——————106-47-8 —————87-68-3 ——————59-50-7 ——————91-57-6 ——————77-47-4————-

95-95-4 ——————

0 fi_*7.rf _4 __.. _.._

131-11-3 ——— '• ———208-96-8 —————606-20-2 —————99-09-2 ——————83-32-9 — — — ——

- — Phenol- — bis (2-Ciiloroethyl) ether• — 2 -Chlorophenol- — i/ 3-Dicniorobenzene• — 1,4-Dicniorobenzene• — 1,2-Dlchlorobenzene• — 2 -Metny ipnenol- — 2 , 2 ' -oxybis (l-Chloropropane)• — 4-Methylphenol• — N-Nitroso-di-n-propyiamine• — Hexactiloroethane• — Nitrobenzene• — isophorone— 2 -Nitrophenol• — 2 . 4-Dimethylphenol• — DIS (2-Chloroethoxy) methane _— 2 , 4 -Dichlorophenol

- — i , 2 , 4~xricnioro&enzene— Naptitnaiene— 4-Chloroaniline— Hexachlorobutadiene— 4-Chloro-3-methylphenol— z-MetnyJLnapntnalene— Hexacftlorocyclopentadiene— 2,4,6-Trichlorophenol— 2 , 4 1 5-Trichlorophenol— 2-Chloronaphthalene~2-Nitroaniline— Dlmethylphthalate— Acenaphthylene— 2 , 6-Dinitrotoluene— 3-Nitroaniline— Acenaptithene

2700420300042018004204204204201800420420420420420420420'

. 18004208404202800420420420420420200042042042016001800

U

U

UUUU

UUUUUUU

UUU

UUUUUUUUUU

L FORM I SV-1 3/90

ARI076U

1C CLIENT SAMPLE NO,SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _____

SVB463Lab Name: INDUSTRIAL & ENVIRONMENTA


Matrix: (soil/water) SOIL Lab Sample ID: SVB463

Sample wt/vol: 30.0 (g/mL) G Lab File ID: 1015F02.D

Level: (low/med) LOW Date Received: / /






51-28-5———————2,4-Dinitrophenol100-02-7——————4-Nitrophenol___~132-64-9——————Dibenzofuran121-14-2——————2,4-Dinitrotoluene84-66-2———————Diethylphthalate7005-72-3—————4 -Chlorophenyl-pheny letner86-73-7———————Fluorene________________100-01-6——————4-Nitroaniline534-52-1——————4,6-Dinitro-2-methylpftenol86-30-6———————N-Nitrosodiphenylamina (l)_101-55-3——————4-Bromophenyl-phenylether__118-74-1——————Hexachlorobenzene________87-86-5———————Pentachlorophenol________85-01-8———————Phenanthrene120-12-7——————Anthracene84-74-2——————Di-n-butylpnthaiate206-44-0——————Fluor an thene______"129-00-0——————Pyrene85-68-7———————Butylbenzylphthalate91-94-1———————3,3' -Dichlorobenzidine56-55-3———————Benzo (a) anthracene218-01-9——————Chrysene117-81-7—————bis (2-Ethylhexyl) phthalate117-84-0——————Di-n-octylphthalate_______205-99-2——————Benzo (b) fluor an thene______207-08-9——————Benzo (k) fluor an thene_____50-32-8———————Benzo (a) pyrene__________193-39-5——————Indeno (1,2,3-cd) pyrene53-70-3———————Dibenz(a,h)anthracene_____191-24-2——————Benzo (g,h, i) perylene______100-51-6——————Benzyl Alcohol____________65-85-0———————Benzoic Acid

16001600330330330330330160016003303303301600330330330330H3303306603303303303303303303303303303306601600

UUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUU


FORM I SV-2 3/90

A R I 0 7 6 I 5

1IB CLIENT SAMPLE NO.

SEMIVOLATILE ORGANICS ANALYSIS DATA £riEET

SVB463Lab Name: INDUSTRIAL & ENVIRONHENTA


Matrix: (soil/water) SOIL Lab Sample ID: SVB463

Sample wt/vol: 30.0 (g/mL) G Lab File ID: 1015F02.D



Concentrated Extract Volume: 1000(uL) Date Analyzed: 10/15/93Injection Volume: 2.0(uL) Dilution Factor: 1.0



111-44-4 ———

541-73-1 ———106-46-7 ———95-50-1 ————95-48-7 ————108-60-1 ———106-44-5 ———621-64-7 ———

98-95-3 ————78-59-1 ————88-75-5 ————105-67-9 ———111-91-1- ——

120-82-1 ———91-20-3 ————106-47-8 ———87-68-3 ————59-50-7 ————O 1 »R*7_£_____

95-95-4 ————91-58-7 ————88-74-4 ————131-11-3 ———208-96-8 ———606-20-2 ———99-09-2 ————83-32-9 ————

——— Phenol—— bis (2-cnioroethyl) ether—— 2-chlorophenol— — 1,3-DicnioroDehzene—— 1, 4-Dichlorobenzene——— l, 2-Dichiorobenzene—— -2-Metnyipnenoi——— 2 , 2 f -oxybis (l-Chloropropane)—— -4 -Methylphenol—— N-NItroso-dl-n-prbpylamine—— Kexachloroethane—— Nitrobenzene—— Isophorone——— 2 -Nitrophenoi——— 2 , 4-Dlmethylphenol——— bis (2-Chloroethoxy) methane—— 2 , 4-Dichlorophenol—— 1,2 , 4-Trlchloro£>enzene——— Naphthalene—— 4-Chloroaniline—— Hexacniorofcutaaiene——— 4-chloro-3-methylphenol——— 2-Methylnaphthalene—— Hexacnlorocyclopentaclierie __

—— 2 , 4 , 5-Tricniorophenol—— 2-Chloronaphthalene—— 2-Nitroaniline——— Dimethylphthalate—— Acenapntnyiene——— 2 , 6-Dinitrotoluene——— 3-Nitroaniline——— Acenaphthene

330330330330330330330330330330330330330330330330330330330660330660330330330330330

1600330330'330800330

UuUuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu

FORM I SV-1 3/90

ARI076I6

1CSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SBLK92Lab Name: INDUSTRIAL & ENVIRONMENTA


Matrix: (soil/water) SOIL Lab Sample ID: SBLK92

Sample wt/vol: 30.0 (g/mL) G Lab File ID: 1011H02.D


% Moisture: 0 decanted: (Y/N) N Date Extracted:10/11/93Concentrated Extract Volume: 1000(uL) Date Analyzed: 10/11/93



51-28-5———————2,4-Dinitrophenol100-02-7——————4-Nitrophenol___~132-64-9——————Dibenzofuran121-14-2——————2,4-Dinitrotoluene84-66-2———————Diethylphthalate7005-72-3—————4-Chlorophenyl-phenylettier86-73-7———————Fluorene________________100-01-6——————4-Nitroaniline534-52-1——————4,6-Dinitro-2-metnyiphenoi86-30-6——————N-Nitrosodiphenylamine (1)_101-55-3——————4-Bromophenyl-phenylether__118-74-1——————Hexachlorobenzene________87-86-5———————Pentachlorophenol_________85-01-8———————Phenanthrene____________120-12-7——————Anthracene84-74-2———————Di-n-butylphthalate206-44-0——————Fluoranthene________129-00-0——————Pyrene_____i^_^r_^_^_85-68-7———————Butylbenzylphthalate91-94-1———————3,3'-Dichlorobenzidine56-55-3———————Benzo (a) anthracene___'218-01-9——————Chrysene117-81-7——————bis (2-Ethyihexylj pntnalate117-84-0——————Di-n-octylphthalate______205-99-2——————Benzo (b)fluoranthene______207-08-9——————Benzo(k)fluoranthene______50-32-8———————Benzo(a)pyrene193-39-5——————Indeno(1 f 2, 3-cdJ pyrene53-70-3———————Dibenz (a,h) anthracene191-24-2——————Benzo(g,h, i)perylene__100-51-6——————Benzyl Alcohol_______65-85-0———————Benzoic Acid

16001600330330330330330

16001600330330330

160033033084330^3303306603303303303303303303303303303306601600

UUUUUUUUUUUUUUUJUUUUUUUUUUUUUUUU


FORM I SV-2 3/90

IB CLIENT SAMPLE NOrSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SBLK92Lab Name: INDUSTRIAL & ENVIRONMENTA

Code: IEA Case No.: 1528-039 Method: SW-846 SDG No.: 10143

Matrix: (soil/water) SOIL Lab Sample ID: SBLK92Sample wt/vol: 30.0 (g/mL) G Lab File ID: 1011H02.DLevel: (low/med) LOW Date Received: / /



Injection Volume: 2.0{uL) Dilution Factor: 1*0GPC Cleanup: (Y/N) N pH:

CAS NO. COMPOUND

108-95-2111-44-49S>— &/— o —541-73-1106-46-795-50-1-95-48-7-108-60-1106-44-5621-64-7£*7»'7r>— 1 _o / — /*— A—98-95-3-78-59-1-88-75-5-105-67-9111-91-1120-83-2120-82-191-20-3-106-47-887-68-3-59-50-7-91-57-6-77-47—4-

