Poly(vinyl alcohol) / Cellulose Barrier Films
description
Transcript of Poly(vinyl alcohol) / Cellulose Barrier Films
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Poly(vinyl alcohol) / Cellulose Barrier FilmsShweta Paralikar John SimonsenWood Science & EngineeringOregon State UniversityJohn LombardiVentana Research Corp.
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OUTLINE
Introduction
Materials
Results and Discussion
Conclusions
Acknowledgements
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Introduction Barrier Films?
Designed to reduce/retard gas migration
Widely used in the food and biomedical industries
Another application is as a barrier to toxic chemicals
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Chemical Vapor Barrier To prevent the diffusion of toxic chemical vapors, while allowing water vapor to pass through
Hydrophilic barriers to protect from hydrophobic toxins
Should be tough and flexible
Useful in protective clothing
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Materials Poly(vinyl alcohol) = PVOH
Nontoxic, good barrier for oxygen, aroma, oil and solvents Prepared by partial or complete hydrolysis of poly(vinyl acetate)
Structure:
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PVOH Water Stability
PVOH films have poor resistance to water
Crosslinking agent reduces water sorption and the crosslinks also act as a barrier to diffusion
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Poly(acrylic acid)-PAA
Poly(acrylic acid) PAA:
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Crosslinking reactionSource: Sanli, O., et al. Journal of applied polymer science, 91( 2003) Heat treatment forms ester linkages
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Cellulose Nanocrystals-(CNXLs)CNXLs were prepared by acid hydrolysis of cellulose obtained from cottonCrystalline regionsAmorphous regionAcid hydrolysisIndividual nanocrystalsIndividual cellulose polymerNative cellulose
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Proposed structurePVOHPAA
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ObjectivesPrepare chemical barrier films with PVOH/ PAA/ CNXL system
To understand the chemistry and physics of this system
Select optimum time and temperature for heat treatment
Find combination which allows moisture to pass through but restricts diffusion of toxic chemical vapors
Surface modify CNXLs to improve interaction with matrix
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MethodsFilm Preparation
Testing methodsWater solubility - Optimize heat treatmentFourier Transform Infrared Spectroscopy - Bond analysisPolarized Optical Microscopy - DispersionWater Vapor Transmission Rate (WVTR)Universal Testing Machine - Mechanical propertiesDifferential Thermogravimetric Analysis - Thermal degradationChemical Vapor Transmission Rate (CVTR)
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Preparation of the Blends5 wt % solution of PVOH and PAA1 wt % solution of dispersed CNXLs in DI waterRemaining composition of the film consists of PVOH
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Film Preparation
Compositions were mixed, sonicated and then air dried for 40 hours
The thickness of the film was controlled by the concentration (%solids) of the dispersion before drying
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Heat treatment optimization
Evaluate via water solubility test At 125 C/1 hr films were completely soluble in water after a dayAt 185 C/1hr color of the films changed to brownAt 150 C and 170 C/45 min films were clear and had good water resistance
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% Solubility =Lower = BetterTotal % Solubility after 72 hours of soaking time
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Fourier Transform Infrared SpectroscopyPVOHPAAAbsorbanceRed: Heat treated film Blue: Non heat treated film
Absorbance
1500 cm-1
2500 cm-1
3500 cm-1
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FTIR of 10% CNXL/10% PAA/80% PVOHWavenumbers (cm-1)AbsorbanceRed: Heat treated film Blue: Non heat treated film
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Polarized Optical MicroscopyDispersion of CNXLsa) 5% CNXL/ 10%PAA b) 10% CNXL/ 10% PAA c) 15% CNXL/ 10% PAA
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Water Permeability Water Vapor Transmission Rate
Test were conducted at 30C and 30% relative humidity
D
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WVTR
Chart1
33.18453570190.65347319570.6534731957
21.38169381750.52693328680.5269332868
12.69711707420.79209441860.7920944186
9.80029155870.15813767560.1581376756
11.82078008710.36795373990.3679537399
18.17283291290.77521295570.7752129557
15.12102237550.3503925610.350392561
10.39149975320.49500681740.4950068174
12.97466301480.71238951710.7123895171
Composition
Flux g/m2 day
Sheet1
gm/mmhr
170
FilmAreawt loss/hrgm/mt^2*hrgm/mt^2*hrgm/mt^2*hrgm/mt^2*daystddev
100 PVOH100 PVOH875.910.1090.029066666733.184535701934.1432.89796.4288568460.6534731957100PVOH
10PAA/0CNXL0CNXL/10PAA760.77540.0610.016266666721.381693817522.01620.97513.16065161940.526933286810%cncc/90pvoh
0PAA/10CNXL10CNXL/0PAA588.060.0280.007466666712.697117074211.89211.113304.73080978130.792094418615%cncc/85pvoh
10PAA/10CNXL10CNXL/10PAA799.97620.02940.007849.80029155879.5919.901235.20699740820.158137675620%cncc/80pvoh
10PAA/20CNXL20CNXL/10PAA789.570.0350.009333333311.820780087111.28611.9912283.69872208920.3679537399
20PAA/0CNXL0CNXL/20PAA719.0220.0490.013066666718.172832912918.37219.604436.14798990850.7752129557
0PAA/20CNXL20CNXL/0PAA864.13910.0490.013066666715.121022375514.94315.619362.90453701260.350392561
20PAA/10CNXL10CNXL/20PAA769.860.030.00810.39149975329.89210.882249.39599407680.4950068174
20PAA/20CNXL20CNXL/20PAA842.6680.0410.010933333312.974663014811.56112.114311.39191235460.7123895171
15CNXL/0PAA835.910.040.010666666712.760544396712.2112.09306.25306552140.3575679238
15CNXL/10PAA840.10.0320.008533333310.1575209310.219.93243.78050232120.1488398616
gm/mt^2*hrstddev
100PVOH84033.1834.1432.890.6542425646
10%C.CNXL/0%PAA84012.1112.0111.590.2759226945
15%C.CNXL/0%PAA84011.7811.9411.620.16
20%C.CNXL/0%PAA84014.2314.9814.050.4932544982
10%C.CNXL/10%PAA8409.359.599.820.2350177298
15%C.CNXL/10%PAA8409.139.319.610.2424871131
20%C.CNXL/10%PAA84010.2310.3110.590.1890326251
100PVOH10%CNXL/0%PAA15%CNXL/0%PAA20%CNXL/0%PAA10%CNXL/10%PAA15%CNXL/10%PAA20%CNXL/10%PAA
C.CNXL33.1812.1111.7814.239.359.1310.23
0.650.790.3570.350.1580.1480.367
CNXL33.1812.6912.7615.129.810.1511.82
0.650.270.160.490.2350.2420.189
0,20268.666250.0930.00350943413.0624295469
0,10268.666250.1380.005207547219.3829599729
10,20268.666250.05730.00216226428.0481420757
20,0268.666250.08820.003328301912.3882396348
20,20268.666250.08080.003049056611.3488635203
10,0268.666250.08950.003377358512.570832736
Sheet1
0.650.650.650.65
0.270.270.790.79
0.160.160.3570.357
0.490.490.350.35
0.2350.2350.1580.158
0.2420.2420.1480.148
0.1890.1890.3670.367
C.CNXL
CNXL
Composition
Flux
Sheet2
116.960.5200.60.0250.025
116.96116.460.8530.50.6688524590.0278688525
116.96115.610.58210.66285714290.0276190476
116.96115.031.27
116.96113.76113.76
Sheet3
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Mechanical tensile testing
27 micron thick films were cut into a dogbone shape
Strain rate: 1 mm/min
Span: 20 mm Stress, MPa
Chart30
0.3317734
1.1124172
3.1616068
5.503538
7.3380506
8.0015978
7.8649852
7.4551474
7.435631
7.5332118
7.5136954
7.7088566
7.7674044
7.5136954
7.8259532
7.8845014
