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Transcript of Questionnaire for Phosgenation Plants - JAAS( … · Web viewPhosgenation section APR 6 100...
CONFIDENTIAL
Questionnaire for Phosgenation Plants CL-475135-1Seite 1 von 11
Please append supplementary information to any section where you consider it may be of use and send it back to [email protected] or Fax: +41 61 8256 737,
1. GENERAL INFORMATION
Customer:
Address:
Contact person:
Phone:
Telefax:
E-mail:
End-user:
Address:
Plant location:
What kind of product(s) shall be manufactured with phosgene?
Formula/Name/Molecular weight Purity wt-%
ISOCYANATES CHLOROFOMATES ACID CHLORIDES POLYCARBONATES
NOTE: Pre filled data refer to BCT Standard, please correct/delete if not applicable.
© BUSS ChemTech AG, 2006Made by: Daniel Hariri
Issue Date: 19.10.2006 Filed by: QM
CONFIDENTIALQuestionnaire for Phosgenation Plants CL-475135-1
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2. PROCESS & TECHNICAL DATA
2.1 Plant capacity
PRODUCT: Annual production MT/year
MT/day
Annual production time hours/year hours/day
800024
Type of operation --- Batch ContinuousProduction rate kg/h Reaction time / Residence time min. Design Pressure // Temperature --- -1 /+6 barg // -0 / +100°CRemarks:
2.2 Reaction conditionsPhysical state - Gas/Liquid Slurry Rated flow rate kg/h Reaction Pressure Min. / Average / Max. barg / / Reaction Temperature Min. / Average / Max. °C / / Reaction Density Min. / Average / Max. kg/m3 / / Reaction Specific Heat capacity Min. / Average / Max. kJ/kgK / / Reaction Therm. Conductivity Min. / Average / Max. W/mK / / Reaction Viscosity Min. / Average / Max. mPas / / Solubility of HCl / / °C mol/mol / / Solubility of CO2 / / °C mol/mol / / Solubility of COCl2 / / °C mol/mol / / Composition wt.-% min. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. balanceRemarks:
2.3 Reaction data
REACTIONS Heat of reaction Reac.P
Reac.T
MAIN REACTION kJ/kmol BASIS barg °C + + + + + + + +
SIDE REACTION kJ/kmol BASIS barg °C + + + + + + + +
CONFIDENTIALQuestionnaire for Phosgenation Plants CL-475135-1
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2.4 Product & Raw material specification
Product: Physical state - Gas Liquid SolidRated flow rate kg/h Supply Pressure Min. / Average / Max. barg / / Supply Temperature Min. / Average / Max. °C / / Density Min. / Average / Max. kg/m3 / / Specific Heat capacity Min. / Average / Max. kJ/kgK / / Therm. Conductivity Min. / Average / Max. W/mK / / Viscosity Min. / Average / Max. mPas / / Melting point / Glas Temperature °C / Vapour pressure / / °C mbara / / Solubility of HCl / / °C mol/mol / / Solubility of CO2 / / °C mol/mol / / Solubility of COCl2 / / °C mol/mol / / Composition wt.-% min. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. balanceOthersColour (Hazen, APHA, …) Appearance (e.g.Turbidity max.) Remarks:
Raw material: Phosgene, COCl2Physical state - Gas Liquid SolidRated flow rate kg/h Supply Pressure at consumer Min. / Average / Max. barg 0.1 / 0.2 / 0.3Supply Temperature at consumer Min. / Average / Max. °C 50 / 55 / 60Density Min. / Average / Max. kg/m3 4.1 / 4.3 / 4.6Specific Heat capacity Min. / Average / Max. kJ/kgK 0.60 / 0.60 / 0.60Therm. Conductivity Min. / Average / Max. W/mK 0.01 / 0.01 / 0.01Viscosity Min. / Average / Max. mPas 0.01 / 0.01 / 0.01CompositionCOCl2 wt.-% min. 98.0000 Ar wt.-% max. 0.0013CO wt.-% max. 1.1893 wt.-% max. CO2 wt.-% max. 0.0374 wt.-% max. HCl wt.-% max. 0.4135 wt.-% max. CCl4 wt.-% max. 0.0197 wt.-% max. Cl2 wt.-% max. 0.0027 N2 wt.-% max. BalanceSupply: Liquid from an existing plant Tank farm
Not available on site Remarks:
CONFIDENTIALQuestionnaire for Phosgenation Plants CL-475135-1
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Raw material: Physical state - Gas Liquid SolidRated flow rate kg/h Supply Pressure Min. / Average / Max. barg / / Supply Temperature Min. / Average / Max. °C / / Density Min. / Average / Max. kg/m3 / / Specific Heat capacity Min. / Average / Max. kJ/kgK / / Therm. Conductivity Min. / Average / Max. W/mK / / Viscosity Min. / Average / Max. mPas / / Melting point / Glas Temperature °C / Vapour pressure / / °C mbara / / Solubility of HCl / / °C mol/mol / / Solubility of CO2 / / °C mol/mol / / Solubility of COCl2 / / °C mol/mol / / Composition wt.-% min. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. balanceOthersColour (Hazen, APHA, …) Appearance (e.g.Turbidity max.) Remarks:
Raw material: Physical state - Gas Liquid SolidRated flow rate kg/h Supply Pressure Min. / Average / Max. barg / / Supply Temperature Min. / Average / Max. °C / / Density Min. / Average / Max. kg/m3 / / Specific Heat capacity Min. / Average / Max. kJ/kgK / / Therm. Conductivity Min. / Average / Max. W/mK / / Viscosity Min. / Average / Max. mPas / / Melting point / Glas Temperature °C / Vapour pressure / / °C mbara / / Solubility of HCl / / °C mol/mol / / Solubility of CO2 / / °C mol/mol / / Solubility of COCl2 / / °C mol/mol / / Composition wt.-% min. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. BalanceSupply: Liquid from an existing plant Tank farm
Not available on site OthersColour (Hazen, APHA, …) Appearance Remarks:
CONFIDENTIALQuestionnaire for Phosgenation Plants CL-475135-1
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2.5 Solvent & Catalyst specificationSolvent: Physical state - Gas Liquid SlurryRated flow rate kg/h Supply Pressure Min. / Average / Max. barg / / Supply Temperature Min. / Average / Max. °C / / Density Min. / Average / Max. kg/m3 / / Specific Heat capacity Min. / Average / Max. kJ/kgK / / Therm. Conductivity Min. / Average / Max. W/mK / / Viscosity Min. / Average / Max. mPas / / Melting point / Glas Temperature °C / Vapour pressure / / °C mbara / / Solubility of HCl / / °C mol/mol / / Solubility of CO2 / / °C mol/mol / / Solubility of COCl2 / / °C mol/mol / / Composition wt.-% min. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. BalanceSupply: Liquid from an existing plant Tank farm
Not available on site Others Remarks:
Catalyst: Type - Heterogeneous
HomogeneousPhysical state - Gas Liquid SlurryRated flow rate kg/h Supply Pressure Min. / Average / Max. barg / / Supply Temperature Min. / Average / Max. °C / / Density Min. / Average / Max. kg/m3 / / Specific Heat capacity Min. / Average / Max. kJ/kgK / / Therm. Conductivity Min. / Average / Max. W/mK / / Viscosity Min. / Average / Max. mPas / / Melting point °C Particle size distribution Min. / Average / Max. m / / Vapour pressure / / °C mbara / / Solubility of HCl / / °C mol/mol / / Solubility of CO2 / / °C mol/mol / / Solubility of COCl2 / / °C mol/mol / / Composition wt.-% min. wt.-% max. wt.-% max. wt.-% max. wt.-% max. wt.-% max. BalanceSupply: Drum Tank farm As slurry Not available on site
Dissolved in as solution
Remarks:
CONFIDENTIALQuestionnaire for Phosgenation Plants CL-475135-1
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3. UTILITIES (conditions defined at BCT battery limit inlet/outlet flange)
Cooling Water Process Water Chilled Water Hot Water Demin. WaterAbbreviation WC WP WCH WH WDMTemperature Min. 12 °C °C 5 °C °C 12 °C
Max. 25 °C °C 10 °C °C 20 °CT Max. 10 °C °C 3 °C °C °CPressure Min. 4.0 barg barg 4.0 barg barg 2.0 barg
Max. 5.0 barg barg 5.0 barg barg 3.0 bargP Max. 1.0 bar bar 1.0 bar bar barFouling factor 0.00052 m2K/W m2K/W 0.00020 m2K/W m2K/W 0.00035 m2K/WAvailable capacity m3/h m3/h m3/h m3/h m3/h
Quality Filtered Treated
Filtered Treated
Filtered Treated
Filtered Treated
Filtered Treated
Remark:
Brine Sat. Steam Abbreviation MBR S Temperature Min. °C 162 °C °C °C °C
Max. °C 165 °C °C °C °CT Max. °C °C °C °C °CPressure Min. barg 5.5 barg barg barg barg
Max. barg 6.0 barg barg barg bargP Max. bar 2.0 bar bar bar barFouling factor m2K/W 0.00026 m2K/W m2K/W m2K/W m2K/WAvailable capacity m3/h kg/h /h /h /h
Quality Filtered Treated
Filtered Treated
Remark:
Instrument Air Purge Air Nitrogen VacuumAbbreviation AI AP N2 VACTemp. Min. 5 °C 20 °C 5 °C °C 10 °C
Max. 30 °C 40 °C 40 °C °C 50 °CDew point (atm. cond.) -50 °C -50 °C -50 °C °C °CPressure Min. 5.0 barg 0.2 barg 6.0 barg barg 10 mbara
Max. 6.5 barg 6.0 barg 8.0 barg barg 50 mbaraAvailable capacity Nm3/h Nm3/h Nm3/h /h kg/h
Quality Filtered Free of oil/dust
Filtered Free of oil/dust
Filtered Free of oil/dust
Available: YES
NO
Remark:
Electric power supplyPower voltage :
Voltage Tolerance:Neutral available:
Frequency ± Tolerance:Available Power:
± %NHzkW
3x400V 1x230V ± 10% ± %
Yes No 50Hz ± 5% 60Hz ± 5% Hz ± %
Control voltage: 24VDC Emergency power available:
YES NO
UPS: Power: kW Diesel generator: Power: kW : Power: kW
Remarks
CONFIDENTIALQuestionnaire for Phosgenation Plants CL-475135-1
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CONFIDENTIALQuestionnaire for Phosgenation Plants CL-475135-1
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4. scope of BCT supply
SCOPE OF BCT
SUPPLY
Abb
revi
atio
n
Bas
ic E
ng.