95-95-4-91-58-7-

131-11-3208-96-8606-20-299-09-2-83-32-9-

—————— Phenol—————— bis(2-Chloroethyl)ether———— — 2-Chlorophenol—————— 1 , 3-DicnioroDenzene- ————— 1 , 4 -Dichlorobenzene—————— 1, 2-Dicnlorobenzene—————— 2-Metnylpnenol—————— 2 , 2 '-oxybis (1-Chloropropane)—— - —— 4-Methylphenol- ————— N-Nltroso-dl-n-prbpylamine—————— Hexachloroethane—————— Nitrobenzene————— -Isopnorone————— -2-Nitrophenol—————— 2 , 4-Dlmethylphenol—————— bis (2-Chloroetnoxy) methane—————— 2 , 4-Dichlorophenol—————— l , 2 , 4-Trichlorobenzene—————— Naphthalene————— -4-Chloroaniline—————— Hexactilorobutadiene——— . —— 4-Chloro-3-methylphenol—————— 2-Hetnylnapntnalene—————— Hexacniorocyclopentadiene _ ————— 2 , 4 , 6-Trichlorophenol—————— 2 , 4 5-Trichlorophenol————— -2-Chloronaphthalene—————— 2-Nitroaniline—————— Dimethylphthalate—————— Acenapnthylene—————— 2 , 6-Dinitrotoluene—————— 3-Nitroaniline—————— Acenaphthene

33033033033033033033033033033033033033033033033033033033066033066O33033033033033016003303303301600330

UUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUU

FORM I SV-1 3/90

ARI076I8

1C CLIENT SAMPLE NO,SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SOUTHPONDLab Name: INDUSTRIAL & ENVIRONMENTA



Sample vt/vol: 30.1 (g/mL) G Lab File ID: 1013604.D







51-28-5———————2,4-Dinitrophenol100-02-7——————4-Nitrophenol___"132-64-9——————Dibenzofuran121-14-2——————2,4-Dinitrotoluene84-66-2———————Diethylphthalate7005-72-3—————4-Chlorophenyl-phenyletner86-73-7———————Fluorene ______________100-01-6——————4-Nitroaniline534-52-1——————4,6"Dinitro-2-metnylphenoi86-30-6——————N-Nitrosodiphenylamine (1)_101-55-3——————4-Bromophenyl-phenylether__118-74-1——————Hexachlorobenzene_________87-86-5———————Pentachlorophenol_________85-01-8———————Phenanthrene______________120-12-7——————Anthracene84-74-2———————Di-n-butylphthalate206-44-0——————Fluoranthene_____"129-00-0——————Pyrene85-68-7———————Butylbenzylphthalate91-94-1———————3,3/-Dichlorobenzidine56-55-3——————Benzo(a) anthracene218-01-9——————Chrysene117-81-7——————bis (2-Ethylhexyl) phthalate117-84-0——————Di-n-octylphthalate_____"205-99-2——————Benzo(b)fluoranthene_____207-08-9——————Benzo(k) fluoranthene_____50-32-8———————Benzo(a)pyrene193-39-5——————Indenofl, 2,3-cd)pyrene53-70-3———————Dibenz(a,hjanthracene_^191-24-2——————Benzo(g,h, i)perylene100-51-6——————Benzyl Alcohol_______65-85-0———————Benzoic Acid

200020004204204204204202000200042042042020004204203504204204208304204204204204204204204204204208302000

UUUUUUUUUUUUUUUJUUUUUUUUUUUUUUUU


FORM I SV-2 3/90

ARI076I9

U.S. EPA - CLP

EPA SAMPLE NO.

SPONDLab Name: INDUSTRIAL AND ENVIRONMEN Contract:

I .b Code: IEA__ Case No:1528_039__ SAS No.: _____ SDG No.: 10143.

Matrix (soil/water): SOIL_ Lab Sample ID: 931014301

I svel (low/med): LOW_ Date Received: 10/06/93

* Solids: _81.6

Concentration Units (ug/L or mg/kg dry weight): MG/KG

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

82604.61.770.80.300.6743312.04.55.4

106008.110101290.115.95890.421.11640.4219.617.1

C

BB

BUB

BB

B

UBBUUBU

- iQ

N

*

N*

•

M

PPFPPPPPPPPFPPCVPPFPPFPPNR

Color Before: BROWN Clarity-Before: ____ Texture: MEDIUM

( >lor After: YELLOW__ Clarity After: ____ Artifacts: ____

Comments:

FORM I - IN3/90

ARI07620

1A CLIENT SAMPLE NO,VOLATILE ORGANICS ANALYSIS DATA SHEET

MIDDLEPONDLab Name: INDUSTRIAL & ENVIRONMENTA Method: SW-846



Sample wt/vol: 5.0 (g/mL) G Lab File ID: 1011711.D


% Moisture: not dec. 39 Data Analyzed: 10/11/93

GC Column:DB-624 ID: 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: ______(mL) Soil Aliquot Volume: ____(uL)


74-87-3————————CHLOROMETHANE_____74-83-9—————-—BROMOMETHANE______75-01-4————————VINYL CHLORIDE____75-00-3————————CHLOROETHANE______75-09-2————————METHYLENE CHLORIDE67-64-1————————ACETONE75-15-0————————CARBON DISULFIDE75-35-4————————1,1-DICHLOROETHENE75-34-3 ———————— 1,1-DICHLOROETHANE_________540-59-0———————1,2-DICHLOROETHENE (TOTAL)67-66-3————————CHLOROFORM107-06-2———————1, 2-DICHLOROETHANE78-93-3————————2-BUTANONE108-05-4———————VINYL ACETATE71-55-6 ————————1,1,1-TRICHLOROETHANE56-23-5————————CARBON TETRACHLORIDE___75-27-4————————BROMODICHLOROMETHANE___78-87-5————————1,2-DICHLOROPROPANE____10061-01-5—————CIS-1,3-DICHLOROPROPENE79-01-6————————TRICHLOROETHENE124-48-1———————DIBROMOCHLOROMETHANE110-75-8———————2-CHLOROETHYLVINYL ETHER79-00-5 ————————1,1,2-TRI CHLOROETHANE__"71-43-2————————BENZENE10061-02-6—————TRANS-1,3-DICHLOROPROPENE75-25-2————————BROMOFORM_______________"108-10-1———————4-METHYL-2-PENTANONE_____591-78-6———————2-HEXANONE127-18-4———————TETRACHLOROETHENE________79-34-5————————1,1,2, 2-TETRACHLOROETHANE108-88-3———————TOLUENE108-90-7———————CHLOROBENZENE100-41-4———————ETHYLBENZENE_^100-42-5———————STYRENE1330-20-7——————XYLENE (TOTAL)

161616168538888881616888888816888816168888888

UUUUUUUUUUUUUUUUUUUUUUUUUUUUU

FORM I VOA 3/90

ARI0762I

1ACLIENT SAMPLE NO,

8015 PETROLEUM HYDROCARBON ANALYSIS DATA SHEET

Middle PondLab Name: INDUSTRIAL & ENVIRONMENTA

Lab Code: IEA Case Ho.: 1528-039 SDG No.: 10143


Sample wt/vol: 30.1 (g/mL) G Lab File ID: F4O20019.D

% Moisture: 29 Date Received: 10/07/93

GC Column: RTX-5 Date Analyzed: 10/20/93

ID: 0.53 Dilution Factor: 1.0Concentrated Extract Volume: 1000(UL) Date Extracted:10/14/93

COMPOUND

AG^ W0 4«

——————— #2-Fuel 6il- ———— • —— Varsol

MDL

1 A .. »1.30.80

CRQL

2 n• u2.0,2.0

RESULTSMG/KG

2" o. o6.22.8

Q

U

u

FORM I 8015 PH Rev 1.0 5/93

1ACLIENT SAMPLE NO,

8015 PETROLEUM HYDROCARBON ANALYSIS DATA SHEET

North Pond ComLab Name: INDUSTRIAL & ENVIRONMENTA



Sample wt/vol: 60.2 (g/mL) G Lab File ID: F4O20020.D



ID: 0*53 Dilution Factor: 1.0

Concentrated Extract Volume: 2000(UL) Date Extracted:10/14/93

COMPOUND

———————— #2-Fuel Oil

MDL

14• *t1.30.80

CRQL

2 n* V2.020• W

RESULTSMG/KG

2(L• o1.62 f L. O

Q1

\ru

FORM I 8015 PH Rev 1.0 V

ARI07623

CLIENT SAMPLE NO,8015 PETROLEUM HYDROCARBON ANALYSIS DATA SHEET

South PondLab Name: INDUSTRIAL & ENVIRONMENTA

Lab Code: IEA Case No.: 1528-039 SDG No.: 10143Matrix: (soil/water) SOIL Lab Sample ID: 931014301

Sample wt/vol: 30.1 (g/mL) 6 Lab File ID: F4O20018.D


«C Column: RTX-5 Date Analyzed: 10/20/93

ID: 0.53 . Dilution Factor: 1.0Concentrated Extract Volume: 1000(UL) Date Extracted:10/14/93

COMPOUND

———————— «-Fuei Oil———— - —— Varsol

MDL

14. §1.30.60

CRQL

20. w2.02.0

RESULTSMG/KG

25• J112.5

Q

uu

'

FORM I 8015 PH Rev 1.0 5/93

ARI07621*

11A

CLIENT SAMPLE NO.8015 PETROLEUM HYDROCARBON ANALYSIS DATA SHEET

Lab Name: INDUSTRIAL & ENVIRONMENTA


Matrix: (soil/water) SOIL Lab Sample ID: PHBLANK248

Sample wt/vol: 30,0 (g/mL) G Lab File ID: F4O20014.D

% Moisture: 0 Date Received: / /


ID: 0,53 Dilution Factor: 1.0


FORM I 8015 PH Rev 1.0

ARI07625

COMPOUND

———————— #2-Fuel Oil———— ——— Varsol

MDL

1 4x . •*1.30.80

CRQL

2 n. V2.02.0

RESULTSMG/KG

2 n. W2.02.0

Q

V

U

South PondMSLab Name: INDUSTRIAL & ENVIRONMENTA


Matrix: (soil/water) SOIL Lab Sample ID: 931014301MSSample wt/vol: 30.0 (g/mL) G Lab File ID: F4O20016.D


JC Column: RTX-5 Date Analyzed: 10/20/93

ID: 0.53 Dilution Factor: 1.0Concentrated Extract Volume: 1000(UL) Date Extracted:10/14/93

COMPOUND

——————— f2-Fuel 6il——————— Varsol

. . .