7.825953
8.0406302
8.2943392
8.2162748
8.3528874
8.6261128
8.7041772
8.5675646
8.9188542
9.094499
9.0944994
9.270144
9.309176
9.484821
9.504337
9.484821
9.543369
9.8556266
10.0898194
10.0703036
9.9922394
10.245948
10.5777224
10.753367
10.8899794
10.8899796
11.2022368
11.1241722
11.5144948
11.3459464545
11.3725593636
11.425785
11.5233653636
11.2927209091
11.4523979091
11.2838496364
11.1064307273
11.0532049091
10.7338505455
10.4144961818
10.3257871818
10.3790127273
10.2282068182
10.0774003636
9.917723
9.8378844545
9.5894980909
9.5628854545
9.4919177273
9.3854660909
9.1370797273
9.0661120909
8.9241767273
8.8265962727
8.6314354545
8.6048224545
8.6225643636
8.2233715455
8.3919196364
7.9040173636
7.620147
7.2298251818
7.0878897273
6.8040192727
6.71531
6.4580525455
6.208557
Strain, mm/mm
Stress vs Strain Curve
sintech data1names
AAAnumberNCCPAA
11520
c21520
c31510
c41520
c51010
c61020
c7520
c8020
c9010
10020
11520
AAA#11
11520
2010
3510
41010
51510
62010
700
850
9100
10150
11100
12200
sintech data1format
EXTENSION (mm)"LOAD (N)
-0.0188240.390266
-0.0188240.682966
-0.0162840
-0.0086640.487833
-0.0035840.682966
0.0065761.073232
0.0116561.463498
0.0218161.658631
0.0268962.048897
0.0370561.951331
0.0446762.439164
0.0522963.512396
0.0624564.292928
0.0700764.097795
0.0802365.561293
0.0878565.658859
0.0954766.049126
0.1005566.829658
0.1107166.536958
0.1157967.122358
0.1259567.219924
0.1310368.098023
0.1411967.90289
0.1488168.585856
0.1589768.390723
0.1665969.171255
0.1767569.268822
0.1843769.756655
0.1919969.268822
0.2021569.659088
0.2097769.561521
0.2173969.659088
0.2224769.659088
0.2300969.854221
0.24025610.14692
0.24787610.049354
0.2529569.756655
0.26311610.14692
0.2707369.756655
0.2808969.659088
0.28851610.244487
0.29613610.244487
0.30375610.14692
0.3139169.659088
0.3215369.756655
0.3291569.756655
0.33931610.244487
0.34693610.14692
0.35709610.537187
0.3647169.659088
0.37233610.049354
0.3774169.659088
0.3875769.756655
0.3951969.756655
0.40535610.14692
0.4129769.659088
0.4231369.951788
0.43075610.537187
0.4383769.463955
0.44853610.342054
0.45361610.14692
0.4637769.854221
0.47139610.342054
0.48155610.14692
0.4891769.854221
0.49933610.537187
0.50441610.049354
0.5145769.854221
0.5221969.756655
0.52981610.14692
0.53743610.14692
0.54759610.14692
0.55521610.537187
0.56283610.439621
0.57045610.439621
0.58061610.439621
0.58823610.439621
0.59839610.342054
0.6060169.854221
0.61363610.244487
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0.63903610.634753
0.64665610.634753
0.6542769.951788
0.66189610.14692
0.67205610.634753
0.6771369.951788
0.68729610.049354
0.69491610.049354
0.70507610.342054
0.71269610.829886
0.72031610.537187
0.73047610.634753
0.73809610.439621
0.7457169.951788
0.75333610.342054
0.76095610.049354
0.76857610.73232
0.77873610.927454
0.78635610.537187
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0.8015969.951788
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0.81937610.537187
0.82699610.342054
0.83715610.537187
0.84477610.439621
0.85493610.927454
0.86255611.02502
0.87017610.244487
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0.88541610.439621
0.89303610.927454
0.90319610.537187
0.91081610.244487
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0.94383610.927454
0.95399610.927454
0.96161610.829886
0.96923610.73232
0.97685610.634753
0.98955611.02502
0.99971610.927454
1.00987610.829886
1.01749610.537187
1.02765611.220153
1.03273610.244487
1.04035610.634753
1.04797610.829886
1.05559610.439621
1.06575610.829886
1.07337611.220153
1.08099610.927454
1.09115611.02502
1.09877610.634753
1.10893610.829886
1.11655611.122586
1.12417610.927454
1.13433610.537187
1.14195610.829886
1.14957611.317719
1.15719610.73232
1.16735611.415286
1.17497610.634753
1.18259611.220153
1.19275610.634753
1.20037610.73232
1.20799610.927454
1.21561610.537187
1.22323610.829886
1.23339610.537187
1.24101610.634753
1.25117610.927454
1.25879610.829886
1.26641610.73232
1.2765767.61019
1.2841968.585856
1.2943569.463955
1.30197610.14692
1.31213610.244487
1.31975610.439621
1.32737610.342054
1.33753610.73232
1.34515610.244487
1.35531610.927454
1.36293610.927454
1.37055610.049354
1.37817610.927454
1.38579610.049354
1.39595610.14692
1.40357610.73232
1.41119610.634753
1.41627610.14692
1.42897610.537187
1.43405610.439621
1.44421610.049354
1.45183610.049354
1.4619969.659088
1.46961610.342054
1.47977610.14692
1.48739610.342054
1.49501610.634753
1.50771610.537187
1.51279610.244487
1.52295610.244487
1.53057610.927454
1.53819610.439621
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1.55343610.634753
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1.56867610.342054
1.57629610.829886
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1.59407610.829886
1.60169610.244487
1.60931610.537187
1.61693610.439621
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1.66519610.342054
1.67535610.244487
1.68297610.049354
1.69059610.634753
1.70075610.049354
1.7109169.951788
1.71853610.342054
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1.78457610.14692
1.7921969.854221
1.79981610.342054
1.8074369.561521
1.81759610.342054
1.8252169.659088
1.8353769.756655
1.8404569.854221
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1.88617610.244487
1.8937969.659088
1.9039569.854221
1.91157610.342054
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1.9547569.366389
1.9623769.756655
1.9725369.561521
1.9801569.659088
1.9903169.561521
1.9979369.561521
2.0055569.659088
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2.0207969.951788
2.0309569.366389
2.03603610.049354
2.0512769.561521
2.0588969.951788
2.0639769.854221
2.07159610.14692
2.0817569.659088
2.0893769.561521
2.09953610.049354
2.1071569.756655
2.1173169.756655
2.12493610.049354
2.13255610.049354
2.1401769.366389
2.1477969.366389
2.1579569.366389
2.1655769.659088
2.1731969.951788
2.1808169.756655
2.1884369.268822
2.1960569.951788
2.2062169.463955
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2.2392369.366389
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2.2722569.659088
2.2798769.659088
2.2874969.463955
2.2925769.756655
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2.3103569.561521
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2.3611569.366389
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3.6336969.951788
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3.6565569.073689
3.6667169.171255
3.6743369.268822
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3.6997369.073689
3.7073569.561521
3.7175169.463955
3.7251368.878556
3.7327569.463955
3.7403768.878556
3.7505368.683423
3.7581569.171255
3.7657768.976122
3.7759368.683423
3.7835569.366389
3.7911768.390723
3.7987968.878556
3.8064168.585856
3.8140368.976122
3.8241968.000457
3.8318168.488289
3.8419768.488289
3.8470568.390723
3.8572168.390723
3.8648368.488289
3.8749968.098023
3.8826168.000457
3.8927768.488289
3.9003968.000457
3.9080168.19559
3.9181767.61019
3.9257967.512624
3.9334167.219924
3.9410367.512624
3.9486567.805324
3.9562768.000457
3.9664367.707757
3.9715167.61019
3.9842167.219924
3.9892967.512624
3.9994567.707757
4.0070767.512624
4.0146977.61019
4.0248567.61019
4.0324767.61019
4.0400967.122358
4.0502567.122358
4.0578777.317491
4.0680367.317491
4.0756567.317491
4.0832767.61019
4.0908977.317491
4.0959767.61019
4.1086767.122358
4.1239167.317491
4.1315367.024791
4.1391567.024791
4.1493166.927225
4.1569367.415058
4.1670966.634525
4.1747166.634525
4.1823367.024791
4.1899567.219924
4.2001167.024791
4.2051967.122358
4.2153566.927225
4.2229766.536958