Exte
nded
Bas
ic E
ng.
Det
ail E
ng.
Softw
are
Eng.
Eq
uipm
ent
Valv
ing
Pipi
ng
Inst
rum
enta
tion
Fiel
d C
ablin
gC
ontr
ol c
abin
etD
CS
Har
dwar
ePH
A S
tudy
( i.e
. Haz
op )
Ex Z
one,
1,
2 or
non
eSt
eel S
truc
ture
Phosgenation section APR -- 2Process Absorption section PA -- 2Caustic Soda dilution section CSD Product treatment section PT Solvent recovery section SR HCL recovery section HCl
PLANT LOCATION: Indoor Outdoor TYPE: Modular built Stick built
Motor Control Centre MCC Distributed Control System DCS YOKOGAWA
Emergency Shutdown System ESD YOKOGAWA PROSAFE HIMA
Remarks
5. DEFINITION OF EXPLOSION ZONE & PROTECTIONHazard Classification
Hazard Zone: Group:Temp. Class: 1-6
Zone 2 IIA IIB IIC T4
Hazard Zone (USA) Class- Division- Group-
EEx-Protection (Multiple options for valves & instrumentation, based on availability of corresponding Ex. Protection)
Drives & Motors e d de Solenoid valves e d i Instrumentation e d i p Remarks
CONFIDENTIALQuestionnaire for Phosgenation Plants CL-475135-1
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6. STANDARDS & CODESApplicable Standard:
DIN ANSI Applicable Code & Regulation (Mechanical Engineering):
Druckgeräterichtlinie 97/23/EG AD 2000 Regelwerk ASME
Applicable Code & Regulation (Electrical Engineering): IEC NEC / NEMA
Applicable Code & Regulation (Explosion Protection): ATEX
Inspection Authority: SVTI TUEV Lloyds Stoomwezen
Remarks:
7. GENERAL DATA REFERENCE
PRICE:Offer Accuracy± 30 % Fixed Price SHIPPING INSTRUCTIONS:
Ex-Works Pratteln FOB CIF
ENGINEERING DOCUMENTATION:English German
Standard number of copies: Additional number of copies:For Approval: 2x Final: 3x
Remarks:
8. construction site & SITE CONDITIONSAvailable space: A & Measures: L x W x H & Max. admissible floor load: FLA = m2 L = m W = m H = m FL= kg/m2
SITE CONDITIONS:Amb. Temperature Min. / Average / Max. °C / / Relative humidity Min. / Average / Max. % / / Barom. Pressure Min. / Average / Max. mbara / / Annual rain fall Min. / Average / Max. mm / / Rain fall Max. during 10-15 min. mm Snow load Design kg/m2 Seismic intensity Max.
Max.Richter scaleAccelerationRated zoneStandard
Wind Max. Max. at 10 m height
m/s // km/hm/s // km/h
// //
N W S E NE NW SW SE
Remarks
9. Material of construction & design conditions
CONFIDENTIALQuestionnaire for Phosgenation Plants CL-475135-1
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SCOPE OF BCT
SUPPLY
Abb
revi
atio
n
Material of construction for all parts in contact with the raw
material or the product
Des
ign
Pres
. ba
rg
Des
ign
Tem
p. °
C
Phosgenation section APR 6 100Process Absorption section PA 0 50Caustic Soda dilution section CSD Product treatment section PT
CONFIDENTIALQuestionnaire for Phosgenation Plants CL-475135-1
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Solvent recovery section SR HCL recovery section HCl
Remarks