MDL

14..*1.30.80

CRQL

20• V2.02.0

RESULTSKG/KG

2 c. 9902.5

Q

U

u

FORM I 8015 PH Rev 1.0 5/93

ARI07626

11A

CLIENT SAMPLE NO,8015 PETROLEUM HYDROCARBON ANALYSIS DATA SHEET

SouthPondMSDLab Name: INDUSTRIAL & ENVIRONMENTA



Sample wt/vol: 30.1 (g/mL) G Lab Pile ID: F4O20017.D



ID: 0,53 Dilution Factor: 1.0


COMPOUND

——————— /2-Fuel Oil

MDL

1.41.30.80

CRQL

2.02.02.0mm . \J

RESULTSMG/KG

2 e. O812 e. D

Q

J-Tw

FORM I 8015 PH Rev 1.0

07627

U.S. EPA - CLP

1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET __________

NPONDCLob Name: INDUSTRIAL AND ENVIRONMEN Contract:

I ib Code: IEA__ Case No:1528_039___ SAS No.: _____ SDG No.: 10143_


3 svel (low/med): LOW_ Date Received: 10/11/93

% Solids: _77.2


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmium !CalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

108003.95.9

88.70.930.62668

21.818.015.73150016.8160014700.1210.8783

0.451.0106

0.4540.835.3

C

U

BUB

U

BUUBU

Q

N

*S

N*

W

M

PPFPPPPPFPPFPPCVPPFPPFPPNR

Color Before: BROWN Clarity Before: _____ Texture: MEDIUM

< 3lor After: YELLOW__ Clarity After: ____ Artifacts: _____

Comments:COMPOSITE

FORM I - IN3/90

U.S. EPA - CLP

1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET

MPONDLab Name: INDUSTRIAL AND ENVIRONMEN Contract:

Lab Code: IEA__ Case No:1528_039__ SAS No.: _____ SDG No.: 10143^


Level (low/med): LOW_ Date Received: 10/07/93

% Solids: _51.3


GAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

66906.18.5111

0.750.96216010.810.811.997706.89274000.168.04070.631.62960.6320.925.0

C

U

BU

B

B

UBBUUBU

Q

N

*

N*

W

M

PPFPPPPPPPPFPPCVPPFPPFPPNR

Color Before: BROWN Clarity Before:

Color After: YELLOW Clarity After:

Comments :LEAVES

Artifacts: YES

FORM I - IN3/90

ARI07629

IE EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

MIDDLEPONDName: INDUSTRIAL & ENVIRONMENTA Method: SW-846



Sample wt/vol: 5.0 (g/raL) G Lab File ID: 1011711.D


% Moisture: not dec* 39 Data Analyzed: 10/11/93


Soil Extract Volume: _____(uL) Soil Aliquot Volume: ____(uL)CONCENTRATION UNITS:

Number TICs found: 0 (ug/L or ug/Kg) UG/KG

CAS NUMBER

1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

COMPOUND NAME

. „

•

.

•

. . , . - .

RT EST. CONC.- - -

-

Q

FORM I VOA-TIC 3/90

1A CLIENT SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

NORTHPONDLab Name: INDUSTRIAL & ENVIRONMENTA Method: SW-846









74-87-3————————CHLOROMETHANE_____74-83-9————————BROMOMETHANE______75-01-4————————VINYL CHLORIDE____75-00-3————————CHLOROETHANE______75-09-2————————METHYLENE CHLORIDE67-64-1————————ACETONE75-15-0————————CARBON DISULFIDE75-35-4————————1 , 1-DICHLOROETHENfi75-34-3————————1,1-DICHLOROETHANE_________540-59-0———————1,2-DICHLOROETHENE (TOTAL)67-66-3————————CHLOROFORM107-06-2———————1, 2-DICHLOROETHANE78-93-3————————2-BUTANONE________~108-05-4———————VINYL ACETATE71-55-6————————1,1,1-TRICHLOROETHANE____56-23-5————————CARBON TETRACHLORIDE_____75-27-4————————BROMODICHLOROMETHANE_____78-87-5————————1,2-DICHLOROPROPANE______10061-01-5—————CIS-1,3-DICHLOROPROPENE79-01-6————————TRICHLOROETHENE__________124-48-1———————DIBROMOCHLOROMETHANE110-75-8———————2-CHLOROETHYLVINYL ETHER79-00-5————————1,1,2-TRI CHLOROETHANE____71-43-2————————BENZENE____________•.____10061-02-6—————TRANS-1, 3-DICHLOROPROPENE75-25-2————————BROMOFORM108-10-1———————4-METHYL-2-PENTANONE591-78-6———————2-HEXANONE127-18-4———————TETRACHLOROETHENE79-34-5————————1,1,2, 2-TETRACHLOROETHANE108-88-3———————TOLUENE_________________~108-90-7———————CHLOROBENZENE100-41-4———————ETHYLBENZENE_____________100-42-5———————STYRENE__________________1330-20-7——————XYLENE (TOTAL)

13131313624666666

13136666666

136666

13136666666


FORM I VGA 3/90

IE EPA SAMPLE 'VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

NORTHPONDName: INDUSTRIAL & ENVIRONMENTA Method: SW-846






GC Columri:DB-624 ID: 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: _____(uL) Soil Aliquot Volume: ____(uL)

CONCENTRATION UNITS:Number TICs found: 0 (ug/L or ug/Kg) UG/KG

CAS NUMBER

1.2*3.4.5.6.1.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

COMPOUND NAME

.

- - •

. •

- - *- - - - '

1

. . . ......

RT EST. CONC.

- . _. .

Q

FORM I VOA-TIC 3/90

11A CLIENT SAMPLE NO.

VOLATILE ORGANICS ANALYSIS DATA SHEET

SOUTHPONDLab Name: INDUSTRIAL & ENVIRONMENTA Method: SW-846




Level: (low/med) LOW Date Received: 10/06/9**




CONCENTRATION UNITS:CAS NO* COMPOUND (ug/L or ug/Kg) UG/KG Q

74-87-3————————CHLOROMETHANE_____74-83-9————————BROMOMETHANE______75-01-4————————VINYL CHLORIDE____75-00-3————————CHLOROETHANE______75-09-2————————METHYLENE CHLORIDE67-64-1————————ACETONE75-15-0————————CARBON DISULFIDE75-35-4————————1,1-DICHLOROETHERE"75-34-3————————1,1-DICHLOROETHANE"540-59-0———————1,2-DICHLOROETHENE (TOTAL)67-66-3————————CHLOROFORM107-06-2 ——————— 1,2-DICHLOROETHANE78-93-3————————2-BUTANONE___________108-05-4———————VINYL ACETATE ~71-55-6————————1,1,1-TRlCHLORO ETHANE56-23-5———•————CARBON TETRACHLORIDE^75-27-4————————BROMODICHLOROMETHANE_78-87-5————————1,2-DICHLOROPROPANE10061-01-5—————CIS-1, 3-DICHLOROPROPENE79-01-6————————TRICHLOROETHENE__________124-48-1———————DIBROMOCHLOROMETHANE110-75-8———————2-CHLOROETHYLVINYL ETHER_79-00-5————————1,1,2-TRICHLOROETHANE____71-43-2————————BENZENE__________________10061-02-6—————TRANS-1,3-DICHLOROPROPENE75-25-2————————BROMOFORM_______________~108-10-1———————4-METHYL-2-PENTANONE_____591-78-6———————2-HEXANONE______________127-18-4———————TETRACHLOROETHENE________79-34-5————————1,1,2,2-TETRACHLORO ETHANE108-88-3———————TOLUENE_________________~108-90-7———————CHLOROBENZENE100-41-4———————ETHYLS ENZENE_____________100-42-5———————STYRENE__________________1330-20-7——————XYLENE (TOTAL)

121212126

386666661212666666612666612126666666


FORM I VOA 3/90

ARI07633

IE i ,:.,. EPA SAMPLEVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

SOUTHPONDName: INDUSTRIAL & SNVIRONMENTA Method: SW-846


Matrix: (soil/water) SOIL Lab Sample ID: 931014301Sample wt/vol: 5.0 (g/mL) G Lab File ID: 1011707.D


% Moisture: not dec. 20 Data Analyzed: 10/11/93GC Column:DB-624 ID: 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: _^____(uL) Soil Aliquot Volume: ____(uL)

CONCENTRATION UNITS:Number TICs found: 0 (ug/L or ug/Kg) UG/KG

CAS NUMBER

1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25. '26.27.28.29.30.