4.2305966.146692
4.2407566.439392
4.2483766.244259
4.2585366.634525
4.2661566.146692
4.2737766.536958
4.2839366.536958
4.2915566.341826
4.3017165.951559
4.3093365.853993
4.3194966.049126
4.3271166.049126
4.3347366.341826
4.3448965.853993
4.3499765.951559
4.3601366.146692
4.3652165.853993
4.3753766.146692
4.3829965.561293
4.3906166.341826
4.4007765.951559
4.4083965.951559
4.4185565.561293
4.4261766.244259
4.4337965.658859
4.4439565.853993
4.4490375.658859
4.4591965.36616
4.4693565.463727
4.4769766.146692
4.4845965.756426
4.4922175.658859
4.4998365.463727
4.5074565.463727
4.5150766.146692
4.5252375.951559
4.5328565.36616
4.5379365.853993
4.5480965.853993
4.5557165.756426
4.5633365.756426
4.5734965.658859
4.5811165.756426
4.5887365.268593
4.5988965.658859
4.6065165.658859
4.6141365.171027
4.6242965.853993
4.6293765.561293
4.6395364.878327
4.6496965.07346
4.6547765.463727
4.6623965.36616
4.6700164.780761
4.6776365.36616
4.6852565.07346
4.6928765.07346
4.7055764.975894
4.7081164.975894
4.7182765.463727
4.7258964.780761
4.7335164.878327
4.7436764.780761
4.7512965.07346
4.7589164.780761
4.7665365.07346
4.7741565.171027
4.7817765.171027
4.7919364.585628
4.7970164.878327
4.8097164.878327
4.8147964.683194
4.8249564.390495
4.8325764.195362
4.8427364.000228
4.8503574.000228
4.8579764.097795
4.8681364.000228
4.8732164.488061
4.8833774.000228
4.8909963.902662
4.8986163.902662
4.9087764.390495
4.9163964.292928
4.9214763.512396
4.9316364.390495
4.9392564.000228
4.9494164.195362
4.9570364.488061
4.9646564.585628
4.9748164.292928
4.9824364.390495
4.9925964.000228
5.0002164.390495
5.0078364.585628
5.0154563.902662
5.0256164.097795
5.0332364.488061
5.0433963.902662
5.0510164.390495
5.0586364.390495
5.0662564.292928
5.0764164.390495
5.0814963.902662
5.0941963.707529
5.0992764.292928
5.1094364.097795
5.1170563.609962
5.1246763.707529
5.1322964.292928
5.1424564.292928
5.1500763.902662
5.1602363.609962
5.1678563.902662
5.1754764.000228
5.1856364.195362
5.1907164.000228
5.2008763.707529
5.2059563.512396
5.2161163.512396
5.2237363.902662
5.2338964.292928
5.2415173.122129
5.2491364.000228
5.2592963.609962
5.2669163.707529
5.2745373.609962
5.2821563.414829
5.2923163.707529
5.2999363.512396
5.3075563.707529
5.3151763.707529
5.3253363.219696
5.3329563.707529
5.3405763.317262
5.3507363.902662
5.3583564.000228
5.3659763.805095
5.3735963.512396
5.3812163.512396
5.3913763.512396
5.3989963.902662
5.4066163.609962
5.4142363.219696
5.4243963.122129
5.4320163.317262
5.4421763.512396
5.4497963.122129
5.4574163.024563
5.4675762.926996
5.4726563.219696
5.4853563.414829
5.4904363.707529
5.5005963.414829
5.5082162.731863
5.5158362.926996
5.5234562.926996
5.5336162.82943
5.5412362.731863
5.5513963.122129
5.5564772.53673
5.5691763.024563
5.5742562.926996
5.5844162.731863
5.5920363.122129
5.5996572.82943
5.6098163.122129
5.6174362.82943
5.6275962.731863
5.6352162.926996
5.6428362.82943
5.6504563.122129
5.6580762.53673
5.6656962.731863
5.6758572.24403
5.6834762.341597
5.6936361.951331
5.6987161.853764
5.7088772.146464
5.7164962.439164
5.7241162.341597
5.7342762.146464
5.7418962.048897
5.7495161.756198
5.7596762.439164
5.7672961.658631
5.7749161.951331
5.7825361.951331
5.7926961.951331
5.8003161.268365
5.8053961.365932
5.8155561.951331
5.8231761.073232
5.8333361.365932
5.8409561.561065
5.8511161.756198
5.8587361.561065
5.8663561.268365
5.8739761.268365
5.8841361.463498
5.8917560.682966
5.9019160.780532
5.9095361.073232
5.9171560.975665
5.9273160.487833
5.9323961.365932
5.9425560.878099
5.9476370.975665
5.9577961.365932
5.9679560.975665
5.9755760.878099
5.9831960.975665
5.9933560.975665
6.0009761.073232
6.0085960.780532
6.0162160.780532
6.0263760.487833
6.0339970.780532
6.0441560.878099
6.0517760.682966
6.0593960.878099
6.0695560.487833
6.0771760.682966
6.0873360.585399
6.0949560.585399
6.1051160.487833
6.1127360.390266
6.1228960.390266
6.1330560.2927
6.1381360.682966
6.1482960.682966
6.1559160.682966
6.1609960.487833
6.1711560.682966
6.1787760.487833
6.1889360.585399
6.1965560.097567
6.2067160.682966
6.2143360.195133
6.2219560.878099
6.2295770.390266
6.2371960.390266
6.2473560.487833
6.2549760.780532
6.2651360.682966
6.2651360.585399
Test Method"CM
Sample I. D."A
Specimen Numbe
EXTENSION (mm)"LOAD (N)
-0.0188240.390266
-0.0188240.682966
-0.0162840
-0.0086640.487833
-0.0035840.682966
0.0065761.073232
0.0116561.463498
0.0218161.658631
0.0268962.048897
0.0370561.951331
0.0446762.439164
0.0522963.512396
0.0624564.292928
0.0700764.097795
0.0802365.561293
0.0878565.658859
0.0954766.049126
0.1005566.829658
0.1107166.536958
0.1157967.122358
0.1259567.219924
0.1310368.098023
0.1411967.90289
0.1488168.585856
0.1589768.390723
0.1665969.171255
0.1767569.268822
0.1843769.756655
0.1919969.268822
0.2021569.659088
0.2097769.561521
0.2173969.659088
0.2224769.659088
0.2300969.854221
0.24025610.14692
0.24787610.049354
0.2529569.756655
0.26311610.14692
0.2707369.756655
0.2808969.659088
0.28851610.244487
0.29613610.244487
0.30375610.14692
0.3139169.659088
0.3215369.756655
0.3291569.756655
0.33931610.244487
0.34693610.14692
0.35709610.537187
0.3647169.659088
0.37233610.049354
0.3774169.659088
0.3875769.756655
0.3951969.756655
0.40535610.14692
0.4129769.659088
0.4231369.951788
0.43075610.537187
0.4383769.463955
0.44853610.342054
0.45361610.14692
0.4637769.854221
0.47139610.342054
0.48155610.14692
0.4891769.854221
0.49933610.537187
0.50441610.049354
0.5145769.854221
0.5221969.756655
0.52981610.14692
0.53743610.14692
0.54759610.14692
0.55521610.537187
0.56283610.439621
0.57045610.439621
0.58061610.439621
0.58823610.439621
0.59839610.342054
0.6060169.854221
0.61363610.244487
0.62379610.14692
0.6288769.951788
0.63903610.634753
0.64665610.634753
0.6542769.951788
0.66189610.14692
0.67205610.634753
0.6771369.951788
0.68729610.049354
0.69491610.049354
0.70507610.342054
0.71269610.829886
0.72031610.537187
0.73047610.634753
0.73809610.439621
0.7457169.951788
0.75333610.342054
0.76095610.049354
0.76857610.73232
0.77873610.927454
0.78635610.537187
0.79397610.244487
0.8015969.951788
0.81175610.244487
0.81937610.537187
0.82699610.342054
0.83715610.537187
0.84477610.439621
0.85493610.927454
0.86255611.02502
0.87017610.244487
0.87779610.634753
0.88541610.439621
0.89303610.927454
0.90319610.537187
0.91081610.244487
0.92097610.439621
0.92859610.439621
0.93621610.14692
0.94383610.927454
0.95399610.927454
0.96161610.829886
0.96923610.73232
0.97685610.634753
0.98955611.02502
0.99971610.927454
1.00987610.829886
1.01749610.537187
1.02765611.220153
1.03273610.244487
1.04035610.634753
1.04797610.829886
1.05559610.439621
1.06575610.829886
1.07337611.220153
1.08099610.927454
1.09115611.02502
1.09877610.634753
1.10893610.829886
1.11655611.122586
1.12417610.927454
1.13433610.537187
1.14195610.829886
1.14957611.317719
1.15719610.73232
1.16735611.415286
1.17497610.634753
1.18259611.220153
1.19275610.634753
1.20037610.73232
1.20799610.927454
1.21561610.537187
1.22323610.829886
1.23339610.537187
1.24101610.634753
1.25117610.927454
1.25879610.829886
1.26641610.73232
1.2765767.61019
1.2841968.585856
1.2943569.463955
1.30197610.14692
1.31213610.244487
1.31975610.439621
1.32737610.342054
1.33753610.73232
1.34515610.244487
1.35531610.927454
1.36293610.927454
1.37055610.049354
1.37817610.927454
1.38579610.049354
1.39595610.14692
1.40357610.73232
1.41119610.634753
1.41627610.14692
1.42897610.537187
1.43405610.439621
1.44421610.049354
1.45183610.049354
1.4619969.659088
1.46961610.342054
1.47977610.14692
1.48739610.342054
1.49501610.634753
1.50771610.537187
1.51279610.244487