COMPOUND NAME

-

•

RT

'

EST. CONC.

•

- - ••

Q

FORM I VOA-TIC 3/90

ARI07631*

1A CLIENT SAMPLE MO.VOLATILE ORGANICS ANALYSIS DATA SHEET

TRIP1005Lab Name: INDUSTRIAL & ENVIRONMENTA Method: SW-846

74-87-3————————CHLOROMETHANE74-83-9————————BROMOMETHANE75-01-4————————VINYL CHLORIDE75-00-3————————CHLOROETHANE75-09-2————————METHYLENE CHLORIDE67-64-1————————ACETONE__________"75-15-0————————CARBON DISULFIDE75-35-4————————1,1-DICHLOROETHENlT75-34-3————————1,1-DICHLOROETHANE"540-59-0———————1,2-DICHLOROETHENE (TOTAL)67-66-3————————CHLOROFORM107-06-2———————1,2-DICHLOROETHANE78-93-3————————2-BUTANONE108-05-4———————VINYL ACETATE71-55-6————————1,1,1-TRICHLOROETHANE56-23-5————————CARBON TETRACHLORIDE___75-27-4————————BROMODICHLOROMETHANE___78-87-5————————1,2-DICHLOROPROPANE____10061-01-5—————CIS-1, 3-DICHLOROPROPENE79-01-6————————TRICHLOROETHENE124-48-1———————DIBROMOCHLOROMETHANE110-75-8———————2-CHLOROETHYLVINYL ETHER79-00-5————————1,1,2-TRICHLOROETHANE__~71-43-2————-——BENZENE10061-02-6—————TRANS-1,3-DICHLOROPROPENE75-25-2————————BROMOFORM108-10-1———————4-METHYL-2-PENTANONE_____591-78-6———————2-HEXANONE______________127-18-4———————TETRACHLOROETHENE________79-34-5————————1,1,2, 2-TETRACHLOROETHANE108-88-3———————TOLUENE_________________'108-90-7———————CHLOROBENZENE100-41-4 ——————— ETHYLBENZENE_____________100-42-5———————STYRENE1330-20-7——————XYLENE (TOTAL)

101010105105555551010555555510555510105555555


Matrix: (soil/water) WATER Lab Sample ID: 931014302

Sample wt/vol: 5.0 (g/mL) mL Lab File ID: 1018103.D


% Moisture: not dec. ______ Data Analyzed: 10/18/93


Soil Extract Volume: ______(uL) Soil Aliquot Volume: ____(uL)


FORM I VGA 3/90

ARI07635

1A i CLIENT SAMPLE NO,VOLATILE ORGANICS ANALYSIS DATA SHEET

TRIP1006Name: INDUSTRIAL & ENVIRONMENTA Method: SW-846

^ 4 f%^ 474-87-3- — — — —74-83-9 —————— •75-01-4 —————— •75-00-3 —————— •75-09-2 —————— -67-64-1 —————— -75-15-0 —————— -75-35—4--™ — •75-34—3——————540-59-0 ————— -. *» f •>67-66-3-—— —— •107-06-2 ————— -78-93-3 ———— ——108-05-4 ————— -71-55-6 —————— -56-23-5 —————— •75-27-4 ——— --—

10061-01-5 ——— -79-01-6 —————— -124-48-1 ————— -110-75-8 ————— -

10061-02-6 ——— -75-25-2 — .------t ** f» ** mt

108-10-1 ————— -591-78-6 ————— -127-18-4 ————— -

108-90-7 ————— -100-41-4 ————— -100-42-5 ————— -1330-20-7 ———— -

— BROMOMETHANE—VINYL CHLORIDE~ CHLOROETHANE— METHYLENE CHLORIDE—ACETONE—CARBON DISULFIDE— 1, 1-DICHLOROETHEKE— 1, 1-DICHLOROETHANE—1,2-DICHLOROETHENE (TOTAL) _

v tlJ-iUrtUr UKM— 1 , 2-DICHLOROETHANE— 2-BUTANONE—VINYL ACETATE—1,1, 1-TRICHLOROETHANE—CARBON TETRACHLORIDE— BROMODICHLOROMETHANE— 1 , 2-DICHLOROPROPANE—CIS-1, 3 -DICHLOROPROtEtifi

--DIBROMOCHLQROMETHANE— 2-CHLOROETHYLVINYL ETHER

—BENZENE— TRANS-1 , 3-bItHLQROPROPENE— BROMOFORM— 4-METHYL-2-PENTANONE— 2-HEXANONE— TETRACHLOROETHENE—1,1,2 , 2-TETRACHLOROETHANE __

iAjjjU£«r*Ci*-CHLOROBENZENE— ETHYLBENZENE— STYRENE— XYLENE (TOTAL)

101010105105555551010555555510555510105555555

UUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUU



Sample wt/vol: 5.0 (g/roL) mL Lab File ID: 1018114.D


% Moisture: not dec. _______ Data Analyzed: 10/18/93



CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

FORM I VOA 3/90

ARI07636


TRIP1007Lab Name: INDUSTRIAL & ENVIRONMENTA Method: SW-846

74-87-3————————CHLOROMETHANE74-83-9————————BROMOMETHANE__75-01-4————————VINYL CHLORIDE75-00-3————————CHLOROETHANE "75-09-2————————METHYLENE CHLORIDE67-64-1————————ACETONE75-15-0————————CARBON DISULFIDE75-35-4————————1,1-DICHLOROETHEKE"75-34-3————————1,1-DICHLOROETHANE~540-59-0———————1,2-DICHLOROETHENE (TOTAL)67-66-3————————CHLOROFORM107-06-2———————1,2-DICHLOROETHANE___78-93-3————————2-BUTANONE___________108-05-4———————VINYL ACETATl ~71-55-6————————1,1,1-TRI CHLOROETHANE56-23-5————————CARBON TETRACHLORIDEj75-27-4———————BROMODICHLOROMETHANE_78-87-5————————1,2-DICHLOROPROPANE10061-01-5—————CIS-1, 3-DICHLOROPROPENE79-01-6————————TRICHLOROETHENE_________124-48-1———————DIBROMOCHLOROMETHANE110-75-8———————2-CHLOROETHYLVINYL ETHER79-00-5————————1,1,2-TRICHLOROETHANE___~71-43-2————————BENZENE10061-02-6—————TRANS-1,3-DICHLOROPROPENE75-25-2————————BROMOFORM_______________~108-10-1———————4-METHYL-2-PENTANONE_____591-78-6———————2-HEXANONE127-18-4———————TETRACHLOROETHENE79-34-5————————1,1,2, 2-TETRACHLOROETHANE108-88-3———————TOLUENE_________________~108-90-7———————CHLOROBENZENE____________100-41-4———————ETHYLBENZENE_____________100-42-5———————STYRENE__________________1330-20-7—————-XYLENE (TOTAL)

101010105105555551010555555510555510105555555

UUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUU1



Sample wt/vol: 5.0 (g/mL) mL Lab File ID: 1020J06.D






FORM I VGA 3/90

07637


VBLK73Name: INDUSTRIAL & ENVIRONMENTA Method: SW-846

74-87-3———————CHLOROMETHANE74-83-9———————BROMOMETHANE ""75-01-4———————VINYL CHLORlBF75-00-3———————CHLOROETHANE "75-09-2———————METHYLENE CHLORIDE67-64-1———————ACETONE75-15-0————————CARBON DISULFIDE75-35-4——-———1,1-DICHLOROETHENE"75-34-3————————1,1-DICHLOROETHANE"540-59-0———————1,2-DICHLOROETHENE (TOTAL)67-66-3———————CHLOROFORM —107^-06-2———————1,2-DICHLORO ETHANE78-93-3———————2-BUTANONE108-05-4———————VINYL ACETATIT71-55-6————————1,1,1-TRICHLOROETHANE56-23-5———————CARBON TETRACHLORIDE "75-27-4———————BROMODICHLOROMETHANE~78-87-5————————1,2-DICHLOROPROPANE10061-01-5—————CIS-1,3-DICHLOROPROPENE79-01-6————————TRICHLOROETHENE_______"124-48-1———————DIBROMOCHLOROMEtHANE———110-75-8———————2-CHLOROETHYLVINYL ETHER79-00-5————-——-1,1,2-TRICHLOROETHANE__"71-43-2————————BENZENE ———10061-02-6—————TRANS-1, 3-DICHLOROPROPENE75-25-2————————BROMOFORM108-10-1———————4-METHYL-2-PENTANONE591-78-6———————2-HEXANONE127-18-4———————TETRACHLOROETHENE79-34-5———————1,1/2,2-TETRACHLOROETHANE108-88-3——————-TOLUENE "108-90-7———————CHLOROBENZENE100-41-4———————ETHYLBEN2ENE "100-42-5——————-STYRENE ""1330-20-7——————XYLENE (TOTAL)

1010101051055555510105555*5510555510105555555



Matrix: (soil/water) SOIL Lab Sample ID: VBLK73Sample wt/vol: 5.0 (g/mL) G Lab File ID: 1011702.D


% Moisture: not dec. 0 Data Analyzed: 10/11/93GC Column:DB-624 ID: 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: _____(mL) Soil Aliquot Volume: ____(uL)


FORM I VOA 3/90

ARI07638


VBLKJ2Lab Name: INDUSTRIAL & ENVIRONMENTA Method: SW-846

74-87-3————————CHLOROMETHANE74-83-9————————BROMOMETHANE__75-01-4————————VINYL CHLORIDE75-00-3————————CHLOROETHANE "75-09-2————————METHYLENE CHLORIDE67-64-1————————ACETONE75-15-0————————CARBON DISULFIDE75-35-4————————1,1-DICHLOROETHEHlT75-34-3————————1,1-DICHLOROETHANE"540-59-0———————1,2-DICHLOROETHENE (TOTAL)__67-66-3———————CHLOROFORM107-06-2 ——————— 1,2-DICHLOROETHANE______78-93-3————————2-BUTANONE______________108-05-4———————VINYL ACETATE71-55-6————————1,1,1-TRI CHLOROETHANE___56-23-5————————CARBON TETRACHLORIDE____75-27-4————————BROMODICHLOROMETHANE____78-87-5 ———————— 1,2-DICHLOROPROPANE_____10061-01-5—————CIS-1,3-DICHLOROPROPENE_79-01-6————————TRICHLOROETHENE_________124-48-1———————DIBROMOCHLOROMEtHANE110-75-8———————2-CHLOROETHYLVINYL ETHER79-00-5————————1,1,2-TRICHLOROETHANE__~_71-43-2————————BENZENE10061-02-6—————TRANS-1, 3-DICHLOROPROPENE75-25-2————————BROMOFORM108-10-1———————4-METHYL-2-PENTANONE591-78-6 ——————— 2-HEXANONE127-18-4———————TETRACHLOROETHENE________79-34-5 ————————1,1,2,2 -TETRACHLORO ETHANE108-88-3———————TOLUENE_________________]108-90-7———————CHLOROBENZENE100-41-4———————ETHYLBENZENE_____________100-42-5———————STYRENE__________________1330-20-7—————

10101010510555555101055555'5510555510105555555



Matrix: (soil/water) WATER Lab Sample ID: VBLKJ2

Sample wt/vol: 5.0 (g/mL) mL Lab File ID: 1018102.D


% Moisture: not dec* ______ Data Analyzed: 10/18/93

GC Column:DB-624 ID: 0.53 (ram) Dilution Factor: 1.0



FORM I VGA 3/90

ARI07639


VBLKJ5Name: INDUSTRIAL & ENVIRONMENTA Method: SW-846

74-87-3———————-CHLOROMETHANE74-83-9————————BROMOMETHANE ~~75-01-4———————VINYL CHLORI5F75-00-3———————-CHLOROETHANE "75-09-2———————METHYLENE CHLORIDE67-64-1———————ACETONE75-15-0————————CARBON DISULFIDE75-35-4———————1,1-DICHLOROETHERE"75-34-3———————1,1-DICHLOROETHANE"540-59-0———————1,2-DICHLOROETHENE (TOTAL)67-66-3———————-CHLOROFORM107-06-2———————1,2 -DICHLOROETHANE78-93-3———————2-BUTANONE108-05-4-——————VINYL ACETATET71-55-6————————1,1,1-TRI CHLOROETHANE56-23-5———————CARBON TETRACHLORIDE "75-27-4———————BROMODICHLOROMETHANE_78-87-5————————1,2-DICHLOROPROPANE10061-01-5—————CIS-1,3-DICHLOROPROPENE79-01-6————————TRICHLOROETHENE124-48-1——————DIBROMOCHLOROMETHANE110-75-8——————2-CHLOROETHYLVINYL ETHER79-00-5———————-1,1, 2-TRICHLOROETHANE71-43-2————————BENZENE10061-02-6—————TRANS-1,3-DICHLOkOPROPENE75-25-2————————-BROMOFORM108-10-1———————-4-METHYL-2-PENTANONE591-78-6——————2-HEXANONE127-18-4———————TETKACHLOROETHENE79-34-5———————1,1,2,2 -TETRACHLOROETHANE108-88-3——————-TOLUENE108-90-7——————-CHLOROBENZENE100-41-4———————ETHYLBENZENE "100-42-5——————'-STYRENE1330-20-7—————XYLENE (TgTAL)

10101010510555555101055555-5510555510105555555



Matrix: (soil/water) WATER Lab Sample ID: VBLKJ5

Sample wt/vol: 5.0 (g/mL) roL Lab File ID: 1020J03.D

Level? (low/med) LOW Date Received: / /




CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

FORM I VOA 3/90


SOUTHPONDMSLab Name: INDUSTRIAL & ENVIRONMENTA Method: SW-846


Matrix: (soil/water) SOIL Lab Sample ID: 931014301MS







74-87-3————————CHLOROMETHANE____________74-83-9————————BROMOMETHANE_____________75-01-4————————VINYL CHLORIDE___________75-00-3————————CHLOROETHANE_____________75-09-2————————METHYLENE CHLORIDE_______67-64-1————————ACETONE__________________75-15-0————————CARBON DISULFIDE_________75-35-4————————1,1-DICHLOROETHENE75-34-3————————1,1-DICHLOROETHANE_______540-59-0———————1,2-DICHLOROETHENE (TOTAL)67-66-3————————CHLOROFORM107-06-2———————1,2-DICHLORO ETHANE______78-93-3————————2-BUTANONE_____________108-05-4———————VINYL ACET5T1T71-55-6————————1,1,1-TRI CHLOROETHANE___56-23-5————————CARBON TETRACHLORIDE____75-27-4————————BROMODICHLOROMETHANE____78-87-5 ———————— 1,2-DICHLOROPROPANE_____10061-01-5—————CIS-1, 3-DICHLOROPROPENE79-01-6————————TRICHLOROETHENE_________124-48-1———————DIBROMOCHLOROMETHANE110-75-8———————2-CHLOROETHYLVINYL ETHER79-00-5 ———————— 1,1,2-TRICHLOROETHANE__"71-43-2————————BENZENE10061-02-6—————TRANS-1, 3-DICHLOROPROPENE75-25-2————————BROMOFORM108-10-1———————4-METHYL-2-PENTANONE591-78-6———————2-HEXANONE127-18-4———————TETRACHLOROETHENE79-34-5————————1,1,2, 2-TETRACHLOROETHANE108-88-3———————TOLUENE_________________"108-90-7———————CHLOROBENZENE100-41-4———————ETHYLBENZENE________-100-42-5———————STYRENE__________________1330-20-7——————XYLENE (TOTAL)

12121212621676666612126666677612676661212667872666

U

FORM I VGA 3/90

ARI076UI

CLIENT SAMPLE NO.

SOUTHPONDMSDab Name: INDUSTRIAL & ENVIRONMENTA Method: SW-846

Lab Code: IEA Case No*: 1528-039 SDG No.: 10143


Sample vt/vol: 5.0 (g/mL) G Lab File ID: 1011709.D

fjevel: (low/med) LOW Date Received: 10/06/93



Soil Extract Volume: _____(mL) Soil Aliquot Volume: ___(uL)CONCENTRATION UNITS:

CAS NO. COMPOUND (ug/L or Ug/Kg) UG/KG Q

74-87-3————————CHLOROMETHANE74-83-9————————BROMOMETHANE ""75-01-4————————VINYL CHLORlBE"75-00-3———————-CHLOROETHANE "75-09-2———————-METHYLENE CHLORIDE67-64-1———————ACETONE75-15-0———————CARBON DISULFIDE75-35-4———————1,1-DICHLOROETHENE"75-34-3———————1,1-DICHLOROETHANE"540-59-0———————1,2-DICHLOROETHENE (TOTAL)67-66-3———————CHLOROFORM —107-06-2———————1,2-DICHLOROETHANE78-93-3———————2-BUTANONE108-05-4——————VINYL ACETATE^71-55-6————————1,1,1-TRICHLOROETHANE56-23-5———————CARBON TETRACHLORIDE "75-27-4———————*-BROMODICHLOROMETHANE__78-87-5————————1,2-DICHLOROPROPANE10061-01-5—————CIS-1,3-DICHLOROPROPENE79-01-6————————TRICHLOROETHENE_______"124-48-1———————DIBROMOCHLOROMETHANE110-75-8——————^2-CHLOROETHYLVINYL ETHER79-00-5———————1,1,2-TRICHLOROETHANE__"71-43-2————————BENZENE10061-02-6—————TRANS-1, 3-DICHLOROPROPENE75-25-2———————BROMOFORM108-10-1———————4 -METHYL-2 -PENTANONE591-78-6———————2-HEXANONE127-18-4———————TETRACHLOROETHENE79-34-5———————1,1,2,2-TETRACHLOR6ETHANE108-88-3———————TOLUENE . "108-90-7——————-CHLOROBENZENE100-41-4———————ETHYLBENZENE "100-42-5———————STYRENE1330-20-7——————XYLENE (TOTAL)

U

FORM I VOA 3/90

IB CLIENT SAMPLE NO,SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

MIDDLEPONDLab Name: INDUSTRIAL & ENVIRONMENTA



Sample vt/vol: 30.1 (g/mL) G Lab File ID: 1022803.DLevel: (low/med) LOW Date Received: 10/07/93