1.52295610.244487
1.53057610.927454
1.53819610.439621
1.54581610.439621
1.55343610.634753
1.56105610.439621
1.56867610.342054
1.57629610.829886
1.58645610.342054
1.59407610.829886
1.60169610.244487
1.60931610.537187
1.61693610.439621
1.62709610.14692
1.63217610.14692
1.64233610.14692
1.64995610.537187
1.65757610.14692
1.66519610.342054
1.67535610.244487
1.68297610.049354
1.69059610.634753
1.70075610.049354
1.7109169.951788
1.71853610.342054
1.72615610.537187
1.7337769.951788
1.74393610.537187
1.75155610.14692
1.75917610.439621
1.76933610.439621
1.7744169.561521
1.78457610.14692
1.7921969.854221
1.79981610.342054
1.8074369.561521
1.81759610.342054
1.8252169.659088
1.8353769.756655
1.8404569.854221
1.85061610.244487
1.85823610.244487
1.8709369.659088
1.87855610.342054
1.88617610.244487
1.8937969.659088
1.9039569.854221
1.91157610.342054
1.9217369.756655
1.92935610.244487
1.9395169.854221
1.9471369.854221
1.9547569.366389
1.9623769.756655
1.9725369.561521
1.9801569.659088
1.9903169.561521
1.9979369.561521
2.0055569.659088
2.0131769.561521
2.0207969.951788
2.0309569.366389
2.03603610.049354
2.0512769.561521
2.0588969.951788
2.0639769.854221
2.07159610.14692
2.0817569.659088
2.0893769.561521
2.09953610.049354
2.1071569.756655
2.1173169.756655
2.12493610.049354
2.13255610.049354
2.1401769.366389
2.1477969.366389
2.1579569.366389
2.1655769.659088
2.1731969.951788
2.1808169.756655
2.1884369.268822
2.1960569.951788
2.2062169.463955
2.2112969.366389
2.2214569.951788
2.2290769.756655
2.2392369.366389
2.2468569.756655
2.2570169.951788
2.2646369.659088
2.2722569.659088
2.2798769.659088
2.2874969.463955
2.2925769.756655
2.3027369.561521
2.3103569.561521
2.3179769.463955
2.3255969.268822
2.3357569.659088
2.3433769.854221
2.3509969.366389
2.3611569.366389
2.3687769.561521
2.3763969.268822
2.3865569.854221
2.3941769.463955
2.4043369.951788
2.4119569.463955
2.4195769.463955
2.4271969.561521
2.4348169.854221
2.4449769.073689
2.4525969.463955
2.4602169.268822
2.4703769.756655
2.4754569.463955
2.4830769.366389
2.4906969.366389
2.5008569.366389
2.5084769.854221
2.5160969.463955
2.5237169.951788
2.5338769.366389
2.5414969.951788
2.55165610.049354
2.5592769.756655
2.5668969.171255
2.5770569.659088
2.5821369.463955
2.5922969.951788
2.5999169.268822
2.6100769.854221
2.6151569.463955
2.6253169.463955
2.6329369.561521
2.6405569.756655
2.6481769.366389
2.6583369.366389
2.6659569.854221
2.6761169.854221
2.6837369.951788
2.6913569.366389
2.6989769.366389
2.7065969.659088
2.71421610.049354
2.72183610.14692
2.73199610.049354
2.73961610.439621
2.74723610.049354
2.75485610.342054
2.76501610.14692
2.77263610.342054
2.78025610.244487
2.7904169.854221
2.79803610.537187
2.8056569.756655
2.81327610.14692
2.8208969.951788
2.82851610.244487
2.83613610.439621
2.84375610.244487
2.85391610.342054
2.86153610.537187
2.87169610.14692
2.87931610.244487
2.8894769.951788
2.89709610.73232
2.90471610.049354
2.91487610.049354
2.92249610.829886
2.93011610.73232
2.94027610.73232
2.94789610.537187
2.95805610.342054
2.96567610.829886
2.97075610.342054
2.98091610.244487
2.98599610.537187
2.99615610.73232
3.00377610.927454
3.01393610.829886
3.02155610.634753
3.02917610.244487
3.03933610.634753
3.04695610.537187
3.05457610.537187
3.06473610.927454
3.07235610.342054
3.07997610.73232
3.09013610.634753
3.09775610.342054
3.10791610.927454
3.11299610.537187
3.12315611.122586
3.13077610.829886
3.14093610.342054
3.14855611.122586
3.15617610.634753
3.16379610.342054
3.17395610.927454
3.18157610.634753
3.19173610.829886
3.19681610.342054
3.20697610.73232
3.21459610.829886
3.22475610.73232
3.23237610.634753
3.23999610.927454
3.25015610.537187
3.25523610.537187
3.26539611.122586
3.27301610.73232
3.27809610.537187
3.28825610.73232
3.29587610.342054
3.30349610.829886
3.31365610.634753
3.32127610.342054
3.32889610.439621
3.33651610.14692
3.34667610.829886
3.35429610.537187
3.36191611.02502
3.37207610.244487
3.37969610.634753
3.38731610.829886
3.39493610.439621
3.40255610.439621
3.41271610.73232
3.42033610.73232
3.4279569.854221
3.43557610.439621
3.4431969.951788
3.45081610.73232
3.46097610.049354
3.46859610.342054
3.47875610.049354
3.48383610.73232
3.49653610.634753
3.50161610.439621
3.50923610.14692
3.51939610.049354
3.5244769.659088
3.53209610.342054
3.54225610.14692
3.54987610.244487
3.55749610.537187
3.56511610.634753
3.57527610.049354
3.5828969.756655
3.59051610.049354
3.6006769.756655
3.6082969.951788
3.61591610.049354
3.6235369.366389
3.6336969.951788
3.6413169.756655
3.6489369.756655
3.6565569.073689
3.6667169.171255
3.6743369.268822
3.6844969.659088
3.6895769.268822
3.6997369.073689
3.7073569.561521
3.7175169.463955
3.7251368.878556
3.7327569.463955
3.7403768.878556
3.7505368.683423
3.7581569.171255
3.7657768.976122
3.7759368.683423
3.7835569.366389
3.7911768.390723
3.7987968.878556
3.8064168.585856
3.8140368.976122
3.8241968.000457
3.8318168.488289
3.8419768.488289
3.8470568.390723
3.8572168.390723
3.8648368.488289
3.8749968.098023
3.8826168.000457
3.8927768.488289
3.9003968.000457
3.9080168.19559
3.9181767.61019
3.9257967.512624
3.9334167.219924
3.9410367.512624
3.9486567.805324
3.9562768.000457
3.9664367.707757
3.9715167.61019
3.9842167.219924
3.9892967.512624
3.9994567.707757
4.0070767.512624
4.0146977.61019
4.0248567.61019
4.0324767.61019
4.0400967.122358
4.0502567.122358
4.0578777.317491
4.0680367.317491
4.0756567.317491
4.0832767.61019
4.0908977.317491
4.0959767.61019
4.1086767.122358
4.1239167.317491
4.1315367.024791
4.1391567.024791
4.1493166.927225
4.1569367.415058
4.1670966.634525
4.1747166.634525
4.1823367.024791
4.1899567.219924
4.2001167.024791
4.2051967.122358
4.2153566.927225
4.2229766.536958
4.2305966.146692
4.2407566.439392
4.2483766.244259
4.2585366.634525
4.2661566.146692
4.2737766.536958
4.2839366.536958
4.2915566.341826
4.3017165.951559
4.3093365.853993
4.3194966.049126
4.3271166.049126
4.3347366.341826
4.3448965.853993
4.3499765.951559
4.3601366.146692
4.3652165.853993
4.3753766.146692
4.3829965.561293
4.3906166.341826
4.4007765.951559
4.4083965.951559
4.4185565.561293
4.4261766.244259
4.4337965.658859
4.4439565.853993
4.4490375.658859
4.4591965.36616
4.4693565.463727
4.4769766.146692
4.4845965.756426
4.4922175.658859
4.4998365.463727
4.5074565.463727
4.5150766.146692
4.5252375.951559
4.5328565.36616
4.5379365.853993
4.5480965.853993
4.5557165.756426
4.5633365.756426
4.5734965.658859
4.5811165.756426
4.5887365.268593
4.5988965.658859
4.6065165.658859
4.6141365.171027
4.6242965.853993
4.6293765.561293
4.6395364.878327
4.6496965.07346
4.6547765.463727
4.6623965.36616
4.6700164.780761
4.6776365.36616
4.6852565.07346
4.6928765.07346
4.7055764.975894
4.7081164.975894
4.7182765.463727
4.7258964.780761
4.7335164.878327
4.7436764.780761
4.7512965.07346
4.7589164.780761
4.7665365.07346
4.7741565.171027
4.7817765.171027
4.7919364.585628
4.7970164.878327
4.8097164.878327
4.8147964.683194
4.8249564.390495
4.8325764.195362
4.8427364.000228
4.8503574.000228
4.8579764.097795
4.8681364.000228
4.8732164.488061
4.8833774.000228
4.8909963.902662
4.8986163.902662
4.9087764.390495
4.9163964.292928
4.9214763.512396
4.9316364.390495
4.9392564.000228
4.9494164.195362
4.9570364.488061
4.9646564.585628
4.9748164.292928
4.9824364.390495
4.9925964.000228
5.0002164.390495
5.0078364.585628
5.0154563.902662
5.0256164.097795
5.0332364.488061
5.0433963.902662
5.0510164.390495
5.0586364.390495
5.0662564.292928
5.0764164.390495
5.0814963.902662
5.0941963.707529
5.0992764.292928
5.1094364.097795
5.1170563.609962
5.1246763.707529