108-95-2———————Phenol___________________111-44-4——————bis(2-Chloroethyl) ether95-57-8———————2-Chlorophenol____________541-73-1——————1,3-Dichlorobenzene_______106-46-7——————1,4-Dichlorobenzene_______95-50-1———————1,2-Dichlorobenzene_______95-48-7———————2-Methylphenol108-60-1——————2,2' -oxybis (1-Chloropropane)106-44-5——————4-Methylphenol_____^_^^_621-64-7——————N-Nitroso-di-n-propylamine67-72-1———————Hexachloroethane__________98-95-3———————Nitrobenzene78-59-1———————Isophorone88-75-5———————2-NitrophenoI105-67-9——————2,4-Dimethylphenol ~111-91-1——————bis(2-Chloroethoxy)methane120-83-2——————2,4-Dichlorophenol________120-82-1——————1,2,4-Trichlorobenzene_____91-20-3———————Naphthalene ____106-47-8——————4-Chloroaniline87-68-3———————Hexachlorobutadiene__59-50-7———————4-Chloro-3-methylphenol91-57-6———————2-Methylnaphthalene77-47-4———————Hexachlorocyclopentadiene88-06-2———————2,4, 6-Trichlorophenol95-95-4———————2,4,5-Trichlorophenol____91-58-7———————2-Chloronaphthalene_____88-74-4———————2-Nitroaniline131-11-3——————Dimethylphthalate_208-96-8——————Acenaphthylene___606-20-2——————2, 6-Dinitrotoluene99-09-2———————3-Nitroaniline___"83-32-9———————Acenaphthene_____

510510510510510510510510510510510510510510510510510510510

1000510

100051051051051051024005105105102400510


FORM I SV-1 3/90

ARI076l*3

1C CLIENT SAMPLE NO,SEMIVOLATILE ORGAKICS ANALYSIS DATA SHEET

HIDDLEPONDName: INDUSTRIAL & ENVIRONMENTA


Matrix: (soil/water) SOIL Lab Sample ID: 931014503Sample vt/vol: 30.1 (g/mL) G Lab File ID: 1022803.D


% Moisture: 35 decanted: (Y/N) N Date Extracted:10/II/93

Concentrated Extract Volume: 1000(uL) Date Analyzed: 10/22/93Injection Volume: 2.0(uL) Dilution Factor: 1.0!PC Cleanup: (Y/N) N pH:


51-28-5 ———— -100-02-7 ——— •132-64-9 ——— -121-14-2 ——— -84-66-2 ———— •7005-72-3-:——

100-01-6 ——— -534-52-1 ——— -86-30-6 ———— -101-55—3~-—JfcWA •*«* •*

118-74-1 ——— •87-86-5 ———— -85-01-8 ———— •120-12-7 ——— •84-74-2 ———— -206-44-0 ——— -129-00-0 ——— -85-68-7 ———— -91-94-1 ———— -56-55-3 ———— •218-01-9 ——— -117-81-7 ——— -117-84-0 ——— -205-99-2 ——— -207-08-9 ——— -50-32-8 ———— -193-39-5 ——— -G*I .*7 n«i ______

100-51-6 ——— -65-85-0 ———— -

——— 2 , 4-Dinitrophenol—— 4 -Nitrophenol—— Dibenzofuran- —— 2 , 4-Dinitrotoluene—— Diettiyipnthalate—— 4 -cnioropheny 1-pheny lether—— Fluorene—— 4-Nitroaniline—— 4 , 6-Dinitro-2-methylpnenoi—— N-Nitrosodiphenylamine (1)* —— 4 -Bromopheny 1-pheny lether __—— Hexach lor obenz ene—— Pentachlorophenol—— pnenantnrene—— Anthracene—— Di-n-butylphthalate—— Fluoranthene—— pyrene—— Butyibenzylpntnalate—— 3,3'-Dichlorobenzidine—— Benzo (a) anthracene—— cnrysene- —— Dis(2-Ethylhexyl)phtnaiate—— Di-n-octylphthalate—— Benzo (b) fluoranthene—— Benzo(k) fluoranthene—— Benzo (a) pyrene—— indeno (1,2,3 -cd) pyrene. —— Dibenz (a , h) anthracene—— Benzo (g,h,i)perylene—— Benzyl Alcohol- —— Benzole Acid

240024005105105105105102400240051OJ i V

5105102400510510230510510510100051051035051051051051051051051010002400

UUUUUUUUUUUUUUUJUUUUUUJUUUUUUUUU

v (1) - Cannot be separated from Diphenylamine

FORM I SV-2 3/90

CLIENT SAMPLE NO.

NORTHPONDCOMLab Name: INDUSTRIAL & ENVIRONMENTA





% Moisture: 20 decanted: (Y/N) N Date Extracted:10/11/9310/15/93





108-95-2——————Phenol__________________111-44-4——————bis(2-Chloroethyl) ether95-57-8———————2-Chlorophenol____________541-73-1——————1,3-Dichlorobenzene_______106-46-7-—————1,4-Dichlorobenzene_______95-50-1———————1,2-Dichlorobenzene_______95-48-7———————2-Methylphenol________108-60-1——————2, 2' -oxybis (1 -Chloropropane}106-44-5——————4-Methylphenol_____^____621-64-7——————N-Nitroso-di-n-propylamine_67-72-1———————Hexachloroethane__________98-95-3———————Nitrobenzene78-59-1———————Isophorone88-75-5———————2 -Nitrophenol105-67-9——————2,4-Dimethylphenol111-91-1——————bis (2-Chloroethoxy) methane120-83-2——————2,4-Dichlorophenol_______~120-82-1——————1,2,4-Trichlorobenzene____91-20-3———————Naphthalene ___________106-47-8——————4-Chloroaniline87-68-3———————Hexachlorobutadiene59-50-7———————4-Chloro-3-methylphenol91-57-6———————2-Methylnaphthalene77-47-4———————Hexachlorocyclopentadiene88-06-2———————2,4,6-Trichlorophenol95-95-4———————2,4, 5-Trichlorophenol____91-58-7———————2-Chloronaphthalene_____88-74-4———————2-Nitroaniline_________131-11-3——————Diroethylphthalate208-96-8——————Acenaphthylene606-20-2——————2 f 6-Dinitrotoluene99-09-2———————3-Nitroaniline___83-32-9———————Acenaphthene_____

41041041041041041041041041041041041041041041041041041041082041082041041041041041020004104104102000410


FORM I SV-1 3/90

ARI076l*5

1C CLIENT SAMPLE NO,SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

NORTHPONDCOM. jow Name: INDUSTRIAL & ENVIRONMENT A


Matrix: (soil/water) SOIL Lab Sample ID: 931023708Sample vt/vol: 60.0 (g/mL) G Lab File ID: 1022804.D

Level: (low/med) LOW Date Received: 10/11/93% Moisture: 20 decanted: (Y/N) N Date Extracted:10/11/93

10/15/93

Concentrated Extract Volume: 10QO(uL) Date Analyzed: 10/22/93Injection Volume: 2.0(uL) Dilution Factor: 1*0JPC Cleanup: (Y/N) N pH:


*« * •• w **

100-02-7 ———132-64-9 ——— •121-14-2 ——— •84-66-2 ———— •7005-72-3 —— •86-73-7 ———— -100-01-6 ——— •534-52-1 ——— -86-30-6 ———— -^^* -^ V^vtf W

118-74-1 ——— -87-86-5 ———— -85-01-8 ———— -120-12-7 ——— -84-74-2 ———— -206-44-0 ——— -129-00-0 ——— -O K £O *J

91-94-1 ———— -56-55-3 ———— -218-01-9 ——— -117-81-7 ——— -117-84-0 ——— -205-99-2 ——— -207-08-9 ——— •

193-39-5 ——— -53-70-3 ———— -191-24-2—- —100-51-6 ——— -65-85-0 ———— -

—— -2 , 4-Dinitrophenol—— 4 -Nitrophenol—— Dibenzofuran—— 2 f 4-Dinltrotoiuene—— Dlethylphthalate—— 4-Chlorophenyl-phenylether _—— Fluorene—— 4-Nitroaniiine—— 4 , 6-DInitro-2-methylphenol— -N-Nitrosodiphenylamine ;(1)——— 4 -Bromophenyl-pheny lather __—— Hexachlorobenzene—— Pentachlorophenol—— Phenanthrene—— Anthracene—— Dl-n-butylphthalate—— Fluoranthene—— Pyrene—— Butylbenzylphthalate—— 3, 3'-Dichlorobenzidine—— Benzo (a) anthracene—— Chrysene- —— bls(2-Ethylhexyi}phthalate—— Di-n-octylphthalate—— Benzo (b) f luoranthene—— Benzo CJc) f luoranthene—— Benzo(a)pyrene. —— Dibenz (a, h) anthracene- —— Benzo (g, h, i) perylene- —— Benzyl Alcohol- —— Benzole Acid. ,

200020004104104104104102000200041041041020004104101404104104108204104103904104104104104104104108202000