5.1322964.292928
5.1424564.292928
5.1500763.902662
5.1602363.609962
5.1678563.902662
5.1754764.000228
5.1856364.195362
5.1907164.000228
5.2008763.707529
5.2059563.512396
5.2161163.512396
5.2237363.902662
5.2338964.292928
5.2415173.122129
5.2491364.000228
5.2592963.609962
5.2669163.707529
5.2745373.609962
5.2821563.414829
5.2923163.707529
5.2999363.512396
5.3075563.707529
5.3151763.707529
5.3253363.219696
5.3329563.707529
5.3405763.317262
5.3507363.902662
5.3583564.000228
5.3659763.805095
5.3735963.512396
5.3812163.512396
5.3913763.512396
5.3989963.902662
5.4066163.609962
5.4142363.219696
5.4243963.122129
5.4320163.317262
5.4421763.512396
5.4497963.122129
5.4574163.024563
5.4675762.926996
5.4726563.219696
5.4853563.414829
5.4904363.707529
5.5005963.414829
5.5082162.731863
5.5158362.926996
5.5234562.926996
5.5336162.82943
5.5412362.731863
5.5513963.122129
5.5564772.53673
5.5691763.024563
5.5742562.926996
5.5844162.731863
5.5920363.122129
5.5996572.82943
5.6098163.122129
5.6174362.82943
5.6275962.731863
5.6352162.926996
5.6428362.82943
5.6504563.122129
5.6580762.53673
5.6656962.731863
5.6758572.24403
5.6834762.341597
5.6936361.951331
5.6987161.853764
5.7088772.146464
5.7164962.439164
5.7241162.341597
5.7342762.146464
5.7418962.048897
5.7495161.756198
5.7596762.439164
5.7672961.658631
5.7749161.951331
5.7825361.951331
5.7926961.951331
5.8003161.268365
5.8053961.365932
5.8155561.951331
5.8231761.073232
5.8333361.365932
5.8409561.561065
5.8511161.756198
5.8587361.561065
5.8663561.268365
5.8739761.268365
5.8841361.463498
5.8917560.682966
5.9019160.780532
5.9095361.073232
5.9171560.975665
5.9273160.487833
5.9323961.365932
5.9425560.878099
5.9476370.975665
5.9577961.365932
5.9679560.975665
5.9755760.878099
5.9831960.975665
5.9933560.975665
6.0009761.073232
6.0085960.780532
6.0162160.780532
6.0263760.487833
6.0339970.780532
6.0441560.878099
6.0517760.682966
6.0593960.878099
6.0695560.487833
6.0771760.682966
6.0873360.585399
6.0949560.585399
6.1051160.487833
6.1127360.390266
6.1228960.390266
6.1330560.2927
6.1381360.682966
6.1482960.682966
6.1559160.682966
6.1609960.487833
6.1711560.682966
6.1787760.487833
6.1889360.585399
6.1965560.097567
6.2067160.682966
6.2143360.195133
6.2219560.878099
6.2295770.390266
6.2371960.390266
6.2473560.487833
6.2549760.780532
6.2651360.682966
6.2651360.585399
Test Method"CM
Sample I. D."A
Specimen Numbe
EXTENSION (mm)"LOAD (N)
-0.060338-0.1953
-0.0603380
-0.060338-0.585901
-0.060338-0.3906
-0.060338-0.488251
-0.060338-0.09765
-0.0552580.1953
-0.050178-0.09765
-0.045098-0.09765
-0.0425580
-0.037478-0.3906
-0.0323980
-0.0273180.29295
-0.0273180.1953
-0.0196980.488251
-0.0171580.1953
-0.0120780.878851
-0.0095380.683551
-0.0044580.683551
0.0031621.660052
0.0057021.562402
0.0107822.050652
0.0158621.953002
0.0184022.343603
0.0234823.320104
0.0285623.515404
0.0311024.198954
0.0361824.589555
0.0412624.394255
0.0463424.784855
0.0488825.273105
0.0539625.370756
0.0590425.956657
0.0641226.542557
0.0641226.151956
0.0717426.933157
0.0742827.421408
0.0793627.226107
0.0819027.128458
0.0869827.323758
0.0895227.909658
0.0946027.519058
0.0996827.909658
0.1022227.421408
0.1073027.909658
0.1098427.812008
0.1174628.300258
0.1174628.690859
0.1250828.495559
0.1276228.495559
0.1327028.495559
0.1352429.37441
0.1403229.66736
0.1454029.86266
0.1479429.66736
0.1530229.96031
0.15810210.253261
0.16318210.155611
0.1657229.96031
0.17080210.643861
0.17334210.057961
0.17842211.034462
0.18350211.034462
0.18604210.936812
0.18858210.839161
0.19620211.327412
0.20128211.522712
0.20382211.620362
0.20890211.620362
0.21398211.620362
0.21906212.010962
0.22160211.913313
0.22414211.522712
0.22922211.718013
0.23176212.010962
0.23938212.303913
0.24192211.815663
0.24700211.522712
0.25208211.425062
0.25462211.229761
0.25716211.522712
0.26224211.327412
0.26732211.034462
0.27240211.132112
0.27494210.546211
0.27748210.44856
0.28510210.839161
0.28764210.643861
0.29272210.253261
0.29272210.44856
0.30034210.350911
0.30288210.546211
0.3079629.86266
0.31050210.253261
0.3155829.96031
0.32066210.253261
0.32828210.546211
0.3308229.56971
0.3359029.56971
0.33844210.155611
0.34352210.155611
0.34606210.155611
0.3511429.37441
0.3562229.56971
0.3587629.47206
0.3638429.47206
0.3663829.76501
0.3714629.47206
0.3765429.86266
0.3816229.86266
0.3841629.86266
0.3892429.47206
0.3943229.37441
0.3968629.86266
0.3994029.37441
0.4070229.66736
0.4095629.27676
0.4146429.86266
0.4171829.081459
0.4222629.86266
0.4273429.96031
0.4324229.27676
0.4349629.96031
0.4375029.56971
0.4451229.86266
0.45020210.155611
0.4527429.76501
0.4552829.66736
0.4603629.86266
0.4629029.27676
0.4705229.47206
0.4705229.47206
0.4781429.66736
0.4806829.37441
0.4857629.27676
0.4883029.66736
0.4933829.76501
0.4984629.47206
0.5035429.081459
0.5060829.081459
0.5111629.17911
0.5162428.98381
0.5187829.37441
0.5238629.37441
0.5264029.47206
0.5314829.17911
0.5365629.56971
0.5416429.27676
0.5416429.17911
0.5492629.47206
0.5543428.593209
0.5594229.27676
0.5619629.27676
0.5670429.17911
0.5721228.886159
0.5746628.788509
0.5772028.788509
0.5822829.17911
0.5873628.886159
0.5924428.788509
0.5949829.081459
0.6026029.081459
0.6051428.788509
0.6102229.27676
0.6153028.98381
0.6203828.690859
0.6229228.98381
0.6280028.98381
0.6305428.886159
0.6356228.495559
0.6381628.788509
0.6432428.495559
0.6457828.788509
0.6508628.690859
0.6559428.98381
0.6610228.788509
0.6635628.788509
0.6686428.202609
0.6737228.495559
0.6788028.397909
0.6813428.104959
0.6864228.495559
0.6889628.202609
0.6940428.300258
0.6991228.202609
0.7016627.812008
0.7092828.007308
0.7118228.300258
0.7169028.788509
0.7194428.202609
0.7245227.812008
0.7296028.007308
0.7346828.593209
0.7372227.714358
0.7423028.104959
0.7448427.909658
0.7499228.007308
0.7524628.007308
0.7575428.690859
0.7626228.202609
0.7677028.007308
0.7702428.495559
0.7753228.495559
0.7804028.690859
0.7854828.202609
0.7880227.812008
0.7931028.397909
0.7981828.007308
0.8032628.397909
0.8058028.202609
0.8083428.593209
0.8134227.909658
0.8185028.397909
0.8235828.690859
0.8261228.202609
0.8312028.007308
0.8337428.593209
0.8388228.593209
0.8413628.593209
0.8489828.690859
0.8515228.397909
0.8566028.593209
0.8591428.593209
0.8642228.593209
0.8667628.495559
0.8718428.202609
0.8769228.886159
0.8769228.104959
0.8845428.690859
0.8870828.104959
0.8921628.300258
0.8947028.593209
0.9023228.495559
0.9048628.788509
0.9099428.104959
0.9124828.007308
0.9175628.593209
0.9226427.812008
0.9251828.788509
0.9302628.104959
0.9328028.300258
0.9378828.007308
0.9429628.300258
0.9480428.104959
0.9505827.812008
0.9556627.812008
0.9582028.300258
0.9632828.495559
0.9658227.909658
0.9734428.007308
0.9785228.397909
0.9810627.812008
0.9861427.812008
0.9912228.495559
0.9937627.616708
1.0013827.714358
1.0039227.909658
1.0090027.909658
1.0115427.909658
1.0166227.616708
1.0191628.104959
1.0267827.909658
1.0293227.714358
1.0344027.714358
1.0369427.519058
1.0420227.616708
1.0471027.909658
1.0521827.812008
1.0547227.812008
1.0598027.421408
1.0623427.714358
1.0699627.812008
1.0699627.421408
1.0775827.909658
1.0801227.616708
1.0877427.616708
1.0902827.128458
1.0928227.616708
1.0979027.616708
1.1004427.226107
1.1055227.519058
1.1106027.519058
1.1156827.421408
1.1182227.812008
1.1233027.323758
1.1258427.519058
1.1309227.909658
1.1360027.812008
1.1410827.519058
1.1436227.616708
1.1487027.519058
1.1512427.812008
1.1563227.421408
1.1588627.421408
1.1639427.323758
1.1690227.714358
1.1715627.714358
1.1766427.714358
1.1791827.421408
1.1842627.616708
1.1893427.519058
1.1944227.616708
1.1969627.030808
1.2020427.128458
1.2071227.226107
1.2122027.323758
1.2122027.616708
1.2172827.909658
1.2223627.812008
1.2249027.421408
1.2299827.323758
1.2325227.616708
1.2376027.421408
1.2426827.421408
1.2477627.226107
1.2477626.933157
1.2553827.128458
1.2604627.128458
1.2630027.519058
1.2655427.030808
1.2731627.226107
1.2757027.519058
1.2807827.128458
1.2833227.812008
1.2884027.226107
1.2934827.421408
1.2985627.714358
1.3011027.909658
1.3036427.128458
1.3112627.421408
1.3163428.007308
1.3188827.714358
1.3214227.421408
1.3265027.323758
1.3315827.714358
1.3366627.519058
1.3392027.812008
1.3442828.104959
1.3468228.104959
1.3519027.909658
1.3544427.519058
1.3595227.616708
1.3646028.007308
1.3696827.909658
1.3722227.909658
1.3773028.104959
1.3798427.909658
1.3849228.104959
1.3874628.007308
1.3925428.007308
1.3976228.495559
1.4027028.007308
1.4052428.495559
1.4077828.495559
1.4154028.300258
1.4204828.300258
1.4230227.909658
1.4255627.909658
1.4331828.495559
1.4357227.812008
1.4408028.007308
1.4433428.104959
1.4484227.812008
1.4535027.714358
1.4585828.007308
1.4611228.300258
1.4662028.397909
1.4687428.104959
1.4763628.690859
1.4789028.300258
1.4839828.397909
1.4865228.397909
1.4916028.495559
1.4941428.593209
1.4992228.690859
1.5043028.397909
1.5068428.397909
1.5119228.104959
1.5144628.495559
1.5195427.909658
1.5246228.007308
1.5297028.397909
1.5297028.202609
1.5373228.593209
1.5398628.007308
1.5474828.397909
1.5474828.300258
1.5525628.300258
1.5551028.202609
1.5601828.397909
1.5652628.593209
1.5678027.909658
1.5728828.397909
1.5754228.104959
1.5805028.397909
1.5830428.104959
1.5881228.690859
1.5932027.909658
1.5982828.495559
1.6008228.593209
1.6059027.812008
1.6084428.397909
1.6135228.007308
1.6186028.593209
1.6211428.202609
1.6262228.202609
1.6287627.909658
1.6338428.300258
1.6363828.007308
1.6440028.397909
1.6465428.397909
1.6516227.909658
1.6541627.616708
1.6592428.007308
1.6643228.397909
1.6694028.202609
1.6719428.397909
1.6744827.714358
1.6795628.300258
1.6846428.007308
1.6897228.202609
1.6922627.909658
1.6973428.202609
1.6998828.007308
1.7075027.812008
1.7075028.300258
1.7151228.397909
1.7176628.104959
1.7252828.593209
1.7278228.007308
1.7329028.300258
1.7354428.397909
1.7405227.714358
1.7430628.397909
1.7481428.300258
1.7506827.909658
1.7557628.495559
1.7583028.007308
1.7633827.714358
1.7684628.397909
1.7735428.300258
1.7786228.202609
1.7786228.104959
1.7862427.714358
1.7887828.202609
1.7938627.812008
1.7964028.007308
1.8014828.202609
1.8040228.397909
1.8116427.616708
1.8141827.519058
1.8192627.519058
1.8218027.616708
1.8294228.397909
1.8319627.323758
1.8370427.714358
1.8395827.812008
1.8421228.104959
1.8472028.007308
1.8497428.007308
1.8573627.812008
1.8599027.909658
1.8649827.714358
1.8675227.421408
1.8751427.323758
1.8776828.104959
1.8827627.714358
1.8853027.812008
1.8903827.421408
1.8954627.714358
1.9005428.202609
1.9005428.007308
1.9056227.714358
1.9107027.519058
1.9157828.202609
1.9183228.007308
1.9234027.714358
1.9284828.007308
1.9310228.007308
1.9361027.421408
1.9386427.128458
1.9437227.226107
1.9488027.812008
1.9538827.030808
1.9538827.421408
1.9615027.323758
1.9640427.714358
1.9691227.812008
1.9716627.812008
1.9767427.323758
1.9818227.128458
1.9843624.980155
1.9894425.273105
1.9919825.566056
1.9970625.663706
2.0021425.859006
2.0072226.347257
2.0072226.054306
2.0148427.128458
2.0173826.640207
2.0250026.933157
2.0300826.737857
2.0351626.542557
2.0377026.444907
2.0427827.323758
2.0453227.226107
2.0504026.835507
2.0554827.421408
2.0605626.542557
2.0605626.542557
2.0681827.030808
2.0707224.394255
2.0758024.589555
2.0783425.370756
2.0834225.468406
2.0859625.663706
2.0935825.663706
2.0961226.249607
2.1012026.737857
2.1037426.151956
2.1088226.249607
2.1113626.542557
2.1164427.030808
2.1215226.542557
2.1240626.542557
2.1291427.030808
2.1316826.444907
2.1367626.737857
2.1393026.835507
2.1443826.640207
2.1494625.468406
2.1520023.906004
2.1570824.784855
2.1621624.980155
2.1672425.273105
2.1697825.859006
2.1748625.761356
2.1799425.566056
2.1824826.054306
2.1850225.566056
2.1901026.542557
2.1951825.956657
2.2002626.835507
2.2028026.054306
2.2078826.249607
2.2129626.347257
2.2180427.030808
2.2205824.687205
2.2256624.589555
2.2282024.589555
2.2332824.882505
2.2358225.566056
2.2434425.077805
2.2459825.468406
2.2510625.566056
2.2536025.956657
2.2586826.054306
2.2637626.054306
2.2688426.444907
2.2713826.249607
2.2739226.347257
2.2815426.444907
2.2840826.151956
2.2891626.249607
2.2917026.151956
2.2967826.444907
2.3018626.444907
2.3069426.640207
2.3069425.956657
2.3120226.737857
2.3171026.542557
2.3221826.542557
2.3247226.347257
2.3272626.249607
2.3323426.640207
2.3374226.640207
2.3425026.640207
2.3450426.249607
2.3501226.835507
2.3552026.151956
2.3602825.956657
2.3602826.835507
2.3679026.640207
2.3704426.444907
2.3755226.054306
2.3780626.347257
2.3831426.347257
2.3856826.347257
2.3907626.542557
2.3958426.347257
2.3983825.859006
2.4034626.151956
2.4085426.542557
2.4136226.835507
2.4136226.054306
2.4187026.151956
2.4237826.737857
2.4288626.444907
2.4314024.394255
2.4364824.491905
2.4390225.077805
2.4441025.370756
2.4491825.077805
2.4517225.663706
2.4568025.859006
2.4618825.663706
2.4669625.761356
2.4695025.859006
2.4745826.151956
2.4771226.151956
2.4822025.663706
2.4847426.054306
2.4898226.444907
2.4923626.151956
2.4974425.663706
2.4999825.956657
2.5050626.249607
2.5101425.468406
2.5152226.151956
2.5203025.663706
2.5228425.663706
2.5279225.566056
2.5330025.468406
2.5380826.151956
2.5380825.273105
2.5431625.370756
2.5482425.566056
2.5533225.761356
2.5558625.956657
2.5609425.956657
2.5634825.761356
2.5711025.468406
2.5736426.054306
2.5787226.151956
2.5812625.761356
2.5888825.859006
2.5914225.761356
2.5939625.468406
2.5990425.663706
2.6015825.566056
2.6066625.761356
2.6117425.566056
2.6168225.175456
2.6219025.370756
2.6244425.175456
2.6269825.273105
2.6346025.566056
2.6371425.468406
2.6422225.468406
2.6447625.566056
2.6498425.663706
2.6549225.273105
2.6600025.370756
2.6625425.663706
2.6676225.370756
2.6701624.980155
2.6752425.566056
2.6777824.882505
2.6828625.273105
2.6879425.468406
2.6904825.956657
2.6955625.175456
2.6981025.468406
2.7031825.370756
2.7082625.175456
2.7133424.980155
2.7133424.980155
2.7209625.566056
2.7235025.175456
2.7285825.663706
2.7311224.980155
2.7362025.566056
2.7412825.566056
2.7463625.077805
2.7489025.077805
2.7514424.980155
2.7590624.980155
2.7616024.980155
2.7666825.566056
2.7666825.273105
2.7743025.370756
2.7768424.980155
2.7819225.370756
2.7844624.589555
2.7870024.882505
2.7946225.566056
2.7997025.273105
2.8022424.980155
2.8047825.273105
2.8098624.980155
2.8149425.468406
2.8200225.370756
2.8200225.077805
2.8251024.003654
2.8301824.101304
2.8327224.784855
2.8378024.491905
2.8403424.784855
2.8454224.980155
2.8505024.589555
2.8530424.784855
2.8581224.589555
2.8632024.882505
2.8682824.882505
2.8708224.589555
2.8759024.980155
2.8784424.687205
2.8835225.077805
2.8911425.468406
2.8911424.687205
2.8987624.784855
2.9038425.077805
2.9089222.831853
2.9114623.906004
2.9165423.613054
2.9216224.394255
2.9267024.589555
2.9292423.906004
2.9343224.589555
2.9368623.906004
2.9419424.687205
2.9444824.491905
2.9521024.491905
2.9546424.784855
2.9597224.394255
2.9622624.394255
2.9673424.491905
2.9698824.394255
2.9749624.491905
2.9800424.687205
2.9825824.589555
2.9876624.980155
2.9927424.687205
2.9952824.101304
2.9978224.784855
3.0029024.491905
3.0079824.882505
3.0130624.394255
3.0156024.784855
3.0206824.882505
3.0232224.394255
3.0283024.296605
3.0333824.296605
3.0359224.394255
3.0410024.980155