UUUUUUUUUUUUUUUJUUUUUUJUUUUUUUUU


FORM I SV-2 . 3/90

IB CLIENT SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: INDUSTRIAL & ENVIRONMENTASOUTHPOND





% Moisture: 21 decanted: (Y/N) N Dace Extracted:10/11/93





108-95-2——————Phenol__________________111-44-4——————bis (2 -cnloroe tny l J ether ~95-57-8———————2-Chlorophenol____________541-73-1——————1,3-Dichlorobenzene_______106-46-7——————1,4-Dichlorobenzene_______95-50-1———————1,2-Dichlorobenzene_______95-48-7———————2-Methylphenol_________108-60-1——————2,2 ' -oxybis (1-Chloropropane)106-44-5——————4-!fethylphenol_____^______621-64-7——————N-Nitroso-di-n-propylamine67-72-1———————Hexachloroethane98-95-3———————Nitrobenzene___78-59-1———————Isojphorone88-75-5———————2-Nitrophenol105-67-9——————2, 4-Dimethylphenol111-91-1——————bis (2-Chloroethoxy) methane120-83-2——————2,4-Dichlorophenol_______"120-82-1——————1,2,4-Trichlorobenzene___91-20-3———————Naphthalene___________106-47-8——————4-Chloroaniline87-68-3———————Hexachlorobutadiene__59-50-7———————4-Chloro-3-methylphenol91-57-6———————2-Methylnaphthalene77-47-4———————Hexachlorocyclopentadiene_88-06-2———————2 f 4 f 6-Trich 1 oropheno 195-95-4———————2,4,5-Trichlorophenol___91-58-7———————2-Chloronaphthalene_____88-74-4———————2-Nitroaniline_________131-11-3——————Dimethylphthalate208-96-8——————Acenajphthylene__________606-20-2——————2 , 6-Dinitrotoluene______99-09-2———————3-Nitroaniline__________83-32-9———————Acenaphthene____________

4204204204204204204204204204204204204204204204204204204208304208304204204204204202000420420,42012000420


FORM I SV-1 3/90

flRI076li7

ID CLIENT SAMPLE NO,PESTICIDE ORGANICS ANALYSIS DATA SHEET

PB98Name: INDUSTRIAL & ENVIRONMENTA


Matrix: (soil/water) SOIL Lab Sample ID: PB9S

Sample wt/vol: 30.0 (g/mL) G Lab File ID: P5O15006.D% Moisture: 0 decanted: (Y/N) N Date Received: / /

Extraction: (SepF/Cont/Sonc) SONG Date Extracted:10/11/93

Concentrated Extract Volume: lOOOO(uL) Date Analyzed: 10/15/93

Injection Volume: l.O(uL) Dilution Factor: 1.0 .SPC Cleanup: (Y/N) N pH: ___ Sulfur Cleanup: (Y/N) N

'CAS NO. COMPOUND

319-84-6——————-alpha-BHC319-85-7———————beta-BHC "319-86-8———•——-delta-BHC58*89-9——————-gamma-BKC (Lindane)76-44-8———————Heptachlor_______|309-00-2——————Aldrin1024-57-3—————Heptacnlor epoxxde959-98-8——————Endosulfan I_____"60-57-1——————Dieldrin72-55-9———————4 , 4 ' -DDE———72-20-8———————Endrin133213-65-9————Endosulfan II72-54-8———————4,4 ' -ODD1031-07-8—————Endosulfan sulfate50-29-3———————4 , 4 ' -DDT__________72-43 -5———————Methoxychlor53494-70-5———Endrin ketone""7421-36-3————-Endrin aldehyde57-74-9———————Chlordane (technical)8001-35-2—————Toxaphene12674-11-2—————Aroclor-lOlF11104-28-2————Aroclor-122r11141-16-5—————Aroclor-1232"53469-21-9——«——Aroclor-1242"12672-29-6—————Aroclor-1248"11097-69-1-————Aroclor-1254"11096-82-5—————Aroclor-1260"

8.08.08.08.08.08.08.08.016161616161616801616801608080808080160160

UUUUUUUUUUUUUUUUUUUUUUUUUUU

FORM I PEST 3/90

ARI076l*8


PIBLKQQLab Name: INDUSTRIAL & ENVIRONMENTA

Lab Code: IEA Case No,: 1528-039 SDG No.: 10143

Matrix: (soil/water) WATER Lab Sample ID: PIBLKQQ

Sample wt/vol: ________ (9/wL) Lab File ID: P6O25003.D

% Moisture: _____ decanted: (Y/N)__ Date Received: _______

Extraction: (SepF/Cont/Sonc) ___ Date Extracted:______Concentrated Extract Volume: ______(uL) Date Analyzed: 10/25/93

Injection Volume: l.O(uL) Dilution Factor: 1.0

GPC Cleanup: (Y/N) N pH: ___ Sulfur Cleanup: (Y/N) N


319-84-6———————alpha-BHC__________319-85-7——————beta-BHC__________319-86-8——————delta-BHC58-89-9———————gamma-BHC (Lindane)76-44-8———————Heptachlor________309-00-2——————Aldrin1024-57-3—————Heptachlor epoxide

-Endosulfan I60-57-1———————Dieldrin72-55-9————————4,4'-DDE'72-20-8———————Endrin72-54-8————————4 , 4 ' -DDD/EndO II1031-07-8—————Endosulfan sulfate50-29-3————————4,4'-DDT72-43-5——————Methoxychlor53494-70-5————Endrin ketone_____7421-36-3—————Endrin aldehyde ~57-74-9———————Chlordane (technical)8001-35-2————— ___12674-11-2—————Aroclor-101611104-28-2—————Aroclor-1221"11141-16-5—————Aroclor-1232"53469-21-9—————Aroclor-1242"12672-29-6—————Aroclor-1248"11097-69-1—————Aroclor-1254"11096-82-5—————Aroclor-1260"

0.0500.0500.0500.0500.0500.0500.0500.0500.10

0*00940.100.100.100.100.500.100.100.101.00.500.500.500.500.501.01.0

FORM I PEST

UUUUUUUUUJUUUUUUUUUUUUUUUU

flRIQ76t*9

CLIENT SAMPLE NO.

PXBLKHHName; INDUSTRIAL & ENVIRONMENTA


Matrix: (soil/water) WATER Lab Sample ID: PIBLKHH

Sample vt/vol: ________ (g/mL) Lab File ID: P6O21Q02.D% Moisture: ____ decanted: (Y/N)__ Date Received: _______

Extraction: (SepF/Cont/Sonc) ___ Date Extracted;Concentrated Extract Volume: _____(UL) Date Analyzed: 10/21/93Injection Volume: 1.0(uL) Dilution Factor: 1.0

PC Cleanup: (Y/N) N pH: ___ Sulfur Cleanup: (Y/N) NCONCENTRATION UNITS:

,. COMPOUND (ug/L or ug/Kg) UG/L Q

319-84-6——————alpha-BHC319-85-7——————beta-BHC "319-86-8——————delta-BHE"58-89-9-——————gamma-BHC (Lindane}76-44-8———————Heptachlor_______"309-00-2——————Aldrin1024-57-3———--Heptachlor epoxide959-98-8——————Endosulfan I60-57-1———————Dieldrin72-55-9———————4,4 ' -DDE"——"72-20-8———————Endrin —————72-54-8———————4,4 '-DDD/Endo II1031-07-8—————Endosulfan sulfa€e~50-29-3———————4,4 ' -DDT72-43-5———————Methoxychlor53494-70-5————Endrin keton~7421-36-3—————Endrin aldehyde57-74-9——————Ch lordane (technical)8001-35-2—————Toxaphene12674-11-2—————ArpClor-101611104-28-2--———-Aroclor-122r11141-16-5—————Aroclor-1232"53469-21-9—————Aroclor-1242"12672-29-6—————Aroclor-1248"11097-69-1—————Aroclor-1254"11096-82-5—————Aroclor-1260"

0.0500.0500.0500.0500.0500.0500.0500.0500.100.100.100.100.100.100.500.100.10O.iO"1.00.500.500.500.500.501.01.0

UuUuuuuuuuuuuuuuuuuuuuuuuu

FORM I PEST 3/90

ARI07650


PIBLKKKLab Name: INDUSTRIAL & ENVIRONMENTA


Matrix: (soil/water) WATER Lab Sample ID: PIBLKKK

Sample wt/vol: _________ (g/mL) Lab File ID: P5O25002.D

% Moisture: _____ decanted: (Y/N)__ Date Received: _______

Extraction: (SepF/Cont/Sonc) ___ Date Extracted:_______

Concentrated Extract Volume: ______(uL) Date Analyzed: 10/25/93



CONCENTRATION UNITS:CAS-NO. COMPOUND (ug/L or ug/Kg) UG/L Q

319-84-6———————alpha-BHC_________319-85-7———————beta-BHC_________319-86-8———————delta-BHC58-89-9———————gamma-BBC (Lindane)76-44-8———————Heptachlor________309-00-2——————Aldrin1024-57-3—————Heptachlor epoxide_959-98-8——————Endosulfan I_____~60-57-1———————Dieldrin_________72-55-9————————4 , 4 ' -DDE__________72-20-8———————Endrin33213-65-9—————Endosulfan II72-54-8————————4 , 4 ' -DDD_____1031-07-8——————Endosulfan sulfate50-29-3————————4 , 4 ' -DOT __________72-43-5———————Methoxychlor53494-70-5—————Endrin ketone_____7421-36-3—————Endrin aldehyde57-74-9———————Chlordane (technical)8001-35-2——————Toxaphene _______12674-11-2—————Aroclor-101611104-28-2—————Aroclor-1221_______11141-16-5—————Aroclor-1232_______53469-21-9—————Aroclor-1242_______12672-29-6—————Aroclor-1248_______11097-69-1—————Aroclor-1254_______11096-82-5—————Aroclor-1260