3.0460824.394255
3.0486224.394255
3.0537024.882505
3.0587824.980155
3.0613224.394255
3.0664024.687205
3.0689424.296605
3.0765624.296605
3.0791024.882505
3.0841824.394255
3.0867224.491905
3.0918024.296605
3.0943424.491905
3.0994224.394255
3.1045024.589555
3.1095824.589555
3.1121224.101304
3.1146624.589555
3.1197424.784855
3.1248224.491905
3.1299024.980155
3.1324424.198954
3.1375224.491905
3.1400624.296605
3.1451424.296605
3.1502224.882505
3.1553024.784855
3.1553024.003654
3.1629224.687205
3.1654624.003654
3.1705424.687205
3.1730824.101304
3.1781624.101304
3.1832424.394255
3.1857824.198954
3.1908624.101304
3.1934023.906004
3.1959424.589555
3.2010224.589555
3.2061024.003654
3.2086424.003654
3.2137224.784855
3.2162623.906004
3.2238824.101304
3.2238824.003654
3.2289624.101304
3.2340423.808354
3.2391224.394255
3.2416624.198954
3.2467424.198954
3.2518224.687205
3.2543624.101304
3.2594423.906004
3.2619824.003654
3.2670624.589555
3.2721424.101304
3.2772224.198954
3.2797623.906004
3.2848424.491905
3.2873824.101304
3.2924624.687205
3.2950024.296605
3.3026224.003654
3.3051624.394255
3.3102424.101304
3.3127824.491905
3.3178624.589555
3.3229423.808354
3.3254824.003654
3.3305624.491905
3.3356424.491905
3.3381824.101304
3.3432623.906004
3.3483424.198954
3.3483424.198954
3.3559623.808354
3.3585023.710704
3.3635823.906004
3.3661224.198954
3.3737424.198954
3.3788224.003654
3.3813624.198954
3.3839024.296605
3.3915223.613054
3.3940623.515404
3.3991423.613054
3.4016822.831853
3.4067623.515404
3.4118423.027153
3.4169223.710704
3.4194623.906004
3.4220023.906004
3.4270823.710704
3.4321624.296605
3.4347024.198954
3.4372424.394255
3.4448624.296605
3.4474024.101304
3.4524824.198954
3.4550224.198954
3.4601023.613054
3.4626423.710704
3.4677223.613054
3.4728023.906004
3.4778823.124803
3.4804222.929503
3.4855023.027153
3.4880423.124803
3.4931223.417754
3.4982023.320104
3.5032824.101304
3.5058224.198954
3.5083624.003654
3.5159823.808354
3.5185224.296605
3.5236023.710704
3.5261424.101304
3.5312223.515404
3.5363023.710704
3.5413822.636553
3.5439223.027153
3.5490023.222453
3.5540823.027153
3.5591623.710704
3.5617023.613054
3.5667824.003654
3.5693223.906004
3.5744023.417754
3.5769423.906004
3.5820223.710704
3.5871023.515404
3.5896423.613054
3.5947224.296605
3.5998024.101304
3.6023423.808354
3.6074223.613054
3.6125023.515404
3.6150423.613054
3.6201223.515404
3.6226624.296605
3.6277423.515404
3.6302824.003654
3.6353623.320104
3.6404424.101304
3.6455223.906004
3.6480623.710704
3.6506023.613054
3.6556823.710704
3.6607623.417754
3.6658424.101304
3.6683823.710704
3.6734622.734203
3.6760023.320104
3.6836223.124803
3.6836223.417754
3.6912423.515404
3.6937823.710704
3.6963223.417754
3.7014024.003654
3.7064824.003654
3.7115623.710704
3.7141023.222453
3.7191823.710704
3.7217224.101304
3.7268023.808354
3.7318822.441253
3.7369623.124803
3.7395022.831853
3.7445823.124803
3.7471223.222453
3.7522023.710704
3.7547422.929503
3.7598223.613054
3.7649024.003654
3.7699823.710704
3.7725223.320104
3.7776023.222453
3.7826823.710704
3.7877623.613054
3.7903023.320104
3.7953822.929503
3.7979223.515404
3.8030023.613054
3.8055423.515404
3.8080823.222453
3.8131623.417754
3.8182423.710704
3.8233223.417754
3.8258623.027153
3.8309423.808354
3.8334823.417754
3.8385623.417754
3.8436423.710704
3.8487223.124803
3.8512623.027153
3.8563423.710704
3.8588823.027153
3.8614223.320104
3.8690423.222453
3.8715822.929503
3.8766623.417754
3.8766622.929503
3.8817422.636553
3.8868223.320104
3.8919022.831853
3.8944423.320104
3.8969822.343603
3.9046023.222453
3.9071422.148302
3.9122222.343603
3.9147622.245952
3.9198422.636553
3.9249222.148302
3.9274622.636553
Test Method"CM
Sample I. D."A
Specimen Numbe
EXTENSION (mm)"LOAD (N)
-0.110573-0.097567
-0.110573-0.2927
-0.1105730.390266
-0.1105730.195133
-0.1105730
-0.1105730.2927
-0.1105730
-0.1105730
-0.1105730.195133
-0.110573-0.097567
-0.1105730.390266
-0.1105730.585399
-0.110573-0.097567
-0.1105730.097567
-0.1105730.195133
-0.1105730.390266
-0.1080330
-0.1080330.390266
-0.108033-0.097567
-0.1080330.2927
-0.1080330.585399
-0.1080330
-0.108033-0.195133
-0.108033-0.195133
-0.1080330.2927
-0.1054930.585399
-0.1054930
-0.105493-0.2927
-0.105493-0.097567
-0.105493-0.195133
-0.1054930.487833
-0.102953-0.195133
-0.1029530.2927
-0.1029530
-0.1029530.2927
-0.102953-0.195133
-0.102953-0.195133
-0.1004130.195133
-0.1004130.390266
-0.1004130.390266
-0.1004130
-0.0978730.585399
-0.097873-0.195133
-0.097873-0.097567
-0.0978730.195133
-0.0953330.2927
-0.0953330.097567
-0.095333-0.2927
-0.0953330.2927
-0.095333-0.097567
-0.0953330.585399
-0.0927930.195133
-0.0927930.097567
-0.092793-0.097567
-0.0927930.390266
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-0.0927930.390266
-0.0927930.487833
-0.0927930.780532
-0.0902530
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-0.0851730
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-0.082633-0.2927
-0.0800930.585399
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-0.080093-0.195133
-0.077553-0.097567
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-0.0750130.097567
-0.0750130.097567
-0.0750130
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-0.075013-0.097567
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-0.0699330.2927
-0.0673930.390266
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-0.0648530.390266
-0.0648530.585399
-0.0623130.097567
-0.0623130.487833
-0.0623130.390266
-0.0623130.585399
-0.059773-0.097567
-0.0597730.390266
-0.059773-0.097567
-0.0597730.2927
-0.0572330.585399
-0.0572330.682966
-0.0572330.195133
-0.0572330
-0.0572330.780532
-0.0572330.390266
-0.0572330.195133
-0.0572330.390266
-0.057233-0.195133
-0.0546930.195133
-0.0546930.682966
-0.0546930.390266
-0.0521530
-0.0521530.195133
-0.0521530.195133
-0.049613-0.097567
-0.0496130.195133
-0.0496130.2927
-0.0496130.487833
-0.049613-0.097567
-0.0496130
-0.0470730.585399
-0.0470730.097567
-0.0470730.585399
-0.0470730.097567
-0.0445330
-0.0445330.097567
-0.0445330.487833
-0.041993-0.097567
-0.0419930.682966
-0.0419930.390266
-0.0419930.682966
-0.0419930.2927
-0.0394530.097567
-0.0394530.487833
-0.0394530.195133
-0.0394530.390266
-0.0394530
-0.0394530.195133
-0.0394530.2927
-0.0369130.487833
-0.0369130.585399
-0.0369130.195133
-0.0343730.2927
-0.0343730.195133
-0.0343730.682966
-0.0343730.585399
-0.0318330.487833
-0.0318330.487833
-0.0318330.195133
-0.0318330.487833
-0.0318330.097567
-0.0318330.097567
-0.0292930.585399
-0.0292930.682966
-0.0292930
-0.0292930.195133
-0.0292930.682966
-0.0267530.487833
-0.0267530.2927
-0.0267530.682966
-0.0267530.487833
-0.0242130.195133
-0.0242130.487833
-0.0242130.682966
-0.0242130.195133
-0.0242130.097567
-0.0216730.682966
-0.0216730.2927
-0.0216730.097567
-0.0216730.878099
-0.0216730.2927
-0.0216730.390266
-0.021673-0.097567
-0.0216730.585399
-0.0191330.487833
-0.0191330.585399
-0.0191330.585399
-0.0191330.2927
-0.0165930.195133
-0.0165930.487833
-0.0165930.195133
-0.0165930
-0.0140530.682966
-0.0140530.682966
-0.0140530.195133
-0.0140530.878099
-0.0140530.682966
-0.0140530.195133
-0.0115130.2927
-0.0115130.780532
-0.0115130.682966
-0.0115130.585399
-0.0089730.878099
-0.0089730.2927
-0.0089730.682966
-0.0089730.682966
-0.0064330.878099
-0.0064330.195133
-0.0064330.390266
-0.0064330.195133
-0.0064331.073232
-0.0064330.390266
-0.0064330.878099
-0.0038930.097567
-0.0038930.195133
-0.0038930.975665
-0.0038930.780532
-0.0038930.2927
-0.0038930.195133
-0.0038930.585399
-0.0038930.878099
-0.0013530.682966
-0.0013530.390266
0.0011870.780532
0.0011870.390266
0.0011870.2927
0.0037270.390266
0.0037271.170799
0.0037270.780532
0.0037270.390266
0.0037270.585399
0.0037270.585399
0.0037271.268365
0.0062671.170799
0.0062671.170799
0.0062671.170799
0.0062670.780532
0.0088070.682966
0.0088070.878099
0.0088071.073232
0.0113470.878099
0.0113471.268365
0.0113471.561065
0.0113471.170799
0.0113470.878099
0.0138871.170799
0.0138871.073232
0.0138871.463498
0.0138871.658631
0.0138871.170799
0.0138871.073232
0.0138871.170799
0.0138871.658631
0.0138870.878099
0.0164271.268365
0.0164271.268365
0.0164271.853764
0.0189671.951331
0.0189671.268365
0.0189671.365932
0.0215071.268365
0.0215071.951331
0.0215072.24403
0.0215072.439164
0.0215072.24403
0.0215071.658631
0.0215072.341597
0.0240472.24403
0.0240471.951331
0.0240471.853764
0.0240472.24403
0.0265872.82943
0.0265872.24403
0.0265872.53673
0.0265872.731863
0.0291272.82943
0.0291272.53673
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0.0291273.219696
0.0291273.219696
0.0316673.024563
0.0316672.439164
0.0316672.926996
0.0316672.731863
0.0316672.439164
0.0316672.82943
0.0316672.731863
0.0316673.219696
0.0316673.122129
0.0342072.926996
0.0342073.024563
0.0342073.122129
0.0367473.609962
0.0367473.219696
0.0367473.707529
0.0367474.292928
0.0392873.609962
0.0392874.097795
0.0392873.902662
0.0392873.512396
0.0392874.292928
0.0392874.488061
0.0418274.097795
0.0418274.292928
0.0418274.390495
0.0418274.683194
0.0443674.585628
0.0443674.488061
0.0443674.488061
0.0443674.585628
0.0469074.975894
0.0469075.171027
0.0469075.561293
0.0469074.878327
0.0469075.07346
0.0469075.658859
0.0494475.36616
0.0494475.658859
0.0494474.975894
0.0494475.463727
0.0494475.268593
0.0494475.268593
0.0494475.36616
0.0519875.951559
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0.0519875.561293
0.0545275.756426
0.0545276.049126
0.0545275.853993
0.0545276.536958
0.0570675.951559
0.0570676.146692
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0.0570675.853993
0.0570676.146692
0.0570676.634525
0.0570676.829658
0.0596076.244259
0.0596076.927225
0.0596076.341826
0.0621476.927225
0.0621476.927225
0.0621477.024791
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0.0646877.219924
0.0646877.024791
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0.0646877.317491
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0.0672276.927225
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0.0697677.122358
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0.0697677.317491
0.0723078.098023
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0.0723077.61019
0.0748478.488289
0.0748478.390723
0.0748478.098023
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0.0748478.293157
0.0748478.683423
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0.0773878.19559
0.0773877.90289
0.0773878.000457
0.0773878.683423
0.0799278.683423
0.0799278.293157
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0.0824678.780989
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0.0824678.976122
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0.0850079.073689
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0.0900879.756655
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0.0951679.659088
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0.09516710.14692
0.0977079.659088
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0.0977079.756655
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0.1002479.756655
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0.10024710.14692
0.10024710.634753
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0.10278710.049354
0.1027879.951788
0.10278710.244487
0.10278710.049354
0.10278710.049354
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0.10532710.14692
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0.10786710.73232
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0.10786710.73232
0.10786710.927454
0.11040710.634753
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0.11040710.829886
0.11040710.634753
0.11040711.220153
0.11294711.122586
0.11294710.927454
0.11294710.829886
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0.11294711.02502
0.11548711.317719
0.11548711.220153
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0.11548710.927454
0.11802710.829886
0.11802711.220153
0.11802711.903119
0.11802711.805552
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0.12056711.512852
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0.12056712.000685
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0.12564712.293384
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0.12818711.805552
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0.13072712.000685
0.13072712.195818
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0.13326712.586084
0.13326712.488518
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0.13580712.488518
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0.14850713.952016
0.14850713.659317
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0.15104713.561749
0.15104713.366617
0.15104713.756883
0.15104713.85445
0.15104714.342283
0.15358713.85445
0.15358714.244715
0.15358713.756883
0.15358714.147149
0.15358713.85445
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0.15358714.049582
0.15612713.756883
0.15612714.439849
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0.15866714.147149
0.15866714.634982
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0.15866714.244715
0.15866714.439849
0.16120714.049582
0.16120714.244715
0.16120714.732548
0.16120714.147149
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0.16374714.342283
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0.16374715.025248
0.16374714.342283
0.16628715.025248
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0.16628715.317948
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0.16882714.927681
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0.17136715.122815
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0.18152715.805781
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0.18914715.805781
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0.20184716.39118
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0.21200716.879012
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0.21962717.269279
0.21962717.561978
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0.22216717.561978
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0.22216717.854678
0.22216717.659545
0.22216717.757112
0.22470717.464411
0.22470717.757112
0.22470716.976578
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0.22470717.171712
0.22470717.561978
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0.22724717.366845
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0.23994718.244945
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0.23994719.22061
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0.24248718.927909
0.24248719.025477
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0.24502718.830343
0.24756719.22061
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0.25010719.513309
0.25010719.610876
0.25010718.537644
0.25010717.757112
0.25010716.781446
Test Method"CM
Sample I. D."A
Specimen Numbe
EXTENSION (mm)"LOAD (N)
-0.104523-0.292971
-0.1045230
-0.104523-0.195314
-0.104523-0.585942
-0.104523-0.292971
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0.0021570.585942
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0.0021570.195314
0.0021570
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