0.0500.0500.0500.0500.0500.0500.0500.0500.100.100.100.100.0540.100.0480.500.0190.100.501.00.500.500.500.500.501.01.0

UUUUUUUUUUUUJUJUJUUUUUUUUUU

FORM I PEST 3/9'

107651

ID CLIENT SAMPLE NO,PESTICIDE ORGANICS ANALYSIS DATA SHEET

PIBLKDDName: INDUSTRIAL & ENVIRONMENTA

Lab Code: IEA Case No.: 1528-039 . SDG No.: 10143

Matrix: (soil/water) WATER Lab Sample ID: PIBLKDD

Sample wt/vol: ________ (9/nL) Lab File ID: P6O15002.D

% Moisture: _____ decanted: (Y/N)__ Date Received: :Extraction: (SepF/Conr/Sonc) ___ Date Extracted:

Concentrated Extract Volume: _____(uL) Date Analyzed: 10/15/93

Injection Volume: 1*0(uL) Dilution Factor: 1.0GPC Cleanup: (Y/N) N pH: ___ Sulfur cleanup: (Y/N) N


319-84-6——————alpha-BHC319-85-7——————beta-BHC "319-86-8——————delta-BHC"58-89-9———————gamma-BHC (Lindane)76-44-8———————Heptachlor________"309-00-2——————'Aldrin ———————1024-57-3—————Heptachlor epoxide959-98-8——————Endosulfan I_____~60-57-1———————Dieldrin7 2 -55-9———————4 , 4 ' -DDE———72-20-8———————Endrin ————————1031-07-8—————Endosultan suit ate50-29-3————————4,4 '-DOT72-43-5———————Methoxycnior53494-70-5————Endrin ketone7421-36-3—————Endrin aldehyde"57-74-9———————Chlordane( technical)8001-35-2—————Toxaphene^______'12674-11-2————Aroclor-101611104-28-2————Aroclor-122111141-16-5————Aroclor-1232~~53469-21-9—————Aroclor-124212672-29-6————Aroclor-1248——11097-69-1————Aroclor-1254——11096-82-5————-Aroclor-1260

0.0500.0500.0500.0500.0500.0500.0500.0500.100.100.100.100.100.500.100.100.5Q1.00.500.500.500.500.501.01.0

UUUUUUUUUUUUUUUUUUUUUUUUU

FORM I PEST 3/90

ARI07652


PIBLKAALab Name: INDUSTRIAL & ENVIRONMENTA


Matrix: (soil/water) WATER Lab Sample ID: PIBLKAA

Sample wt/vol: _________ (g/mL) Lab File ID: P5O15002.D

% Moisture: ____ decanted: (Y/N)__ Date Received: _______

Extraction: (SepF/Cont/Sonc) ___ Date Extracted:_______

Concentrated Extract Volume: ______(uL) Date Analyzed: 10/15/93




319-84-6———————alpha-BHC_________319-85-7———————beta-BHC__________319-86-8——————delta-BHC58-89-9———————gamma-BHC (Lindane)76-44-8———————Heptachlor_______309-00-2——————Aldrin1024-57-3——————Heptachlor epoxide959-98-8——————Endosulfan I_____~60-57-1———————Dieldrin________72-55-9————————4, 4'-DDE_________72-20-8———————Endrin33213-65-9—————Endosulfan II72-54-8————————4,4'-DDD1031-07-8—————Endosulfan sulfate50-29-3————————4, 4 ' -DDT72-43-5 ———————Methoxychlor53494-70-5—————Endrin ketone______7421-36-3——————Endrin aldehyde57-74-9———————Chlordane( technical)8001-35-2——————Toxaphene________12674-11-2—————Aroclor-101611104-28-2—————Aroclor-1221_______11141-16-5—————Aroclor-1232_______53469-21-9—————Aroclor-124212672-29-6—————Aroclor-1248_______11097-69-1—————Aroclor-1254_______11096-82-5—————Aroclor-1260

0.0500.0500.0500.0500.0500.0500.0500.0500.100.100.100.100.100.100.100.500.100.100.501.0

0.500.500.500.500.501.01.0

FORM I PEST 3/9C

ARI07653

. xID CLIENT SAMPLE NO.

PESTICIDE ORGANICS ANALYSIS DATA SHEET

PB980Name: INDUSTRIAL & ENVIRONMENTA


Matrix: (soil/water) SOIL Lab Sample ID: PB980


% Moisture: 0 decanted: (Y/N) N Date Received: / /;

Extraction: (SepF/Cont/Sonc) SONC Date Extracted:10/11/93


Injection Volume: l.O(uL) Dilution Factor: 1*0

•SPC Cleanup: (Y/N) N pH: ___ Sulfur Cleanup: (Y/N) N

' CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

319-85-7 ————

58-89-9 —————76-44-8 —————309-00-2 —— --1024-57-3 ———959-98-8 ————60-57-1 —————72-55-9 —————72-20-8 —————33213-65-9 ——72-54-8 —————1031-07-8 ———en OQ *>______72-43-5 —————53494-70-5 ——7421-36-3 ———57-74-9-- — -™8001-35-2 ———12674-11-2 ——11104-28-2 ——11141-16-5 ——53469-21-9 ——12672-29-6 ——11097-69-1 ——11096-82-5 ——

—— alpha-BHC—— beta-BHC—— ...Hd *•»— RH/"*— — —vie j. ta — on\~—— gamma-BHC (Lindane)—— Heptacnior—— Aldrin—— Heptacnior epoxide—— Endosulfan I—— Dieiorin—— 4, 4 '-DDE—— Endrin—— Endosulfan II—— 4, 4 '-ODD—— Endosulfan sulfate———A A'— DDT-m g t WA

—— Metnoxychlor—— Endrin Ketone—— Endrin aiaenyde—— Chlordane( technical)—— Toxaphene—— Arocior-i&ie— — Aroclor-1221—— Arocior-1232— '-ATOClor-1242—— Aroclor-1248—— Airoclor-12 54—— Aroclor-1260

8.08.08.08.08.08.08.08.016161616161616801616801608080808080160160

UuUuuuuuuuuuuuuuuuuuuuuuuuu

FORM I PEST 3/90

ARI07651*




Matrix: (soil/water) SOIL Lab Sample ID: 931014301MS


% Moisture: 21 decanted: (Y/N) N Date Received: 10/06/93






319-84-6———————alpha-BHC319-85-7——————beta-BHC_2319-86-8——————delta-BHC58-89-9———————gamma-BHC (Lindane)76-44-8———————Heptachlor_______309-00-2——————Aldrin1024-57-3 —————Heptachlor epoxide_959-98-8——————Endosulfan I_____~60-57-1———————Dieldrin________72-55-9————————4,4 ' -DDE__________72-20-8———————Endrin72-54-8———————4 ,4 ' -DDD/Endo II1031-07-8——————Endosulfan sulfate50-29-3————————4 , 4 ' "DOT ________72-43-5———————Methoxychlor53494-70-5————Endrin ketone7421-36-3—————Endrin aldehyde ~57-74-9———————Chlordane (technica 1)8001-35-2—————Toxaphene12674-11-2—————Aroclor-101611104-28-2—————Aroclor-1221"11141-16-5—-——Aroclor-1232"53469-21-9—————Aroclor-1242"12672-29-6—————Aroclor-1248"11097-69-1—————Aroclor-1254"11096-82-5—————Aroclor-1260"

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ID CLIENT SAMPLE HO/PESTICIDE ORGANICS ANALYSIS DATA SHEET

. SOUTHPONDMSD\_<ib Name: INDUSTRIAL & ENVIRONMENTA



Sample vt/vol: 30.1 (g/mL) G Lab File ID: P6O15007.D

% Moisture: 21 decanted: (Y/N) N Date Received: 10/06/93


Concentrated Extract Volume: 10000(uL) Date Analyzed: 10/15/93Injection Volume: l.O(uL) Dilution Factor: 1.0

'-PC Cleanup: (Y/N) N pH: ___ Sulfur Cleanup: (Y/N) NCONCENTRATION UNITS:

GAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

319-85-7 ———319-86-8 ———58-89-9 ———— •76-44-8 ————309-00-2 ———1024-57-3 ——

60-57-1 ————72-55-9 ————72-20-8 ——— -72-54-8 ————1031-07-8 ——50-29-3 ————72-43-5 ————53494-70-5 —7421-36-3 ——57-74-9 ————8001-35-2 ——12674-11-2—11104-28-2™11141-16-5—53469-21-9—12672-29-6—11097-69-1—11096-82-5—

——— alpha-BHC——— beta-BHC——— delta-BHC—— gamma-EHC ( Lindane)— — Heptachlor—— Aldrin—— Heptachlor epoxide— — Endosulfan I—— Dieldrin——— 4, 4 '-DDE— --Endrin—— 4,4'-DDD/Endo II—— -Endosulfan sulfate——— 4, 4 '-DOT—— Methoxychlor——— Endrin ketone—— Endrin aldehycle—— Chlordane( technical)—— Toxaphene—— — Aroclor-1016- —— Aroclor-1221——— Aroclor-1232— >-Aroclor-1242——— Aroclor-1248

CVLWV* s*. . <j.«* -«— — Aroclor-1260

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